ICE 2020/1 Seized Materials Test Group

Home , Desomorphine, Methorphan, Misuse of Drugs Act 1971, Tropacocaine

INTERNATIONAL COLLABORATIVE EXERCISES (ICE)

Summary Report

ICE Round 2020/1 1

SEIZED MATERIALS

ICE 20

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Final summary report for ICE 2020/1 Seized Materials Test Group

Original language: English

The designations employed and the presentation of material in this publication do not imply the expression of any opinion whatsoever on the part of the Secretariat of the United Nations concerning the legal status of any country, territory, city or area, or of its authorities, or concerning the delimitation of its frontiers or boundaries.

This publication has not been formally edited.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Acknowledgements

The Laboratory and Scientific Section (LSS) of the UNODC, headed by Dr. Justice Tettey, wishes to express its appreciation and thanks to all laboratories for participating in the International Collaborative Exercises (ICE) round 2020/1.

The valuable comments and contribution from the following members of the International Panel of Forensic Experts are gratefully acknowledged:

Mr. Benoit Archambault, Health Canada, Canada Mr. Elvio Dias Botelho, Brazilian Federal Police, Brazil Prof. Heesun Chung, Sungkyunkwan University, Republic of Korea Prof. Niamh Nic Daéid, University of Dundee, Scotland, UK Mr. Scott Oulton, Drug Enforcement Administration, USA Ms. Catherine Quinn, Victoria Police, Australia Prof. Franco Tagliaro, University of Verona, Italy Dr. Angeline Tiong Whei Yap, Health Sciences Authority, Singapore

In addition, LSS would like to acknowledge the valuable contribution of the Chemical Metrology Laboratory of the Health Sciences Authority, Singapore, for the provision of specific software used for the quantitative statistical calculations in the ICE programme.

The ICE is coordinated by Ms. Yen Ling Wong, Scientific Affairs Officer, a staff member of LSS. The assistance and the contributions of the following LSS staff members are gratefully acknowledged.

Dr. Conor Crean, Scientific Affairs Officer Mr. Joao Rodrigues, Scientific Affairs Officer Ms. Romana Luger, Research Assistant Dr. Gerd Krapf, Laboratory Technician Mr. Michael Bell, Laboratory Technician Ms. Mikaela Edwards, Laboratory Team Assistant

For additional information or comments, please contact:

Ms. Yen Ling Wong ICE Coordinator Scientific Affairs Officer Laboratory and Scientific Section UNODC, Vienna International Centre Wagramer Strasse 5, P.O. Box 500 A-1400, Vienna, AUSTRIA Email: [email protected]

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Contents

1. Codes and Abbreviations ...... 4 2. Test samples information ...... 5 3. Introduction ...... 6 4. Comments from the International Panel of Forensic Experts ...... 7 5. New Psychoactive Substances (NPS) reported ...... 9 6. Summary of responses for Test Sample-1 ...... 11 7. Summary of responses for Test Sample-2 ...... 16 8. Summary of responses for Test Sample-3 ...... 21 9. Summary of responses for Test Sample-4 ...... 22 10. ANNEX 1: Participants’ results for Test Sample-1 ...... 26 11. ANNEX 2: Participants’ results for Test Sample-2 ...... 47 12. ANNEX 3: Participants’ results for Test Sample-3 ...... 68 13. ANNEX 4: Participants’ results for Test Sample-4 ...... 85

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

1. Codes and Abbreviations

(+) “positive” Indicates that the analyte is identified; for presumptive tests (e.g. colour reactions), indicates that a positive reaction was obtained.

(-) “negative” Indicates that the analyte is not identified.

(ANP) Analysis not performed.

Tech Code Name 140 Colorimetric reactions 141 Marquis test 142 Cobalt thiocyanate test 150 Thin layer chromatography (TLC) 160 High/ultra high performance liquid chromatography with ultraviolet-visible spectroscopy (HPLC/UPLC) 161 High/ultra high performance liquid chromatography with diode array detection (HPLC-DAD or UPLC-DAD)* 170 Gas chromatography with nitrogen-phosphorous detection (GC-NPD) 171 Gas chromatography with flame ionization detection (GC-FID) 172 Gas chromatography with electron capture detection (GC-ECD) 180 Gas chromatography with mass spectrometry (GC-MS) 190 Fourier transform infrared spectrometry (FTIR) 200 Spectrophotometry (visible, UV) 210 Others 211 Nuclear magnetic resonance spectroscopy (NMR) 220 Microcrystal test 230 Liquid chromatography with mass spectrometry (LC-MS) 231 Liquid chromatography with tandem mass spectrometry (LC-MS/MS) 250 Raman spectroscopy *similar to 160

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

2. Test samples information

The following four (4) test samples for the Seized Materials test group were prepared by the Laboratory and Scientific Section, UNODC:

Test Sample-1 (SM-1) SM-1 was prepared from a seizure containing 42.9% (w/w) Heroin base. The test sample also contained acetylcodeine, caffeine, methorphan*, 6-acetylmorphine and trace amounts of morphine. Note: *Stereochemical orientation of this substance was not determined.

Test Sample-2 (SM-2) SM-2 was prepared from a seizure containing 48.3% (w/w) Cocaine base. The test sample also contained dexamisole/levamisole/tetramisole* and traces of benzoylecgonine, trans-cinnamoylcocaine, methylecgonine, norcocaine and tropacocaine. Note: *Stereochemical orientation of this substance was not determined.

Test Sample-3 (SM-3) SM-3 was a blank test sample prepared from plant material and contained caffeine.

Test Sample-4 (SM-4) SM-4 was prepared from a seizure containing 19.6% (w/w) Metamfetamine base. The test sample also contained lactose.

All test samples were prepared by preliminary grounding by mortar and pestle followed by homogenisation using a centrifugal mill and a dry powder rotator. Aliquots (230 mg) of each test samples were weighed into glass vials.

For each test sample, sufficient homogeneity was assured and stability studies were carried out in accordance with methods outlined in ISO 13258:2015 “Statistical methods for use in proficiency testing by interlaboratory comparisons” and “The international harmonized protocol for the proficiency testing of analytical chemistry laboratories”1.

______1 Thompson, M., Ellison, S. L. and Wood, R., The International Harmonised Protocol for the Proficiency Testing of Analytical Chemistry Laboratories, Pure Appl. Chem., 78 (1), 145-196, 2006.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

3. Introduction

An important element of the UNODC International Quality Assurance Programme (IQAP) is the implementation of the International Collaborative Exercises (ICE). The exercises allow laboratories, from both developing and developed countries to continuously monitor their performance in drug testing on a truly global scale. This report provides information on analytical results of laboratories participating in the Seized Materials (SM) test group. In order to maintain confidentiality, the participating laboratories have been assigned random “Round Codes”, which change every round.

The analytical results returned by laboratories participating in ICE are evaluated by UNODC and a confidential report is provided to each laboratory on its own performance. The overall analytical results are reviewed by the UNODC’s International Panel of Forensic Experts which oversees the implementation of these exercises, and offers guidance and support in addressing relevant quality issues. The exercises provide an overview of the performance and capacity of participating laboratories and enable UNODC to tailor technical support in the laboratory sector for greatest impact.

The ICE programme is a UNODC mandated activity and is implemented through regular budget funds and through the UNODC Global Scientific and Forensic Programme – Support Project (GLOU54), which operationalizes the forensic aspects of the UNODC Thematic Programme on Research, Trend Analysis and Forensics". Figure 1 shows the growth of the programme in recent years for both the Seized Materials (SM) and the Biological Specimens (BS) test groups.

250 222 217 SM BS 204 204 204 195 200 184 185 179 179 173 159 151 150 129 132 131 116 102 106 100 97 101 94 95 92 96 93 100 86 90 87 No. of of laboratories No. 83 77 72 74 66 62 62 62 54 58 47 50 42 33 37 26 27

ICE round Note: Reduced participation rate in round 2020/1 resulted from the challenges arising from the COVID-19 pandemic.

Figure 1. Growth of the ICE programme (as of 23 December 2020)

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

4. Comments from the International Panel of Forensic Experts

4.1 Participation of Laboratories in ICE round 2020/1

In the 2020/1 round of the ICE programme, results were submitted within both the Seized Materials (SM) and Biological Specimens (BS) test groups by 215 laboratories in 59 countries. Within the SM test group, there were 179 participating laboratories from 51 countries and within the BS test group, results were submitted by 83 laboratories from 39 countries. The reduced participation rate of this round is mainly due to shipping restrictions to a number of countries experiencing on-going COVID-19 pandemic. On an exceptional basis, laboratories could request test samples for both rounds, i.e. 2020/1 and 2020/2 to be sent together. However, results submitted will not be included in this summary report.

4.2 Qualitative Analysis

Colour tests (50% of participants) were the most commonly used screening techniques for test samples in the SM test group, while GC-MS (94% of participants) was the most commonly used technique for identification/confirmation of the components in the test samples followed by FTIR (36% of participants). The results for the qualitative identification of the substances in the SM test group, the number of false positive/negative results and the analyses not performed are shown in the Table 1.

Table 1. Performance of participants in the 2020/1 round of ICE.

SM-1 SM-2 SM-3 SM-4 Test sample (Heroin) (Cocaine) (Caffeine) (Metamfetamine) Correct identification 99.4% 100.0% 82.7% 98.9% by participants Number of false 7 9 1 5 positives Number of false 1 0 23 2 negatives Number of analyses 0 0 8 0 not performed

Overall, 83% of participants were able to identify all 4 test samples correctly. This is mainly due to difficulties several participants had with SM-3 which resulted in 23 false negative results reported. With regards to false positive results, there were a total of 22 false positive results (7 for SM-1, 9 for SM-2, 1 for SM-3 and 5 for SM-4), which is a slight increase in number compared to the previous round. Laboratories reporting false positive or false negative results should investigate the reasons for this and corrective actions should be taken as soon as possible in order to continuously improve performance. A total of 8 participants did not perform analysis for SM-3 which contained caffeine. ICE participants should note that test samples can contain any of the substances in the ICE menu and screening and identification carried out should take this into account.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

4.3 Quantitative Analysis

The number of participants who carried out quantitative analysis, 115 (64%) for SM-1, 127 (71%) for SM-2 and 96 (54%) for SM-4 continues to be encouraging. A total of 133 (74%) participants in the SM test group performed quantitation and of these, 119 (89%) quantified more than one substance and 86 (65%) quantified all three test samples. It is understood that quantitative analysis of controlled substances is often governed by local legislation and the requirements of prosecution. With regards to the analytical techniques used by participants performing quantitation, 63% used GC-FID, 28% used UPLC/HPLC-DAD and 16% used mass spectrometric methods (i.e. GC-MS, GC-MS/MS, LC-MS, LC-MS/MS). z-Scores obtained by participants in quantification are shown in Table 2 below.

Table 2. Quantitative performance of participants in the 2020/1 round of ICE.

Test sample z-score SM-1 SM-2 SM-4 (42.9% Heroin) (48.3% Cocaine) (19.6% Metamfetamine) |z| ≤ 2.00, acceptable 83.5% (96) 85.8% (109) 82.3% (79) 2.00 < |z| < 3.00, questionable 6.1% (7) 6.3% (8) 5.2% (5)

|z| ≥ 3.00, unacceptable 10.4% (12) 7.9% (10) 12.5% (12)

According to the recommendations in ISO 13528:2015, an unacceptable z-score is considered to give an action signal and a questionable z-score is considered to give a warning signal. A single action signal or warning signal in two successive rounds shall be taken that an anomaly has occurred that requires investigation. Participants with z-scores outside acceptable limits should review their quantification procedures as soon as possible.

The following 8 laboratories obtained a single action signal or warning signal in the two successive rounds of 2019/2 and 2020/1 and shall take this as an anomaly, which requires further investigation: 3CAJ33, EQNEIU, FTFGF7, GIG3NC, JYYOJY, NT6XKR, PKIAAH and T6MTE2.

Of the 15 laboratories that obtained a single action or warning signal in ICE rounds 2019/1 and 2019/2 reported in the previous summary report, 5 performed quantitation in 2020/1 and 2 of these improved their performance in quantitation. The following 3 laboratories also obtained an action or warning signal in 2020/1: 3CAJ33, GIG3NC and JYYOJY.

Laboratories that need to perform quantitation routinely are encouraged to participate regularly in external proficiency testing or collaborative exercises such as the ICE programme. This will enable laboratories to assess the quality of their quantitative methods through the z-score values obtained. In addition to the use of z-scores as a measure of performance in quantitation, participants are encouraged to compare their results with the assigned values provided in individual quantification reports, to assess the accuracy of their quantitative performance. Laboratories reporting false positive or false negative results should investigate the root causes and corrective actions taken promptly in order to continuously improve performance. Participation in the ICE programme also helps in monitoring the effect of corrective actions.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

5. New Psychoactive Substances (NPS) reported

During the 2020/1 round of ICE, participating laboratories provided information on NPS that had been identified in their laboratories. In total there were 153 reports of 110 substances and the most commonly reported substances were synthetic cannabinoids (29%) followed by phenethylamines (20%) as shown in Figure 2.

5% 1% 19% 13% Aminoindanes Other substances Phencyclidine-type-substances Phenethylamines 11% Piperazines Plant-based substances Synthetic cannabinoids Synthetic cathinones 29% Tryptamines

20% 1% 1%

Figure 2. Distribution of classes of NPS reported by ICE laboratories during the 2020/1 round of ICE

In terms of the mode of action of the NPS reported by ICE participants, the predominant substances reported were synthetic cannabinoid receptor agonists (28%) followed by stimulants (26%), while 23% were hallucinogens as shown in Figure 3.

1% 11%

28% Dissociative Hallucinogen 23% Synthetic opioid Sedative hypnotic Stimulant Synthetic cannabinoid N/A

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

The substances most often reported by ICE participants were Ketamine, 5F-MDMB-PICA and MDMB- 4en-PINACA. While ketamine is currently not under international control, 5F-MDMB-PICA was placed in schedule II of the 1971 convention effective 3rd November 2020. MDMB-4en-PINACA was recommended by the WHO to be placed in schedule II of the 1971 convention and this decision will be voted upon at the 64th session of the Commission on Narcotic Drugs in 2021.

Effective date of Name Convention Schedule international control 2-(2-chlorophenyl)-2- Ketamine Currently not under international control (methylamino)cyclohexan-1-one methyl 2-(1-(5-fluoropentyl)-1H- 5F-MDMB-PICA indole-3-carboxamido)-3,3- 1971 II 3rd November 2020 dimethylbutanoate methyl 3,3-dimethyl-2-(1-(pent-4- MDMB-4en-PINACA en-1-yl)-1H-indazole-3- Recommended for scheduling in April 2021 carboxamido)butanoate

For further details on these substances and others reported to the UNODC Early Warning Advisory, ICE participants can log on to the UNODC ICE portal, www.unodc.org/lss, and select the icon for the Early Warning Advisory on New Psychoactive substances as shown below.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

6. Summary of responses for Test Sample-1

The summary of responses of all 179 participating laboratories for the identification of SM-1:

Correct identification of Test Sample-1:

Substance Name Number of laboratories Percentage Caffeine 153 85.5%

Heroin 178 99.4%

False positives for Test Sample-1 (technique(s) used):

Round Code Substance Reported Tech Code 43BPPC Desomorphine, thebacon 180, 190 9L9I9M Cocaine 180, 190 EQNEIU Nalaxone, naltrexone 180

GSHGOF Paracetamol 180 HOOOOO Desomorphine 180, 190 KZRYK5 Hydromorphone 180 WARWWC Epinephrine, nordazepam 180

False negatives for Test Sample-1 with respect to Heroin (technique(s) used):

Round Code Tech Code HOOOOO 180, 190

Analysis not performed for Test Sample-1 with respect to Heroin: All participating laboratories carried out analysis for Heroin

Frequency of use of screening, identification and quantification techniques:

Test Sample-1: Response Summary

No of Participants: 179 (Qualitative); 115 (Quantitative) Technique 140 141 142 150 160 161 170 171 180 190 210 211 230 231 250 Screening (No.) 58 63 49 10 0 0 1 5 68 16 5 2 0 0 4 (%) 32.4 35.2 27.4 5.6 0.0 0.0 0.6 2.8 38.0 8.9 2.8 1.1 0.0 0.0 2.2 Identification 12 4 4 26 4 14 1 29 169 65 5 6 3 5 5 (No.(%) 6.7 2.2 2.2 14.5 2.2 7.8 0.6 16.2 94.4 36.3 2.8 3.4 1.7 2.8 2.8 Quantification (No.) 0 0 0 0 3 19 1 75 8 0 1 3 1 3 0 (%) 0.0 0.0 0.0 0.0 2.6 16.5 0.9 65.2 7.0 0.0 0.9 2.6 0.9 2.6 0.0

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Score Report per Sample per Substance: Round: 2020/1 UNODC value: 42.9% Robust mean: 41.8% Max reported: 76.6% Robust SD: 3.08% Substance: SM-1; Heroin Min reported: 3.29% Robust CV%: 7.37% No of labs: 115 4.00 3.37 3.02 3.00 2.56 2.08 2.01 1.95 1.95 1.91 1.91 1.85

2.00 1.72 1.36 1.19 1.17 1.04 0.87 0.81 0.79

1.00 0.71 0.71 0.71 0.67 0.65 0.63 0.61 0.61 0.55 0.52 0.45 0.42 0.42 0.42 0.39 0.39 0.39 0.39 0.39 0.39 0.37 0.36 0.35 0.32 0.26 0.26 0.26 0.22 0.21 0.19 0.16 0.14 0.13 0.13 0.09 0.09 0.08 0.03 0.03 7.30 11.29 0.00 5.28 4.42 3.87 3.83 0.01 0.04 - - - - - 0.07 12.51 11.92 11.86 - 0.10 - - - - 0.13 - - 0.20 0.20 0.23 0.23 - - 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.26 ------0.32 0.33 0.36 - - 0.38 0.39 0.39 - 0.42 - 0.43 - - 0.47 - - 0.49 0.49 - 0.52 - - - 0.60 0.62 0.64 - -

-1.00 - 0.72 - 0.77 - 0.85 0.85 0.88 - - 0.91 0.91 - - - 1.20 1.24 - - 1.33 - 1.62

-2.00 - 1.81 - 2.21 2.21 - - 2.54 2.58 - -3.00 - 3.19 - -4.00 IKISEG RILD6I K2KJIK 9YIBLY CSFZJZ TFB6JZ SEJFEA SIF50H BYLJA9 BRJPLX EIECD7 YSEXJD J9A365 T8ZTTT IQLV57 XKKFPL VRAJLX RTTTXL 3CAJ33 RTRIO9 N9Y5J4 KTL2KK FTFGF7 JCPDEV 8X8488 KZRYK5 G4IK4G PVVVKJ YD88F8 JNKRGL F3HS08 2VY888 XS9KCX 9X9XK9 U7IBAC PKIAAH YRVPY5 BG2SLB VP4FPK 8TDKSP 3DB3YF A99LH9 L0SOSG 43BPPC O888FC GIG3NC EQNEIU 1D31A3 NT6XKR KUOOIY 3VAS7U FBOH8T 4CCTQB HFYHFD 8K8OSH 78PEHN JQGKRH GWFSGI V8EXVQ ATVQQJ TKVKOB PRYEOG T6MTE2 HOU5IO HLHPRH O77FQX BTUABB GKGVZX TVETMT O37CO6 EGNF7G ZECZ6W ZWYPLA WS6KSK 22M222 XVXMYY TFXAMC BVQYTQ GSHGOF YMBZHZ AR7S7W 4TZWAV R7RR6M PAMP84 DQQX66 DBHUHY 9PLW9Q FWRG58 YRARMC NRHUYD 9POVHQ XQOBO8 RWTRU8 P7XJWM WRGTRP CCORYM TWPVRD FAHHM9 OMOLC6 GNGGG8 PMCINM G5GNGG TCEWUO WM44EE BNQNNV CABMNN QQCQAQ MMNPPT OOCWTO AMOGGG RMBHBW MWSMPP VWWXWB WARWWC DMMMMG Z-scores can be interpreted by participants in line with ISO 13528:2015*, section 9.4.2 as follows: IzI ≤ 2.00 is considered to be acceptable 2.00 < IzI < 3.00 is considered to be questionable (or warning signal) IzI ≥ 3.00 is considered to be unacceptable (or action signal)

A single action signal or warning signal in two successive rounds shall be taken that an anomaly has occurred that requires investigation.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Score Report per Sample per Substance:

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Scores for Test Sample-1

Heroin Heroin Deviation Deviation Code Concentration from robust Code Concentration from robust z-score z-score (mass%) average (mass%) average (mass%) (mass%) XKKFPL 3.3 -38.5 -12.51 T6MTE2 41.0 -0.8 -0.26 WARWWC 5.1 -36.7 -11.92 9POVHQ 41.0 -0.8 -0.26 K2KJIK 5.3 -36.5 -11.86 9YIBLY 41.0 -0.8 -0.26 FBOH8T 25.6 -16.3 -5.28 P7XJWM 41.0 -0.8 -0.26 TVETMT 28.2 -13.6 -4.42 J9A365 41.0 -0.8 -0.26 GIG3NC 29.9 -11.9 -3.87 SEJFEA 41.1 -0.7 -0.23 1D31A3 30.0 -11.8 -3.83 RILD6I 41.1 -0.7 -0.23 3DB3YF 32.0 -9.8 -3.19 JNKRGL 41.2 -0.6 -0.20 PVVVKJ 33.9 -7.9 -2.58 L0SOSG 41.2 -0.6 -0.20 NT6XKR 34.0 -7.8 -2.54 FTFGF7 41.4 -0.4 -0.13 O37CO6 35.0 -6.8 -2.21 BG2SLB 41.5 -0.3 -0.10 FWRG58 35.0 -6.8 -2.21 HFYHFD 41.6 -0.2 -0.07 JCPDEV 36.2 -5.6 -1.81 DMMMMG 41.7 -0.1 -0.04 TFB6JZ 36.8 -5.0 -1.62 CABMNN 41.8 0.0 -0.01 4CCTQB 37.7 -4.1 -1.33 WM44EE 41.9 0.1 0.03 8X8488 38.0 -3.8 -1.24 GSHGOF 41.9 0.1 0.03 EGNF7G 38.1 -3.7 -1.20 HOU5IO 42.1 0.3 0.08 AMOGGG 39.0 -2.8 -0.91 V8EXVQ 42.1 0.3 0.09 GNGGG8 39.0 -2.8 -0.91 YSEXJD 42.1 0.3 0.09 YRVPY5 39.1 -2.7 -0.88 F3HS08 42.2 0.4 0.13 EIECD7 39.2 -2.6 -0.85 CSFZJZ 42.2 0.4 0.13 JQGKRH 39.2 -2.6 -0.85 22M222 42.3 0.5 0.14 AR7S7W 39.4 -2.4 -0.77 SIF50H 42.3 0.5 0.16 A99LH9 39.6 -2.2 -0.72 2VY888 42.4 0.6 0.19 OOCWTO 39.8 -2.0 -0.64 RTRIO9 42.4 0.6 0.21 KZRYK5 39.9 -1.9 -0.62 BYLJA9 42.5 0.7 0.22 PMCINM 40.0 -1.8 -0.60 BNQNNV 42.6 0.8 0.26 YRARMC 40.2 -1.6 -0.52 WRGTRP 42.6 0.8 0.26 4TZWAV 40.3 -1.5 -0.49 O888FC 42.6 0.8 0.26 ZECZ6W 40.3 -1.5 -0.49 QQCQAQ 42.8 1.0 0.32 IKISEG 40.4 -1.4 -0.47 BVQYTQ 42.9 1.1 0.35 VRAJLX 40.5 -1.3 -0.43 R7RR6M 42.9 1.1 0.36 YD88F8 40.5 -1.3 -0.42 RMBHBW 42.9 1.1 0.37 ZWYPLA 40.6 -1.2 -0.39 N9Y5J4 43.0 1.2 0.39 DBHUHY 40.6 -1.2 -0.39 T8ZTTT 43.0 1.2 0.39 XVXMYY 40.7 -1.2 -0.38 CCORYM 43.0 1.2 0.39 NRHUYD 40.7 -1.1 -0.36 YMBZHZ 43.0 1.2 0.39 GWFSGI 40.8 -1.0 -0.33 FAHHM9 43.0 1.2 0.39 KUOOIY 40.8 -1.0 -0.32 KTL2KK 43.0 1.2 0.39 RWTRU8 41.0 -0.8 -0.26 HLHPRH 43.1 1.3 0.42 PRYEOG 41.0 -0.8 -0.26 O77FQX 43.1 1.3 0.42 TFXAMC 41.0 -0.8 -0.26 VP4FPK 43.1 1.3 0.42

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Heroin Deviation Code Concentration from robust z-score (mass%) average (mass%) XS9KCX 43.2 1.4 0.45 RTTTXL 43.4 1.6 0.52 G4IK4G 43.5 1.7 0.55 MMNPPT 43.7 1.9 0.61 TCEWUO 43.7 1.9 0.61 9X9XK9 43.7 1.9 0.63 XQOBO8 43.8 2.0 0.65 43BPPC 43.9 2.1 0.67 8TDKSP 44.0 2.2 0.71 BRJPLX 44.0 2.2 0.71 3VAS7U 44.0 2.2 0.71 MWSMPP 44.3 2.5 0.79 U7IBAC 44.3 2.5 0.81 8K8OSH 44.5 2.7 0.87 WS6KSK 45.0 3.2 1.04 IQLV57 45.4 3.6 1.17 TWPVRD 45.5 3.7 1.19 PAMP84 46.0 4.2 1.36 BTUABB 47.1 5.3 1.72 OMOLC6 47.5 5.7 1.85 ATVQQJ 47.7 5.9 1.91 GKGVZX 47.7 5.9 1.91 VWWXWB 47.8 6.0 1.95 G5GNGG 47.8 6.0 1.95 9PLW9Q 48.0 6.2 2.01 DQQX66 48.2 6.4 2.08 PKIAAH 49.7 7.9 2.56 3CAJ33 51.1 9.3 3.02 TKVKOB 52.2 10.4 3.37 78PEHN 64.3 22.5 7.30 EQNEIU 76.6 34.8 11.29

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

7. Summary of responses for Test Sample-2

The summary of responses of all 179 participating laboratories for the identification of SM-2:

Correct identification of Test Sample-2:

Substance Name Number of laboratories Percentage Cocaine 179 100%

False positives for Test Sample-2 (techniques(s) used):

Round Code Substance Reported Tech Code 2VY888 Procaine 180 78PEHN Tetraimidazole 180, 231 EQNEIU Aminorex 180

IK4RMW Levorphanol 180, 231 KZRYK5 Caffeine 180 RNTT7L Caffeine 180, 231 RWTRU8 Lidocaine (Lignocaine) 180, 171 WARWWC Epinephrine 180 WZDE4O Caffeine 180

False negatives for Test Sample-2 with respect to Cocaine (technique(s) used):

There were no false negative results for SM-2

Analysis not performed for Test Sample-2 with respect to Cocaine:

All participating laboratories carried out analysis for Cocaine

Frequency of use of screening, identification and quantification techniques:

Test Sample-2: Response Summary

No of Participants: 179 (Qualitative); 127 (Quantitative) Technique 140 141 142 150 160 161 170 171 180 190 210 211 230 231 250 Screening (No.) 58 63 49 10 0 0 1 5 68 16 5 2 0 0 4 (%) 32.4 35.2 27.4 5.6 0.0 0.0 0.6 2.8 38.0 8.9 2.8 1.1 0.0 0.0 2.2 Identification 12 4 4 26 4 14 1 29 169 65 5 6 3 5 5 (No.(%) 6.7 2.2 2.2 14.5 2.2 7.8 0.6 16.2 94.4 36.3 2.8 3.4 1.7 2.8 2.8 Quantification (No.) 0 0 0 0 6 23 2 74 11 0 1 3 2 3 0 (%) 0.0 0.0 0.0 0.0 4.7 18.1 1.6 58.3 8.7 0.0 0.8 2.4 1.6 2.4 0.0

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Score Report per Sample per Substance: Round: 2020/1 UNODC value: 48.3% Robust mean: 48.1% Max reported: 73.9% Robust SD: 2.41% Substance: SM-2; Cocaine Min reported: 0.74% Robust CV%: 5.01% No of labs: 127 4.00

3.00 2.76 2.51 2.33 2.26 2.14 2.06 1.95 1.76

2.00 1.72 1.72 1.35 1.22 1.22 1.10 1.02 0.93 0.89 0.88 0.81 0.81 0.81 0.81 0.78 1.00 0.76 0.68 0.64 0.63 0.60 0.57 0.52 0.52 0.48 0.48 0.46 0.44 0.44 0.39 0.39 0.33 0.31 0.30 0.29 0.27 0.26 0.14 0.12 0.10 0.10 0.10 0.10 0.10 0.04 0.02 0.02 0.02 0.02 0.02 0.02 3.76 4.34 7.08 10.74 0.00 8.85 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 - 0.06 0.06 ------19.65 17.61 13.31 11.99 0.10 ------0.15 - 0.19 0.19 - 0.23 0.23 0.23 0.23 - - 0.25 0.27 - - - - 0.30 - 0.31 - - 0.35 - 0.40 0.40 - 0.42 0.44 0.44 0.44 - - 0.47 0.47 ------0.56 - 0.64 0.64 0.64 0.64

-1.00 - - - - 0.77 0.81 0.81 - 0.84 0.85 0.85 0.85 0.85 ------0.94 - 0.99 - 1.06 - 1.14 1.18 - - 1.43 - 1.64 1.68 1.68 1.68

-2.00 - - - - 1.82 1.85 - - 2.18 2.19 - - -3.00 35 3. - -4.00 I77IF7 IKISEG RILD6I K2KJIK 9YIBLY CSFZJZ TFB6JZ JYYOJY SIF50H SEJFEA BYLJA9 BRJPLX 9FSJAA EIECD7 YSEXJD HZRLLL J9A365 IQLV57 T8ZTTT 3CAJ33 XKKFPL VRAJLX RTRIO9 ETRYEE KTL2KK N9Y5J4 FTFGF7 9L9I9M KZRYK5 G4IK4G JCPDEV 8X8488 YD88F8 PKIAAH JNKRGL PVVVKJ F3HS08 XS9KCX 9X9XK9 2VY888 U7IBAC 8TDKSP VP4FPK YRVPY5 BG2SLB 07HEEE 3DB3YF 43BPPC EQNEIU AVRBSE GIG3NC NT6XKR 1D31A3 KUOOIY 3VAS7U FBOH8T 8K8OSH 78PEHN 4CCTQB HFYHFD ATVQQJ V8EXVQ JQGKRH GWFSGI TKVKOB HOU5IO PRYEOG HLHPRH GKGVZX T6MTE2 O77FQX BTUABB EGNF7G TVETMT WS6KSK O37CO6 ZECZ6W ZWYPLA 1UDDLA VVNYVV 22M222 UFPUBG BVQYTQ TFXAMC YMBZHZ GSHGOF A33M3R PAMP84 R7RR6M DQQX66 4TZWAV AR7S7W WN364S 9PLW9Q DBHUHY 9POVHQ YRARMC NRHUYD YAFCMU FWRG58 XQOBO8 RWTRU8 P7XJWM CCORYM WRGTRP TWPVRD OMOLC6 ORPW0X UBNBHN FAHHM9 GNGGG8 PMCINM G5GNGG TCEWUO WM44EE BNQNNV QQCQAQ CABMNN MMNPPT UWUGNF OOCWTO AMOGGG RMBHBW MWSMPP VWWXWB WARWWC DMMMMG Z-scores can be interpreted by participants in line with ISO 13528:2015*, section 9.4.2 as follows: IzI ≤ 2.00 is considered to be acceptable 2.00 < IzI < 3.00 is considered to be questionable (or warning signal) IzI ≥ 3.00 is considered to be unacceptable (or action signal)

A single action signal or warning signal in two successive rounds shall be taken that an anomaly has occurred that requires investigation.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Score Report per Sample per Substance:

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Scores for Test Sample-2

Cocaine Cocaine Deviation Deviation Code Concentration from robust Code Concentration from robust z-score z-score (mass%) average (mass%) average (mass%) (mass%) RTRIO9 0.7 -47.4 -19.65 V8EXVQ 47.4 -0.7 -0.25 K2KJIK 5.7 -42.4 -17.61 XKKFPL 47.5 -0.6 -0.23 UWUGNF 16.0 -32.1 -13.31 YRVPY5 47.5 -0.6 -0.23 WARWWC 19.2 -28.9 -11.99 N9Y5J4 47.5 -0.6 -0.23 A33M3R 26.7 -21.4 -8.85 BG2SLB 47.5 -0.6 -0.23 9FSJAA 40.0 -8.1 -3.35 WN364S 47.6 -0.5 -0.19 EQNEIU 42.8 -5.3 -2.19 NRHUYD 47.6 -0.5 -0.19 3CAJ33 42.8 -5.3 -2.18 VWWXWB 47.7 -0.4 -0.15 FBOH8T 43.6 -4.5 -1.85 RILD6I 47.8 -0.3 -0.10 J9A365 43.7 -4.4 -1.82 WM44EE 47.9 -0.2 -0.06 8K8OSH 44.0 -4.1 -1.68 I77IF7 47.9 -0.2 -0.06 8TDKSP 44.0 -4.1 -1.68 PMCINM 48.0 -0.1 -0.02 GNGGG8 44.0 -4.1 -1.68 9PLW9Q 48.0 -0.1 -0.02 TCEWUO 44.1 -4.0 -1.64 WS6KSK 48.0 -0.1 -0.02 UFPUBG 44.6 -3.5 -1.43 BYLJA9 48.0 -0.1 -0.02 9L9I9M 45.2 -2.9 -1.18 RWTRU8 48.0 -0.1 -0.02 EGNF7G 45.3 -2.8 -1.14 PRYEOG 48.0 -0.1 -0.02 VP4FPK 45.5 -2.6 -1.06 3DB3YF 48.0 -0.1 -0.02 78PEHN 45.7 -2.4 -0.99 SIF50H 48.0 -0.1 -0.02 TVETMT 45.8 -2.3 -0.94 P7XJWM 48.0 -0.1 -0.02 AMOGGG 46.0 -2.1 -0.85 YD88F8 48.1 0.0 0.02 PAMP84 46.0 -2.1 -0.85 PKIAAH 48.1 0.0 0.02 9POVHQ 46.0 -2.1 -0.85 JNKRGL 48.1 0.0 0.02 9YIBLY 46.0 -2.1 -0.85 O37CO6 48.1 0.0 0.02 TFB6JZ 46.0 -2.1 -0.84 1D31A3 48.1 0.0 0.02 NT6XKR 46.1 -2.0 -0.81 JQGKRH 48.1 0.0 0.02 YMBZHZ 46.1 -2.0 -0.81 CABMNN 48.2 0.0 0.04 OMOLC6 46.2 -1.9 -0.77 GIG3NC 48.3 0.2 0.10 IKISEG 46.5 -1.6 -0.64 PVVVKJ 48.3 0.2 0.10 YRARMC 46.5 -1.6 -0.64 YSEXJD 48.3 0.2 0.10 FTFGF7 46.5 -1.6 -0.64 BVQYTQ 48.3 0.2 0.10 ETRYEE 46.5 -1.6 -0.64 DBHUHY 48.3 0.2 0.10 CSFZJZ 46.7 -1.4 -0.56 RMBHBW 48.4 0.3 0.12 ORPW0X 46.9 -1.2 -0.47 HLHPRH 48.4 0.3 0.14 AVRBSE 46.9 -1.2 -0.47 MMNPPT 48.7 0.6 0.26 XQOBO8 47.0 -1.1 -0.44 F3HS08 48.7 0.6 0.27 EIECD7 47.0 -1.1 -0.44 GKGVZX 48.8 0.6 0.29 KTL2KK 47.0 -1.1 -0.44 GWFSGI 48.8 0.7 0.30 QQCQAQ 47.0 -1.1 -0.42 CCORYM 48.8 0.7 0.31 IQLV57 47.1 -1.0 -0.40 XS9KCX 48.9 0.8 0.33 4CCTQB 47.1 -1.0 -0.40 TFXAMC 49.0 0.9 0.39 KZRYK5 47.2 -0.9 -0.35 T6MTE2 49.0 0.9 0.39 ATVQQJ 47.3 -0.8 -0.31 G4IK4G 49.1 1.0 0.44 HOU5IO 47.3 -0.8 -0.30 SEJFEA 49.1 1.0 0.44 R7RR6M 47.4 -0.7 -0.27 JCPDEV 49.2 1.1 0.46

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Cocaine Deviation Code Concentration from robust z-score (mass%) average (mass%) UBNBHN 49.2 1.1 0.48 VVNYVV 49.2 1.1 0.48 ZECZ6W 49.3 1.2 0.52 O77FQX 49.3 1.2 0.52 22M222 49.4 1.3 0.57 BNQNNV 49.5 1.4 0.60 OOCWTO 49.6 1.5 0.63 8X8488 49.6 1.5 0.64 GSHGOF 49.7 1.6 0.68 9X9XK9 49.9 1.8 0.76 YAFCMU 49.9 1.8 0.78 ZWYPLA 50.0 1.9 0.81 2VY888 50.0 1.9 0.81 G5GNGG 50.0 1.9 0.81 FAHHM9 50.0 1.9 0.81 VRAJLX 50.2 2.1 0.88 WRGTRP 50.2 2.1 0.89 3VAS7U 50.3 2.2 0.93 DQQX66 50.5 2.4 1.02 KUOOIY 50.7 2.6 1.10 BRJPLX 51.0 2.9 1.22 FWRG58 51.0 2.9 1.22 MWSMPP 51.3 3.2 1.35 4TZWAV 52.2 4.1 1.72 BTUABB 52.2 4.1 1.72 HZRLLL 52.3 4.2 1.76 HFYHFD 52.7 4.6 1.95 1UDDLA 53.0 4.9 2.06 U7IBAC 53.2 5.1 2.14 T8ZTTT 53.5 5.4 2.26 AR7S7W 53.7 5.6 2.33 43BPPC 54.1 6.0 2.51 TWPVRD 54.7 6.6 2.76 TKVKOB 57.1 9.0 3.76 DMMMMG 58.5 10.4 4.34 07HEEE 65.1 17.0 7.08 JYYOJY 73.9 25.8 10.74

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

8. Summary of responses for Test Sample-3

The summary of responses of all 179 participating laboratories for the identification of SM-3:

Correct identification of Test Sample-3:

Substance Name Number of laboratories Percentage Caffeine 148 82.7%

False positives for Test Sample-3 (technique(s) used):

Round Code Substance Reported Tech Code WZDE4O ∆9-Tetrahydrocannabinol 180

False negatives for Test Sample-3 with respect to Caffeine (technique(s) used):

Round Code Tech Code Round Code Tech Code 22M222 140, 171 LC00BZ 180 4TZWAV 180 P7FEGC 180, 190 5JIQGU 180 RTRIO9 161 AR7S7W 180 T6MTE2 180 ATVQQJ 180 T8ZTTT 171, 180 BSUUJE 180 TCEWUO 171, 180

GBACTG 150 UWUGNF 180, 210 GIG3NC 180 VVNYVV 180 GWFSGI 171, 180 WARWWC 180 HOOOOO 150, 180 WZDE4O 180 I77IF7 161, 180 XJRFNX 150, 180 KZRYK5 180

Analysis not performed for Test Sample-3 with respect to Caffeine: DUEWAQ, NT6XKR, QYQLQW, SIF50H, TKVKOB, VP4FPK, YD88F8 and YMBZHZ

Frequency of use of screening, identification and quantification techniques:

Test Sample-3: Response Summary

No of Participants: 179 (Qualitative); 0 (Quantitative) Technique 140 141 142 150 160 161 170 171 180 190 210 211 230 231 250 Screening (No.) 58 63 49 10 0 0 1 5 68 16 5 2 0 0 4 (%) 32.4 35.2 27.4 5.6 0.0 0.0 0.6 2.8 38.0 8.9 2.8 1.1 0.0 0.0 2.2 Identification 12 4 4 26 4 14 1 29 169 65 5 6 3 5 5 (No.(%) 6.7 2.2 2.2 14.5 2.2 7.8 0.6 16.2 94.4 36.3 2.8 3.4 1.7 2.8 2.8 Quantification (No.) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 (%) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

9. Summary of responses for Test Sample-4

The summary of responses of all 179 participating laboratories for the identification of SM-4:

Correct identification of Test Sample-4:

Substance Name Number of laboratories Percentage Lactose 80 44.7%

Metamfetamine 177 98.9%

False positives for Test Sample-4 (technique(s) used): Round Code Substance Reported Tech Code A33M3R Cyclopentolate, mephedrone 180, 190 IK4RMW Amfetamine, caffeine, mephedrone 180, 231 RNTT7L Caffeine 180, 231 WARWWC Epinephrine 180 XKKFPL Phentermine 140, 180

False negatives for Test Sample-4 with respect to Metamfetamine (technique(s) used):

Round Code Tech Code BSUUJE 180 P7FEGC 180, 190

Analysis not performed for Test Sample-4 with respect to Metamfetamine: All participating laboratories carried out analysis for Metamfetamine

Frequency of use of screening, identification and quantification techniques:

Test Sample-4: Response Summary

No of Participants: 179 (Qualitative); 96 (Quantitative) Technique 140 141 142 150 160 161 170 171 180 190 210 211 230 231 250 Screening (No.) 58 63 49 10 0 0 1 5 68 16 5 2 0 0 4 (%) 32.4 35.2 27.4 5.6 0.0 0.0 0.6 2.8 38.0 8.9 2.8 1.1 0.0 0.0 2.2 Identification 12 4 4 26 4 14 1 29 169 65 5 6 3 5 5 (No.(%) 6.7 2.2 2.2 14.5 2.2 7.8 0.6 16.2 94.4 36.3 2.8 3.4 1.7 2.8 2.8 Quantification (No.) 0 0 0 0 4 20 1 53 4 0 1 5 1 5 0 (%) 0.0 0.0 0.0 0.0 4.2 20.8 1.0 55.2 4.2 0.0 1.0 5.2 1.0 5.2 0.0

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Score Report per Sample per Substance: Round: 2020/1 UNODC value: 19.6% Robust mean: 19.6% Max reported: 1967% Robust SD: 1.29% Substance: SM-4; Metamfetamine Min reported: 2.49% Robust CV%: 6.54% No of labs: 96 4.00 3.23 3.07 3.00 2.61

2.00 1.83 1.36 1.36 1.29 1.21 1.21 1.21 0.90 0.82 0.82

1.00 0.74 0.66 0.51 0.51 0.51 0.48 0.43 0.43 0.39 0.37 0.35 0.35 0.29 0.27 0.27 0.27 0.27 0.27 0.27 0.25 0.12 0.12 0.09 0.04 0.04 0.04 4.16 5.39 6.11 13.35 27.10 1515.44 0.00 0.02 0.04 0.04 0.04 0.04 0.04 0.05 - 13.35 ------0.10 0.11 - 0.12 0.12 0.12 0.12 ------0.17 0.17 0.19 - - - 0.27 - 0.35 0.35 0.35 0.35 0.35 - - - - - 0.43 0.43 - - 0.51 0.51 0.51 - - -

-1.00 0.66 0.66 0.66 - - - 0.74 - 0.82 0.82 - - 0.89 0.89 0.89 - - - 0.97 1.02 - - 1.21 - 1.28 1.28 1.31 - - - 1.60

-2.00 - 2.06 - 2.31 -

-3.00 2.68 - 2.92 - 3.00 - 3.05 3.07 - -

-4.00 RILD6I IKISEG K2KJIK CSFZJZ 9YIBLY JYYOJY SEJFEA SIF50H BYLJA9 BRJPLX HZRLLL EIECD7 YSEXJD T8ZTTT IQLV57 J9A365 VRAJLX 3CAJ33 RTTTXL N9Y5J4 RTRIO9 FTFGF7 8X8488 G4IK4G XS9KCX JNKRGL 2VY888 F3HS08 9X9XK9 PKIAAH PVVVKJ U7IBAC 8TDKSP BG2SLB YRVPY5 VP4FPK 43BPPC A99LH9 L0SOSG O888FC EQNEIU AVRBSE GIG3NC NT6XKR 1D31A3 KUOOIY 3VAS7U 8K8OSH 4CCTQB 78PEHN HFYHFD GWFSGI JQGKRH TKVKOB HOU5IO PRYEOG HLHPRH GKGVZX BTUABB T6MTE2 EGNF7G TVETMT ZWYPLA 22M222 BVQYTQ XVXMYY GSHGOF YMBZHZ PAMP84 4TZWAV R7RR6M AR7S7W DQQX66 YRARMC 9POVHQ NRHUYD FWRG58 XQOBO8 WRGTRP RWTRU8 CCORYM FAHHM9 OMOLC6 GNGGG8 PMCINM G5GNGG TCEWUO BNQNNV WM44EE MMNPPT UWUGNF AMOGGG RMBHBW VWWXWB DMMMMG XWWGWW Z-scores can be interpreted by participants in line with ISO 13528:2015*, section 9.4.2 as follows: IzI ≤ 2.00 is considered to be acceptable 2.00 < IzI < 3.00 is considered to be questionable (or warning signal) IzI ≥ 3.00 is considered to be unacceptable (or action signal)

A single action signal or warning signal in two successive rounds shall be taken that an anomaly has occurred that requires investigation.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Score Report per Sample per Substance:

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Z-Scores for Test Sample-4

Metamfetamine Metamfetamine Deviation Deviation Code Concentration from robust Code Concentration from robust z-score z-score (mass%) average (mass%) average (mass%) (mass%) K2KJIK 2.5 -17.1 -13.35 L0SOSG 19.6 0.0 -0.04 NT6XKR 15.7 -3.9 -3.07 CSFZJZ 19.6 0.0 -0.04 XS9KCX 15.7 -3.9 -3.05 IKISEG 19.6 0.0 -0.02 FTFGF7 15.8 -3.8 -3.00 G4IK4G 19.7 0.1 0.04 T8ZTTT 15.9 -3.7 -2.92 IQLV57 19.7 0.1 0.04 WRGTRP 16.2 -3.4 -2.68 HLHPRH 19.7 0.1 0.04 GWFSGI 16.7 -2.9 -2.31 KUOOIY 19.8 0.2 0.09 PAMP84 17.0 -2.6 -2.06 YSEXJD 19.8 0.2 0.12 22M222 17.6 -2.0 -1.60 BVQYTQ 19.8 0.2 0.12 HOU5IO 18.0 -1.6 -1.31 9X9XK9 20.0 0.4 0.25 GNGGG8 18.0 -1.6 -1.28 N9Y5J4 20.0 0.4 0.27 PRYEOG 18.0 -1.6 -1.28 BRJPLX 20.0 0.4 0.27 4TZWAV 18.1 -1.5 -1.21 AR7S7W 20.0 0.4 0.27 43BPPC 18.3 -1.3 -1.02 SIF50H 20.0 0.4 0.27 UWUGNF 18.4 -1.2 -0.97 FAHHM9 20.0 0.4 0.27 HZRLLL 18.5 -1.1 -0.89 9YIBLY 20.0 0.4 0.27 JYYOJY 18.5 -1.1 -0.89 78PEHN 20.0 0.4 0.29 GSHGOF 18.5 -1.1 -0.89 CCORYM 20.1 0.5 0.35 YRARMC 18.6 -1.0 -0.82 PKIAAH 20.1 0.5 0.35 RWTRU8 18.6 -1.0 -0.82 XVXMYY 20.1 0.5 0.37 BNQNNV 18.7 -0.9 -0.74 VRAJLX 20.2 0.5 0.39 8K8OSH 18.8 -0.8 -0.66 EGNF7G 20.2 0.6 0.43 A99LH9 18.8 -0.8 -0.66 3CAJ33 20.2 0.6 0.43 1D31A3 18.8 -0.8 -0.66 J9A365 20.3 0.7 0.48 AMOGGG 19.0 -0.6 -0.51 WM44EE 20.3 0.7 0.51 8TDKSP 19.0 -0.6 -0.51 O888FC 20.3 0.7 0.51 9POVHQ 19.0 -0.6 -0.51 JQGKRH 20.3 0.7 0.51 BG2SLB 19.1 -0.5 -0.43 TVETMT 20.5 0.9 0.66 4CCTQB 19.1 -0.5 -0.43 NRHUYD 20.6 1.0 0.74 TCEWUO 19.2 -0.4 -0.35 GKGVZX 20.7 1.1 0.82 YRVPY5 19.2 -0.4 -0.35 RTTTXL 20.7 1.1 0.82 XQOBO8 19.2 -0.4 -0.35 ZWYPLA 20.8 1.2 0.90 BYLJA9 19.2 -0.4 -0.35 PVVVKJ 21.2 1.6 1.21 JNKRGL 19.2 -0.4 -0.35 VWWXWB 21.2 1.6 1.21 8X8488 19.3 -0.3 -0.27 3VAS7U 21.2 1.6 1.21 VP4FPK 19.4 -0.2 -0.19 HFYHFD 21.3 1.7 1.29 EQNEIU 19.4 -0.2 -0.17 BTUABB 21.4 1.8 1.36 AVRBSE 19.4 -0.2 -0.17 G5GNGG 21.4 1.8 1.36 XWWGWW 19.5 -0.1 -0.12 FWRG58 22.0 2.4 1.83 2VY888 19.5 -0.1 -0.12 T6MTE2 23.0 3.4 2.61 RILD6I 19.5 -0.1 -0.12 OMOLC6 23.6 4.0 3.07 F3HS08 19.5 -0.1 -0.12 DQQX66 23.8 4.2 3.23 MMNPPT 19.5 -0.1 -0.11 U7IBAC 25.0 5.4 4.16 PMCINM 19.5 -0.1 -0.10 TKVKOB 26.6 7.0 5.39 R7RR6M 19.6 0.0 -0.05 DMMMMG 27.5 7.9 6.11 SEJFEA 19.6 0.0 -0.04 GIG3NC 36.8 17.2 13.35 YMBZHZ 19.6 0.0 -0.04 RTRIO9 54.5 34.9 27.10 EIECD7 19.6 0.0 -0.04 RMBHBW 1967.0 1947.4 1515.44 ICE 2020/1-SM Copyright © 2021 UNODC Page 25 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

10. ANNEX 1: Participants’ results for Test Sample-1 Identified substances for Test Sample 1

Code Identified Substances 07HEEE Heroine 0V0005 Heroin and Caffeine 1D31A3 Heroin and Morphine 1UDDLA Caffeine, Racemethorphan, acetylcodein, 6-monoacetylmorphine, diacetylmorphine 22M222 heroína 2VY888 heroine 3CAJ33 Opiaces 3CW3T3 heroin 3DB3YF Heroin 3MBOO3 Heroin 3VAS7U heroine, morphine, codeine 3ZZ7LZ heroin 43BPPC Heroin, 6-monoacetylmorphine 4CCTQB Heroin 4TZWAV eroine 5BQYQN Heroine 5JIQGU Heroine 78PEHN Codeine, Acetylcodeine, Morphine, Papaverine 8K8OSH HEROINE 8TDKSP Heroin 8X8488 heroin, morphin, 3- and 6-monoacetylmorphin 9FSJAA HEROIN 9L9I9M diacetylmorphine and caffeine 9PLW9Q Diamorphine 9POVHQ heroin hcl 9X9XK9 heroin HCl 9YIBLY Diamorphine Hydrochloride A33M3R Heroin A99LH9 Heroin and monoacetylmorphines AMOGGG heroin AR7S7W Diamorphine HCL ATVQQJ Heroin AVRBSE Heroin B6QWQM Heroin BFQULP heroin BG2SLB heroin BNQNNV Heroine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances BRJPLX Heroin BSUUJE Morphine, Heroin, Codeine, 6-MAM BTUABB heroin BVQYTQ Diamorphine BYLJA9 heroin,acetylcodein,06-monoacetylmorphine,methorphan CABMNN heroin CBRWNZ Heroine and Monoacetylmorphines CCORYM Heroin CSFZJZ heroin DBHUHY Heroin DGUTVL Heroin DMMMMG heroin DQQX66 Heroin. DUEWAQ heroine EGNF7G HEROINE, CODEINE EIECD7 heroin EQNEIU Heroin, Morphine and Caffein ETRYEE Heroin F3HS08 heroin FAHHM9 Diamorphine Hydrochloride FBIONY Heroine, Morphine FBOH8T Heroin FTFGF7 heroin FWRG58 Heroin,Morphine G4IK4G Heroin G5GNGG heroin GBACTG HEROIN GIG3NC Heroin GKGVZX Heroin GNGGG8 Heroin GSHGOF heroin GWFSGI heroin H1111A heroin hydrochloride HFYHFD heroin, morphine HLHPRH heroin HMKGFH heroine HOOOOO Desomorphine and caffeine HOU5IO Heroin HZRLLL Heroin, caffeine I35533 heroin, monoacetyl morphine, acetyl codeine, trace amount of morphine and codeine I77IF7 heroin IK4RMW Heroine, Caffeine ICE 2020/1-SM Copyright © 2021 UNODC Page 27 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances IKISEG heroin IQLV57 Heroine IZMILZ heroin J9A365 HEROINE JCI9GI Heroine, Morphine JCPDEV HEROIN JKTQXD heroine JM4L8J Diamorphine JNKRGL Heroin JQGKRH Heroin JVAW1W Heroin JYYOJY Heroin, 6-MAM, Caffeine, Methorphan, Acetyl Codeine K2KJIK Heroin KTL2KK Diamorphine KUOOIY Heroin HCl KZRYK5 heroin L0SOSG Heroin and monoacetylmorphines LC00BZ Heroin MMNPPT Diamorphine Hydrochloride MWSMPP HEROIN N9Y5J4 Heroin NRHUYD HEROIN 40.7% NT6XKR Heroin O37CO6 Heroine + 6-MAM O77FQX Heroin, Morphine, 6-Monoacetyl morphine (6-MAM) O888FC Heroin and Monoacetylmorphines OASBL3 Heroin, Dextromethorphan OKGKFC Heroin and Monoacetylmorphines OMOLC6 Heroin OOCWTO Diamorphine, Methorphan ORPW0X Heroin P7FEGC heroin, 6-MAM P7XJWM HEROIN PAMP84 6-mam, Morphine PCZ8NU Heroin PKIAAH Heroin PMCINM HEROIN PMVPBP Heroin PRYEOG Heroin PVVVKJ Heroine QHD076 Heroin and caffeine QQCQAQ héroïne ICE 2020/1-SM Copyright © 2021 UNODC Page 28 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances QYQLQW Heroin R7RR6M HEROINE REHHTU HEROIN, DEXTROMETHORPHAN RILD6I Diamorphine, Acetylcodeine, 6-monoacetylmorphine, morphine RMBHBW Heroin 42.94% RNTT7L Heroin RTRIO9 dextromethorphan RTTTXL Heroin RWTRU8 Heroin, Monoacetylmorphin, Morphin, Dextromethorphan SEJFEA Heroin SIF50H heroin SYIONF Heroin T6MTE2 Heroin T777GE heroin T8ZTTT heroin, 6-monoacethylmoprhine TCEWUO heroin TFB6JZ heroin TFXAMC Diamorphine, 6-Monoacetylmorphine and Caffeine, and indicated the presence of Dextromethorphan TKVKOB Heroin TTGC6K OPIATES TVETMT HEROINA TWPVRD Heroin & Caffeine U7IBAC Heroine UBNBHN Heroin UFPUBG Heroin, 6-Monoacetylmorphine, morphine UMRFHI Heroin, Dextromethorphan, Caffeine UWUGNF Heroin HCl V8EXVQ Heroíne V8U885 heroin VFTM1K Heroin VP4FPK Heroin VRAJLX Heroin HCl VVNYVV HEROIN VWWXWB Heroin (Diacetylmorphine) WARWWC Diacetylmorphine, epinephrine, Nordazepam WM44EE HEROIN WN364S Heroin WNUDTF HEROINA WRGTRP heroin, morphine, 6-MAM WS6KSK Heroin WZDE4O heroin ICE 2020/1-SM Copyright © 2021 UNODC Page 29 of 104

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Code Identified Substances XJRFNX HEROIN XKKFPL Heroina XQOBO8 heroin, 6-MAM XS9KCX Heroin XSESED Heroin XVXMYY heroin XWWGWW Heroine, Dextromethorphan and MAM XYECSA Heroin YAFCMU Heroin YD88F8 heroina YMBZHZ Heroin YRARMC Mop, Heroin and Caffeine YRVPY5 Heroine, dextro-/levomethorphan YSEXJD Heroin YU1911 Heroin, Caffeine ZECZ6W Heroin ZWYPLA heroine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Statement of findings for Test Sample 1

Code Caffeine Heroin 07HEEE + +

0V0005 + + Heroin is controlled under Malaysian Dangerous Drugs Act 1952. Caffeine is controlled under Malaysian Poison Act 1952. SM1 also to contain Monoacetylmorphines which is controlled under Malaysian Dangerous Drugs Act 1952. SM1 also to contain Dextromethorphan which is controlled under Malaysian Poison Act 1952. 1D31A3 + + Caffeine, Acetylcodeine, 06-monoacetylmorphine and Dextromethorphan 1UDDLA + + The sample was analysed with FTIR and GCMS in two different solvents. 22M222 + + Adulterantes: cafeína, dextrometorfano, 6-monoacetilmorfina 2VY888 - +

3CAJ33 + + heroin, morphine, 6-MAM, codeine, noscapine 3CW3T3 - +

3DB3YF + + Sample was found to contain Heroin, with a W:W % purity of 32%. The sample also contained Caffeine 3MBOO3 + + The sample contains Heroin. The concentration has not been determined. 3VAS7U + +

3ZZ7LZ + +

43BPPC + + SM-1 was prepared from a seizure containing 43.88%(w/w)Heroin base. The test sample also contained 6-monoacetylmorphine with caffeine, Acetylcodein, dextromethorphan, desomorphine and Thebacon as minor components. 4CCTQB + + İt also includes acetylcodeine,6-monoacetylmorphine, codeine, morphine, dextromethorphan, caffeine 4TZWAV + + eroine was detected by GC/MS, confirmed by FTIR and quantified by GC/FID 5BQYQN + + It also contains dextromethorphan, acetylcodeine, monoacetylmorphine 5JIQGU + + The analyzed sample contains Heroin, Caffeine and Dextrometrophan. 78PEHN + +

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin 8K8OSH - +

8TDKSP + + On chemical analysis of a representative sample of the powder heroin was detected with a purity of approximately 44% (calculated as base). 8X8488 + + caffeine (3.7 %), dextrometorphan, acetylcodein 9FSJAA + + HEROIN+CAFFEINE+METHORPHAN+ACETYL CODEIN 9L9I9M + + the test sample also contained 6-monoacetylmorphine, vevomethorphan and cocaine as minos components 9PLW9Q + + 0.228g of powder containing 48% Diamorphine. Diamorphine is a Class A controlled drug subject to the provisions of the Misuse of Drugs Act 1971. 9POVHQ + + dextrometorphan caffein 9X9XK9 + + 43,74 % (w/w) heroin base, the sample also contained 6-monoacethylmorphine, dextromethorphan, caffeine, 9YIBLY + + Sample 2020/1/SM-1 was found to contain 47% diamorphine hydrochloride (41% as diamorphine base), together with caffeine and methorphan. The enantiomer of methorphan present could not be determined A33M3R + + Examination and analyses performed on the white solid in SM-1 showed it to contain heroin ( a narcotic analgesic) and caffeine (a xanthine stimulant). A99LH9 + + Sample 2020/1/SM-1 was found to contain 39.6% of heroin, 4.5% of monoacetylmorphines, dextromethorphan and caffeine. AMOGGG + + Heroin, methorphan and caffeine confirmed in the composite. AR7S7W - + Diamorphine HCL; Methorphan; Caffeine ATVQQJ - + Heroin 47.7 % and dextromethorphan, acetyl codeine and 6-mono-acetyl-morphine. AVRBSE + + Sample contained heroin as hydrochloride, monoacetylmorphine and caffeine. Identification of heroin by FTIR and GC/MS. Identification of caffeine and monoacetylmorphine by GC/MS. B6QWQM + + Presence of heroin was detected in the sample. The sample also contains chemical compounds suchs as: caffeine, acetylcodein, 6-monoacetylmorphine, diacetylmorphine and dextromethorphan. BFQULP + + Sample 2020/1/SM-1 is a light beige powder, gave a positive result for heroin,substance under national legislation on drugs.Caffeine and dextromethorphan were also detected. BG2SLB + + this sample is heroin

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin BNQNNV + + This sample is adulterated with caffeine and dextromethorphan. BRJPLX + + That I examined and analysed the said sample and found to contain: controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 1. (10) Diacetylmorphine (heroin) calculated as the hydrochloride 48% (w/w). The following non-controlled substances (s) has (have) been detected but not certified : Dextromethorphan, Cafffeine, Should you need this (these) detected substance(s) to be certified, please contact us. BSUUJE + + 6-MAM, Morphine, Heroin and Codeine were found in the 2020/1/SM-1 sample. Caffeine was also found. BTUABB + + the white-grey powder contains diacetylmorphine (47.1% w/w) and 6- monoacetylmorphine (9.57% w/w) whiche are controlled by national law. The sample contains methorphan too, that in its levogyre form is controlled by law. We can't identify which isomer is. BVQYTQ + + The sample was found to contain 42.9% of diamorphine (as base). BYLJA9 + + caffeine CABMNN + + heroin + cafein CBRWNZ ANP + Based on the above analysis, the sample was found to contain Heroine and Monoacetylmorphines. CCORYM + + Substance usually detected in our laboratory CSFZJZ + + Heroin. The sample also contained acetylcodeine, dextromethotphan and traze amounts of morphine, codeine and caffeine DBHUHY + + ./. DGUTVL + + Heroin+Dextromethorphan+Caffeine+6MAM+codeine DMMMMG + + SM1 contains heroin , caféine and also acetylcodein 6 monoacetylmorphine DQQX66 + + Heroin, caffeine and Dextromethorphan DUEWAQ ANP + Gov.Decision No. 1088/2004 Schedule.1 List 1 EGNF7G + + The sample SM1 is a mix of HEROINE, CODEINE, CAFFEINE and DEXTROMETHORPHAN. EIECD7 + + the sample contains a scheduled substance EQNEIU + + Retention time of Heroin, Morphine and Caffein were 24.004 min, 21.746 min and 14.587 min respectively. The concentration of sample injected in GC/MS was 126.5 ppm.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin ETRYEE + +

F3HS08 + + One glass bottle containing 0.22 grammes of a solid containing 96 milligrammes of heroin. FAHHM9 + + Item 2020/1/SM-1 contained a brown powder which was found to contain diamorphine hydrochloride, together with methorphan and caffeine. Diamorphine hydrochloride is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended). Methorphan comes in two isomeric forms, dextromethorphan which is not controlled under the Misuse of Drugs Act (as amended) and levomethorphan which is a class A controlled drug under the Misuse of Drugs Act (as amended). The analytical methods used in this trial were unable to distinguish between the two forms of methorphan in this powder. Caffeine is not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended). FBIONY + + The sample No. 2020/1/SM1 was found heroine, morphine, caffeine and dextormethorphan FBOH8T + + Mass spectrometry profile correlation between sample and reference material certified FTFGF7 + + it also includes acetyl codeine, 6-monoacetylmorphine,codeine, morphine, dextromethorphan and caffeine FWRG58 - +

G4IK4G + + In the test sample 2020/1/SM-1 was detected heroin, 6-monoacetylmorphine, acetilcodeine, caffeine and dextromethorphan. G5GNGG + + heroin, caffeine,dextromethorphan, codein, morphin, acetylcodein,6-monoacetylmorphin, papaverin GBACTG + + Sample 2020/1/SM-1 consists of light brown powder. Heroin, a prohibited substance included in the National Law for Narcotics, is found to be present in this sample. GIG3NC - +

GKGVZX + + İt also includes Morphine, Codeine, 6-monoacetylmorphine, acetylcodeine, Caffeine, Dextromethorphan GNGGG8 + + That I examined and analysed the said sample and found to contain: controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 1. (10) Diacetylmorphine (heroin) calculated as the hydrochloride 43% (w/w). That I examined and analysed the said sample and found to contain: The following non- controlled substances (s) has (have) been detected but not certified : Dextromethorphan, Caffeine, Should you need this (these) detected substance(s) to be certified, please contact us. GSHGOF + + heroin is controlled by the law of 7th February 2014 and regulated by the RD of 6th September 2017 GWFSGI + + brownish powder containing 40.8%(w/w) heroin, 8.93%(w/w) 6-monoacetylmorphine and caffeine, methorphan, acetylcodeine not quantified

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin H1111A + + Sample also contain: caffeine, dextromethorphan, morphine, acetylcodeine, 6- monoacetylmorphine, codeine and papaverine. HFYHFD + + - HLHPRH + + The sample contains 43.1±2.5 weight% heroin-base. The sample also contains caffeine, acetyl-codeine, O-6-monoacetyl-morphine. The sample also contains levomethorphane and/or its stereoisomer. HMKGFH + + also contains dextromethmorphan, acetyl-codeine, 6-monoacetyl-morphine and coffeine in traces HOOOOO + - The analysis detected desomorphine and caffeine, using Gas Chromatography/Mass Spectrometry and Fourier Transform Infrared Spectrometry. HOU5IO + + The sample contains Heroin and Caffeine. HZRLLL + +

I35533 + + Test sample 2020/1 /SM1 having gross weight 05.94 grams of light brown powder in amber glass bottle contains heroin, monoacetyl morphine, acetyl codeine, morphine and codeine. Moreover, caffeine and dextromethorphan (non-controlled substances) are also confirmed. I77IF7 + + In the powder heroin, caffeine and dextromethorphan are present. IK4RMW + + The above two drugs were detected in the sample using the laboratory technique that were used in the laboratory. IKISEG - +

IQLV57 + + It has been detected the presence of heroine and by-products of the acetylation of morphine. IZMILZ + + trace amount: morphine J9A365 + + DEXTROMETOPHANE JCI9GI + + The chemical tests and the coincidence on the retention time and mass fragmentogram with the reference material in the same conditions that the analyzed samples indicates the heroin, morphine, acetilcodeine, 6-MAM, dextromethorphan and caffeine presence. JCPDEV + + ALSO FOUNDED CAFFEINE, DEXTROMETORFANO, ACETILCODEINA, 6MAM JKTQXD + + Also contains acetyl-codeine, 6-monoacetyl-morphine, dextromethmorphan and coffeine in traces JM4L8J + + Powder contains Diamorphine with indications of caffeine and Dextromethorphan.. Diamorphine is a controlled drug under the Misuse of Drugs Acts, 1977 to 2016.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin JNKRGL ANP + The sample contains heroin.The amount of heroin is determined to 41% (as heroin base). Heroin is a controlled substance. JQGKRH + + Powder containing heroin. Additionally identified caffeine, dextromethorphan, codeine, morphine, acetylcodeine, 6-monoacethylmorphne. JVAW1W + + Sample was found containing Heroin, 6-Monoacetylmorphine, Dextromethorphan and Caffeine JYYOJY + + From screening test by using (MR) and from confirmation test by (GC-MS), the sample found to contain the controlled drug (Heroin) K2KJIK + + Caffeine, Dextromethprphan, O-6-Monoacetylmorphine KTL2KK + + The powder was found to contain diamorphine at a concentration of 43%. Diamorphine is controlled under the misuse of Drugs Act 1971 (as amended) as a class A drug. Caffeine was also detected. Caffeine is not controlled under the misuse of Drugs Act 1971 (as amended). KUOOIY + + Heroin as base 40.82% Other drugs found are Acetyl codeine, 6MAM, Morphine, Dextromethorphan and Caffeine KZRYK5 + + Test sample contained 39.9% diacetylmorphine, 8.6% 6-monoacetylmoprhine, methorpan, hydromorphone, codeine, acetylcodeine and caffeine L0SOSG + + The sample contained 41.2 % (w/w) heroin (base) and 8.4 % (w/w) monoacetylmorphines LC00BZ + + Heroin was identified in the sample 2020/1/SM1. MMNPPT + + One brown glass vial with black screw cap labelled "2020/1/SM-1 188" containing 228 milligrams of off-white powder. This powder was found to contain Diamorphine Hydrochloride at a purity of 50%. This is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended). MWSMPP + +

N9Y5J4 + + acetylcodeine, caffeine, methorphan, 6-monoacetylmorphine NRHUYD + + caffeine and d,l-metorphan NT6XKR + + Also found: 6-MAM, Morphine, Acetylcodeine O37CO6 + + 35% heroine + 4% 6-MAM + acetylcodeine + destromethorphane + caffein O77FQX + + 1- List I and IV of the Single Convention of 1961 2- List I of the Single Convention of 1961 3- List I of the Single Convention of 1961 O888FC + + Heroin, Monoacetylmorphine, Dextromethorphan and Caffeine was detected ICE 2020/1-SM Copyright © 2021 UNODC Page 36 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin OASBL3 ANP + Light brown powder analysed by GC/MS was found to contain Heroin & Dextromethorphan. Mass spectras were similar to CRM. OKGKFC + + Sample 2020/1/SM-1 found to contain Heroin, Monoacetylmorphines, Dextromethorphan and Caffeine. OMOLC6 + + The sample contains heroin which is listed as a controlled drug according to french order, appendix I of February 22nd 1990. OOCWTO + + A brown glass vial labelled 2020/1/SM-1 containing 0.23g of brown powder. A portion was analysed and found to contain diamorphine at a purity of 40%, together with Caffeine. Methorphan listed as an unconfirmed compound as we cannot confirm if D/L version and no reference standard available. ORPW0X + + In the sample 1 there is heroin P7FEGC + + heroin, 6-MAM, dextromethorphan, caffeine P7XJWM + + DEXTROMETORPHAN, CAFFEIN, ACETYLCODEIN, O6 MAM, MORPHIN, CODEIN, PAMP84 + + Dextromethorphan PCZ8NU ANP + Sample 2020/1/SM-1 found to contain Heroin PKIAAH + + Heroine and caffeine were identified PMCINM + + The test sample contained CAFFEINE and DEXTROMETHORPHAN (only by GCMS). The test sample also contained acetylcodeine, 6-monoacetylmorphine, and papaverine as minor components PMVPBP + + Dextromethorphan, 6-Monoacetylmorphine, Acetylcodeine and Caffeine PRYEOG ANP + That I examined and analysed the said sample and found it to contain: controlled subsatnce(s) within the meaningof the Controlled Drugs and Substances Act: Schedule I 1.(10) Diacetylmorphine (heroin) calculated as the hydrochloride 45 % (w/w). The following non-controlled substances(s) has(have) been detected but not certified: Dextromethorphan PVVVKJ Should you- need this (these) detected+ substance(s) to be certified, please contact us. The sample contains Heroine at 33.8 % purity and 6-MAM at 6.7 % and dextromethorphan QHD076 + + Heroin, caffeine, dextromethorphan, 6-monoacetylmorphine, 6-acetilcodeine, noscapine and papaverine were detected in SM-1 sample. QQCQAQ + + Héroïne is sheduled as illicit drug in France QYQLQW ANP + Brownish powder of SM-1 contains Heroin. R7RR6M + + acetylcodeine, caffeine, methophan, monoacetylmorphine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin REHHTU + + Off-white powder containing heroin, dextromethorphan, acetylcodeine, monoacetylmorphine and caffeine. RILD6I - + The sample is a mixture of opiates (street heroin).Diamorphine, Acetylcodeine, 6- monoacetylmorphine and morphine are Schedule I, drug substances. The purity of Diamorhine as base is 41.1%. RMBHBW + + Trace amounts of morphine, 6-monoacetyl morphine (6-MAM), caffeine RNTT7L + + Heroin is found with presence of caffeine RTRIO9 + +

RTTTXL + + Heroin is listed in the First Schedule of Dangerous Drug Act 1952 RWTRU8 + +

SEJFEA + + Mixture of heroin, caffeine and traces of natural accompanying substances - acetylmorphine, acetyl codeine, morphine a noscapine and traces of opioids of dextromethorphan structure. SIF50H ANP +

SYIONF + + The sample contains the substance Heroin. T6MTE2 + +

T777GE + + The sample contains heroin, caffeine, DXM. T8ZTTT + + greyish powder containing heroin, dextromethorphan and 6-MAM TCEWUO + + beige powder containing 43.7%w/w of heroin and 12.3% m/m of 6-MAM TFB6JZ + + caffeine, dextromethofphan, acetylcodeine, 6-monoacetylmorphine were also in the sample TFXAMC + + We would not typically report 6-MAM, Caffeine or Dextromethorphan in a sample containing Diamorphine, so our statement would read: “The above item was found to contain a glass vial with a lid, containing a quantity of off- white powder. The powder, which weighed 0.23 grams, was analysed and found to contain Diamorphine. A portion of the powder was further analysed and found to contain not less than 39% Diamorphine, by weight.” TKVKOB ANP + The ICE sample 2020/1 SM1 was found to contain Heroin. TTGC6K + + HEROIN 6-MAM CAFFEINE ACETYL CODEINE TVETMT + +

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin TWPVRD + + This sample was found to contain Diamorphine (also known as Heroin) which is a Class A controlled substance under the Misuse of Drugs Act 1971. This sample was also found to contain Caffeine, which is not controlled under the Misuse of Drugs Act 1971 and Methorphan. The analytical findings support the view that this compound is Methorphan. Methorphan is available in two different isomeric forms – Levomethorphan, which is a Class A controlled substance, and Dextromethorphan, which is not controlled under the Misuse of Drugs Act 1971. The analytical techniques available at this laboratory are unable to determine the difference between the two forms, and therefore I am unable to determine the legal status of the Methorphan in this sample. U7IBAC + +

UBNBHN + + Dextrometorphan also identified UFPUBG - + Sample 2020/1/SM-1 contains Heroin, 6-Monoacetylmorphine, Morphine, Acetylcodein and Dextromethorphan UMRFHI + + Retention time and fragmentation patterns obtained with samples are equivalent to those obtained with heroin, Dextromethorphan and Caffeine. UWUGNF + + Additionally it was identified caffeine and dextromethophan. V8EXVQ + + Lista I y IV de la Convención Única de 1961 V8U885 + + caffeine, 6-MAM, acetil-codeine, dextromethorphan and/or stereo isomers VFTM1K ANP + Ex#1;Heroin mixed with caffeine, Dextromethorphan, acetylcodeine, 6 monoacetylmorphine VP4FPK + + No Certificate of Analyst issued, R&D laboratory VRAJLX + + SM1 contains Heroin with Caffeine and Dextrometorphan; 40.49% Heroin base; the sample also contains Morphine and Codeine; VVNYVV + + THE SAMPLE CONTAIN CAFFEINE, DEXTROMETHORPHAN, ACETYLCODEINE AND 6- MONOACETYLMORPHINE dextromethorphan VWWXWB + + The sample contains diacetylmorphine (47.8% as free base), caffeine, dextromethorphan, acetylcodeine, 6-monoacetylmorphine. WARWWC - + Sample tested positive for diacetylmorphine using TLC and GC-MS WM44EE + + CAFFEINE, ACETYLCODEINE, MORPHINE, 6MAM, METHORPHAN WN364S + + It also contains Caffeine, Dextromethorphan WNUDTF + + LA MUESTRA 1 CONTIENE HEROINA Y CAFEINA

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin WRGTRP + + Heroin was detected by GC/MS and quantified by GC/FID. 6-MAM and morphine were detected by GC/MS. The sample contains also caffeine and dextromethorphan. WS6KSK + + Heroin 45% +/- 4, also found dextrometorphane,caffeine, acetylcodein, 6-MAM WZDE4O + +

XJRFNX + + Beige powder that contains controlled drug HEROIN. XKKFPL + + Cafeína, acetilcodeina, 6-acetilmorfina, dextrometorfano XQOBO8 + + 43.8% amount of Heroine is found with the help of quantitative methods of GC-MS. Beside, we have identified that 6-MAM is present. Also, we have observed that acetyl codeine, methorphan and Caffeine are present. XS9KCX + + it also includes acetylcodeine, 6-monoacetylmorphine, caffeine, dextromethorphan and codeine, morphine by trace XSESED + + 2020/1/SM-1 contains Heroin, a dangerous drug. It also contains Caffeine, Dextromethorphan, Acetylcodeine, and O-6 monoacetylmorphine. XVXMYY + + SM-1 was found to contain heroin. Also contain monoacetylmorphines, dextromethorphan and caffeine. XWWGWW + + Heroin and Monoacetylmorphines (MAM) is listed in the First Schedule of The Dangerous Drugs Acts 1952. Dextromethorphan is listed in the First Schedule of Poison Acts 1952 XYECSA - + Heroin was detected in the SM-1 sample. YAFCMU - + Dextrometorphane YD88F8 ANP +

YMBZHZ ANP + No CofA issued, R&D laboratory YRARMC + + The samples 2020/1/SM-1 contains Mop, Heroin and Caffeine detected by GC/MS and FTIR. The percentage by weight of Heroin is 40.2%. YRVPY5 + + Controlled drug, heroine, present in sample. Concentration approx 39%. Other controlled substances found is dextro-/levomethorphan. Other substance found is caffeine (no controlled drug). YSEXJD + + It contains heroin at 42.1%. It contains also caffeine, dextrométhorphane, morphine and codeine. YU1911 + + 2020/1/SM-1 was confirmed for Heroin which is a schedule I controlled substance in the US and caffeine which is not a controlled substance in the US.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine Heroin ZECZ6W + + Other compounds found: Caffein ZWYPLA + + caffeine, dextromethorphane, 6-MAM, 6-acetylcodeine, morphine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Identification methods for Test Sample 1

Legend: S ... used for Screening I ... used for Identification SI ... used for both

Analytical Technique Codes Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 07HEEE I S 0V0005 S I I 1D31A3 S I I I 1UDDLA S S I I 22M222 SI SI SI I 2VY888 I 3CAJ33 I I S 3CW3T3 SI 3DB3YF SI 3MBOO3 S I I S Raman 3VAS7U SI I 3ZZ7LZ S I I 43BPPC S I I 4CCTQB S S S I I 4TZWAV SI I 5BQYQN SI 5JIQGU S S S SI 78PEHN I SI I 8K8OSH SI I I 8TDKSP S S S I HRMS 8X8488 SI 9FSJAA SI I I SI 9L9I9M S S S I I S HNO3 9PLW9Q S S I 9POVHQ SI I 9X9XK9 SI I SI 9YIBLY S S S I I A33M3R S S S I I I A99LH9 S S SI AMOGGG SI I AR7S7W S S SI I ATVQQJ S S S I AVRBSE I SI I ICE 2020/1-SM Copyright © 2021 UNODC Page 42 of 104

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Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 B6QWQM S I I BFQULP S S S I I BG2SLB S I I BNQNNV S I I BRJPLX S I I BSUUJE SI BTUABB I S BVQYTQ I SI BYLJA9 I SI CABMNN I S CBRWNZ S I CCORYM S S S S I CSFZJZ I SI DBHUHY SI SI DGUTVL I SI I DMMMM S I I I HPLC/RID G DQQX66 S I DUEWAQ S S I I I Fast Blue EGNF7G SI S SI I I S IMMUNOCHROMA- TOGRAPHY EIECD7 I I EQNEIU S I ETRYEE SI S I I I F3HS08 S S I SI I FAHHM9 S S SI I S Simons Reagent FBIONY S I FBOH8T SI I FTFGF7 S S S I I FWRG58 I SI G4IK4G I G5GNGG SI SI SI I SI I I GBACTG S S I GIG3NC SI GKGVZX S S S I I GNGGG8 S I I GSHGOF I SI GWFSGI I I SI

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 H1111A S I I I HFYHFD SI HLHPRH S I SI I HMKGFH S I SI I HOOOOO S S S I I I HOU5IO SI I HZRLLL I S I35533 S S SI I I77IF7 I SI IK4RMW I I S GC-MS/MS IKISEG S S I I IQLV57 SI S I IZMILZ S I I J9A365 S I JCI9GI S S I S Dragendorff JCPDEV S I SI JKTQXD S I SI I JM4L8J I I JNKRGL I I I JQGKRH SI JVAW1W S I JYYOJY S S I S Negm's Test K2KJIK I I SI I KTL2KK S S I KUOOIY S S I I I KZRYK5 SI L0SOSG S S S I I LC00BZ S S I I Duquenois MMNPPT S S I I S Simon's MWSMPP S S S I I I DRX N9Y5J4 SI I NRHUYD I SI NT6XKR I SI O37CO6 SI O77FQX S S S I O888FC SI OASBL3 I SI

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 OKGKFC S I S Stereomicroscope OMOLC6 I I OOCWTO S S I I S micro/macroscopic ORPW0X S I I I I P7FEGC I SI P7XJWM SI PAMP84 I SI PCZ8NU S I PKIAAH SI PMCINM S I PMVPBP I I SI I PRYEOG I S I I PVVVKJ S S S I QHD076 I S I QQCQAQ SI I QYQLQW S I I R7RR6M I SI I REHHTU I I SI RILD6I SI RMBHBW I I SI I RNTT7L S S SI I RTRIO9 I S RTTTXL S I I S Janovsky RWTRU8 I SI I SEJFEA I I I I I S SIF50H I SI SYIONF S S I S SI T6MTE2 I SI T777GE S S I I I T8ZTTT I I S TCEWUO I SI TFB6JZ S S S I TFXAMC S I TKVKOB S I TTGC6K SI TVETMT S I I TWPVRD S S I

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 U7IBAC I UBNBHN SI I UFPUBG S S S I I I UMRFHI S S S I UWUGNF SI I I XRD V8EXVQ S S S I I S Simon test V8U885 S I SI SI VFTM1K S S I I VP4FPK S SI VRAJLX S I VVNYVV S I I VWWXW I I SI GCMSMS-TOFMS- B LCCDD WARWW S I C WM44EE SI WN364S S S S I WNUDTF S I WRGTRP SI WS6KSK S S S I WZDE4O I XJRFNX S S SI I XKKFPL SI I I I I XQOBO8 SI I SI I XS9KCX SI S S I I I XSESED S S S I I XVXMYY S S I I Raman XWWGW S S I W XYECSA SI I YAFCMU S I YD88F8 SI S S I YMBZHZ SI YRARMC I SI I YRVPY5 SI YSEXJD I YU1911 S I ZECZ6W S S I I S Duquenois Levine ZWYPLA SI I

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

11. ANNEX 2: Participants’ results for Test Sample-2 Identified substances for Test Sample 2

Code Identified Substances 07HEEE Cocaine 0V0005 Cocaine 1D31A3 Cocaine 1UDDLA Cocaine, levamisole 22M222 cocaína 2VY888 cocaine 3CAJ33 cocaine 3CW3T3 cocaine 3DB3YF Cocaine 3MBOO3 Cocaine 3VAS7U cocaine 3ZZ7LZ cocaine 43BPPC cocaine 4CCTQB Cocaine 4TZWAV cocaine 5BQYQN Cocaine 5JIQGU Cocaine 78PEHN Tetraimidazole 8K8OSH COCAINE 8TDKSP Cocaine 8X8488 cocaine 9FSJAA COCAIN 9L9I9M cocaine 9PLW9Q Cocaine 9POVHQ cocain hcl+ base 9X9XK9 cocaine HCl 9YIBLY Cocaine Hydrochloride A33M3R Cocaine A99LH9 Cocaine AMOGGG Cocaine AR7S7W Cocaine HCL ATVQQJ Cocaine AVRBSE Cocain B6QWQM Cocaine BFQULP cocaine BG2SLB cocaine BNQNNV Cocaine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances BRJPLX Cocaine, Levamisole (PDL in Canada) BSUUJE Cocaine BTUABB cocaine BVQYTQ Cocaine BYLJA9 cocaine CABMNN cocaïne CBRWNZ Cocaine CCORYM Cocaine CSFZJZ cocaíne DBHUHY Cocaine DGUTVL Cocaine DMMMMG COCAINE DQQX66 Cocaine DUEWAQ Cocaine EGNF7G COCAINE EIECD7 cocaine EQNEIU Cocaine ETRYEE Cocaine F3HS08 cocaine FAHHM9 Cocaine Hydrochloride FBIONY Cocaine FBOH8T Cocaine FTFGF7 Cocaine FWRG58 Cocaine G4IK4G Cocaine G5GNGG cocaine GBACTG COCAINE GIG3NC Cocaine GKGVZX Cocaine GNGGG8 Cocaine, Levamisole (PDL in Canada) GSHGOF cocaine GWFSGI cocaine H1111A cocaine hydrochloride, tropacocaine HFYHFD cocaine HLHPRH cocaine HMKGFH cocaine HOOOOO Cocaine and levamisol HOU5IO Cocaine HZRLLL Cocaine I35533 Cocaine and other coca products I77IF7 cocaine IK4RMW Cocaine ICE 2020/1-SM Copyright © 2021 UNODC Page 48 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances IKISEG cocaine IQLV57 Cocaine IZMILZ cocaine J9A365 COCAINE JCI9GI Cocaine JCPDEV COCAINE JKTQXD cocaine JM4L8J Cocaine JNKRGL Cocaine JQGKRH Cocaine JVAW1W Cocaine JYYOJY Cocaine K2KJIK Cocaine KTL2KK Cocaine KUOOIY Cocaine HCl KZRYK5 cocaine L0SOSG Cocaine LC00BZ Cocaine MMNPPT Cocaine Hydrochloride MWSMPP COCAINE N9Y5J4 Cocaine NRHUYD COCAINE 47.6% NT6XKR Cocaine O37CO6 Cocaine O77FQX Cocaine O888FC Cocaine OASBL3 Cocaine, Levamisole OKGKFC Cocaine OMOLC6 Cocaine OOCWTO Cocaine ORPW0X Cocaine P7FEGC cocaine P7XJWM COCAIN PCZ8NU Cocaine PKIAAH Cocaine PMCINM COCAINE PMVPBP Cocaine PRYEOG Cocaine, Levamisole (PDL in Canada) PVVVKJ cocaine QHD076 Cocaine QQCQAQ cocaïne QYQLQW Cocaine ICE 2020/1-SM Copyright © 2021 UNODC Page 49 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances R7RR6M COCAINE REHHTU COCAINE RILD6I Cocaine, Levamisole RMBHBW Cocaine 48.35% RNTT7L Cocaine RTTTXL Cocaine RWTRU8 Cocaine SEJFEA Cocaine SIF50H cocaine SYIONF Cocaine T6MTE2 cocain T777GE cocaine T8ZTTT cocaine TCEWUO cocaine TFB6JZ Cocaine TFXAMC Cocaine and Levamisole TKVKOB Cocaine TTGC6K COCAINE TVETMT COCAINA TWPVRD Cocaine U7IBAC Cocaine UBNBHN Cocain UFPUBG Cocaine UMRFHI Cocaine UWUGNF Cocaine HCl V8EXVQ Cocaine V8U885 cocain VFTM1K Cocaine VP4FPK Cocaine, Levamisole (PDL in Canada) VRAJLX Cocaine HCl VVNYVV COCAINE 49,2% VWWXWB cocaine WARWWC Cocaine, Epinephrine WM44EE COCAINE WN364S Cocaine WNUDTF COCAINA WRGTRP cocaine WS6KSK Cocaine WZDE4O cocaine XJRFNX COCAINE XKKFPL Cocaina XQOBO8 cocaine ICE 2020/1-SM Copyright © 2021 UNODC Page 50 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances XS9KCX Cocaine XSESED Cocaine XVXMYY cocaine XWWGWW Cocaine XYECSA Cocaine YAFCMU Cocaine YD88F8 cocaina YMBZHZ Cocaine YRARMC Cocaine YRVPY5 Cocaine YSEXJD Cocain YU1911 Cocaine ZECZ6W Cocaine ZWYPLA cocaine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Statement of findings for Test Sample 2

Code Cocaine 07HEEE +

0V0005 + Cocaine is controlled under Malaysian Dangerous Drugs Act 1952. 1D31A3 + Levamisole, Methylecgonine and Benzoylecgonine 1UDDLA + The sample was analysed with FTIR and GCMS in two different solvents 22M222 + Adulterantes: levamisol 2VY888 +

3CAJ33 +

3CW3T3 +

3DB3YF + Sample was found to contain Cocaine, with a W:W % purity of 48%. The sample also contained Levamisole. 3MBOO3 + The sample contains Cocaine. The concentration has not been determined. 3VAS7U +

3ZZ7LZ +

43BPPC + SM-2 was prepared from a seizure containing 54.1%(w/w) cocaine base.The test sample also contained lactose. 4CCTQB + it also includes tetramisole 4TZWAV + cocaine was detected by GC/MS, confirmed by FTIR and quantified by GC/FID 5BQYQN + It also contains Levamisole 5JIQGU + The sample analyzed contains Cocaine and Levamisole 78PEHN +

8K8OSH +

8TDKSP + On chemical analysis of a representative sample of the powder cocaine was detected with a purity of approximately 44% (calculated as base).

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine 8X8488 + levamisole 9FSJAA + COCAIN + LEVAMISOL 9L9I9M + the test sample also contained Levamisole 9PLW9Q + 0.224g of powder containing 48% Cocaine. Cocaine is a Class A controlled drug subject to the provisions of the Misuse of Drugs Act 1971. 9POVHQ + levamisole 9X9XK9 + 49,88 % (w/w) cocaine base, the sample also contained methylecgonidin, levamisol hydrochlorid 9YIBLY + Sample 2020/1/SM-2 was found to contain 52% cocaine hydrochloride (46% as cocaine base), together with levamisole. A33M3R + Examination and analyses performed on the white solid in SM-2 showed it to contain cocaine ( a central stimulant). A99LH9 + Sample 2020/1/SM-2 was found to contain cocaine. AMOGGG + Cocaine and phenyltetrahydroimidazothiazole confirmed in the composite. AR7S7W + Cocaine HCL; Levamisole ATVQQJ + Cocaine 47.3 % and levamisole, ecgonidine-metyl-ester AVRBSE + Sample contained cocaine as hydrochloride and levamisole. Identification of cocaine by FTIR and GC/MS, quantification by GC/FID. Identification of levamisole by GC/MS. B6QWQM + In addition to cocaine, this sample also contains levamisole. BFQULP + Sample 2020/1/SM-2 a white powder gave a positive result for cocaine ,substance under national legislation on drugs. BG2SLB + this sample is cocaine BNQNNV + This sample is adulterated with levamisole. BRJPLX + That I examined and analysed the said sample and found to contain: controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonine) calculated as the base 51%(w/w. The following substances (s) from the Prescription Drug List of the Food and Drug Regulations has (have) been detected but not certified : Levamisole or its salts. Should you need this (these) detected substance(s) to be certified, please contact us. BSUUJE + Cocaine was found in sample 2020/1/SM-2. Levamisole was also found.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine BTUABB + the white powder contains cocaine (52.27% w/w) which is controlled by national law BVQYTQ + The sample was found to contain 48.3% of cocaine (as base). BYLJA9 + levamisole,benzoylecgonine,transcinnamoylococaine,methylecgonine,norcaine CABMNN + cocaine + levamisole CBRWNZ + Based on the above analysis, the sample was found to contain Cocaine. CCORYM + Substance usually detected in our laboratory CSFZJZ + cocaíne and levamisole powder DBHUHY + ./. DGUTVL + Cocaine+Levamisole DMMMMG + SM 2 contains cocaine. DQQX66 + Cocaine and Levamisole DUEWAQ + Gov.Decision No. 1088/2004 Schedule.2 List 1 EGNF7G + The sample SM2 is a mix of COCAINE, LEVAMISOL, TROPACOCAINE and METHYLECGONIDINE. EIECD7 + the sample contains a scheduled substance EQNEIU + Retention time of cocaine was 18.108 min. The concentration of the sample injected in GC/MS was 115 ppm. ETRYEE +

F3HS08 + One glass bottle containing 0.22 grammes of a solid containing 0.11 grammes of heroin. FAHHM9 + Item 2020/1/SM-2 contained a white powder which contained cocaine hydrochloride, together with levamisole. Cocaine Hydrochloride is a Class A controlled drugs under the provisions of the Misuse of Drugs Act 1971 (as amended). Levamisole is not controlled under this legislation. FBIONY + The sample No. 2020/1/SM2 was found cocaine and levamisole FBOH8T + Mass spectrometry profile correlation between sample and reference material certified FTFGF7 +

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine FWRG58 +

G4IK4G + In the test sample 2020/1/SM-2 was detected cocaine and levamisole. G5GNGG + cocaine,lactose GBACTG + Sample 2020/1/SM-2 consists of white powder. Cocaine, a prohibited substance included in the National Law for Narcotics, is found to be present in this sample. GIG3NC +

GKGVZX + İt also includes Tropaicocaine, Levamisole and Norcocaine GNGGG8 + That I examined and analysed the said sample and found to contain: controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonine) calculated as the hydrochloride 49%(w/w). That I examined and analysed the said sample and found to contain: The following substances (s) from the Prescription Drug List of the Food and Drug Regulations has (have) been detected but not certified : Levamisole or its salts. Should you need this (these) detected substance(s) to be certified, please contact us. GSHGOF + cocaine is controlled by the law of 7th February 2014 and regulated by the RD of 6th September 2017 GWFSGI + white powder containing 48.78 %(w/w) cocaine and levamisole not quantified H1111A + Sample also contain: levamisol hydrochloride, sodium bicarbonate. HFYHFD + - HLHPRH + The sample contains 48.4±2.4 weight% cocaine-base. The sample also contains levamisole and/or its stereoisomer. HMKGFH + contains levamisole HOOOOO + The analysis detected cocaine and levamisol, using Gas Chromatography/Mass Spectrometry and Fourier Transform Infrared Spectrometry. HOU5IO + The sample contains Cocaine. HZRLLL +

I35533 + Test sample 2020/1/SM2 having gross weight 05.96 grams of white powder in amber glass bottle contains cocaine and other coca products namely anhydroecgonine methyl ester, ecgonine methyl ester, tropacocaine, norcocaine, cinnamoyl cocaine and benzoyl ecgonine. Moreover, levamisole ( a non-controlled substance) is also detected. I77IF7 + In het powder cocaïne and levamisole (adulterant) are present

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine IK4RMW + the above drug was detected in the preliminary screening and the analytical techniques used. IKISEG +

IQLV57 + It has been detected the presence of cocaine in the sample. IZMILZ +

J9A365 + LEVAMISOLE JCI9GI + The chemical tests and the coincidence on the retention time and mass fragmentogram with the reference material in the same conditions that the analyzed samples indicates the cocaine and levamisole presence. JCPDEV + ALSO FOUNDED LEVAMISOL JKTQXD + in traces levamisole JM4L8J + Powder contains Cocaine with indications of Levamisole (Tetramisole). Cocaine is a controlled drug under the Misuse of Drugs Acts, 1977 to 2016. JNKRGL + The sample contains cocaine.The amount of cocaine is determined to 48% (as cocaine base). Cocaine is a controlled substance. JQGKRH + Powder containing cocaine, additionally identified levamisole. JVAW1W + Sample was found containing Cocaine and Levamisole JYYOJY + From screening test by using (CT) and from confirmation test by (GC-MS and LC-MS- MS), the sample found to contain the controlled drug (Cocaine) K2KJIK + Levamisole KTL2KK + The powder was found to contain cocaine at a concentration of 47%. Cocaine is controlled under the Misuse of Drugs act 1971 (as amended) as a class A drug. Levamisole was also detected. KUOOIY Levamisole+ is not controlled under the Misuse of Drugs Act 1971 (as amended). Cocaine as base 50.70% KZRYK5 + test sample contained 47.2% cocaine and caffeine L0SOSG + The sample contained cocaine LC00BZ + Cocaine was identified in the sample 2020/1/SM2.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine MMNPPT + One brown glass vial with black screw cap labelled "2020/1/SM-2 240" containing 227 milligrams of white powder. This powder was found to contain Cocaine Hydrochloride at a purity of 55%. This is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended). MWSMPP +

N9Y5J4 + Levamisole NRHUYD + levamisol NT6XKR + Also found: Benzoylecgonine and tetramisole O37CO6 + 48.10% cocaine + levamisole O77FQX + List I of the Single Convention of 1961 O888FC + Cocaine and Tetramisole was detected OASBL3 + White powder analysed by GC/MS was found to contain Cocaine & Levamisole. Mass spectras were similar to CRM. OKGKFC + Sample 2020/1/SM-2 found to contain Cocaine and Tetramisole. OMOLC6 + The sample contains cocaine which is listed as a controlled drug according to french order, appendix I of February 22nd 1990. OOCWTO + A brown glass vial labelled 2020/1/SM-2 containing 0.22g of white powder. A portion was analysed and found to contain cocaine at a purity of 50%, together with tetramisole. ORPW0X + In the sample 2 there is cocaine P7FEGC + cocaine, levamisole P7XJWM + LEVAMISOLE, METHYLECGONIDINE, ECGONINE METHYLESTER, TROPACOCAINE, CINNAMOYLCOCAINE, BENZOYLECGONINE PAMP84 + Levamisole PCZ8NU + Sample 2020/1/SM-2 found to contain Cocaine PKIAAH + Cocaine and levamisole/tetramisole were identified PMCINM + The test sample contained LEVAMISOLE PMVPBP + Levamisole, Tropacocaine and Ecgonine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine PRYEOG + That I examined and analysed the said sample and found to contain: controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonine) calculated as the hydrochloride 54%(w/w). The following substances (s) from the Prescription Drug List of the Food and Drug Regulations has (have) been detected but not certified : Levamisole or its salts. Should you need this (these) detected substance(s) to be certified, please contact us PVVVKJ + the sample contains cocaine at 48.3 % purity and tetramisole QHD076 + Cocaine and levamisol were detected in SM-2 sample. QQCQAQ + cocaïne is sheduled as illicit drug in France QYQLQW + Whitish powder of SM-2 contains Cocaine. R7RR6M + levamisole REHHTU + White powder containing cocaine and levamisole. RILD6I + The sample is Cocaine Hyrochloride salt of a purity 47.8 as base. Cocaine is a schedule I, drug substance. RMBHBW + Levamisole RNTT7L + Presence of cocaine is detected with caffeine diluents. RTRIO9 +

RTTTXL + Cocaine is listed in the First Schedule of Dangerous Drug Act 1952 RWTRU8 +

SEJFEA + Mixture of cocaine (approx. 50 %) with levamisole and natural accompanying substances - cinnamoylcocaine and benzoylecgonine. SIF50H +

SYIONF + The sample contains the substance Cocaine. T6MTE2 +

T777GE + The sample contains cocaine, levamisole. T8ZTTT + white powder containing cocaine and levamisole TCEWUO + white powder containing 44.1% w/w of cocaine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine TFB6JZ + Cocaina and levamisol were founded in sample TFXAMC + We would not typically report Levamisole in a sample containing Cocaine, so our statement would read: “The above item was found to contain a glass vial with a lid, containing a quantity of white powder. The powder, which weighed 0.23 grams, was analysed and found to contain Cocaine. A portion of the powder was further analysed and found to contain not less than 47% Cocaine, by weight.” TKVKOB + The ICE sample 2020/1 SM2 was found to contain Cocaine. TTGC6K + COCAINE LEVAMISOLE TVETMT +

TWPVRD + This sample was found to contain Cocaine which is a Class A controlled substance under the Misuse of Drugs Act 1971. This sample was also found to contain Tetramisole, which is not controlled under the Misuse of Drugs Act 1971 U7IBAC +

UBNBHN + Levamisol also identified UFPUBG + Sample 2020/1/SM-2 contains Cocaine, Levamisole and Cocaine derivates as minor components, such as Anhydroecgonine methyl ester, Ecgonine methyl ester, Tropacocaine and Cynnamoilcocaine Cis/Trans Isomers. Cocaine base concentration is 44.6% UMRFHI + Retention time and fragmentation patterns obtained with samples are equivalent to those obtained with cocaine and levamisol. UWUGNF + Additionally it was identified levamisole, NaCl, Na2SO4. V8EXVQ + Lista I CU 1961 V8U885 + levamisole and/or stereoisomers VFTM1K + Ex#2; Cocaine mixed with Levamisol VP4FPK + No Certificate of Analyst issued, R&D laboratory VRAJLX + SM2 contains Cocaine and Levamisole withs 50.17% Cocaine base; the sample also contains ecgonine, methylecgonine and benzoylecgonine; VVNYVV + THE SAMPLE CONTAIN TETRAMISOLE VWWXWB + The sample contains cocaine (47.7% as free base), methylbenzoate, ecgonidine methyl ester, ecgonine methyl ester, levamisole.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine WARWWC + Sample tested positive for Cocaine using TLC and GC-MS WM44EE + LEVAMISOLE WN364S + It also contains Levamisole WNUDTF + LA MUESTRA 2 CONTIENE COCAINA Y LEVAMISL WRGTRP + Cocaine was detected by GC/MS and quantified by GC/FID. The sample contains also levamisole. WS6KSK + Cocaine 48% +/-4 WZDE4O +

XJRFNX + White powder that contains controlled drug COCAINE. XKKFPL + Levamisol XQOBO8 + 47% amount of Cocaine is found with the help of quantitative methods of GC-MS. Also, we have observed that Levamisole is present. XS9KCX +

XSESED + 2020/1/SM-2 contains Cocaine, a dangerous drug. It also contains Levamisole. XVXMYY + SM-2 was found to contain cocaine. Also contain tetramisole. XWWGWW + Cocaine is listed in the First Schedule of The Dangerous Drugs Acts 1952. Tetramisole (Levamisole) was also detected in SM-2 XYECSA + Cocaine was detected in the SM-2 sample. YAFCMU + Tetramisole YD88F8 +

YMBZHZ + No CofA issued, R&D laboratory YRARMC + The samples 2020/1/SM-2 contains Cocaine detected by GC/MS and FTIR. The percentage by weight of Cocaine is 46.5%. YRVPY5 + Controlled drug, cocaine, present in sample. Concentration approx 47%. Other substance found is tetramisol (no controlled drug). YSEXJD + It contains cocain at 48.3%. In addition, it contains levamisole.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Cocaine YU1911 + 2020/1/SM-2 was confirmed for Cocaine which is a Schedule II controlled substance in the US. ZECZ6W +

ZWYPLA + tetramisol

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Identification methods for Test Sample 2

Legend: S ... used for Screening I ... used for Identification SI ... used for both

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 ATVQQJ S S S I AVRBSE I SI I B6QWQM S I I BFQULP S S S I I BG2SLB S I I BNQNNV S I I BRJPLX S I I BSUUJE SI BTUABB I S BVQYTQ I SI BYLJA9 I SI CABMNN I S CBRWNZ S I CCORYM S S S S I CSFZJZ I SI DBHUHY SI SI DGUTVL I SI I DMMMM S I I I HPLC/RID G DQQX66 S I DUEWAQ S S I I I Fast Blue EGNF7G SI S SI I I S IMMUNOCHROMA- TOGRAP HY EIECD7 I I EQNEIU S I ETRYEE SI S I I I F3HS08 S S I SI I FAHHM9 S S SI I S Simons Reagent FBIONY S I FBOH8T SI I FTFGF7 S S S I I FWRG58 I SI G4IK4G I G5GNGG SI SI SI I SI I I GBACTG S S I GIG3NC SI GKGVZX S S S I I GNGGG8 S I I

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 GSHGOF I SI GWFSGI I I SI H1111A S I I I HFYHFD SI HLHPRH S I SI I HMKGFH S I SI I HOOOOO S S S I I I HOU5IO SI I HZRLLL I S I35533 S S SI I I77IF7 I SI IK4RMW I I S GC-MS/MS IKISEG S S I I IQLV57 SI S I IZMILZ S I I J9A365 S I JCI9GI S S I S Dragendorff JCPDEV S I SI JKTQXD S I SI I JM4L8J I I JNKRGL I I I JQGKRH SI JVAW1W S I JYYOJY S S I S Negm's Test K2KJIK I I SI I KTL2KK S S I KUOOIY S S I I I KZRYK5 SI L0SOSG S S S I I LC00BZ S S I I Duquenois MMNPPT S S I I S Simon's MWSMPP S S S I I I DRX N9Y5J4 SI I NRHUYD I SI NT6XKR I SI O37CO6 SI O77FQX S S S I

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 O888FC SI OASBL3 I SI OKGKFC S I S Stereomicroscope OMOLC6 I I OOCWTO S S I I S micro/macroscopic ORPW0X S I I I I P7FEGC I SI P7XJWM SI PAMP84 I SI PCZ8NU S I PKIAAH SI PMCINM S I PMVPBP I I SI I PRYEOG I S I I PVVVKJ S S S I QHD076 I S I QQCQAQ SI I QYQLQW S I I R7RR6M I SI I REHHTU I I SI RILD6I SI RMBHBW I I SI I RNTT7L S S SI I RTRIO9 I S RTTTXL S I I S Janovsky RWTRU8 I SI I SEJFEA I I I I I S SIF50H I SI SYIONF S S I S SI T6MTE2 I SI T777GE S S I I I T8ZTTT I I S TCEWUO I SI TFB6JZ S S S I TFXAMC S I TKVKOB S I TTGC6K SI

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 TVETMT S I I TWPVRD S S I U7IBAC I UBNBHN SI I UFPUBG S S S I I I UMRFHI S S S I UWUGNF SI I I XRD V8EXVQ S S S I I S Simon test V8U885 S I SI SI VFTM1K S S I I VP4FPK S SI VRAJLX S I VVNYVV S I I VWWXW I I SI GCMSMS-TOFMS- B LCCDD WARWW S I C WM44EE SI WN364S S S S I WNUDTF S I WRGTRP SI WS6KSK S S S I WZDE4O I XJRFNX S S SI I XKKFPL SI I I I I XQOBO8 SI I SI I XS9KCX SI S S I I I XSESED S S S I I XVXMYY S S I I Raman XWWGW S S I W XYECSA SI I YAFCMU S I YD88F8 SI S S I YMBZHZ SI YRARMC I SI I YRVPY5 SI YSEXJD I YU1911 S I

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 ZECZ6W S S I I S Duquenois Levine ZWYPLA SI I

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

12. ANNEX 3: Participants’ results for Test Sample-3 Identified substances for Test Sample 3

Code Identified Substances 0V0005 Caffeine 1UDDLA Caffeine (trace), oleamide (trace) 3CW3T3 caffeine (in Brazil caffeine isn´t considered a drug, but a adulterant) 3DB3YF None 3MBOO3 nihil 43BPPC caffeine 4CCTQB Caffeine 4TZWAV -- 8K8OSH CAFFEINE 9L9I9M caffeine 9PLW9Q No controlled drugs 9X9XK9 no A33M3R caffeine A99LH9 Caffeine ATVQQJ none B6QWQM In this sample has not been identified any drug. BNQNNV none BTUABB -- DGUTVL Caffeine DUEWAQ - EGNF7G CAFFEINE EQNEIU Caffein FTFGF7 Caffeine G5GNGG - GKGVZX Caffeine GWFSGI -- HFYHFD - HZRLLL Caffeine IK4RMW Caffeine JCPDEV CAFFEINE JM4L8J Caffeine KUOOIY None O37CO6 None OASBL3 Caffeine OOCWTO N/A ORPW0X no drug in the sample P7FEGC --

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances PCZ8NU Caffeine QHD076 Caffeine QQCQAQ no drug QYQLQW No drugs found RILD6I Caffeine RMBHBW Caffeine T777GE - T8ZTTT -- TCEWUO -- TFXAMC Caffeine and indicated the presence of Theobromine TKVKOB NIL TVETMT CAFEINA TWPVRD Caffeine V8EXVQ Caffeine VFTM1K No controlled substances VRAJLX - WARWWC Not applicable WM44EE CAFFEINE WNUDTF CAFEINA WRGTRP -- WZDE4O THC XJRFNX NONE XS9KCX Caffeine XSESED None XVXMYY caffeine XWWGWW Caffeine XYECSA None YRARMC Caffeine YU1911 Caffeine ZECZ6W Caffein

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Statement of findings for Test Sample 3

Code Caffeine 07HEEE + Caféine 0V0005 + Caffeine is controlled under Malaysian Poison Act 1952.

1D31A3 + Caffeine 1UDDLA + The sample was analysed with GCMS in two different solvents 22M222 -

2VY888 + cafeine 3CAJ33 +

3CW3T3 +

3DB3YF + Sample was negative for scheduled substances.The sample also contained Caffeine 3MBOO3 + The sample contains caffeine and theobromine. No drugs have been detected. 3VAS7U +

3ZZ7LZ +

43BPPC + SM-3 was prepared from a seizure containing caffeine and Theobromine. 4CCTQB + İt inculudes caffeine 4TZWAV - no compounds were detected by GC/MS 5BQYQN + It contains cafeine 5JIQGU - The sample analyzed does not contain substances subject to control. 78PEHN +

8K8OSH +

8TDKSP + A representative sample of the powder was analysed in order to detect the presence of a range of controlled drugs; however none were detected. Caffeine was detected within the powder.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine 8X8488 + caffeine 9FSJAA - TRACES OF CAFFEINE 9L9I9M + the test sample also contained theobromine and dietyl phthalate 9PLW9Q + 0.227g of green herbal material. No controlled substances were detected. 9POVHQ + caffein theobromin 9X9XK9 + plant material containing caffeine 9YIBLY + Sample 2020/1/SM-3 was found to contain no cotnrolled drugs, however, it was found to contain caffeine. A33M3R + Examination and analyses performed on the green solid in SM-3 showed it to contain caffeine ( a xanthine stimulant). A99LH9 + Sample 2020/1/SM-3 was found to contain caffeine. AMOGGG + Caffeine confirmed in the composite. AR7S7W - Negative. Ran two GCMS samples, both negative. ATVQQJ -

AVRBSE + Sample contained small amounts of caffeine. B6QWQM + Has been detected the presence of caffeine. BFQULP + Sample 2020/1/SM-3 a plant material, gave a negative result for substance under national legislation on drugs. BG2SLB + this sample contains caffeine BNQNNV + This sample might contain caffeine. BRJPLX + That I examined and analysed the said sample and found to contain: The following non- controlled substances (s) has (have) been detected but not certified : Caffeine, Should you need this (these) detected substance(s) to be certified, please contact us. BSUUJE - In sample 2020/1/SM-3 is not was found drugs. BTUABB + the green-brown powder contains caffeine BVQYTQ + The sample was analysed and no common controlled drug was detected.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine BYLJA9 + caffeine CABMNN + cafein CBRWNZ + Based on the above analysis, the sample was found to contain Caffeine. CCORYM + Herbal matrix with cafeine CSFZJZ + caffeine DBHUHY + ./. DGUTVL + Caffeine DMMMMG + SM3 contains caféine DQQX66 + Caffeine. DUEWAQ ANP

EGNF7G + The sample SM3 is CAFFEINE. EIECD7 + the sample does not contain any scheduled substance EQNEIU + Retention time of caffein was 14.587 min. The concentration of the sample injected in GC/MS was 1680.5 ppm. ETRYEE + Caffeine was determined F3HS08 + One glass bottle containing 0.22 grammes of a solid which did not contain any controlled substance. FAHHM9 + Item 2020/1/SM-3 contained a green herbal material that was analysed for the presence of controlled drugs with negative results. The herbal material was found to contain caffeine, detected at a low level. Caffeine is not controlled under the provisions of the Misuse of Drugs Act (as amended). FBIONY + The sample No. 2020/1/SM3 was found caffeine FBOH8T +

FTFGF7 + it is not contain drugs FWRG58 + Caffeine G4IK4G + In the test sample 2020/1/SM-3 was detected caffeine and theobromine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine G5GNGG + caffeine GBACTG - Sample 2020/1/SM-3 consists of dried herbal material. No prohibited substances are detected in this sample. GIG3NC -

GKGVZX +

GNGGG8 + That I examined and analysed the said sample and found to contain: The following non- controlled substances (s) has (have) been detected but not certified : Caffeine, Should you need this (these) detected substance(s) to be certified, please contact us. GSHGOF + no drugs found only low amount of caffeine detected GWFSGI - heterogeneous material composed of parts of plants H1111A + Sample contain: caffeine and theobromine. HFYHFD + - HLHPRH + The sample contains caffeine. HMKGFH + contains coffeine HOOOOO - The analysis didn´t detected any drugs, using Gas Chromatography/Mass Spectrometry and HOU5IO Fourier Transform+ Infrared Spectrometry. The sample contains Caffeine. HZRLLL +

I35533 + Test sample 2020/1/SM3 having gross weight 05.97 grams of crushed dried green plant material in amber glass bottle contains No narcotic and psychotropic substance. However, caffeine ( a non- controlled substance) is confirmed. Moreover, theobromine (a non- controlled substance) is also detected. I77IF7 -

IK4RMW + The above drug was detected in the sample using the analytical techniques that is, GC- MS/MS and LC-MS/MS IKISEG +

IQLV57 +

IZMILZ +

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine J9A365 + LACTOSE JCI9GI + The chemical tests and the coincidence on the retention time and mass fragmentogram with the reference material in the same conditions that the analyzed samples indicates the caffeine presence. JCPDEV +

JKTQXD + Contains coffeine JM4L8J + Plant material contains caffeine. Caffeine is not a controlled drug. JNKRGL + With the methods applied, it is not identified any controlled substances in the sample. JQGKRH + plant material, identified caffeine. JVAW1W + Sample was found containing Caffeine JYYOJY +

K2KJIK + Caffeine KTL2KK + The material was found to contain caffeine. Caffeine is not controlled under the misuse of Drugs Act 1971 (as amended). KUOOIY + No Drug found. Contain Caffeine KZRYK5 -

L0SOSG + The sample contained caffeine LC00BZ - In sample 2020-1-SM3 no controlled substances were identified MMNPPT + One brown glass vial with black screw cap labelled "2020/1/SM-3 148" containing 224 milligrams of green herbal material. This material was found to contain caffeine which is not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended). MWSMPP +

N9Y5J4 + Caffeine NRHUYD + CAFFEINE NT6XKR ANP

O37CO6 + Presence of caffein

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine O77FQX +

O888FC + Caffeine was detected OASBL3 + Greenish vegetal material extracted & analysed by GC/MS was found to contain Caffeine. Mass spectra was similar to CRM. OKGKFC + Sample 2020/1/SM-3 found to contain Caffeine. OMOLC6 + The analysis did not reveal any controlled drug according to french order, decree of February 22nd 1990. OOCWTO + A brown glass vial labelled 2020/1/SM-3 containing 0.23g of green vegetable matter. A portion was analysed and found to contain caffeine. ORPW0X + There is no drug in the sample 3. P7FEGC - -- P7XJWM + TRACES OF CAFFEIN PAMP84 +

PCZ8NU + Sample 2020/1/Sm-3 found to contain Caffeine PKIAAH + only caffeine was identified PMCINM + The test sample contained CAFFEINE and THEOBROMINE PMVPBP + Caffeine PRYEOG + The following non-controlled substances(s) has(have) been detected but not certified: Caffeine, Theobromine Should you need this (these) detected substance(s) to be certified, please contact us. PVVVKJ + the sample containes only caffeine QHD076 + Caffeine was detected in SM-3 sample. QQCQAQ +

QYQLQW ANP Neither GC-MS nor TLC have detected drugs in the loose plant of SM-3 test sample. R7RR6M + caffeine REHHTU + Herbal material containing caffeine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine RILD6I + No controlled drug detected. RMBHBW +

RNTT7L + No controlled drug is found. Caffeine is detected. RTRIO9 -

RTTTXL + Caffeine is detected and listed in the First Schedule of Poison Act 1952 RWTRU8 +

SEJFEA + Plant material containing caffeine SIF50H ANP

SYIONF + The analysed sample does not contain controlled drugs. T6MTE2 -

T777GE + The sample contain caffeine T8ZTTT - plant material with characteristic smell without any controlled drug TCEWUO - greenish and fibrous substance not containing any controlled drug TFB6JZ + No controlled substances were detected, caffeine was detected in the plant sample TFXAMC + We would not typically report non-controlled substances in a sample of vegetable material, so our statement would read: “The above item was found to contain a glass vial with a lid, containing a quantity of chopped green vegetable material. The vegetable material, which weighed 0.22 grams, was analysed for the presence of controlled drugs, within the provisions of the Misuse of Drugs Act 1971, with a negative result.” TKVKOB ANP The ICE sample 2020/1 SM3 was found to contain no drug. TTGC6K + CAFFEINE TVETMT +

TWPVRD + This sample was found to contain Caffeine which is not controlled under the Misuse of Drugs Act 1971. U7IBAC +

UBNBHN +

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine UFPUBG + Sample 2020/1/SM-3 is plant material that contains Caffeine and Theobromine as main compounds. UMRFHI + Retention time and fragmentation patterns obtained with samples are equivalent to those obtained with Caffeine. UWUGNF - It was blank sample. V8EXVQ + Caffeine is not a controlled drug V8U885 + caffeine VFTM1K + Caffeine VP4FPK ANP

VRAJLX + SM3 contains Caffeine; VVNYVV -

VWWXWB + The sample doesn't contain any controlled drug. It contains only caffeine. WARWWC - No narcotic drug was detected WM44EE +

WN364S + Caffeine WNUDTF + LA MUESTRA 3 CONTIENE CAFEINA WRGTRP + the sample contains only caffeine WS6KSK + Caffeine WZDE4O - cannabinoids XJRFNX - Brown herbal material that contains no controlled substances. XKKFPL - cafeína? XQOBO8 + Caffeine is found during identification step. No drug is found. XS9KCX +

XSESED + 2020/1/SM-3 does not contain any dangerous drug. It contains Caffeine.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Caffeine XVXMYY + SM-3 was found to contain caffeine. XWWGWW + Caffeine detected in SM-3 XYECSA + No controlled drugs were found in the SM-3 sample. YAFCMU + Caffeine YD88F8 ANP

YMBZHZ ANP

YRARMC + The samples 2020/1/SM-3 contains Caffeine detected by GC/MS and FTIR. YRVPY5 + No substance controlled in legislation is found, caffeine was found (no controlled drug). YSEXJD + It contains a mixture of: fructose, coffein, glucose, inositol, sucrose, cafeic acid, palmitic acid, maleic acid, glicerol, sitosterol. YU1911 + 2020/1/SM-3 was confirmed for Caffeine which is not a controlled substance in the US. ZECZ6W + Tha sample does not contain illicit drugs ZWYPLA + caffeine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Identification methods for Test Sample 3

Legend: S ... used for Screening I ... used for Identification SI ... used for both

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 ZECZ6W S S I I S Duquenois Levine ZWYPLA SI I

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

13. ANNEX 4: Participants’ results for Test Sample-4 Identified substances for Test Sample 4

Code Identified Substances 07HEEE Metamphétamine 0V0005 Methamphetamine 1D31A3 Metamfetamine 1UDDLA Matanfetamine, lactose 22M222 metanfetamina 2VY888 methamphetamine 3CAJ33 methamphetamine 3CW3T3 Metamfetamine 3DB3YF Methamphetamine 3MBOO3 Metamfetamine 3VAS7U metamphetamine 3ZZ7LZ methamphetamine 43BPPC Metamfetamine 4CCTQB Methamphetamine 4TZWAV metamphetamine 5BQYQN Methamphetamine 5JIQGU Metanphetamine 8K8OSH METAMFETAMINE 8TDKSP Methylamphetamine 8X8488 metamfetamine 9FSJAA METAMFETAMIN 9L9I9M methamphetamine and lactose 9PLW9Q Methylamphetamine 9POVHQ methamphetamin hcl 9X9XK9 metamfetamine HCl 9YIBLY Methylamphetamine Hydrochloride A33M3R Methamphetamine, Mephedrone A99LH9 Metamfetamine AMOGGG Methamphetamine HCl AR7S7W Methylamphetamine ATVQQJ Methamphetamine AVRBSE Metamfetamine B6QWQM Methamphetamine BFQULP methamphetamine BG2SLB methamphetamine BNQNNV Methamphetamine BRJPLX Methamphetamine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances BTUABB methamphetamine BVQYTQ Methamphetamine BYLJA9 metamfetamine CABMNN metamfétamine CBRWNZ Methamphetamine CCORYM Metamphetamine CSFZJZ metamfetamine DBHUHY METAMFETAMINE DGUTVL Metamfetamine DMMMMG METAMFETAMINE DQQX66 Methamphetamine DUEWAQ methamphetamine EGNF7G METAMFETAMINE EIECD7 methamphetamine EQNEIU Metamfetamine ETRYEE Metamfetamine F3HS08 methamphetamine FAHHM9 Methamphetamine Hydrochloride FBIONY Metanphetamine FBOH8T Metamfetamine FTFGF7 Methampetamine FWRG58 Metamfetamine G4IK4G Methamphetamine G5GNGG methamphetamine GBACTG METAMFETAMINE GIG3NC Metamfetamine GKGVZX Methamphetamine GNGGG8 Methamphetamine GSHGOF methamphetamine GWFSGI metamphetamine H1111A methamphetamine hydrochloride HFYHFD metamfetamine HLHPRH metamfetamine HMKGFH methamphetamine HOOOOO Methamphetamine HOU5IO Metamphetamine HZRLLL Metamfetamine I35533 Methamphetamine I77IF7 metamphetamine IK4RMW Amphetamine, Metamphetamine, Caffeine IKISEG metamfetamine IQLV57 metamfetamine ICE 2020/1-SM Copyright © 2021 UNODC Page 86 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances IZMILZ metamfetamine J9A365 METANPHETAMINE JCI9GI Metanphetamine JCPDEV METAMPHETAMINE JKTQXD methamphetamine JM4L8J Methylamphetamine JNKRGL Methamphetamine JQGKRH Methamphetamine JVAW1W Methamphetamine JYYOJY Methamphetamine K2KJIK Metamfetamine KTL2KK Methylamphetamine KUOOIY Methamphetamine HCl KZRYK5 metamfetamine L0SOSG Methamphetamine LC00BZ Methamphetamine MMNPPT Methylamphetamine Hydrochloride MWSMPP METHAMPHETAMINE N9Y5J4 Metamfetamine NRHUYD METAMFETAMINE 20.6% NT6XKR Metamphetamine O37CO6 Methamphetamine O77FQX Methamphetamine O888FC Methamphetamine OASBL3 Metamfetamine OKGKFC Methamphetamine OMOLC6 Metamfetamine OOCWTO Methylamphetamine ORPW0X metamphetamine P7FEGC -- P7XJWM METAMPHETAMINE PCZ8NU Metamfetamine PKIAAH Methamfetamine PMCINM METHAMPHETAMINE PMVPBP Methamphetamine PRYEOG Methamphetamine PVVVKJ metanfetamine QHD076 Methamphetamine and lactose QQCQAQ méthamphétamine QYQLQW Methamphetamine R7RR6M METAMPHETAMINE REHHTU METHAMPHETAMINE ICE 2020/1-SM Copyright © 2021 UNODC Page 87 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances RILD6I Methamhetamine RMBHBW Metamfetamine 19.67% RNTT7L Methamphetamine RTTTXL Methamphetamine RWTRU8 methamphetamin SEJFEA Metamfetamine SIF50H metamfetamine SYIONF Metamfetamine T6MTE2 metamfetamine T777GE methamphetamine T8ZTTT methamphetamine TCEWUO metamfetamine TFB6JZ Methanphetamine TFXAMC Methylamphetamine (Metamphetamine) TKVKOB Metamfetamine. TTGC6K AMPHETAMINES TVETMT METANFETAMINA TWPVRD Methamphetamine U7IBAC Methanphetamine UBNBHN Methamfetamin UFPUBG Metamphetamine UMRFHI Metanphetamine UWUGNF Methamphetamine HCl V8EXVQ Metamfetamine V8U885 methamphetamine VFTM1K Methmphethamine VP4FPK Methamphetamine HCl VRAJLX Metamfetamine HCl VVNYVV THE SAMPLE CONTAINE METHAMPHETAMINE VWWXWB methamphetamine WARWWC Methamphetamine, epinephrine, Lactose WM44EE Metamfetamine WN364S Metamfetamine WNUDTF METANFETAMINA WRGTRP metamfetamine WS6KSK Metamphetamine WZDE4O methamphetamine XJRFNX METHAMPHETAMINE XKKFPL Metanfetamina XQOBO8 metamfetamine XS9KCX Methampfetamine XSESED Methamphetamine ICE 2020/1-SM Copyright © 2021 UNODC Page 88 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Identified Substances XVXMYY methamphetamine XWWGWW Methamphetamine XYECSA Metamfetamine YAFCMU Metanphetamine YD88F8 metanfetamina YMBZHZ Methamphetamine HCl YRARMC Metamfetamine，Lactose YRVPY5 Metamfetamine YSEXJD Methamphetamine YU1911 Methamphetamine ZECZ6W Metamfetamine ZWYPLA methamphetamine

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Statement of findings for Test Sample 4

Code Lactose Metamfetamine 07HEEE ANP +

0V0005 ANP + Methamphetamine is controlled under Malaysian Dangerous Drugs Act 1952. 1D31A3 + + Lactose 1UDDLA + + The sample was analysed with FTIR and GCMS in two different solvents 22M222 - +

2VY888 - +

3CAJ33 + +

3CW3T3 ANP +

3DB3YF ANP + Sample tested positive for Methamphetamine. 3MBOO3 + + The sample contains Metamfetamine. The concentration has not been determined. 3VAS7U + +

3ZZ7LZ + +

43BPPC + + SM-4 was prepared from a seizure containing 18.34%(w/w) Metamfetamine base.The test sample also contained lactose. 4CCTQB - + it includes only methamphetamine 4TZWAV + + methamphetamine was detected by GC/MS, confirmed by FTIR and quantified by GC/FID 5BQYQN ANP +

5JIQGU ANP + The sample analyzed contains Methamphetamine and lactose. 78PEHN + +

8K8OSH ANP +

8TDKSP ANP + On chemical analysis of a representative sample of the powder methylamphetamine was detected with a purity of approximately 19% (calculated as base). 8X8488 + + lactose ICE 2020/1-SM Copyright © 2021 UNODC Page 90 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Lactose Metamfetamine 9FSJAA ANP +

9L9I9M + +

9PLW9Q ANP + 0.229g of powder containing Methylamphetamine. Methylamphetamine is a Class A controlled drug subject to the provisions of the Misuse of Drugs Act 1971. 9POVHQ + + lactose 9X9XK9 + + 19,97 % (w/w) metamfetamine base, the sample also contained lactose 9YIBLY + + Sample 2020/1/SM-4 was found to contain 25% methylamphetamine hydrochloride (20% as methylamphetamine base), together with lactose. A33M3R + + Examination and analyses performed on the white solid in SM-4 showed it to contain methamphetamine ( a central stimulant) and mephedrone ( a synthetic stimulant). A99LH9 ANP + Sample 2020/1/SM-4 was found to contain 18.8% of metamfetamine. AMOGGG - + Methamphetamine confirmed in the composite. AR7S7W + + Methylamphetamine; Lactose ATVQQJ - +

AVRBSE + + Sample contained Metamfetamine as hydrochloride and lactose. B6QWQM + + This sample was found to contain methamphetamine and lactose. BFQULP ANP + Sample 2020/1/SM-4 a white powder gave a positive result for a methamphetamine, substance under national legislation on drugs. BG2SLB + + this sample is methamphetamine BNQNNV ANP +

BRJPLX ANP + That I examined and analysed the said sample and found to contain: controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 18. Methamphetamine BSUUJE (N,α-dimethylbenzeneethanamine)ANP - calculated as the hydrochloride 25% (w/w) In sample 2020/1/SM-4 is not was found drugs. BTUABB ANP + the white powder contains methamphetamine (21.4% w/w) which is controlled by law BVQYTQ ANP + The sample was found to contain 19.8% of methamphetamine (as base). BYLJA9 + + lactose

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Lactose Metamfetamine CABMNN - + metamfetamine + lactose CBRWNZ ANP + Based on the above analysis, the sample was found to contain Methamphetamine. CCORYM ANP + Not very usually detected substance in seized material which is analyzed in this laboratory CSFZJZ + + metamfetamine in lactose powder DBHUHY + + ./. DGUTVL + + Metamfetamine+Lactose DMMMMG + + SM4 contains METAMFETAMINE and LACTOSE. DQQX66 + + Methamphetamine and lactose DUEWAQ ANP + Gov.Decision Nr. 1088/2004 Schedule.2 List 2 EGNF7G + + The sample SM4 is a mix of METAMFETAMINE and LACTOSE. EIECD7 + + the sample contains a scheduled substance EQNEIU - + Retention time of metamfetamine was 5.990 min. The concentration of the sample injected in GC/MS was 118.5 ppm ETRYEE + +

F3HS08 + + One glass bottle containing 0.23 grammes of a solid containing 45 milligrammes of methamphetamine. FAHHM9 + + Item 2020/1/SM-4 contained a white powder which contained methylamphetamine hydrochloride, together with lactose. Methylamphetamine Hydrochloride is a Class A controlled drugs under the provisions of the Misuse of Drugs Act 1971 (as amended). Lactose is not controlled under this legislation. FBIONY ANP + The sample No. 2020/1/SM4 was found Metanphetamine FBOH8T + + Mass spectrometry profile correlation between sample and reference material certified FTFGF7 - + it includes only methampetamine drugs FWRG58 + + Lactose G4IK4G ANP + In the test sample 2020/1/SM-4 was detected methamphetamine G5GNGG + + methamphetamine, lactose

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Lactose Metamfetamine GBACTG ANP + Sample 2020/1/SM-4 consists of white powder. Metamfetamine, a prohibited substance included in the National Law for Narcotics, is found to be present in this sample. GIG3NC ANP +

GKGVZX - +

GNGGG8 ANP + That I examined and analysed the said sample and found to contain: controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 18. Methamphetamine GSHGOF (N,α-dimethylbenzeneethanamine)+ + calculated as the hydrochloride 22% (w/w) methamphetamine is controlled by the law of 7th February 2014 and regulated by the RD of 6th September 2017 GWFSGI + + white powder containing 16.68%(w/w) methamphetamine and lactose not quantified H1111A + + Sample also contain lactose. HFYHFD ANP + - HLHPRH + + The sample contains 19.7±1.2 weight% metamfetamine-base. The sample also contains lactose. HMKGFH + + contains lactose HOOOOO ANP + The analysis detected methamphetamine, using Gas Chromatography/Mass Spectrometry and Fourier Transform Infrared Spectrometry. HOU5IO + + The sample contains Metamphetamine and Lactose. HZRLLL ANP +

I35533 ANP + Test sample 2020/1/SM4 having gross weight 05.94 grams of white powder in amber glass bottle contains methamphetamine. I77IF7 ANP + In the powder metamphetamine is present IK4RMW - + The above drugs were detected on both screening (AMP, METH) and on analytical techniques for all of them. IKISEG + +

IQLV57 + + It has been detected the presence of metamphetamine in the sample. IZMILZ + +

J9A365 - +

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Lactose Metamfetamine JCI9GI ANP + The chemical tests and the coincidence on the retention time and mass fragmentogram with the reference material in the same conditions that the analyzed samples indicates the metanphetamine presence. JCPDEV - +

JKTQXD + + Also contains lactose JM4L8J - + Powder contains Methylamphetamine. Methylamphetamine is a controlled drugs under the Misuse of Drugs Acts, 1977 to 2016. JNKRGL + + The sample contains metamphetamine.The amount of metamphetaine is determined to 19% (as metamphetamin base). Metamphetamine is a controlled substance. JQGKRH ANP + powder containing methamphetamine. JVAW1W ANP + Sample was found containing Methamphetamine JYYOJY ANP + From screening test by using (MR) and from confirmation test by (GC-MS and LC-MS- MS), the sample found to contain the controlled drug (Methamphetamine) K2KJIK + + Lactose KTL2KK - + The power was found to contain Methylamphetamine. Methylamphetamine is controlled under the Misuse of Drugs Act 1971 (as amended) as a class A drug. KUOOIY + + Methamphetamine HCl as base 19.76% contain Lactose KZRYK5 ANP + test sample contained metamphetamine L0SOSG + + The sample contained 19.6 % (w/w) methamphetamine (base) and lactose LC00BZ ANP + Methamphetamine was identified in the sample 2020/1/SM4 MMNPPT + + One brown glass vial with black screw cap labelled "2020/1/SM-4 198" containing 229 milligrams of white powder. This powder was found to contain Methylamphetamine Hydrochloride at a purity of 24%. This is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended). MWSMPP + +

N9Y5J4 + + Lactose NRHUYD - +

NT6XKR ANP +

O37CO6 ANP + Presence of methamphetamine not quantified

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Lactose Metamfetamine O77FQX - + List II of the Convention on Psychotropic Substances of 1971 O888FC - + Methamphetamine was detected OASBL3 ANP + White powder analysed by GC/MS was found to contain Metamfetamine. Mass spectra was similar to CRM. OKGKFC ANP + Sample 2020/1/SM-4 found to contain Methamphetamine. OMOLC6 + + The sample contains metamfetamine which is listed as a controlled drug according to french order, appendix III of February 22nd 1990. OOCWTO + + A brown glass vial labelled 2020/1/SM-4 containing 0.23g of white powder. A portion was analysed and found to contain methylamphetamine, together with lactose. ORPW0X + + In the sample 4 thre is metamphetamine. P7FEGC + - lactose P7XJWM - +

PAMP84 + +

PCZ8NU ANP + Sample 2020/1/SM-4 found to contain Metamfetamine PKIAAH - + Methamfetamine was identified PMCINM ANP +

PMVPBP + + Lactose PRYEOG + + That I examined and analysed the said sample and found it to contain: controlled subsatnce(s) within the meaningof the Controlled Drugs and Substances Act: Schedule I 18. Methamphetamine (N,α-dimethylbenzeneethanamide calculated as the hydrochloride 22 % (w/w). PVVVKJ ANP + the sample containes metanfetamine at 21.2 % purity QHD076 + + Methamphetamine and lactose were detected in SM-4 sample. QQCQAQ + + méthamphétamine is sheduled as illicit drug in France QYQLQW ANP + Whitish powder of SM-4 contains Methamphetamine. R7RR6M + + lactose REHHTU ANP + White powder containing methamphetamine ICE 2020/1-SM Copyright © 2021 UNODC Page 95 of 104

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Lactose Metamfetamine RILD6I ANP + The sample is Methamphetamine hydrochloride salt of a purity 19.5%.Methamphetamine is a schedule I, drug substance. RMBHBW + + Lactose RNTT7L ANP + Along with the presence of caffeine, methamfetamine is detected. RTRIO9 ANP +

RTTTXL ANP + Methamphetamine is listed in the First Schedule of Dangerous Drug Act 1952 RWTRU8 + +

SEJFEA + + Mixture of metamfetamine with lactose (approx. 70 %). SIF50H ANP +

SYIONF - + The sample contains the substance Metamfetamine. T6MTE2 + +

T777GE + + The sample contains methamphetamine and lactose T8ZTTT + + white powder containing methamphetamine and lactose TCEWUO ANP + white powder containing 19.2%w/w of metamfetamine TFB6JZ ANP +

TFXAMC - + As we do not quant Methylamphetamine, our statement would read: “The above item was found to contain a glass vial with a lid, containing a quantity of fine white powder. The powder, which weighed 0.23 grams, was analysed and found to contain Methylamphetamine.” TKVKOB ANP + The ICE sample 2020/1 SM4 was found to contain Metamfetamine. TTGC6K ANP + METHAMPETHAMINE TVETMT - +

TWPVRD ANP + This sample was found to contain Methamphetamine which is a Class A controlled substance under the Misuse of Drugs Act 1971 U7IBAC ANP +

UBNBHN + +

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Lactose Metamfetamine UFPUBG + + Sample 2020/1/SM-4 contains Metamphetamine and Lactose. UMRFHI ANP + Retention time and fragmentation patterns obtained with samples are equivalent to those obtained with Metahphetamine. UWUGNF + + Additionally it was identified lactose. V8EXVQ ANP + Lista II C 1971 V8U885 + + lactose VFTM1K ANP +

VP4FPK ANP + No Certificate of Analyst issued, R&D laboratory VRAJLX + + SM4 contains Metamfetamine and Lactose with 20.15% Metamfetamine base; the sample also contains Linoleic acid; VVNYVV + + THE SAMPLE CONTAIN LACTOSE VWWXWB - + The sample contains methamphetamine (21.2% as free base). WARWWC + + Sample tested positive for methamphetamine rapid test strip, TLC and GC-MS WM44EE + + LACTOSE WN364S ANP +

WNUDTF ANP - LA MUESTRA 4 CONTIENE METANFETAMINA WRGTRP ANP + Metamfetamine was detected by GC/MS and quantified by LC/MS/MS WS6KSK - +

WZDE4O ANP +

XJRFNX ANP + White powder that contains controlled substance METHAMPHETAMINE. XKKFPL ANP + Phentermine XQOBO8 + + 19.2% amount of Metamfetamine is found with the help of quantitative methods of GC-MS. Also, we have observed that Lactose is present. XS9KCX - +

XSESED + + 2020/1/SM-4 contains Methamphetamine. It also contains Lactose.

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code Lactose Metamfetamine XVXMYY + + Sm-4 was found to contain methamphetamine. Also contain lactose. XWWGWW ANP + Methamphetamine is listed in the First Schedule of The Dangerous Drugs Acts 1952.

XYECSA ANP + Metamfetamine was detected in the SM-4 sample. YAFCMU - +

YD88F8 ANP +

YMBZHZ ANP + No CofA issued, R&D laboratory YRARMC + + The samples 2020/1/SM-4 contains Metamfetamine and Lactose detected by GC/MS and FTIR. The percentage by weight of Metamfetamine is 18.6%. YRVPY5 ANP + Controlled drug, Metamfetamine, present in sample. Concentration approx 19% YSEXJD + + It contains methamphetamine at 19.8%. In addition, it contains lactose, palmitic acid and stearic acid. YU1911 ANP + 2020/1/SM-4 was confirmed for Methamphetamine which is a Schedule II controlled substance in the US. ZECZ6W - +

ZWYPLA + + lactose

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Identification methods for Test Sample 4

Legend: S ... used for Screening I ... used for Identification SI ... used for both

International Collaborative Exercises (ICE) Summary report 2020/1-Seized Materials

Code 140 141 142 150 160 161 170 171 180 190 211 230 231 250 210 ZECZ6W S S I I S Duquenois Levine ZWYPLA SI I

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