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Status PETRA III Including PETRA IV PETRA III and PETRA IV at DESY Research opportunities for the Baltic Sea Region Hans-Christian Wille DESY, Hamburg Baltic Science Network e-conference Symposium "Photon and Neutron Science in the Baltic Sea Region“, October 26-29, 2020 Campus Bahrenfeld Accelerator-based X-Ray Free-Electron Laser fs dynamics of complex matter photon sources on the atomic scale PETRA III Ada Yonath Hall CXNS NanoLab PETRA III Paul Peter Ewald Hall CHyN HARBOR PETRA III MPI-SD FLASH Synchrotron Radiation VUV & Soft X-ray of Highest Brightness Free-Electron Laser atomic structure of complex fs dynamics of complex matter matter (spectroscopy) 2 Outlook • PETRA III / PETRA IV some features, scientific scope • Some research examples /highlights • Outlook PETRA IV - The call for Scientific Instrument Proposals Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 PETRA III fact sheet The PETRA III experimental hall „Max von Laue“ DESY’s Brilliant Synchrotron Radiation Source History of PETRA: 1978: PETRA I built for high-energy physics, first direct observation of the gluon 1988: PETRA II as pre-accelerator for HERA 2007: rebuild of PETRA as a 3. generation synchrotron radiation source (PETRA III) electron energy 6 GeV 2010: start of user operation with the first three stored current 100 / 120 mA (top-up) beamlines emittance (h × v) 1.2 nmrad × 10 pmrad 2013: all 15 beamlines fully operational in the circumference 2304 m experimental hall “Max v. Laue” photon energy range 250 eV - 150 keV Mar. 2014 - Apr. 2015: beamlines in operation 23 PETRA III Shutdown for extension project after the beamlines under construction 2 DORIS III shutdown beamlines still open 2 2016: PETRA III extension project starts users user operation (hours/year) 5000 operation with the first two beamlines bunch separation 192 ns or 16 ns Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 4 Verbundforschung P01: Dynamics beamline, IXS, NRS PETRA III P02.1: Powder diffraction & total scattering Beamlines P02.2: Extreme conditions P03: Micro-, nano-SAXS, WAXS (DESY, HZG) Max v. Laue Hall P04: Variable polarisation XUV Paul Peter Ewald Hall P05: Micro-, nano-tomography (HZG) P64 P65 P06: Hard X-ray micro-, nanoprobe P07: High-energy materials sci. (HZG, DESY) P08: High-resolution diffraction P62 P09: Resonant scattering/diffraction P61 (HZG,DESY) P10: Coherence applications P11: Bioimaging/diffraction P12: BioSAXS (EMBL) Ada Yonath Hall P61: High-energy wiggler beamline (HZG, DESY commissioning) P13/14: MX (EMBL) P22 P21 P24 P62: Small-angle X-ray scattering P23 P21: Swedish materials science beamline (construction, commissioning) P21.1 High-energy broad band diffraction P21.2 High-energy diffraction and imaging P63: MPG catalysis (in planning) P22: Hard X-ray photoelectron spectroscopy P64: Advanced XAFS P23: In-situ and nano diffraction beamline (KIT) P65: Applied XAFS P24: Chemical crystallography P66: Time-resolved luminescence spectroscopy (operational 2021) P25: TBD (in planning) Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 5 Hall „Paul Peter Ewald“ Verbundforschung PETRA III BLs P61 … P65 23 Beamlines operational P66 Methods at beamlines With experiments optimized for: - Scattering - Large coherence volume - Diffraction - High flux - Spectroscopy - Small focus - Imaging - High energy resolution - Coherence applications - High stability - Speed - In-situ & operando methods N External contributions or responsibilities HZG 3 Beamlines operated by EMBL EMBL 2.5 Beamlines operated by HZG Sweden 1.3 „Indian virtual beamline“ ➔ priority access 1.89 Swedish beamline equivalents ➔ priority access Swedish Material Science beamlines P21.1 and P21.2 several MPI/Helmholtz involvements adding up to 1 beamline ➔ priority access Hall „Ada Yonath“ Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 BLs P21…P25 6 Hall „Paul Peter Ewald“ Verbundforschung PETRA III BLs P61 … P65 more than 50 experiments covering most relevant methods P66 Diffraction & Scattering P02.1, P02.2, P07, P21.1, P21.2, P61 High energy X-ray, white beam diffraction & imaging P03, P12, P62 Small angle scattering, GISAXS, µASAXS (➔ 2020) P08, P23, P24 Crystallography & Surfaces scattering P11, P13, P14 Macromolecular crystallography P04, P06, P10 Coherent diffraction & scattering P09 Resonant magnetic scattering Spectroscopy P01 Inelastic and nuclear scattering P22 Hard X-ray photoelectron spectroscopy N P04 Soft X-ray photoelectron spectroscopy P64, P65 X-ray absorption & fluorescence spectroscopy P09 XMCD HZG P66 VUV spectroscopy, t-resolved (➔ 2021) EMBL Imaging Sweden P04, P06, P10 Micro & Nano imaging (coherence) P05, P06, P07, P14, P61, P23-KIT Micro & Nano imaging (absorption & phase contrast, laminography ➔ 2021) P03, P06, P21.1, P21.2, P62 Micro & Nano imaging (fluorescence, dark field, SAXS, etc. ) ➔ multiple beamlines host different methods (P01, P04, P07, P09, P10, P23) Hall „Ada Yonath“ Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 BLs P21…P25 7 PETRA III PETRA users in 2019: User Statistics 3155 unique users 6306 user visits PETRA user community growing due to higher number of beamlines & high throughput experiments Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 8 PETRA III Baltic User Statistics Baltic users in 2019: 593 unique users Denmark Estonia Finland Lithuania 167 Latvia Norway 212 Poland Russia Sweden 4 17 5 Swedish Research Council 16 4 strategic partner 41 Beamtime of 1.89 BL equivalents 127 Swedish Material Science Beamline P21 Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 9 DESY – Baltic Sea Science Networking Many succesfull cooperations Networks • Baltic Science Network • LEAPS • HALOS • CREMLINplus • CALIPSOplus • Röntgen-Angstrom Cluster • CAROTS • Baltic Tram Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 10 DESY – Baltic Sea Science Networking Many succesfull cooperations Partners • Aarhus University (in-situ- x-ray scattering, materials crystallography) • Budker Institute of Nuclear Physics (accelerator technology) • Efremov Scientific Research Institute (accelerator technology) • KTH Stockholm (joint Profs, RAC projects, joint PhDs…) • Swedish Research Council (Center for X-rays in Swedish Materials Science (CeXS) - Swedish Material Science beamline P21) • Lund University (HALOS, HELIOS grad school, RAC projects) • MAXIV • …. Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 11 P21 Beamline overview EH3: Diffraction station Swedish Material Science beamline • Beamsize: 1 mm … 6 mm • Energy bandwidth: 10-4 … 2´10-3 • Time resolution down to milli-seconds EH1: Side station (broad band diffraction) ▪Beamsize: 0.05 mm … 2 mm • Techniques: ▪Energy bandwidth: 2´10-3 … 10-2 WAXS combined with SAXS & imaging ▪Techniques: WAXS & PDF OH1 OH2 P21.1 OH3 IVU P21.2 e 50 m 100 m EH2: “roll-in” station (not instrumented) ▪Beamsize: 0.05 mm … 6 mm ▪Bulky sample environments | MSE 2020 | Ulrich Lienert, Sept. 23 P21 Beamline overview Swedish Material Science beamline Side station, large 2-D detector, heavy load stage EH3 diffraction station, SAXS, WAXS, micron beamsize | MSE 2020 | Ulrich Lienert, Sept. 23 PETRA III Science examples PETRA III users conduct science in many areas - 4 e Auger transition 750GPa Osmium NaHe2 compound Extreme States of Matter: From Cold Ions to Hot Plasmas Quantum Condensed Matter: CDWs in YBCO Spin Waves in Iridates Skyrmions Magnetism, Superconductivity, and Beyond Nano-Indenter Li/S fuel cell XRF & Ptychography Materials and Processes for Energy and Transport Technologies Grain Rotation Nano-dot Surfaces Nanofocus Multilayer-Laue Lens Nanoscience and Materials for Information Technologies Strongest Protein Fiber Ancient Midge Lytb/IspH Structure Soft Matter, Health and Life Sciences Baltic Science Network e-conference Symposium, Hans-Christian Wille, October 26-29, 2020 14 Hydrogen infusion in duplex stainless steel • KTH (Stockholm) • Cathodic hydrogen charging under constant tensile load Scanning procedure • 20 µm depth increments • (current density 38 mA/cm2) • 1 mm translation • 6 min per depth scan • Depth profiling of lattice spacing • P21.2, 96 keV, beamsize 20x55 µm (h x v) 100 µm Örnek et al., Corr. Sci. 175 (2020) 108899 | MSE 2020 | Ulrich Lienert, Sept. 23 Cellulose-based materials I – highest strength fibers Daniel Söderberg, KTH, Stockholm P03 beamline (GISAXS, WAXS, SAXS) • Defect free fibers • Functional fibers • Monitoring of in situ spinning • Energy harvesting via piezoelectricity: AgNW Mittal, … Roth, …Söderberg, ACS Nano 12, 6378 (2018) Shin et al., ACS Omega 3, 16150 (2018) Beschichtungsprozesse direkt beobachten | Stephan V. Roth, 01.11.2019 Example III - Microfluidics for fibre spinning Söderberg group, KTH, Stockholm • Cellulose nanofibrils (TEMPO) • µSAXS: CNF orientation into filaments • nanoWAXS Trebbin, …, Roth,… PNAS 110, 6706 (2013) Håkansson, …, Roth,…, Nat. Commun. 5, 4018 (2014) Beschichtungsprozesse direkt beobachten | Stephan V. Roth, 01.11.2019 PETRA III Corona related experiments with priority from directorate P03 S Techert (DESY), SV Roth (PETRA III) (SAXS): Introduction of chloroquine-based derivatives in complementary matrices for oral drug delivery of anti-corona substances P08 & P23 & P12 (P62) C Wölk (U Leibzig), R Harvey & G Bello (U Wien), C Shen (PETRA III) (A combined
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