Annual Report 2006 and Engineering and Science Materials of Department and Engineering and Science Materials of Department Table of Contents

Editorial ...... 3 Science Stories ...... 5 Publications ...... 27 Equipment ...... 34 Guest Lecturers ...... 36 Staff ...... 38 Graduate Studies ...... 41 Course Program ...... 46 M.Sc. Students ...... 47 Graduated M.Sc. Students with Titles of their Diploma Works ...... 49 Extracurricular Activities ...... 51

Picture on front page: Silicon solar cells. Photo: Hanne Hox.

Annual report for Department of Materials Science and Engineering Norwegian University of Science and Technology NO-7491 ,

Internet address: http://www.ntnu.no/materialteknologi

The editor thanks

- Brit Wenche Meland, Åse Lill Salomonsen, Hilde Martinsen Nordø, Martha Bjerknes and Trond Einar Hagen for collecting the administrative data and taking care of the process of printing the report.

- Skipnes AS for printing From the editors

The annual report from the Department of Materials initiate a second international program in 2008. 33 master Science and Engineering (DMSE) consists of two parts. The students graduated from DMSE in 2007, and the number first part comprises short reports giving an impression is expected to increase in the years ahead. The number of of the current research conducted in the four research exchange students from European universities at NTNU is groups at DMSE, the annual list of publications and also increasing. This year the number of exchange students conference proceedings and the laboratory infrastructure at DMSE was 37. The first students were also enrolled in at DMSE. We hope that this first part of the annual report the new program in nanotechnology at NTNU in 2006, and give external readers an impression of the research being DMSE has ambitions to be one of the leading departments performed at DMSE. The second part, which comprises an in this new emerging field. overview of the staff, master students and PhD students, last years Masters and PhD candidates and their thesis’ The annual number of publications in peer reviewed titles and finally extracurricular activities, is presenting journals has never been higher at DMSE than in 2006. In a comprehensive overview of the annual activity at DMSE fact DMSE is among the best departments at NTNU with and is more intended for the archives. regard to the annual number of publications per faculty member. We intend to continue to deliver research at a The rector at NTNU has in the last year focused on the high international level, but in order to do so our project new strategy plan for the university. NTNU has strong portfolio has to be maintained in order to keep the number ambitions and aims to be among the top 10 technical of PhD students and post docs at the current level. In universities in Europe by 2020. NTNU has also entered a 2006 the Norlight program sponsored by The Research strategic alliance with SINTEF to develop the technological Council of Norway and Norwegian light metal industry environment in Trondheim internationally. The aim is to be came to an end. The light metals industry is one of the among the world leaders in selected areas of R&D. The largest industries in Norway and is consequently the recruitments of excellent faculty and students are maybe most important research fields for DMSE. The light metal the most important step towards future international industry is an important potential employer for our master competitiveness. This year we have recruited one new and PhD students. We expect that light metals will continue associate professor, while one has unfortunately left. As to be important for DMSE, and several new projects in this a part of the strategy at DMSE a new plan defining the field have recently been initiated. DMSE was also heavily research field of four new faculty members has recently involved in several proposals for the Centre for Excellence been submitted to the faculty, and we hope to start the and the Centre for Research-based Innovation sponsored process of recruiting the four new faculty members in by the Research Council of Norway. Unfortunately only one 2007. Unfortunately, the recruitment of both staff and of the initiatives was successful. Despite the low success PhD students is challenging at the time being due to rate we will continue our efforts to strengthen our position the strong demand for new people from the Norwegian to the next call in about five years time. industry. Recruitment of talented staff and students is probably the single most critical factor for our success in The International Course on Process Metallurgy of the years to come. Recruitment of both students and staff Aluminium celebrated its 25th anniversary in 2006. Every members from foreign countries is expected to be much year more than 100 scientists and engineers are visiting more important in the future. At present 25 % of our PhD NTNU to attend this course. This year the 8th Summer student, 40 % of our post-docs and 15 % of our faculty are School on Casting and Solidification of Aluminium and non-native Norwegians. Magnesium Alloys has also been arranged. DMSE, and particularly professor Trygve Foosnæs, have also made The recruitment of good students is fortunately much important contribution for the success of the arrangement better when the demand for master and PhD candidates to “Researchers Night”, where about 1000 pupils from the the Norwegian industry is very high. The students at DMSE vicinity­of Trondheim visit the campus on a Friday evening are enrolled via three different master programs. One of to learn about science and engineering. these is an international masters program, and we plan to

 From the editors

Several of our staff and students were awarded for colleagues at both national and international universities their outstanding contribution during 2006. Professor and institutions. Collaboration is the key element to Lars Arnberg was together with Ragnvald Mathiesen our success and we would like to acknowledge our (SINTEF) awarded the SINTEF Research Award 2006 collaborators at home and abroad. Finally, we would like for their contribution in research on solidifications of to express our gratitude to our sponsors; the Research metals. Moreover, PhD Aaron Marshall received the Council of Norway, the 6th EU framework programs and ExxonMobil award in 2006 for outstanding PhD thesis on finally the Norwegian industry. electrocatalysis. Finally, MSc Trine Okstad was awarded for best MSc thesis in environmental technology.

In several of the research fields we work closely together NTNU April 2007 with researchers at SINTEF, industrial partners and Tor Grande and Knut Marthinsen

Anodized aluminium in polarized light Photo: Gaute Svenningsen

 Physical metallurgy Dendrite fragmentation in aluminium alloys

Columnar-to-equiaxed transition has been studied in situ by X-radiography.

Fragmentation of columnar dendrites during growth is important for the formation of an equiaxed zone in castings. This phenomenon has been studied in situ by X-radiography during directional solidification of Al- Cu alloys. The observations demonstrate that different mechanisms promote dendrite detachment at different location on the mush and compare well with models proposed for fragmentat ion.

Buoyant and settling motions of crystals and liquid play an important role for the detachment of crystal fragments, for their transport out of the columnar mush and for their possibility of survival in the melt and promote a columnar- to-equiaxed transition in the casting. Fragmentation close to the dendrite growth front in the sequence shown below is due to heavy Cu-rich melt that flows into the mush and

causes secondary and ternary arms to melt at their roots, Photo: Lars Arnberg and Ragnvald Mathiesen see Fig. 1.

Other fragmentation mechanisms have also been Fig. 1 studied; coarsening and recalescence, but they occur Fragment (dark feature centre)­ that has just detached from deeper in the mush and the fragments can not readily be dendrite (dark feature lower)­. Distributions of alloying transported to the front and contribute to a columnar-to- elements are also shown (coloured background)­. equiaxed transition.

Lars Arnberg and Ragnvald Mathiesen Fig. 2 Columnar-to-equiaxed transition in an Al-20%Cu alloy. The transition occurs through detachment and growth of dendrite fragments that stops the columnar growth front. Photo: Lars Arnberg and Ragnvald Mathiesen

 Physical Metallurgy

New advance forming press

During the spring semester of 2006 FORMLAB received a but soon also titanium and iron-based materials will be new 1000 kN servo-hydraulic forming press. produced with bulk nanostructure. Because of the second 100 kN load cylinder, bi-axial experiments can be run and The press is financed by theR esearch Council of Norway also ECAP with fully controllable back pressure. and efforts to find financial support for the investment started back in 1999. It has been specially engineered by Other research activities include classical formability the MTS GmbH in Germany and MTS Inc. in the USA. The studies (Marciniak-type FLDs), ram extrusion, forging equipment is already in active use and has proven to be and development of new deformation tools for advanced very accurate for advanced laboratory forming studies. material studies, development of new plastic forming processes and novel joining methods. A major activity is concerned with nano-structuring light metals by Equal Channel Angular Pressing (ECAP), Hans Jørgen Roven

Some of the users surrounding the new 1000 kN forming press. From left to right: Przemyslaw Szczygiel, Tore Jørgensen, Håkon Nesbø, Anders Lilleby, Manping Liu, professor Hans Jørgen Roven (responsible)­, Pål Ulseth and Pål Skaret. Photo: Yongjun Chen

 Physical Metallurgy

Multiscale modelling of age-hardened aluminium alloys

Age hardened aluminium alloys have important applica- components and their crash worthiness, in particular tions in the automotive industry. They are formed in the concerning welded components. soft condition and hardened by a heat treatment. Even though automotive components are not supposed to be The modelling group at our department presented here exposed for plastic deformation after the tempering, is involved in a new centre for research based innovation, knowledge of this matter may be a matter of life and “CRI-SIMLab”, which was established 1 January 2007. This death when accidents occur. project will last for 8 years and is funded by the Norwegian Research Council and industrial partners: Hydro, the In the present multiscale modelling approach two Norwegian defence estate agency, the Norwegian public previously developed microstructure models (Namo road administration, Renault, BMW and Audi. and Alflow) have been combined to predict the effect of precipitates and solute atoms on the work hardening of age hardened aluminium alloys (see Figure). This kind Bjørn Holmedal, Jesper Friis, Erik Nes, Knut Marthinsen of modelling is important concerning automotive safety and Øystein Grong

The strength and ductility of a weld depends on the spatial distribution of the particle sizes, which is a result of the heating history of each location through the heat affected zone (HAZ)­. Photo: Ole Runar Myhr, Hydro Aluminium Structures

 Physical Metallurgy

In-situ mechanical EBSD investigations

A new technique for characterisation of microstructures transformation in these steels. Some examples of outputs in pipeline steels. from the analyses are shown in the figures.

During the last decade supermartensitic stainless At the top row is seen an EBSD orientation map, a phase steel (SMSS) have been applied as subsea pipelines by map (martensite coloured green and retained austenite the oil industry. The need for environmental friendly and red) and a martensite pole figure of the microstructure cost effective solutions has been an important incentive in the as-received condition. At the bottom row the same for the development of these steels. The materials have information is shown for the microstructure after 10 % competitive mechanical and corrosion properties and nominal strain. The volume fraction of retained austenite provide significant cost savings compared to conventional has dropped from 40 % to about 6 % because of the duplex stainless steels. imposed deformation. Also, the pole figures show that the deformation induced martensite has the same orientation As part of an ongoing PhD project at IMT, SEM/EBSD in- as the martensite present in the as-received condition, situ investigations have been conducted on three different indicating that no new variants are formed during the SMSS types. The SEM/EBSD in-situ technique provides plastic deformation. detailed information about the deformation induced phase

Morten Karlsen, Jarle Hjelen and Øystein Grong

The images at the top row show an EBSD orientation map, a phase map and a martensite pole figure of the steel microstructure in the as-received condition. At the bottom row the same information is presented for the microstructure after 10 % plastic deformation. Photo: Morten Karlsen

 Physical Metallurgy

Extensive dispersoid effects achieved by additions of Zr, Sc and Hf to Al-alloys

Dispersoid efficiency understood by 3D atom probe However, recently it has been found that by using Sc in tomography investigations. combination with Zr, homogeneously distributed Al3(Sc,Zr)- dispersoids form. These dispersoids also display other In order to develop aluminium alloys for high attractive properties like rapid precipitation and slow temperature applications it is important to provide alloys, coarsening. However, despite the attractive properties, which after cold and hot deformation can withstand high the high price of Sc has so far limited its use as an alloying temperatures without recrystallising, as recrystallisation element in commercial aluminium alloys. is associated with a considerable strength loss, which in many cases is undesirable. An interesting alternative is hafnium (Hf). Due to Hf’s chemical resemblance with Zr and Sc, it is expected to In commercial aluminium alloys structural stability is show many similarities with these elements. Besides, Hf usually obtained by adding alloying elements like Mn, Cr is naturally always found together with Zr. The objective for and Zr which form finely dispersed precipitates which a recent PhD work was therefore to investigate the effect prevent nucleation and growth of recrystallisation. Of of combined additions of Zr, Sc and Hf on the precipitation these elements, Zr is considered to be the most efficient, behaviour and the recrystallisation resistance after although in most alloys the coherent, metastable Al3Zr- various deformation and annealing conditions of these dispersoids are heterogeneously distributed, implying that alloys, and in particular to investigate to what extent Hf in regions where the dispersoid number density is low, the may substitute or replace Sc. alloy may still be prone to recrystallisation.

Fig. 1 Microstructure in extruded profiles after 1 hr annealing at 600oC of extruded and 0%, 20%, 50%, and 80 % cold rolled pro- files, respectively. Except for some re- crystallised grains in the surface region there are almost no signs of recrystalli- sation even after extrusion and 80% addi­ tional deformation. Photo: Håkon Hallem

Fig. 2 Principle of 3D Atom Probe Tomogra- phy: Single atoms are ionized, repelled from a needle shaped specimen and accelerated towards a position sensi- tive detector in a strong electric field. A ”Time of Flight” (TOF)­ spectrometer gives the mass/charge-ratio for each ion and discriminate between different atom species. Position- and TOF-data are coupled and analysed in a compu- ter and enable 3D-reconstruction of the analysed volume.

 Physical Metallurgy

The investigations revealed that Hf cannot fully replace The 3DAP/TEM-investigations showed that a high Sc, as only heterogeneous dispersoid distributions number density of Sc-rich clusters formed in the early are obtained in the absence of Sc. However, as an stages of precipitation (between 250ºC and 350ºC during extra addition to the already remarkably stable Sc+Zr- heating to the homogenisation temperature). These

containing alloys, Hf can lead to further improvements clusters subsequently transformed to spherical Al3Sc- and consequently open for the use of aluminium alloys at dispersoids. very high temperatures. The more slowly diffusing elements Zr and Hf began

The Al3(Sc,Zr,Hf)-dispersoids were found to be present to segregate to the dispersoid/α-Al matrix interfaces

at even larger volume fractions than the Al3(Sc,Zr)- at higher temperatures (~400ºC), and upon completion ­dispersoids and they also displayed a lower coarsening of the annealing Zr-, Hf-, and Sc-containing “shells”

rate. In both alloys an extraordinary resistance towards could be observed around the Al3Sc-“cores” (Fig 3). recrystallisation was observed, as few (Al-Zr-Sc-Hf alloy) From these findings it could be concluded that Sc is the or no (Al-Zr-Sc) signs of recrystallisation were observed “catalyst” for the rapid formation of homogeneously even after 1 hour annealing of extruded and 80 % cold distributed dispersoids, while the presence of Hf and/or rolled profiles at 600ºC (Fig. 1). Zr in the surrounding ”shell” slow down the coarsening

of the Al3(Sc,Zr) and Al3(Sc,Zr,Hf) dispersoids by reducing To explain why the Al-Sc-Zr- and the Al-Hf-Sc-Zr-alloys the mismatch between dispersoid and matrix lattice behaved so well, 3D atom probe tomography (3D APT) and parameters providing the excellent recrystallisation TEM were used (Fig. 2). resistance that was observed.

Knut Marthinsen

Fig. 3 (a)­ Rebuilt 3D volume with dimensions 4x420 mm2 in an Al-Hf-Sc-Zr-alloy showing a dispersoid. Red, black, blue and green spheres denote Sc, Hf-, Zr-, and Al-atoms, respectively. (b)­ Corresponding chemical composition through dispersoid, clearly demonstrating that the dispersoid consist of a Sc-rich core surrounded by a Zr- and Hf- rich shell.

(a) (b) 100 90 80

) 70 Aluminium % t a ( 60 Zirconium on

i 50 Scandium t i s 40 Hafnium po

m 30 o C 20 10 0 0 2 4 6 8 10 Distance (nm) Photo: Frederic Danoix and Håkon Hallem

10 Physical Metallurgy

Nano-structured magnesium alloys for hydrogen storage

Extremely fine-grained metals for hydrogen storage Improved H-absorption kinetics through microstructural refine- purposes are produced by rapid solidification in a chill- ment by increasing speed of copper wheel (300-2000 REM)­. block melt spinner.

The metal is induction melted in a quartz crucible and is extruded through an orifice by applying a top pressure of inert gas. When the melt hits a spinning copper wheel positioned underneath the crucible, it is rapidly solidified and is thrown off the wheel as a thin solid ribbon, some mm wide and down to 20 μm in thickness.

Magnesium-based alloys are considered promising candidates for hydrogen storage for automotive applications due to their low specific weight, high hydrogen storage capacity (7.6 wt. %) and rich abundance of the Photo: Ying Wu constituent metals. Melt spun ribbons. In order to improve the applicability of magnesium, several methods as adding transition and rear earth metals have been employed to modify the reaction pathway and to enhance the H-sorption kinetics. In addition, rapid solidification has been employed to produce nano-sized grains and even amorphous microstructures to improve the hydrogenation characteristics.

Jan Ketil Solberg, Photo: Ying Wu

Nanocrystalline Mg and Mg2Ni particles (TEM)­. Microstructure after hydrogenation (TEM)­. Photo: Ying Wu Photo: Ying Wu

11 Extractive metallurgy Application of computational fluid dynamics (CFD) to process metallurgy

Fluid flow related phenomena during process metallurgy Fig. 1 are very important to metal quality because they affect Fluid flow in steel continuous cast- other important phenomena during these mixing, ing strands (pathline and trajec- refining, casting and solidification processes. tories of 50μm inclusions respect­ ively)­. These phenomena include turbulent flow in the molten Fig. 2 metal, the transport of bubbles and inclusions, multi-phase Top surface fluctuation and gas flow phenomena, chemical and transport interactions entrainment in an ingot during

between the metal and the slag, the effect of heat transfer, Photo: Lifeng Zhang steel bottom teeming process. the transport of solute elements and segregation.

The flow pattern in the metallurgical vessels can be controlled by many variables, including geometry, metal flow rate, injected gas flow rate, other force sources such as electromagnetic stirring, and slag layer properties. Many of these parameters are easy and inexpensive to change and yet have a profound influence on flow and corresponding quality.

Measurements of various parameters of the hot metal Photo: Lifeng Zhang are not always available and feasible. With the high cost of empirical investigation and the increasing power of Fig. 3 computer hardware and software, Computational Fluid Turbulent energy dissipation rate and bubble plumes in a Dynamics (CFD) simulation is becoming an important tool three gas jets stirring process of steel. to understand these fluid flow-related phenomena during metal refining and casting processes.

A typical CFD simulation includes three dimensional fluid flow model solving the continuity equation and Navier Stokes equations, fluid turbulence models, multiphase

models and particle motion models. CFD can be used Photo: Lifeng Zhang to design furnaces (metallurgical vessels) and optimize operation processes. Fig. 4 Velocity contour (m/s)­ at the top surface and temperature (K)­ Lifeng Zhang at walls in an aluminum casting launder system. Photo: Lifeng Zhang

12 Extractive metallurgy

Refining and recycling of metals

Recycling represents an important opportunity for develop efficient refining methods to purify these metals sustainable and environmentally friendly production by removing impurity elements and inclusions. of light metals. In order to expand the use in Europe of high performance light metals, while reducing energy This research includes fundamentals analysis, consumption and environmental pollution, it is urgent to mathematical modeling, water modeling and pilot hot develop improved ways of recycling light metals. metal experiments, and will combine interdisciplinary knowledge such as physicochemistry (thermodynamics The aim in legislation is to increase the proportion of and kinetics), materials and metallurgical engineering, recycled light metals from the current 25-35 % to 65-70 % mathematics and Computational Fluid Dynamics (as in the steel industry). Recycling aluminum process simulation. only needs 5 % of the energy used in primary aluminum process, and emits 95 % less greenhouse gas than primary The transport phenomena during recycling and refining aluminum. Furthermore, there is an increasing shortage of metals will be investigated, such as fluid flow, free of supply of primary light metals, e.g. light metals surface phenomena and particle motion in molten metal, produced by energy-intensive electrolytic reduction from electromagnetic forces application, chemical reactions, their ores. ignition and combustion of burning materials, heat transfer, radiation, and melting of scraps and fluxes. Recycled light metals should play a major role in the production of light-metal alloy components. The life circle There are many research challenges and potential for of recycling and refining of metals from scrap and dross promoting innovation in this project. The accomplishment is shown in Fig. 1. of this research will gain and maintain the internationally leading position of European research organizations in The current research is to develop efficient methods the research of recycling and refining of metals, and for the recycling of Aluminum, Silicon, Magnesium and encourage small and medium-sized enterprises to initiate Titanium with low input of energy and salt, low secondary new business in the recycling field. dross generation and low greenhouse gas emission, and to Lifeng Zhang

Fig. 1 Fig. 2 Recycling and refining of metals from scrap and dross. Inclusions in a silicon scrap. Photo: Lifeng Zhang Photo: Lifeng Zhang and Arjan Ciftja

13 Electrochemistry Sustainable electrolysis

Continuous development of the modern society including sulphur containing impurities have been studied in recent new and important regions of the world, mainly in China and ongoing research projects. and India, will require increasing energy consumption. Anode processes in aqueous solutions The success of this development will depend on Oxygen is the desired anode product in many industrial sustainable utilisation of the resources in terms of energy electrolysis processes, such as electrowinning of copper and environment. It will be of importance to reduce the and zinc. Currently lead is used as anode material. Oxygen amount of fossil energy sources to avoid possible harmful evolution on titanium based DSA anodes coated with and irreversible impact on the climate. ruthenium and iridium oxide is under investigation.

Electrolysis has grown into a large world-wide industry, The possibilities for developing a method for water and many important chemicals and metals are being electrolysis to supply dissolved oxygen in lakes suffering produced. The future society will depend on the continued from eutrophication is studied in a project collaboration production of traditional and new materials, metals and with Japanese universities and research institutes. chemicals. The anode process in cobalt electrowinning from Of great concern are the increasing emissions of chloride electrolyte has been studied in a PhD project. The

greenhouses gases, especially CO2. The future need for mechanism for the formation of solid CoOOH at the anode increasing quantities of new products inevitably causes an has been studied. Possible methods to prevent this scale increased consumption of energy. Therefore it is important formation have been proposed. to develop new and sustainable industrial processes and the exploration of renewable energy sources. Electrolysis Iron electrowinning (ULCOS, Integrated project 6th can also become and important tool for future development framework programme) of sustainable processes for future production of new and A large research project supported by the steel industry advanced materials, metals and chemicals. in Europe and the EU was established in order to develop a new process for the production of iron and steel with

Norway has a long and rich tradition in the field of drastic reduction of the emissions of CO2. Electrowinning industrial electrolysis. Modern industry was established of iron from molten salts and alkaline aqueous electrolytes mainly through the development of water electrolysis is being studied. plants using hydroelectric power. More recently aluminium electrolysis has become the major electrochemical Silicon electrorefining (FoXy, STREP project, 6th industry, and Norwegian technology development and framework programme) scientific research within aluminium electrolysis are There is a lack of silicon of solar grade quality to meet recognised throughout the world. the demand for the production of solar energy. Therefore there is a need to develop an alternative and cheaper The following research activities within electrolysis and less energy consuming process. Electrorefining of are currently being undertaken, mainly in experimental metallurgical grade silicon in a molten salt is an alternative laboratory studies by researchers, post docs, PhD being studied experimentally. students and MSc students. Many research projects are carried out in cooperation with SINTEF. Electrolytic titanium production A new company, Norsk Titanium AS, was established Aluminium electrowinning recently. Its goal is to become a major player in the world The effects of impurities on important process within titanium production. The possibilities for developing

parameters such as current efficiency and metal quality a molten salt process for electrodeoxidation of solid TiO2 are studied by electrochemical methods. Phosphorus and are studied in a new research project.

14 Electrochemistry Photo: Geir Martin Haarberg Jana Hajasova (Ph.D.-student)­, Ann-Mari Svensson (SINTEF)­, Lars-Erik Owe (Ph.D.-student)­, Ole Edvard Kongstein (postdoc)­, Espen Sandnes (Ph.D.-student)­ and professor Geir Martin Haarberg.

15 Electrochemistry

High temperature PEM fuel cells operating with organic fuels

Employing polymer membranes that operate up to 200 °C biofuels). However, catalytic poisonous species like CO is allows for higher tolerance towards the catalytic formed during the electrochemical conversion of organic poisonous CO during direct oxidation of organic fuels. fuels, which is detrimental for the fuel cell performance. Mechanistic and kinetic considerations are in this context This project is a new research project (2007-2009) funded important in order to be able to determine aspects that by the Norwegian research council. It builds upon our promote a negative or positive effect on the performance extensive experience in the fundamental understanding and efficiency. Enabling an operating temperature above of the oxidation of small organic molecules, catalyst 150°C is important for the CO-tolerance of today’s fuel preparation and preparation of gas diffusion electrodes cell electrocatalysts. Application of carbon nanofibres for high temperature polymer fuel cells operating supported fuel cell electrocatalysts represents a new with phosphoric acid doped polybenzimidazole (PBI) area of scientific interest in this context due to the possible membranes. The latter represent an ongoing research high surface area and an enhanced stability at elevated field together with various international partners. It temperatures. started with the EU-project AMFC (advanced methanol fuel cells, 2001-2003) in the 5th Framework Programme Overall, the ultimate goal of this project is to understand and continued with FURIM (further improvement, active the nature of the electrochemical conversion processes till summer 2008) in the 6th Framework Programme. by employing fundamental methods, and develop and produce electrocatalysts suitable for a biofuel fuel cell Fuel cells can be made sustainable by employing organic operating at temperatures up to 200 °C. fuels, or hydrogen, produced from biomass (so-called

Frode Seland Fig. 1 (a)­ Surface of a gas-diffusion electrode before hot-pressing with membrane, (b)­ cross-section of a tested membrane- electrode assembly (MEA)­. Fig. 2 TEM picture of a carbon nanofibre supported platinum electro­ catalyst prepared by a polyol method. Photo: Gaute Svenningsen and Frode Seland Photo: Mikhail Tsypkin

16 Electrochemistry

Digital acquisition system for FFT ac voltammetry

The software and some ancillary hardware were for use in his laboratories at the University of Victoria, BC, developed by Professor David A. Harrington during his Canada. guest professorship at IMT fall 2006. One complete system is finished and located at the electrochemistry group at IMT. Prof. Harrington is currently building a second system Frode Seland

David Harrington building ancillary hardware. Photo: Frode Seland

17 Electrochemistry

PEM water electrolysis

Water electrolysis currently appears as the only viable The electrode catalysts and especially the anode large-scale technology for converting renewable energy catalyst for oxygen evolution play a critical role in the to hydrogen. total electrolyser efficiency. Typically, noble metals/ metal oxides with rather high loadings have been used. Water electrolysis has been practiced industrially on a Ruthenium oxide is the most catalytic active for the anodic large scale for hundred years, and is a well established oxygen reaction but is highly unstable. Iridium oxide is technology for applications where purity is at premium less active but still considered as the most promising such as the food industries or cooling of power-plant material, either pure or mixed with other noble or non- generators. In other applications hydrogen produced by noble materials. The cathode process requires catalyst water electrolysis is currently too costly to compete with as metallic particles, mostly platinum finely distributed hydrogen derived from fossil fuels. on a support. Current research at the Department of electrocatalytic fine particles of oxide catalysts by modern To realise the grander vision of the hydrogen economy, techniques shows their nanocrystalline and partly improvements in efficiency as well as cost and durability amorphous structure. of electrolysers are required. The Department is involved in this, primarily through its research on polymer For a given composition catalyst activity and stability exchange membranes (PEM) water electrolysis. PEM will depend on composition and preparation procedures. water electrolysis appears as a very promising technology A priori prediction of electrocatalytic activity and stability as far as efficiency and compactness is concerned. of metal oxides for oxygen evolution as a function of these Current densities are typically two to five times those of factors is difficult. However, there is wide agreement that the traditional alkaline electrolysers at similar voltages. the reaction generally occurs via adsorption/desorption reactions involving hydroxyl groups attached to the oxide surface. The electrochemical reaction is thus believed to frequently involve valence changes of the cation of the oxide catalysts. The anode electrocatalyst research at the Department aims at developing a deeper understanding of reaction mechanisms and their dependence on the catalyst composition. Through this we hope to develop a rational basis for electrocatalyst design.

The work is funded by Norwegian industry and the Research Council of Norway. Photo: Aaron Marshall

Svein Sunde Voltage vs. current density for a PEM water electrolysis cell with anode electrocatalysts of different composition.

18 Inorganic chemistry Carbon nanofiber additions to electrodes for the aluminium electrolysis The aluminium industry experiences significant changes gases such as methane and other light paraffins (C1-C5), in calcined petroleum coke quality. Can carbon nano­ ethene, acetylene or CO over metal catalysts. Typically fibers remedy this situation? transition metals such as Fe, Co and Ni are used as catalysts. Using this method, a wide range of carbon Increased demand from the aluminium industry is met nanofiber structures ranging from single-walled carbon by non-traditional cokes that may be of inferior quality. nanotubes to structures where the graphene planes are Such cokes can be more isotropic and have a higher aligned perpendicular to the fiber axis can in principle be impurity content of for example sulfur, vanadium and synthesized. A wide range of carbon nanofiber structures nickel. As a result the anodes may be more exposed to that may become available in sufficient quantities that thermal shock and excess air and CO2 gasification, and are interesting for the aluminium industry in the near there will be increased possibility for metal contamination future is selected in this work. The typical binder matrix of and SO2 emissions. electrodes used in the industry is studied with the impact of different CNFs and manufacturing variables on the Due to their extraordinary material properties there structure and properties of the electrodes. is considerable attention to carbon nanotubes (CNTs) and carbon nanofibers (CNFs) worldwide. Commercially TEM observations reveal detailed information about available carbon nanotubes are readily available from the interfaces between fibers and the binder coke with a number of different production methods including direct evidence for the pitch coke-fiber interaction. In Fig. arc-discharge, laser-ablation and chemical vapour 1 images of two of the fibers are shown, and it is seen deposition (CVD) methods. However, the CVD method has that the binder coke aligns parallel with the tube walls been identified as the most promising for large-scale in the electrodes where multi-walled carbon nanotubes (thousands of tons) and low-cost production of CNTs and (MWNT) are added, while the binder coke is attached to CNFs. The CVD method utilizes pyrolysis of hydrocarbon the graphene plane edges of the fiber in the commercial PR24 samples.

Fig. 1 TEM images of pitch/fiber interfaces in electrodes containing (a)­ MWNT (Original fiber diameter indicated)­, (b)­ PR24. Photo: Department of Materials Science and Engineering

19 Inorganic chemistry

Fig. 2 Fractured surfaces of electrodes with CNF added. (a)­ Fiber bridging (B)­, pullout (P)­ and fracture (F)­, PR24 electrodes, (b)­ Poor dispersion and wetting of CNF, MWNT electrodes. Photo: Sten Yngve Larsen and Trygve Foosnæs Sten Yngve Larsen and Trygve Foosnæs

Fig. 3 Evidence of typical reinforcement mechanisms of fibers Thermal expansion 20-1000 ºC of electrodes with 50 % carbon in composites can be observed by SEM in the fractured nanofibers added. Reference is without fiber added samples containing CNF. However, the full dispersion of the nanofibers is difficult and poorly wetted fibers agglomerate; this may favor stress concentration and crack formation, see Fig. 2. By adding 15 % Fishbone or Fishbone-Tubular carbon nanofiber types to electrode binder matrices a + 30 % increase in the fracture toughness

parameter KIvb was observed compared with reference electrodes without fiber additions.

Isotropic petroleum cokes will give anodes with higher CTEs and accordingly lower resistance towards thermal shocks. Possibly, this effect can be compensated for by the addition of certain nano-fiber qualities, where a 30 % reduction of CTE seems possible. Fig. 3 shows the thermal

expansion of electrodes with a carbon nanofiber content Photo: Sten Yngve Larsen and Trygve Foosnæs of 50 %, compared with reference electrodes without fiber additions.

Sten Yngve Larsen og Trygve Foosnæs

20 Inorganic chemistry

Modelling of baked anodes

An investigation of properties related to thermal shock in The influence of gradients in a carbon anode anodes used in aluminium production. The most common way to form anodes today is by vacuum vibration compaction. In this production stage When an ambient temperature anode is introduced unwanted gradients are made. By taking core samples into an electrolytic pot, it is exposed to a thermal shock through the anode in all direction and analyze these, we as it comes into contact with the electrolytic bath at can visualize the gradients by modelling. Furthermore, approximately 960°C. Sometimes this thermal shock can these material parameters can be used in finite element cause partial or total fracture of the anode. modelling, indicating the cracking probability during electrolysis caused by internal gradients. The cracking of a piece of the anode that falls into the pot will not only significantly perturb the operations of the High density anodes with corresponding high thermal pot, but will also deteriorate the working conditions for conductivity are positive parameters regarding thermal the operators and increase carbon consumption. Hence, shock resistance. The heat from bath will flow faster it is an essential criterion of quality that anodes are highly through the body and provide longer distance between resistant to thermal shock. isotherms. By using the measured material parameters from figure 1 in the finite element modelling program Carbon anode producers are challenged by the ANSYS, we see in the following figures the temperature electrolysis who wants to operate at higher specific development during the first 24 hours through the anode. amperage and have longer cycle time in the pots. This is Tension stresses1 develop in the same pattern as the a hard task knowing the raw material available at market, temperature. i.e. petroleum coke, is degrading. Hence, research work on anode quality is therefore important.

Fig. 1 The plots show density gradients in three horizontal levels of a regular industry anode; top, middle and bottom. This pattern is common for anode blocks produced by vibration compaction. In the upper level there is a typical trough profile, while in the lower part the gradients are more levelled out. Photo: Odd Einar Frosta

21 Inorganic chemistry

Figures 2-4 are results from modelling in ANSYS. the first period of time in the electrolysis cell. Due to a They show temperature profile in a quarter of an anode lower heat conductivity in the upper middle part of the (simplification due to symmetry) at three different time anode and cover material only at the top surface, tension stages after being submerged 16 cm into the molten bath. stresses are created in the anode top. These can cause The view is from centre. A layer of frozen bath immediately cracks similar to those expansion of yoke and stubs are forms around the immersed part with a temperature at responsible for. 650°C. As a boundary condition the anode is only covered at top surface and there is no Joule heating due to current As a conclusion, finite element modelling can be a very at this early stage. Initial temperature of anode is 15°C. useful remedy when investigating the conditions in a cell and what to expect if e.g. specific amperage increase. Given normal boundary conditions and regular trough shape of density gradients in the upper part of the carbon block, the anode temperature profile will change during Odd Einar Frosta and Trygve Foosnæs

Fig. 2 After 15 minutes the temperature shows a U-profile in the lower part. The temperature varies from 15 to 650°C. Photo: Odd Einar Frosta Fig. 4 After 24 hours the temperature has started to increase in the Fig. 3 upper part. Minimum and maximum temperatures are 82 and 1 hour after insertion the heat has moved further up in the 650°C. The profile in the upper part is opposite compared to body. The temperature varies from ca 18 to 650°C and the the profile in the lower part during the first minutes. profile is rather flat in the middle part. Photo: Odd Einar Frosta Photo: Odd Einar Frosta

22 Inorganic chemistry

Water solutions instead of concrete

During tunnel making water leaks from rock may be a leaks in the smallest cracks. The pumping pressure is serious problem. much less than for the traditional concrete pumping, and much less material have to be used since only the narrow Such leaks are traditionally closed by pumping concrete cracks have to be closed to obtain a good result. into the leaking cracks. Due to its particle size concrete cannot reach the smallest pores easily, and high pressure The new method has been tested successfully during must be used to drive the concrete slurry into the cracks. the making of Eikesundstunnelen in the district of Møre, This may result in outbreak of the concrete slurry from Norway in the autumn 2005. Only one injection reduced unwanted positions in the tunnel wall/roof. the water leak with 80 %. The Norwegian road authorities, Vegvesenet, are planning more tests using the new A water solution containing a high amount of “dissolved method.

CaCO3” may be used instead. When this solution is pumped into the rock, Calcite, is precipitated and closes the water Terje Østvold

Tunnel under construction. Photo: Byggeindustrien

23 Inorganic chemistry

The production of nanosized ceramic powders by spray pyrolysis

There are significant activities world wide related to the day. Since establishment we have produced a variety of development of ceramic materials. different compositions and the method has demonstrated its versatility producing high purity, homogeneous In particular there are substantial efforts associated powders with particle size less than 100 nm. The powders with improving the functional properties of a number of have shown excellent sintering properties resulting in multi component oxide based materials. The functional well defined micro structures in the sub micron range. properties are typically related to electronic and The pilot plant is one of only a few production facilities in ionic (protons or oxygen ions) conductivity at elevated Europe. temperatures relevant for the development of solid oxide fuel cells (SOFC) and oxygen permeable membranes as well as materials more typical for the electronic industry Kjell Wiik such as dielectrics (ferro- and piezo-electric). Materials with tailored catalytic properties are also important in a number of applications of significant industrial interest. These material systems have all in common that they are oxide based with rather complex compositions and materials processing is usually based on the availability of homogeneous, nano sized powders.

A particular powerful method to obtain ceramic powders with nano-homogeneity and nano-size combined with a high production rate is spray pyrolysis. The precursors are typically based on water soluble metal salts (e.g. nitrates) mixed in correct proportions and atomized using pressurized air and subsequently fed into a hot rotating chamber where drying and reaction takes place.

A complete pilot plant for powder production based Photo: Tommy Mokkelbost on spray pyrolysis is established at our department with Fig. 1: capacity to produce between 5 and 10 kilos of powder per Process steps for producing ceramic powders by spray pyrolysis.

Fig. 2: a)­ From raw powder, b)­ via calcined powder and c)­ to final high density ceramic bulk material. Photo: Tommy Mokkelbost

24 Inorganic chemistry

A simple method for determination of oxygen transport properties in mixed conducting oxides is established Oxide based ceramic materials showing both electronic exchange of oxygen between sample and ambience. In and ionic conductivity at elevated temperatures are particular the electronic conductivity relaxation resulting useful compounds in a number of applications. from a stepwise change in the ambient partial pressure of oxygen may relatively easy be converted to useful

They may be used as electrodes in Solid Oxide Fuel Cells coefficients related to oxygen bulk diffusion D ( chem) and

(SOFCs) as well as in membranes for separating oxygen oxygen surface exchange (kchem), respectively. from air integrated in processes for producing syngas from natural gas or they may be used simply as an oxygen A dedicated apparatus specially designed for this type of monitor. In all these applications the transport properties measurements have been established at the department of oxygen is of importance, including both the rate of oxygen since long, and is routinely used for characterization exchange between solid surface and ambient atmosphere of transport properties of mixed conducting oxides at as well as the rate of bulk (solid state) diffusion. temperatures up to 1000°C in both oxidizing and reducing atmospheres. Since the electronic conductivity in these materials is proportional with the oxygen content which again is proportional with the ambient partial pressure of oxygen, Kjell Wiik we can easily relate the electronic conductivity with the

Fig. 2 The experimental setup for the electrical conductivity relaxation measurements.

Fig. 1

Oxygen bulk diffusion coefficient (Dchem)­ and oxygen sur- face exchange coefficient (kchem)­ as determined for Sr-doped lanthanum cobaltite (La0.5Sr0.5CoO3-a)­ by the electrical conduct­ ivity relaxation method. Photo: Ivar Wærnhus

Fig. 3 Sample geometry and positioning of electrodes. Photo: Espen Rudberg Photo: Ivar Wærnhus

25 Inorganic chemistry

Self-assembled growth of PbTiO3 nanorods

There is a grate interest in nanostructured materials with dimensional ferroelectric oxides such as PbTiO3. They various functional properties and particles, nanorods and have recently succeeded in developing a novel route to

thin films of a whole range of metals, semiconductors and PbTiO3 nanorods. magnetic materials have been fabricated. The method is based on hydrothermal synthesis using Oxide nano-materials have also been synthesised and a precursor prepared by sol-gel technology. Bur-like particularly the oxide thin film technology have become very structures were shown to be formed under hydrothermal advanced. However, the production of one-dimensional conditions using surfactants. The bure-like structures

(1D) complex oxide nanomaterials has lingered far behind consisted of a core of aggregated nanocrystals of PbTiO3

the preparation of particles and thin films, and to date surrounded by nanorods of PbTiO3 growing out of the core. only a limited number of papers have been published on Surfactants containing phenyl-sulfonic groups resulted in

1D nanomaterials of complex oxides. self-assembly of PbTiO3 nanocrystals resulting in growth of the nanorods. The group has recently been investigating The Inorganic materials and ceramics research group the fundamentals of the growth process. at Department of Materials Science and Engineering have recently started a program on the synthesis of low Tor Grande

Bur-like structures of PbTiO3 nanorods. Photo: Guozhong Wang

26 PUBLICATIONS IN REFEREED JOURNALS AND BOOKS

• EXTRACTIVE METALLURGY Journal of Iron and Steel Research International 13 (2006) 1-8.

Ciftja, A.; Zhang, L.; Engh, T. A.; Kvithyld, A.: Zhang, L.: Purification of solar cell silicon materials through filtration. State of the art in recovery of aluminum from aluminum Rare Metals 25 (2006) 180-185. dross. Light Metals 4 (2006) 931-936. Espelund, A. W.: Frühe eisenmetallurgie in Norwegen. Zhang, L.: Stahl und Eisen 126 (2006) 88-91. State of the art in the control of inclusions in tire cord steels - a review. Espelund, A. W.: Steel Research 77 (2006) 158-169. Pit metallurgy? Metalurgija 12 (2006) 155-164. Zhang, L.: State of the art in the refining and recycling of magnesium. Espelund, A. W.: Materials Science Forum 546-549 (2006) 25-37. Viking to Victorian - exploring the use of iron in ship building. Maritime - Life and Traditions 33 (2006) 78-79. Zhang, L.; Aoki, J.; Thomas, B. G.: Inclusion removal by bubble flotation in a continuous casting Görner, H.; Engh, T. A.; Syvertsen, M.: mold. Kinetics of an AlF aluminium filter. 3 Metallurgical and Materials Transactions B - Process Light Metals 4 (2006) 765-771. Metallurgy and Materials Processing Science 37 (2006) 361- 379. Görner, H.; Engh, T. A.; Syvertsen, M.; Zhang, L.: Removal of Na and Ca from aluminum scrap through filtration. Zhang, L.; Thomas, B. G.: Materials Science Forum 546-549 (2006) 801-806. Fluid flow and inclusion removal in continuous casting strand. Johnsen, K. A.; Grace, J. R.; Elnashaie, S. S. E. H.; Kolbeinsen, Journal of University of Science and Technology Beijing 13 L.; Eriksen, D.: (2006) 293-300. Modeling of sorption-enhanced steam reforming in a dual fluidized bubbling bed reactor. Zhang, L.; Thomas, B. G.: Industrial & Engineering Chemistry Research 45 (2006) 4133- State of the art in the control of inclusions during steel ingot 4144. casting. Metallurgical and Materials Transactions B - Process Metallurgy Meskers, C. E. M.; Kvithyld, A.; Reuter, M. A.; Engh, T. A.: and Materials Processing Science 37 (2006) 733-761. Thermal de-coating of magnesium - a first step towards recycling of coated magnesium. Zhang, L.; Rietow, B.; Thomas, B. G.; Eakin, K.: Magnesium Technology (2006) 33-38. Large inclusions in plain-carbon steel ingots cast by bottom teeming. Safarian-Dastjerdi, J.; Grong, Ø.; Kolbeinsen, L.; Olsen, S. E.: ISIJ International 46 (2006) 670-679. A process model for the carbothermic reduction of MnO from high carbon ferromanganese - the model. Zhang, L.; Zhi, J.; Mei, F.; Zhu, L.; Jiang, X.; Shen, J.; Cui, J.; ISIJ International 46 (2006) 1120-1129. Cai, K.; Thomas, B. G: Basic oxygen furnace based steelmaking processes and Saevarsdottir, G; Palsson, H; Jonsson, M; Bakken, J. A.: cleanliness control at baosteel. Electrode erosion due to high-current electric arcs in silicon Ironmaking & Steelmaking 33 (2006) 129-139. and ferrosilicon furnaces. Steel Research 77 (2006) 385-391.

Tang, K.; Olsen, S. E.: • PHYSICAL METALLURGY Computer simulation of equilibrium relations in manganese ferroalloy production. Bentzen, A.; Holt, A.; Kopecek, R.; Stokkan, G.; Christensen, J. Metallurgical and Materials Transactions B - Process S.; Svensson, B. G.: Metallurgy and Materials Processing Science 37B (2006) 599- Gettering of transition metal impurities during phosphorus 606. emitter diffusion in multicrystalline silicon solar cell processing. Zhang, L.: Journal of Applied Physics 99 (2006) 1-6. Inclusions and bubbles in steel - a review. Journal of Iron and Steel Research International 13 (2006) 1-8. Bjerkaas, H.; Fjeldbo, S. K.; Roven, H. J.; Hjelen, J.; Chiron, R.; Furu, T.: Zhang, L.: Study of microstructure and texture evolution using in-situ Indirect methods of detecting and evaluating inclusions in EBSD investigations and SE imaging in SEM. steel - a review. Materials Science Forum 519-521 (2006) 809-814.

27 Publications in refereed journals and books

Di Sabatino, M.; Arnberg, L.; Brusethaug, S.; Apelian, D.: Johansen, A.; Bauger, Ø.; Embury, J. D.; Ryum, N.: Fluidity evaluation methods for Al-Mg-Si alloys. Alloy development in the Al-Mg-alloy system. Part 1 B. International Journal of Cast Metals Research 19 (2006) 94- Aluminium 82 (2006) 980-984. 97. Johansen, A.; Bauger, Ø.; Ryum, N.: Forbord, B.; Auran, L.; Lefebvre, W.; Hallem, H.; Marthinsen, K.: Aluminium. Rapid precipitation of dispersoids during extrusion of an Al- Aluminium 82 (2006) 1097-1102. 0.91 wt. % Mn-0.13 wt. % Zr-0.17 wt. % Sc-alloy. Materials Science and Engineering A –Structural Materials Johansen, A.; Bauger, Ø.; Ryum, N.: Properties Microstructure and Processing 424 (2006) 174- Alloy development in the Al-Mg-alloy system. 180. Aluminium 82 (2006) 1218-1222.

Friis, J.; Holmedal, B.; Ryen, Ø.; Nes, E. A.; Myhr, O. R.; Grong, Ladanova, E.; Solberg, J. K.; Rogne, T.: Ø.; Furu, T.; Marthinsen, K.: Carbide precipitation in HAZ of multipass welds in titanium Work hardening behaviour of heat-treatable Al-Mg-Si-alloys. containing and titanium free supermartensitic stainless Materials Science Forum 519-521 (2006) 1901-1906. steels. Part 1: Proposed precipitation mechanisms. Corrosion Engineering Science and Technology 41 (2006) 143- Furu, T.; Dons, A. L.; Berstad, T.; Holmedal, B.; Marthinsen, K.: 151. Through process modeling of extrusion: evolution in microstructure and mechanical properties through the Ladanova, E.; Solberg, J. K.; Rogne, T.: whole process chain from as cast and homogenized condition Carbide precipitation in HAZ of multipass welds in titanium to forming of profiles. containing and titanium free supermartensitic stainless Virtual Fabrication of Aluminium Products (2006) 363-376. steels. Part 2: Weld simulation studies. Corrosion Engineering Science and Technology 41 (2006) 152- Grab, T.; Arnberg, L.: 160.

Influence of TiB2 particles on growth of eutectic silicon in aluminium-silicon alloys. Lou, D.; Akselsen, O. M.; Onsøien, M. I.; Solberg, J. K.; International Journal of Cast Metals Research 19 (2006) 201- Berget, J.: 209. Surface modification of steel and cast iron to improve corrosion resistance in molten aluminium. Grong, Ø.; Kolbeinsen, L.; Tranell, G.; Van der Eijk, C.: Surface & Coatings Technology 200 (2006) 5282-5288. Microstructure control of steels through dispersoid metallurgy using novel grain refining alloys. Lou, D.; Akselsen, O. M.; Solberg, J. K.; Onsøien, M. I.; Berget, ISIJ International 46 (2006) 824-831. J.; Dahl, N.: Silicon-boronising of nimonic 90 superalloy. Hallem, H.; Lefebvre, W.; Forbord, B.; Danoix, F.; Marthinsen, K.: Surface & Coatings Technology 200 (2006) 3582-3589.

The formation of Al3(Scx,Zry,Hf1-x-y)-dispersoids in aluminium alloys. Magnabosco, I.; Ferro, P.; Bonollo, F.; Arnberg, L.: Materials Science and Engineering A – Structural Materials An investigation of fusion zone microstructures in electron Properties Microstructure and Processing 421 (2006) 154- beam welding of copper-stainless steel. 160. Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing A424 (2006) 161- Hallem, H.; Rittel, W.; Forbord, B.; Marthinsen, K.: 173. Recrystallisation resistance of extruded and cold rolled aluminium alloys with additions of Hf, Sc and Zr. Marthinsen, K.; Abtahi, S.; Holmedal, B.; Nes, E. A.; Johansen, Materials Science Forum 519-521 (2006) 525-530. A.; Furu, T.; Engler, O.; Lok, Z. J.; Miroux, A.; Talamantes-Silva, J.: Holmedal, B.; Nes, E. A.; Marthinsen, K.: Through process simulation of EN AW-3103 sheet production Work hardening of aluminium alloys - a review of selected modelling the evolution of microstructure, texture, work hardening models. microchemistry and mechanical properties. Virtual Fabrication of Aluminium (2006) 129-156. Virtual Fabrication of Aluminium Products (2006) 343-362.

Hunderi, O.; Friis, J.; Marthinsen, K.; Ryum, N.: Mathiesen, R.; Arnberg, L.; Bleuet, P.; Somogyi, A.: Grain size correlation during normal grain growth in one Crystal fragmentation and columnar-to-equiaxed transitions dimension. in Al-Cu studied by syncrotron X-ray video microscopy. Scripta Materialia 55 (2006) 939-942. Metallurgical and Materials Transactions A - Physical Metallurgy and Materials Science 37A (2006) 2515-2524. Hunderi, O.; Ryum, N.: Introduction to “On the theory of normal and abnormal grain Mathiesen, R.; Arnberg, L.: growth”. Time-resolved X-ray imaging studies of advanced alloy Thermodynamics and Phase Transformations (2006) 231- solidification processes. 233. Advances in X-ray Analysis 49 (2006) 37-45.

Johansen, A.; Bauger, Ø.; Embury, J. D.; Ryum, N.: Mathiesen, R.; Arnberg, L.: Alloy development in the Al-Mg-Alloy system. Part 1 A. X-ray monitoring of solidification phenomena in Al-Cu alloys. Aluminium 82 (2006) 868-872. Materials Science Forum 508 (2006) 69-74.

28 Publications in refereed journals and books

Morgenstern, R.; Videm, M.; Marthinsen, K.; Nes, E. A.; Furu, T.: Graver, B. K. F; Van Helvoort, A. T. J.; Walmsley, J. C.; Deformation and recrystallization behaviour of a Nisancioglu, K.: homogenized and a heterogenized Al-Mg-Si alloy. Surface segregation of indium and tin by heat treatment of Materials Science Forum 519-521 (2006) 1611-1616. aluminium. Materials Science Forum 519-521 (2006) 673-678. Nes, E. A.; Holmedal, B.; Forbord, B.: The effect of boundary structure on the mechanical Halseid, R.; Bystron, T.; Tunold, R.: properties of aluminium alloys. Oxygen reduction on platinum in aqueous sulphuric acid in Materials Science Forum 519-521 (2006) 63-70. the presence of ammonium. Electrochimica Acta 51 (2006) 2737-2742. Roven, H. J.; Hjelen, J.: In-situ deformation of aluminium in the SEM. Halseid, R.; Tunold, R.: Aluminium 82 (2006) 935-935. Hydrogen oxidation on PtRu PEM anodes - mechanism,

effective mass transfer and influence of CO2. Ryen, Ø.; Laukli, H. I.; Holmedal, B.; Nes, E. A.: Journal of the Electrochemical Society 153 (2006) A2319- Large strain work hardening of aluminum alloys and the A2325. effect of Mg in solid solution. Metallurgical and Materials Transactions A – Physical Halseid, R.; Vie, P.; Tunold, R.: Metallurgy and Materials Science 37A (2006) 2007-2013. Effect of ammonia on the performance of polymer electrolyte membrane fuel cells. Ryen, Ø.; Nijs, O.; Sjölander, E.; Holmedal, B.; Ekström, H. E.; Journal of Power Sources 154 (2006) 343-350. Nes, E. A.: Strengthening mechanisms in solid solution aluminum alloys. Krstajic, N. V.; Vracar, L. M.; Neophytides, S. G.; Jaksic, J. M.; Metallurgical and Materials Transactions A - Physical Murase, K.; Tunold, R.; Jaksic, M. M.: Metallurgy and Materials Science 37A (2006) 1999-2006. Supported interactive electrocatalysts for hydrogen and oxygen electrode reactions. Schaffer, P. L.; Arnberg, L.; Dahle, A. K.: Journal of New Materials for Electrochemical Systems 9 Segregation of particles and its influence on the fluidity of an (2006) 83-97. Al-7wt %Si alloy. Scripta Materialia 54 (2006) 677-682. Larsen, M. H.; Walmsley, J. C; Lunder, O.; Nisancioglu, K.: Significance of low copper content on grain boundary Werenskiold, J. C.; Roven, H. J.: nanostructure and intergranular corrosion of AlMgSi(Cu) On the grain refinement mechanisms in SPD - applying high model alloys. resolution electron microscopy and the LEDS approach. Materials Science Forum 519-521 (2006) 667-671. Materials Science Forum 503-504 (2006) 45-50. Marshall, A.; Børresen, B.; Hagen, G. K; Sunde, S.; Tsypkin, Werenskiold, J. C.; Roven, H. J.: M.; Tunold, R.: Understanding the textural and microstructural development Iridium oxide-based nanocrystalline particles as oxygen in two-pass ECAP by route A of a commercial aluminium evolution electrocatalysts. alloy. Russian Journal of Electrochemistry 42 (2006) 1134-1140. NATO Science Series II: Mathematics, Physics and Chemistry 212 (2006) 137-144. Marshall, A.; Børresen, B.; Hagen, G. K; Tsypkin, M.; Tunold, R.:

Electrochemical characterisation of IrxSn(1-x)O2 powders as oxygen evolution electrocatalysts. Electrochimica Acta 51 (2006) 3161-3167. • ELECTROCHEMISTRY Ambrova, M.; Danielik, V.; Fellner, P.; Thonstad, J.: Miland, H.; Glöckner, R.; Taylor, P.; Aaberg, R. J.; Hagen, G. K.: The cathode process in sodium chloride melts containing Load control of a wind-hydrogen stand-alone power system. sulphate. International Journal of Hydrogen Energy 31 (2006) 1215- Electrochimica Acta 51 (2006) 5825-5828. 1235.

Castrillejo, Y.; Bermejo, M. R.; Barrado, E.; Medina, J.; Nisancioglu, K.; Sævik, Ø.; Yu, Y.: Martinez, A. M. C.: Passivity breakdown of aluminium alloys by trace element Electrodeposition of Ho and electrochemical formation of lead. Ho-Al alloys from the eutectic LiCl-KCl. Passivation of Metals and Semiconductors and Properties of Journal of the Electrochemical Society 153 (2006) C713-C721. Thin Oxide Layers (2006) 621-621

Fellner, P.; Jurisova, J.; Khandl, V.; Sykorova, A.; Thonstad, J.: Rodahl, S.; Nisancioglu, K.; Knudsen, O. Ø.: Fracture mechanical testing of adhesion of organic coatings Adsorption of SO2 on alumina. Chemické Zvesti 60 (2006) 311-314. on aluminium. Materials Science Forum 519-521 (2006) 655-660. Giskeødegård, N. H.; Blaijev, O.; Hubin, A.; Terryn, H.; Hunderi, O.; Nisancioglu, K.: Seland, F.; Berning, T.; Børresen, B.; Tunold, R.: Properties of oxide formed on aluminium in aqueous acetate Improving the performance of high-temperature PEM fuel buffer. cells based on PBI electrolyte. Materials Science Forum 519-521 (2006) 717-722. Journal of Power Sources 160 (2006) 27-36.

29 Publications in refereed journals and books

Seland, F.; Harrington, D. A.; Tunold, R.: • INORGANIC CHEMISTRY Fast methanol oxidation on polycrystalline Pt. Electrochimica Acta 52 (2006) 773-779. Chmelar, J.; Foosnæs, T.; Øye, H. A.: Thermal dilation of green anodes during baking. Seland, F.; Tunold, R.; Harrington, D. A.: Light Metals 3 (2006) 597-602. Impedance study of methanol oxidation on platinum electrodes. Ibrahiem, M. O.; Foosnæs, T.; Øye, H. A.: Stability of TiB - C composite coatings. Electrochimica Acta 51 (2006) 3827-3840. 2 Light Metals 3 (2006) 691-696. Stafford, G. R.; Kongstein, O. E.; Haarberg, G. M.: In situ stress measurements during aluminum deposition Kaus, I.; Dahl, P. I.; Mastin, J.; Grande, T.; Einarsrud, M.-A.: Synthesis and characterization of nanocrystalline YSZ from Al Cl3 -EtMeImCl ionic liquid. Journal of the Electrochemical Society 153 (2006) C207- powder by smoldering combustion synthesis. C212. Journal of Nanomaterials (2006) 1-7.

Svenningsen, G.; Larsen, M. H.; Nordlien, J. H.; Nisancioglu, Lein, H. L.; Andersen, Ø. S.; Vullum, P. E.; Lara-Curzio, E; K.: Holmestad, Randi; Einarsrud, M.-A.; Grande, T.: Effect of high temperature heat treatment on intergranular Mechanical properties of mixed conducting La Sr Fe Co O (0,5 ≤ x ≤ 1) materials. corrosion of AlMgSi(Cu) model alloy. 0.5 0.5 1-x x 3-δ Corrosion Science 48 (2006) 258-272. Journal of Solid State Electrochemistry 10 (2006) 635-642.

Svenningsen, G.; Larsen, M. H.; Walmsley, J. C; Nordlien, J. Lein, H. L.; Wiik, K.; Einarsrud, M.-A.; Grande, T.: H.; Nisancioglu, K.: High-temperature creep behavior of mixed conducting La Sr Fe Co O (0,5 ≤ x ≤ 1) materials. Effect of artificial aging on intergranular corrosion of 0.5 0.5 1-x x 3-δ extruded AlMgSi alloy with small Cu content. Journal of the American Ceramic Society 89 (2006) 2895- Corrosion Science 48 (2006) 1528-1543. 2898.

Svenningsen, G.; Lein, J. E.; Bjørgum, A.; Nordlien, J. H.; Yu, Lein, H. L.; Wiik, K.; Grande, T.: Y.; Nisancioglu, K.: Kinetic demixing and decomposition of oxygen permeable Effect of low copper content and heat treatment on membranes. intergranular corrosion of model AlMgSi alloys. Solid State Ionics 117 (2006) 1587-1590. Corrosion Science 48 (2006) 226-242. Lein, H. L.; Wiik, K.; Grande, T.: Svensson, A. M.; Nisancioglu, K.: Thermal and chemical expansion of mixed conducting La Sr Fe Co O materials. Effect of non-uniform reaction rates at solid-oxide interfaces 0.5 0.5 1-x x 3-δ on the electrochemical impedance. Solid State Ionics 177 (2006) 1795-1798. Solid State Ionics 177 (2006) 1955-1959. Madshus, S.; Foosnæs, T.; Hyland, M.; Krane, J.; Øye, H. A.: Thisted, E. W.; Haarberg, G. M.; Thonstad, J.: Composition and intermolecular reactivity of binder pitches and the influence on structure of carbonized pitch cokes. Solubility of AlPO4 in cryolite melts. Thermochimica Acta 447 (2006) 41-44. Light Metals 3 (2006) 541-546.

Thomassen, M. S.; Børresen, B.; Scott, K.; Tunold, R.: Mastin, J. R. M; Einarsrud, M.-A.; Grande, T.: A computational simulation of a hydrogen/chlorine single Crystal structure and thermal properties of La Sa Fe CoO (0 ≤ x ≤ 0.4). fuel cell. 1-x x 1-x 3-δ Journal of Power Sources 157 (2006) 271-283. Chemistry of Materials 18 (2006) 1680-1687.

Thomassen, M. S.; Karlsen, C.; Børresen, B.; Tunold, R.: Mastin, J. R. M; Einarsrud, M.-A.; Grande, T.: Structural and thermal properties of La Sr CoO . Kinetic investigation of the chlorine reduction reaction on 1-x x 3-δ electrochemically oxidised ruthenium. Chemistry of Materials 18 (2006) 6047-6053. Electrochimica Acta 51 (2006) 2909-2918. Nielsen, R. K. B.; Kongshaug, K. O.; Fjellvåg, H.: Thomassen, M. S.; Sandnes, E.; Børresen, B.; Tunold, R.: Syntheses, crystal structures and thermal properties of 3D Evaluation of fuel cell concepts for hydrogen-chlorine fuel coordination polymers assembled from 1,4,5,8-naphthalene­ cells. tetracarboxylic acid. Journal of Applied Electrochemistry 36 (2006) 813-819. Solid State Sciences 8 (2006) 1237-1242.

Thonstad, J.; Kisza, A.; Hives, J.: Ochoa-Fernandez, E.; Rønning, M.; Grande, T.; Chen, D.: Synthesis and CO capture properties of nanocrystalline Overvoltage on metallic inert anodes in low-melting bath. 2 Light Metals 2 (2006) 373-378. lithium zirconate. Chemistry of Materials 18 (2006) 6037-6046. Zenith, F.; Seland, F.; Kongstein, O. E.; Børresen, B.; Tunold, R.; Skogestad, S.: Ochoa-Fernandez, E.; Grande, T.; Rønning, M.; Chen, D.: Control-oriented modelling and experimental study of the Nanocrystalline lithium zirconate with improved kinetics for high temperature CO capture. transient response of a high-temperature polymer fuel cell. 2 Journal of Power Sources 162 (2006) 215-227. Chemistry of Materials 18 (2006) 1383-1385.

30 Publications in refereed journals and books Publications in refereed journals and books

Palcut, M.: Oxidation of a cysteinato ligand by peroxodisulfate in a water-methanol solvent. Mendeleev Communications 16 (2006) 106-107.

Rørvik, S.; Ratvik, A. P.; Foosnæs, T.: Characterization of green anode materials by image analysis. Light Metals 3 (2006) 553-558.

Sagdahl, L. T.; Einarsrud, M.-A.; Grande, T.: Sintering behaviour of La Sr FeO mixed conductors. 1-x x 3-δ Journal of the European Ceramic Society 26 (2006) 3665- 3673.

Sandengen, K.; Kaasa, B.: Estimation of monoethylene glycol (MEG) content in water +

MEG + NaCl + NaHCO3 solutions. Journal of Chemical and Engineering Data 51 (2006) 443-447.

Sansom, J. E. H.; Kendrick, E.; Tolchard, J. R.; Islam, M. S.; Slater, P. R.: A comparison of the effect of rare earth vs Si site doping on the conductivities of apatite-type rare earth silicates Journal of Solid State Electrochemistry 10 (2006) 562-568.

Schøning, C.; Grande, T.: The stability of refractory oxides in sodium-rich environments. Journal of the Minerals Metals & Materials Society 58 (2006) 58-61.

Smith, J. B.; Norby, T.; Fossdal, A.: Electron probe micro analysis of a-site inter-diffusion between LaFeO3 and NdFeO3. Journal of the American Ceramic Society 89 (2006) 582-586.

Søndenå, R.; Ravindran, P.; Stølen, S.; Grande, T.; Hanfland, M.: Electronic structure and magnetic properties of cubic and hexagonal SrMnO3. Physical Review B 74 (2006) 144102-1-144102-12.

Vullum, P. E.; Mastin, J. R. M; Wright, J; Einarsrud, M.-A.; Holmestad, R.; Grande, T.: In situ synchrotron X-ray diffraction of ferroelastic

La0.8Ca0.2CoO3 ceramics during uniaxial compression. Acta Materialia 54 (2006) 2615-2624.

31 CONFERENCE PROCEEDINGS, OTHER REPORTS AND PUBLICATIONS

Bjørgum, E.; Lein, H. L.; Chen, D.; Grande, T.; Holmen, A.: Lou, D.; Akselsen, O. M.; Solberg, J. K.: Reduction/oxidation of La Sr Fe CO O 0,5 0,5 y 1-y 3-δ Surface treatment techniques and materials for advanced perovskite oxides studied by TEOM-MS. aluminium forming tools. 12th Nordic Symposium on Catalysis (2006) 108-109. SINTEF Report STF80MK; F06076. 76 pages.

Ciftja, A.; Kvithyld, A.; Zhang, L.; Engh, T. A.: Moen, K.; Malvik, T.; Breivik, T.; Hjelen, J.: Removal of inclusions from silicon by filtration. Particle texture analysis in process mineralogy. Silicon for the Chemical Industry VIII (2006) 63-70. Proceedings of the XXIII International Mineral Processing Congress (2006) 242-246. Espelund, A. W.: Jern fra keltertid til middelalder. Nisancioglu, K.: Adresseavisen (2006) 07.08.2006. Corrosion science and engineering of light metals: past, present and future. Espelund, A. W.: Korrosionmekanismer, havarier, beskyttelse (2006) 143-143. Ljåsmiing, ljåslått og bruk av slipestein/bryne i tid og rom. Håndverk og kunnskap (2006) 77-95. Robertson, D. G. C.; Peaslee, K. D.; Peter, J. J.; Zhang, L.; Thomas, B. G.: Graver, B. K. F.; Sævik, Ø.; Yu, Y.; Nisancioglu, K.: Continuous steel production and apparatus. Passivity breakdown of aluminium alloys by surface Patent number US20060272447 (2006). enrichment of group IIIA - VA trace elements. Passivation of Metals and Semiconductors and Properties of Szczygiel, P.; Roven, H. J.; Simensen, C.; Reiso, O.: Thin Oxide Layers (2006) 627-627. Microstructural development of “recycled-like” alloys during ECAP: particle break-up, microstructure evolution Grong, Ø.; van der Eijk, C.; Tranell, G.; Kolbeinsen, L.: and mechanical properties. Kornforfiningslegering. The Minerals, Metals, and Materials Society (2006). 497 Patent number 20062484 (2006). pages.

Hirsch, J; Holmedal, B.; Nes, E. A.; Marthinsen, K.; Engler, O.; Tranell, G.; Aarstad, K.; Syvertsen, M.; Engh, T. A.: Abtahi, S.; Schneider, W.; Grun, G. A.; Hamerton, R.; Ekström, The role of fluorine solubility in the protection of molten H. E.; Hurd, T.; Van der Vinden, M.; Brunger, E.; Pettersen, magnesium. T.; Furu, T.; Gottstein, G.; Jacot, A.; Van houtte, P.; Saiyi, L.; Proceedings of the 7th International Conference on Kalz, S.; Miroux, A.; Lok, Z. J.; Anselmino, E.; van der Zwaag, Magnesium Alloys and their Applications (2006) 270-214. S.; Talamantes-Silva, J.; Beynon, J. H.; Pina, C.; Banabic, D.; Erman Tekkaya, A.; Asboel, K.; Karhausen, K.; Crumbach, M.; Tuset, J. K.: Neuman, L.; Kopp, R.; Johansen, A.; Dons, A. L.; Berstad, T.: Thermodynamics of the carbothermic silicon process. Virtual fabrication of aluminium products. Silicon for the Chemical Industry VIII (2006) 23-33. John Wiley & Sons (2006). 405 pages. Wang, X.; Zhang, L.: Kolbeinsen, L.: Effect of operation parameters on the fluid flow and Ferrolegeringer. inclusion motion in continuous casting strands: water Avanserte materialer i Norge 2020. Vedlegg 1: model, numerical simulation and industry measurement, Materialforskning i Norge (2006) 33-36. control of steel cleanliness at unsteady casting period during steel continuous casting. Kolbeinsen, L.: Iron & Steel Technology Conference Proceedings, AISTech Silisium (teknisk). (2006) 371-379. Avanserte materialer i Norge 2020. Vedlegg 1: Materialforskning i Norge (2006) 36-38. Ystenes, M.: Barn med høy intelligens, barn uten stammefrender. Kvithyld, A.; Chithambaranadhan, D.; Ciftja, A.; Øvrelid, E.; Pedagogisk profil 13 (2006) 5-9. Engh, T. A.: Filtration of solar cell silicon scrap. Ystenes, M.: EPD Congress (2006) 919-928. Fra naturlig uran til atombombe. MEMO 1 (2006) 53. Liu, S.; Liang, M.; Niu, S.; Li, C.; Wang, X.; Zhang, L.: Control of steel cleanliness at unsteady casting period Ystenes, M.: during steel continuous casting. Norges miljøbløff. Iron & Steel Technology Conference Proceedings, AISTech MEMO 1 (2006) 34. (2006) 915-927. Ystenes, M.: Oss nerder imellom. MEMO 1 (2006) 79.

32 Conference proceedings, other reports and publications

Ystenes, M.: Overdreven strålefare. MEMO 1 (2006) 67.

Ystenes, M.: Vi aper, uten å forstå. MEMO 1 (2006) 79.

Zhang, L.: Fluid flow, heat transfer and inclusion removal in continuous casting strands. 5th International Conference on Computational Fluid Dynamics in the Process Industries (CFD) (2006) 1-9.

Zhang, L.: Fluid flow, heat transfer and inclusion motion in continuous casting tundishes. 5th International Conference on Computational Fluid Dynamics in the Process Industries (CFD) (2006) 1-9.

Zhang, L.: Fluid flow and transport phenomena during steel refining and casting process. EPD Congress (2006) 659-668.

Zhang, L.: Transport phenomena and CFD application during process metallurgy. Sohn International Symposium (2006) 247-262.

Øye, H. A.; Brekken, H.; Foosnæs, T.; Nygaard, L.: Silicon for the Chemical Industry VIII. Tapir Uttrykk (2006). 256 pages.

33 EQUIPMENT

EXTRACTIVE METALLURGY • Furnace laboratory 5 salt bath furnaces (250°C-590°C), 5 oil bath furnaces Furnaces (50°C-250°C), 9 fluid bed furnaces (0°C-600°C), 2 muffle • Crucible furnace, capacity 140 kg aluminium; with gas furnaces (0°C-800°C, 0°C-1300°C), 2 air circulation purging unit etc. for metal refinery studies. furnaces (0°C-650°C), one with large chamber (Multitherm • Induction furnace, capacity 200 kg of steel, Eloterm. S250/65A, 450mm×450mm×600mm, anno 2003). • Induction furnace, capacity 20 kg of steel, ASEA. • Vacuum induction furnace, capacity 2 kg of steel, Balzer. Mechanical testing • Plasma pilot facility/furnace, capacity 30 kg/h and plasma MTS 810 universal testing machine (10 tons), MTS 880 temperatures up to ~ 3000°C. universal testing machine (10 tons) equipped with 250°C • Electro-melting furnace, one-phase current, for pilot furnace chamber and MTS Teststar control units , shear production of metals. tester, bend tester, compression tools, formability tools, • Small induction furnace up to 3600°C. fatigue and fracture grips, high rate tensile grips, ordinary extensometers and clip gauges for room temperature Water model testing, laser speckle analyser. • Laser methods applied to follow fluid flow and gas bubble flow behaviour in light-transparent models representing Metal forming industrial processes. 60 and 100 tons hydraulic presses, equal channel angular • Pilot scale gas injections (in water). pressing tools, hydroforming tools, Marciniak formability tester (used also in MTS 880), ASAME equipment for Miscellaneous automatic 3-dimensional strain analysis and measurements. • High temperature microscope for wettability studies; Hot torsion machine, two cold rolling mills. sessile drop method. • 10-15 different vertical ‘versatile’ furnaces, temperatures Casting up to 1600°C. • Small scale solidification laboratory • Thermo Gravimetric Analyzer with mass spectrometer. 3 resistor furnaces (max 1000°C), reometer, Podfa filter for • Vacuum/inert gas facility for measurements of diffusion analysing melt quality, Bridgeman furnace (ferro alloys), constants, up to 1200°C. Seiko differential scanning calorimeter (-150°C - 600°C). • Instruments for solubility measurements. • Casting laboratory ASEA 3830 Hz induction furnace (6.5 liters, max 1700°C), Balzer VSG10 3830Hz vacuum induction furnace (1-2 liters, PHYSICAL METALLURGY max 2000°C), induction melt spinner for rapid solidification (5cm3), Marco arc melt spinner for rapid solidification Metallography (100cm3). • Specimen preparation and light optical laboratory Traditional specimen preparation equipment for cutting, Welding embedding, grinding and mechanical polishing, Struers (SINTEF but used by Department of Materials Science and RotoPol-31 automatic grinding and polishing machine, Engineering) Struers Lectropol-5 electropolisher, Struers Tenopol- Hyperbaric welding equipment, ABB welding robot station, 5 for TEM thin foil preparation, 4 optical microscopes Smitweld TCS 1405 resistor weld simulator, 2 high frequency attached with digital cameras (Leica MeF4, Leitz MM6, induction generators (6kW, 12kW), medium frequency Leitz Metalloplan, Zeiss Axiovert 25), Matuzawa DVK-1S generator (50kW), IRC (Instrumented Restrained Cracking) microhardness tester (0.5 – 10 kg), Leica VMHT MOT micro jig, Satoh jig for welding prestrained specimens, Ströhlein hardness tester (1g – 2000g, anno 2003). TCD (Thermal Conductivity Detection) instrument for • Scanning electron microscope (SEM) laboratory hydrogen measurement, mercury based hydrogen analysis Zeiss SUPRA 55VP (LVFESEM, 2006), Hitachi S-4300SE apparatus. (FESEM, 2002), Hitachi S-3500N (LVSEM, 2002), Jeol 840 (1989), Jeol 840 (1985). 4 SEMs are equipped with EDS and Wear testing EBSD. The laboratory has an in-situ sub-stage for combined Pin on disk -, pin on ring - and pin on plate machines, EBSD-thermo mechanical experiments. Struers Microwave abrasive testing machine, water jet • Electron probe microanalyzer (EPMA) erosion machine. Jeol JXA-8500F field emission gun hyperprobe with 5 wavelength dispersive spectrometers, special crystals for Pressing light element analysis, EDS, and cathodoluminescence ABB hot isostatic press (2000 bar, 2000°C), ABB cold system (2006). Chemical analysis of submicron volumes. isostatic press (6000 bar), Thermal Technology Inc. • Transmission electron microscope hydraulic hot axial press (200kPa).

Jeol JEM-2010 (1994) with LaB6 filament equipped with STEM, EDS and Gatan GIF imaging filter. Solar silicon • X-ray diffraction Clean room class 10000, Crystalox DS 250 Bridgeman Siemens D5000 X-ray diffractometer equipped with Euler furnace for directional solidification of (solar cell) silicon, cradle for texture measurements. saw for cutting silicon ingots, Jandel four points probe

34 Equipment

for resistivity measurements, Leo Gieken instrument strength tests up to 1000°C. for measurement of lifetime of minority charge carriers, • Equipment for mechanical characteri¬zation of bending PVScan 6000 instrument for measurement of dislocation strength, E-modulus, fracture toughness and creep up to densities and detection of grain boundaries, GTSolar LBIC 1100°C under controlled atmosphere. (Light Beam Induced Current) measuring device. • Equipment for mechanical 3-point bending of gels (100 g load cell). • Thermal dilation measurements in controlled atmosphere up to 1450°C. ELECTROCHEMISTRY • LECO TC-436 Oxygen and Nitrogen Determinator. Electrochemical equipment: • Micromeretics AccuPyc 1330 Pycnometer. Potentiostates, frequency analysers and sweep generators. Electrochemical quartz crystal microbalance and an Production of carbon materials electrochemical quartz crystal nanobalance. • Pilot plant scale for mixing anode, cathode or ramming Digital Acquisition system for FFT ac voltammetry. paste including sigma-mixer and vibration press.

Surface characterisation: Production of ceramic materials Electrochemical STM/AFM microscopy for performing in • Spray pyrolysis unit for large scale production of ceramic situ combined electrochemical and surface studies. powders. • Spray dryer. Adsorption measurements: • Cold isostatic press (Flow Autoclave Systems). A volumetric PCT (Pressure Composition Temperature) • Uniaxial press. equipment for measurements of hydrogen adsorption in • Tape Caster (Richard E. Mistler). hydride forming materials. Spectroscopy Miscellaneous: • Bruker IFS 66v Fourier Transform Infrared Spectrometer Preparative equipment, vacuum systems, glove boxes, test (4500 100 cm 1). IR microscope. rigs. • Cary 5, UV-VIS-NIR Spectrometer (57000 - 333 cm-1). X-ray diffraction equipment INORGANIC CHEMISTRY • Bruker D8 ADVANCE X-ray diffractometer. - Cu Kα X-ray tube, variable divergence slit assembly Materials characterization: - Theta/theta base goniometer, automatic sample changer, • Thermobalances equipped for rotating reflection sample stage. - Vapour pressure measurements by boiling point and - Variable antiscatter slit assembly, scintillation detector. Knudsen effusion method for use up to 2200°C. - VANTEC-I 1D detector with large active area. - High temperature gravimetric analysis (max. 2200°C) in - TC-Wide Range low/high temperature chamber, rotating controlled atmosphere. ceramic sample stage. • Calorimeters • Siemens D5005 powder X-ray diffracto¬meter, unit A: - Calvet type reaction calorimeters (max. 1120°C). - primary monochromator (quartz) - Differential scanning calorimeter (Perkin-Elmer DSC-2) - Cu Kα X-ray tube, automatic antiscatter slit, scintillation for use up to 727°C. detector - DTA/Reaction calorimeter (max 1200°C). • Siemens D5005 powder X-ray diffractometer, unit B. - TGA/DTA/DSC for use up to 1600°C. - secondary monochromator (graphite), autom. • Viscometers antiscatter and divergence slit, Göbel mirror system, - Precision viscometers for determination of the viscosity high temp. system HTK 15, pos. sensitive and scintillation of molten salts, metals and hydrocarbons at high tem detector, grazing incidence attachment, sample changer peratures and pressures. 40 pos, capillary sample holder. • Equipment for the measurement of thermal conductivity • Philips counter X-ray diffractometer. and thermal diffusivity by the hot strip method of solids or - Diffractogram analysis software with complete ICDD liquids up to 700°C (R and D Carbon). Powder Diffraction File. • Equipment for the measurement of thermal conductivity of • Expectron XDC 1000 precision Guinier camera. bricks and powders up to 1200°C. • High temperature Guinier - Simon camera (Eurat Nonius • Hitatchi S-3400N variable pressure SEM equipped with Delft, FR 533). INCA Energy EDS system and EBSD. • KEJ densitometer for Guinier film. • Reichert-Jung MeF3A optical microscope for metal and mineralogical applications equipped with computerized Catalysis image analysis system. • Reactor for Ziegler-Natta polymerization with continuous • Porosimeters gas flow measurements. - Carlo Erba 2000 WS, (pore radius: 0.004-7.5 mm), Ma • Reactors for production of dimethyl dichlorosilane and cropore 120 (pore radius: 7.5-600 mm). trichlorosilane both with computerized on-line gas - Micromeritics TRISTAR 3000, (pore diameter: 3.5-2100 Å). chromatographs for continuous analysis. One of the • Rapoport test apparatus (R and D Carbon). reactors can be pressurized up to 4 bar. • Rammability (R and D Carbon). • Air Permeability (R and D Carbon). • Specific Electrical Resistance (R and D Carbon). • Sodium resistance test equipment (carbon). • Abrasion tester. • Lloyd LR 100K Materials Testing Machine. Yield and

35 GUEST LECTURERS

Dr. Kevin Dring, Imperial College of London, United Kingdom, Special Adviser Olav Vikane, STATOIL, September 21, 2006. “Water chemistry in oil production”. January 27, 2006. “Electrochemical reduction of solid TiO2 in

molten Cacl2”. Professor Kazushi Mashima, Osaka University, Japan, Professor Dave Embury, McMaster University, Canada, September 27, 2006. “Molecular catalyst: A practical tool to February 2, 2006. “Ultra-high strength materials”. make chiral catalysts”.

Professor Dave Embury, McMaster University, Canada, Professor Tadeusz Kulik, Warsaw University of Technology, February 7, 2006. “Mechanical properties of modern structural Poland, October 16, 2006. “Study and research at Warsaw steels”. University of technology”.

Professor Dave Embury, McMaster University, Canada, Professor Tadeusz Kulik, Warsaw University of Technology, February 8, 2006. “Fracture and formability of 5000-series Poland, October 16, 2006. “Recycling of metals in Poland”. alloys”. Professor Jan Dutkiewicz, Polish Academy of Sciences, Siv.ing. Odd Einar Frosta, Hydro Aluminium, Norway, Poland, October 16, 2006. “Study and research at Institute February 14, 2006. “Raw materials, production and preferred of Metallurgy and Materials Science, The Polish Academy of properties of anodes for the Al-industry”. Sciences”.

Associate Professor Magne Waskaas, Telemark University Professor Jan Dutkiewicz, Polish Academy of Sciences, College, Norway, February 23, 2006. ”Can changes in Poland, October 16, 2006. “Development of a new AlSiMg alloys the interfacial layer in water pipes increase hydro power with scancium addition and (or) on the development of a new production?”. nanocrystalline titanium alloys with Nb and Ta additions using powder metallurgy technique”. Senior Project Engineer Tor Helge Vee, Hydro Aluminium, Norway, March 7, 2006. “Controlling high performance M.Sc. Pawel Widlicki, Warsaw University of Technology, aluminium reduction cells - today’s and tomorrow’s Poland, October 16, 2006. “Warsaw University of Technology solutions”. from a perspective of Ph.D. students”.

Mr.Sc. Inger Johanne Eikeland, Elkem, Norway, March 22, Dr. inz. Zbigniew Pakiela, Warsaw University of Technology, 2006. “Produksjon av Si – hvor har vi vært og hvor går vi?”. Poland, October 16, 2006. “Plastic deformation of metals”.

Mr.Sc. Lars Nygård, Fesil, Norway, March 22, 2006. Professor Blazej Skoczen, Cracow University of Technology, “Prosessindustriens Miljøfond – et rasjonelt miljøtiltak for Poland, October 16, 2006. “Functionally graded materials obtained via the low temperature plastic strain induced phase SO2”. transformation”. Olaf Brastad and Gunnar Grini, Bellona, Norway, March 22, 2006. “Av industri er du kommet, til industri skal du bli og av Professor Adolf Kisza, University of Wroclaw, Poland, industri skal du gjenoppstå”. October 17, 2006. “A new approach to electrochemical methods. The forgotten chronoamperometry”. Dr. Bodil Monsen, SINTEF, Norway, March 22, 2006. “Biokarbon – svaret på Kyoto-protokollen”. Dr. Jerzy Kazmierczak, University of Wroclaw, Poland, October 17, 2006. “Electrode kinetics of the magnesium electrode in Dr. Gabriella Tranell, SINTEF, Norway, March 22, 2006. chloride melts”. “Norges bidrag til internasjonale miljøstandarder”. Research Scientist Karen Sende Osen, SINTEF, October 17, Dr. Tore Torp, Statoil, Norway, March 22, 2006. “Lagring av 2006. ”Oxoacidity studies in chloride melts”.

CO2 i undergrunnen”. Dr. inz. Stanislaw Pietrzyk, AGH University of Science and Competence Manager, Dr. Nancy J. Holt, Hydro Aluminium, Technology, Poland, October 17, 2006. “Electrochemical Norway, April 4, 2006. “Hydro Aluminum: production of testing of inert anodes for aluminium electrowinning”. primary aluminium - to care for the environment”. Research Manager Egil Skybakmoen, SINTEF, Norway, Competence Manager, Dr. ing. Asgeir Bardal, Hydro October 17, 2006. “Laboratory test methods for determining Aluminium, Norway, April 21, 2006. “Technology development the cathode wear mechanism in aluminium cells”. for primary aluminium production”. Senior Scientist Sverre Rolseth, SINTEF, October 17, 2006. Chief Engineer Albert Berveling, Hydro Aluminium, Norway, “Aluminium carbide in hall heroult cells. A permanent layer at April 25, 2006. “Challenges facing the primary aluminium the metal-carbon interface?” industry - Hall-Heroult aluminium reduction - energy consumption”.

36 Guest lecturers

Research Scientist, Dr. Claude Estournès, National Center for Scientific Research (CNRS), France, October 26, 2006. “Spark plasma sintering: Potentialities and limitations”.

Professor, Ph.D. David Harrington, University of Victoria, Canada, October 27, 2006. “Surface electrochemistry of iodine modified Pt (111)”.

Professor Hans J. Möller, TU Bergakademie, Freiberg, Germany, November 28, 2006. ”Hydrodynamic processes in multi-wire sawing (slurry, viscosity, mechanisms for material reoving, sawing, damage, cracks”.

Senior Researcher Trond Bergstrøm, SINTEF, Norway, November 28, 2006. “Projects in sawing at SINTEF”.

Technology Manager Stian Sannes, RecWafer, Norway, November 28, 2006. “Wafer sawing in the PV value chain - prospects and challenges”.

Professor, Dr. Fabrice Mauvy, Bordeaux Institute of Condensed Matter Chemistry, University of Bordeaux, France, November 29, 2006. “New MIEC oxides for SOFC cathode application”.

Professor, Dr. Victor Zymla, Laboratoire de Génie des Procédés et Materiaux, Ecole Centrale de Paris, France, December 8, 2006. “French research on carbonaceous materials in the metallurgical industry”.

Technical Director Jacob Steinmo, Finnfjord Smelteverk, Finnfjord, Norway, December 8, 2006. “The international marked of carbonaceous materials”.

Professor Oleg Ostrovski, School of Materials Science and Engineering, University of New South Wales, Sydney, Australia, December 14, 2006. ”Reduction of manganese-, titanium- and aluminium-oxides with methane”.

37 STAFF

SCIENTIFIC STAFF TECHNICAL STAFF Professor, Ph.D. Lars Arnberg Senior Engineer Rune Thorsen Barland, Professor emeritus Jon Arne Bakken from December 18, 2006 Associate Professor, Dr.ing. Dagfinn Bratland Engineer Jan Arve Baatnes Professor, Dr.ing. Mari-Ann Einarsrud, leave of absence Engineer Terje Forsaa, to June 1, 2006 from November 7, 2006 Engineer Fritz Helgemo Professor emeritus, Dr.ing. Thorvald Abel Engh Senior Engineer Eli Beate Jakobsen Professor emeritus Arne Wang Espelund Senior Engineer Torild Krogstad Professor, Dr.ing. Trygve Foosnæs Chief Engineer Elin Nilsen Professor, Dr.ing. Tor Grande Senior Engineer Tor Arild Nilsen Professor, Dr.ing. Øystein Grong Engineer Kjell Røkke Professor, Dr.scient. Jarle Hjelen Chief Engineer Morten Raanes Professor emeritus, Dr.techn. Jan Lützow Holm Senior Engineer Pål Skaret Professor, Dr.ing. Geir Martin Haarberg Engineer Odd Steinar Strømsli Associate Professor, Dr.ing. Håvard Karoliussen, Engineer May Grete Sætran leave of absence from to June 30, 2006 October 13, 2006 Professor, Dr.ing. Leiv Kolbeinsen Senior Engineer Pål Ulseth Associate Professor, Dr.scient. Kjell Ove Kongshaug, Senior Engineer Torill Anita Hoem Weisethaunet, to June 30, 2006 from October 30, 2006 Associate Professor, Dr.ing. Hilde Lea Lein, Engineer Gunn Torill Wikdahl from November 7, 2006 Chief Engineer Yingda Yu Professor, Dr.philos. Otto Lohne Engineer Trine Øyås Professor, Dr.ing. Knut Marthinsen Professor emeritus, M.Sc.Eng. Ketil Motzfeldt ADMINISTRATIVE STAFF Professor, Ph.D. Erik Nes Professor, Ph.D. Kemal Nisancioglu Head of Administration Trond Einar Hagen Professor emeritus Sverre Olsen Executive Officer Martha Bjerknes Professor emeritus, Dr.techn. Terkel Rosenqvist Office apprentice Hoai Kim Barstad, Professor, Dr.techn. Hans Jørgen Roven from November 6, 2006 Professor emeritus, Dr.techn. Nils Ryum Executive Officer Elsa Mari Florhaug Associate Professor, Ph.D. Frode Seland, Executive Officer Unni Keiseraas from December 1, 2006 Higher Executive Officer Brit Wenche Meland Professor, Dr.philos Jan Ketil Solberg Executive Officer Hilde Martinsen Nordø Professor emeritus, Dr.ing. Åsmund Sterten Secretary Åse Lill Salomonsen Professor, Dr.techn. Svein Sunde Professor, Dr.ing. Merete Tangstad RESEARCH SCIENTISTS Professor emeritus, Dr.techn. Jomar Thonstad Ph.D. Stephane Dumoulin Professor emeritus Reidar Tunold Dr.ing. Ole Edvard Kongstein, from March 1, 2006 Professor emeritus Johan Kristian Tuset Ph.D. Ana Maria Martinez, to September 30, 2006 Associate Professor, Dr.ing. Kjell Wiik Tommy Mokkelbost, from September 1 to October 27, 2006 Professor, Dr.ing. Martin Ystenes Saima Sultan Kazi, from January 23 to May 31, 2006 Professor, Ph.D. Lifeng Zhang Dr.ing. Gaute Stokkan (50 %) Professor, Dr.techn. Terje Østvold Ph.D. Mikhail Tsypkin Professor emeritus, Dr.techn. Harald Arnljot Øye Adjunct Professor, Ph.D. Olaf Engler GUEST PROFESSORS/RESEARCHERS Adjunct Associate Professor, Dr.ing. Øyvind Gustavsen, to August 31, 2006 Professor, Ph.D. Henny J. M. Bouwmeester, Adjunct Professor, Dr.ing. Ola Jensrud from March 6 to April 14, 2006 Adjunct Professor, Dr.techn. Stein Julsrud Professor, Ndabezinhle Dube, from January 4 to Adjunct Professor, Dr.ing. Harald Justnes March 31, 2006 Adjunct Professor, Dr.ing. Tor Lindstad, to May 31, 2006 Professor, David A. Harrington, from August 6 to Adjunct Professor, Dr.ing. Knut Arne Paulsen November 30, 2006 Adjunct Professor, Dr.techn. Oddvin Reiso Dr. Tsuyoshi Murakami, to January 31, 2006 Adjunct Professor, Dr.ing. Christian Rosenkilde Professor, Alexander Zolochevsky, from January 4 to March Adjunct Professor, Dr.ing. Morten Sørlie 31, 2006 Adjunct Professor, Dr.ing. Halvard Tveit Shulan Wang, from January 19 to March 31, 2006 Adjunct Professor, Ph.D. Volodymyr Yartys

38 Staff

POST DOCTORAL FELLOWS Axel Baumann Ofstad Silje Rodahl Dr.ing. Jesper Friis Espen Rudberg Dr.ing. Bjørn Holmedal Birgit Ryningen Ph.D. Zhihong Jia Per Martin Rørvik Dr.ing. Ole Edvard Kongstein, to February 28, 2006 Kristin Vasshaug Dr.ing. Anne Kvithyld Yufeng Wang, from October 30, 2006 Dr.ing. Tore Larsen Andreas Westermoen Dr.ing. Hilde Lea Lein, to November 6, 2006 Ph.D. Yanjun Li EXTERNAL SCHOLARSHIP HOLDERS Ph.D. Manping Liu Ph.D. Raymond Longbottom Jorun Zahl Albertsen Ph.D. Tommy Mokkelbost, from October 28, 2006 Shahid Akhtar, from October 24, 2006 Ph.D. Fride Vullum Hans Bjerkaas, to February 28, 2006 Ph.D. Guozhong Wang Arjan Ciftja, from fall 2006 Ph.D. Ying Wu, from February 7, 2006 Odd Einar Frosta Ph.D. Marisa Di Sabatino Harald Görner, to March 31, 2006 Ph.D. Paul Schaffer Raimo Helenius Ph.D. Frode Seland, to November 30, 2006 Mohamed Ibrahiem, to October 26, 2006 Dr.ing. Magnus Skinlo Thomassen, to August 31, 2006 Jakub Kaczorowski, to October 18, 2006 Ph.D. Julian Tolchard Martin Keppert, to September 30, 2006 Ph.D. Jens Christofer Werenskiold Rannveig Kvande Dr.ing. Kari Aarstad, to January 14, 2006 Sten Yngve Larsen Anders Lilleby SCIENTIFIC ASSISTANTS Francesco Madaro, from June 22, 2006 Johann Mastin, to August 6, 2006 Øystein Andersen, to February 28, 2006 Marian Palcut Sjur Dalsbotten, from September 01, 2006 Jafar Safarian-Dastjerdi Saima Sultana Kazi, from January 23 to May 31, 2006 Kristian Sandengen, to October 13, 2006 Eirin Kvalheim, to February 28, 2006 Maneesh C. Srivastava Håkon Nesbø, from August 15, 2006 Przemyslaw Szczygiel Håvard Norum, to August 15, 2006 Michal Tkac Anne Marthe Pedesen, from October 14 to Helge Weydahl, to April 30, 2006 November 24, 2006 Dongju Zhao Segolene Pelisset, from August 1, 2006 Dimitriy Slizovskiy UNDERGRADUATE ASSISTANTS Ruth Astrid Strøm, from November 13, 2006 Spring term 2006 DEPARTMENT SCHOLARSHIP HOLDERS Andersen, Hanne F. Asbjørnsen, Ingvild Ole-Kristian Eide, to July 13, 2006 Bakke, Olaf Morten Karlsen Bergum, Kristin Tommy Mokkelbost, to July 31, 2006 Brataas, Ingvild Ø. Lars-Erik Owe, from August 14, 2006 Børgund, Monica Sverre Magnus Selbach Eide, Kjersti Meldal Xiangjun Zuo, from October 6, 2006 Eiesland, Jon Cecilie Ødegård Engesvold, Marion Fagerbekk, Siri A. EXTERNAL SCHOLARSHIP Fahadi, Jalal HOLDERS WITH TEACHING DUTIES Frydenberg, Tone Gleditsch , Morten Anawati, from December 13, 2006 Hagen , Linda J. Stein Trygve Briskeby Hasanbegovic, Nedim Paul Inge Dahl, to August 15, 2006 Haugen, Astrid B Halvor Dalaker Haugmo, Ingvild Per Anders Eidem Hognes, Erik Tomas Erlien Holm, Øyvind Egil Fjeldberg Holsæter, Hege Nils Håvard Giskeødegård Hox, Hanne Brit Kathrine F. Graver Høgmoen, Hanne Jana Hajasova Høva, Endre Magnus Fredrik Haakonsen Håland, Torfinn Morten Sundheim Jensen Johansen, Tor Lina M. Jonasson Jøndahl, Mari Eirin Kvalheim, from March 1, 2006 Jørgensen, Vegard Magnus Hurlen Larsen Karlsen, Rolf Magne Ingrid Anne Lervik Kjos, Ole S. Viktor A. K. Myrvågnes Landsem, Eva Erlend Fjøsne Nordstrand

39 Staff

Larsen, Ernst R. Hans Ove Hagen Lerstad, Dag Ola Magnus Hjelen Lied, Ole Kr. Erik Skontorp Hognes Nag, Silje Ole S. Kjos Owe, Lars Erik Marte B. Ludvigsen Ramdal, Ingunn Jarosz Lukasz Roll, Sebastian Ingunn Ramdal Rød, Erik Stian Sjølie Råkvåg, Knut Pietrzyk Stanislaw Slevolden, Elisabeth Ida Svanberg Stangeland, Helga W. Silvie Svarcova Strand, Lilian Helen S. Thang Van Vo Sunde, Tor Olav L. Zhaohui Wang Tennøe, Andreas Camilla Wollan Tjelta, Morten Michelle Ystad Voldsund, Mari Westermann, Ida APPRENTICE Wilhelmsen, Øyvind Wollan, Camilla S. Mari Bakken to June, 2006 Yelikaya Ekrem from August, 2006 UNDERGRADUATE ASSISTANTS ADVISORY BOARD Fall term 2006 Asbjørnsen, Ingvild Lars Arnberg Andersen, Hanne F. Per Anders Eidem Astad, Kristian P. Mari-Ann Einarsrud Bakke, Olaf Trond Einar Hagen (Secretary) Brynjulfsen, Ingvild Vigdis Hjertaker Eide, Kjersti Meldahl Odd Sture Hopperstad Engesvold, Marion Ørjan F. Lohne Erlingsen, Espen Kemal Nisancioglu Fahadi, Jalal Brit Wenche Meland Framnes, Rasmus Aud Nina Wærnes (chair) Haugen, Astrid Bjørgetun Haugmo, Ingvild Eide SUBSTITUTES Hognes, Erik Skontorp Kjell Wiik Holsæter, Hege Chr. Leiv Kolbeinsen Høva Endre M. Geir Martin Haarberg Jensen, Geir Trygve Johansen, Tor DEPARTMENT MANAGEMENT Jørgensen, Vegard Karlsen, Rolf Magne Trygve Foosnæs Kjos, Ole Sigmund Tor Grande Kvitvang, Hans Fredrik N. Øystein Grong Larsen, Ernst Richard Trond Einar Hagen Lied, Ole Kristian Vigdis Hjertaker Opdahl, Christian Geir Martin Haarberg Resell, Martin Eli Beate Jakobsen Roll, Sebastian Leiv Kolbeinsen Skjeldestad, Aslak Manus H. Larsen Slevolden, Elisabeth Ørjan F. Lohne Stangeland, Helga Knut Marthinsen Sunde, Tor Olav Løveng Pål Ulseth Tennøe, Andras Tjelta, Morten Torvanger, Håvard Skomedal Voldsund, Mari Westermann, Ida Wilhelmsen, Øyvind Wollan, Camilla Skotnes Wåsjø, Johanna

SUMMER STUDENTS Elisabeth Adlam Maren Bjørnstad Pioir Drzystek Merethe Falstad Heiko Gaertner

40 GRADUATE STUDIES

Dr.ing./Ph.D. Degrees

During 2006, 60 Dr.ing./Ph.D. students have worked at Department of Materials Science and Engineering. 10 students have been awarded the degree Dr.ing./Ph.D.:

Dahl, Paul Inge: “Synhesis and characterization of ionic conductors based on ZrO2, BaZrO3 and SrCeO3 and preparation

of LaFeO3 and LaCoO3 thin films”. Doctoral thesis 2006:198, IMT-report 2006:86. September 2006. Major Subject: Inorganic chemistry. Dr. lecture: “Single chamber solide oxide fuel cells”. Thesis advisor: Professor, Dr.ing. Mari-Ann Einarsrud. Co-supervisor: Professor, Dr.ing. Tor Grande. Examination committee: Senior Scientist, Dr. Finn Willy Poulsen, Fuel Cells and Solid State Chemistry Department, Risø National Laboratory, Roskilde, Denmark. Professor, Ph.D. Peter Hugh Middleton, Faculty of Engineering and Science, Agder University College, Norway. Professor May-Britt Hägg, Department of Chemical Engineering, NTNU (chair).

Ibrahiem, Mohamed O.: “Pitch and furan-based TiB2-C composite coatings on carbon cathodes”. Doctoral thesis 2006:85, IMT-report 2006:85. September 2006. Major Subject: Inorganic chemistry. Dr. lecture: “Technologies for primary magnesium production - evaluation of development trends”. Thesis advisor: Professor, Dr.ing. Trygve Foosnæs. Co-supervisor: Professor emeritus Harald A. Øye. Examination committee: Professor, Dr. John W. Patrick, School of Chemical, Environmental and Mining Engineering, Nottingham, United Kingdom. Chief Engineer, Dr.ing. Ole-Jacob Siljan, Hydro Aluminium AS, Porsgrunn, Norway. Professor, Dr.ing. Martin Ystenes, Department of Materials Science and Engineering, NTNU (chair).

Johnsen, Kim Andre: “Sorption-enhanced steam methane reforming in fluidized bed reactors”. Doctoral thesis 2006:116, IMT-report 2006:87. October 2006. Major Subject: Extractive metallurgy. Dr. lecture: “Reactor concepts in membrane enhanced steam methane reforming”. Thesis advisor: Professor, Dr.ing. Leiv Kolbeinsen. Co-supervisor: Senior Scientist Dag Øistein Eriksen, Institute for Energy Technology, Kjeller, Norway. Examination committee: Professor emeritus, Douglas Patrick Harrison, Cain Department of Chemical Engineering, Lousianna State University, Baton Rouge (LA), USA. Project Manager Morten Rønnekleiv, Hydrogen FoU, Statoil Research Centre, Trondheim, Norway. Associate Professor Magnus Rønning, Department of Chemical Engineering, NTNU (chair).

Kaczorowski, Jakub: “The boudouard reaction in manganese production”. Doctoral thesis 2006:224, IMT-report 2006:88. December 2006. Major Subject: Extractive metallurgy. Dr. lecture: “Technical solutions on environmental issues in the FeMn production”. Thesis advisor: Adjunct Professor, Dr.ing. Tor Lindstad. Co-supervisor: Research Scientist Martin Syvertsen, SINTEF Materials and Chemistry, Trondheim, Norway. Examination committee: Professor, Dr. Victor Zymla, Laboratoire de Génie des Procédés et Materiaux, Ecole Centrale de Paris, France. Process Engineer, Ph.D. Rodney Ishak, Eramet Norway, Sauda, Norway. Professor, Dr.ing. Merete Tangstad, Department of Materials Science and Engineering, NTNU (chair).

41 Graduate studies

Keppert, Martin: “Electrochemical behaviour of phosphorus species in fluoride melts”. Doctoral thesis 2006:245, IMT-report 2006:89. December 2006. Major Subject: Electrochemistry. Dr. lecture: “Comparison of electrochemical and conventional methods for handling and treatment of waste from nuclear power plants”. Thesis advisor: Professor, Dr.ing. Geir Martin Haaberg. Co-supervisor: Senior Scientist Sverre Rolseth, SINTEF Materials and Chemistry, Trondheim, Norway. Examination committee: Professor, Ph.D. Pavel Fellner, Slovak University of Technology, Department of Inorganic Technology, Bratislava, Slovakia. Chief Engineer, Dr.ing. Odd-Arne Lorentsen, Hydro O&E Research Centre, Porsgrunn, Norway. Adjunct Professor, Dr.ing. Knut Arne Paulsen, Department of Materials Science and Engineering, NTNU (chair).

Mastin, Johann: “Structure, ferroelastic properties and mechanical behaviour of LaCoO3-based materials”. Doctoral thesis 2006:182, IMT-report 2006:83. October 2006. Major Subject: Inorganic chemistry. Dr. lecture: “Texturing of polycrystalline piezoelectric ceramics”. Thesis advisor: Professor, Dr.ing. Mari-Ann Einarsrud. Co-supervisor: Professor, Dr.ing. Tor Grande. Examination committee: Professor Gunnar Svensson, Structural Chemistry, Arrhenius Laboratory, Stockholm University, Sweden. Research Scientist, Dr.ing. Anita Fossdal, SINTEF Materials and Chemistry,Trondheim, Norway. Professor Thomas Tybell, Department of Electronics and Telecommunications, NTNU (chair).

Mjøs, Øyvind: “Directional solidification of silicon for solar cells”. Doctoral thesis 2006:109. June 2006. Major Subject: Physical metallurgy. Dr. lecture: “Production of silicon in a submerged arc furnace”. Thesis advisor: Professor, Ph.D. Lars Arnberg. Examination committee: Professor, Ph.D. Torbjörn Carlberg, Department of Engineering, Physics and Mathematics, Mid Sweden University, Sundsvall, Sweden. Technology Manager, Ph.D. Rita Glenne, Renewable Energy Corporation ASA, Høvik, Norway. Professor, Dr.philos. Otto Lohne, Department of Materials Science and Engineering, NTNU (chair).

Mokkelbost, Tommy: “Synthesis and characterization of CeO2- and LaNbO4-based ionic conductors”. Doctoral thesis 2006:181, IMT-report 2006:84. September 2006. Major Subject: Inorganic chemistry. Dr. lecture: “Nanodesign of metallic particles by spray pyrolysis”. Thesis advisor: Professor, Dr.ing. Mari-Ann Einarsrud. Co-supervisor: Professor, Dr.ing. Tor Grande. Examination committee: Professor, Ph.D. John A. Kilner, Department of Materials, Imperial College, London, United Kingdom. Chief Engineer, Dr.ing. Bent Vigeland, Hydro Oil & Energy, Hydro, Porsgrunn, Norway. Professor, Ph.D. Kemal Nisanciouglu, Department of Materials Scinece and Engineering, NTNU (chair).

Sandengen, Kristian: “Prediction of mineral scale formation in wet gas condensate pipelines and in MEG (mono ethylene glycol”) regeneration plants”. Doctoral thesis 2006:137, IMT-report 2006:82, IUK-Thesis 118. September 2006. Major Subject: Inorganic chemistry. Dr. lecture: “Methods of scale removal – the potential usefulness of crown ethers and other complexing agents”. Thesis advisor: Professor, Dr.techn. Terje Østvold.

42 Graduate studies

Examination committee: Managing Director, Dr. Graham M. Gordon, Scaled Solutions Ltd., Livingston, United Kingdom. Special Adviser Production Technology, Dr.philos. Olav Vikane, STATOIL ASA, Stavanger, Norway. Associate Professor, Dr.ing. Jens-Petter Andreassen, Department of Chemical Engineering, NTNU (chair).

Weydahl, Helge: “Dynamic behaviour of fuel cells”. Doctoral thesis 2006:94. August 2006. Major Subject: Electrochemistry. Dr. lecture: “Unitized regenerative fuel cells. Opportunities and obstacles”. Thesis advisor: Professor, Dr.techn. Svein Sunde. Examination committee: Professor, Dr. Keith Scott, School of Chemical Engineering and Advanced Materials, University of Newcastle upon Tyne, United Kingdom. Professor, Dr. Göran Lindbergh, Department of Chemical Engineering and Technology, Applied Electrochemistry, The Royal Institute of Technology, Stockholm, Sweden. Associate Professor Hilde Venvik, Department of Chemical Engineering, NTNU (chair).

The following Dr.ing./Ph.D. projects are in progress:

Name Title Thesis advisor

Akhtar, Shahid Hydrogen porosity in aluminum castings. Arnberg, Lars

Albertsen, Jorun Zahl Experimental and theoretical investigations of metal dusting Grong, Øystein corrosion in plant exposed nickel-based alloys.

Bjerkaas, Hans In-situ deformation of AlMgSi-alloys, experiments, state of the art Roven, Hans Jørgen equipment and theoretical modelling of plastic flow.

Briskeby, Stein Trygve Electrocatalysts of noble metals supported on carbon nanofibres. Sunde, Svein

Ciftja, Arjan Refining of recycled photo voltaic silicon by filtration and argon gas Zhang, Lifeng bubbling

Dalaker, Halvor Thermodynamics of solar cell silicon in the high temperature Tangstad, Merete area.

Eide, Ole-Kristian IR and NMR spectroscopy of catalyst for olefin polymerization. Ystenes, Martin

Eidem, Per Anders Electrical conductivity of coke beds. Tangstad, Merete

Erlien, Tomas Laugsand Cold bonding mechanisms in aluminium alloys. Grong, Øystein

Fjeldberg, Egil Modelling and simulation of nano- and microstructure in Al-alloys. Marthinsen, Knut

Frosta, Odd Einar Modeling of baked anodes. Foosnæs, Trygve

Giskeødegård, Nils Håvard Adhesion of organic functional groups on aluminium. Nisancioglu, Kemal

Graver, Brit K. F. Modification of properties of aluminium alloys by surface Nisancioglu, Kemal segregation of nanoscale trace element particles.

Görner, Harald Development of an AlF3 active filter for Al. Zhang, Lifeng

Hajasova, Jana Electrochemical behaviour of dissolved impurity species of sulphur Haarberg, Geir Martin and phosphorus in molten salts.

Helenius, Raimo High pressure die casting of light metals. Lohne, Otto

Haakonsen, Fredrik Optimazing of strømhard austenitic manganese steel. Solberg, Jan Ketil

Jensen, Morten Sundheim Chemical degradation, wetting and electrochemical properties of Grande, Tor

polycrystalline TiB2 inert cathodes.

Jonasson, Lina Margareta Cathode structure and cathode wear in aluminium electrolysis Foosnæs, Trygve cells.

Karlsen, Morten Thermo-mechanical in-situ investigations using the EBSD. Hjelen, Jarle

43 Graduate studies

Kvalheim, Eirin Oxygen evolving anodes for electrowinning from molten salts. Haarberg, Geir Martin

Kvande, Rannveig Casting of silicon for use in solar cells. Arnberg, Lars

Larsen, Magnus Hurlen Effect of composition and thermomechanical processing on the Nisancioglu, Kemal intergranular corrosion of AA6000 aluminium alloys.

Larsen, Sten Yngve Novel carbon materials in electrometallurgical applications. Foosnæs, Trygve

Lervik, Ingrid Anne Electrocatalyst for PEM water electrolysis. Sunde, Svein

Lilleby, Anders Sunde Mathematical modelling of material flow during extrusion and Grong, Øystein joining of aluminium based on the HYMEN bonding method.

Madaro, Francesco Synthesis of textured piezo- and ferroelectric materials by chemical Grande, Tor and ceramic techniques.

Myrvågnes, Viktor Alfred Structure and behaviour of fossil reduction materials in the silicon- Lindstad, Tor and ferrosilicon process.

Nordstrand, Erlend Fjøsne Effects of non-metallic inclusions on the transformation behaviour Grong, Øystein of steel.

Ofstad, Axel Baumann Increasing the lifetime of PEM fuel cells - a fundamental study of Sunde, Svein degradation mechanisms.

Owe, Lars-Erik Oxide electrocatalysts for the oxygen evolution reaction during Sunde, Svein water electrolysis.

Palcut, Marian Cation diffusion in ABO3 perovskite oxides. Grande, Tor

Paulsen, Ove Bjørn Sealing of high temperature membrane reactors. Grande, Tor

Rodahl, Silje Chromate-free pre-treatment of aluminium for organic coating. Nisancioglu, Kemal

Rudberg, Espen Andre Oxygen and hydrogen exchange on functional oxide membranes. Nisancioglu, Kemal

Ryningen, Birgit Characterisation of solar cell – silicon. Lohne, Otto

Rørvik, Per Martin Ceramic nanoparticles and nanostructures by chemical methods. Einarsrud, Mari-Ann

Rørvik, Stein Migration effects in prebaked anodes. Foosnæs, Trygve

Safarian-Dastjerdi, Jafar Kinetics and mechanisms of reduction of MnO containing silicate Kolbeinsen, Leiv slags by selected forms of carbonaceous materials (slag-carbon reactivity).

Sandnes, Espen The anode process on carbon in chloride melts. Haarberg, Geir Martin

Selbach, Sverre Magnus Size and strain effects in ferroelectric and piezoelectric materials. Grande, Tor

Sorin, Isac Metal powder project – “metal printing process”. Arnberg, Lars

Srivastava, Maneesh High pressure die casting of aluminium and magnesium alloys. Lohne, Otto

Szczygiel, Przemyslaw ECAP recycled Al alloys – experimental characterization of Roven, Hans Jørgen properties and microstructure.

Tkac, Michal Porosity development in composite carbon materials during heat Foosnæs, Trygve treatment.

Vasshaug, Kristin Electrochemical wear of carbon materials in fluoride melts. Haarberg, Geir Martin

Westermoen, Andreas Modelling of dynamic arc behaviour in a plasma reactor. Tangstad, Merete

Zhao, Dongju Processing, properties and performance in use of direct reduced Kolbeinsen, Leiv iron pellets containing added material to control steel structure.

Ødegård, Cecilie Conversion of silicon tetrachloride to trichlorosilane. Foosnæs, Trygve

Åkre, Torjus Depolarised anodes for electrowinning of cobalt from chloride Haarberg, Geir Martin solutions.

44 Graduate studies

The following Dr.ing. projects are co-supervised in other departments

Name Title Thesis advisor

Arvaniti, Eleni Soil stabilization and waterproofing of concrete constructions. Payatakes, Alkiviades (University of Patras, Department of Chemical Engineering, Patras, Greece) Østvold, Terje

Canelopoulo, Maria CaCO3 scale formation in 2D model pore networks. Payatakes, Alkiviades (University of Patras, Department of Chemical Engineering, Patras, Greece) Østvold, Terje

Chmelar, Juraj Size reduction and specification of granular petrol coke with respect Sandvik, Knut Lyng to chemical and physical properties. (NTNU, Department of Geology and Mineral Resources) Foosnæs, Trygve

Fjeldbo, Snorre Kjørstad Experimental studies and simulation of structure evolution and Støre, Sigurd formability along complex loading paths (NTNU, Department of Engineering Design and Materials) Roven, Hans Jørgen

Psarrou, Maria Protecting soil from water erosion through precipitation of calcium Payatakes, Alkiviades phosphate. (University of Patras, Department of Chemical Engineering, Patras, Greece) Østvold, Terje

Sæterli, Ragnhild Kjæstad Electronic structure of thermoelectric materials - TEM studies at the Holmestad, Randi nanoscale. (NTNU, Department of Physics) Marthinsen, Knut

Søndenå, Rune Dynamic structure energetics and phase stability of 1D, 2D and 3D Stølen, Svein network-forming compounds and melts. (University of Oslo, Department of Chemistry) Grande, Tor

45 COURSE PROGRAM

Descriptions of the courses offered at the Department are included in the University Course Catalogue that can be obtained from Student and Academic Section, NTNU. The present survey lists the courses given by our scientific staff.

Course Semester: Title Lectures and exercise Passed/ no. Spring=S Credits in parenthesis coordinators Started Autumn=A TMT4105 S Gen. Chem., (7.5) M. Ystenes 5/20 TMT4106 S Gen. Chem., (7.5) M. Ystenes 198/262 TMT4110 S Gen. Cemi. (7.5) D. Bratland 103/122 TMT4120 S Gen. Chem., 2 (7.5) T. Foosnæs 59/61 TMT4130 S Inorg. Chem., (7.5) T. Grande, M-A. Einarsrud 61/72 TMT4140 S Appl. Thermodyn., (7.5) T. Østvold, T. Haug-Warberg 36/60 TMT4150 S Refractories, (7.5) K. Wiik 13/13 TMT4160 S Hightemp. Chem., (7.5) K. Wiik 16/16 TMT4175 S Materials Technology 2 (7.5) Ø. Grong, K. Marthinsen, O. Lohne 29/29 TMT4206 S Fluid and Heat Transfer, Intr. Course T. Lindstad, R. Kristoffersen, H. F. Svendsen 16/23 TMT4210 S Material and Process Modelling (7.5) K. Marthinsen 22/22 TMT4215 S Casting (7.5) L. Arnberg 2/3 TMT4225 S Mech.Prop. of Eng. Mat. 2 (7.5) E. Nes 10/10 TMT4235 S Refin. and Recycl. of Met. (7.5) L. Zhang 12/12 TMT4240 S Microstruc. and Prop. of Mat. (7.5) J. K. Solberg 16/17 TMT4245 S Functional Materials (7.5) K.O. Kongshaug 14/15 TMT4250 S Elect.chem.., basis cour. (7.5) G. M. Haarberg 29/31 TMT4260 S Phase Trans. in Metals (7.5) K. Marthinsen 6/7 TMT4265 S Mater.Techn.-Form. Light Met. (7.5) H. J. Roven, O. Jensrud, O. Reiso 11/11 TMT4270 S Refin. and Recycl. of Met., Adv. (7.5) L. Zhang 3/3 TMT4285 S Hydrogen Techn., Fuel/Solar Cells (7.5) S. Sunde 45/47 TMT4290 S Mater. and Surf. Chem. (7.5) H. Karoliussen 37/38 TMT4310 S Electrocat. and Ener. Techn. (7.5) Magnus. S Thomassen 13/16 TMT4315 S Electrochem. Eng., (7.5) K. Nisancioglu 11/12 TMT4851 S Experts in team, (7.5) T. Foosnæs 23/23 TMT4100 A Gen. Chem., (7.5) M. Ystenes 341/387 TMT4115 A Gen. Chem., 1 7.5) T. Foosnæs 82/91 TMT4145 A Ceramic Engin. (7.5) M-A. Einarsrud 17/18 TMT4155 A Heterog. Equilib. 7.5) T. Grande 42/50 TMT4170 A Mater. Techn. 1 (7.5) H. J. Roven, M.Tangstad 29/29 TMT4185 A Mater. Techn. (7.5) J. Hjelen, L.Arnberg 39/43 TMT4190 A Applied Materials Technology (7.5) O. Lohne, K. H. Holthe 22/23 TMT4220 A Mech.Prop. of Eng. Mat. 1 (7.5) E. Nes, N. P. Vedvik 13/20 TMT4255 A Corr. and Corr.Protec. (7.5) B.K. Graver, R. Johnsen 20/25 TMT4280 A Extractive metallurgy (7.5) L. Kolbeinsen 3/3 TMT4292 A Mater. and Surface Chem. (7.5) S. Sunde, K. Wiik 21/25 TMT4295 A Electro. Proc. (7.5) G. M. Haarberg 25/28 TMT4300 A Light and Electr. Micro. (7.5) J. K. Solberg, J. Hjelen 25/26 TMT4305 A Electrometallurgy (7.5) M. Tangstad, H. Tveit 4/4 TMT4320 A Nanomaterials (7.5) A. Fossdal, K.Kleveland, F. Vullum 5/5 TMT4325 A Refin. and Recycl. of Met. (7.5) L. Zhang 12/12 TMT4725 A Materials Techn., special. (22.5) K.Wiik, T. Foosnæs, H.J. Roven, S. Sunde, R. Johnsen 36/36 TMT5730 A Proc. Metal. and Elect., Spec. (22.5) T. Østvold, T. Foosnæs 9/9 MT8100 A-05/S-06 Transport Phenomena (12.0) K. Nisancioglu 8/8 MT8200 S Advanced Chemical Metallurgy (7.5) L.Kolbeinsen 1/1 MT8206 S Iron and Steel Metallurgy (7.5) Ø. Grong 3/3 MT8207 S Electron Microscopy (7.5) J. K. Solberg 6/6 MT8209 S Failure Analysis of Metals (7.5) J. K. Solberg 2/2 MT8214 S Advanced Silicon –Solar Cells (7.5) O. Lohne, T. Worren 4/4 MT8216 S Recrystallization and Texture (7.5) E. Nes 3/3 MT8305 S Cement Semestry (7.5) H. Justnes 1/1 MT8306 S Advanced Ceramics Processing (7.5) M.-A. Einarsrud 1/1 MT8308 S Advanced Solid State Chemistry S. Julsrud 6/6 MT8205 A Metallurgical Modelling of Welding (7.5) Ø. Grong 1/1 MT8210 A Advanced Solidification Metallurgy (7.5) L. Arnberg 4/4 MT8213 A Modelling and Simulation of Materials (7.5) K. Marthinsen 1/1 MT8217 A Kinetics of Metallurgical Reactions (7.5) L. Kolbeinsen 2/2 MT8307 A Thermodynamics of Materials (7.5) T. Grande 5/5

46 M.Sc. STUDENTS

Master of Science in Materials Technology Skjevrak, Sveinung (5 years) Sørgjerd, Arve Julian Van Vo, Thang 3rd year Westermann, Ida Alknes, Patrick Wiig, Kenneh Brynjulfsen, Ingvild Wåsjø, Johanna Egholm, Andreas Østrem, Øyvind Hals, Terje Helsem, Morten Ro Graduated Master of Technology students - spring semester Jahren, Katja Ekroll Boberg, Linn Kamlow, Fenar Frydenberg, Tone Kløgetvedt, Kristoffer Hals, Stine Lohne, Ørjan Fossmark Jahren, Hans Martin Moen, Christoffer Vikne Ljones, Nina Nilsen, Rune Løken, Sondre Nordby, Trygve Ottemo Mikalsen, Christian Odd, Thomas Owe, Lars-Erik Ringstad, Richard Hagvåg Pedersen, Anne Marthe Rosario, Boots Christoffer Demez Rannestad, Øyvind Gustav Rønning, Yngve Rese, Henrik Schrøder, Erling Gjestvang Reinskou, Beate Sivaneesan, Vaseeharan Wangensteen, Torgeir Snilsberg, Knut Erik Yttervik, Stian Hatling Sørensen, Marte Aadland Aaserud, Siw-Christin

4th year Master of Science in Chemistry and Biotechnology, Andersen, Elin Christine Specialization in Materials Chemistry and Energy Brinchmann, Kristoffer Cao, Thien Thanh Nguyen Technology Engebretsen, Torbjørn 3rd year Hagen, Hans Ove Tinnan Andersen, Hanne Flåten Helland, Tore Bakken, Astrid Johansen, Tor Berg, Marianne Elisabeth Nordnes, Elise Tverberg Bergum, Kristin Rønningen, Dag Eikevik, Tine Slevolden, Elisabeth Ervik, Torunn Kringlen Stangeland, Helga Wiig Foss, Carl Eik Lie Strømstad, Stian Haga, Silje Aamot Syvertsen, Guttorm Ernst Haugen, Astri Bjørnetun Søfferud, Mario Kokolakis Ramstad, Caroline Vingsand, Håvard Sletnes, Malin Sunde, Tor Olav Løveng 5th year Tandberg, Paul Bragelien Binai-Faal, Navid Tjelta, Morten Festervoll, Knut Voldsund, Mari Grøtte, Andreas Øygarden, Vegar Hermstad, Ole Andrers Hilden, Erik 4th year Haaland, Bjørnar Øvrum Bjørnstad, Maren Karlsen, Rolf Magne Brandtzæg, Aleksander R. M. Kjøsnes, Rune Christian Dahlstrøm, Per Kristian Krog, Kaja Falstad, Merethe Lerstad, Dag Ola Fredriksen, Asle Lillevik, Håkon Halvorsen, Magnus Torleif Rune Printzell Nguyen, Hue Thai Holme, Caroline Nygård, Ane Nærland, Kristine Uberg Nygård, Ida Onsrud, Morten Andreas Opdahl, Christian Pedersen, Øystein Edland Rotan, Magnus Ramdal, Ingunn Sandbu, Paal Henrik Skjeldestad, Aslak Seim, Stian Svanberg, Ida Sjølie, Stian

47 M.Sc. Students

Wollan, Camilla Skotnes Foreign guest students at Department of Material Ystad, Michelle Cecilia Scince and Engineering Østby, Heidi Therese Bachmaier, Andrea (Austria) 5th year Casimiro Ramòn, Maria (Spain) Asbjørnsen, Ingvild Choo, Jun Quan (Singapore) Bjørnsdotter, Marte Dallera, Andrea (Italy) Dahl, Ole Andreas Drzystek, Piotr (Poland) Hope, Vigdis Hjertaker Dupont, Tiphaine (France) Hognes, Erik Skontorp Eidenberger, Norbert (Austria) Iglebekk, Eivind Garcia Coque, Alejandro (Spain) Kjos, Sigmund Guiton, Mèlaine (France) Mo, Torun Stub Hederström, Ida (Sweden) Slåtten, Sølvi Heinze, Christoph (Germany) Stabell, Tone Hansen Hornscheidt, Julia (Germany) Syre, Marie Vardenær Höpfner, Veronika (Germany) Tennøe, Andreas Ival, Emmanuel Jean Michel (France) Øyen, Anne Jamarillo Gajardo, Carla Jocelyn (Chile) Jeskanen, Ilkka (Finland) Keyzer, Steven (Belgium) Master of Technology in Materials Technology Lecarme, Liza (Fance) (2 years) Lee, Hwa Su (South Corea) Lee, Myoung-Jae (South Corea) (Master Programme in Materials Technology for Engineers) Leroy, Delphine (France) Lin, Yi (China) Nordtømme, Siv Malm Mauget, Florent (France) Michud, Claire (France) Graduated Master of Technology students - spring semester Nessmann, Martin (Austria) Helgetun, Brynjar Hoff Nitsche, Fabian (Germany) Karlsen, Linda Pelisset, Segolene (France) Nijs, Oscar Cornelis Johanna Porte, Jessica (France) Solem, Ola Regnier, Baptiste (France) Reinhold, Anne (Germany) Rueda Verano, Maria Jesus (Spain) Master of Science Program in Light Metals Slizovskiy, Dmitriy (Russia) Production Sørensen, Kari Bjerke (Danmark) Tokoro, Maiko (Japan) 1st year Tonolli, Andrea (Italy) Agyei-Tuffour, Benjamin (Ghana) Tschöpe, Kati (Germany) Aregawi, Wondowsen Abebe (Ethiopia) Vaganov, Danil Valerevich (Russia) Fladerer, Jens (Germany) Senanu, Samuel (Ghana) Tan, Chunming (China) Twum, Eric Barimah (Ghana) Yanney, Michael (Ghana)

2nd year Gelaw, Tilahun Kidanemariam (Ethiopia) Bensah, Yaw Delali (Ghana) Damoah, Lucas Nana Wiredu (Ghana) Adegboyega, Nathaniel Femi (Ghana) Balaba, Ronald Sempagama (Uganda) Gaertner, Heiko (Germany) Einarsson, Sigurdur Agust (Iceland) Wang, Zhaohui (China)

48 GRADUATED M.Sc. STUDENTS WITH TITLES OF THEIR DIPLOMA WORKS

PHYSICAL METALLRUGY Name and title Supervisor Examiner

Hals, Stine Effect of vacuum in mechanical properties Professor Otto Lohne. Dr.ing Haavard Gjestland, and microstructures of HPDC Al-Si alloys. Norsk Hydro, Porsgrunn.

Helgetun, Brynjar Hoff Welding methods and properties for cracker Professor Einar Halmøy. Examined at the Department of tubing of ODS materials. Engineering Design and Materials.

Karlsen, Linda Heat treatment, characterization and SSRT Professor Jan Ketil Solberg. Siv.ing. Bjørn Borchgrevink, Oslo. testing of supermartensitic weldments.

Løken, Sondre Hydrogen storage in an Mg-Mm-Ni alloy. Professor Jan Ketil Solberg. Dr.ing. Børre Tore Børresen, Statoil, Trondheim. Mikalsen, Christian Formalability of ultra fine grained aluminium alloys. Professor Hans Jørgen Roven. Dr.ing. Trond Furu, Norsk Hydro, Sunndalsøra. Nijs, Oscar Cornelis Johanna Work hardening of solid solution and grain- Professor Erik Aasmund Nes. Dr.ing. Trond Furu, Norsk Hydro, boundary strengthened Al-alloys. Sunndalsøra.

Reinskou, Beate Characterization of silicon solar cells. Professor Otto Lohne. Dr.ing. Ketill O. Pedersen, SINTEF, Trondheim. Rese, Henrik The seawater system on the Draugen platform Professor Roy Johnsen. Dr.ing. Sarbjyot Haarberg, - how to secure technical integrity until year 2030. SINTEF, Trondheim.

Solem, Ola Welding methods and properties for cracker Professor Einar Halmøy. Examined at the Department of tubing of ODS materials. Engineering Design and Materials.

INORGANIC CHEMISTRY Name and title Supervisor Examiner

Yttervik, Stian Hatling

Hot pressing of TiB2-ceramics. Professor Tor Grande. Dr.ing. Eirik Hagen, Norsk Hydro, Porsgrunn. Aaserud, Siw-Christin Syntheses of monodisperse nanocrystals. Professor Mari-Ann Einarsrud. Dr.ing. Anita Fossdal, SINTEF, Trondheim.

ELECTROCHEMISTRY Name and title Supervisor Examiner

Boberg, Linn Hydrogen permeation in steel. Professor Kemal Nisancioglu. Dr.ing. Astrid Bjørgum, SINTEF, Trondheim. Frydenberg, Tone Degradation of organic coatings on steel construc- Professor Kemal Nisancioglu. Siv.ing. Olav Gautefall, Trondheim. tions exposed in marine atmosphere – chemically active pigments and mechanisms.

49 GRADUATED M.Sc. STUDENTS WITH TITLES OF THEIR DIPLOMA WORKS

Iglebekk, Eivind The influence of manganese on electrowinning Professor Geir Martin Haarberg. To be examined in 2007. of nickel from chloridesolutions.

Jahren, Hans Martin Inert anodes for oxygen evolution during metal Professor Geir Martin Haarberg. Professor Douglas Inman, deposition by the FFC Cambridge process. Imperial College London, United Kingdom. Ljones, Nina Grainy appearance on anodised profiles. Professor Kemal Nisancioglu. Dr.ing. Håkon Leth-Olsen, Norsk Hydro, Porsgrun Owe, Lars-Erik Oxide electrocatalyst for the oxygen evolution Professor Svein Sunde. Dr.ing. Egil Rasten, Norsk Hydros reaction in water electrolysis. Forskningssenter, Porsgrunn.

Pedersen, Anne Marthe Hydrogen exchange and diffusion in stainless steel Professor Kemal Nisancioglu. Dr. ing. Otto Lunder, under cathodic protection. SINTEF, Trondheim.

Rannestad, Øyvind Gustav Hydrogen evolution, calcareous scale deposition Professor Kemal Nisancioglu. Dr.ing. Hjalmar Sigurdsson, and current requirement during cathodic protection Norges forskningsråd, Oslo. of steel in seawater.

Slåtten, Sølvi

CO2 korrosjon av karbonstål ved lav temperatur. Professor Kemal Nisancioglu. To be examined in 2007.

MASTER OF SCIENCE PROGRAMME IN LIGHT METALS PRODUCTION Name and title Supervisor Examiner

Adjaye-Mensah, Edward Solubility of alumina in fluoride melts for Professor Geir Martin Haarberg. Dr.ing. Sverre Rolseth, brazing of aluminium. SINTEF, Trondheim.

Akhtar, Shahid Effect of nano dispersant additions to lab scale Professor Trygve Foosnæs. Dr.ing. Arne Petter Ratvik, electrodes for aluminium electrolysis. SINTEF, Trondheim.

Boateng, Abraham The role of barium sulphate as anti-wetting agent Associate professor Kjell Wiik. Dr.ing. Bjarte Øye, in aluminasilicate refractory castables. SINTEF, Trondheim.

Hussain, Tajammul

TiB2 inert cathodes for aluminium electrolysis. Professor Tor Grande. Dr.ing. Eirik Hagen, Norsk Hydro, Porsgrunn Tettey, Anita Naa Nyerley A new method to characterise the strength of petrol Professor Trygve Foosnæs. Dr.ing. Arne Petter Ratvik, coke grains. SINTEF, Trondheim.

GRADUATED M.Sc. STUDENTS WITH TITLES OF THEIR DIPLOMA WORKS

50 EXTRACURRICULAR ACTIVITIES,

Honours, Participation in Courses, Conferences, Lectures and Study Visits

Lars Arnberg Jon Arne Bakken Lars Arnberg is an Affiliate Professor at the Department of Jon Arne Bakken cooperates with the University of Iceland Mechanical Engineering, Worcester Polytechnic Institute, on Industrial Electric Arcs. He is also a Board Member USA. He is representing NTNU on the Board of SINTEF of Elkems Forskningsfond. He is a collaborator on three Materials and Chemistry and is the leader of the Strategic SINTEF projects: “PPM”, “Conductivity of Coke” and “FoXy”. university program Light Metals Technology. Elkem Icelandic Alloys, Iceland, October 30-31, 2006. Lecturing Institut für Maschinenbau, TU Bergakademie, Freiberg, external course: ”Kretsanalyse for elektriske smelteovner”. Germany, January 8 - April 8, 2006. Visiting Professor. Elkem Seminar, Trondheim, Norway, November 28, 2006. Meeting on EU proposal NADIA, Padova, Italy, January 11-12, Lecturing external course: ”Elektro-lysbuer”. 2006. Ph.D.-Seminar, Crete, Greece, June 8-15, 2006. Meeting on EU-project METRO, Bilbao, Spain, January 19-20, 2006. Norwegian Metallurgical Society Summer Meeting, Oslo, Norway, May 4-5, 2006. AC-Tech, Freiberg, Germany, March 15, 2006. Study visit. Compendium “Electric melting furnaces – circuit analyses” Georg Fischer Foundry, Leipzig, Germany, March 16, 2006. written for CVRD, Brazil. Study visit. Stein Trygve Briskeby Deutsche Solar, Freiberg, Germany, March 17, 2006. Study visit. 3rd National FUNMAT Meeting, Trondheim, Norway, January 5- 6, 2006. Lecture on: “Carbon nanofibre supported Pt catalysts University of Clausthal, Germany, March 20-21, 2006. for high temperature polymer electrolyte fuel cells”. Lecture on: “Imaging of alloy solidification by synchrotron X- radiation”. Nordic Hydrogen Seminar 2006, Oslo, Norway, February 6-8, 2006. Lecture on: “Nanostructured electrocatalysts for PBI Meeting on ESA project MONOPHAS, Braunschweig, fuel cell”. Germany, April 3-4, 2006. 12th Nordic Symposium on Catalysis, Trondheim, Norway, SINTEF award for outstanding research, shared with May 28-30, 2006. Lecture on: “Development of nanostructured Dr. Ragnvald Mathiesen (SINTEF), April 19, 2006. Pt-based electrocatalyst for high temperature polymer electrolyte fuel cells”. EU-project NADIA, Vicenza, Italy, May 10-11, 2006. Kick-off Meeting. 57th Annual Meeting of the International Society of Electrochemistry, Edinburgh, Scotland, August 27 - September Worcester Polytechnic Institute, USA, May 18-26, 2006. Visit. 1, 2006. Poster on: “PBI fuel cell catalysts prepared by colloidal routes”. Meeting EU-project METRO, Jönköping, Sweden, June 29-30, 2006. 5th International Conference on Electrocatalysis (ECS’06), Montenegro, September 10-14, 2006. Poster on: “Synthesis 8th International Summer School of Aluminium Alloy and characterization of CNF – supported catalysts for high Technology; Casting and Solidification of Aluminium and temperature polymer electrolyte fuel cells”. Magnesium Alloys, Trondheim, Norway, August 21-25, 2006. Marisa Di Sabatino 21st European Photovoltaic Solar Energy Conference, Dr. Di Sabatino started her Post Doctoral at the Department of Dresden, Germany, September 4-8, 2006. Materials Science and Engineering in January 2006.

3rd International Conference on High Tech Die Casting, FoXy Kick-off Meeting, Trondheim, Norway, January 26-27, Vicenza, Italy, September 21-22, 2006. 2006.

McMaster’s University, Canada, October 6, 2006. Lecture on: 6M FoXy Meeting at ECN, Petten, The Netherlands, “Dendrite fragmentation in aluminium alloys”. June 21-22, 2006.

NorLight Conference, Oslo, Norway, October 17-18, 2006. ECN, Petten, The Netherlands, June 19-21, 2006. Study visit.

European Synchrotron Radiation Facility, Grenoble, France, 8th International Summer School of Aluminium Alloy November 1-3, 2006. Technology; Casting and Solidification of Aluminium and Magnesium Alloys, Trondheim, Norway, August 21-25, 2006. Royal Institute of Technology, Stockholm, Sweden, December 15, 2006. Opponent at doctoral dissertation. 21st European Photovoltatic Solar Energy Conference,

51 Extracurricular Activities

Dresden, Germany, September 4-8, 2006. Invited presentation of EiT project: “New aluminium plant at Byneset in Trondheim”. Opening Seminar, Gemini Centre, PV Solar Cell Materials, Trondheim, Norway, September 11, 2006. Researchers’ Night, NTNU, Trondheim, Norway, September 22, 2006. Co-organizer and demonstration lecture. 3rd International Conference on High Tech Die Casting, Vicenza, Italy, September 21-22, 2006. Opening Seminar, Chemistry Building II, Trondheim, Norway, October 13, 2006. Seminar, UNIMIB, Milan, Italy, October 10-12, 2006. IMPEC AS, Trondheim, Norway, October 23, 2006. Strategy NorLight Conference, Oslo, Norway, October 17-18, 2006. and business planning.

European Synchrotron Radiation Facility, Grenoble, France, Orklamessa, Meldal Community College, Løkken Verk, November 1-7, 2006. Norway, October 24, 2006. Three demonstration lectures.

SILOBO Meeting, Elkem Solar, Kristiansand, Norway, Hydro Aluminium, BIP HCD, Sundvolden Hotell, Hole, Norway, November 21, 2006. November 21-22, 2006. Lecture on: “Primary aluminium at NTNU and SINTEF 1991-2006”. Research Award, Aldo Daccò Award from the Italian Association of Metallurgy (AIM), Italy, November 22, 2006. Research Council of Norway, Oslo, Norway, November 23, 2006. Lecture on: “Researchers’ Night og Forskningstorget i 12M FoXy Meeting, UNIMIB, Milan, Italy, December 13-15, 2006. Trondheim 2006”.

Arne Espelund Tor Grande Trøndelag folkemuseum, Trondheim, Norway, October 2, Tor Grande is the head of the Department of Materials 2006. Lecture on: “Iron from the outfields during 2000 years”. Science and Engineering and he is a board member of NTNU Nanolab. He is currently NTNUs representative in the steering 10th Nordic Bronze Age Symposium, Trondheim, Norway, committee in the research consortium FUNMAT between October 5-8, 2006. Lecture on: “Parallell features for the NTNU, UiO, SINTEF and IFE. extraction of copper and iron?”. FUNMAT scientific advisory committee and steering committee The Country and the Iron, Örebro, Sweden, November 11, 2006. meetings, Oslo and Trondheim, Norway, January 4, February 16, March 13, May 8 and November 27-28, 2006. Cooperation with the County of Oppland on experimental ironmaking, , Norway. Board Meeting,NTNU Nanolab, Trondheim, Norway, March 31, October 19, 2006. Ancient Metallurgical Experiments, Eindhoven, The Netherlands, September 13.-19, 2006. Lecture on: “Bloomery 3rd National FUNMAT Meeting, Trondheim, Norway, January ironmaking as seen from Norway”. 5-6, 2006. Lecture on: “Mechanical properties of perovskite materials”. Gauldal secondary school, Norway, all year. Project work with teachers and students in chemistry. Leader Seminar NTNU, Røros Norway, January 22-24, 2006.

Trygve Foosnæs Hydro Research Center, Porsgrunn, Norway, March 7, 2006. Hydro Aluminium, Sunndalsøra, Norway, February 22, 2006. Visit. Excursion with participants in Experts in Team. Seminar NTNU Nanolab, Jægtvolden Fjordhotell, Inderøy, 135th TMS Annual Meeting, San Antonio, USA, March 12-16, Norway, March 9-10, 2006. 2006. Chairman anode baking session. 4th Topical THIOX Meeting, Jægtvolden Fjordhotell, Inderøy, Miljøarbeid og Prosessindustri, “Hund og katt” eller “som Norway, March 20-21, 2006. Hånd i hanske”, Trondheim, Norway, March 22, 2006. Lecture on: ”Aluminium primærproduksjon og miljø”. Milan, Italy, April 3-11, 2006. Student excursion with master students from Chemistry and Biotechnology. In-situ Analytics ApS, Hørsholm, Denmark, May 3-6, 2006. Project work. DIFFRAC plus and TOPAS course, Villamartin, Spain, April 22- 29, 2006. Hydro Aluminium, Årdal, Norway, July 4-6, 2006. Invited presentation of EiT project: “New aluminium plant at Byneset ePhorte course, Trondheim, Norway, May 3, 2006. in Trondheim”. NANOMAT Seminar on ”Nanoteknologi - nye muligheter IMPEC AS, Årdal, Norway, July 5, 2006. Project meeting and for norsk industri”, Oslo, Norway, June 8, 2006. Lecture on: research discussions. ”Nanopartikler - muligheter innen nanoteknologi”.

In-situ Analytics ApS, Hørsholm, Denmark, August 7-10, 2006. Seminar on ”Nasjonal strategi for nanovitenskap og Project work and research discussions. nanoteknologi”, Oslo, Norway, June 9, 2006.

Hydro Aluminium, Sunndalsøra, Norway, September 1, 2006.

52 Extracurricular Activities

Seminar on the Strategic Area MATERIALS at NTNU, Stjørdal, Jarle Hjelen Norway, June 13-14, 2006. Seminar, University of Stavanger, Norway, May 3, 2006. Lecture on: “Elektronmikrodiffraksjon i SEM (EBSD)- Department Seminar, Brekstad, Norway, June 15-16, 2006. muligheter og anvendelser”. Lecture on: “Instituttlederen har ordet”. IMC16 , Japan, September 3-8, 2006. Lecture on: 9th International Conference on Inorganic Membranes, ”SEM in-situ thermo-mechanical deformation studies using Lillehammer, Norway, June 25-29, 2006. Lecture on: EBSD”. Poster presentation: “In-situ SEM/EBSD investigations “Mechanical stability of oxygen permeable membranes”. of grain rotations in an Al-Mg-Si alloy during deformation”.

Opening Seminar, NTNU Nanomekanisk laboratorium, Department of Materials Science and Engineering, Trondheim, Trondheim, Norway, August 29, 2006. Norway. Administrated the purchase of a low vacuum field emission scanning electron microscope (LVFESEM). The 2nd KIFEE Symposium, Trondheim, Norway, 7-8 September, equipment was installed in May. 2006. Lecture on: “Oxide materials for solid oxide fuel cells and gas separation membranes”. Bjørn Holmedal McMaster University, Hamilton, Canada, February/March/ Opening Seminar, Gemini Centre, PV Solar Cell Materials, April, 2006. Grant: Leiv Eiriksson mobility program Norway- Trondheim, Norway, September 11, 2006. USA/Canada.

Workshop, Functional Oxide for Energy Technology, Trondheim, Geir Martin Haarberg Norway, October 2, 2006. Bo Håkansson Symposium, KTH, Stockholm, Sweden, January 31, 2006. Lecture on: “Saltsmelteelektrolytter”. Opening Seminar, Chemistry Building II, Trondheim, Norway, October 13, 2006. Lecture on: ”Nyetableringen”. CORUS, ULCOS Meeting, Ijmuiden, The Netherlands, February 21, 2006. Seminar on ”Nyskaping og utvikling av Midt-Norge”, Trondheim, Norway, November 21, 2006. University of Cambridge, United Kingdom, March, 2006. Master student supervision and study visit, one week. Øystein Grong Associated Member of the newly established SFI Centre at 2nd Solar Silicon Conference, Munich, Germany, April 3, 2006. NTNU “Structural Impact Laboratory”. Lecture on: “Solar grade silicon through electrolysis”.

8th International Conference on Numerical Analysis of ULCOS Meeting, Paris, France, May 11, 2006 Weldability, Graz, Austria, September 25-27, 2006. Invited Key Note Paper: “A multiscale modelling approach to the DEANEW Meeting, KTH, Stockholm, Sweden, May 15, 2006. optimisation of welding conditions and heat treatment schedules for age hardening aluminium alloys”. Kyoto and Tokyo, Japan, June – July, 2006. Workshop and study visit, one week. Harald Görner TMS Light Metals Conference, San Antonio, USA, March 12-16, Molten Salts Discussion Group, Cambridge, United Kingdom,

2006. Lecture on: “Kinetics of an AlF aluminium filter“. July 10-11, 2006. Lecture on: “Solar grade silicon by electrorefining in molten salts”. Norwegian Metallurgical Society Summer Meeting, Oslo,

Norway, May 4-5, 2006. Lecture on: “Kinetics of an AlF3 University of Cambridge, United Kingdom, July, 2006. Master aluminium filter“. student supervision and study visit, two weeks.

NorLight Conference, Oslo, Norway, October 18, 2006. 57th Annual Meeting of the International Society of

Lecture on: “Development of an AlF3 active filter for aluminium Electrochemistry, Edinburgh, Scotland, August 27 - September melts - summary”. 1, 2006. Lecture on: “Electrodeposition of iron from molten salts”. Jana Hajasova Doshisha University, Kyotanabe, Japan, March 31 - June 29, University of Newcastle, United Kingdom, September 2-3, 2006. Study visit. 2006. Study visit.

2nd KIFEE Symposium, Trondheim, Norway, September 6-8, 2nd KIFEE Symposium, Trondheim, Norway, September 6-8, 2006. Lecture on: “Materials and processes for environment 2006. Organizing and presentations. and energy”. EUCHEM Conference on Molten Salts and Ionic Liquids, POLEN 2006 Seminar, Trondheim, Norway, October 17, 2006. Hammamet, Tunisia, September 17-22, 2006. Lecture on: Lecture on: “Electrochemical behaviour of sulphur containing “Production of iron by electrolysis in molten salts”. species in molten salts”. KTH, Stockholm, Sweden, November 27-28, 2006. DEANEW 210th Meeting of the Electrochemical Society, Cancun, Mexico, and opponent at doctor’s defence. October 29 - November 3, 2006. Poster on: “Electrochemical behaviour of sulphur species in molten chlorides”. 210th Meeting of the Electrochemical Society, Cancun, Mexico, October 29 - November 3, 2006. Lecture on: “Electrodeposition of iron from molten mixed chloride/fluorideelectrolytes”.

53 Extracurricular Activities

Northeastern University, Shenyang, China, November, 2006. 2006. Lecture on: “Novel carbon materials”. Study visit and two presentations. CarboMat Meeting, NTNU, Trondheim, Norway, March 7, 2006. 16th Iketani Conference, Masuko Symposium, Tokyo, Japan, Lecture on: “Novel carbon materials”. November 13-15, 2006. Lecture on: “Sustainable electrolysis for electrowinning of iron and electrorefining of silicon”. Steering Committee Meeting, Elkem ASA Carbon, Kristiansand, Norway, May 2, 2006. Lecture on: “Novel carbon materials in ECHEM, Wiener Neustadt, Austria, December 4, 2006. Study electrometallurgical applications”. visit and presentation. NKS Seminar, Anvendelse av molekylærspektroskopi i Molten Salts Discussion Group, London, United Kingdom, forskning og industri, Oslo, Norway, May 4, 2006. December 18, 2006. Lecture on: “Electrochemistry in pure molten lead chloride”. Norwegian Metallurgical Society Summer Meeting, Oslo, Norway, May 5, 2006. Lecture on: “Properties of carbon Ole Edvard Kongstein electrodes by carbon nanofiber addition”. 5th International Conference on Electrocatalysis (ECS’06), Montenegro, September 10-14, 2006. Poster on: “Synthesis Elkem ASA Carbon, Kristiansand, Norway, July 10-14, 2006. and characterization of CNF – supported catalysts for high Study visit and experimental work. temperature polymer electrolyte fuel cells”. Opening Seminar, NTNU Nanomekanisk laboratorium, Rannveig Kvande Trondheim, Norway, August 29, 2006. Vesuvius, Feignies, France, March 20-21, 2006. Study visit. Lecture on: “Effect of crucible purity on multicrystalline National Centre of Raman Spectroscopy, University of Oslo, silicon quality”. Norway, August 30 - September 1, 2006. Study visit and experimental work. Hands-on Workshop on Silicon Solar Cells, IFE, Kjeller, Norway, April 3-7, 2006. CarboMat Seminar, NTNU, Trondheim, Norway, November 15- 16, 2006. Poster on: “Carbon nanofiber additions in electrode 21st European Photovoltaic Solar Energy Conference, binder matrixes”. Dresden, Germany, September 4-8, 2006. Poster session: “Effect of crucible purity and interface characteristics on Internal Board Meeting, Elkem Carbon AS, Oslo, Norway, multicrystalline silicon ingot quality”. December 14, 2006. Invited presenter.

Project Meeting, IFE, Kjeller, Norway, December 19, 2006. Tore Larsen Lecture on: “Impurities in multicrystalline silicon”. 8th International Symposium on Oilfield Scale, Aberdeen, United Kingdom, May 31 - June 1, 2006. Lecture on: “Quasi Magnus Hurlen Larsen natural consolidation of poorly consolidated oil field Aluminium Surface Science and Technology, Beaune, France, reservoirs”. May 14-18, 2006. Lecture on: “Grain boundary microstructure and intergranular corrosion of AlMgSi(Cu) model alloys”. Hilde Lea Lein 3rd National FUNMAT Meeting, Trondheim, Norway, January 10th International Conference on Aluminum Alloys (ICAA), 6, 2006. Lecture on: “Aqueous tape casting”. Vancouver, Canada, July 9-13, 2006. Lecture on: “Significance of low copper content on grain boundary nanostructure and International Conference on Inorganic Membranes (ICIM9), intergranular corrosion of AlMgSi(Cu) model alloys”. Lillehammer, Norway, June 25-29, 2006. Lecture on: “Asymmetric proton conducting oxide membranes prepared Gordon Research Conference on Aqueous Corrosion, by aqueous tape casting”. Colby-Sawyer College, USA, July 16-21, 2006. Poster on: “Intergranular corrosion and grain boundary composition in 2nd KIFEE Symposium, Trondheim, Norway, September 6-8, 6000-series model alloys with low Cu-content”. 2006.

57th Annual Meeting of the International Society of FOET workshop, Trondheim, Norway, October 2, 2006. Electrochemistry, Edinburgh, Scotland, August 27 - September Lecture on: “Asymmetric membranes and fuel cells prepared 1, 2006. Lecture on: “Intergranular corrosion of AlMgSi(Cu) by aqueous tape casting”. model alloys”. Tor Lindstad International Workshop on Future Perspectives of Corrosion Lead Author writing section about ferroalloy production Research, Ringberg Castle, Tegernesee, Germany, December in “2006 IPCC Guidelines for National Greenhouse Gas 13-16, 2006. Inventories, Volume 3 Industrial Processes and Product Use”, UNEP-WMO. (United Nations Environment Programme - Researchers’ Night, NTNU, Trondheim, Norway, September World Meteorological Organization). Reviewer for “2006 IPCC 22, 2006. Lecture on: “History, chemistry and principles”. Guidelines for National Greenhouse Gas Inventories”, UNEP- WMO. Forskningstorget, Trondheim, Norway, 2006. Lecture on: “History, chemistry and principles”. Knut Marthinsen Knut Marthinsen is deputy head at the Department of Materials Sten Yngve Larsen Science and Engineering. He is member of the International Internal CarboMat Seminar, Trondheim, Norway, February 16, Committee for the Joint International Conferences on

54 Extracurricular Activities

Recrystallization and Grain Growth, and is also chairman FOET workshop, NTNU, Trondheim, Norway, October 2, 2006. of the Steering Committee for the NorLight project “Heat Lecture on: “Current status on spray pyrolysis”. Treatment Fundamentals”. Kemal Nisancioglu Department of Materials Science and Engineering, McMaster Laboratory for Industrial Energy Systems (LENI), STI, Ecole University, Hamilton, Canada, June 26 – July 3, 2006. Lecture Polytechnique Fédérale de Lausanne (EPFL), January 12, on: “Precipitation behaviour and recrystallisation resistance 2006. Continuing collaboration on oxygen transport and in Al-alloys with additions of Zr, Sc and Hf”. exchange in solid oxide membranes.

Thermec’2006, International Conference on Manufacturing Various meetings, NorLight Program, Light Metal Surface of Advanced Materials, Vancouver, Canada, July 4 - 8, 2006. Science Research Project: Topics coordinator and Session Chairman for the Aluminium - Resource Group meetings: January 20 (Holmestrand) Alloys session. Invited keynote, lecture on: “Development of and April 21, 2006. aluminium alloys with ultimate recrystallisation resistance”. - Technical meetings and seminars: March 15, May 31 and October 21, 2006. International Conference on Aluminium Alloys (ICAA10), Vancouver, Canada, July 9-13, 2006. Member of the poster Meetings of Working Group on Surface Science and Corrosion prize nomination committee. Poster on: “Deformation of European Aluminium Technology Platform, Brussels, and recrystallization behaviour of a homogenized and a Belgium, March 2 and August 18, 2006. heterogenized Al-Mg-Si alloy”. International Conference on Aluminium Surface Science Fundamentals of Deformation and Annealing Symposium and Technology, Beaune, France, May 14-18, 2006. Member, (Prof. F. J. H. Humphrey’s retirement symposium), University International Scientific Committee. Keynote lecture: “Activation of Manchester, United Kingdom, September 5-7, 2006. of aluminium alloys by low melting point trace elements”. Co-author of other presentations entitled: “Interface studies Lettmetall 2006, NorLight End Seminar, Grand Hotel, Oslo, relevant to corrosion processes in aluminium alloys”, “Grain Norway, October 2, 2006. Poster on: “Overview of NorLight boundary microstructure and intergranular corrosion of heat treatment fundamentals (HTF)”. AlMgSi(Cu) model alloys”, “Compatibility of chromium free conversion and organic coatings on 6000 series aluminium Department of Metal Physics and Metallurgy, RWTH Aachen, alloys”, “In situ ellipsometric and electrochemical monitoring Germany, October 13, 2006. Discussion meeting re possible of oxide formed on aluminium in acetate buffer” and new European collaborative research projects. Lecture on: “Electrochemical activation of aluminium by trace elements “SFF proposal OptiMa and relevant research interests at indium and tin”. DMSE, NTNU”. SAPA Technology, Finspång, Sweden, May 29, 2006. Lecture Kick-off Meeting, RCN BIA project “Nucelation control on: “Effect of small copper content and heat treatment on for optimized properties”, Department of Physics, NTNU, intergranular corrosion of an AA6000-series model alloy”. Trondheim, Norway, October 31 – November 1, 2006. Member of the steering committee. International Conference on Aluminium Alloys (ICAA10), Vancouver, Canada, July 9-13, 2006. Co-author of papers SAPA Technology, Finspång, Sweden, November 16-17, 2006. entitled: “Fracture mechanical testing of adhesion of organic Visit and presentation of relevant project activities at NTNU coatings on aluminium”, “Significance of low copper content and status on possible new European collaborative research on grain boundary nanostructure and intergranular corrosion projects. of AlMgSi(Cu) model alloys”, “Surface segregation of indium by heat treatment of aluminium” and “Properties of oxide Department of Physics, NTNU, Trondheim, Norway, formed on aluminium in aqueous acetate buffer”. November 24, 2006. Member of the adjudication committee and administrator for Siv.ing.’s Håkon Hasting Stokka’s Ph.D. Gordon Research Conference on Aqueous Corrosion, New defence. London, New Hampshire, USA, July 16-21, 2006. Lecture on: “Activation of aluminum by segregation of low melting point NorLight Heat Treatment Fundamentals (HTF) Seminar, trace elements”. Bårdshaug, Orkanger, Norway, December 7-8, 2006. Lecture on: “HTF summary - status with respect to original plans and Sabbatical leave, August 15, 2006 - August 15, 2007. ambitions”. Department of Materials Science and Engineering, Istanbul Technical University (ITU), Turkey, September 9 - October 2, Referee for Acta Materialia, Acta Crystallographica, Physica 2006. Visiting Professor. Scripta, Materials Letters, Materials Science and Engineering, Modelling and Simulation in Materials Science. Department of Materials Science and Engineering, Istanbul Technical University (ITU), Turkey, September 19, 2006. Lecture Tommy Mokkelbost on: “Corrosion science and engineering of light metals: Past, 3rd National FUNMAT Meeting, Trondheim, Norway, January present and future”.

4-6, 2006. Lecture on: “Sintering and characterization of La1- xSrxNbO4”. Department of Materials Science and Engineering, Istanbul Technical University (ITU), Turkey, October 11, 2006. Lecture 11th International Ceramics Congress, Acireale, Italy, June on: “Correlation of electrochemical behavior, corrosion 4-9, 2006. Lecture on: “Sintering and characterization of morphology and microstructure of aluminum alloys”.

La1-xSrxNbO4”.

55 Extracurricular Activities

Department of Materials Science and Engineering, Istanbul mechanical testing laboratories at the DMSE. Technical University (ITU), Turkey, October 18, 2006. Lecture on: “Chromate-free conversion coatings for aluminum alloys”. Organizing Internal Seminar on “Nanostructuring Metals” with Professor Dave Embury, Trondheim, Norway, February Department of Manufacturing Engineering and Management, 3, 2006. Technical University of Denmark (DTU), Denmark, November 6 - December 12, 2006. Visiting Professor. Helsinki University of Technology, Materials Science, Finland, April 20, 2006. Visit. Seminar on Aluminium Surface Modification, DTU, Lyngby, Denmark, November 8, 2006. Lecture on: “Adhesion of organic Ph.D. defence opponent for dr. Terhi Glas, Tampere University of coatings on modified chrome free surface”. Technology, Finland, April 21, 2006.

210th Meeting of the Electrochemical Society, Cancun, 14th International Conference on Strength of Metals and Alloys Mexico, October 29 - November 3, 2006. Paper entitled: (ICSMA 14), Xian, China, June 4-9, 2006. “Effect of heat treatment on grain boundary nano-structure and corrosion of low copper AlMgSi alloy”. Hydro Magnesium Xi’an Plant, Xian, China, June 7, 2006. Study visit and discussions. 16th Iketani Conference, Electrochemistry and Thermodynamics of Materials Processing for Sustainable Seminar Strategic Area Materials at NTNU, Stjørdal, Norway, Production, Tokyo, Japan, November 13-15, 2006. Lecture on: June 13-14, 2006. “Effect of modified composition and processing on surface nanostructure and electrochemical properties of recycled Department Seminar, Brekstad, Norway, June 15-16, 2006. aluminum alloys”. Lecture on: “Ph.D. education at NTNU and at DMSE”.

111th Conference of Japan Institute of Light Metals, Tokyo, International Conference Ultrafine Grained Materials 2006 Japan, November 18-19, 2006. Lecture on: “Corrosion science - from Basics to Applications (UFG 2006), Kloster Irsee, and engineering of light metals: Past, present and future”. Germany, September 25-27, 2006.

Sverre Olsen POLEN 2006 Seminar, Trondheim, Norway, October 16, 2006. Companhia Vale do Rio Doce (CVRD), Brazil, August 7-11, 2006. Presentation. Visit production plants. NorLight Conference, Oslo, Norway, October 17, 2006. Ouro Preto University, Brazil, August 14-17, 2006. Post graduate course. Lectures on: ”Metallurgy of manganese Hydro Aluminium R&D Centre, Karmøy, Norway, November ferroalloys”. 13, 2006. Guest lecture.

Lead Author writing section about ferroalloy production Dragvoll Forum for Globalisering, Dragvoll, Trondheim, in “2006 IPCC Guidelines for National Greenhouse Gas Norway, November 16, 2006. Lecture on: ”Smakebiter Inventories, Volume 3 Industrial Processes and Product Kinaforskningen ved NTNU - Materialteknologi”. Use”, UNEP-WMO. (United Nations Environment Programme – World Meteorological Organization). NTNU delegation to Shanghai Jiaotong University, Royal Norwegian Consulate in Shanghai and to Chongqing University, Lars-Erik Owe November 26-31, 2006. Seminars and lectures. 210th Meeting of the Electrochemical Society, Cancun, Mexico, October 29 - November 3, 2006. Poster on: “Electrochemical Espen Rudberg studies in pure molten lead chloride.” 3rd National FUNMAT Meeting, Trondheim, Norway, January 4-6, 2006. Lecture on: “Interpretation of oxygen diffusion and Marian Palcut surface exchange data for La1-xSrxCoO3-δ”. Inorganic Group Seminar, Trondheim, Norway, February 27,

2006. Lecture on: “Caution diffusion in LaMnO3 and LaCoO3”. Inorganic Group Seminar, Trondheim, Norway, February 27, 2006. Lecture on: “Electrochemical measurements of oxygen

9th International Conference on Inorganic Membranes, exchange and transport in La0.7Sr0.3CoO3-δ”. Lillehammer, Norway, June 25-29, 2006. Poster on: “Caution

diffusion in LaCoO3”. 9th International Conference on Inorganic Membranes, Lillehammer, Norway, June 25 - 29, 2006. Poster on: ”Oxygen Terkel Rosenqvist exchange and transport in membranes La1-xSrxCoO3-δ”. Sohn International Symposium, San Diego, California, August 27-31, 2006. 57th Annual Meeting of the International Society of Electrochemistry, Edinburgh, Scotland, August 27 - September Hans Jørgen Roven 1, 2006. Poster on: ”Measurement and interpretation of oxygen

Hans Jørgen Roven is Vice-Chair Strategic Area Materials at diffusion and surface exchange data for La1-xSrxCoO3-δ”. NTNU and responsible for Light Materials within the same. He is also Head of the Advisory Board, the national research FOET work shop, NTNU, Trondheim, Norway, October 2,

program ‘NorLight’ on Light Metals. 2006. Lecture on: “Supported dense thin film La0.7Sr0.3CoO3-δ membrane - preparation and oxygen permeation”. Member of the www.nanospd.org promoting international research collaboration on bulk nanostructured materials and Per Martin Rørvik Head of FORMLAB, the forming, new forming technology and 3rd National FUNMAT Meeting, Trondheim, Norway, January

56 Extracurricular Activities

5-6, 2006. Lecture on: “Chemical preparation of ferroelectric Maneesh Srivastava nanorods”. Magnesium Competence Centre, Hydro Aluminium and Research Centre, Porsgrunn, Norway, April 6, 2006. Lecture 2nd KIFEE Symposium, Trondheim, Norway, September 6-8, on: “Improving energy absorption of HPDC Mg alloys”. 2006. Hydro, Sunndalsøra, Norway, May 8, 2006. Lecture on: Frode Seland “Improving energy absorption of HPDC Al-Si alloys”. 3rd National FUNMAT Meeting, Trondheim, Norway, January 5-6, 2006. Lecture on: “Electrochemical oxidation of methanol 8th International Summer School of Aluminium Alloy and formic acid in fuel cell processes”. Technology; Casting and Solidification of Aluminium and Magnesium Alloys, Trondheim, Norway, August 21-25, 2006. Meeting on EU-project FURIM, Trondheim, Norway, April 3-4, 2006. 3rd International Conference on High Tech Die Casting, Vicenza, Italy, September 21-22, 2006. Poster on: “Energy 209th Meeting of The Electrochemical Society, Denver, absorption of HPDC aluminium and magnesium alloys”. Colorado, USA, May 7-12, 2006. Lecture on: “Mechanistic aspects of oxidation of methanol, formic acid and CO on Pt”. NorLight Conference, Oslo, Norway, October 17-18, 2006. Lecture on: “Improving energy absorption of HPDC Al-Si and NREL, Golden, Colorado, USA, May 12, 2006. Visit. Mg alloys”.

One-day Seminar, DMSE, Trondheim, Norway, June 1, 2006. Svein Sunde Visitors from Permascand and KTH. Lecture on: “Hydrogen 3rd National FUNMAT Meeting, Trondheim, Norway, January 5- og biobrensel i brenselceller”. 6, 2006. Lecture on: “Carbon nanofibre supported Pt catalysts for high temperature polymer electrolyte fuel cells”. 10th Ulm ElectroChemical Talks, Ulm, Germany, June 27-28, 2006. Award winning poster, 3rd price: “High-temperature Nordic Hydrogen Seminar 2006, Oslo, Norway, February 6-8, PEM fuel cells based on acid doped PBI membranes”. 2006. Lecture on: “Nanostructured electrocatalysts for PBI fuel cell”. European Synchrotron Radiation Facility, Grenoble, France, September 5-12, 2006. 12th Nordic Symposium on Catalysis, Trondheim, Norway, May 28-30, 2006. Lecture on: “Development of nanostructured NordicPEMfc06, Stockholm, Sweden, September 25-27, 2006. Pt-based electrocatalyst for high temperature polymer Poster presentation: “High-temperature PEM fuel cells based electrolyte fuel cells”. on acid doped PBI membranes”. 57th Annual Meeting of the International Society of Meeting on EU-project FURIM, Gothenburg, Sweden, October Electrochemistry, Edinburgh, Scotland, August 27 - September 11-13, 2006. 1, 2006. Poster on: “PBI fuel cell catalysts prepared by colloidal routes”. Sverre Magnus Selbach 3rd National FUNMAT Meeting, Trondheim, Norway, January 5th International Conference on Electrocatalysis (ECS’06),

5-6, 2006. Lecture on: “Cation non-stoichiometry of PbTiO3”. Montenegro, September 10-14, 2006. Poster on: “Synthesis and characterization of CNF – supported catalysts for high 4th Topical THIOX Meeting, Jægtvolden Fjordhotell, Inderøy, temperature polymer electrolyte fuel cells”. Norway, March 19-21, 2006. Lecture on: “The effect of PbO- deficiency in Pb1-xTiO3-d”. Prsemyslaw Szczygiel 2006 TMS Annual Meeting & Exhibition, San Antonio, USA, Jan Ketil Solberg March 12-16, 2006. Presentation on: “Microstructural Project meeting, Scana Steel Stavanger, Jørpeland, Norway, development of “recycled-like” alloys during ECAP: particle February 21, 2006. break-up, microstructure evolution and mechanical properties”. Administrated the purchase and installation of a field emission gun microprobe analyzer, JEOL JXA-8500F EPMA, installed WEBCAST: Enhancing the Value Proposition Through Metals April 2006. Recycling, Trondheim, Norway, September 28, 2006.

NORSTORE International Seminar on Hydrogen Storage and POLEN 2006 Seminar: Fundamentals, Practice and Modeling Supply Systems, Jyllinge, Denmark, May 30-31, 2006. during Metal Recycling, Refining and Processing, October 16, 2006. Organization and presentation. Project plan meeting, IFE, Kjeller, Norway, August 30, 2006. Merete Tangstad Project meeting, Scana Steel Stavanger, Jørpeland, Norway, Merete Tangstad is Chairman of the Norwegian Metallurgical November 17, 2006. Society, Trondheim, Norway. She is also Deputy Board Member of FFF (The Norwegian Ferroalloy Producers Research Meeting at FMC Technologies (arranged by Idéfondet NTNU), Association). Kongsberg, Norway, November 20, 2006. Miljøarbeid og Prosessindustri, “Hund og katt” eller “som Hånd Nanotechnology Seminar, Kongsberg Industripark, Norway, i hanske”, Trondheim, Norway, March 22, 2006. Administrator November 21, 2006. (60 participants).

57 Extracurricular Activities

Carbonaceous Materials in the Ferromanganese Production, 1, 2006. Poster on: “PBI fuel cell catalysts prepared by colloidal NTNU, Trondheim, Norway, December 8, 2006. Administrator routes”. (20 participants). 5th International Conference on Electrocatalysis (ECS’06), Operator Seminar, Eramet, Sauda, Norway, April 25-26, 2006. Montenegro, September 10-14, 2006. Poster on: “Synthesis Lecturing external course: “Production of ferromanganese and characterization of CNF - supported catalysts for high alloys”. temperature polymer electrolyte fuel cells”.

University of Ouro Preto and CVRD, Brazil, August 4-19, 2006. Reidar Tunold Lecturing external course: “Production of ferromanganese 3rd National FUNMAT Meeting, Trondheim, Norway, January alloys”. 5-6, 2006. Lecture on: “Electrocatalysts for water electrolysis using polymer electrolyte membrane”. Jomar Thonstad TMS Annual Meeting, San Antonio, Texas, USA, March 12-16, Arranged discussion and presentation meeting with Prototech 2006. Lecture on: ”Anode overvoltage on metallic inert anodes (CMI, Bergen), NTNU, Trondheim, Norway, February 9, 2006. in low-melting bath”. Lecture on: “Research activities on energy processes; water electrolysis and fuel cells at electrochemistry group”. Aluminium of Siberia, Krasnoyarsk, Russia, September 5-7, 2006. Lecture on: “Anode effect (AE) in aluminium cells, and Nordic Hydrogen Seminar 2006, Oslo, Norway, February 6-8, how to reduce AE frequency”. Workshop on: “The optimum 2006. Lecture on: “Nanostructured electrocatalysts for PBI bath composition in aluminium electrolysis”. fuel cell”.

University of Moscow, Moscow, Russia, September 8, 2006. Arranged General Assembly Meeting, EU-project FURIM, Visit to “The Electrochemistry Group”. Seminar: “Are inert NTNU, Trondheim, Norway, April 3-4, 2006. anodes for aluminium production close to a technological breakthrough”? 209th Meeting of the Electrochemical Society, Denver, USA, May 7-12, 2006. Lecture on: “Nanocrystalline oxides as oxygen 45th Annual Conference of Metallurgists of CIM/17th evolution electrocatalysts for PEM water electrolysis”. International Symposium of ICSOBA, Montreal, Canada, October 1-4, 2006. Lecture on: “Adsorption of SO2 on smelter 12th Nordic Symposium on Catalysis, Trondheim, Norway, grade alumina”. May 28-30, 2006. Lecture on: “Development of nanostructured Pt-based electrocatalyst for high temperature polymer Julian Tolchard electrolyte fuel cells”. 3rd National FUNMAT Meeting, Trondheim, Norway, January 4-6, 2006. Permascand and KTH, Sweden, May 31 – June 1, 2006. Co-arranged discussion and presentation meeting. Lecture Researchers’ Night, NTNU, Trondheim, Norway, September on: “Electrocatalysis in electrochemical energy systems”. 22, 2006. Practical demonstrations. 57th Annual Meeting of the International Society of Solid State Proton Conductors 13 (SSPC-13), St Andrews, Electrochemistry, Edinburgh, Scotland, August 27 - September 4+ 5+ United Kingdom, September 4-6, 2006. Lecture on: “Chemical 1, 2006. Lecture on: “Kinetic studies of the V /V Red/Ox system in sulphuric acid”. compatibility of the proton conductor BaZrO3”.

Workshop – “Functional Oxides for Energy Technology”, 2nd KIFEE Symposium, Trondheim, Norway, September 6-8, Trondheim, Norway, October 2, 2006. Lecture on: “A kinetically 2006. hindered phase transition in Ba Sr Co Fe O ”. x 1-x 0.8 0.2 3-δ 5th International Conference on Electrocatalysis (ECS’06), Solid State Group Meeting, Sheffield, United Kingdom, Montenegro, September 10-14, 2006. Poster on: “Synthesis December 18-19, 2006. Poster on: “Choosing the right and characterization of CNF – supported catalysts for high electrode: chemical compatibility of the proton conductor temperature polymer electrolyte fuel cells”. SrCeO “. 3 Volvo, Chalmers Science Park, Göteborg, Sweden, October 12- Mikhail Tsypkin 13, 2006. General Assembly meeting EU-project FURIM. 3rd National FUNMAT Meeting, Trondheim, Norway, January 5- 6, 2006. Lecture on: “Carbon nanofibre supported Pt catalysts POLEN 2006 Seminar, Trondheim, Norway, October 13-22, for high temperature polymer electrolyte fuel cells”. 2006. Lecture on: “Metal deposition from molten chlorides, diffusion and nucleation processes”. Nordic Hydrogen Seminar 2006, Oslo, Norway, February 6-8, 2006. Lecture on: “Nanostructured electrocatalysts for PBI Johan Kr. Tuset fuel cell”. Silicon for the Chemical Industry VIII, Trondheim, Norway, June 12-15, 2006. Lecture on: “Thermodynamics of the 12th Nordic Symposium on Catalysis, Trondheim, Norway, Carbothermic Silicon Process”. May 28-30, 2006. Lecture on: “Development of nanostructured Pt-based electrocatalyst for high temperature polymer Kristin Vasshaug electrolyte fuel cells”. Internal CarboMat Seminar, Trondheim, Norway, February 16, 2006. Lecture on: “Electrochemical wear of carbon materials 57th Annual Meeting of the International Society of in fluoride melts”. Electrochemistry, Edinburgh, Scotland, August 27 - September

58 Extracurricular Activities

CarboMat Resource Group Meeting, Trondheim, Norway, FUNMAT-subproject Meeting, Functional Oxides for Energy March 7, 2006. Lecture on: “Electrochemical wear of carbon Technology (FOET), Trondheim, Norway, October 2, 2006. materials in fluoride melts”. Lecture on: “Oxygen transport in La2NiO4+ δ and the effect of Department of Environmental Systems Science, Doshisha water”. University, Kyotanabe, Japan, April 1 - June 29, 2006. Grant: The Scandinavia-Japan Sasakawa Foundation. Study visit. COST-539, Workshop, Electroceramics from Nanopowders Produced by Innovative Methods (ELENA), Brüssels, Belgium, Lake Biwa Environmental Research Institute, Otsu, Japan, November 15-16, 2006. Session chairman. Lecture on: May 20, 2006. Study visit and meeting. ”Production of nanoscaled complex oxide powders by spray pyrolysis and the relation between powder characteristics Internal Seminar, Department of Environmental Systems and densification properties”. Science, Doshisha University, Kyotanabe, Japan, May 23, 2006. Lecture on: “Electrochemical wear of carbon materials Gemini Centre, Seminar on Energy and Materials, Trondheim, in fluoride melts”. Norway, November 24, 2006. Lecture on: ”Production of high quality ceramic powders by spray pyrolysis”. SEC Corp., Fukuchiyama, Japan, June 9, 2006. Study visit and meeting. Lecture on: “Aluminium electrolysis and carbon Lifeng Zhang material science”. Lifeng Zhang is a Senior Guest Consultant for Shougang Research Institute of Technology (Shougang Steel, Beijing, Lake Biwa Environmental Research Institute, Otsu, Japan, China). He is a Key reader (Member of Board of Review) for the June 27, 2006. Seminar. journal of Metallurgical & Materials Transactions B. He is also a scientific adviser at SINTEF, Trondheim, Norway. 2nd KIFEE Symposium, Trondheim, Norway, September 6-8, 2006. Research projects in 2006: “Water modeling on the fluid flow-related phenomena in aluminum electrolysis cell”, Annual CarboMat Seminar, Trondheim, Norway, November “Purification of aluminum through coated porous filter”, 15-16, 2006. Lecture on: “Cathode wear mechanisms”. “Investigation on the oxidation layer on the top of molten aluminum”, “Fundamentals, practice and modeling during Fride Vullum metal recycling, refining and processing”, “Recycling light 3rd National FUNMAT Meeting, Trondheim, Norway, January metals for high value-added use”, “Mathematical simulation 4-6, 2006. on the fluid flow and heat transfer in a sodium silicate furnace”, “Integrated nordplus postgraduate education and research Ph.D.-pool Seminar, The Gas Technology Center (GTS), network in steel research (INPERNSR)” and “Purification of Si Trondheim, Norway, March 10, 2006. Lecture on: “Development melts by filtration process”. of electrolyte material for proton SOFC”. University of Illinois, Urbana-Champaign, USA, December 16, Contact Meeting GTS, NTNU, Trondheim, Norway, May 15, 2005 - January 4, 2006. Research visit. 2006. Lecture on: “GTS Ph.D.-pool pilotprosjekt”. Elkem Company, Kristiansand, Norway, February 7, 2006. Department Seminar, Brekstad, Norway, June 15-16, 2006. Lecture on: “Refining, casting and recycling of aluminum and silicon”. 9th International Conference on Inorganic Membranes, Lillehammer, Norway, June 25-29, 2006. Cores Steel Research Center, The Netherlands, February 9, 2006. Lecture on: “Inclusions related research during steel 2nd KIFEE Symposium, Trondheim Norway, 7-8 September, refining and continuous casting”. 2006. University of Science and Technology, Beijing, China, February FOET work shop, NTNU, Trondheim, Norway, October 2, 2006. 22, 2006. Research visit, host Professor: Hongmin Zhu. Lecture on: “Synthesis routes and transport properties of tetragonal CeNbO ”. 4+δ TMS 2006 Annual Meeting, San Antonio, Texas, USA, March 12-16, 2006. Lectures on: “State of the art in recovery of Journalism and research course, Fredrikstad, Norway, aluminum from aluminum dross” and “Fluid flow and transport November 9-10, 2006. phenomena during steel refining and casting process”.

Kjell Wiik MAP Project: Molten Aluminium Purification, Hotel Tulip Inn 3rd National FUNMAT Meeting, Trondheim, Norway, January Boulevard, Brussels, Belgium, April 24-25, 2006. End-term 5-6, 2006. Lecture on: “Production of multicomponent oxide conference and meetings. powders by spray pyrolysis”. Hydro Aluminum, Sunndalsøra, Norway, April 28, 2006. Electroceramics X, International Conference on Lecture on: “Purification of aluminum and silicon and inclusion Electroceramics and their Applications, Toledo, Spain, June 18- detection”. 22, 2006. Session chairman. Lecture on: “Production of nano- scaled complex oxide powders by spray pyrolysis”. Norwegian Metallurgical Society Summer Meeting, Oslo, Norway, May 4-5, 2006. COST-539, Electroceramics from Nanopowders Produced by Innovative Methods (ELENA), Toledo, Spain, June 19, 2006. Department of Mechanical and Industrial Engineering, Management Committee Meeting. University of Illinois, Urbana-Champaign, USA, June 6-7, 2006. Awarded as a visiting professor.

59 Extracurricular Activities

2006 Beijing International Materials Week (2006 BIMW), Buenos Aires, December 2-8 and 11-15, 2006. Study visit to oil Beijing, China, June 25-28, 2006. Lectures on: “State of the and gas research institutions. art in the refining and recycling of magnesium”, “Removal of impurity elements from aluminum scrap through” and Celta industrias, Dir. Carlos Luengo, Punta Del Este, “Filtration purification of solar cell silicon materials through Uruguay, December 8-11, 2006. Meetings. filtration”. Courses in the use of MEGScale 7.0 developed for Statoil and Norsk Hydro, Bergen, Norway, January 31 – February 2, Symposium on the Economical and Technology Cooperation of 2006. Chinese Experts in Other Countries, June 29 - July 2, 2006. Petrotech, Haugesund, Norway, October 31 – November 4, Shanghai Jiaotong University, China, November 27-28, 2006. 2006. Lecture on: “Norwegian and international oil industry”. Lecture on: “Refining and recycling of metals”. Meeting with Radcon Italia, Modena, Italy, May 11-12, 2006. Chongqing University, China, November 29-30, 2006. Awarded as a guest professor. Lecture on: “Refining and recycling of Department of Chemical Engineering, University of Patras, metals”. Greece, November 6, 2006. Katerina Kofina and Marianna Lioliou’s Ph.D. defence. 5th International Conference on Computational Fluid Dynamics in the Process Industries (CFD2006), Melbourne, Australia, Harald A. Øye December 11-15, 2006. Lectures on: “Fluid flow, heat transfer Harald A. Øye is chairman of the technical committee ISO TC and inclusion removal in continuous casting strands” and 226 (Materials for the Production of Primary Aluminium). He “Fluid flow, heat transfer and inclusion motion in continuous is member of the Scientific Board for the company Metalysis, casting tundishes”. Rotherham, United Kingdom.

CSIRO Minerals (Light Metal Group, CFD Group, and High The Norwegian Academy of Technical Sciences, Oslo, Norway, Temperature Group), Australia, December 18, 2006. Research March 2, 2006. Industrial council meeting. visit. Host researchers: Dr. Alan Manzoori, Dr. Phil Schwarz and Dr. Sun Shouyi. 135th TMS Annual Meeting, San Antonio. Texas, USA, March 10-16, 2006. Terje Østvold Terje Østvold is a member of the TEKNA Oil field chemistry ARABAL 2006, Sharm El-Sheikh, Egypt, April 2-5, 2006. symposium board. Meetings in Oslo, Norway, May and Lecture on: “The importance of ISO testing of materials used October, 2006. in the primary aluminium industry”.

Project and board meetings related to “Sand Stabilisation Egyptalum, Nag Hammady, Egypt, April 8-10, 2006. Lectures and Water Proofing of Tunnels”. This project is operated by on: “Aluminium electrolysis. Principles, environmental the spin-off company Impermeable AS. Project meetings: concerns and new technologies”, “Cathode materials”, Statoil Stjørdal; Norway, January 11, 2006. Radcon “Cathode construction”, “Chemical reaction and physical Scandinavia, Oslo, Norway, February 3-5 and 9-12, August 18- changes”, “Start and operation”, “Cell autopsy manual”, “How 20 and December 30, 2006. to obtain long-lived cells”, “Test procedures and ISO standard work”, “Test methods” and “Spent potlining treatment”. ICE/HT-FORTH, and University of Patras, Patras, Greece, June 5 - July 5, 2006. Study visit and guidance of 5 Ph.D. students at Department of Chemistry, Alexandria University, Alexandria, Department of Chemical Engineering. Egypt, April 13-14, 2006. Lecture on: “The power of thermodynamic modelling”. Cooperation with SINTEF Petroleum Research. Project meetings and reporting, Statoil, Trondheim, Norway, January In-Situ Analysis, Hørsholm, Denmark, May 4-5, 2006. 13, February 15 and September 7, 2006. A series if meetings Research cooperation. during the year at Statoil; Rotvoll and Stjørdal, Norway. Strategy meeting, Torpberget, Norway, October 25-26, 2006. Metalysis, London, United Kingdom, May 25, 2006. Scientific board meeting. 17th International Oil Field Chemistry Symposium, Geilo, Norway, March 19-22, 2006. Member of committee and session Fundamentals of Aluminium Production 2006, Trondheim, Chairman. Paper on: “Prediction of scale potential in ethylene Norway, May 15-26, 2006. Chairman. glycol containing solutions”. 25th International Course on Process Metallurgy of Aluminium, 8th International Symposium on Oilfield Scale, Aberdeen, Trondheim, Norway, May 29 - June2, 2006. Chairman and Scotland, May 30 - June 1, 2006. Paper on: “Quasi natural lectures on: “The principles of aluminium electrolysis” and consolidation of poorly consolidated oil field reservoirs”. “How to obtain long-lived cells”.

The Oil and Gas Research Institution, Petrobras, Rio de Silicon for the Chemical Industry VIII, Trondheim, Norway, Janeiro, November 18 - December 2, 2006. Study visit and June 12-15, 2006. Chairman. courses on: “Mineral scale prediction and evaluation of new gas field developments with respect to the possible scale RUSAL, Sajanogorsk and Krasnoyarsk, June 19-30, 2006. Cell problems that could occur when these fields are starting autopsy. production”. In-situ Analysis, Hørsholm, Denmark, August 8-9, 2006. Research cooperation.

60 Extracurricular Activities

R and D Carbon, Sierre, Switzerland, August 11, 2006. Research cooperation.

EUCHEM, Hammamet, Tunisia, September 16-22, 2006. Lecture on: “Molten salt experimental methodology. In retrospect”.

ISO/TC 226, Materials for the primary production of aluminium, Paris, France, September 26-28, 2006. Chairman.

COM 2006, 45th Annual Conference of Metallurgy of CIM, Quebec, Canada, October 1-4, 2006. Lecture on: “International standards (ISO) testing of materials used in the primary aluminium industry”.

Norsk Kjemisk Selskap, Trondheim, Norway, October 31, 2006. Lecture on: ”ISO-standardisering av materialer”.

Torjus Åkre KTH, Stockholm, Sweden, May 15, 2006. Project meeting. Lecture on: “Anode scaling in cobalt electrowinning: Project status May 2006”.

Xstrata Nickel Falconbridge Nikkelverk, Kristiansand, Norway, August 14 - December 28, 2006. Supervisor of Eivind Iglebekk’s diploma work: ”Influence of manganese on the electrowinning of nickel from chloride solutions”.

2nd KIFEE Symposium, Trondheim, Norway, September 6-8, 2006. Lecture on: “Pilot cell studies of cobalt electrowinning from chloride solution”.

KTH, Stockholm, Sweden, November 27, 2006. Project meeting. Lecture on: “Influence of manganese on the electrowinning of nickel from chloride solutions”.

61 Notes

62 Notes

63 Notes

64 Notes Skipnes AS

Annual Report resultsinideas noone else has thought of, and creative solutions that arts,medicine, architecture tofine arts. Cross-disciplinary cooperation wellasinother academic disciplines ranging from the social sciences, the representsacademic eminence intechnology and thenatural sciences as TheNorwegian University ofScience and Technology (NTNU) inTrondheim NTNUInnovation– and Creativity NO-7491Trondheim, Norway NorwegianUniversity ofScience and Technology DepartmentofMaterials Science and Engineering changeour daily lives. Innovation and Creativity and Innovation www.ntnu.no