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Uranium Technology Proceedings of the International Symposium on URANIUM TECHNOLOGY VOLUME I BHABHA ATOMIC RESEARCH CENTRE, TROMBAY, BOMBAY, 400 085 DECEMBER 13-IS, 1989 Organised by ENGINEERING SCIENCES COMMITTEE BOARD Of RESEARCH IN NUCLEAR SCIENCES DEPARTMENT OF ATOMIC ENERGY GOVERNMENT OF INDIA SYMPOSIUM ORGANISING COMMITTEE 1. Shri S. Sen, BARC - Chairman 2. Shri R.K. Garg - IRE Ltd, Bombay Z. Shri M.K. 8atra - UCIL Jaduguda 4. Shri J.L. Bhasin - UCIL Jaduguda 5. Shri K. Balaramamoorthy, - NFC Hyderabad 6. Shri P.R. Roy - BARC 7. Shri A.N. Prasad - BARC 8. Dr.R.M. Iyer - BARC 9. Shri T.K.S. Murthy - IRE Ltd. 10. Prof. S.L. Narayanamurthy - IIT, Bombay 11. Shri T.A. Menon - FACT, Cochin 12. Comdo. K.C. Chatterjee - DCL Bombay 13. Shri CM. Das - NPC, Bombay 14. Dr.C.K. Gupta - BARC 15. Shri K.S. Koppiker - BARC 16. Dr. Ashok Mohan - BARC 17. Dr.V. Venkat Raj - BARC 18. Shri G.R. Balasubramanian - JCCAP. l<*. l»r.G. Viowan.3th.in - HMD.Hyderabad 20. Chi i M.R. Balakriahnan fennc I'l. Uhri u.R. Marw.ih - Member .Secrotary TECHNICAL COMMITTEE 1. Shri K.S. Koppiker, 8ARC - Chairman 2. Shri V.S. Keni, BARC 3. Shri S.K. Chandra, IRE Ltd, Bombay 4. Dr.T.K. Mukherjee, BARC 5. Or.A. Ramanujam, BARC t>. Shri S.N. Bagchi. BARC 7. Shri U.ft. Marwah, BARC - Member Secretary The National Symposium on Uranium Technology was held at BARC, Bombay during Dec. 13-15,1989 under the auspices of Engi- neering Science Committee of Board of Research in Nuclear Science, Department, of Atomic. Energy. In the context of expanding nuclear power programme in Indiai the need for production of large quantity of uranium fuel from indigeneous resources hardly needs any elaboration. After three decades of experience in this area, it is thus appropriate to pool together the expertise and experience gained in the country during this period in various aspects of uranium technol- ogy like exploration, mining, ore processing, refining and con- version to oxide and metal. This symposium has provided an opportunity to the uranium technologists to interact and exchange their experience and plan future strategies. Being the first symposium on this toppic the response has been excellent as evidenced by the extensive participation and contribution of papers covering almost all aspects of uranium technology. Altogether 69 papers, including invited lectures have been presented and the proceeding* have been brought out in two volumes. It is our hope that this technical coverage of the pro- ceedings and panel discussion would serve as a valuable reference material for uranium technologists in the coming years; We wish to record our sincere thanks to the members of the organising and various other committees, authors of invited lectures, and contributed papers, and panel members for making it possible to bring out this proceedings. The cooperation extended by Head, Library and Information Division, BARC is gratefuly acknowledged. TECHNICAL COMMITEE CONTENTS INAUGURAL SESSION 1. Introductory Remarks by Al Shrl S. Sen, Chariman, Organizing Committee 2. Welcome Address by AS Dr. P.K. Iyengar, Director, BARC 3. Presidential Address by A7 Dr. M.R. Srlnivasan, Chairman, AEC 4. Inaugural Address by A13 Dr. H.M. Sethna, Chairman, TOMCO 4 Tata Electric Companies 5. Vote of thanks by A18 U.R. Marwah, Member Secretary, Organizing Committee 6. Keynote Address by A20 Shri R.K. Carg, CMD, IRE Ltd. TECHNICAL SESSION I Plenary Lectures Uranium mining In India - A38 Past, present and the future H.K. Betra, Adviser, UCIL, Jaduguda. TECHNICAL SESSION II II A Uranium Prospecting Contributed Papers 1 Structure as a guide for uranium exploration In the Turamdlh-Mohuldlh area, Slngbhum Dt.Bihar. R. Mohanty, M.B. Vcrma Prospecting for uraniua in carbonate rocks of 19 Vempalli formation, Cuddappah Basin, Andhra Pradesh H. Vasudeva Rao, J.C. Nagabhushana, A.V. Jeygopal and M. Thiaaiah Evaluation of favourable structural features for 36 uranium f roa airborne geophysical surveys over parts of Hadhya Pradesh X.L. Tiku, S.V. Krishna Rao and Bipan Behari Integrated geophysical investigation for uraniua 49 A case study froa Jaaini, Nest Xaaerg Dt. R. Srinivas, J.K. Dash, S. Sethuraa, K.L. Tlku, Bipan Behair K.L. Tlku, Bipan Beharl t Natural theraoluainescence of whole- 74 rock as a potential tool in the exploration for sandstone type uranium deposits: Application to the lower Mahadek sandstone of Meghalaya R. Dhana Raju, R.C. Bhargava, A.Paneerselvaa and S.M. Vlrnave Hydrogcochealcal exploration for uraniua: 90 A cast study froa the Cuddappah Basin, Andhra Pradesh R.P. Singh, P.X. Jala, B.l.H. Kuaar, S.S. Rao, A.V. Patwardhan and S.C. Vasudeva An Alpha-gaaaa counting integrating device 109 for uraniua exploration G. Jha, M. Gaghavayya, H.H. Srlnlvasan, S. Sastry. Ceostatlstlcal study of Bhaten ore deposit C.V.L. Bajpal and P.P. Shai II B Analytical Techniques in Uranium Technology Uranium analysis using an on-lone background 147 correction programme with carrier-distillation technique by a computer controlled spectrometer R.K. Dhumwad, A.B. Patwardhan, V.T. Kulkarni, K.Radhakrislinan Deterainatlon of trace metals in uranium oxide 152 by ICP-MS S. Vijayalakshmi, R. Krishna Prabhu, T.R. Mahalingam and C.K. Mathews Development of flow-injection analysis technique for 157 uranium estimation A.H. Paranjape, S.S. Pandit, S.S. Shinde, A. Ramanujam and R.K. Dhumwad Standardisation of DC Arc carrir-distlllation 166 procedure on a direct reading spectrometer for the deterainatlon of B, Cd etc. in nuclear grade uranium S.S. Biswas, P.S. Murty, S.H. Msrathe, A. Sethuaadhavan V.S. Oixit 1. Kalaal and A.V. Sankaran Spectrographic determination of B,Cd and Nl in 182 aagnesiua fluoride A. Sethuaadhavan, V.S. Dixlt and P.S. Murty. Estiaatloo of uranlua in leach liquors of low 189 iron content: Modification of a spectro- photoaetrlc method using *-(2-pyridil a 20) resorclnol G. Suryaprabhavati, Leela Copal, G.S. Chawdary and Radha R. Das. Discussions 200 TECHNICAL SESSION III III A Mining and Ore Benefeclation Contributed Papers 204 Development of mining at Jaduguda J.L. Bhasln Role of support services at Jaduguda uranium mine 232 S.D. Khanwalkar, V.N. Radhakrlshnana, M.N. Srinivasan, Pinaki Roy, S.N. Bannerji Recovery of uranium concentrate from copper tailings 254 S. Chakraborty, U.K. Tiwari and K.K. Beri Significance of petrology in the ore processing 284 technology with special reference to the uranium processing from the copper tailings of Singbhua Thrust Belt N.P. Subrshmanyam, T.S. Sunilkuaar, D. Naraslahan and N.K. Rao Improved gravity flow sheet for the recovery of 300 uranium values from the copper tailings R. Natarajan, R.S. Jha, U. Sridhar, N.K. Rao Magnetic separation for precoocentration of uranium 318 values from copper plant tailings R.S. Jha, T. Srinivasan, R. Katarajan, U. Srldhar and N.K. Rao Preliminary beneficiatlon studies on uranium ore 332 from Tummalapalli, Andhra Pradesh N.P.H. Padmanabhan, U.Sridhar, N.K. Rao Discussions TECHNICAL SESSION III 111 H An.Tlytic.il Tochniques in Uranium Technology-II Contributed Papers 349 Rapid determination of uranium in uranyl nitrate solution by Ganma Spectronetry T.K. Shankaranarayanan and D.S. Gupta Modification of fluoriaetric Method of uranlua 356 analysis for Jaduguda Plant Saaples A.B. Chakraborty and V.H. Pandey Determination of uraniua In sea water by 369 adsorptlve differential pulse voltaaetry R.N. Xhandekar and Radha Raghunath Difficulties In preparing a standard saaple 376 of uraniua aetal having traces of nitrogen R.S.D. Toteja, B.L. Jangida, N. Sundaresan Estlaation of Bangancse in tailings plant 382 effluents by ICP-AES Joydeb Roy and V.H. Pandey Voltasaetric studies of uraniua (VI) 389 reduction Discussions 402 TECHNICAL SESSION IV Uranium Ore Process Technology Invited Lecture Technologies for processing low-grade uranium 403 ores and their relevance to Indian Situation T.K.S. Murthy Contributed Papers Jaduguda Uranium Mill-Rich experience 431 for future challenges K.K. Berl Grinding and leaching characteristics 463 of the Indian uraniua ores. V.M. Pandey and R.U. Choudhary Recovery of uraniua by direct low-acid 477 leaching froa copper concentrator tailings V.M. Pandey, R.U. Choudhary, A.K. Sarkar, A.P. Bannerjee, A.B. Chakraborty, N. Malty Selection of ion exchange resin for uraniua 485 adsorption froa Jaduguda leach liquors D.P. Saha and V.M. Pandey Apprlicatlon of advanced technologies for uraniua 498 •inlng and processing at Narwa Pahar and Turaadih Projects R.C. Purl and R.P. Veraa Impounding of tailings at Jaduguda - 528 Planning, design and aanageaent of tailings daa S.N. Prasad and K.K. Beri TECHNICAL SESSION V Uranium Ore Process Technology-contd and Byproduct Uranium Contributed Papers Nuclear pure uranium from ores using weak 555 base ion-exchange resins S.V. Parab, S.S. Charat, G. Cherian and K.S. Koppiker Development of an Integrated process for recovery 570 of uranium from ore and its refining at the location of new uranium mill at Turamdlh R.A. Nagle, S.V. Parab, S.S. Charat, A.B. Giriyalkar and K.S. Koppiker Preparation of nuclear grade uranium oxide 582 from Jaduguda leach liquor V.M. Pandey, A.B. Charkraborty and N. Haity Uranium recovery from phosphoric add 592 G. Sivaprakaah On-site teats for recovery of uranium from wet 621 process phosphoric acid at FACT H. Singh, R.A. Hagle, A.B. Giriyalkar, M.F. Fonseca and K.S. Koppiker - Recovery of uranium from nltro-phos acid 628 R.A. Nagle, A.B. Giriyalkar and K.S. Koppiker Recovery of uranium from monazlte - a fresh 635 look at the current practice S.L. Mishra and K.S.
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