FOOD AND BEVERAGE CHEMISTRY Proficiency Test List - EUR EUR

Jan 2021 - Mar 2022 2

FOOD & BEVERAGE CHEMISTRY PROFICIENCY TESTS The confidence in analytical data provided to producers can be enhanced through using proficiency testing. Proficiency testing (PT) provides evidence, from an independent source, regarding the competency of the laboratory supplying the analytical service. Important commercial and safety decisions are made on the results of laboratory analysis, so it pays to monitor performance to ensure you can rely on these results.

Our programme covers chemical analysis of real food samples for a wide range of target analytes including: nutritional components, additives, allergens, natural contaminants, and veterinary medicine residues, and packaging chemical migrants.

Quantity discounts (for materials purchased in a single order) excluding blank materials

Quantity Discount Applied Purchased 21 - 45 tests 5% 46 - 70 tests 10% 71 or more 20%

Courier 74€ / EU 79€ / Non-EU Courier 34€ / EU 50€ / Non-EU Express

Note: The information in this price list is designed to assist you in choosing proficiency tests to meet your needs. Whilst every care has been taken in producing this information, we do not guarantee its accuracy. The Fapas® website is the definitive source of information about our proficiency tests. Orders are subject to the Fapas® terms and conditions, which are available on our website. Please check the website before placing your order.

ALCOHOL

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (EUR) alcoholic strength (real and/or apparent), ethanal (acetaldehyde), ethyl acetate, 1398 Whisky methanol, propan-1-ol, 2- FCOH3-DRA10 200 ml 17/03/2021 363 methylpropan-1-ol & 2- methylbutan-1-ol + 3- methylbutan-1-ol (sum)

alcoholic strength, total SO2, 1399 Wine total acidity, volatile acidity and FCOH4-DRA13 220 ml 05/08/2021 373 wine quality indicators alcoholic strength (real and/or apparent), ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2- 13100 Brandy FCOH2-DRA4 200 ml 04/11/2021 373 methylpropan-1-ol, 2- methylbutan-1-ol + 3- methylbutan-1-ol (sum) & ethyl carbamate 3

Item Code Matrix Analytes Product Code Approx. Size Start Date alcoholic strength (real and/or apparent), ethanal (acetaldehyde), ethyl acetate, 13101 Whisky methanol, propan-1-ol, 2- FCOH3-DRA10 200 ml 09/03/2022 373 methylpropan-1-ol & 2- methylbutan-1-ol + 3- methylbutan-1-ol (sum) alcohol (ethanol) 3115 Beverage FCOH1-DRA2 3 x 200 ml 16/08/2021 308+74 Halal Compliance Check

ALLERGENS

Item Code Matrix Analytes Product Code Approx. Size Start Date Infant Soya 27285 milk (BLG) FCAL13-INF13 2 x 20 g 07/01/2021 295 Formula Infant Formula 27294 milk (BLG) FCAL13-INF20 2 x 20 g 15/01/2021 295 (Hydrolysed) 27286 Cooked Biscuit gluten, milk and egg FCAL7-PRO14 30 g 21/01/2021 377 27287 Chocolate peanut, peanut protein FCAL16-CON2 2 x 20 g 05/02/2021 295 Infant Soya 27288 milk (casein) & gluten FCAL15-INF13 2 x 20 g 18/02/2021 377 Formula 27289 Cumin gluten & sesame FCAL22-SPI8 2 x 20 g 26/02/2021 295 27290 Flour lupin FCAL12-CCP28 2 x 20 g 04/03/2021 295 27291 Cooked Biscuit hazelnut, peanut FCAL9-PRO14 50 g 12/03/2021 377 histamine (high level >50 27292 Canned Fish FCAL10-SEA7 145 g 25/03/2021 295 mg/kg) 27295 Wheat Flour soya, soya protein FCAL17-CCP49 2 x 20 g 09/04/2021 304 27296 Cake Mix egg, egg white protein FCAL5-PRO10 2 x 20 g 15/04/2021 304 27297 Garlic Powder peanut, peanut protein FCAL16-SPI10 2 x 20 g 29/04/2021 304 27298 Cake Mix gluten FCAL6-PRO10 2 x 20 g 07/05/2021 304 27299 Chocolate hazelnut, hazelnut protein FCAL8-CON2 2 x 20 g 20/05/2021 304 Instant Soup 27300 celery, mustard FCAL2-PRO27 2 x 20 g 04/06/2021 304 Powder Infant 27322 Breakfast milk (casein and BLG) FCAL21-INF6 2 x 20 g 16.06.2021 388 Cereal 27301 Cake Mix gluten, milk and egg FCAL7-PRO10 2 x 30 g 08/07/2021 388 Oat Based 27302 gluten FCAL6-CCP37 2 x 20 g 21/07/2021 304 Foodstuff histamine (low level, <50 27303 Canned Fish FCAL11-SEA7 145 g 06/08/2021 304 mg/kg) Infant Formula 27304 milk (casein and BLG) FCAL21-INF20 2 x 20 g 26/08/2021 304 (Hydrolysed) 27305 Chocolate almond, almond protein FCAL1-CON2 2 x 20 g 02/09/2021 304 27306 Wheat Flour soya, soya protein FCAL17-CCP49 2 x 20 g 23/09/2021 304 27307 Jam sulphites FCAL18-CON7 80 g 28/09/2021 304+74 27308 Beer gluten FCAL6-DRA1 2 x 50 ml 11/10/2021 373+74 histamine (high level >50 27309 Canned Fish FCAL10-SEA7 145 g 29/10/2021 304 mg/kg) Sauce 27310 Fish FCAL20-CON23 2 x 30 g 01/11/2021 388+74 (Cooked) 27311 Cake Mix gluten & egg FCAL23-PRO10 2 x 30 g 19/11/2021 345 4

Item Code Matrix Analytes Product Code Approx. Size Start Date contamination (presence/absence) of matrix with one or more from the following list: Almond, Hazelnut, 27312 Chocolate FCAL3-CON2 50 g 25/11/2021 388 Walnut, Cashew, Pecan nut, Brazil nut, Pistachio nut, Macadamia/Queensland nut, Peanut Infant Soya 27313 milk (BLG) FCAL13-INF13 2 x 20 g 06/01/2022 304 Formula 27314 Cooked Biscuit gluten, milk and egg FCAL7-PRO14 30 g 20/01/2022 388 27315 Chocolate peanut, peanut protein FCAL16-CON2 2 x 20 g 03/02/2022 304 Infant Soya 27316 milk (casein) & gluten FCAL15-INF13 2 x 20 g 17/02/2022 388 Formula 27317 Cumin gluten & sesame FCAL22-SPI8 2 x 20 g 24/02/2022 304 27318 Flour lupin FCAL12-CCP28 2 x 20 g 02/03/2022 304 27319 Cooked Biscuit hazelnut, peanut FCAL9-PRO14 50 g 11/03/2022 388 histamine (high level >50 27320 Canned Fish FCAL10-SEA7 145 g 24/03/2022 304 mg/kg) Sausage Meat 27321 gluten FCAL6-MRP39 2 x 20 g 29/03/2022 304+74 (Raw)

AUTHENTICITY

Adulteration

Item Code Matrix Analytes Product Code Approx. Size Start Date 2992 Vanilla Extract detection of adulteration FCAA1-CON31 30 g 12/01/2021 284 one or more from: chicken, 2991 Beef FCAA4-MRP2 30 g 03/02/2021 284 horse, lamb or pork one or more from: beef, lamb, 2993 Chicken FCAA3-MRP14 30 g 08/04/2021 293 pork or turkey one or more from: beef, 2994 Lamb FCAA2-MRP22 30 g 09/07/2021 293 chicken, goat or pork 3302 Oil Cannabidiol FCAA5-OIL20 2 x 2 ml 05/10/2021 461+74 Herb 2996 (Origanum detection of adulteration FCAA1-VEG44 3 x 7g 11/11/2021 549 spp.) 14244 Olive Oil detection of adulteration FCAA1-OIL22 3 x 50 ml 13/12/2021 549+74 2997 Vanilla Extract detection of adulteration FCAA1-CON31 30 g 14/01/2022 293 one or more from: chicken, 2998 Beef FCAA4-MRP2 30 g 02/02/2022 293 horse, lamb or pork

Contamination

Item Code Matrix Analytes Product Code Approx. Size Start Date pork (DNA) 3114 Beef FCAC1-MRP2 2 x 30 g 20.04.2021 399+74 Halal Compliance Check 5

Speciation

Item Code Matrix Analytes Product Code Approx. Size Start Date identification of unknown fish 2995 Fish (3 samples from a list). FCAS1-SEA11 3 x 10 g 11/10/2021 293+74 See list on p31

CONTAMINANTS

Environmental Contaminants

Item Code Matrix Analytes Product Code Approx. Size Start Date perfluoroalkylated substances 0696 Fish FCCE5-SEA11 50 g 05/01/2021 375+74 (PFASs) 0697 Palm Oil PAHs (including PAH4 sum) FCCE2-OIL24 30 ml 25/02/2021 532 0698 Shellfish PAHs (including PAH4 sum) FCCE2-SEA23 50 g 27/04/2021 548+74 all 16 EU priority PAHs 0699 Olive Oil FCCE1-OIL22 30 ml 28/05/2021 609 (including PAH4 sum) 06100 Pork dioxins and PCBs FCCE3-MRP35 70 g 03/06/2021 548 06101 Cocoa Butter PAHs (including PAH4 sum) FCCE2-FAT7 50 g 06/07/2021 548+74 06102 Infant Formula dioxins and PCBs FCCE3-INF10 70 g 12/08/2021 548 Smoked Fish 06103 PAHs (including PAH4 sum) FCCE2-SEA25 50 g 06/09/2021 548+74 Product CBD Product 06110 PAHs (including PAH4 sum) FCCE2-UMI44 10 ml 11/10/2021 548+74 (Oil Based) 06104 Cod Liver Oil dioxins and PCBs FCCE3-OIL10 30 ml 21/10/2021 548 Spice - 06105 Smoked Black PAHs (including PAH4 sum) FCCE2-SPI26 15 g 12/11/2021 547 Pepper brominated flame retardants 06106 Cod Liver Oil FCCE6-OIL10 30 ml 09/12/2021 548 (BFRs) perfluoroalkylated substances 06107 Fish FCCE5-SEA11 50 g 04/01/2022 386+74 (PFASs) 06108 Palm Oil PAHs (including PAH4 sum) FCCE2-OIL24 30 ml 18/02/2022 548 06109 Milk dioxins and PCBs FCCE3-DRY13 70 g 14/03/2022 548+74

Overall Migration (Packaging Contaminants)

Item Code Matrix Analytes Product Code Approx. Size Start Date 6 sheets, each overall migration into ethanol by 1163 Nylon Film FCCO1-PMM13 12 cm x 16 14/04/2021 295 total immersion cm overall migration into olive oil by to be 1164 Plastic Film FCCO2-PMM16 20/10/2021 337 total immersion confirmed

Processing Contaminants

Item Code Matrix Analytes Product Code Approx. Size Start Date 3-MCPD, 1,3-DCP and 2663 Soy Sauce FCCP2-CON15 40 g 24/02/2021 293 2-MCPD 3-MCPD esters, glycidyl esters 2664 Vegetable Oil (ester-bound glycidol) and 2- FCCP1-OIL30 50 ml 14/04/2021 301 MCPD esters 3-MCPD esters, glycidyl esters 2665 Potato Crisps (ester-bound glycidol) and 2- FCCP1-PRO31 50 g 06/05/2021 301 MCPD esters 6

Item Code Matrix Analytes Product Code Approx. Size Start Date 3-MCPD esters, glycidyl esters 2666 Infant Formula (ester-bound glycidol) and 2- FCCP1-INF10 50 g 09/06/2021 330 MCPD esters 3-MCPD esters, glycidyl esters 2667 Vegetable Oil (ester-bound glycidol) and 2- FCCP1-OIL30 50 ml 15/09/2021 301 MCPD esters 3-MCPD, 1,3-DCP and 2668 Soy Sauce FCCP2-CON15 40 g 23/02/2022 301 2-MCPD furan, 2-methylfuran & 3- 30108 Coffee FCCP9-DRH6 100 g 18/01/2021 280+74 methylfuran 30109 Potato Crisps acrylamide FCCP3-PRO31 50 g 10/02/2021 280 & cyanuric acid (> 5 30110 Infant Formula FCCP7-INF10 50 g 05/03/2021 280 mg/kg) Vegetable 30111 acrylamide FCCP3-PRO37 50 g 07/05/2021 288 Crisps 30112 Infant Food acrylamide FCCP3-INF8 50 g 04/06/2021 288 30113 Animal Feed melamine & cyanuric acid FCCP5-AFE1 50 g 24/06/2021 288 Biscuit 30114 acrylamide FCCP3-PRO2 50 g 30/07/2021 288 (Cookie) French Fries 30115 acrylamide FCCP3-PRO25 50 g 14/09/2021 288+74 (Pre-Cooked) melamine & cyanuric acid (low 30116 Milk Powder FCCP6-DRY14 50 g 06/10/2021 288 levels, <5 mg/kg) Coffee 30117 acrylamide FCCP3-DRH12 50 g 03/11/2021 288 (Instant) 30118 Crispbread acrylamide FCCP3-PRO15 50 g 02/12/2021 288 furan, 2-methylfuran & 3- 30119 Coffee FCCP9-DRH6 100 g 24/01/2022 288+74 methylfuran 30120 Potato Crisps acrylamide FCCP3-PRO31 50 g 17/02/2022 288 melamine & cyanuric acid (> 5 30121 Infant Formula FCCP7-INF10 50 g 04/03/2022 288 mg/kg)

Specific Migration (Phthalates, BPA, PAA)

Item Code Matrix Analytes Product Code Approx. Size Start Date 12103 Oil phthalates FCCS5-OIL20 2 x 50 ml 24/03/2021 287 3% aq. Acetic 12104 melamine FCCS4-PMM3 50 ml 26/05/2021 296 Acid 50% Aqueous 12105 FCCS2-PMM4 50 ml 07/07/2021 296 Ethanol 3% aq. Acetic 12106 FCCS3-PMM3 50 ml 01/09/2021 296 Acid 3% aq. Acetic 12107 total primary aromatic amines FCCS6-PMM3 >300 ml 15/10/2021 296 Acid 3% aq. Acetic barium, cobalt, copper, iron, 12108 FCCS1-PMM3 50 ml 24/11/2021 296 Acid lithium, manganese & zinc 12109 Oil phthalates FCCS5-OIL20 2 x 50 ml 23/03/2022 296 7

Trace Elements

Note: The description 'natural/low levels' indicates naturally incurred elements at the typical ranges expected. The description 'natural levels' indicates naturally incurred elements, but some or all analytes may be at levels above the typically expected ranges.

Item Code Matrix Analytes Product Code Approx. Size Start Date arsenic (total), cadmium, lead & 07387 Milk Powder mercury (total) (all natural/low FCCM12-DRY14 50 g 06/01/2021 280 levels) antimony, arsenic (total), 07388 Soft Drink cadmium, chromium, copper & FCCM3-DRN29 50 ml 20/01/2021 280 zinc (all high levels) arsenic (total), arsenic Canned Crab (inorganic), cadmium, lead & 07389 FCCM6-SEA6 150 g 29/01/2021 280 Meat mercury (total) (all natural levels) cadmium, iron, lead & tin (all 07390 Tomato Paste FCCM21-VEG74 50 g 08/02/2021 280+74 high levels) Bivalve cadmium, lead & mercury (total) 07391 Molluscs FCCM36-SEA29 50 g 08/02/2021 280+74 (all natural/low levels) (Mussels) aluminium, arsenic (total), Soya Lecithin 07392 cadmium, lead & mercury (total) FCCM42-VEG90 50 g 24/02/2021 280 (Liquid) (all natural/low levels) Grapefruit cadmium, copper, iron, lead & 07393 FCCM23-FRU51 50 g 23/03/2021 280+74 Purée tin (all high levels) arsenic (total), mercury (total) & 07394 Canned Fish methyl mercury (all natural FCCM17-SEA7 150 g 31/03/2021 280 levels) arsenic (total), arsenic (inorganic), cadmium, lead & 07395 Rice Cakes FCCM6-PRO33 35 g 01/04/2021 288 mercury (total) (all natural/low levels) aluminium, arsenic (total), cadmium, copper, lead, 07396 Barley Flour FCCM28-CCP4 50 g 15/04/2021 288 mercury, nickel (total) (all natural/low levels) aluminium, cadmium, chromium, iodine, molybdenum, 07397 Infant Formula FCCM38-INF10 50 g 23/04/2021 288 selenium, tin and nickel (all natural/low levels) arsenic (total), cadmium & 07398 Canned Fish mercury (total) (all natural FCCM15-SEA7 150 g 30/04/2021 288 levels) cadmium & lead (all natural/low 07399 Honey FCCM19-HON2 50 g 05/05/2021 288 levels) aluminium, arsenic (total), cadmium, copper, iron, lead, 07400 Wheat Flour FCCM32-CCP49 50 g 26/05/2021 288 mercury (total), nickel & zinc (all natural/low levels) arsenic (total), copper, iron & 07401 Vegetable Oil FCCM16-OIL30 50 ml 02/06/2021 288 lead (all high levels) 8

Item Code Matrix Analytes Product Code Approx. Size Start Date Vegetable cadmium, lead, arsenic (total) FCCM39- 07402 Purée (Root and mercury (total) (all 50 g 14/06/2021 288+74 VEG103 Vegetables) natural/low levels) aluminium, arsenic (total), cadmium, copper, iron, lead, 07403 Cocoa Powder FCCM33-DRH5 50 g 23/06/2021 288 manganese, nickel & zinc (all natural levels) arsenic (total), cadmium & lead 07404 Chilli Powder FCCM10-SPI6 50 g 01/07/2021 288 (all high levels) arsenic (total), arsenic Powdered (inorganic), cadmium, iron, lead 07405 FCCM34-CCP41 50 g 14/07/2021 288 Brown Rice & mercury (total), nickel & zinc (all natural/low levels) arsenic (total), cadmium, lead & 07406 Offal (Liver) FCCM13-MRP27 50 g 28/07/2021 288 mercury (total) (all high levels) cadmium, copper, iron, lead & 07407 Wine FCCM40-DRA13 50 ml 04/08/2021 288 pH Baby Food arsenic (total), cadmium & lead 07408 (Vegetable FCCM31-INF19 50 g 09/08/2021 288+74 (all low levels) Based) Herb (mixed, cadmium, lead & nickel (all 07409 FCCM35-VEG89 30 g 11/08/2021 288 dried) natural/low levels) arsenic (total), cadmium, lead & 07410 Milk Powder mercury (total) (all natural/low FCCM12-DRY14 50 g 25/08/2021 288 levels) arsenic (total), cadmium, 07411 Canned Fish mercury (total) (all natural FCCM15-SEA7 150 g 03/09/2021 288 levels) cadmium, lead & mercury (total) 07412 Squid FCCM36-SEA27 50 g 06/09/2021 288+74 (all natural / low levels) arsenic (total), arsenic (inorganic), cadmium, Infant Cereal 07413 chromium, lead, mercury (total) FCCM22-INF18 50 g 16/09/2021 288 (Rice Based) & selenium (all natural/low levels) arsenic (inorganic) (natural/low 07414 Fruit Juice level), cadmium, iron, lead & tin FCCM5-DRN17 50 ml 28/09/2021 288+74 (all high levels) arsenic (total), arsenic (inorganic), cadmium, iodine, 07415 Seaweed FCCM37-VEG64 25 g 01/10/2021 288 lead, mercury (total) & nickel (all natural levels) arsenic (total), cadmium, lead, Mushroom 07416 mercury (total), nickel (all FCCM30-VEG51 30 g 08/10/2021 288 Powder natural/low levels) aluminium, arsenic (total), 07417 Soya Flour cadmium, lead & mercury (total) FCCM1-VEG68 50 g 20/10/2021 288 (all high levels) Vegetable cadmium, lead, nickel & tin (all 07418 FCCM24-VEG79 50 g 01/11/2021 288+74 Purée high levels) arsenic (total), arsenic 07419 Powdered Rice (inorganic), cadmium, lead & FCCM7-CCP42 50 g 10/11/2021 288 mercury (total) (all high levels) 9

Item Code Matrix Analytes Product Code Approx. Size Start Date arsenic (total), cadmium, lead, Animal Feed 07420 mercury (total), nickel (all FCCM30-AFE1 50 g 25/11/2021 288 (Cereal Based) natural/low levels) Nutritional arsenic (total), cadmium, 07421 Food chromium, lead & mercury FCCM27-SUP2 50 g 01/12/2021 288 Supplement (total) (all natural/low levels) arsenic (total), cadmium, lead & 07422 Milk Powder mercury (total) (all natural/low FCCM12-DRY14 50 g 05/01/2022 288 levels) antimony, arsenic (total), 07423 Soft Drink cadmium, chromium, copper & FCCM3-DRN29 50 ml 19/01/2022 288 zinc (all high levels) Bivalve cadmium, lead & mercury (total) 07424 Molluscs FCCM36-SEA29 50 g 24/01/2022 288+74 (all natural / low levels) (Mussels) arsenic (total), arsenic Canned Crab (inorganic), cadmium, lead & 07425 FCCM6-SEA6 150 g 28/01/2022 288 Meat mercury (total) (all natural/low levels) cadmium, iron, lead & tin (all 07426 Tomato Paste FCCM21-VEG74 50 g 08/02/2022 288+74 high levels) aluminium, arsenic (total), Soya Lecithin 07427 cadmium, lead & mercury (total) FCCM42-VEG90 50 ml 23/02/2022 288 (Liquid) (all natural/low levels) Animal Feed arsenic (total), cadmium, lead, 07428 (Vegetable mercury (total), nickel (all high FCCM43-AFE23 50 g 10/03/2022 288 Based) levels) Grapefruit cadmium, copper, iron, lead & 07429 FCCM23-FRU51 50 g 22/03/2022 288+74 Purée tin (all high levels) arsenic (total), cadmium, 07430 Canned Fish mercury (total) & methyl FCCM41-SEA7 150 g 31/03/2022 288 mercury (all natural levels) CBD Product arsenic (total), cadmium, lead & 07431 FCCM14-UMI44 7 g 29/10/2021 288+74 (Oil Based) mercury (total)

FAT, FATTY ACIDS & OILS

Item Code Matrix Analytes Product Code Approx. Size Start Date saturates, mono-unsaturates & 14229 Vegetable Oil FCFO3-OIL30 30 ml 17/02/2021 274 poly-unsaturates total fat, saturates, mono- unsaturates, poly-unsaturates, trans fatty acids (& possibly 14232 Infant Formula FCFO13-INF10 50 g 22/04/2021 283 individual fatty acids: linoleic acid, a-linolenic acid (ALA), ARA, DHA & EPA) total fat, saturates, mono- Mixed Fat 14233 unsaturates, poly-unsaturates & FCFO8-FAT12 50 g 11/05/2021 283+74 Spread total trans fatty acids saturates, mono-unsaturates & 14235 Vegetable Oil poly-unsaturates & limited fatty FCFO4-OIL30 30 ml 30/06/2021 283 acid profile 10

Item Code Matrix Analytes Product Code Approx. Size Start Date Total fat, saturates, mono- unsaturates, poly-unsaturates, total trans fatty acids, total Mixed Fat 14237 omega-3, total omega-6 & total FCFO10-FAT12 50 g 16/08/2021 283+74 Spread omega-9 series fatty acids, (& possibly individual omega-3, omega-6 & omega-9 fatty acids)

Total omega-3, total omega-6 & total omega-9 series fatty acids, 14239 Fish Oil FCFO1-OIL13 30 ml 22/09/2021 283 (& possibly individual omega-3, omega-6 & omega-9 fatty acids) total fat, saturates, mono- Biscuit unsaturates & poly-unsaturates, 14240 FCFO7-PRO2 50 g 05/10/2021 283+74 (Cookie) total trans fatty acids & butyric acid total fat, saturates, mono- Infant unsaturates, poly-unsaturates 14241 Breakfast (& possibly individual fatty FCFO9-INF6 50 g 21/10/2021 283 Cereal acids: linoleic acid, a-linolenic acid (ALA), ARA, DHA & EPA) Mixed Fat total fat, butyric acid, cholesterol 14243 FCFO14-FAT12 50 g 30/11/2021 283+74 Spread & selected plant sterols Biscuit fatty acid profile (inc. butyric 14246 FCFO12-PRO2 50 g 11/01/2022 283+74 (Cookie) acid) & cholesterol saturates, mono-unsaturates & 14247 Vegetable Oil FCFO3-OIL30 30 ml 16/02/2022 283 poly-unsaturates

FOOD ADDITIVES & INGREDIENTS

, caffeine, 03164 Cola Drink FCFA2-DRN12 150 ml 15/01/2021 273 acesulfame-K & sweeteners: acesulfame-K, 03165 Soft Drink , cyclamate & FCFA26-DRN29 150 ml 17/03/2021 287 saccharin Coffee 03166 caffeine FCFA28-DRH10 2 x 30 g 12/05/2021 286 (Ground) brix, pH, citric acid, sorbic acid, 03167 Soft Drink cyclamate, saccharin & benzoic FCFA7-DRN29 150 ml 16/07/2021 286 acid colours, a selection from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, 03168 Soft Drink Erythrosine, Green S, Indigo FCFA20-DRN29 150 ml 04/08/2021 286 Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine caffeine, benzoic acid, total 03169 Cola Drink & phosphoric acid (as FCFA13-DRN12 150 ml 14/10/2021 286 P2O5) 11

Item Code Matrix Analytes Product Code Approx. Size Start Date benzoic acid, quinine, 03170 Tonic Water FCFA3-DRN32 150 ml 03/11/2021 286 acesulfame-K & aspartame benzoic acid, caffeine, 03171 Cola Drink FCFA2-DRN12 150 ml 21/01/2022 286 acesulfame-K & saccharin sweeteners: acesulfame-K, 03172 Soft Drink aspartame, cyclamate & FCFA26-DRN29 150 ml 17/03/2022 286 saccharin nitrate as NaNO & nitrite as 15150 Meat 3 FCFA18-MRP23 25 g 13/01/2021 277 NaNO2 nitrate as NaNO & nitrite as 15151 Milk Powder 3 FCFA18-DRY14 40 g 26/02/2021 277 NaNO2 nitrate as NaNO & nitrite as 15152 Meat 3 FCFA18-MRP23 25 g 13/05/2021 286 NaNO2 Cabbage 15153 nitrate FCFA17-VEG32 70 g 08/06/2021 286+74 Purée 15154 Lettuce Purée nitrate FCFA17-VEG49 70 g 09/08/2021 286+74 nitrate as NaNO & nitrite as 15155 Meat 3 FCFA18-MRP23 25 g 10/09/2021 286 NaNO2 Rocket 15156 nitrate FCFA17-VEG60 70 g 26/10/2021 286+74 (Rucola) Purée 15157 Spinach Purée nitrate FCFA17-VEG70 70 g 23/11/2021 286+74 nitrate as NaNO & nitrite as 15158 Meat 3 FCFA18-MRP23 25 g 12/01/2022 286 NaNO2 nitrate as NaNO & nitrite as 15159 Milk Powder 3 FCFA18-DRY14 40 g 24/02/2022 286 NaNO2 brix, pH, total acidity, sodium, 20179 Tomato Sauce FCFA8-CON21 150 g 06/01/2021 277 chloride & benzoic acid 20180 Meat sulphur dioxide FCFA22-MRP23 100 g 01/03/2021 277+74 20181 Prawns sulphur dioxide FCFA22-SEA20 100 g 12/04/2021 286+74 brix, pH, benzoic acid, citric acid 20182 Jam FCFA4-CON7 70 g 29/04/2021 286 & sorbic acid caffeine, sorbic acid, Chocolate 20183 theobromine & total sugars FCFA14-PRO13 50 g 23/06/2021 286 Cake Mix (expressed as sucrose) Dried Apricot 20184 (Water/Fruit sulphur dioxide FCFA22-FRU37 100 g 12/07/2021 286+74 Slurry) colours, a selection from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Confectionery 20185 Erythrosine, Green S, Indigo FCFA20-CON17 50 g 15/07/2021 286 (Boiled Carmine, Patent Blue V, Sweets) Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine antioxidants: total BHA (E320), 20186 Oil total BHT (E321) & propyl FCFA1-OIL20 50 ml 24/09/2021 286 gallate (E310)

20187 Meat sulphur dioxide FCFA22-MRP23 100 g 04/10/2021 286+74 12

Item Code Matrix Analytes Product Code Approx. Size Start Date non-permitted colours (illegal dyes) high level, a selection from the following list: Butter Yellow, Orange II, Para Red, Hot Pepper 20188 Rhodamine B, Sudan (I, II, III, FCFA19-CON5 50 ml 11/11/2021 286 Sauce IV), Sudan Black B, Sudan Orange G, Sudan Red B, Sudan Red 7B, Sudan Red G, Toluidine Red Dried Apple 20189 (Water/Fruit sulphur dioxide FCFA22-FRU36 100 g 22/11/2021 286+74 Slurry) brix, pH, total acidity, sodium, 20191 Tomato Sauce FCFA8-CON21 150 g 05/01/2022 286 chloride & benzoic acid 20192 Meat sulphur dioxide FCFA22-MRP23 100 g 01/03/2022 286+74 colours, a selection from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Sweets (gum- 20193 Erythrosine, Green S, Indigo FCFA20-CON32 50 g 30/03/2022 286 based) Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine

MYCOTOXINS

Aflatoxins

Item Code Matrix Analytes Product Code Approx. Size Start Date 04403 Maize B & G &/or total FCMA2-CCP30 55 g 07/01/2021 274 Pistachio 04404 (Water/Nut aflatoxins B & G &/or total FCMA2-NUT14 100 g 18/01/2021 274+74 Slurry)

04406 Milk Powder M1 FCMA1-DRY14 55 g 17/02/2021 274 Peanut 04408 (Water/Nut aflatoxins B & G &/or total FCMA2-NUT9 100 g 15/03/2021 274+74 Slurry) Animal Feed 04410 aflatoxins B & G &/or total FCMA2-AFE2 55 g 01/04/2021 283 (Cereal Based) Almond 04413 (Water/Nut aflatoxins B & G &/or total FCMA2-NUT1 100 g 11/05/2021 283+74 Slurry) 04414 Maize aflatoxins B & G &/or total FCMA2-CCP30 55 g 19/05/2021 283

04415 Milk Powder aflatoxin M1 FCMA1-DRY14 55 g 03/06/2021 283 Peanut 04422 (Water/Nut aflatoxins B & G &/or total FCMA2-NUT9 100 g 21/09/2021 283+74 Slurry)

04423 Milk Powder aflatoxin M1 FCMA1-DRY14 55 g 29/09/2021 283 13

Animal Feed 04425 aflatoxins B & G &/or total FCMA2-AFE2 55 g 14/10/2021 283 (Cereal Based) 04428 Rice aflatoxins B & G &/or total FCMA2-CCP43 55 g 18/11/2021 283

Item Code Matrix Analytes Product Code Approx. Size Start Date Peanut Butter 04429 (Water/Nut aflatoxins B & G &/or total FCMA2-CON12 100 g 23/11/2021 283+74 Butter Slurry) 04431 Maize aflatoxins B & G &/or total FCMA2-CCP30 55 g 06/01/2022 283 Pistachio 04432 (Water/Nut aflatoxins B & G &/or total FCMA2-NUT14 100 g 25/01/2022 283+74 Slurry)

04434 Milk Powder aflatoxin M1 FCMA1-DRY14 55 g 16/02/2022 283 Peanut 04436 (Water/Nut aflatoxins B & G &/or total FCMA2-NUT9 100 g 14/03/2022 283+74 Slurry)

Ergot Alkaloids

Item Code Matrix Analytes Product Code Approx. Size Start Date ergot alkaloids: contamination of matrix with two or more from ergometrine, ergotamine, 22180 Rye Flour FCME1-CCP47 55 g 10/03/2021 581 ergosine, ergocristine, ergocryptine & ergocornine & their related-inines ergot alkaloids: contamination of matrix with two or more from ergometrine, ergotamine, 22184 Baby Food FCME1-INF1 30 g 18/08/2021 598 ergosine, ergocristine, ergocryptine & ergocornine & their related-inines ergot alkaloids: contamination of matrix with two or more from ergometrine, ergotamine, 22190 Rye Flour FCME1-CCP47 55 g 09/03/2022 598 ergosine, ergocristine, ergocryptine & ergocornine & their related-inines

Fusarium

Item Code Matrix Analytes Product Code Approx. Size Start Date Breakfast deoxynivalenol (DON) & 22178 FCMF1-CCP13 55 g 08/01/2021 358 Cereal zearalenone (ZON) tropane alkaloids: atropine & 22179 Cereal FCMF6-CCP15 30 g 10/02/2021 358 scopolamine deoxynivalenol (DON), zearalenone (ZON), T-2 & HT-2 22181 Dried Pasta FCMF2-PRO17 75 g 19/05/2021 369 toxins & as a sum of T-2 & HT- 2 toxins FB & FB and total fumonisins 22182 Maize Flour 1 2 FCMF3-CCP32 55 g 18/06/2021 275 (as a sum of FB1 & FB2) 14

trichothecenes: nivalenol, DON, 3 Ac DON, 15 Ac DON, T-2 & 22183 Maize Flour FCMF5-CCP32 100 g 21/07/2021 672 HT-2 toxins & as a sum of T-2 & HT-2 toxins

Item Code Matrix Analytes Product Code Approx. Size Start Date deoxynivalenol (DON), zearalenone (ZON), T-2 & HT-2 22185 Animal Feed FCMF2-AFE1 75 g 23/09/2021 428 toxins & as a sum of T-2 & HT- 2 toxins Baby Food tropane alkaloids: atropine & 22186 FCMF6-INF17 30 g 07/10/2021 369 (Multigrain) scopolamine Breakfast deoxynivalenol (DON) & 22188 FCMF1-CCP13 55 g 07/01/2022 369 Cereal zearalenone (ZON) tropane alkaloids: atropine & 22189 Cereal FCMF6-CCP15 30 g 23/02/2022 369 scopolamine

Multi-

Item Code Matrix Analytes Product Code Approx. Size Start Date aflatoxin B &/or total, DON, 04405 Maize 1 FCMM1-CCP30 100 g 04/02/2021 476 ZON & OTA Spice (Black aflatoxins B & G &/or total & 04407 FCMM4-SPI1 75 g 04/03/2021 367 Pepper) OTA aflatoxin B & G &/or total, OTA, 04409 Oat Flour T-2 & HT-2 toxins, sum of T-2 & FCMM11-CCP38 55 g 25/03/2021 476 HT-2 toxins & sterigmatocystin

, DON, ZON, OTA,

FB1 & FB2 & total fumonisins

04411 Maize (as a sum of FB1 & FB2), T-2 & FCMM3-CCP30 100 g 07/04/2021 686 HT-2 toxins & as sum of T-2 & HT-2 toxins contamination of matrix with two or more from the following list: aflatoxins B & G &/or total,

04412 Infant Food OTA, ZON, DON, FB1 & FB2 & FCMM6-INF8 150 g 22/04/2021 490 total fumonisins (as a sum of

FB1 & FB2) & T-2 & HT-2 toxins & as sum of T-2 & HT-2 toxins aflatoxins B & G &/or total & 04416 Paprika FCMM4-SPI14 75 g 17/06/2021 378 OTA Hazelnut aflatoxins B & G &/or total & 04417 (Water/Nut FCMM4-NUT6 100 g 29/06/2021 283+74 OTA Slurry)

aflatoxin B1, DON, ZON, OTA,

FB1 & FB2 & total fumonisins (as

04418 Maize a sum of FB1 & FB2), T-2 & HT-2 FCMM3-CCP30 100 g 22/07/2021 686

toxins & as sum of T-2 & HT-2 toxins 15

Dried Figs aflatoxins B & G &/or total & 04419 (Water/Fruit FCMM4-FRU38 150 g 03/08/2021 378+74 OTA Slurry) Sesame Paste aflatoxins B & G &/or total & 04420 FCMM4-NUT17 100 g 17/08/2021 378+74 (Tahini) OTA aflatoxins B & G &/or total & 04421 Chilli Powder FCMM4-SPI6 75 g 09/09/2021 378 OTA

Item Code Matrix Analytes Product Code Approx. Size Start Date aflatoxins B & G &/or total & 04424 Infant Food FCMM4-INF8 55 g 07/10/2021 378 OTA

04426 Maize aflatoxin B1, DON, ZON & OTA FCMM2-CCP30 150 g 27/10/2021 490 aflatoxins B & G &/or total & 04427 Ginger FCMM4-SPI23 75 g 04/11/2021 378 OTA

contamination of matrix with two or more from the following list: Animal Feed 04430 aflatoxin B1, OTA, ZON, DON, FCMM5-AFE2 150 g 03/12/2021 490 (Cereal Based) FB1 & FB2 & total fumonisins

(as a sum of FB1 & FB2)

aflatoxin B &/or total, DON, 04433 Maize 1 FCMM1-CCP30 100 g 03/02/2022 490 ZON & OTA Spice - Black aflatoxins B & G &/or total & 04435 FCMM4-SPI1 75 g 03/03/2022 378 Pepper OTA aflatoxin B & G &/or total, OTA, 04437 Oat Flour T-2 & HT-2 toxins, sum of T-2 & FCMM11-CCP38 55 g 23/03/2022 490 HT-2 toxins & sterigmatocystin 17210 Flour OTA & citrinin FCMM8-CCP28 100 g 25/02/2021 274 17221 Flour OTA & citrinin FCMM8-CCP28 75 g 02/03/2022 283 deoxynivalenol (DON), zearalenone (ZON), T-2 & HT-2 22187 Wheat Flour toxins, sum of T-2 & HT-2 FCMM10-CCP49 75 g 10/11/2021 490 toxins & aflatoxin B & G &/or total

Ochratoxin A (OTA)

Item Code Matrix Analytes Product Code Approx. Size Start Date 17209 Wheat Flour OTA FCMO1-CCP49 55 g 27/01/2021 274 17211 Offal (Liver) OTA FCMO1-MRP27 75 g 22/03/2021 274+74 Dried Vine 17212 Fruit (Water/ OTA FCMO1-FRU43 100 g 06/04/2021 283+74 Fruit Slurry) 17213 Barley Flour OTA FCMO1-CCP4 55 g 20/05/2021 283 17214 Coffee (Green) OTA FCMO1-DRH9 55 g 01/07/2021 283 17215 Wine OTA FCMO1-DRA13 55 ml 12/08/2021 283 17216 Maize Flour OTA FCMO1-CCP32 55 g 02/09/2021 283 17217 Instant Coffee OTA FCMO1-DRH18 55 g 15/10/2021 283 17218 Animal Feed OTA FCMO1-AFE1 55 g 05/11/2021 283 Roasted 17219 OTA FCMO1-DRH21 55 g 24/11/2021 283 Coffee 17220 Wheat Flour OTA FCMO1-CCP49 55 g 26/01/2022 283 17222 Grape Juice OTA FCMO1-DRN19 55 ml 22/03/2022 283+74 16

Patulin

Item Code Matrix Analytes Product Code Approx. Size Start Date Apple Juice 1675 patulin FCMP1-DRN2 50 ml 26/01/2021 274+74 (Clear) 1676 Apple Purée patulin FCMP1-FRU2 60 g 04/05/2021 283+74 Apple Juice 1677 patulin FCMP1-DRN3 50 ml 26/10/2021 283+74 (Cloudy) Apple Juice 1678 patulin FCMP1-DRN2 50 ml 11/01/2022 283+74 (Clear)

NUTRITIONAL & PROXIMATES

Nutritional Components

Item Code Matrix Analytes Product Code Approx. Size Start Date moisture, ash, total fat, 01141 Canned Meat FCNC15-MRP12 150 g 14/01/2021 269 nitrogen, sodium & chloride Canned Meat moisture, ash, total fat, 01142 FCNC15-MRP13 150 g 18/03/2021 269 Meal nitrogen, sodium & chloride moisture, ash, total fat, nitrogen 01145 Canned Meat FCNC11-MRP12 150 g 14/05/2021 287 & hydroxyproline moisture, ash, total fat, 01146 Canned Meat FCNC15-MRP12 150 g 09/07/2021 287 nitrogen, sodium & chloride Canned Meat total fat, saturated fatty acids, 01147 FCNC25-MRP13 150 g 27/08/2021 287 Meal protein, total sugars & moisture, ash, total fat, nitrogen 01148 Canned Meat FCNC11-MRP12 150 g 30/09/2021 287 & hydroxyproline moisture, ash, total fat, Canned Meat 01149 nitrogen, sodium, chloride & FCNC16-MRP13 150 g 19/11/2021 287 Meal total sugars moisture, ash, total fat, 01150 Canned Meat FCNC15-MRP12 150 g 13/01/2022 287 nitrogen, sodium & chloride Canned Meat moisture, ash, total fat, 01151 FCNC15-MRP13 150 g 17/03/2022 287 Meal nitrogen, sodium & chloride brix, pH, total acidity, sugars, 0879 Apple Juice calcium, magnesium, FCNC27-DRN1 250 ml 28/01/2021 277 phosphorus, sodium ash, brix, pH, total acidity, Pineapple fructose, sucrose, glucose, total 0880 FCNC1-DRN27 250 ml 12/05/2021 286 Juice sugars, calcium, magnesium, potassium & sodium nutritional elements brix, pH, citric acid, fructose, sucrose, 0881 Orange Juice glucose, total sugars, calcium, FCNC31-DRN26 250 ml 18/08/2021 303 magnesium, phosphorus, sodium & potassium brix, pH, total acidity, fructose, Banana sucrose, glucose, total sugars, 0882 FCNC34-DRN40 250 ml 27/10/2021 286 Smoothie calcium, magnesium, potassium & sodium 17

Item Code Matrix Analytes Product Code Approx. Size Start Date brix, pH, total acidity, fructose, sucrose, glucose, total sugars, 0883 Apple Juice FCNC27-DRN1 250 ml 27/01/2022 286 calcium, magnesium, phosphorus, sodium moisture, ash, total oil, protein, 10175 Dairy Ration crude fibre, iron, magnesium, FCNC20-AFE7 225 g 19/03/2021 511 manganese & selenium moisture, ash, total oil, protein, 10176 Pig Ration crude fibre, aNDF, vitamin E & FCNC19-AFE14 150 g 02/06/2021 315 zinc moisture, ash, protein & crude 10177 Soybean meal FCNC7-AFE20 150 g 24/09/2021 291 fibre

moisture, ash, protein, total oil, Pet Dog Food 10178 crude fibre, starch & total FCNC9-PFO7 150 g 28/10/2021 315 (Dry) sugars

moisture, ash, total oil, protein, 10179 Poultry Ration crude fibre, starch, total sugars, FCNC21-AFE16 225 g 03/12/2021 526 calcium & phosphorus moisture, ash, total oil, protein, 10181 Dairy Ration crude fibre, iron, magnesium, FCNC20-AFE7 225 g 18/03/2022 526 manganese & selenium Sweets (Gum- 20190 fructose, glucose & sucrose FCNC38-CON32 50 g 10/12/2021 286 based) moisture at 130°C, ash, 2491 Wheat Flour nitrogen & total dietary fibre by FCNC4-CCP49 150 g 12/02/2021 269 AOAC moisture at 130°C, ash, total 2492 Porridge Oats fat, nitrogen & total dietary fibre FCNC5-CCP40 150 g 23/04/2021 277 by AOAC moisture at 130°C, ash, 2493 Cereal nitrogen & total dietary fibre by FCNC4-CCP15 150 g 02/07/2021 277 AOAC

moisture, ash, nitrogen, starch, 2494 Breadcrumbs sodium & total dietary fibre by FCNC6-PRO9 150 g 09/09/2021 277 AOAC

moisture, ash, total fat, Baby Food 2495 nitrogen, dietary fibre, starch, FCNC39-INF21 150 g 28/10/2021 277 (Cereal Based) sodium & chloride Biscuit moisture, ash, total fat, nitrogen 2496 FCNC13-PRO2 150 g 12/11/2021 277 (Cookie) & total dietary fibre by AOAC moisture at 130°C, ash, 2497 Wheat Flour nitrogen & total dietary fibre by FCNC4-CCP49 150 g 11/02/2022 277 AOAC Cheese & moisture, ash, total fat, 25192 FCNC15-PRO12 100 g 14/01/2021 269 Pasta Meal nitrogen, sodium & chloride moisture, total fat, non-fat 25193 Butter FCNC24-DRY6 200 g 23/02/2021 269+74 solids, pH & chloride Corn/Maize moisture, ash, total fat, 25195 based Snack FCNC15-PRO39 50 g 24/03/2021 269 nitrogen, sodium & chloride Food 18

Item Code Matrix Analytes Product Code Approx. Size Start Date moisture, ash, total fat, 25198 Fish Paste FCNC15-SEA15 150 g 09/04/2021 287 nitrogen, sodium & chloride Condensed moisture, ash, total fat, nitrogen 25199 FCNC14-DRY9 150 ml 13/05/2021 306 Milk & total sugars Milkshake fructose, galactose, glucose, 25200 FCNC3-DRY15 50 g 11/06/2021 277 Powder lactose, maltose & sucrose moisture, ash, total fat, 25201 Cheese nitrogen, sodium, chloride & FCNC37-DRY7 150 g 29/06/2021 277+74 starch moisture, total fat, nitrogen, 25202 Chocolate FCNC23-CON2 150 g 12/07/2021 277+74 butyric acid, lactose & sucrose moisture, ash, total fat, 25203 Infant Formula nitrogen, pH, titratable acidity, FCNC29-INF10 50 g 19/08/2021 277 lactose, sodium & chloride moisture, ash, total fat, 25205 Milk Powder nitrogen, titratable acidity, FCNC17-DRY14 50 g 29/10/2021 277 lactose & pH Corn/Maize pH, titratable acidity, total 25206 based Snack sugars, , FCNC30-PRO39 50 g 05/11/2021 277 Food magnesium, potassium Cheese & moisture, ash, total fat, 25207 FCNC15-PRO12 100 g 13/01/2022 287 Pasta Meal nitrogen, sodium & chloride ash, total fat, nitrogen, pH, 25208 Yoghurt FCNC40-DRY19 150 g 08/02/2022 277+74 titratable acidity, & total sugars moisture, total fat, non-fat 25209 Butter FCNC24-DRY6 200 g 22/02/2022 277+74 solids, pH & chloride Corn/Maize moisture, ash, total fat, 25211 based Snack FCNC15-PRO39 50 g 16/03/2022 277 nitrogen, sodium & chloride Food Processed nutritional components, 3203 Food (Ready to elements, allergens & FCXS1-PRO41 300 g 02/11/2021 643+74 Eat Meal) contaminants

Nutritional Elements

Item Code Matrix Analytes Product Code Approx. Size Start Date

calcium, magnesium, 10174 Premix manganese, phosphorus, FCNE5-AFE17 150 g 28/01/2021 283 sodium & zinc calcium, magnesium, 10180 Premix manganese, phosphorus, FCNE5-AFE17 150 g 27/01/2022 291 sodium & zinc calcium, copper, iodine, iron, magnesium, manganese, 18101 Infant Formula FCNE1-INF10 50 g 11/03/2021 283 phosphorus, potassium, selenium, sodium & zinc calcium, iron, magnesium, Breakfast 18103 phosphorus, potassium, sodium FCNE4-CCP13 50 g 07/07/2021 291 Cereal & zinc 19

Item Code Matrix Analytes Product Code Approx. Size Start Date calcium, copper, iron, manganese, magnesium, Coconut 18104 molybdenum, phosphorus, FCNE9-NUT28 50 g 03/09/2021 291 Powder potassium, selenium, sodium & zinc calcium, copper, iodine, iron, manganese, magnesium, 18105 Milk Powder molybdenum, phosphorus, FCNE8-DRY14 50 g 17/11/2021 291 potassium, selenium, sodium & zinc calcium, copper, iodine, iron, magnesium, manganese, 18106 Infant Formula FCNE1-INF10 50 g 10/03/2022 291 phosphorus, potassium, selenium, sodium & zinc

Vitamins

Item Code Matrix Analytes Product Code Approx. Size Start Date Breakfast vitamins B , B (total), B , B , 21123 1 2 6 12 FCNV9-CCP13 100 g 03/02/2021 296 Cereal total niacin & folic acid Powdered vitamins A, B , B , B , B , C, E, 21124 1 2 6 12 FCNV10-INF15 140 g 08/04/2021 349 Baby Food folic acid & total niacin

21125 Infant Formula vitamins A, B12, C, D3, E & K1 FCNV5-INF10 100 g 27/05/2021 315 21126 Fruit Purée vitamin C FCNV2-FRU47 100 g 21/06/2021 291+74 Liquid Vitamin 21127 vitamins B , B (total), B & D FCNV11-SUP4 40 ml 01/09/2021 315+74 Supplement 1 2 6 3 Breakfast vitamins B , B (total), B , B , 21128 1 2 6 12 FCNV9-CCP13 100 g 10/02/2022 315 Cereal total niacin & folic acid

PESTICIDES (for list of possible residues see pages 30 to 32)

Blank matrix samples are available to purchase with many of the proficiency test materials. Every effort has been made to ensure these do not contain the target analytes. Other analytes may be present.

Combined Multi-residue and Single-residue Methods

Item Code Matrix Analytes Product Code Approx. Size Start Date pesticide residues [multi- residue methods] including 09136 Basmati Rice FCPM15-CCP51 50 g 27/01/2021 279 bromide [single-residue methods] Blank Basmati 09136b BLANK BLPM2-CCP52 50 g 27/01/2021 88 Rice pesticide residues [multi- Soya Beans residue methods] including 09141 FCPX6-VEG67 90 g 10/09/2021 287 (Dried) glyphosate & AMPA [single- residue methods] Blank Soya 09141b BLANK BLPM2-VEG104 90 g 10/09/2021 91 Beans (Dried) 20

Item Code Matrix Analytes Product Code Approx. Size Start Date pesticide residues [multi- residue methods] including 09144 Basmati Rice FCPX2-CCP51 50 g 26/01/2022 287 bromide [single-residue methods] Blank Basmati 09144b BLANK BLPM2-CCP52 50 g 26/01/2022 91 Rice pesticide residues [multi- Cucumber residue methods] including 19313 FCPX4-VEG38 90 g 07/06/2021 287+74 Purée chlormequat/mepiquat [single- residue methods] Blank 19313b Cucumber BLANK BLPM2-VEG13 90 g 07/06/2021 91+74 Purée biocides (quaternary ammonium compounds) [multi- Salad Leaf 19324 residue methods] including FCPX1-VEG62 90 g 19/10/2021 287+74 Purée (per)chlorates [single-residue methods] Blank Salad 19324b BLANK BLPM6-VEG24 90 g 19/10/2021 91+74 Leaf Purée pesticide residues (tea matrix) [multi-residue] including 19327 Green Tea FCPX5-DRH14 50 g 02/12/2021 287 perchlorate (single residue method) Blank Green 19327b BLANK BLPM3-DRH1 50 g 02/12/2021 91 Tea biocides (quaternary ammonium compounds) [multi- Herb (Parsley) 19330 residue methods] including FCPX1-VEG45 90 g 21/02/2022 287+74 Purée (per)chlorates [single-residue methods] Blank Herb 19330b (Parsley) BLANK BLPM6-VEG15 90 g 21/02/2022 91+74 Purée pesticide residues (tea matrix) [multi-residue methods] 19332 Tea (Herbal) FCPX5-DRH23 50 g 03/03/2022 287 including perchlorate [single- residue methods] Blank Tea 19332b BLANK BLPM3-DRH26 50 g 03/03/2022 91 (Herbal)

Multi Residue Methods

Item Code Matrix Analytes Product Code Approx. Size Start Date pesticide residues (fat soluble, 05149 Infant Formula inc. EU 'red list' - low level and FCPM10-INF10 50 g 13/01/2021 294 perchlorate) Blank Infant 05149b BLANK BLPM10-INF5 50 g 13/01/2021 88 Formula Chicken pesticide residues (fat soluble 05150 FCPM11-EGG2 50 g 01/03/2021 294+74 (Hens) Eggs and recommended monitoring) Blank Chicken 05150b BLANK BLPM11-EGG1 50 g 01/03/2021 88+74 (Hens) Eggs 21

Item Code Matrix Analytes Product Code Approx. Size Start Date 05151 Oily Fish pesticide residues (fat soluble) FCPM9-SEA18 50 g 25/05/2021 303+74 05151b Blank Oily Fish BLANK BLPM9-SEA3 50 g 25/05/2021 91+74 pesticide residues (specified 05152 Infant Formula FCPM20-INF10 50 g 09/06/2021 303 residues) [fat soluble] Blank Infant 05152b BLANK BLPM20-INF5 50 g 09/06/2021 91 Formula 05153 Milk Powder pesticide residues (fat soluble) FCPM9-DRY14 50 g 29/07/2021 303 Blank Milk 05153b BLANK BLPM9-DRY2 50 g 29/07/2021 91 Powder Animal Fat 05154 pesticide residues (fat soluble) FCPM9-FAT2 50 g 07/09/2021 303+74 (Pork) Blank Animal 05154b BLANK BLPM9-FAT3 50 g 07/09/2021 91+74 Fat (Pork) Olive Oil pesticide residues (multi- 05155 FCPM2-OIL34 50 g 13/10/2021 303 (Virgin) residue) Blank Olive Oil 05155b BLANK BLPM2-OIL36 50 g 13/10/2021 91 (Virgin) biocides (quaternary 05156 Prawns FCPM7-SEA20 50 g 23/11/2021 303+74 ammonium compounds) 05156b Blank Prawns BLANK BLPM7-SEA4 50 g 23/11/2021 91+74 pesticide residues (fat soluble, 05157 Infant Formula inc. EU 'red list' - low level, and FCPM10-INF10 50 g 12/01/2022 303 perchlorate) Blank Infant 05157b BLANK BLPM10-INF5 50 g 12/01/2022 91 Formula CBD Product pesticide residues (multi- 05158 FCPM2-UMI44 10 g 02/02/2022 303+74 (Oil Based) residue) Blank CBD 05158b BLANK BLPM2-UMI45 10 g 02/02/2022 91+74 Product (Oil Chicken pesticide residues (fat soluble & 05159 FCPM11-EGG2 50 g 01/03/2022 303+74 (Hens) Eggs recommended monitoring) Blank Chicken 05159b BLANK BLPM11-EGG1 50 g 01/03/2022 91+74 (Hens) Eggs pesticide residues (multi- 09137 Wheat Flour FCPM2-CCP49 50 g 11/02/2021 279 residue) Blank Wheat 09137b BLANK BLPM2-CCP11 50 g 11/02/2021 88 Flour pesticide residues (multi- 19309 Lime Purée FCPM2-FRU53 90 g 13/04/2021 287+74 residue) Brown Rice pesticide residues (multi- 09139 FCPM2-CCP14 50 g 10/06/2021 287 (Powdered) residue) Blank Brown 09139b BLANK BLPM2-CCP5 50 g 10/06/2021 91 Rice pesticide residues (multi- 09140 Wheat Flour FCPM2-CCP49 50 g 11/08/2021 287 residue) Blank Wheat 09140b BLANK BLPM2-CCP11 50 g 11/08/2021 91 Flour pesticide residues (multi- 09142 Animal Feed FCPM2-AFE1 50 g 06/10/2021 287 residue) Blank Animal 09142b BLANK BLPM2-AFE4 50 g 06/10/2021 91 Feed 22

Item Code Matrix Analytes Product Code Approx. Size Start Date pesticide residues (multi- 09145 Wheat Flour FCPM2-CCP49 50 g 10/02/2022 287 residue) Blank Wheat 09145b BLANK BLPM2-CCP11 50 g 10/02/2022 91 Flour pesticide residues (honey 19304 Honey FCPM8-HON2 90 g 11/01/2021 279+74 matrix) [multi-residue] 19304b Blank Honey BLANK BLPM8-HON1 90 g 11/01/2021 88+74 Spice pesticide residues (multi- 19305 FCPM2-SPI21 50 g 11/01/2021 279+74 (Turmeric) residue) Blank Spice 19305b BLANK BLPM2-SPI25 50 g 11/01/2021 88+74 (Turmeric) pesticide residues (specified 19306 Melon Purée FCPM22-FRU56 90 g 16/02/2021 279+74 residues) [multi-residue] Blank Melon 19306b BLANK BLPM22-FRU20 90 g 16/02/2021 88+74 Purée pesticide residues (multi- 19307 Apple Purée FCPM2-FRU2 90 g 08/03/2021 279+74 residue) Blank Apple 19307b BLANK BLPM2-FRU5 90 g 08/03/2021 88+74 Purée Blank Lime 19309b BLANK BLPM2-FRU17 90 g 13/04/2021 91+74 Purée Yard Long pesticide residues (multi- 19310 FCPM2-VEG106 90 g 13/04/2021 287+74 Bean Purée residue) Blank Yard 19310b Long Bean BLANK BLPM2-VEG105 90 g 13/04/2021 91+74 Purée pesticide residues (multi- 19311 Tomato Purée FCPM2-VEG76 90 g 10/05/2021 287+74 residue) Blank Tomato 19311b BLANK BLPM2-VEG29 90 g 10/05/2021 91+74 Purée Chilli Pepper pesticide residues (multi- 19312 FCPM2-SPI22 90 g 10/05/2021 287+74 Purée residue) Blank Chilli 19312b BLANK BLPM2-SPI24 90 g 10/05/2021 91+74 Pepper Purée pesticide residues (multi- 19314 Lettuce Purée FCPM2-VEG49 90 g 07/06/2021 287+74 residue) Blank Lettuce 19314b BLANK BLPM2-VEG18 90 g 07/06/2021 91+74 Purée pesticide residues (multi- 19315 Celery Purée FCPM2-VEG81 90 g 20/07/2021 287+74 residue) Blank Celery 19315b BLANK BLPM2-VEG84 90 g 20/07/2021 91+74 Purée pesticide residues (multi- 19316 Broccoli Purée FCPM2-VEG30 90 g 20/07/2021 287+74 residue) Blank Broccoli 19316b BLANK BLPM2-VEG7 90 g 20/07/2021 91+74 Purée Strawberry pesticide residues (multi- 19317 FCPM2-FRU67 90 g 24/08/2021 287+74 Purée residue) Blank 19317b Strawberry BLANK BLPM2-FRU30 90 g 24/08/2021 91+74 Purée pesticide residues (multi- 19318 Potato Purée FCPM2-VEG59 90 g 24/08/2021 287+74 residue) Blank Potato 19318b BLANK BLPM2-VEG23 90 g 24/08/2021 91+74 Purée 23

Item Code Matrix Analytes Product Code Approx. Size Start Date Herb pesticide residues (multi- 19319 (Coriander) FCPM2-VEG35 90 g 13/09/2021 287+74 residue) Purée Blank Herb 19319b (Coriander) BLANK BLPM2-VEG11 90 g 13/09/2021 91+74 Purée pesticide residues (multi- 19321 Mango Purée FCPM2-FRU55 90 g 21/09/2021 287+74 residue) Blank Mango 19321b BLANK BLPM2-FRU19 90 g 21/09/2021 91+74 Purée Grape (Table) pesticide residues (multi- 19323 FCPM2-FRU48 90 g 19/10/2021 287+74 Purée residue) Blank Grape 19323b BLANK BLPM2-FRU14 90 ml 19/10/2021 91+74 (Table) Purée pesticide residues (multi- 19325 Peach Purée FCPM2-FRU59 90 g 08/11/2021 287+74 residue) Blank Peach 19325b BLANK BLPM2-FRU23 90 g 08/11/2021 91+74 Purée pesticide residues (honey 19326 Honey FCPM8-HON2 90 g 08/11/2021 287+74 matrix) [multi-residue] 19326b Blank Honey BLANK BLPM8-HON1 90 g 08/11/2021 91+74 Spice (Black pesticide residues (multi- 19328 FCPM2-SPI1 50 g 17/01/2022 287+74 Pepper) residue) Blank Spice 19328b BLANK BLPM2-SPI2 50 g 17/01/2022 91+74 (Black Pepper) pesticide residues (specified FCPM22- 19329 Pumpkin Purée 90 g 17/01/2022 287+74 residues) [multi-residue] VEG102 Blank Pumpkin 19329b BLANK BLPM22-VEG101 90 g 17/01/2022 91+74 Purée pesticide residues (multi- 19331 Apple Purée FCPM2-FRU2 90 g 21/02/2022 287+74 residue) Blank Apple 19331b BLANK BLPM2-FRU5 90 g 21/02/2022 91+74 Purée

Single Residue Methods

Item Code Matrix Analytes Product Code Approx. Size Start Date chlormequat, mepiquat, 09138 Oats FCMS2-CCP39 100 g 28/04/2021 287 glyphosate & AMPA Blank Oat 09138b BLANK BLMS5-CCP67 100 g 28/04/2021 91 Flour chlormequat, mepiquat, 09143 Wheat Flour FCMS2-CCP49 100 g 18/11/2021 287 glyphosate & AMPA Blank Wheat 09143b BLANK BLMS5-CCP11 100 g 18/11/2021 91 Flour 19308 Pear Purée dithiocarbamates FCMS3-FRU60 90 g 22/03/2021 374+74 Blank Pear 19308b BLANK BLMS3-FRU24 90 g 22/03/2021 115+74 Purée 19320 Lettuce Purée dithiocarbamates FCMS3-VEG49 90 g 13/09/2021 385+74 Blank Lettuce 19320b BLANK BLMS3-VEG18 90 g 13/09/2021 118+74 Purée 24

Item Code Matrix Analytes Product Code Approx. Size Start Date single residue monitoring (see 19322 Tomato Purée FCMS5-VEG76 100 g 04/10/2021 490+74 page 30 for potential residues) Blank Tomato 19322b BLANK BLPM1-VEG29 100 g 04/10/2021 118+74 Purée 19333 Grape Purée dithiocarbamates FCMS3-FRU49 90 g 21/03/2022 385+74 Blank Grape 19333b BLANK BLMS3-FRU15 90 g 21/03/2022 118+74 Purée

QUALITY

Honey

Item Code Matrix Analytes Product Code Approx. Size Start Date moisture, fructose, glucose, 2848 Honey sucrose, hydroxymethylfurfural FCQH3-HON2 100 g 09/03/2021 274+74 (HMF), diastase & free acid moisture, fructose, glucose, 2849 Honey sucrose, hydroxymethylfurfural FCQH2-HON2 100 g 22/06/2021 283+74 (HMF) & diastase fructose, glucose, sucrose, hydroxymethylfurfural (HMF), 2850 Honey FCQH1-HON2 100 g 02/11/2021 283+74 diastase, electrical conductivity, lead (Pb) & pH moisture, fructose, glucose, 2851 Honey sucrose, hydroxymethylfurfural FCQH3-HON2 100 g 08/03/2022 283+74 (HMF), diastase & free acid

Meat & Fish Indices

Item Code Matrix Analytes Product Code Approx. Size Start Date 15 g 01144 Salami Water Activity FCQW1-MRP38 04/05/2021 287+74 (4 slices) total volatile basic nitrogen 01152 Canned Meat FCQT1-MRP12 150 g 31/03/2022 287 (TVB-N) total volatile basic nitrogen 25194 Canned Fish FCQT1-SEA7 150 g 05/03/2021 269 (TVB-N) total volatile basic nitrogen 25204 Canned Fish FCQT1-SEA7 150 g 08/09/2021 287 (TVB-N) total volatile basic nitrogen 25210 Canned Fish FCQT1-SEA7 150 g 04/03/2022 287 (TVB-N) 25

Olive Oil and Vegetable Oil

Item Code Matrix Analytes Product Code Approx. Size Start Date

peroxide value, acidity, 14228 Olive Oil FCQO1-OIL22 100 ml 12/01/2021 274+74 anisidine value & iodine value

peroxide value, acidity, K & 14230 Olive Oil 232 FCQO2-OIL22 100 ml 30/03/2021 274+74 K270 peroxide value (lower level), 14234 Vegetable Oil acidity (lower level), anisidine FCQO1-OIL30 50 ml 14/06/2021 283+74 value & iodine value peroxide value, acidity, 14236 Olive Oil FCQO1-OIL22 100 ml 13/07/2021 283+74 anisidine value & iodine value

Item Code Matrix Analytes Product Code Approx. Size Start Date peroxide value, acidity, K & 14238 Olive Oil 232 FCQO2-OIL22 100 ml 14/09/2021 283+74 K270 peroxide value (lower level), 14242 Vegetable Oil acidity (lower level), anisidine FCQO1-OIL30 50 ml 09/11/2021 283+74 value & iodine value peroxide value, acidity, 14245 Olive Oil FCQO1-OIL22 100 ml 04/01/2022 283+74 anisidine value & iodine value peroxide value, acidity, K & 14248 Olive Oil 232 FCQO2-OIL22 100 ml 29/03/2022 283+74 K270 26

Veterinary Drug Residues (for list of possible residues please see pages 33-34)

Blank matrix samples are available to purchase with many of the proficiency test materials. Every effort has been made to ensure these do not contain the target analytes. Other analytes may be present. Where possible, naturally incurred residues are used. Item Code Matrix Analytes Product Code Approx. Size Start Date malachite green, 02418 Fish Muscle leucomalachite green & total FCVD11-SEA13 20 g 04/01/2021 361+74 malachite green Blank Fish 02418b BLANK BLVD11-SEA2 20 g 04/01/2021 109+74 Muscle 02419 Fish Muscle sulfonamides FCVD20-SEA13 20 g 04/01/2021 361+74 Blank Fish 02419b BLANK BLVD20-SEA2 20 g 04/01/2021 109+74 Muscle 02420 Honey tetracyclines & macrolides FCVD27-HON2 40 g 19/01/2021 361+74 02420b Blank Honey BLANK BLVD27-HON1 40 g 19/01/2021 109+74 02421 Honey nitrofuran metabolites FCVD12-HON2 20 g 19/01/2021 361+74 Chicken 02422 quinolones & fluoroquinolones FCVD15-MRP17 20 g 01/02/2021 361+74 Muscle Blank Chicken 02422b BLANK BLVD15-MRP50 20 g 01/02/2021 109+74 Muscle 02423 Bovine Liver glucocorticoids FCVD9-MRP7 20 g 01/02/2021 361+74 02424 Prawns tetracyclines FCVD22-SEA20 20 g 15/02/2021 361+74 02424b Blank Prawns BLANK BLVD22-SEA4 20 g 15/02/2021 109+74 sulfonamides & trimethoprim & 02425 Bovine Liver FCVD29-MRP7 20 g 15/02/2021 361+74 macrolides Blank Bovine 02425b BLANK BLVD29-MRP51 20 g 15/02/2021 109+74 Liver 02426 Bovine Serum specified hormones FCVD31-MRP52 2 x 25 ml 08/03/2021 413+74

Blank Bovine 02426b BLANK BLVD31-MRP53 2 x 25 ml 08/03/2021 109+74 Serum

chloramphenicol, florfenicol, 02427 Honey FCVD5-HON2 20 g 12/04/2021 372+74 thiamphenicol & total phenicols 02427b Blank Honey BLANK BLVD5-HON1 20 g 12/04/2021 112+74

02428 Fish Muscle quinolones & fluoroquinolones FCVD15-SEA13 20 g 26/04/2021 372+74 Blank Fish 02428b BLANK BLVD15-SEA2 20 g 26/04/2021 112+74 Muscle 27

Chicken 02429 nitrofuran metabolites FCVD12-MRP17 20 g 26/04/2021 372+74 Muscle Blank Chicken 02429b BLANK BLVD12-MRP50 20 g 26/04/2021 112+74 Muscle

Item Code Matrix Analytes Product Code Approx. Size Start Date Chicken 02430 tetracyclines FCVD26-MRP17 40 g 17/05/2021 372+74 Muscle Blank Chicken 02430b BLANK BLVD22-MRP50 20 g 17/05/2021 112+74 Muscle 02431 Fish Muscle avermectins FCVD1-SEA13 20 g 17/05/2021 372+74 Blank Fish 02431b BLANK BLVD1-SEA2 20 g 17/05/2021 112+74 Muscle 02432 Pig Liver Beta-agonists FCVD17-MRP30 20 g 01/06/2021 372+74 02432b Blank Pig Liver BLANK BLVD17-MRP56 20 g 01/06/2021 112+74 02433 Fish Muscle illegal dyes (veterinary drugs) FCVD10-SEA13 20 g 01/06/2021 372+74 Blank Fish 02433b BLANK BLVD10-SEA2 20 g 01/06/2021 112+74 Muscle 02434 Bovine Urine synthetic hormones FCVD21-MRP9 25 ml 21/06/2021 372+74 Blank Bovine 02434b BLANK BLVD21-MRP46 25 ml 21/06/2021 112+74 Urine 02435 Bovine Liver tetracyclines & aminoglycosides FCVD26-MRP7 40 g 05/07/2021 372+74 Blank Bovine 02435b BLANK BLVD26-MRP51 40 g 05/07/2021 112+74 Liver chloramphenicol, florfenicol, 02436 Fish Muscle FCVD5-SEA13 20 g 05/07/2021 372+74 thiamphenicol & total phenicols Blank Fish 02436b BLANK BLVD5-SEA2 20 g 05/07/2021 112+74 Muscle 02437 Honey sulfonamides FCVD20-HON2 20 g 19/07/2021 372+74 02437b Blank Honey BLANK BLVD20-HON1 20 g 19/07/2021 112+74 02438 Fish Muscle nitrofuran metabolites FCVD12-SEA13 20 g 19/07/2021 372+74 Blank Fish 02438b BLANK BLVD12-SEA2 20 g 19/07/2021 112+74 Muscle 02439 Chicken Liver coccidiostats FCVD7-MRP16 20 g 02/08/2021 372+74 Blank Chicken 02439b BLANK BLVD7-MRP54 20 g 02/08/2021 112+74 Liver Chicken 02440 nitroimidazoles FCVD13-MRP17 20 g 02/08/2021 372+74 Muscle Blank Chicken 02440b BLANK BLVD13-MRP50 20 g 02/08/2021 112+74 Muscle 02441 Honey quinolones & fluoroquinolones FCVD15-HON2 20 g 17/08/2021 372+74 02441b Blank Honey BLANK BLVD15-HON1 20 g 17/08/2021 112+74 02442 Sheep Muscle avermectins & anthelmintics FCVD2-MRP42 40 g 31/08/2021 372+74 Blank Sheep 02442b BLANK BLVD23-MRP57 40 g 31/08/2021 112+74 Muscle 02443 Pig Muscle tranquilizers FCVD32-MRP32 20 g 31/08/2021 372+74 Blank Pig 02443b BLANK BLVD24-MRP48 20 g 31/08/2021 112+74 Muscle chloramphenicol, florfenicol, 02444 Bovine Milk FCVD5-DRY4 25 ml 27/09/2021 372+74 thiamphenicol & total phenicols Blank Bovine 02444b BLANK BLVD5-DRY20 25 ml 27/09/2021 112+74 Milk Beta-lactams (penicillins & 02445 Bovine Milk FCVD18-DRY4 25 ml 27/09/2021 372+74 cephalosporins) Blank Bovine 02445b BLANK BLVD18-DRY20 25 ml 27/09/2021 112+74 Milk 28

Item Code Matrix Analytes Product Code Approx. Size Start Date coccidiostats & chloramphenicol 02446 Poultry Feed FCVD8-AFE15 40 g 01/10/2021 372 (contaminant levels) 02447 Prawns nitrofuran metabolites FCVD12-SEA20 20 g 18/10/2021 372+74 02447b Blank Prawns BLANK BLVD12-SEA4 20 g 18/10/2021 112+74 02448 Fish Muscle tetracyclines FCVD22-SEA13 20 g 18/10/2021 372+74 Blank Fish 02448b BLANK BLVD22-SEA2 20 g 18/10/2021 112+74 Muscle chloramphenicol, florfenicol, 02449 Prawns FCVD5-SEA20 20 g 15/11/2021 372+74 thiamphenicol & total phenicols 02449b Blank Prawns BLANK BLVD5-SEA4 20 g 15/11/2021 112+74 non-steroidal anti-inflammatory 02450 Bovine Muscle FCVD24-MRP8 25 g 15/11/2021 372+74 drugs (NSAIDs) Blank Bovine 02450b BLANK BLVD25-MRP49 25 g 15/11/2021 112+74 Muscle 02451 Corned Beef Beta-agonists FCVD17-MRP18 20 g 22/11/2021 372+74 nitroimidazoles & 02452 Honey FCVD14-HON2 40 g 06/12/2021 372+74 aminoglycosides 02452b Blank Honey BLANK BLVD14-HON1 40 g 06/12/2021 112+74 Natural Hormones and 02453 Bovine Urine FCVD33-MRP9 25 ml 06/12/2021 372+74 Thyrostats malachite green, 02454 Fish Muscle leucomalachite green & total FCVD11-SEA13 20 g 10/01/2022 372+74 malachite green Blank Fish 02454b BLANK BLVD11-SEA2 20 g 10/01/2022 112+74 Muscle 02455 Fish Muscle sulfonamides FCVD20-SEA13 20 g 10/01/2022 372+74 Blank Fish 02455b BLANK BLVD20-SEA2 20 g 10/01/2022 112+74 Muscle 02456 Honey tetracyclines & macrolides FCVD27-HON2 40 g 18/01/2022 372+74 02456b Blank Honey BLANK BLVD27-HON1 40 g 18/01/2022 112+74 02457 Honey nitrofuran metabolites FCVD12-HON2 20 g 18/01/2022 372+74 02457b Blank Honey BLANK BLVD12-HON1 20 g 18/01/2022 112+74 Chicken 02458 quinolones & fluoroquinolones FCVD15-EGG2 20 g 31/01/2022 372+74 (Hens) Eggs Blank Chicken 02458b BLANK BLVD15-EGG1 20 g 31/01/2022 112+74 (Hens) Eggs 02459 Bovine Muscle glucocorticoids FCVD9-MRP8 20 g 31/01/2022 372+74 Blank Bovine 02459b BLANK BLVD28-MRP49 20 g 31/01/2022 112+74 Muscle 02460 Prawns tetracyclines FCVD22-SEA20 20 g 14/02/2022 372+74 02460b Blank Prawns BLANK BLVD22-SEA4 20 g 14/02/2022 112+74 sulfonamides & trimethoprim & 02461 Bovine Liver FCVD29-MRP7 40 g 14/02/2022 372+74 macrolides Blank Bovine 02461b BLANK BLVD29-MRP51 20 g 14/02/2022 112+74 Liver 02462 Bovine Serum specified hormones FCVD31-MRP52 2 x 25 ml 07/03/2022 425+74 Blank Bovine 02462b BLANK BLVD31-MRP53 2 x 25 ml 07/03/2022 112+74 Serum 29

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Potential pesticide residues

multi-residue heptachlor-epoxide (cis), heptachlor-epoxide (trans), 2,4-D (free acid only), 2-phenylphenol (ortho- heptenophos, hexaconazole, hexythiazox, imazalil, phenylphenol), 6-benzylaminopurine, abamectin (sum of imidacloprid, indoxacarb (sum of indoxacarb and its R avermectin B1a and B1b only), acephate, acetamiprid, enantiomer), iprodione, iprovalicarb, isocarbofos, acetochlor, aclonifen, acrinathrin, , aldicarb- isofenphos (ethyl), isofenphos-methyl, isoprocarb, sulfone (aldoxycarb), aldicarb-sulfoxide, aldrin, allethrin, isoprothiolane, isoproturon, kresoxim-methyl, lenacil, ametoctradin, amidosulfuron, atrazine, azinphos-ethyl, linuron, ufenuron, malaoxon, , azinphos-methyl, azoxystrobin, benalaxyl, bendiocarb, mandipropamid, mecarbam, mepanipyrim, benthiavalicarb-isopropyl, bifenthrin (sum of isomers), metaflumizone (sum of E and Z isomers), metalaxyl biphenyl, bitertanol, boscalid, bromophos-ethyl, (sum of constituent isomers including metalaxyl-M), bromopropylate, bromuconazole (sum of metamitron, metconazole, methacrifos, , diastereoisomers), bupirimate, buprofezin, cadusafos, methidathion, methiocarb, methiocarb-sulfone, carbaryl, carbendazim, carbofuran, carbofuran (3- methiocarb-sulfoxide, methomyl, methoxychlor, hydroxy), carboxin, chlorantraniliprole (rynaxypyr), methoxyfenozide, metolachlor (sum of constituent chlordane (cis), chlordane (oxy), chlordane (trans), isomers including S-metolachlor), metrafenone, chlorfenapyr, chlorfenvinphos (sum of E and Z isomers), metribuzin, mevinphos (sum of E and Z isomers), chloridazon, chlorobenzilate, chlorothalonil, molinate, monocrotophos, monolinuron, myclobutanil, chlorpropham, (ethyl), chlorpyrifos-methyl, nitrofen, novaluron, omethoate, oxadiazon, oxadixyl, chlorthaldimethyl, clofentezine, clothianidin, oxamyl, oxyfluorfen, paclobutrazol, parathion (- coumaphos, cyazofamid, cyflufenamid, cyfluthrin (sum ethyl),parathion-methyl, penconazole, pencycuron, of constituent isomers), cyhalothrin-lambda (includes pendimethalin, penflufen, pentachloroaniline, cyhalothrin-gamma) (sum of R,S and S,R isomers), penthiopyrad, permethrin (sum of isomers), phenthoate, cymoxanil, cypermethrin (sum of constituent isomers), phorate, phorate-sulfone, phorate-sulfoxide, phosalone, cyproconazole, cyprodinil, cyromazine, DDD-pp (TDE), phosmet, phosphamidon, phoxim, phthalimide, DDE-pp, DDT-op, DDT-pp, deltamethrin, demeton-S- picoxystrobin, piperonyl butoxide, pirimicarb, pirimicarb methyl, demeton-S-methyl-sulfone, demeton-S-methyl- (desmethyl), pirimiphos-ethyl,pirimiphos-methyl, sulfoxide (oxydemeton-methyl), diafenthiuron, diazinon, prochloraz (parent compound only), procymidone, dichlorvos, dicloran, dicofol (sum of p,p' and o,p' profenofos, promecarb, prometryn, propamocarb, isomers), dicrotophos, , diethofencarb, propargite, propetamphos, propiconazole, propoxur, difenoconazole, diflubenzuron, dimethoate, propyzamide, proquinazid, prosulfocarb, dimethomorph (sum of isomers), dimoxystrobin, prothioconazole-desthio (sum of isomers), prothiofos, diniconazole, dinotefuran, diphenylamine, disulfoton, pymetrozine, pyraclostrobin, pyrazophos, pyrethrin disulfoton-sulfone, disulfoton-sulfoxide, diuron, dodine, (sum), pyridaben, pyridalyl, pyridaphenthion, Emamectin (as emamectin benzoate B1a, expressed as pyrimethanil, pyriproxyfen, quassia, quinalphos, emamectin), endosulfan I (alpha), endosulfan II (beta), quinoxyfen, quintozene, spinetoram, spinosad (sum of endosulfan-sulfate, endrin, EPN, epoxiconazole, spinosyn A and D), spirodiclofen, spiromesifen, ethiofencarb, ethiofencarb-sulfone, ethiofencarb- spirotetramat (parent compound only), spirotetramat- sulfoxide, ethion, ethirimol, ethoprophos, etofenprox, enol (expressed as spirotetramat), spiroxamine, etoxazole, etrimfos, famoxadone, fenamidone, tebuconazole, tebufenozide, tebufenpyrad, tecnazene, fenamiphos, fenamiphos-sulfone, fenamiphos-sulfoxide, teflubenzuron, tefluthrin, terbufos, terbufos-sulfone, fenarimol, fenazaquin, fenbuconazole, fenbutatin oxide, terbufos-sulfoxide, terbuthylazine, tetrachlorvinphos, fenhexamid, fenitrothion, fenoxycarb, fenpropathrin, tetraconazole, tetradifon, tetramethrin (sum of fenpropidin (sum of fenpropidin and its , expressed constituent isomers), TFNA, TFNG, thiabendazole, as fenpropidin), fenpropimorph (sum of isomers), thiacloprid, thiamethoxam, thiodicarb, thiophanate- fenpyroximate, fensulfothion, fensulfothion-oxon, methyl, THPI, tolclofos-methyl, tolfenpyrad, tolylfluanid, fensulfothion-oxon-sulfone, fensulfothion-sulfone, triadimefon, triadimenol, triallate, triazophos, fenthion (parent compound only), fenthion-sulfone, tricyclazole, trifloxystrobin, triflumuron, trifluralin, fenthion-sulfoxide, fenvalerate (sum of constituent triticonazole, vinclozolin, zoxamide isomers in any ratio including esfenvalerate), fipronil (parent compound only), fipronil-desulfinyl,fipronil- multi-residue: honey matrix sulfone, flonicamid, fluazifop (free acid), fluazinam, acetamiprid, amitraz (parent compound only), flubendiamide, flucythrinate, fludioxonil, flufenacet clothianidin, coumaphos, dinotefuran, (parent compound only), flufenoxuron, fluopicolide, DMF (N-2,4-dimethylformamide) fluopyram, fluoxastrobin (sum of fluoxastrobin and its DMPF (N-2,4-dimethylphenylformamide), fluvalinate Z-isomer), fluquinconazole, flusilazole, flutolanil, (tau), imidacloprid, methamidophos, nitenpyram, flutriafol, fluvalinate (tau), fluxapyroxad, fonofos, thiacloprid, thiamethoxam fosthiazate, furathiocarb, haloxyfop (free acid), HCB (hexachlorobenzene), HCH-A (alpha hexachlorocyclohexane), HCH-B (beta hexachlorocyclohexane), HCH-G (gamma hexachlorocyclohexane / ), heptachlor, 32 hexachlorocyclohexane / lindane), heptachlor, multi-residue: tea matrix aldicarb-sulfoxide, aldrin, allethrin, azamethiphos, 2-phenylphenol (ortho-phenylphenol), abamectin (sum azinphos-ethyl, azinphos-methyl, bendiocarb, bifenthrin of avermectin B1a and B1b only), acetamiprid, (sum of isomers), bixafen, boscalid, bromophos-ethyl, anthraquinone, bifenthrin (sum of isomers), boscalid, cadusafos, carbaryl, carbendazim, carbofuran, buprofezin, carbaryl, carbendazim, chlorfenapyr, carbofuran (3-hydroxy), chlordane (cis), chlordane chlorfenvinphos (sum of E and Z isomers), (oxy), chlordane (trans), chlorfenvinphos (sum of E and chlorothalonil, chlorpyrifos (ethyl), cyhalothrin-lambda Z isomers), chlorobenzilate, chlorpropham, chlorpyrifos (includes cyhalothrin-gamma) (sum of R,S and S,R (ethyl), chlorpyrifos-methyl, coumaphos, cyfluthrin (sum isomers), cypermethrin (sum of constituent isomers), of constituent isomers), cyhalothrin-lambda (includes DDD-pp (TDE), DDE-pp, DDT-op, DDT-pp, cyhalothrin-gamma) (sum of R,S and S,R isomers), deltamethrin, diazinon, dicofol (sum of p,p' and o,p' cypermethrin (sum of constituent isomers), isomers), dimethoate, dinotefuran, diuron, endosulfan I cyproconazole, cyromazine, DDD-pp (TDE), DDE-pp, (alpha), endosulfan II (beta),endosulfan-sulfate, ethion, DDT-op,DDT-pp, deltamethrin, diazinon, dieldrin, fenazaquin, fenitrothion, fenpropathrin, fenpropimorph diflubenzuron, dimethoate, endosulfan I (alpha), (sum of isomers), fenvalerate (sum of constituent endosulfan II (beta),endosulfan-sulfate, endrin, isomers in any ratio including esfenvalerate), fipronil- epoxiconazole, ethoprophos, etofenprox, etoxazole, sulfone, flubendiamide, HCB (hexachlorobenzene), famoxadone, fenitrothion, fenoxycarb, fenpropathrin, HCH-A (alpha hexachlorocyclohexane), HCH-B (beta fenpropidin (sum of fenpropidin and its salts, expressed hexachlorocyclohexane), HCH-G (gamma as fenpropidin), fenpropimorph (sum of isomers), hexachlorocyclohexane / lindane), imidacloprid, linuron, fensulfothion-sulfone, fenthion (parent compound only), malathion, methomyl, monocrotophos, oxadixyl, fenthion-sulfoxide, fenvalerate (sum of constituent permethrin (sum of isomers), phenthoate, phosalone, isomers in any ratio including esfenvalerate), fipronil picoxystrobin, pirimiphos-methyl, procymidone, (parent compound only), fipronil-desulfinyl, fipronil- propargite, propiconazole, pyridaben, pyrimethanil, sulfone, fluazifop (free acid), flufenoxuron, flumethrin, quinalphos, tebuconazole, terbuthylazine, tolfenpyrad, fluquinconazole, flusilazole, fluvalinate (tau), haloxyfop triazophos, trifloxystrobin (free acid), HCB (hexachlorobenzene), HCH-A (alpha hexachlorocyclohexane), HCH-B (beta specified residues hexachlorocyclohexane), HCH-D (delta acetamiprid, aldrin, azoxystrobin, bifenthrin (sum of hexachlorocyclohexane), HCH-G (gamma isomers), chlorpyrifos (ethyl), chlorpyrifos-methyl, hexachlorocyclohexane / lindane), heptachlor, cypermethrin, (sum of constituent isomers), DDE-pp, heptachlor-epoxide (cis), heptachlor-epoxide (trans), deltamethrin, dichlorvos, dieldrin, dimethoate, indoxacarb (sum of indoxacarb and its R enantiomer), endosulfan I (alpha), endosulfan II (beta), endosulfan- lufenuron, malathion, metaflumizone (sum of E and Z sulfate, endrin, ethion, fenpropathrin, fenthion-sulfone, isomers),metazachlor,methacrifos,methamidophos,meth HCH-A (alpha hexachlorocyclohexane), idathion,methiocarb,methiocarb-sulfone,methiocarb- HCH-B (beta hexachlorocyclohexane), sulfoxide, methomyl, methoxychlor, nitrofen, omethoate, HCH-G (gamma hexachlorocyclohexane / lindane), oxamyl, parathion (-ethyl), parathion-methyl, PCB 101, malathion, parathion-methyl, permethrin (sum of PCB 118, PCB 138, PCB 153, PCB 180, PCB 28, PCB isomers), triazophos 52, pendimethalin, permethrin (sum of isomers), phosmet, phoxim, pirimicarb, pirimicarb (desmethyl), recommended monitoring pirimiphos-methyl, prochloraz (parent compound only), abamectin (sum of avermectin B1a and B1b only) profenofos, propetamphos, propoxur, prothioconazole- amitraz (parent compound only), bifenthrin, desthio (sum of isomers), pyrazophos, pyridaben, cypermethrin (sum of constituent isomers), diazinon, pyriproxyfen, quintozene, spinosad (sum of spinosyn A dichlorvos, DMF (N-2,4-dimethylformamide), and D), tebuconazole, tecnazene, teflubenzuron, DMPF (N-2,4-dimethylphenylformamide), etoxazole, tefluthrin, tetrachlorvinphos, tetraconazole, thiacloprid, fipronil (parent compound only), fipronil-desulfinyl, thiamethoxam, thiodicarb, triazophos, trifluralin, fipronil-sulfone, flufenoxuron, pyridaben, pyriproxyfen, vinclozolin thiamethoxam EU red list single residues monitoring aldrin, cadusafos, chlorpropham, demeton-S-methyl, 2,4-DB, AMPA, bromide, chlormequat (sum of demeton-S-methyl-sulfone, demeton-S-methyl-sulfoxide chlormequat and its salts, expressed as chlormequat (oxydemeton-methyl), dieldrin, dimethoate, chloride), dithiocarbamates, ethephon, ETU, fenbutatin diphenylamine, disulfoton, disulfoton-sulfone, disulfoton- oxide, glyphosate, haloxyfop (free acid), maleic sulfoxide, endrin, ethoprophos, fensulfothion hydrazide, mepiquat (sum of mepiquat and its salts, fensulfothion-oxon, fensulfothion-oxon-sulfone, expressed as mepiquat chloride) MPPA, phosphoric fensulfothion-sulfone, fentin (as triphenyltin cation), acid, PTU, quizalofop (free acid) fipronil (parent compound only), fipronil desulfinyl, fipronil sulphone, haloxyfop (free acid), HCB Fat soluble (hexachlorobenzene), heptachlor, nitrofen, omethoate, abamectin (sum of avermectin B1a and B1b only), terbufos, terbufos-sulfone, terbufos-sulfoxide, acephate, aldicarb,aldicarb-sulfone (aldoxycarb), 33 abamectin (sum of avermectin B1a and B1b only), terbufos, terbufos-sulfone, terbufos-sulfoxide, acephate, aldicarb,aldicarb-sulfone (aldoxycarb),

Quaternary Ammonium Compounds BAC 10 (Benzyldimethyldecylammonium Chloride), BAC 12 (Benzyldimethyldodecylammonium Chloride), BAC 14 (Benzyldimethyltetradecylammonium Chloride), BAC 16 (Benzyldimethylhexadecylammonium Chloride), DDAC (Didecyldimethylammonium Chloride)

disinfection by-products BAC 10 (Benzyldimethyldecylammonium Chloride), BAC 12 (Benzyldimethyldodecylammonium Chloride), BAC 14 (Benzyldimethyltetradecylammonium Chloride), BAC 16 (Benzyldimethylhexadecylammonium Chloride), DDAC (Didecyldimethylammonium Chloride), chlorate, perchlorate

specified residues (infant formula) DDD-pp, (TDE), DDE-pp, HCB (hexachlorobenzene), HCH-B (beta hexachlorocyclohexane), HCH-G (gamma hexachlorocyclohexane / lindane), PCB 52, PCB 138

Potential Fish Species

fish speciation Gadus macrocephalus (Tilesius 1810), Gadus morhua (Linnaeus 1758), Hippoglossus hippoglossus (Linnaeus 1758), Limanda limanda (Linnaeus 1758), Melanogrammus aeglefinus (Linnaeus 1758), Merlangius merlangus (Linnaeus 1758), Merluccius merluccius (Linnaeus 1758), Pangasius hypophthalmus (Sauvage 1878), Pleuronectes platessa (Linnaeus 1758), Pollachius virens (Linnaeus 1758), Gadus chalcogrammus (Pallas 1814) (previously Theragra chalcogramma) 34

Potential veterinary drug residues

aminoglycosides illegal dyes (veterinary drugs) apramycin, dihydrostreptomycin, gentamicin, brilliant green, crystal violet, leucomalachite kanamycin, neomycin, paromomycin, spectinomycin, green,malachite green, total malachite green, streptomycin, total aminoglycosides leucocrystal violet, total crystal violet, total veterinary dyes anthelmintics 5-hydroxythiabendazole, albendazole, albendazole-2- nitrofuran metabolites amino-sulfone, albendazole-sulfone, albendazole- AHD (bound), AHD (total), AMOZ (bound), AMOZ sulfoxide, aminoflubendazole, aminomebendazole (total), AOZ (bound), AOZ (total), SEM (bound), SEM (mebendazole amine), amino-oxibendazole, (total), total nitrofuran metabolites cambendazole, clorsulon, closantel, coumaphos, derquantel, febantel, fenbendazole, flubendazole, nitroimidazoles hydroxyflubendazole, hydroxymebendazole, 2-hydroxy dimetridazole (HMMNI), 2-hydroxy ketotriclabendazole, levamisole, mebendazole, ipronidazole, 2-hydroxy metronidazole, dimetridazole, monepantel, monepantel-sulfone, morantel, niclosamide, nitroxinil (nitroxynil), oxfendazole, ipronidazole, metronidazole, ronidazole, total oxfendazole-sulfone, oxibendazole, oxyclozanide, nitroimidazoles rafoxanide, thiabendazole, total albendazole-sulfone, total benzimidazoles, total flubendazole, total macrolides mebendazole, total oxfendazole-sulfone (sum of 3-O-acetyltylosin, erythromycin, gamithromycin, extractable residues which may be oxidized to josamycin, lincomycin, oleandamycin, pirlimycin, oxfendazole sulfone), total thiabendazole, total rifampicin, spiramycin, tildipirosin, tilmicosin, total triclabendazole, triclabendazole, triclabendazole- macrolides, total tylosin, tulathromycin, tylosin A, tylosin sulfone, triclabendazole-sulfoxide B, tylvalosin (aivlosin), virginiamycin

avermectins natural hormones abamectin (avermectin B1a only), doramectin, 17alpha-19-nortestosterone, 17beta-oestradiol emamectin, eprinomectin, ivermectin, moxidectin, total (estradiol), 17beta-testosterone, beta-boldenone, avermectins boldenone, methyltestosterone, total natural hormones

b-agonists non-steroidal anti-inflammatory drugs (NSAIDs) brombuterol, bromchlorbuterol, cimaterol, cimbuterol, 5-hydroxyflunixin, carprofen, diclofenac, flunixin, clenbuterol, clenpenterol, clenproperol, ibuprofen, ketoprofen, meloxicam, naproxen, niflumic hydroxyclenbuterol, hydroxymethylclenbuterol, acid, oxyphenylbutazone, phenylbutazone, tolfenamic isoxsuprine, mabuterol, mapenterol, ractopamine, acid, total NSAIDs, vedaprofen ritodrine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol, total β-agonists phenicols chloramphenicol, florfenicol, florfenicol-amine, b-lactams thiamphenicol amoxicillin, ampicillin, benzyl penicillin (penicillin G), cefalexin, cefalonium, cefapirin, cefazolin, quinolones & fluoroquinolones cefoperazone, cefquinome, cloxacillin, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, desacetylcefapirin, dicloxacillin, nafcillin, oxacillin, flumequine, marbofloxacin, nalidixic acid, norfloxacin, penicillin V oxolinic acid, sarafloxacin, total quinolones

coccidiostats sulfonamides clopidol, decoquinate, diclazuril, DNC (nicarbazin dapsone, sulfachloropyridazine, sulfadiazine, component), halofuginone, lasalocid, maduramycin, sulfadimethoxine, sulfadimidine (sulfamethazine), monensin, narasin, robenidine, salinomycin, sulfadoxine, sulfaguanidine, sulfamerazine, semduramycin, toltrazuril-sulfpne, total coccidiostats sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, glucocorticoids sulfamoxole, sulfanilamide, sulfapyridine, betamethasone, dexamethasone, prednisolone, total sulfaquinoxaline, sulfathiazole, sulfisoxazole, total glucocorticoids sulfonamides

gestagens, altrenogest, chlormadinone, medroxyprogesterone, megestrol, melengestrol, total gestagens 36

Notes: 37