MECHANICAL TESTING AND EVALUATION OF HIGH-SPEED AND LOW-

SPEED FRICTION STIR WELDS

A Thesis by

Nitin Banwasi

Bachelor of Engineering, Bangalore University, Bangalore, India 2000

Submitted to the College of Engineering and the faculty of the Graduate School of Wichita State University in partial fulfillment of the requirements for the degree of Master of Science

Fall 2005

EXPERIMENTAL TESTING AND EVALUATION OF HIGH-SPEED AND LOW-

SPEED FRICTION STIR WELDS

I have examined the final copy of this thesis for form and content and recommend that it be accepted in partial fulfillment of the requirements for the degree of Master of Science, with a major in Mechanical Engineering.

George E. Talia, Committee Chair

We have read this thesis and recommended its acceptance:

Dr. Hamid M. Lankarani, Department Chair, Committee Member

Dr. Krishna K. Krishnan, Committee Member

ii DEDICATION

To My Parents

iii ACKNOWLEDGEMENTS

I am grateful to all that are part of my efforts during my work both academically and personally. I am thankful to my committee chair, Dr.George E.Talia, for being not only supportive in my endeavors but also patient and informative. I appreciate the involvement of both Dr. Hamid M. Lankarani and Dr. Krishna K. Krishnan for their involvement in its fulfillment. I also want to remember fellow student’s help and suggestions in making it possible with gratitude.

iv ABSTRACT

The potential of the Friction Stir (FSW) process is easily observed in the

creation of defect free welds in almost all of the Aluminum alloys. The success and

applicability of the process, however, will depend on the performance of the welds

compared to other joining processes. Experimental testing and evaluation are necessary

for the determination of the mechanical response of Friction Stir Welds and vital to the development and optimization of the FSW process. The goal of this experimental testing of Friction Stir Welds is to obtain the data necessary to begin understanding the effects of the FSW process. An attempt has been made to systematically examine the effects of

FSW process parameters and alloy on the weld properties. An attempt has been made to evaluate and compare High Speed and Low Speed Friction Stir Welds.

v TABLE OF CONTENTS

1. INTRODUCTION 1

1.1. Welding 3

1.2. The physical nature of joining 4

1.3. Welding, from a metallurgical point of view 4

1.4. A metallurgical classification of the welding processes 5

1.5. Types of welding 5

1.6. Solid state welding 7

1.7. 7

1.8. 8

2. ALUMINUM WELDING

2.1. Introduction 9

2.2. Characteristics of Aluminum 10

2.3. Aluminum alloy designation – wrought alloys 11

2.4. Nonheat treatable Aluminum alloys 12

2.5. Heat treatable Aluminum alloys 12

2.6. Wrought Aluminum alloys 12

2.7. Welding Aluminum 14

3.

3.1. Introduction 17

3.2. Different parameters in FSW 18

3.3. Process advantages 20

3.4. Microstructure classification 22

vi 3.5. Joint geometries 24

3.6. Applications 25

4. MECHANICAL TESTING AND METALLOGRAPHY

4.1. Testing 28

4.2. Tensile Test 28

4.3. Tensile Specimens 29

4.4. Hardness Test 30

4.5. Types of hardness tests 31

4.6. Factors for selection of hardness testing methods 32

4.7. Rockwell hardness test 32

4.8. Metallographic specimen preparation basics 34

5. EXPERIMENTAL PROCEDURE

5.1. Tensile test 37

5.2. Hardness test 37

5.3. Metallographic analysis 38

6. RESULTS AND DISCUSSIONS

6.1. Effect of changing welding speed at constant weld pitch 40

6.2. Temper effects on required loads and weld energy 41

6.3. Alloy effects on specific weld energy 42

6.4. Low-speed friction stir weld 1 43

6.5. Low-speed friction stir weld 2 47

6.6. Low-speed friction stir weld 3 53

6.7. Low-speed friction stir weld 4 64

vii 6.8. Low-speed friction stir weld 5 69

6.9. Low-speed friction stir weld 6 73

6.10. Low-speed friction stir weld 7 77

6.11. Low-speed friction stir weld 8 81

6.12. Low-speed friction stir weld 9 88

6.13. Low-speed friction stir weld 10 92

6.14. Tool geometry effects 97

6.15. High-speed friction stir weld 11 100

6.16. High-speed friction stir weld 12 104

6.17. High-speed friction stir weld 13 107

6.18. High-speed friction stir weld 14 110

6.19. High-speed friction stir weld 15 116

6.20. High-speed friction stir weld 16 118

6.21. High-speed friction stir weld 16 119

7. CONCLUSIONS AND FUTURE SCOPE 121

8. REFERENCES 125

viii LIST OF FIGURES

1.1. Friction stir welding process 2

1.2. Master chart of welding and allied processes 6

1.3. Friction stir welding and processing technologies 8

3.1. Friction stir welding 18

3.2. Microstructure of a friction stir weld 20

4.1. Tensile test specimen 29

4.2. Rockwell principle 33

6.1. Required energy and specific weld energy at constant weld pitch 40

6.2. X-axis force for welds made at constant weld pitch 41

6.3. Specific weld energy as a function of welding speed 42

6.4(a). Hardness graph – across the weld 46

6.4(b). Microstructure of the weld 47

6.5(a). Hardness graph – across the weld @ 10”/min 52

6.5(b). Hardness graph – across the weld @ 15”/min 52

6.6(a). Hardness graph – across the weld @ 10”/min 58

6.6(b). Hardness graph – across the weld @ 15”/min 58

6.6(c). Peak/Yield stress of the weld – 10”/min @ 750, 760 & 600 rpm 59

6.6(d). Break stress of the weld – 10”/min @ 750, 760 & 600 rpm 60

6.6(e). Weld 2 – change in stress due to change in welding pitch 61

6.6(f). Weld 3 – change in stress due to change in welding pitch 62

6.6(g). Weld 2 & weld 3 – change in hardness due to change in welding pitch 63

6.7(a). Hardness graph – across the weld 67

ix 6.7(b). Microstructure of the weld nugget 68

6.8(a). Hardness graph – across the weld 72

6.8(b). Microstructure of the weld 73

6.9(a). Hardness graph – across the weld 76

6.10(a). Hardness graph – across the weld 80

6.11(a). Hardness graph – across the weld 84

6.11(b). Peak/yield stress variation 85

6.11(c). Break stress variation 85

6.11(d). Variation in hardness 86

6.12(a). Hardness graph – across the weld 91

6.12(b). Microstructure of the weld nugget 92

6.13(a). Hardness graph – across the weld 95

6.13(b). Microstructures of the weld 96

6.14(a). Specific weld energy as a function of welding speed and tool geometry 97

6.14(b). Required weld power as a function of tool geometry and welding speed 98

6.14(c). Transverse tensile strength of the welds as a function of tool geometry

and welding speed 99

6.14(d). X axis force as a function of tool geometry and welding pitch 99

6.15(a). Hardness graph – across the weld 103

6.15(b). Microstructure of the weld 103

6.16(a). Microstructure of the weld nugget 106

6.17(a). Microstructure of the weld nugget 109

6.18(a). Hardness graph - across the weld 113

x 6.18(b). Microstructure of the weld 113

6.18(c). Variation in peak and yield stress 114

6.18(d). Variation in break stress 114

6.18(e). Variation in hardness 115

xi LIST OF TABLES

6.4(a). Tensile test data of parent 1 – Alclad 2024-T3 43

6.4(b). Tensile test data of parent 2 - Al 7075-T6 44

6.4(c). Tensile test data of the weld 44

6.4(d). Hardness test data – along the weld 45

6.4(e). Hardness test data – across the weld 46

6.5(a). Tensile test data of parent 1 – Alclad 2024-T3 48

6.5(b). Tensile test data of parent 2 – Al 7075-T6 48

6.5(c). Tensile test data of weld @ 10”/min 49

6.5(d). Tensile test data of the weld @ 15”/min 49

6.5(e). Hardness test data – along the weld 51

6.5(f). Hardness test data – across the weld 51

6.6(a). Tensile test data of parent1 – Alclad 2024-T3 54

6.6(b). Tensile test data of parent 2 - Al 7075-T6 54

6.6(c). Tensile test data of the weld @10"/min 55

6.6(d). Tensile test data of the weld @ 15"/min 55

6.6(e). Hardness test data - along the weld 57

6.6(f). Hardness test data - across the weld 57

6.7(a). Tensile test data of parent1 - Alclad 2024-T3 64

6.7(b). Tensile test data of parent 2 - Al 7075-T6 65

6.7(c). Tensile test data of the weld 65

6.7(d). Hardness test data- along the weld 66

6.7(e). Hardness test data - across the weld 67

xii 6.8(a). Tensile test data of parent1 – Alclad 2024-T3 69

6.8(b). Tensile test data of parent2 - Al 7075-T6 69

6.8(c). Tensile test data of the weld 70

6.8(d). Hardness test data – along the weld 71

6.8(e). Hardness test data – across the weld 71

6.9(b). Tensile test data of the parent – Al 6061-T6 74

6.9(b). Tensile test data of the weld 74

6.9(c). Hardness test data – along the weld 75

6.9(d). Hardness test data – across the weld 75

6.10(a). Tensile test data of the parent – Al 6061-T6 77

6.10(b). Tensile test data of the weld 78

6.10(c). Hardness test data – along the weld 79

6.10(d). Hardness test data – across the weld 79

6.11(a). Tensile test data of the parent – Al 6061-T6 81

6.11(b). Tensile test data of the weld 82

6.11(c). Hardness test data - along the weld 83

6.11(d). Hardness test data – across the weld 83

6.12(a). Tensile test data of the parent – Al 2024-T3 88

6.12(b). Tensile test data of the weld 89

6.12(c). Hardness test data – along the weld 90

6.12(d). Hardness data – across the weld 90

6.13(a). Tensile test data of the parent – Alclad 2024-T3 93

6.13(b). Tensile test data of the weld 93

xiii 6.13(c). Hardness test data – along the weld 94

6.13(d). Hardness test data – across the weld 95

6.14. Tool geometry 97

6.15(a). Tensile test data of the parent - Al 7075-T6 100

6.15(b). Tensile test data of the weld 101

6.15(c). Hardness test data – along the weld 102

6.15(d). Hardness test data – across the weld 102

6.16(a). Tensile test data of the parent Al 7075-T6 104

6.16(b). Tensile test data of the weld 105

6.16(c). Hardness test data – along the weld 106

6.17(a). Tensile test data of the parent Al 7075-T6 107

6.17(b). Tensile test data of the weld 108

6.17(c). Hardness test data – along the weld 109

6.18(a). Tensile test data of the parent Al 7075-T6 110

6.18(b). Tensile test data of the weld 111

6.18(c). Hardness test data – across the weld 112

6.18(d). Hardness test data – across the weld 112

6.19(a). Tensile test data of the parent Al 7075-T6 116

6.19(b). Tensile test data of the weld (tilted). 117

6.19(c). Tensile test data of the weld (untilted). 117

6.20(a). Hardness test data of the weld 119

6.21(a). Hardness test data of the weld 120

xiv CHAPTER 1

INTRODUCTION

Friction Stir Welding (FSW) was developed at and patented by The Welding Institute

(Cambridge, UK) in 1991. Since the time of its invention, the process has been continually improved and its scope of application expanded. Friction Stir Welding is a solid state joining process combining deformation heating and mechanical work to obtain high quality, defect free joints. Friction stir welding is especially well suited to joining

Aluminum alloys in a large range of plate thickness and has particular advantages over fusion welding when joining of highly alloyed Aluminum is considered [1].

Because of many demonstrated advantages of FSW over fusion welding techniques, the commercialization of FSW is proceeding at a rapid pace. Much of the work done to bring

FSW to production applications has been of a very practical nature, driven primarily by the pressing industrial need. Industry, federal laboratories and universities have been investigating this technique for joining Aluminum, Steel, Titanium, Metal matrix composites and even hard metals. Research and engineering is rapidly progressing across many fronts. Fundamental research is investigating critical phenomenon through process modeling, microstructure studies, properties and tool wear. FSW has matured to a point where laboratory research is beginning to transition to Aluminum alloy structural applications [1].

1 In principle, Friction Stir Welding is a very simple process. The two plates to be welded are butted together (lap and other configurations are also possible) and clamped to a rigid backing plate. The rotating FSW tool is plunged into the plates at the joint line and traversed along the line, the joint.

Fig 1.1: Friction stir welding process [34].

Because the FSW process has only recently become a subject of wide study, there are currently no large databases of weld properties and, in fact, no specifications on how to make or test friction stir welds currently exist. In general, the process is robust and a wide range of processing parameters and tool designs can be used to make metallurgically sound welds in a given alloy and plate thickness. While weld free of defects may be made using a wide range of processing parameters, the chosen process parameters may significantly affect the mechanical properties of the weld either through direct modification of the weld microstructure or by indirect influence (e.g. by modification of residual stress state) [1].

2 1.1. Welding

Welding can be defined as the joining of two components by a coalescence of the

surfaces in contact with each other. This coalescence can be achieved by melting the two

parts together – fusion welding – or by bringing the two parts together under pressure, perhaps with the application of heat, to form a metallic bond across the interface. This is known as solid phase joining [2].

Welding is by no means a new science. According to some researchers, its origin dates back to the very beginning of the technology of metals. For instance, some welded utensils have been traced to the days of the Sumerian civilization (14th century B.C).

Also, welding is mentioned by the prophet Isaiah in the Old Testament, by the Greek historian Herodotus in his “Clio”, by the Latin writer Pliny the Elder in his “Naturalis

Historia”, and by many other prominent contributors to ancient history. Coming down through the ages, welding and its application progressed rather slowly, principally because of the limitations of the primitive methods used and of the empirical technical knowledge available. However, toward the end of the 19th century and the beginning of

the 20th century, the art and science of welding began to advance at a very rapid pace.

Today it constitutes, by far, one of the most important and widely used tools for the joining of metals [9].

Welding is the most economical and efficient way to join metals permanently. Welding ranks high among industrial processes and involves more sciences and variables than those involved in any other industrial process. In many cases welding is the most cost effective and structurally sound joining technique. Welding can be performed almost any

3 where out doors, indoors, under sea or in space. Some of the processes cause sparks

where as others do not even require extra heat. Most of the things we use in our daily life

are welded.

1.2. The Physical Nature of Joining [5]

Theoretically, to produce a weld, one need only bring the atoms on the opposing metallic

surfaces close enough to establish the spontaneous attractive forces. Ideally, two perfectly

plane surfaces, if treated in this fashion, would be drawn together spontaneously until the distance separating them corresponds to the equilibrium interatomic spacing. At this point, perfect “coalescence” would result and the two objects would merge to comprise a single solid body.

1.3. Welding, From a Metallurgical Point of View [5]

The forces inherent in the metallic objects can bring about perfect coalescence only if:

• The oxides and other non-metallic films present on real metallic surfaces can

either be removed or completely dispersed from the areas being joined.

• The distance separating the metallic atoms on one surface of the proposed joint

from those on the opposing surface of the joint can be reduced consistently to a

value approximately the equilibrium atomic spacing for the metal, thus producing

a metallic bond.

4 1.4. A Metallurgical Classification of the Welding Processes [5]

Basically, it is convenient to divide the welding processes into two major categories:

• The Pressure Welding Processes, in which externally applied forces play an

important role in the bonding operation, whether consummated at room or

elevated temperature.

• The Fusion Welding Processes, in which the joining operation involves melting

and solidification, and any external forces applied to the system play no active

role in producing coalescence.

1.5. Types of Welding

1.

• Shielded Metal Arc Welding

• Gas Metal Arc and Flux Cored Arc Welding

• Electroslag and Electrogas Welding

2. Resistance Welding

3.

4. Oxyfuel Gas Welding

5. Solid State Welding

• Friction Welding

5 • Friction stir welding

• Diffusion Welding

6. Electron Beam Welding

7.

8. Brazing

9. Soldering

10.

Fig 1.2: Master chart of welding and allied processes [30].

6 1.6. Solid State Welding (SSW)

Solid state welding is "a group of welding processes which produces coalescence at

temperatures essentially below the melting point of the base materials being joined

without the addition of a brazing . Pressure may or may not be used".

The oldest of all welding processes belongs to this group. Others include cold welding, diffusion welding, explosion welding, friction welding, hot pressure welding, and . These processes are all different and utilize different

forms of energy for making welds [30].

1.7. Friction Welding

Friction, which requires relative motion, pressure and time, is an efficient thermal energy

source for the welding of materials. Friction welding is a solid state welding process

which produces coalescence of materials by the heat obtained from mechanically induced

sliding motion between rubbing surfaces. The work parts are held together under

pressure. This process usually involves the rotating of one part against another to

generate frictional heat at the junction. When a suitable high temperature has been

reached, rotational motion ceases and additional pressure is applied and coalescence

occurs [33].

7

Fig 1.3: Friction welding and processing technologies [32].

1.8. Rotary Friction Welding

Two variants of the rotary friction welding process have been developed. These are known as conventional ‘continuous drive friction welding’ and stored energy friction welding where the most widely adopted is inertia friction welding. In both these methods, friction welds are made by holding a rotating component in contact with a non-rotating component while under a constant or increasing axial load. The interface reaches the appropriate welding temperature, at which point rotation is stopped and the weld completed [31].

8 CHAPTER 2

ALUMINUM WELDING

2.1. Introduction

Aluminum is the most abundant metal in nature. Some 8% by weight of the Earth’s crust is Aluminum. Many rocks and minerals contain a significant amount of Aluminum.

Unfortunately, Aluminum does not occur in nature in the metallic form. In rocks,

Aluminum is present in the form of silicates and other complex compounds. The ore from which most Aluminum is presently extracted, Bauxite, is a hydrated Aluminum oxide [1].

The existence of Aluminum was postulated by Sir Humphrey Davy in the first decade of the nineteenth century and the metal was isolated in 1825 by Hans Christian Oersted. It remained as somewhat of a laboratory curiosity for the next 30 years when some limited commercial production began, but it was not until 1886 that the extraction of Aluminum from Bauxite became a truly viable industrial process [2].

Pure Aluminum is a silvery-white metal with many desirable characteristics. It is light, nontoxic (as the metal), nonmagnetic and nonsparking. It is somewhat decorative. It is easily formed, machined and cast. Pure Aluminum is soft and lacks strength, but alloys with small amounts of Copper, Magnesium, Silicon, Manganese and other elements have very useful properties [4].

Aluminum is the most difficult metal to weld. Aluminum oxide should be cleaned from the surface prior to welding. Aluminum comes in heat treatable and non heat treatable alloys. Heat treatable aluminum alloys get their strength from a process called ageing.

9 Significant decrease in tensile strength can occurs when welding aluminum due to over aging [3].

2.2. Characteristics of Aluminum [2]

Listed below are the main physical and chemical Characteristics of Aluminum, contrasted with those of Steel:

• The difference in the melting points of the two metals and their oxides. The

oxides of Iron all melt close or below the melting point of the metal; Aluminum

oxide melts at 20600 C, some 14000 C above the melting point of Aluminum.

• The oxide film on Aluminum is durable, highly tenacious and self-healing. This

gives the Aluminum alloys excellent corrosion resistance.

• The coefficient of thermal expansion of Aluminum is approximately twice that of

Steel.

• The coefficient of thermal conductivity of Aluminum is six times that of Steel.

• The specific heat of Aluminum – the amount of heat required to raise the

temperature of a substance – is twice that of Steel.

• Aluminum has high electrical conductivity, only three-quarters that of Copper but

six times that of Steel.

• Aluminum does not change color as its temperature rises.

• Aluminum is non-magnetic.

• Aluminum has a modulus of elasticity three times that of Steel.

10 • Aluminum does not change its crystal structure on heating and cooling, unlike

Steel which undergoes crystal transformations or phase changes at specific

temperatures.

2.3. Aluminum Alloy Designation – Wrought Alloys [6]

Pure Aluminum is readily alloyed with many other metals to produce a wide range of physical and mechanical properties. This means by which the alloying elements strengthen Aluminum are used as the basis to classify Aluminum alloys into two categories: nonheat treatable and heat treatable.

1. First digit – Principal alloying constituent(s)

2. Second digit – Variations of initial alloy

3. Third and fourth digits – Individual alloy variations

• 1xxx – Pure Al (99.00% or greater)

• 2xxx – Al-Cu alloys

• 3xxx – Al-Mn alloys

• 4xxx – Al-Si alloys

• 5xxx – Al-Mg alloys

• 6xxx – Al-Mg-Si alloys

• 7xxx – Al-Zn alloys

• 8xxx – Al + other elements

• 9xxx – Unused series

11 2.4. Nonheat Treatable Aluminum Alloys [6]

The initial strength of the nonheat treatable Aluminum alloys depends primarily upon the

hardening effect of alloying elements such as Silicon, Iron, Manganese and Magnesium.

These elements affect increase in strength either as dispersed phases or by solid solution

strengthening. The nonheat treatable alloys are mainly found in the 1xxx, 3xxx, 4xxx, and 5xxx alloy series depending upon their major alloying elements.

2.5. Heat Treatable Aluminum Alloys [6]

The initial strength of Aluminum alloys in this group depends upon the alloy composition, just as the nonheat treatable alloys. Heat treatable Aluminum alloys develop their properties by solution heat treating and quenching, followed by either natural or artificial aging. The heat treatable alloys are found primarily in the 2xxx, 6xxx and 7xxx alloy series.

2.6. Wrought Aluminum Alloys [6, 2]

1xxx: This series represent the commercially pure Aluminum, ranging from the baseline

1100 (99% min Al) to relatively purer 1050/1350 (99.5% min Al) and 1175 (99.75% min

Al).These grades of Aluminum are characterized by excellent corrosion resistance, high thermal and electrical conductivities, low mechanical properties, and excellent workability. Moderate increases in strength may be obtained by strain hardening. Iron and silicon are the major impurities.

12 2xxx: The major alloying element in 2xxx series alloys is Copper. The alloys in this series are heat treatable and possess good combinations of high strength (especially at elevated temperatures), toughness and in specific cases, . They are not resistant to atmospheric corrosion and so are usually painted or clad in such exposures.

3xxx: The major alloying element in 3xxx series alloys is Manganese. These alloys are strain hardenable, have excellent corrosion resistance and are readily welded, brazed and soldered.

4xxx: The major alloying element in 4xxx series alloys is Silicon, which can be added in sufficient quantities (up to 12%) to cause substantial lowering of the melting range. For this reason, Aluminum-Silicon alloys are used in welding wire and as brazing alloys for joining Aluminum, where a lower melting range than that of the base metal is required.

These alloys have good flow characteristics and medium strength.

5xxx: The major alloying element is Magnesium and when it is used as a major alloying element or with Manganese, the result is a moderate-to-high-strength work-hardenable alloy. Magnesium is considerably more effective than Manganese as a hardener, about

0.8% Mg being equal to 1.25% Mn, and it can be added in considerably higher quantities. Alloys in this series possess excellent corrosion resistance even in salt water and very high toughness even at cryogenic temperature to near absolute zero.

6xxx: Alloys in the 6xxx series contain Silicon and Magnesium. Although not as strong as most 2xxx and 7xxx alloys, 6xxx series alloys have relatively good formability,

13 weldability, machinability, and relatively good corrosion resistance, with medium strength.

7xxx: Zinc, in amounts of 1 to 8% is the major alloying element in 7xxx series alloys.

These alloys are heat treatable and possess very high strength.

8xxx: The alloys in this series have high conductivity, strength and hardness.

2.7. Welding Aluminum

GTAW Welding

Gas Tungsten Arc Welding (GTAW) is frequently referred to as TIG welding. TIG welding is a commonly used high quality welding process. TIG welding has become a popular choice of welding processes when high quality, precision welding is required.

In TIG welding an arc is formed between a non consumable tungsten and the metal being welded. Gas is fed through the torch to shield the electrode and molten weld pool. If filler wire is used, it is added to the weld pool separately.

MIG Welding

Gas Metal Arc Welding (GMAW) is frequently referred to as MIG welding. MIG welding is a commonly used high deposition rate welding process. Wire is continuously fed from a spool. MIG welding is therefore referred to as a semiautomatic welding process.

14 Flux Cored Welding

Flux Cored Arc Welding (FCAW) is frequently referred to as flux cored welding. Flux cored welding is a commonly used high deposition rate welding process that adds the benefits of flux to the welding simplicity of MIG welding. As in MIG welding wire is continuously fed from a spool. Flux cored welding is therefore referred to as a semiautomatic welding process.

Self shielding flux cored arc welding wires are available or gas shielded welding wires may be used. Flux cored welding is generally more forgiving than MIG welding. Less precleaning may be necessary than MIG welding. However, the condition of the base metal can affect weld quality. Excessive contamination must be eliminated.

Stick Welding

Shielded Metal Arc Welding (SMAW) is frequently referred to as stick or covered electrode welding. Stick welding is among the most widely used welding processes.

The flux covering the electrode melts during welding. This forms the gas and to shield the arc and molten weld pool. The slag must be chipped off the weld bead after welding. The flux also provides a method of adding scavengers, deoxidizers, and alloying elements to the weld metal.

Resistance Welding

Resistance (RSW), Resistance Seam Welding (RSEW), and Projection

Welding (PW) are commonly used resistance welding processes. Resistance welding

15 uses the application of electric current and mechanical pressure to create a weld between

two pieces of metal. Weld conduct the electric current to the two pieces of

metal as they are forged together.

The welding cycle must first develop sufficient heat to raise a small volume of metal to

the molten state. This metal then cools while under pressure until it has adequate strength

to hold the parts together. The current density and pressure must be sufficient to produce

a weld nugget, but not so high as to expel molten metal from the weld zone.

Electron Beam Welding

Electron Beam Welding (EBW) is a fusion joining process that produces a weld by

impinging a beam of high energy electrons to heat the weld joint. Electrons are

elementary atomic particles characterized by a negative charge and an extremely small

mass. Raising electrons to a high energy state by accelerating them to roughly 30 to 70 percent of the speed of light provides the energy to heat the weld.

The electron beam is always generated in a high vacuum. The use of specially designed orifices separating a series of chambers at various levels of vacuum permits welding in medium and no vacuum conditions. Although, high vacuum welding will provide maximum purity and high depth to width ratio welds.

16 CHAPTER 3

FRICTION STIR WELDING

3.1. Introduction [11]

Conventional friction welding has been around for many years, but relies on relative motion between the parts to be joined while pressure is applied. The need to move one or both parts restricts the conventional friction process between relatively simple shapes – thus joining plate or sheet is almost impossible. In Friction Stir Welding (FSW), a cylindrical, shouldered tool with a profiled probe is rotated and slowly plunged into the joint line between two pieces of sheet or plate material, which are butted together. The parts have to be clamped onto a backing bar in a manner that prevents the abutting joint faces from being forced apart. Frictional heat is generated between the wear resistant welding tool and the material of the work pieces. This heat causes the latter to soften without reaching the melting point and allows traversing of the tool along the weld line.

The plasticized material is transferred from the leading edge of the tool to the trailing edge of the tool probe and is forged by the intimate contact of the tool shoulder and the pin profile. It leaves a solid phase bond between the two pieces. The process can be regarded as a solid phase keyhole welding technique since a hole to accommodate the probe is generated, then filled during the welding sequence.

17

Figure 3.1: Friction stir welding [11].

3.2. Different parameters in FSW [11]

The whole of rotating device between the machine spindle and the work piece is referred

to as the ‘tool’. The part of the tool, which is embedded in work piece during welding, is referred to as the ‘probe’. The part of the tool, which is pressed onto the surface of the work piece during welding, is referred to as the ‘shoulder’.

In a non-cylindrical tool the terms ‘leading edge’ (front face of shoulder during welding) and ‘trailing edge’ (rear face of shoulder during welding) are used, whereas in cylindrical tools there is clearly no edge, and so the terms ‘leading face’ and ‘trailing face’ may be

preferred. ‘Probe leading face’ is the front face of the probe during welding. Similarly

‘probe trailing face’ is the rear face of the probe during welding.

As the tool may in some circumstances be tilted through a small angle, part of the

shoulder may be embedded deeper into the work piece. That part of the shoulder which

experiences the greatest penetration is referred to as the ‘heel’ and the maximum depth of

the shoulder penetration below the work piece surface is defined as the ‘heel plunge

18 depth’. The angle of tilt is referred to as the ‘tilt angle’, or ‘travel angle’. In some instances the tool is tilted sideways, and in this case the angle is described as the

‘sideways tilt angle’ or ‘work angle’.

The side of the weld where the local direction of the tool is the same as the traversing direction or the side of the weld where direction is the same as the direction of rotation of the shoulder is called the ‘advancing side’. Similarly, the side where the directions are opposite and the local movement of the shoulder is against the traversing direction or side of the weld where direction of travel is opposed to direction of rotation of shoulder is called the ‘retreating side’. The total area of the tool on the work piece surface is described as the ‘tool shoulder footprint’.

The term ‘Welding speed’ is preferred to traversing speed or traversing rate, which is the rate of travel of tool along joint line. ‘Tool Rotation speed’ is the rotation speed of the friction stir welding tool. ‘Clockwise Rotation’ is when viewed from above the tool, looking down onto the work piece.

Forces are an important part of friction stir welding technology. The force applied parallel to the axis of rotation of the tool (Z-direction) is the ‘down force’, and the force applied parallel to the welding direction (X-direction) is the ‘traversing force’. The force developed in a direction perpendicular to both X and Z forces is ‘Side force’ (Y- direction).

19 3.3. Process Advantages [11]

The key benefits of this newly developed welding process include an increase in joint efficiency and process robustness, as well as a greater range of applicable alloys that can be welded. Friction Stir Welding will permit production-welding opportunities relative to dissimilar alloys and materials previously thought to be "unweldable" such as Aluminum alloy. Composite materials are also candidate materials for this welding process. Friction

Stir Welding's solid-phase, low distortion welds are achieved with relatively low costs, use simple energy efficient mechanical equipment, and require minimal operator expertise and training. The process advantages result from the fact that the FSW process

(as all Friction Welding of metals) takes place in the solid phase below the melting point of the materials to be joined. The benefits therefore include the ability to join materials that are difficult to fusion weld, for example 2000 and 7000 Aluminum. Other advantages are as follows:

• Low distortion, even in long welds

• Excellent mechanical properties as proven by fatigue, tensile and bend tests

• No fume, No porosity

• No spatter

• Low shrinkage

• Can operate in all positions

• Energy efficient

20 Friction Stir Welding can use existing and readily available machine tool technology. The process is also suitable for automation and adaptable for robot use. Its main advantages are:

• Non-consumable tool, No filler wire

• One tool can typically be used for up to 1000m of weld length in 6000 series

aluminum alloys

• No gas shielding for welding aluminum

• No certification required

• Some tolerance to imperfect weld preparations - thin oxide layers can be accepted

• No grinding, brushing or pickling required in mass production

The limitations of the FSW process are being reduced by intensive research and development. However, the main limitations of the FSW process are at present:

• Welding speeds are moderately slower than those of some fusion welding

processes (up to 750mm/min for welding 5mm thick 6000 series aluminum alloy

on commercially available machines)

• Work pieces must be rigidly clamped

• Backing bar required

• Keyhole at the end of each weld

The repeatable quality of the solid-phase welds can improve existing products and lead to a number of new product designs previously not possible. Welds with the highest quality can be achieved by Friction Stir Welding. The crushing, stirring and forging action of the

21 FSW tool produces a weld with a finer microstructure than the parent material. The weld metal strength can be, in the as welded condition, in excess of that in the thermo- mechanically affected zone.

3.3. Microstructure Classification [11]

The first attempt at classifying microstructures was made by P L Threadgill (Bulletin,

March 1997). This work was based solely on information available from Aluminum alloys. However, it has become evident from work on other materials that the behavior of

Aluminum alloys is not typical of most metallic materials, and therefore the scheme cannot be broadened to encompass all materials. It is therefore proposed that the following revised scheme is used. This has been developed at TWI, but has been discussed with a number of appropriate people in industry and academia, and has also been provisionally accepted by the Friction Stir Welding Licensees Association. The system divides the weld zone into distinct regions as follows:

Figure 3.2: Microstructure of a friction stir weld [11].

A. Unaffected material or parent metal

B. Heat affected zone (HAZ)

22 C. Thermo-mechanically affected zone (TMAZ)

D. Weld Nugget

Unaffected material or parent metal: This is material remote from the weld, which has not been deformed, and which although it may have experienced a thermal cycle from the weld is not affected by the heat in terms of microstructure or mechanical properties.

Heat affected zone (HAZ): In this region, which clearly will lie closer to the weld centre, the material has experienced a thermal cycle, which has modified the microstructure and/or the mechanical properties. However, there is no plastic deformation occurring in this area. In the previous system, this was referred to as the "thermally affected zone". The term heat affected zone is now preferred, as this is a direct parallel with the heat affected zone in other thermal processes, and there is little justification for a separate name.

Thermo-mechanically affected zone (TMAZ): In this region, the Friction Stir Welding tool has plastically deformed the material, and the heat from the process will also have exerted some influence on the material. In the case of aluminum, it is possible to get significant plastic strain without recrystallisation in this region, and there is generally a distinct boundary between the recrystallised zone and the deformed zones of the TMAZ.

In the earlier classification, these two sub-zones were treated as distinct micro structural regions. However, subsequent work on other materials has shown that aluminum behaves in a different manner to most other materials, in that it can be extensively deformed at high temperature without recrystallisation. In other materials, the distinct recrystallised

23 region (the nugget) is absent, and the whole of the TMAZ appears to be recrystallised.

This is certainly true of materials, which have no thermally induced phase transformation, which will in itself induce recrystallisation without strain, for example pure Titanium, b

Titanium alloys, Austenitic Stainless Steels and Copper. In materials such as Ferritic

Steels and a-b Titanium alloys (e.g.Ti-6Al-4V), understanding the microstructure is made more difficult by the thermally induced phase transformation, and this can also make the

HAZ/TMAZ boundary difficult to identify precisely.

Weld Nugget: The recrystallised area in the TMAZ in Aluminum alloys has traditionally been called the nugget. Although this term is descriptive, it is not very scientific.

However, its use has become widespread, and as there is no word, which is equally simple with greater scientific merit, this term has been adopted. It has been suggested that the area immediately below the tool shoulder (which is clearly part of the TMAZ) should be given a separate category, as the grain structure is often different here. The microstructure here is determined by rubbing by the rear face of the shoulder, and the material may have cooled below its maximum. It is suggested that this area is treated as a separate sub-zone of the TMAZ.

3.4. Joint Geometries

The process has been used for the manufacture of butt welds; overlap welds, T-sections, fillet, and corner welds. For each of these joint geometries specific tool designs are required which are being further developed and optimized. Longitudinal butt welds and circumferential lap welds of Al alloy fuel tanks for space flights have been Friction Stir

Welded and successfully tested.

24 The FSW process can also cope with circumferential, annular, non-linear, and three- dimensional welds. Since gravity has no influence on the solid-phase welding process, it can be used in all positions, viz:

1. Horizontal

2. Vertical

3. Overhead

4. Orbital

3.5. Applications

Shipbuilding and marine industries

The and marine industries are two of the first industry sectors, which have adopted the process for commercial applications. The process is suitable for the following applications:

• Panels for decks, sides, bulkheads and floors

• Aluminum extrusions

• Hulls and superstructures

• Helicopter landing platforms

• Offshore accommodation

• Marine and transport structures

• Masts and booms, e.g. for sailing boats

• Refrigeration plant

25 Aerospace industry

At present the aerospace industry is welding prototype parts by Friction Stir Welding.

Opportunities exist to weld skins to spars, ribs, and stringers for use in military and civilian aircraft. This offers significant advantages compared to riveting and from solid, such as reduced manufacturing costs and weight savings. Longitudinal butt welds and circumferential lap welds of Al alloy fuel tanks for space vehicles have been friction stir welded and successfully tested. The process could also be used to increase the size of commercially available sheets by welding them before forming. The Friction Stir

Welding process can therefore be considered for:

• Wings, fuselages, empennages

• Cryogenic fuel tanks for space vehicles

• Aviation fuel tanks

• External throw away tanks for military aircraft

• Military and scientific rockets

• Repair of faulty MIG welds

Railway industry

The commercial production of high-speed trains made from Aluminum extrusions which may be joined by friction stir welding has been published. Applications include:

• High speed trains

• Rolling stock of railways, underground carriages, trams

• Railway tankers, goods wagons and Container bodies

26 Land transportation

The friction stir welding process is currently being experimentally assessed by several

automotive companies and suppliers to this industrial sector for its commercial

application. A joint EWI/TWI Group Sponsored Project is investigating representative joint designs for automotive lightweight structures. Potential applications are:

• Engine, chassis cradles and wheel rims

• Attachments to hydro formed tubes

• Tailored blanks, e.g. welding of different sheet thicknesses

• Space frames, e.g. welding extruded tubes to cast nodes

• Truck bodies, Tail lifts for lorries, Mobile cranes

• Armor plate vehicles and Fuel tankers

• Ships, buses and airfield transportation vehicles

• Motorcycle, bicycle frames and Repair of aluminum cars

• Articulated lifts and personnel bridges

• Magnesium and magnesium/aluminum joints

Construction industry

The use of portable FSW equipment is possible for:

• Aluminum bridges

• Facade panels made from aluminum, copper or titanium

• Window frames and Aluminum pipeline.

27 CHAPTER 4

MECHANICAL TESTING AND METALLOGRAPHY

4.1. Testing [7]

Mechanical testing of materials is generally performed for one of the following reasons:

1. Test development: to create or refine the test method itself.

2. Design: to create or select materials for specific applications.

3. Quality control: to verify that incoming material is acceptable.

4.2. Tensile Test [7]

Uniaxial tensile test is one of the most frequently performed mechanical tests. This type of test generally involves gripping a specimen at both ends and subjecting it to increasing axial load until it breaks. Recording of load and elongation data during the test allows the investigator to determine several characteristics about the mechanical behavior of the material.

There are several reasons for performing tensile tests. The results of tensile tests are used in selecting materials for engineering applications. Tensile properties frequently are included in material specifications to ensure quality. Tensile properties often are measured during development of new materials and processes, so that different materials and processes can be compared. Finally, tensile properties often are used to predict the behavior of a material under forms of loading other than uniaxial tension.

28 The strength of a material often is the primary concern. The strength of interest may be measured in terms of either the stress necessary to cause appreciable plastic deformation or the maximum stress that the material can withstand. Also of interest is the material’s ductility, which is a measure of how much it can be deformed before it fractures. Low ductility in a tensile test often is accompanied by low resistance to fracture under other forms of loading.

4.3. Tensile Specimens [7]

The figure below shows a typical tensile test specimen. It has enlarged ends or shoulders for gripping. The important part of the specimen is the gage section. The cross-sectional area of the gage section is reduced relative to that of the remainder of the specimen so that deformation and failure will be localized in this region. The gage length is the region over which measurements are made and is centered within the reduced section. The distances between the ends of the gage section and the shoulders should be great enough so that the larger ends do not constrain deformation within the gage section.

Figure 4.1: Tensile test specimen [11].

29 A tensile test involves mounting the specimen in a machine and subjecting it to tension.

The tensile force is recorded as a function of the increase in gage length. When force- elongation data are converted to engineering stress and strain, a stress-strain curve that is identical in shape to the force-elongation curve can be plotted. The advantage of dealing with stress versus strain rather than load versus elongation is that the stress-strain curve is virtually independent of specimen dimensions.

4.4. Hardness Test [8]

Hardness has a variety of meanings. To the metal industry, it may be thought of as resistance to permanent deformation. To the metallurgist, it means resistance to penetration. To the lubrication engineer, it means resistance to wear. To the design engineer, it is a measure of flow stress. To the mineralogist, it means resistance to scratching. To the machinist, it means resistance to machining. Hardness may also be referred to as mean contact pressure. All of these characteristics are related to the plastic flow stress of materials.

Hardness test is one of the most valuable and widely used mechanical tests for evaluating the properties of metals as well as certain other materials. The hardness of a material usually is considered resistance to permanent indentation. In general, an indenter is pressed into the surface of the metal to be tested under a specific load for a definite time interval and a measurement is made of the size or depth of the indentation. Hardness is not a fundamental property of a material. Hardness values are arbitrary and there are no absolute standards of hardness. Hardness has no quantitative value, except in terms of a

30 given load applied in a specific manner for a specified duration and a specified penetrator shape.

The principal purpose of the hardness test is to determine the suitability of a material for a given application or the particular treatment to which the material has been subjected.

The importance of hardness testing has to do with the relationship between hardness and other properties of material. The hardness test is simple, easy and relatively nondestructive.

Hardness test is divided into two categories: Macrohardness and Microhardness.

Macrohardness refers to testing with applied loads on the indenter of more than 1 Kg and covers, for example, the testing of tools, dies and sheet material in the heavier gages. In microhardness testing, applied loads are 1 Kg and below and material being tested is very thin (down to 0.0125 mm). Applications include extremely small parts, thin superficially hardened parts, plated surfaces and individual constituents of materials.

4.5. Types of Hardness Tests [8]

1. Indentation tests

2. Microhardness testing

3. Scratch hardness test

4. Special indentation tests

5. Rebound principle

6. Abrasion and erosion testing

7. Laboratory wear tests

31 8. Service tests

9. Electromagnetic testing

4.6. Factors for Selection of Hardness Testing Methods [8]

1. Hardness range of the test material

2. Size of the workpiece

3. Shape of the workpiece

4. Degree of flatness of the workpiece

5. Surface condition of the workpiece

6. Nature of the test material: homogeneous or nonhomogeneous

7. Effect of indentation marks

8. Number of identical pieces to be tested

9. Equipment availability

4.7. Rockwell Hardness Test [15]

The Rockwell hardness test method consists of indenting the test material with a diamond cone or hardened steel ball indenter. The indenter is forced into the test material under a preliminary minor load F0 usually 10 kgf. When equilibrium has been reached, an indicating device, which follows the movements of the indenter and so responds to changes in depth of penetration of the indenter, is set to a datum position. While the preliminary minor load is still applied an additional major load is applied with resulting increase in penetration. When equilibrium has again been reach, the additional major load is removed but the preliminary minor load is still maintained. Removal of the additional

32 major load allows a partial recovery, so reducing the depth of penetration. The permanent increase in depth of penetration, resulting from the application and removal of the additional major load is used to calculate the Rockwell hardness number.

HR = E - e

F0 = preliminary minor load in kgf

F1 = additional major load in kgf

F = total load in kgf e = permanent increase in depth of penetration due to major load F1 measured in units of

0.002 mm

E = a constant depending on form of indenter: 100 units for diamond indenter, 130 units for steel ball indenter

HR = Rockwell hardness number

D = diameter of steel ball

Figure 4.2: Rockwell Principle [15]

33 Advantages of the Rockwell hardness method include the direct Rockwell hardness number readout and rapid testing time. Disadvantages include many arbitrary non-related scales and possible effects from the specimen support anvil.

4.8. Metallographic Specimen Preparation Basics [14]

Metallography is the study of a materials microstructure. Analysis of a materials microstructure aids in determining if the material has been processed correctly and is therefore a critical step for determining product reliability and for determining why a material failed. The basic steps for proper metallographic specimen preparation include:

Documentation - Metallographic analysis is a valuable tool. By properly documenting the initial specimen condition and the proceeding microstructural analysis, metallography provides a powerful quality control as well as an invaluable investigative tool.

Sectioning and Cutting - Following proper documentation, most metallographic samples need to be sectioned to the area of interest and for easier handling. Depending upon the material, the sectioning operation can be obtained by abrasive cutting (metals and metal matrix composites), diamond wafer cutting (ceramics, electronics, biomaterials, minerals), or thin sectioning with a microtome (plastics).

Proper sectioning is required to minimize damage, which may alter the microstructure and produce false metallographic characterization. Proper cutting requires the correct selection of abrasive type, bonding, and size; as well as proper cutting speed, load and coolant.

34 Mounting - The mounting operation accomplishes three important functions (1) it protects the specimen edge and maintains the integrity of a materials surface feature (2) fills voids in porous materials and (3) improves handling of irregular shaped samples, especially for automated specimen preparation. The majority of metallographic specimen mounting is done by encapsulating the specimen into a compression mounting compound

(thermosets - phenolics, epoxies, diallyl phthalates or thermoplastics - acrylics), casting into ambient cast able mounting resins (acrylic resins, epoxy resins, and polyester resins), and gluing with a thermoplastic glues.

Planar Grinding - or course grinding is required to planarize the specimen and to reduce the damage created by sectioning. The planar grinding step is accomplished by decreasing the abrasive grit/ particle size sequentially to obtain surface finishes that are ready for polishing. Care must be taken to avoid being too abrasive in this step, and actually creating greater specimen damage than produced during cutting (this is especially true for very brittle materials such as silicon).

The machine parameters which effect the preparation of metallographic specimens includes: grinding/polishing pressure, relative velocity distribution, and the direction of grinding/polishing.

Rough Polishing - The purpose of the rough polishing step is to remove the damage produced during cutting and planar grinding. Proper rough polishing will maintain specimen flatness and retain all inclusions or secondary phases. By eliminating the previous damage and maintaining the microstructural integrity of the specimen at this

35 step, a minimal amount of time should be required to remove the cosmetic damage at the final polishing step.

Rough polishing is accomplished primarily with diamond abrasives ranging from 9 micron down to 1 micron diamond. Polycrystalline diamond because of its multiple and small cutting edges, produces high cut rates with minimal surface damage, therefore it is the recommended diamond abrasive for metallographic rough polishing on low napped polishing cloths.

Final Polishing - The purpose of final polishing is to remove only surface damage. It should not be used to remove any damage remaining from cutting and planar grinding. If the damage from these steps is not complete, the rough polishing step should be repeated or continued.

Etching - The purpose of etching is to optically enhance microstructural features such as grain size and phase features. Etching selectively alters these microstructural features based on composition, stress, or crystal structure. The most common technique for etching is selective chemical etching and numerous formulations have been used over the years. Other techniques such as molten salt, electrolytic, thermal and plasma etching have also found specialized applications.

36 CHAPTER 5

EXPERIMENTAL PROCEDURE

5.1. Tensile test

The most common measure of FSW quality after visual inspection for surface breaking defects may be the transverse tensile test (loading direction perpendicular to the welding direction) [1]. The objective of transverse tensile test is to determine whether or not the weld is suitable for its intended use. The Low-Speed Friction Stir welds and the High-

Speed Friction Stir welds were cut into straps perpendicular to the welding direction.

These straps were then cut or machined into a ‘dog-bone’ shape, according to the ASTM standards. The tensile tests were carried out at room temperature at a crosshead speed of

1 mm/min using a computer controlled testing machine. Load and strain ranges were selected so that the test will fit the range. The tensile properties of each weld were evaluated by a number of samples or tensile specimens cut from the same weld. The data obtained from the tensile test such as Peak load, Break stress, Peak stress, Yield stress and the elongation were recorded. These properties of the weld were then compared with that of its parent metal to obtain the weld or joint efficiency.

5.2. Hardness Test

Rockwell hardness tester was employed to measure the hardness of the welds. The hardness was measured in two ways:

37 Along the weld or longitudinal hardness of the weld: The hardness values of the weld were recorded on the weld, from the starting point of the weld to the end point. This shows the variation of the weld hardness from beginning to the end of the weld.

Across the weld or transverse hardness of the weld: Hardness measurements were made across a weld, in a line, perpendicular to the welding direction. Made on the top surface of the weld, a hardness traverse is a useful tool to help identify the weak zones of a weld.

The hardness values of the weld were then compared with that of its parent metal to obtain the relative hardness of the weld or the hardness joint efficiency.

5.3. Metallographic Analysis

Metallographic analyses of the welds were carried out to detect weld defects present and the microstructure of the weld zone. The welds were cross-sectioned perpendicularly to the welding direction for metallographic analyses. These samples were then mounted in a transparent epoxy. These mounted samples were then grinded and polished on abrasive silicon carbide sheets. The samples were then fine polished, etched with Keller’s reagent and observed by optical microscopy.

38 CHAPTER 6

RESULTS AND DISCUSSIONS

In the early days of Friction Stir Welding, most welding was performed on modified machine tools. The level of instrumentation available for process monitoring was often minimal leading to a great deal of speculation on the quantitative effects of process variable and tool geometry changes. Generally, these changes were correlated either with improved joint strength or the ability to make a weld with greater speed: these are at best indirect correlations with the true, physical, process changes. As the sophistication of

FSW equipment has increased, so has our ability to quantify the effects of process variables. Correlation between the indirect effects of process changes and the direct effects will greatly enhance our understanding of the process. With sufficient understanding of these effects and high fidelity models of the process developed using this understanding, we may in time be able to predict many of the effects which must now be determined via trial and error [21].

Because the FSW process has only recently become a subject of wide study, there are currently no large databases of weld properties and, in fact, no specifications on how to make or test friction stir welds currently exist. In general, the process is robust and a wide range of processing parameters and tool designs can be used to make metallurgically sound welds in a given alloy and plate thickness. While weld free of defects may be made using a wide range of processing parameters, the chosen process parameters may significantly affect the mechanical properties of the weld either through direct

39 modification of the weld microstructure or by indirect influence (e.g. by modification of residual stress state) [1].

6.1. Effect of Changing Welding Speed at Constant Weld Pitch [21]

A series of welds was made in 6.4 mm thick plate at a weld pitch of 0.43 mm/rev. In order to maintain constant weld pitch, the welding speed and the rpm were increased by the same factors for the various welds. Z axis load was varied to accommodate the varying weld speeds.

) 3000 m m / 2500 (J y g 2000 er n Specific weld energy E

r 1500 power ) o 1000 atts (w

r 500 e w o 0 P 0246 welding speed, mm/s

Fig 6.1: Required power and specific weld energy at constant weld pitch.

In the Fig 6.1, the relationship of weld power and the specific weld energy to welding speed at constant weld pitch is illustrated. Weld energy decreases and the required power increases with increasing welding speed at constant weld pitch. This indicates that weld pitch is not, as sometimes suggested, a very good indicator of weld energy. Neither does an advance per revolution that produces good welds at one speed guarantee good welds at another.

40

12

10

N

k 8 , e c r

o 6 f

is x

a 4 - X 2

0 0123456 Welding speed, mm/s

Fig 6.2: X-axis force for welds made at constant weld pitch.

In the Fig 6.2, the relationship of X axis force to welding speed at constant weld pitch is illustrated. The increase in X axis force with increasing welding speed at constant weld pitch may indicate that the material being involved in the process is in different stages of evolution when welded using different speeds. It is also interesting to note the lack of profound effect of the Z axis force on the weld energy and power.

6.2. Temper Effects on Required Loads and Weld Energy [21]

Alloys 7075 and 7050 were each welded in three different tempers (0, T6 and T7). The plate thickness was 9.5 mm and the same tool was used for all welds. All six welds were made using 240 rpm tool rotation rate and 2.4 mm/s welding speed. For all six welds, the x axis forces did not vary by more than 12%. The weld energies for both 7050 and 7075 varied by less than 3%. These results indicate that the composition is critical and the welding forces and torques may be independent of starting microstructure.

41 6.3. Alloy Effects on Specific Weld Energy [21]

Al 6061-T6, Al 7075-T6 and Al 2024-T3 were welded at three different welding speeds

of 1.3 mm/s, 2.4 mm/s and 3.3 mm/s. For each weld, the specific weld energy decreases

with increase in welding speed. This effect may be observed in Fig 6.3.

2500 m

m 2000 J/ ,

y g 7075-T6

er 1500

en 6061-T6 d l 1000 e 2024-T3 w

c i f

i 500 c e

p S 0 01234 Welding Speed, mm/s

Fig 6.3: Specific weld energy as a function of welding speed.

The highest energy per unit weld length is observed when welding alloy 6061. This is

probably because of the relatively high thermal conductivity of the alloy and hence,

thermal energy would diffuse away from the weld zone at the greatest rate in 6061. The relative changes in weld energy associated with decreasing welding speed are essentially

the same for all the alloys tested.

42 6.4. LOW-SPEED FRICTION STIR WELD 1

Weld Specifications

Materials: Alclad 2024-T3 (0.080”) & Al 7075-T6 (0.040”)

Type of Joint: Lap

Welding Speed: 10”/min

Rotational Speed: 750 rpm

Tool Shoulder Diameter: 0.375 in

6.4.1. Tensile Test – Parent 1 (Alclad 2024-T3)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 1121.63 37387.70 35441.30 16.20 37387.70 15.2 735124

2 1121.63 56081.60 53648.60 16.00 56081.60 13.8 1084599

3 1121.63 56081.60 53648.60 15.00 56081.60 13.7 998141

Avg 1121.63 49850.30 47579.5 15.70 49850.30 14.2 939288

Table 6.4(a): Tensile test data of parent 1 – Alclad 2024-T3.

43 6.4.2. Tensile Test – Parent 2 (Al 7075-T6)

Peak Peak Break Break Yield Yield Tangent SI Load Stress Stress Elongation Stress Elongation Modulus

(lb) (psi) (psi) (%) (psi) (%) (psi)

1 722.61 72261.30 70314.90 11.10 72261.30 8.8 2324608

2 712.88 71288.10 68368.50 10.30 71288.10 8.8 2035341

3 693.42 69341.70 67395.30 10.20 69341.70 8.6 2086943

Avg 709.64 70963.70 68692.90 10.50 70963.70 8.6 2148964

Table 6.4(b): Tensile test data of parent 2 - Al 7075-T6.

6.4.3. Tensile Test - Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 1637.44 54581.20 54256.80 7.30 54581.20 7.30 911848

2 1715.29 57176.50 56852.10 8.10 57176.50 8.10 924842

3 1520.65 50688.40 50364.00 6.20 50688.40 6.20 980258

4 1549.85 51661.60 51661.60 7.00 51661.60 7.10 843674

Avg 1566.53 52217.73 51986.01 7.10 52217.73 7.1 941437

Table 6.4(c): Tensile test data of the weld.

44

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent 1

(Alclad 2024-T3) are 1.09 and 1.05 for Break stress and Peak / Yield stress

respectively. This implies that the tensile strength of the weld is more than parent

1.

• The joint efficiencies of the weld with respect to parent 2 (Al 7075-T6) are 0.76

and 0.74 for Break stress and Peak / Yield stress respectively. This implies that

the tensile strength of the weld is less than parent 2.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• All the weld tensile test specimens fractured in the TMAZ on the retreating side.

• Parent 2, even though has a better tensile properties than parent 1, was the first to

fracture. This might be due to the constant contact of parent 2 with tool shoulder.

6.4.4. Hardness Test – Along the Weld

Parent SI No Weld Al 7075-T6 Alclad 2024-T3

1 84.30 70.00 77.00 2 84.00 69.40 74.60 3 84.70 68.90 74.60 4 84.00 70.20 76.50 Avg 84.25 69.63 75.68

Table 6.4(d): Hardness test data – along the weld.

45 6.4.5. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

83.80 81.10 73.40 73.80 72.50 76.80 83.70

Weld 84.30 77.80 68.90 76.20 73.80 75.70 84.80

84.10 81.90 73.40 77.00 74.70 69.50 84.30

Avg 84.07 80.27 71.90 75.67 73.67 74.00 84.27

Table 6.4(e): Hardness test data – across the weld.

1. HARDNESS TEST ( HRB )

86.00

84.00

82.00

80.00

B 78.00 HR

76.00

74.00

72.00

70.00 012345678

Figure 6.4(a): Hardness graph – across the weld.

• As seen in the Table 6.4(d), the weld has a better hardness value compared to

parent 1 and is softer than parent 2. The hardness joint efficiencies are 1.10 and

0.90 for parent 1 and parent 2 respectively.

• It can be seen from Figure 6.4(a) that a hardness degradation region (i.e. softened

region) has occurred in each joint [10].

46 • There are two low hardness zones on the two sides of the weld center, but the

minimum hardness value exists in the low hardness zone on the retreating side,

accordingly the joint is fractured on the retreating side [10]. This implies that the

tensile properties and fracture locations are related to the hardness profile of the

weld.

6.4.6. Microstructure

Figure 6.4(b): Microstructure of the weld.

6.5. LOW-SPEED FRICTION STIR WELD 2

Weld Specifications

Materials: Alclad 2024-T3 (0.080”) & Al 7075-T6 (0.040”)

Type of Joint: Lap

Welding Speed: 10”/min & 15”/min

Rotational Speed: 760 rpm

Tool Shoulder Diameter: 0.375 in

47 6.5.1. Tensile Test – Parent 1 (Alclad 2024-T3)

Peak Peak Break Break Yield Yield Tangent SI Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 1121.63 37387.70 35441.30 16.20 37387.70 15.2 735124

2 1121.63 56081.60 53648.60 16.00 56081.60 13.8 1084599

3 1121.63 56081.60 53648.60 15.00 56081.60 13.7 998141

Avg 1121.63 49850.30 47579.5 15.70 49850.30 14.2 939288

Table 6.5(a): Tensile test data of parent 1 – Alclad 2024-T3.

6.5.2. Tensile Test – Parent 2 (Al 7075-T6)

Peak Peak Break Break Yield Yield Tangent SI Load Stress Stress Elongation Stress Elongation Modulus

(lb) (psi) (psi) (%) (psi) (%) (psi)

1 722.61 72261.30 70314.90 11.10 72261.30 8.8 2324608

2 712.88 71288.10 68368.50 10.30 71288.10 8.8 2035341

3 693.42 69341.70 67395.30 10.20 69341.70 8.6 2086943

Avg 709.64 70963.70 68692.90 10.50 70963.70 8.6 2148964

Table 6.5(b): Tensile test data of parent 2 – Al 7075-T6.

48 6.5.3. Tensile Test – Weld (10”/min)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 1559.58 51986.00 51986.00 6.70 51986.00 6.70 969705

2 1452.53 48417.50 48093.10 6.50 48417.50 6.50 836114

3 1559.58 51986.00 51337.20 6.90 51986.00 6.80 895946

Avg 1523.90 50796.50 50472.10 6.70 50796.50 6.70 900588

Table 6.5(c): Tensile test data of weld @ 10”/min.

6.5.4. Tensile Test – Weld (15”/min)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 1374.67 45822.30 32521.70 5.60 45822.30 4.80 1013254

2 1384.40 46146.70 45822.30 5.90 46146.70 5.80 844730

3 1403.87 46795.50 46795.50 6.50 46795.50 6.50 773184

Avg 1387.65 46254.83 41713.17 6.00 46254.83 5.70 877056

Table 6.5(d): Tensile test data of the weld @ 15”/min.

49 • The joint efficiencies (weld / parent ratio) of the weld @ 10”/min with respect to

parent 1 (Alclad 2024-T3) are 1.06 and 1.02 for Break stress and Peak / Yield

stress respectively. This implies that the tensile strength of the weld is more than

parent 1.

• The joint efficiencies of the weld @ 10”/min with respect to parent 2 (Al 7075-

T6) are 0.73 and 0.72 for Break stress and Peak / Yield stress respectively. This

implies that the tensile strength of the weld is less than parent 2.

• The average break and yield elongation of the weld @ 10”/min is much lower

than the average break and yield elongation of its parents.

• The joint efficiencies (weld / parent ratio) of the weld @ 15”/min with respect to

parent 1 (Alclad 2024-T3) are 0.88 and 0.93 for Break stress and Peak / Yield

stress respectively. This implies that the tensile strength of the weld is less than

parent 1.

• The joint efficiencies of the weld @ 15”/min with respect to parent 2 (Al 7075-

T6) are 0.61 and 0.65 for Break stress and Peak / Yield stress respectively. This

implies that the tensile strength of the weld is less than parent 2.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• All the weld tensile test specimens fractured in the TMAZ on the retreating side.

• Parent 2, even though has a better tensile properties than parent 1, was the first to

fracture. This might be due to its constant contact with tool shoulder.

• The weld @ 10”/min has better tensile properties than the weld @ 15”/min.

50 6.5.5. Hardness Test – Along the Weld

Parent Weld SI No Al 7075-T6 Alclad 2024-T3 Weld -10”/min Weld – 15”/min

1 83.70 69.60 78.70 77.70 2 84.00 69.00 80.50 76.70 3 83.40 68.80 79.50 78.80 4 84.10 68.80 79.10 76.30 5 83.70 69.50 81.20 77.70 Avg 83.78 69.14 79.80 77.44

Table 6.5(e): Hardness test data – along the weld.

6.5.6. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

15”/min 83.70 77.70 77.40 78.40 76.80 77.20 83.20

Interface 83.60 74.90 74.60 77.70 71.20 74.20 83.80

10”/min 83.90 79.00 78.60 80.60 77.00 77.30 83.50

Avg 83.73 77.20 76.87 78.90 75.00 76.23 83.50

Table 6.5(f): Hardness test data – across the weld.

51 Weld2 Hardness Test (HRB) 10"/min

85.00

84.00

83.00

82.00

81.00 B HR 80.00

79.00

78.00

77.00

76.00 012345678

Figure 6.5(a): Hardness graph – across the weld @ 10”/min.

Weld2 Hardness Test (HRB) 15"/min

85.00

84.00

83.00

82.00

81.00 B HR 80.00

79.00

78.00

77.00

76.00 012345678

Figure 6.5(b): Hardness graph – cross the weld @ 15”/min.

• As seen in the Table 6.5(e), the weld @ 10”/min has a better hardness value

compared to parent 1 and is softer than parent 2. The hardness joint efficiencies

are 1.15 and 0.95 for parent 1 and parent 2 respectively.

52 • As seen in the Table 6.5(e), the weld @ 15”/min has a better hardness value

compared to parent 1 and is softer than parent 2. The hardness joint efficiencies

are 1.12 and 0.92 for parent 1 and parent 2 respectively.

• The hardness profiles of both the welds are almost the same, as seen in Figures

6.5(a) and 6.5(b), with the minimum hardness value existing in the TMAZ on the

retreating side. Accordingly all the tensile specimens fractured in the TMAZ on

the retreating side.

• The interface between weld @ 10”/min and weld @ 15”/min has hardness values

lower than the two welds.

6.6. LOW SPEED FRICTION STIR WELD 3

Weld Specifications

Materials: Alclad 2024-T3 (0.080”) & Al 7075-T6 (0.040”)

Type of Joint: Lap

Welding Speed: 10”/min & 15”/min

Rotational Speed: 600 rpm

Tool Shoulder Diameter: 0.375 in

53 6.6.1. Tensile Test – Parent 1 (Alclad 2024-T3)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 1121.63 37387.70 35441.30 16.20 37387.70 15.2 735124

2 1121.63 56081.60 53648.60 16.00 56081.60 13.8 1084599

3 1121.63 56081.60 53648.60 15.00 56081.60 13.7 998141

Avg 1121.63 49850.30 47579.5 15.70 49850.30 14.2 939288

Table 6.6(a): Tensile test data of parent1 – Alclad 2024-T3.

6.6.2. Tensile Test – Parent 2 (Al 7075-T6)

Peak Peak Break Break Yield Yield Tangent SI Load Stress Stress Elongation Stress Elongation Modulus

(lb) (psi) (psi) (%) (psi) (%) (psi)

1 722.61 72261.30 70314.90 11.10 72261.30 8.8 2324608

2 712.88 71288.10 68368.50 10.30 71288.10 8.8 2035341

3 693.42 69341.70 67395.30 10.20 69341.70 8.6 2086943

Avg 709.64 70963.70 68692.90 10.50 70963.70 8.6 2148964

Table 6.6(b): Tensile test data of parent 2 - Al 7075-T6.

54 6.6.3. Tensile Test - Weld (10"/min)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 1364.94 45497.90 39334.20 10.00 45497.90 5.30 889318

2 1413.60 47119.90 44952.70 5.70 47119.90 5.50 907242

3 1306.54 43551.40 39009.80 9.90 43551.40 5.00 891491

Avg 1369.80 45660.08 40657.73 8.90 45660.08 5.30 908639

Table 6.6(c): Tensile test data of the weld @10"/min.

6.6.4. Tensile Test - Weld (15"/min)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 1111.90 37063.30 30575.20 6.70 35116.90 3.60 994281

2 1296.81 43227.00 39658.60 9.50 43227.00 4.30 1042696

3 1209.22 40307.40 31548.40 7.60 40307.40 4.60 879070

Avg 1206.79 40226.28 35035.80 7.90 39739.68 4.40 937781

Table 6.6(d): Tensile test data of the weld @ 15"/min.

55 • The joint efficiencies (weld / parent ratio) of the weld @ 10”/min with respect to

parent 1 (Alclad 2024-T3) are 0.64 and 0.92 for Break stress and Peak / Yield

stress respectively. This implies that the tensile strength of the weld is less than

parent 1.

• The joint efficiencies of the weld @ 10”/min with respect to parent 2 (Al 7075-

T6) are 0.44 and 0.64 for Break stress and Peak / Yield stress respectively. This

implies that the tensile strength of the weld is less than parent 2.

• The average break and yield elongation of the weld @ 10”/min is much lower

than the average break and yield elongation of its parents.

• The joint efficiencies (weld / parent ratio) of the weld @ 15”/min with respect to

parent 1 (Alclad 2024-T3) are 0.74, 0.81 and 0.80 for Break stress, Peak stress

and Yield stress respectively. This implies that the tensile strength of the weld is

less than parent 1.

• The joint efficiencies of the weld @ 15”/min with respect to parent 2 (Al 7075-

T6) are 0.51, 0.57 and 0.56 for Break stress, Peak stress and Yield stress

respectively. This implies that the tensile strength of the weld is less than parent 2.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• All the weld tensile test specimens fractured in the TMAZ on the retreating side.

The parent 2 of two of the tensile specimen fractured in HAZ.

• Parent 2, even though has a better tensile properties than parent 1, was the first to

fracture. This might be due to its constant contact with tool shoulder.

• The weld @ 10”/min has better tensile properties than the weld @ 15”/min.

56 6.6.5. Hardness Test - Along the Weld

Parent Weld SI No Al 7075-T6 Alclad 2024-T3 Weld -10”/min Weld – 15”/min

1 82.80 69.30 77.00 75.10 2 83.50 68.30 77.80 74.20 3 82.40 68.80 76.70 74.80 4 82.90 69.80 77.70 75.00 5 82.90 69.60 Avg 82.78 69.16 77.30 74.78

Table 6.6(e): Hardness test data - along the weld.

6.6.6. Hardness Test - Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

15"/min 82.90 78.90 75.40 75.00 74.20 77.50 82.50

Interface 83.20 78.20 73.60 74.80 73.00 75.00 82.90

10"/min 83.30 79.80 76.80 77.70 76.40 78.80 82.90

Avg 83.13 78.97 75.27 75.83 74.53 77.10 82.77

Table 6.6(f): Hardness test data - across the weld.

57 Hardness - across the Weld 3 @ 10"/min

84.00

83.00

82.00

81.00

B 80.00 HR

79.00

78.00

77.00

76.00 012345678

Figure 6.6(a): Hardness graph - across the weld @ 10"/min.

Hardness - across the Weld 3 @ 15"/min

84.00

83.00

82.00

81.00

80.00

79.00 B HR 78.00

77.00

76.00

75.00

74.00

73.00 012345678

Figure 6.6(b): Hardness graph - across the weld @ 15"/min.

• As seen in the Table 6.6(e), the weld @ 10”/min has a better hardness value

compared to parent 1 and is softer than parent 2. The hardness joint efficiencies

are 1.12 and 0.93 for parent 1 and parent 2 respectively.

• As seen in the Table 6.6(e), the weld @ 15”/min has a better hardness value

compared to parent 1 and is softer than parent 2. The hardness joint efficiencies

are 1.08 and 0.90 for parent 1 and parent 2 respectively.

58 • The hardness profiles of both the welds are almost the same, as seen in Figures

6.6(a) and 6.6(b), with the minimum hardness value existing in the TMAZ on the

retreating side. Accordingly all the tensile specimens fractured in the TMAZ on

the retreating side.

• The interface between weld @ 10”/min and weld @ 15”/min has hardness values

lower than the two welds.

6.6.7. Comparison - Weld 1, Weld 2 and Weld 3

54000

52000

50000 Peak / Yield Stress 48000 (psi) 46000

44000 10"/min @ 10"/min @ 10"/min @ 600 rpm 750 rpm 760 rpm 42000

Figure 6.6(c): Peak/yield stress of weld - 10"/min @ 750,760 & 600rpm.

59

60000

50000

) si

p 40000 ( ss e r

t 30000

k S

ea 20000 r B 10000 10"/min @ 10"/min @ 10"/min @ 600 rpm 750 rpm 760 rpm 0

Figure 6.6(d): Break stress of weld - 10"/min @ 750, 760 & 600 rpm.

• It can be seen from Figures 6.6(c) and 6.6(d) that the tensile properties of each

joints change considerably with the change in the welding pitch (the ratio of the

rotational speed to the welding speed).

• When the welding pitch is smaller than 75 r/in, the tensile properties of the joints

increases with the increase in the welding pitch.

• When the welding pitch is greater than 75 r/in, all tensile properties tend to

decrease with the increase in the welding pitch.

• These results indicate that a softening effect has taken place in the joint. The

softened levels or the tensile properties of the joints are significantly affected by

the welding parameters. For example, the welding pitch of 75 r/in, corresponding

to the rotational speed of 750 rpm and the welding speed of 10"/min, is optimum

for the tensile properties of the joints in case of welds 1, 2 & 3.

60 • None of the tensile test specimens failed on the advancing side of the joint, which

implies that the tensile properties of the welds are not the same on either sides of

the weld center. This also implies that the retreating side of the joint is weaker

than the advancing side.

• There are two low hardness zones on the two sides of the weld center, but the

minimum hardness value exists in the low hardness zone on the retreating side,

accordingly the joint is fractured on the retreating side. This implies that the

tensile properties and fracture locations are related to the hardness profile of the

weld.

60000

50000 )

i 40000 s

(p Peak / Yield Stress (psi)

s 30000 s

e Break Stress (psi)

Str 20000

10000

0 10"/min 15"/min Welding Speed (in/min)

Figure 6.6(e): Weld 2 - change in stress due to change in welding pitch.

61 It can be seen from Figure 6.6(e) that the tensile properties of weld 2 change considerably with change in its welding pitch. Break, Peak and Yield stress of weld 2 decrease with the decrease in the welding pitch from 76 r/in to 50.67 r/in (i.e. increase in welding speed from 10"/min to 15"/min).

50000 45000 40000

) 35000

si Peak Stress (psi) p 30000 ( 25000 Break Stress (psi) ss e r

t 20000 Yield Stress (psi) S 15000 10000 5000 0 10"/min 15"/min Welding Speed (in/min)

Figure 6.6(f): Weld 3 - change in stress due to change in welding pitch.

It can be seen from Figure 6.6(f) that the tensile properties of weld 3 too changes considerably with change in its welding pitch. Peak and Yield stress of the weld decrease and its Break stress increases with the decrease in the welding pitch from 60 r/in to 40 r/in (i.e. increase in welding speed from 10"/min to 15"/min).

62

80 79.5

) 79 B R

H 78.5 ( s

s 78 Weld 2

dne 77.5 r

a

H 77 76.5 76 10"/min 15"/min Welding Speed (in/min)

78 77.5 77 )

B 76.5 R

H 76 ( s

s 75.5 Weld 3 75 dne r

a 74.5

H 74 73.5 73

10"/min 15"/min Welding Speed (in/min)

Figure 6.6(g): Weld 2 & weld 3 - change in hardness due to change in welding pitch

Figure 6.6(g) shows the change in the hardness of weld 2 and weld 3, along the weld, with change in the welding pitch. In weld 2, as the welding pitch decreases from 76 r/in to 50.67 r/in, there is a decrease in the hardness of the weld. In weld 3, the hardness along the weld reduces with the decrease in the welding pitch from 60 r/in to 40 r/in. These

63 results indicate that softening effect takes place in the weld with an increase in its welding speed.

6.7. LOW-SPEED FRICTION STIR WELD 4

Weld Specifications

Materials: Alclad 2024-T3 (0.080”) & Al 7075-T6 (0.063”)

Type of Joint: Lap - Double pass

Welding Speed: 10”/min

Rotational Speed: 760 rpm

Tool Shoulder Diameter: 0.375 in

6.7.1. Tensile Test – Parent 1 (Alclad 2024-T3)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 2217.39 55434.80 53260.9 29.30 55434.80 27.2 1880680

Table 6.7(a): Tensile test data of parent1 - Alclad 2024-T3.

64 6.7.2. Tensile Test – Parent 2 (Al 7075-T6)

Peak Peak Break Break Yield Yield Tangent SI Load Stress Stress Elongation Stress Elongation Modulus

(lb) (psi) (psi) (%) (psi) (%) (psi)

1 2156.52 68461.00 65976.50 20.10 68461.00 18.6 1088848.00

Table 6.7(b): Tensile test data of parent 2 - Al 7075-T6.

6.7.3. Tensile Test - Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 973.91 13621.20 13621.20 3.90 13621.20 3.90 381015

2 947.83 13256.30 13256.30 5.80 13256.30 5.80 396472

3 965.22 13499.50 13377.90 4.10 13499.50 4.10 363561

4 947.83 13256.30 13256.30 4.00 13256.30 4.00 358545

5 973.91 13621.20 13499.50 4.10 13621.20 4.00 364711

Avg 961.72 13450.90 13402.24 4.38 13450.90 4.36 372861

Table 6.7(c): Tensile test data of the weld.

65 • The joint efficiencies (weld / parent ratio) of the weld with respect to parent 1

(Alclad 2024-T3) are 0.25 and 0.24 for Break stress and Peak / Yield stress

respectively. This implies that the tensile strength of the weld is less than parent1.

• The joint efficiencies of the weld with respect to parent 2 (Al 7075-T6) are 0.20

and 0.19 for Break stress and Peak / Yield stress respectively. This implies that

the tensile strength of the weld is less than parent 2.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• All the weld tensile test specimens fractured in the TMAZ.

• Parent 2, even though has a better tensile properties than parent 1, was the first to

fracture.

6.7.4. Hardness Test – Along the weld

Parent SI No Al 7075-T6 Alclad 2024-T3 Weld

1 88.50 70.20 77.60 2 88.60 69.30 77.80 3 88.60 70.00 78.30 4 89.10 70.00 78.30 5 89.10 70.40 78.60 Avg 88.78 69.98 78.12

Table 6.7(d): Hardness test data- along the weld.

66 6.7.5. Hardness Test - Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

86.30 83.50 76.10 79.20 77.00 84.50 88.50

Weld 85.20 80.50 75.80 78.70 78.00 79.40 89.00

87.20 83.30 76.30 78.20 77.60 82.00 86.00

Avg 86.23 82.43 76.07 78.70 77.53 81.97 87.83

Table 6.7(e): Hardness test data - across the weld.

HARDNESS TEST ( HRB )

90.00

88.00

86.00

84.00

B 82.00 HR

80.00

78.00

76.00

74.00 012345678

Figure 6.7(a): Hardness graph - across the weld.

67 • As seen in the Table 6.7(d), the weld has a better hardness value compared to

parent 1 and is softer than parent 2. The hardness joint efficiencies are 1.12 and

0.88 for parent 1 and parent 2 respectively.

• The hardness of the weld does not vary much on both sides of the weld center,

with the minimum hardness value existing in the TMAZ. Accordingly all the

tensile specimens fractured in the TMAZ.

• Though the weld has good hardness values, it displays very poor tensile

properties.

6.7.6. Metallography

Fig 6.7(b): Microstructure of the weld nugget.

68 6.8. LOW-SPEED FRICTION STIR WELD 5

Weld Specifications

Materials: Alclad 2024-T3 (0.080”) & Al 7075-T6 (0.063”)

Type of Joint: Lap – Double pass

Welding Speed: 15”/min

Rotational Speed: 760 rpm

Tool Shoulder Diameter: 0.375 in

6.8.1. Tensile Test – Parent 1 (Alclad 2024-T3)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 2191.30 54782.60 52391.30 31.10 54782.60 28.30 780511

Table 6.8(a): Tensile test data of parent1 – Alclad 2024-T3.

6.8.2. Tensile Test – Parent 2 (Al 7075-T6)

Peak Peak Break Break Yield Yield Tangent SI Load Stress Stress Elongation Stress Elongation Modulus

(lb) (psi) (psi) (%) (psi) (%) (psi)

1 2173.91 69013.10 67080.70 19.70 69013.10 17.70 1277115

Table 6.8(b): Tensile test data of parent2 - Al 7075-T6.

69 6.8.3. Tensile Test - Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 730.43 10215.90 10215.90 3.60 10215.90 3.60 306131

2 756.52 10580.70 10459.10 3.80 10580.70 3.70 319643

3 713.04 9972.60 9729.40 3.50 9972.60 3.40 345836

Avg 733.33 10256.40 10134.80 3.63 10256.40 3.57 323870

Table 6.8(c): Tensile test data of the weld.

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent 1

(Alclad 2024-T3) are 0.19 and 0.18 for Break stress and Peak / Yield stress

respectively. This implies that the tensile strength of the weld is less than parent1.

• The joint efficiencies of the weld with respect to parent 2 (Al 7075-T6) are 0.15

and 0.15 for Break stress and Peak / Yield stress respectively. This implies that

the tensile strength of the weld is less than parent 2.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• All the weld tensile test specimens fractured in the TMAZ.

70 6.8.4. Hardness Test – Along the weld

Parent SI No Al 7075-T6 Alclad 2024-T3 Weld

1 88.70 68.60 79.60 2 89.30 69.00 80.20 3 87.70 68.10 83.90 4 87.90 70.40 83.40 Avg 88.40 69.03 81.78

Table 6.8(d): Hardness test data – along the weld.

6.8.5. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

86.70 83.80 75.10 77.00 75.90 78.20 87.40

Weld 87.90 81.50 76.40 78.50 77.10 82.20 87.70

87.00 83.60 72.00 77.00 73.60 80.40 88.50

Avg 87.20 82.97 74.50 77.50 75.53 80.27 87.87

Table 6.8(e): Hardness test data – across the weld.

71 HARDNESS TEST ( HRB )

90.00

88.00

86.00

84.00

82.00 B HR 80.00

78.00

76.00

74.00

72.00 012345678

Figure 6.8(a): Hardness graph - across the Weld.

• As seen in the Table 6.8(d), the weld has a better hardness value compared to

parent 1 and is softer than parent 2. The hardness joint efficiencies are 1.18 and

0.93 for parent 1 and parent 2 respectively.

• The hardness of the weld does not vary much on both sides of the weld center,

with the minimum hardness value existing in the TMAZ. Accordingly all the

tensile specimens fractured in the TMAZ.

• Though the weld has good hardness values, it displays very poor tensile

properties.

72 6.8.6. Metallography

Fig 6.8(b): Microstructure of the weld.

6.9. HIGH-SPEED FRICTION STIR WELD 6

Weld Specifications

Materials: Al 6061-T6 (0.125”)

Type of Joint: Butt

Welding Speed: 15”/min

Rotational Speed: 1500 rpm

Tool Shoulder Diameter: 0.375 in

73 6.9.1. Tensile Test – Parent (Al 6061-T6)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 4037.50 64600.00 59502.80 20.80 64600.00 17.70 1367795

2 4019.80 64316.90 59361.20 20.80 64316.90 18.00 1320557

Avg 4028.65 64458.45 59432.00 20.80 64458.45 17.85 1344176

Table 6.9(b): Tensile test data of the parent – Al 6061-T6.

6.9.2. Tensile Test - Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3232.21 51715.40 49520.80 8.20 51715.40 7.30 1283741

2 3218.94 51503.00 49308.40 8.80 51503.00 7.80 1324307

3 3223.36 51573.80 49166.80 8.20 51573.80 7.10 1294124

4 3218.94 51503.00 49096.00 8.40 51503.00 7.40 1295279

Avg 3226.52 51624.37 49450.00 8.50 51624.37 7.59 1283318

Table 6.9(b): Tensile test data of the weld.

74 • The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

6061-T6) are 0.83 and 0.80 for Break stress and Peak / Yield stress respectively.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• All the weld tensile test specimens fractured in the HAZ.

6.9.3. Hardness test – along the Weld

SI NO PARENT WELD

1 51.50 21.80

2 49.90 21.00

3 46.90 20.00

Avg 49.43 20.93

Table 6.9(c): Hardness test data – along the weld.

6.9.4. Hardness Test – across the weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

49.80 16.40 27.70 21.80 29.80 20.20 51.50

Weld 48.40 14.80 27.70 21.00 27.70 18.20 49.90

50.50 13.80 26.80 20.00 26.70 18.80 49.00

Avg 49.60 15.00 27.40 20.93 28.10 19.10 50.13

Table 6.9(d): Hardness test data – across the weld.

75

Hardness (HRB) across the Weld, Al6061-T6 @ 15"/min

60.00

50.00

40.00

B 30.00 HR

20.00

10.00

0.00 012345678

Figure: 6.9(a): Hardness graph - across the weld.

• As seen in the Table 6.9(c), the weld is softer than the parent. The hardness joint

efficiency is 0.42.

• It can be seen from Figure 6.9(a) that a hardness degradation region (i.e. softened

region) has occurred in each joint, with the weld nugget having a hardness value

less than the TMAZ hardness values.

• There are two low hardness zones on the two sides of the weld center, but the

minimum hardness value exists in the low hardness zone on the retreating side,

accordingly the joint is fractured on the retreating side. From Figure6.6(c) it can

be found that the minimum hardness occurs in the HAZ adjacent to the TMAZ on

the retreating side. Therefore, the joint is fractured in the HAZ on the retreating

side and the fracture surface is parallel to the TMAZ / HAZ interface on the

retreating side [10].

76 6.10. LOW-SPEED FRICTION STIR WELD 7

Weld Specifications

Materials: Al 6061-T6 (0.125”)

Type of Joint: Butt

Welding Speed: 20”/min

Rotational Speed: 1500 rpm

Tool Shoulder Diameter: 0.375 in

6.10.1. Tensile Test – Parent (Al6061-T6)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3921.30 67242.20 60970.00 23.10 67242.20 19.60 1563554

2 3830.93 65692.60 59346.60 21.50 65692.60 18.30 1566628

Avg 3876.12 66467.40 60158.30 22.30 66467.4 18.95 1565091

Table 6.10(a): Tensile test data of the parent – Al 6061-T6.

77 6.10.2. Tensile Test - Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3262.91 55952.20 53369.50 9.00 55952.20 8.10 1366549

2 3262.91 55952.20 54402.50 8.40 55952.20 7.60 1425574

Avg 3262.91 55952.20 53886.00 8.70 55952.20 7.85 1396062

Table 6.10(b): Tensile test data of the weld.

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

6061-T6) are 0.90 and 0.84 for Break stress and Peak / Yield stress respectively.

This implies that the tensile strength of the weld is less than parent.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• All the weld tensile test specimens fractured in the HAZ.

78 6.10.3. Hardness Test – Along the weld

SI NO PARENT WELD

1 50.90 28.50

2 49.80 28.50

3 48.90 27.00

Avg 49.87 28.00

Table 6.10(c): Hardness test data – along the weld.

6.10.4. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

49.80 26.70 29.78 28.50 34.30 29.80 49.60

Weld 51.70 25.80 30.40 28.50 32.40 31.40 50.40

50.00 27.00 29.60 27.00 34.40 30.60 48.70

Avg 50.50 26.50 29.93 28.00 33.70 30.60 49.60

Table 6.10(d): Hardness test data – across the weld.

79 Hardness (HRB) across the Weld Al6061-T6, 20'/min

60

50

40

B 30 HR

20

10

0 012345678

Figure 6.10(a): Hardness graph - across the weld.

• As seen in the Table 6.10(c), the weld is softer than the parent. The hardness joint

efficiency is 0.56.

• It can be seen from Figure 6.10(a) that a hardness degradation region (i.e.

softened region) has occurred in each joint, with the weld nugget having a

hardness value less than the TMAZ hardness values.

• There are two low hardness zones on the two sides of the weld center, but the

minimum hardness value exists in the low hardness zone on the retreating side,

accordingly the joint is fractured on the retreating side. From Figure 6.7(c) it can

be found that the minimum hardness occurs in the HAZ adjacent to the TMAZ on

the retreating side. Therefore, the joint is fractured in the HAZ on the retreating

side and the fracture surface is parallel to the TMAZ / HAZ interface on the

retreating side.

80 6.11. LOW-SPEED FRICTION STIR WELD 8

Weld Specifications

Materials: Al 6061-T6 (0.125”)

Type of Joint: Butt

Welding Speed: 25”/min

Rotational Speed: 1500 rpm

Tool Shoulder Diameter: 0.375 in

6.11.1. Tensile Test – Parent (Al6061-T6)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 4042.37 64677.90 58303.90 23.00 64677.90 19.60 1494830

2 4051.22 64819.50 58445.60 23.40 64819.50 20.10 1373849

3 4006.96 64111.30 57737.30 23.30 64111.30 19.90 1292505

4 4042.37 64677.90 57879.00 23.20 64677.90 20.00 1395983

Avg 4035.73 64571.65 58091.45 23.23 64571.65 19.90 1389292

Table 6.11(a): Tensile test data of the parent – Al 6061-T6.

81 6.11.2. Tensile Test - Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3378.41 54054.60 52921.50 9.30 54054.60 8.40 1295614

2 3382.84 54125.40 52496.50 9.90 54125.40 9.00 1317391

3 3378.41 54054.60 52638.20 9.20 54054.60 8.40 1313819

4 3391.96 54267.10 53133.90 9.40 54267.10 8.60 1293661

Avg 3382.84 54125.43 52797.53 9.45 54125.43 8.60 1305121

Table 6.11(b): Tensile test data of the weld.

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

6061-T6) are 0.91and 0.84 for Break stress and Peak / Yield stress respectively.

This implies that the tensile strength of the weld is less than parent.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• The weld tensile test specimens fractured in the HAZ, with one of the specimen

fracturing in the weld nugget due to crack like defect in the joint.

82 6.11.3. Hardness Test – Along the Weld

SI NO PARENT WELD

1 50.00 27.60

2 50.40 28.80

3 52.40 23.20

Avg 50.93 26.53

Table 6.11(c): Hardness test data - along the weld.

6.11.4. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

50.40 24.80 28.60 26.60 28.80 27.80 50.00

Weld 51.50 24.80 29.00 27.60 29.70 28.20 52.40

51.20 25.20 28.30 27.00 28.60 28.60 50.80

Avg 51.03 24.93 28.63 27.10 29.03 28.20 51.10

Table 6.11(d): Hardness test data – across the weld.

83 Hardness (HRB) across the Weld, Al 6061-T6 @ 25"/min

60

50

40

B 30 HR

20

10

0 012345678

Figure 6.11(a): Hardness graph - across the weld.

• As seen in the Table 6.11(c), the weld is softer than the parent. The hardness joint

efficiency is 0.52.

• It can be seen from Figure 6.11(a) that a hardness degradation region (i.e.

softened region) has occurred in each joint, with the weld nugget having a

hardness value less than the TMAZ hardness values.

• There are two low hardness zones on the two sides of the weld center, but the

minimum hardness value exists in the low hardness zone on the retreating side,

accordingly the joint is fractured on the retreating side. From Figure 6.11(c) it can

be found that the minimum hardness occurs in the HAZ adjacent to the TMAZ on

the retreating side. Therefore, the joint is fractured in the HAZ on the retreating

side and the fracture surface is parallel to the TMAZ / HAZ interface on the

retreating side.

84 6.11.5. Comparison - Weld 6, Weld 7 & Weld 8

57000 56000 ) i s

p 55000 ( s

s 54000 e r t

S 53000 ld

ie 52000

/Y k

a 51000 e

P 20"/min 25"/min 50000 15"/min 49000 Welding Speed (in/min)

Figure 6.11(b): Peak/yield stress variation.

55000

54000

) 53000 si p ( 52000 ss e r

t 51000

k S 50000 ea r

B 49000 48000 15"/min 20"/min 25"/min

47000 Weldi ng Speed (in/min)

Figure 6.11(c): Break stress variation.

85 • It can be seen from Figures 6.11(b) and 6.11(c) that the tensile properties of each

joints change considerably with the change in the welding pitch.

30

25

) B 20 R H

( s

s 15

dne r

a 10 H

5 15"/min 20"/min 25"/min

0 Welding Speed (in/min)

Figure 6.11(d): Variation in hardness.

• It can be seen from Figures 6.11(d) that the hardness values of each joints change

considerably with the change in the welding pitch.

• When the welding pitch is smaller than 75 r/in, the tensile properties and the

hardness of the joints decreases with the decrease in the welding pitch.

• When the welding pitch is greater than 75 r/in, all tensile properties and the

hardness of the joints tend to increase with the decrease in the welding pitch.

• These results indicate that a softening effect has taken place in the joint. The

softened levels or the tensile properties of the joints are significantly affected by

the welding parameters. For example, the welding pitch of 75 r/in, corresponding

to the rotational speed of 1500 rpm and the welding speed of 20"/min, is optimum

for the tensile properties of the joints in case of welds 6, 7 & 8.

86 • None of the tensile test specimens failed on the advancing side of the joint, which

implies that the tensile properties of the welds are not the same on either sides of

the weld center. This also implies that the retreating side of the joint is weaker

than the advancing side.

• The hardness of the weld center is lower than TMAZ, but the minimum hardness

value exists in the HAZ on the retreating side, accordingly the joint is fractured in

HAZ on the retreating side. This implies that the tensile properties and fracture

locations are related to the hardness profile of the weld.

87 6.12. LOW-SPEED FRICTION STIR WELD 9

Weld Specification

Materials: Al 2024-T3 (0.090”)

Type of Joint: Butt

Welding Speed: 20”/min

Rotational Speed: 955 rpm

Tool Shoulder Diameter: 0.375 in

6.12.1. Tensile Test – Parent (Al 2024-T3)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3917.32 87051.60 84100.70 28.40 86658.10 22.90 1826437

2 3873.06 86068.00 83707.20 27.60 85674.50 22.30 1838938

3 3917.32 87051.60 84297.40 27.20 87051.60 22.30 1805899

Avg 3904.04 86756.53 83658.05 28.05 86559.78 23.55 1830592

Table 6.12(a): Tensile test data of the parent – Al 2024-T3.

88 6.12.2. Tensile Test - Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3452.55 76723.40 76625.10 13.30 76723.40 13.30 1661615

2 3518.95 78198.90 78002.20 14.80 78198.90 14.70 1661268

3 3496.82 77707.10 77707.10 14.70 77707.10 14.70 1656029

Avg 3494.61 77657.90 77559.55 14.45 77657.90 14.40 1642937

Table 6.12(b): Tensile test data of the weld.

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

2024-T3) are 0.93 and 0.90 for Break stress and Peak / Yield stress respectively.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• The weld tensile test specimens fractured in the TMAZ.

89 6.12.3. Hardness Test – Along the Weld

SI NO PARENT WELD

1 73.80 72.80

2 72.00 71.60

3 74.10 65.50

4 74.40 67.50

Avg 73.70 68.70

Table 6.12(c): Hardness test data – along the weld.

6.12.4. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

73.80 70.80 66.60 68.70 65.90 71.90 74.10

Weld 73.70 68.00 64.30 69.60 64.40 68.30 73.80

72.90 73.50 64.00 71.00 68.30 70.00 73.70

Avg 73.46 70.76 64.96 69.76 66.20 70.06 73.86

Table 6.12(d): Hardness data – across the weld.

90 Hardness (HRB) - Across the Weld.

75.00

74.00

73.00

72.00

71.00

70.00 B HR 69.00

68.00

67.00

66.00

65.00

64.00 012345678

Figure 6.12(a): Hardness graph - across the weld.

• As seen in the Table 6.12(c), the weld is softer than the parent. The hardness joint

efficiency is 0.93.

• It can be seen from Figure 6.12(a) that a hardness degradation region (i.e.

softened region) has occurred in each joint.

• There are two low hardness zones on the two sides of the weld center, but the

minimum hardness value exists in the low hardness zone on the retreating side,

accordingly the joint is fractured on the retreating side. From Figure 6.12(c) it can

be found that the minimum hardness occurs in the TMAZ on the retreating side.

Therefore, the joints fractured in the TMAZ on the retreating side.

91 6.12.5. Metallography

Fig 6.12(b): Microstructure of the weld nugget.

6.13. LOW-SPEED FRICTION STIR WELD 10

Weld Specifications

Materials: Alclad 2024-T3 (0.080”)

Type of Joint: Butt

Welding Speed: 10”/min

Rotational Speed: 500 rpm

Tool Shoulder Diameter: 0.375 in

92 6.13.1. Tensile Test – Parent (Alclad 2024-T3)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3788.96 94723.90 91846.80 28.80 94723.90 26.90 1549111

2 3749.12 93728.00 91182.90 27.30 93728.00 25.00 1624823

3 3762.40 94060.00 91293.50 29.10 94060.00 26.90 1658996

4 3802.24 95055.90 92178.80 28.80 95055.90 27.30 1547559

Avg 3775.68 94391.95 91625.50 28.50 94391.95 26.53 1595122

Table 6.13(a): Tensile test data of the parent – Alclad 2024-T3.

6.13.2. Tensile Test - Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 2642.53 66063.30 3.50 66063.30 66063.30 3.50 1988631

2 2629.25 65731.30 3.50 65731.30 65731.30 3.50 1977220

3 2646.96 66174.00 3.60 66174.00 66174.00 3.60 1937763

Avg 2635.89 65897.33 3.55 65897.33 65897.33 3.55 1952399

Table 6.13(b): Tensile test data of the weld.

93 • The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

clad 2024-T3) are 0.72 and 0.70 for Break stress and Peak / Yield stress

respectively. This implies that the tensile strength of the weld is less than parent.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• All the weld tensile specimens failed in the weld nugget due to crack like defects

in the joint.

6.13.3. Hardness Test – Along the Weld

SI NO Parent Weld

1 70.20 57.00

2 69.94 58.80

3 70.00 57.40

Avg 70.09 57.85

Table 6.13(c): Hardness test data – along the weld.

94 6.13.4. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

70.40 66.90 62.70 57.40 62.40 69.20 70.00

Weld 70.00 68.80 61.80 58.70 65.70 70.90 70.20

70.40 68.20 62.30 57.80 64.40 68.30 69.98

Avg 70.26 67.96 62.26 58.00 64.16 69.46 70.06

Table 6.13(d): Hardness test data – across the weld.

Hardness (HRB) - across the Weld

80.00

70.00

60.00

50.00

B 40.00 HR

30.00

20.00

10.00

0.00 012345678

Figure 6.13(a): Hardness graph - across the weld.

• As seen in the Table 6.13(c), the weld is softer than the parent. The hardness joint

efficiency is 0.83.

• It can be seen from Figure 6.13(a) that a hardness degradation region (i.e.

softened region) has occurred in each joint.

95 • The hardness values decrease gradually across the weld, with the minimum

hardness value in the weld center or weld nugget. Hence all the tensile specimens

failed at the weld nugget.

6.13.5. Metallography

Fig 6.13(b): Microstructures of the weld.

96 6.14. Tool Geometry Effects [21]

For a given alloy and plate thickness, the required z-axis load for production of a sound weld is primarily a function of shoulder diameter.

Tool Number Pin Dia (mm) Shoulder Dia (mm)

1 10 25

2 8 25

3 12 25

4 10 20

5 10 30

6 10 28

7 7.2 20

Table 6.14: Tool geometry.

In Table 6.14, tools 1, 2 and 3 all required approximately the same loads. Tool number 5, with the largest shoulder, required z-axis loads from 5-10% greater while tool number 4, with the smallest shoulder, needs loads as much as 40% lower than the other tools.

2500

m m 2000 J/

, 3.3 mm/s welding y

g speed

er 1500 2.4 mm/s welding en

d speed l

e 1000

w 1.3 mm/s welding

c

i speed f 500 eci p S 0 0246 Tool number

Fig 6.14(a): Specific weld energy as a function of welding speed and tool geometry.

97 In Fig 6.14(a), the specific weld energy as a function of welding speed and tool geometry

is shown. For each tool, increased welding speed (for the rpm’s chosen in this study)

results in reduced weld energy. In addition, for each welding speed, tool number 4

(smallest shoulder) results in the lowest weld energy and tool number 5 (largest shoulder)

results in the highest weld energy. The use of a large diameter pin (tool 3) also increases

the weld energy and the required power, but this effect is less than that associated with

the shoulder diameter changes.

3500

s 3000 t t

a 1.3 mm/s welding

w 2500

, speed r e 2000 w 2.4 mm/s welding speed po 1500 d

e

r 3.3 mm/s welding 1000 speed qui e R 500 0 0246 Tool number

Fig 6.14(b): Required weld power as a function of tool geometry and welding speed.

In Fig 6.14(b), the required power for the three welding speeds is plotted against the tool number. In this case, it is shown that the highest welding speed requires the greatest power delivery from the machine and again, the shoulder size appears to be the primary determinant of the power requirement for a given set of welding parameters (rpm and welding speed).

98

a 430 P M

425 ,

h t 420 g 1.3 mm/s welding n 415 e

r speed t 410

e s 405 2.4 mm/s welding l i

s 400 speed n e 395 3.3 mm/s welding 390 se t speed r 385

sve 380 an

r 375

T 0246 Tool number

Fig 6.14(c): Transverse tensile strength of the welds as a function of tool geometry and

welding speed.

Fig 6.14(c) shows the transverse tensile strength of the welds as a function of tool geometry and welding speed. For each tool, it is shown that increasing the weld speed results in a small but consistent increase in the tensile strength of the weld.

12

10

N 1.3 mm/s welding

k 8 speed e,

c r 2.4 mm/s welding

o 6 speed s f 3.3 mm/s welding

axi 4 -

X speed 2

0 0246 Tool number

Fig 6.14(d): X axis force as a function of tool geometry and welding speed.

Fig 6.14(d) shows X axis force as a function of tool geometry and welding speed. The force on the welding tool in the X direction is a critical variable in that, if it becomes too large the tool will break due to bending stresses. For each tool, the X axis force increases with increasing welding speed even though the intermediate welding speed weld has the highest advance per revolution.

99 6.15. HIGH-SPEED FRICTION STIR WELD 11

Weld specification

Materials: Al 7075-T6 (0.062”)

Type of Joint: Butt

Welding Speed: 1”/min

Rotational Speed: 12000 rpm

Tool Shoulder Diameter: 0.375 in

Pin length: 0.053 in

Shoulder angle: 3.7730

6.15.1. Tensile Test – Parent Al 7075-T6

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3279.93 104957.70 99008.70 10.40 104957.70 8.70 2425350

2 3293.21 105382.60 100141.80 10.30 105382.60 8.80 2340873

3 3293.21 105382.60 99433.60 10.50 105382.60 9.20 2331391

Avg 3288.78 105240.97 99528.03 10.40 105240.97 8.90 2365871

Table 6.15(a): Tensile test data of the parent - Al 7075-T6.

100 6.15.2. Tensile Test of the Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 426.19 27496.20 27496.20 4.80 27496.20 4.80 1207796

2 416.67 26881.70 26881.70 4.00 26881.70 4.00 1305856

3 311.90 20122.90 20122.90 1.90 20122.90 1.90 2130791

Avg 384.92 24833.60 24833.60 3.60 24833.60 3.60 1548148

Table 6.15(b): Tensile test data of the weld.

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

7075-T6) are 0.25 and 0.24 for Break stress and Peak / Yield stress respectively.

This implies that the tensile strength of the weld is less than parent.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• The weld tensile test specimens fractured in the weld nugget.

101 6.15.3. Hardness Test – Along the Weld

SI NO Parent Weld

1 88.80 55.20

2 88.90 51.50

3 88.80 51.90

4 88.80

Avg 88.83 52.90

Table 6.15(c): Hardness test data – along the weld.

6.15.4. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

89.90 60.80 73.50 55.40 72.30 58.50 90.00

Weld 90.00 62.90 70.80 50.90 77.80 61.60 90.00

90.00 66.70 72.80 51.50 74.10 63.80 90.00

Avg 90.00 63.50 72.40 52.60 74.73 61.30 90.00

Table 6.15(d): Hardness test data – across the weld.

102 Hardness across the weld

100

90

80

70

) 60 RB H ( s

s 50 e n d r

Ha 40

30

20

10

0 012345678

Figure 6.15(a): Hardness graph – across the weld.

• As seen in the Table 6.15(c), the weld is softer than the parent. The hardness joint

efficiency is 0.60. It can be seen from Figure 6.15(a) that a hardness degradation

region (i.e. softened region) has occurred in each joint.

• The hardness values decreases across the weld, with the minimum hardness value

in the weld center or weld nugget. Hence all the tensile specimens failed at the

weld nugget.

6.15.5. Microstructure

Figure 6.15(b): Microstructure of the Weld nugget.

103 6.16. HIGH-SPEED FRICTION STIR WELD 12

Weld specification

Materials: Al 7075-T6 (0.062”)

Type of Joint: Butt

Welding Speed: 1”/min

Rotational Speed: 12000 rpm

Tool Shoulder Diameter: 0.375 in

Pin length: 0.053 in

Shoulder angle: 9.8860

6.16.1. Tensile Test – Parent Al 7075-T6

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3279.93 104957.70 99008.70 10.40 104957.70 8.70 2425350

2 3293.21 105382.60 100141.80 10.30 105382.60 8.80 2340873

3 3293.21 105382.60 99433.60 10.50 105382.60 9.20 2331391

Avg 3288.78 105240.97 99528.03 10.40 105240.97 8.90 2365871

Table 6.16(a): Tensile test data of the parent Al 7075-T6.

104 6.16.2. Tensile Test of the Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 550.00 35483.90 35483.90 4.00 35483.90 4.00 1648618

2 207.14 13364.10 12749.60 1.90 13364.10 1.80 3225932

3 292.86 18894.00 18279.60 2.50 18894.00 2.50 1366332

4 473.81 30568.40 30568.40 3.80 30568.40 3.80 1345966

Avg 381.00 24577.60 24270.38 3.05 24577.60 3.03 1896712

Table 6.16(b): Tensile test data of the weld.

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

7075-T6) are 0.24 and 0.23 for Break stress and Peak / Yield stress respectively.

This implies that the tensile strength of the weld is less than parent.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parent.

• The weld tensile test specimens fractured in the weld nugget.

105 6.16.3. Hardness Test – Along the Weld.

SI NO Parent Weld

1 88.80 56.8

2 88.90 62.7

3 88.80 62.6

4 88.80

Avg 88.83 60.70

Table 6.16(c): Hardness test data – along the weld.

• As seen in the Table 6.16(c), the weld is softer than the parent. The hardness joint

efficiency is 0.68.

6.16.4. Microstructure

Fig 6.16(a): Microstructure of the weld nugget.

106 6.17. HIGH-SPEED FRICTION STIR WELD 13

Weld specification

Materials: Al 7075-T6 (0.062”)

Type of Joint: Butt

Welding Speed: 1”/min

Rotational Speed: 12000 rpm

Tool Shoulder Diameter: 0.375 in

Pin length: 0.053 in

Shoulder angle: 15.7860

6.17.1. Tensile Test – Parent Al 7075-T6

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3279.93 104957.70 99008.70 10.40 104957.70 8.70 2425350

2 3293.21 105382.60 100141.80 10.30 105382.60 8.80 2340873

3 3293.21 105382.60 99433.60 10.50 105382.60 9.20 2331391

Avg 3288.78 105240.97 99528.03 10.40 105240.97 8.90 2365871

Table 6.17(a): Tensile test data of the parent Al 7075-T6.

107 6.17.2. Tensile Test of the Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 445.24 28725.00 28725.00 3.40 28725.00 3.40 1949039

2 350.00 22580.60 22580.60 2.90 22580.60 2.90 1439180

3 216.67 13978.50 13978.50 1.50 13978.50 1.50 1526225

4 435.71 28110.60 28110.60 3.40 28110.60 3.40 1418963

5 369.05 23809.50 23809.50 3.30 23809.50 3.30 1268191

Avg 363.34 23440.84 23440.84 2.90 23440.84 2.90 1520320

Table 6.17(b): Tensile test data of the weld.

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

7075-T6) are 0.24 and 0.22 for Break stress and Peak / Yield stress respectively.

This implies that the tensile strength of the weld is less than parent.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• The weld tensile test specimens fractured in the weld nugget.

108 6.17.3. Hardness Test – Along the Weld

SI NO Parent Weld

1 88.80 70.10

2 88.90 66.70

3 88.80 66.50

4 88.80 72.50

Avg 88.83 68.95

Table 6.17(c): Hardness test data – along the weld.

• As seen in the Table 6.17(c), the weld is softer than the parent. The hardness joint

efficiency is 0.78.

6.17.4. Microstructure

Fig 6.17(a): Microstructure of the weld nugget.

109 6.18. HIGH-SPEED FRICTION STIR WELD 14

Weld specification

Materials: Al 7075-T6 (0.062”)

Type of Joint: Butt

Welding Speed: 1”/min

Rotational Speed: 12000 rpm

Tool Shoulder Diameter: 0.375 in

Pin length: 0.053 in

Shoulder angle: 21.3540

6.18.1. Tensile Test – Parent Al 7075-T6

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3279.93 104957.70 99008.70 10.40 104957.70 8.70 2425350

2 3293.21 105382.60 100141.80 10.30 105382.60 8.80 2340873

3 3293.21 105382.60 99433.60 10.50 105382.60 9.20 2331391

Avg 3288.78 105240.97 99528.03 10.40 105240.97 8.90 2365871

Table 6.18(a): Tensile test data of the parent Al 7075-T6.

110 6.18.2. Tensile Test of the Weld

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 521.43 33640.60 33640.60 3.80 33640.60 3.80 1471862

2 671.43 43318.00 43318.00 6.00 43318.00 6.00 1134024

3 376.19 24270.40 24270.40 3.00 24270.40 3.00 1449471

4 652.38 42089.10 42089.10 3.40 42089.10 3.40 1302887

5 595.24 38402.50 38402.50 3.40 38402.50 3.40 1125304

6 471.43 30414.70 30414.70 3.30 30414.70 3.30 1418458

Avg 548.02 35355.88 35355.88 3.82 35355.88 3.82 1317001

Table 6.18(b): Tensile test data of the weld.

• The joint efficiencies (weld / parent ratio) of the weld with respect to parent (Al

7075-T6) are 0.36 and 0.34 for Break stress and Peak / Yield stress respectively.

This implies that the tensile strength of the weld is less than parent.

• The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

• The weld tensile test specimens fractured in the weld nugget.

111 6.18.3. Hardness Test – Along the Weld

SI NO Parent Weld

1 88.80 64.70

2 88.90 39.10

3 88.80 72.5

4 88.80 26.2

Avg 88.83 50.62

Table 6.18(c): Hardness test data – across the weld.

6.18.4. Hardness Test – Across the Weld

SI No Parent HAZ TMAZ Nugget TMAZ HAZ Parent

89.90 61.30 71.30 55.40 71.80 64.40 90.00

Weld 90.00 65.90 73.60 64.70 74.30 65.90 90.00

88.90 63.50 63.90 49.50 40.30 70.20 90.00

Avg 89.60 63.60 69.60 56.53 62.13 66.83 90.00

Table 6.18(d): Hardness test data – across the weld.

112 Hardness across the weld

100

90

80

70

) 60 RB H ( s

s 50 e n d r

Ha 40

30

20

10

0 012345678

Figure 6.18(a): Hardness graph - across the weld.

• As seen in the Table 6.18(c), the weld is softer than the parent. The hardness joint

efficiency is 0.57. It can be seen from Figure 6.18(a) that a hardness degradation

region (i.e. softened region) has occurred in each joint.

• The hardness values decreases across the weld, with the minimum hardness value

in the weld center or weld nugget. Hence all the tensile specimens failed at the

weld nugget.

6.18.5. Microstructure

Figure 6.18(b): Microstructure of the weld.

113 6.18.5. Comparison – Weld 11, Weld 12, Weld 13 and Weld 14

` 40000 21.354 deg 35000 )

i s

p 30000 (

s 3.773 deg 9.886 deg 15.786 deg s 25000 e r t

S 20000 ld

ie 15000 /Y

k a 10000 e P 5000 0 Shoul der Angles (deg)

Figure 6.18(c): Variation in peak & yield stress.

40000 21.354 deg 35000

) 30000 si 3.773 deg 9.886 deg 15.786 deg p ( 25000 ss e r

t 20000

k S 15000 ea r

B 10000 5000

0 Shou lder Angle (deg)

Figure 6.18(d): Variation in break stress.

• It can be seen from Figures 6.18(b) and 6.18(c) that the tensile properties of each

joints change considerably with the change in the shoulder angles.

114 80 15.786 deg 70 9.886 deg

) 60

B 3.773 deg 21.354 deg

R 50 H ( s s 40

dne 30 r a

H 20

10 0 Shoulder Angle (deg)

Figure 6.18(e): Variation in hardness.

• It can be seen from Figures 6.18(d) that the hardness values of each joints change

considerably with the change in the shoulder angles.

• When the shoulder angle is smaller than 15.7860, the tensile properties decreases

with increase in the shoulder angle and the hardness of the joints increases with

the increase in the shoulder angle.

• When the shoulder angle is greater than 15.7860, all tensile properties increase

with the increase in the shoulder angle and the hardness of the joints tend to

decrease with the increase in the shoulder angle.

• The joints have the best tensile properties and lowest hardness value, of the four

welds, when the shoulder angle is 21.3540 and highest hardness value and lowest

tensile properties, of the four welds, when the shoulder angle is 15.7860.

• The minimum hardness value exists in the weld nugget, accordingly the joints

fractured in the weld nugget.

115 6.19. HIGH-SPEED FRICTION STIR WELD 15

Weld specification

Materials: Al 7075-T6 (0.125”)

Type of Joint: Butt – Tilted and Untilted

Welding Speed: 2”/min

Rotational Speed: 12000 rpm

Tool Shoulder Diameter: 0.375 in

6.19.1. Tensile Test – Parent (Al 7075-T6)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 3279.93 104957.70 99008.70 10.40 104957.70 8.70 2425350

2 3293.21 105382.60 100141.80 10.30 105382.60 8.80 2340873

3 3293.21 105382.60 99433.60 10.50 105382.60 9.20 2331391

Avg 3288.78 105240.97 99528.03 10.40 105240.97 8.90 2365871

Table 6.19(a): Tensile test data of the parent Al 7075-T6.

116 6.19.2. Tensile Test – Weld (Tilted)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 637.39 20396.60 20396.60 3.10 20396.60 3.10 976818

2 699.36 22379.60 22379.60 3.10 22379.60 3.10 1119785

3 885.00 28328.70 28328.70 2.60 28328.70 2.60 2331391

Avg 740.58 23701.63 23701.63 2.93 23701.63 2.93 1059765

Table 6.19(b): Tensile test data of the weld (tilted).

6.19.3. Tensile Test – Weld (Untilted)

SI Peak Peak Break Break Yield Yield Tangent Load Stress Stress Elongation Stress Elongation Modulus (lb) (psi) (psi) (%) (psi) (%) (psi)

1 402.80 12889.50 12889.50 1.70 12889.50 1.70 793020

2 358.53 11473.10 11473.10 1.50 11473.10 1.50 808284

3 309.84 9915.00 9915.00 0.80 9915.00 0.80 1262390

Avg 357.06 11425.87 11425.87 1.33 11425.87 1.33 954565

Table 6.19(c): Tensile test data of the weld (untilted).

117 • The joint efficiencies (weld / parent ratio) of the weld (tilted) with respect to

parent (Al 7075-T6) are 0.24 and 0.23 for Break stress and Peak / Yield stress

respectively. This implies that the tensile strength of the weld is more than the

parent.

• The joint efficiencies of the weld (untilted) with respect to parent (Al 7075-T6)

are 0.12 and 0.11 for Break stress and Peak / Yield stress respectively. This

implies that the tensile strength of the weld is less than parent.

• The average break and yield elongation of the weld (tilted) and weld (untilted) are

much lower than the average break and yield elongation of its parent.

• All the weld tensile test specimens fractured in the weld nugget.

• The weld (tilted) has better tensile properties than the weld (untilted).

118 6.20. HIGH-SPEED FRICTION STIR WELD 16

Weld specification

Materials: Al 7075-T6 (0.125”)

Type of Joint: Butt – Ceramic tool

Welding Speed: 1”/min

Rotational Speed: 15000 rpm

Tool Shoulder Diameter: 0.38 in

6.20.1. Hardness Test – Along the Weld

SI NO Parent Welds

1 2 3

1 88.80 65.00 69.90 60.10

2 88.90 71.70 68.40 48.10

3 88.80 62.50 63.80 43.80

4 88.80

Avg 88.83 66.40 67.37 50.67

Table 6.20(a): Hardness test data of the weld.

• The hardness weld efficiency (weld/parent) obtained are 0.75, 0.76 and 0.57 for

welds 1, 2 and 3 respectively.

119 6.21. HIGH-SPEED FRICTION STIR WELD 17

Weld specification

Materials: Al 7075-T6 (0.125”)

Type of Joint: Butt – Ceramic tool

Welding Speed: 1”/min

Rotational Speed: 15000 rpm

Tool Shoulder Diameter: 0.50 in

6.21.1. Hardness Test – Along the Weld

SI NO Parent Welds

1 2 3

1 88.80 46.10 66.20 56.30

2 88.90 44.30 42.00 60.00

3 88.80 53.50 57.80 32.40

4 88.80

Avg 88.83 47.97 55.33 49.57

Table 6.21(a): Hardness test data of the weld.

• The hardness weld efficiency (weld/parent) obtained are 0.54, 0.62 and 0.56 for

welds 1, 2 and 3 respectively.

120 CHAPTER 7

CONCLUSIONS AND FUTURE SCOPE

1. The average break and yield elongation of the weld is much lower than the

average break and yield elongation of its parents.

2. None of the tensile test specimens failed on the advancing side of the joint, which

implies that the tensile properties of the welds are not the same on either sides of

the weld center. This also implies that the retreating side of the joint is weaker

than the advancing side.

3. The flow patterns on the advancing side and retreating sides of the weld are

different. The FSW can be roughly described as an in-situ extrusion process

where the tool shoulder, the pin, the backing plate and the cold base material form

an extrusion die. Near the top of the weld, because of the shape of the tool, a

substantial amount of material is moved from the retreating side of the weld to the

advancing side. This movement of material causes vertical mixing in the weld and

a complex circulation of material around the longitudinal axis of the weld. This

may be one of the reasons for the failure of the weld in the retreating side [1].

4. The microstructure of the advancing side is characterized by a sharp boundary

between the nugget and TMAZ. The retreating side of the joint has a more

complex microstructure, with no clear boundary between the nugget and TMAZ.

Also the texture is the strongest on the advancing side and weak on the retreating

side. This may be another reason for the failure of the weld in the retreating side

[35].

121 5. There are two low hardness zones on the two sides of the weld center, but the

minimum hardness value exists in the low hardness zone on the retreating side,

accordingly the joints fractured on the retreating side. This implies that the tensile

properties and fracture locations are related to the hardness profile of the weld.

6. The Al 7075-T6 and Alclad 2024-T3 Lap weld tensile test specimens fractured in

the TMAZ on the retreating side.

7. The tensile properties of Al 7075-T6 and Alclad 2024-T3 Lap joints change

considerably with the change in the welding pitch. When the welding pitch is

smaller than 75 r/in, the tensile properties of the joints increases with the increase

in the welding pitch. When the welding pitch is greater than 75 r/in, all tensile

properties tend to decrease with the increase in the welding pitch.

8. The hardness values of Al 7075-T6 and Alclad 2024-T3 Lap joints reduce with a

decrease in the welding pitch. This indicates that softening effect takes place in

the weld with an increase in its welding speed (i.e., decrease in the welding pitch).

9. The Al 6061-T6 Butt joints fractured in the Heat Affected Zone (HAZ). In this

case the minimum hardness zone occurs in HAZ and the fracture surface is

parallel to the TMAZ / HAZ interface on the retreating side.

10. The properties of Al 6061-T6 Butt joints change considerably with the change in

the welding pitch. When the welding pitch is smaller than 75 r/in, the tensile

properties and the hardness of the joints decreases with the decrease in the

welding pitch. When the welding pitch is greater than 75 r/in, all tensile properties

and the hardness of the joints tend to increase with the decrease in the welding

pitch.

122 11. In Al 2024-T3 Butt joints the minimum hardness occurs in the TMAZ on the

retreating side. Therefore, the joints fractured in the TMAZ on the retreating side.

12. All the Alclad 2024-T3 Butt weld tensile specimens failed in the weld nugget due

to crack like defects in the joint and the weld nugget is the minimum hardness

zone in this case.

13. The properties of the welds change considerably with the change in the shoulder

angles. When the shoulder angle is smaller than 15.7860, the tensile properties

decreases with increase in the shoulder angle and the hardness of the joints

increases with the increase in the shoulder angle. When the shoulder angle is

greater than 15.7860, all tensile properties increase with the increase in the

shoulder angle and the hardness of the joints tend to decrease with the increase in

the shoulder angle.

14. Weld energy decreases and the required power increases with the increase in

welding speed at constant weld pitch [21].

15. X axis force increases with the increase in the welding speed at constant welding

pitch. This may indicate that the material being involved in the process is in

different stages of evolution when welded using different speeds [21].

16. The highest energy per unit weld length is required when welding Al 6061-T6.

This is probably because of the relatively high thermal conductivity of the alloy

[21].

123 Because the Friction Stir Welding process has only recently become a subject of wide study, there are currently no large databases of weld properties and, in fact, no specifications on how to make or test friction stir welds exist. In general, the process is robust and a wide range of processing parameters and tool designs can be used to make metallurgically sound welds in a given alloy and plate thickness. In this thesis, only a few friction stir welds, welded in a limited range of welding speed, rotational speed, were tested for their mechanical properties and fracture locations. Tool parameters of the welds considered were not extensive. Further studies have to be done, considering most of the welding parameters, on a wider range of values. Different types of tools, tool parameters have to be considered to determine the effect they have on the resultant welds. Fatigue analysis, shear tests have to be conducted. Some of the tables in this thesis report may not contain all the experimentally obtained values. But the average value in the tables was calculated considering all the values obtained experimentally.

124

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128