9400 CODS Crude Oil Distillation System
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B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 2 of 20
Section 1 – Commercial Summary
All of the following equipment will be as detailed in the attached Technical Summary and Technical Comments and will be subject to the attached Commercial Comments.
Unit Price Part Number Description USD
CODS P50 Crude Oil Distillation System including: . Column and condenser with 50 liter stainless steel boiling flask with drain valve. . Automatic 4 Place Fraction collector with four 19 liter receivers . Automatic Vacuum Regulation System . Bath for temperature control of the condenser and side arm . Cold Traps for Collecting Light Ends . Enclosed Mounting Frame with Plexiglas Doors . Microprocessor Controller . PC with PC Interface and software
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 3 of 20
Optional Equipment
Part Description Total Price Number USD 9M-50- Spare 50 liter stainless steel boiling flask with drain and quench coil. $5,850 10275 Automatic electronic cold finger for the collection of butane and the CC-100-220 protection of vacuum pumps and pressure sensors. Eliminates the need for $10,795 dry ice (solid CO2). 20L 20 liter stainless steel boiling flask with quench coil, stirring heating mantle, $5,450 Conversion mantle top and labjack. PC-D2892- 70 mm SS 15 Plate Packed Column with Jacket $5,200 70
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 4 of 20
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 5 of 20
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 6 of 20 Section 4 – Technical Summary
9400 CODS Crude Oil Distillation System
This crude oil distillation system is designed to semi-automatically distill crude oil and petroleum samples. Parameters are programmed into the PC. The distillation is carried out according to these parameters. Fractions are collected automatically. Reflux ratio, and vacuum level are controlled automatically.
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 7 of 20
1. Boiling Flask:
Feature Description Benefit Stainless steel provides extra Stainless Steel, other safety because it is rugged. Material materials available upon Welded construction request prevents vacuum leaks. PRT temperature probe Provides accurate Boiling Flask inserted in a stainless temperature measurement of Temperature steel thermowell the boiling flask contents. Rapid cooling of boiling flask Automatically Cools using at the end of pressure Quench Coil air or nitrogen sequences or in case of emergency. Allows rapid heating when Bottom Heater Electrically Heated needed. Prevents condensation in the Top Heater Electrically Heated top of the boiling flask. Manually operated drain Allows for easy removal of Drain valve pot residue. Heat Control Automatic Allows unattended operation.
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 8 of 20
2. Distillation Column:
Feature Description Column Diameter 70 mm Column Material Borosilicate Glass Propak 316 SS (other types Packing Type available) Theoretical Plates 15
Vapor Temperature PRT temperature probe for Probe measuring vapor temperature.
Integral glass column and reflux divider totally enclosed in a highly Column Vacuum reflective vacuum jacket having a Jacket permanent vacuum of less than 0.1 mPa.
PRT Temperature probe located Column Heated below the reflux divider and in Jacket Temperature between the heated jacket and Probe column wall.
Column Heated Electrically heated and Jacket automatically controlled
3. Condenser:
Feature Description Material Borosilicate Glass Condensing Surface Very High Area Number of Cooling 2 Coils
Outer Cooling Jacket Yes
As short as possible with insulation to Cooling Lines prevent condensation.
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 9 of 20
4. Reflux Divider for Column:
Feature Description
Location 1 column diameter above top of packing
Reflux Ratio Programmable
Default Setting 5:1 reflux ratio (according to ASTM D2892)
Programmable range From 0:1 to 99:1 reflux ratio
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 10 of 20
5. Butane Collection:
Traditional manual butane traps (cooled with dry ice) are provided.
Manual Butane Traps
Feature Description
Manual Butane Traps with dewars 2
Material Borosilicate Glass
Cooling Medium Dry Ice
Optional Automatic Butane Trap
Feature Description Cooling Automatic (No dry ice needed)
Cooling -75 °C Temperature
Type of Cooling Cold Finger Prevents condensation on outside Cold Trap of cold trap in humid Insulation environments.
Removable receiver with silvered Collection Receiver vacuum jacket.
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 11 of 20
6. Fraction Collector System:
Feature Description Fraction Collector Type Cow
Operation Automatic
Stainless Steel Receivers 19 liter (other sizes available)
Number of Receivers 4
The 7704 fraction collector automatically collects distillate fractions according to their vapor temperature. Up to four fractions can be collected. The collector directs distillate in a temperature range into a receiver.
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 12 of 20
7. Vacuum Regulation System:
The vacuum regulation system is composed of the following components: Vacuum Pump Manual Cold Trap (Optional automatic cold trap available) Pressure sensor Vacuum control valve
Vacuum Pump Specifications
Feature Vacuum Pump
Pump Capacity 12 m3/hour
Oil Capacity 1 liter
Two stage Rotary Pump Type Vain
Pressure Sensors Specifications
Feature Range 100-1 mmHg Precision 0.1 mmHg Accuracy (non-linearity, hysteresis, and non- 0.25% of Reading repeatability) Materials Exposed to Inconel and Gases stainless steel Operating Temperature 0 C to 50 C
Vacuum Control Valve Specifications B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 13 of 20
Feature Exposed Metal 316 stainless steel Surfaces Response Time 15 msec Pressure Control 100 – 1 mmHg Range Proportioning, electro- Type of Valve magnetically operated
Vacuum Control: The pressure sensor interfaces with the controller. At reduced pressures, the controller compares the target vacuum with the actual vacuum level from the pressure sensor. The control valve is then opened or closed enough to achieve the target vacuum level.
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 14 of 20
8. Cooling/Heating Bath:
A cooling/heating bath for temperature control of the condenser is provided.
Bath Specifications
Feature Condenser Bath Reservoir Volume 13 liters Compressor 1 hp Heater 1100 watts Low Liquid Cut Off Yes Over Temp Cut Off Yes Optional Heat Transfer Ethylene Glycol Fluid Programmable Yes Temperature
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 15 of 20
9. Controller:
The unit is controlled by a microprocessor along with peripheral equipment.
Feature Hand Held Keypad and Display
Stores up to 20 distillation programs
Automatically controls the distillation system for minimal operator attention Each distillation program can have 8 programmable temperature fractions Each fraction has programmable Mantle Heating Rates Starting Temperature Finish Temperature Reflux Ratio Programs may be edited during a distillation There are hot keys for making quick adjustments
Displays Vapor and Liquid Temperatures as well as other important information during the distillation
The microprocessor automatically alarms and shuts down the distillation if safety parameters are exceeded.
The microprocessor has complete diagnostics for easy maintenance and servicing
Supports an optional automatic fraction collector for unattended collection of fractions
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 16 of 20
10. Safety System:
Feature Benefit Pot Quench Quick cooling in case of emergency shut down
Programmable maximum boiling Operator can set the maximum safe boiling flask flask temperature temperature to assure safe operation
Power loss safety state System is self sealing during power failure
Temperature probes are checked for short or open Frequent Temperature Probe Test circuits every second Computer checks that all parameters are within Safety parameter Test safe limits every second Safety prompts during startup assure that Safety questions during start up equipment is properly prepared for the distillation to begin
Cooling/heating bath has built-in maximum Cooling/heating bath self temperature, low liquid volume and other safety diagnostics checks
Safety doors Separate the operator from the distillation system.
11. Computer Specifications:
Feature Description Operating System Windows Vista Processor State of the Art Pentium RAM 2 Gigabytes Optical Drive CD/DVD ROM Hard Drive 60 Gigabyte Mouse Optical Network Connection Ethernet Printer Color HP Printer
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 17 of 20
12. Software with Computer:
The computer provides an easy to us PC software for operating the distillation system. Temperature versus time data is collected along with much other information.
Feature Description Benefit Operating System Windows Vista Genuine Windows based program
Distillation Easy to create, use and edit. Make individual programs for each Programs* crude oil type or modify standard programs according to your needs
Semi Automatic control of the distillation system according to D2892
View, print, export or store for Store and use data according to your Data** later use needs
Full data log of all parameters Easily view all aspects of a distillation and setting during distillation stored several times per minute. Logs View a log of any errors and when the occurred Error Log
Schematic of system with Makes visualizing the distillation Process Diagram current sensor outputs and system easy status
Allows Calibration of all PRT Check or calibrate temperature Calibration Screen temperature sensors and probes and vacuum sensors to vacuum sensors comply with ASTM requirements
All functions can be manually Manual Controls operated from the Manual Simplifies maintenance and service Controls Screen
Distillation Programs* B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 18 of 20
Feature Description Distillation Easy to use distillation programs Programs Can be changed before or during Parameters the distillation. Fraction By temperature Collection Temperature range Adjustable Reflux ratio parameters for Heating Rate each fraction
Data**
Feature Description
Time vs. temperature View Graph during or after distillation
During or after View Data distillation
Can be printed directly Results or downloaded to a Output spread sheet or flat file.
Thousands of results can be stored. Stored Result results can be recalled Storage later for view, printing or downloading.
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 19 of 20 9400 Crude Oil Distillation System Specifications:
Control Unit
System Dimensions: Width 75” Depth 36” Height 121” Weight: 500 lbs
Utility Requirements: Electrical 220-230 VAC, @ 75 amps Compressed Air 2 bar, dry and oil free
D2892 Column
D2892 Distillation Column Efficiency: 15 Theoretical Plates Diameter: 70 mm Length: 91 cm Packed Height Packing Type Propak (other types available) Pot Flask Size: 50 liter Stainless Steel (other sizes available) Receiver Size: 19 liters Minimum Operating Vacuum 1 mmHg
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected] page 20 of 20 Section 5 – Technical Comments
This equipment meets the specifications of ASTM D2892, Distillation of Crude Petroleum (15-Theoretical Plate Column) and its annexes. This distillation system is intended for the distillation of crude oil and other petroleum products from their initial boiling points up to 400 °C. The D2892 method does not permit the collection of fractions above 400 °C. However, in most cases this equipment is capable of distilling out to 450°C if desired.
Crude oil distillations are normally performed at multiple pressure levels. The crude oil is first distilled at atmospheric pressure out to a vapor temperature of around 180 °C. Butane and lower boiling materials are collected in special “cold traps” that are cooled by solid carbon dioxide (dry ice).
After cooling the boiling flask, the distillation system is put under a vacuum around 100 or 50 mm Hg. The distillation is resumed. This portion of the distillation is continued to an atmospheric equivalent temperature of around 280 °C. The boiling flask is cooled and then the vacuum level is reduced to around 10 mmHg.
The distillation is resumed. This portion of the distillation is continued to an atmospheric equivalent temperature of around 400 °C ET.
Of course this is only an example of how this equipment would be used. The operator can choose different starting and stopping temperatures as well as different vacuum levels and numbers of vacuum levels.
B/R Instrument Corporation 9119 Centreville Road, Easton, MD 21601 USA Phone: 410.820.8102, Fax: 410.820.8141 Email [email protected]