Reaction Systems International Catalogue

Unpriced 2 GENERAL GLASSBLOWING INTRODUCTION Specialist ScientificGlassblowing replacement. complete refundor you mayreturnitfora performance ofanyproduct, satisfied withthequalityor ... ifyouarenotcompletely pleased toproveit...... and wewillbe are thesame... all scientificglassblowers At Radleyswebelievethatnot Interchim 211 bis avenue JF Kennedy - BP1140 - 03100 Montluçon - Franc - Montluçon 03100 - BP1140 - Kennedy JF avenue bis 211 Interchim e: f: t: +33470038855 unrivalledscientificglassblowingservice...an with youprovide contractlargequantities...vessel,foror will large singleRadleys a orspecialisedprecisionitemsmall,made require a Whetheryou V purchased,youmay return itfor complete a refund orreplacement. completelysatisfied with the quality orperformance ofany product firstpriority andwe aim tokeep itthat way. Therefore, ifyou arenot AtRadleys, ourcustomers areour future. Customer care isour Policy...HassleNo accommodateneeds.toyour pleased be will we replacementitem,or new urgentlyrequirea orrepairquick a need urgentprojects.Whetheryouryou with deal tocapacity the have scientificskilledwe thatglassblowersofmeans team large Our delivery...Fast trustin. can youthat glasswarereliableconsistent and strain.youGiving andstones scratches,lines,airimperfections,as: offreesuch andhand-made requirementsproductyourexactly.meets glasswareisour All importantotherspecifications.any andend Ensuringthethat thicknesstolerances,sizes,wall jointseals,on made are checks priority.highest our Throughoutprocessconstantglassblowingthe precisionsample,is a sketch,ordrawing a from working are we quality.with hand in handPrecisiongoes whetherRegardlessof W withinfull. requirementsthat may have been specified, have been complied stressfree before leaving ourfactory, andthat any important safety glassware.We ensure that allour glassware isannealed and Safetyisverya important factor inthe manufacture oflaboratory commitmentsafety...toA System. ISO9002AssuranceapprovedQualityoperatea Radleys such strictfromProductas standards;comesqualityexcellence and say,to customersglassblowers.bestare our of somethat proudare best.Indeed,we therightly demandcustomers quite our andscientific goodglassblowing ofessence the Qualityis QualityAssurance breweries.todairiesfrom universities and to electronics,engineeringstationsmechanicalto powerfrom environmentalrefineries,monitoring,hospitalstofrom from pharmaceuticalsagrochemicals,toresearchmedical fromto from applications- industriesandof wealth a items,fordiverseof multitudea make to asked been haveRadleys years 35 last theIn Flexibility... credit.theirexperienceto glassblowing ofyearstechnologists glassmany and have glassblowersskilled highly ofteam our proficiency ofdegreeand anyglassblowing toof perfectskill totheyears takes itIndeed craft.handskilled highly scientificremainsa stillglassblowing specialisedthen,sincechanges many been have thereWhilst establishedfirstRadleysglassblowing a facility1968.in Glassblowing Scientific Specialist ersatility... orking to your precisescientificorkingyourto specifications... +33 470038260 [email protected] e e www.interc

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or viaon-sitevisits. requirements, wecanhelp. or wouldlikeanewitemalteredduringmanufacturetosuityour If youhaveanexistingpieceofglasswarewantmodified Need amodificationorsomethingslightlydifferent... requirements. FREEquotationsaregivenforanyquantity. We OEM/Contract enquirieswelcome... what youwantandwewillprovidewithadrawingtoapprove. with adetailedfaxedquotationbyreturn.Alternatively, describe relevant dimensionsandspecifications,wewillprovideyou complexity. Simplyfaxorsendusasketch,sample,withthe Free quotationsaregivenforanyitemregardlessofsizeor Fax usasketchandwe’llsendyouquote... a vastexperienceinthedesignofalltypesscientificglassware. Radleys’ teamofglasstechnologistandproductspecialistshave Custom GlassblowingService Contact ustodayon... • • • • • • • • • Services serviceavailable.Pleaseseeoverleafformoredetails. and delivery ofchargequotations,withacollection unnecessary waste.FREE Our glasswarerepairservicewillsaveyoumoneyandreduce Glassware Repairs Scope ofOurServices Advice canbegiven Stainless Steel,Polycarbonate,HDPEandPolypropylene. range ofmaterials,including:PTFE,PEEK,Acrylic,Aluminium, We overhead stirrers,lids,thermoregulatorsandprobes. full rangeofreactionsystemaccessoriessuchasframeworks, of glassreactionvessels,from250mlto30litres-includingthe We and problemsolving. specialists havemanyyearsofexperienceinprojectdevelopment stage. Ourexperiencedglasstechnologistsandproduct project, wewillbehappytoassistinallaspectsofthedesign Whether yourequirealargeprocessrigorhavesmallprototype Give usacall... Need somehelpdesigningyourglasswareorsystem? Glassware DesignService : 3 4 0 3 8 5 60 82 03 55 70 88 e: [email protected] 4 03 +33 70 f: 4 +33 t: Glassware safetyaudits Installation oflargesystemsorcomplexassemblies Amber Staining&PlasticCoating Enamel Transfers &ScreenPrinting Graduating, Grinding&Cutting Large ProductionRuns Prototype &DevelopmentProjects Custom GlassFabrication Borosilicate &QuartzScientificGlassblowing will bepleasedtoquoteforyourOEMequipment can alsoprovidecustomengineeringsolutionsinawide have aparticularexpertiseinthedesignandmanufacture FREE ofCharge t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] by telephone,email

Specialist ScientificGlassblowing

3 GENERAL GLASSBLOWING INTRODUCTION 4 GENERAL GLASSBLOWING INTRODUCTION Specialist ScientificGlassblowing nterchim 211 bis avenue JF Kennedy - BP1140 - 03100 Montluçon - Franc - Montluçon 03100 - BP1140 - Kennedy JF avenue bis 211 Interchim • • • • Benefits to ‘web’.Fluoralon‘G’hasanexceptionallywidetemperaturetolerancefrom-200˚C+250˚C. complex geometrywithcompleteintegrity, unlikeconventionalprotectivesleevingwhichtends Fluoralon ‘G’issprayedonandthenheatcured.Itthereforecapableoffollowingthemost safety barrier. is appliedtotheexteriorsurfacesofglasswareprovidinganimmenselystrong‘plastic’ dangerous shardsandcontaminationofworkareasintheeventbreakage.Thecoating The Fluoralon‘G’safetycoatinghasbeendevelopedtoprotectusersofglasswarefrom glassware itemandoffersexceptionalchemicalresistancetemperaturerange... This uniqueFluoropolymercoatingcanbeappliedtoalmostanyborosilicatescientific NEW Contact ustodayforaFREEquotation and wewillbepleasedtoamberstainanystandardorspecialistitemyoumayrequire. Beakers, Cylinders,Test Tubes, Bottlesetc.Howeverthisisbynomeansacompletelist most commonitemsweamberareSeparatingFunnels,ReactionVessels, Burettes,Flasks, addition tospecialisinginthemanufactureandamberingofourownglassware.Some We of glassware. overcomes theseproblems,becauseitisascosteffective toapplyoneorahundredpieces making productionincolouredglass,bothimpracticalanduneconomic.Amberstaining approximately 500nm.Thequantitiesofglasswarerequiringamberingareusuallysmall, It hasbeenshownthatglasswhichamberedcanabsorbshortwavelengthsupto Amber stainedglasswareisoftenessentialwhenworkingwithphotosensitivesubstances. Amber stainingiscosteffectivetoapplyoneorahundredpiecesofglassware... Amber StainingService • Our RepairServiceincludes:- it generallycostsbetweena1/3and1/2ofthenewpricetorepairbrokenglassitem. same attentiontoqualitythatweundertakerepairbrokenglassware.Asarule-of-thumb, We Save £££’s onourglasswarerepairservice.. Glassware RepairService 33 4 70 03 88 55 88 03 70 4 +33 on today us Contact • • • • • • Protects userfromhazardousspilledliquids Improves theresistanceofglasstothermalshock Reduces liabilityriskforschools Reduces riskofinjuryduetoglasswarecuts We the glasswaretoyou,ordisposeofit. If anitemisunrepairableoritnoteconomicaltorepair, wewillinformyouandeitherreturn We packing andcleaningofbrokenglassware.PlusapaircutresistantPolysafeGlassGloves. Included witheachRepairsBoxisafullsetofsafetyinstructionsforthesafehandling, to ownershipofreturneditems. This helpsdepartmentalcostingandavoidsanyconfusionwithindepartmentswithregard Included witheachRepairsBoxwillbeadedicatedsheetforthelistingofitemsrepair. We We We believe thatthequalityofourmanufacturedglasswareissecond-to-none,anditwith undertake toamberalltypesofglassware,includingthatsuppliedbythecustomer, in can arrangeforaregularcollectionanddelivery. will provideafreeofchargewrittenquotation,whichbefaxedtoyoubyreturn. will provideaheavydutyplasticRepairsCollectionBox. will proceedwiththerepairsonlyonreceiptofyourauthorisation. Fluoralon ® ‘G’ SafetyCoatingforGlassware for more information more for e e www.interchim.com Contact us today on today us Contact more... much and transfers enamel printing, screen plate, glass prisms, and discs optical blasting, sand graduating, etching, polishing, grinding, centreless ends, tube of grinding parallel grinding, flat cutting, Drilling, include... services working glass cold specialist of range Our WorkingGlass Cold on today us contact please testing pressure or vacuum on information more for or vacuum/pressure, with working on advice For impractical.thisconditionsmake variabilityoperatingtheof and glassof nature implied.The or given be operatingconditionscan actual under performance its of guarantee no conditions, test specific under glassware the of performance the indicate will certification and testing pressure/vacuum whilst that note Please request. on items multiple or individual for given are Quotations standards. national to traceable used, equipment of certification and item each for record individual an includes Certification level. predetermined a at vacuum, a of case the in or pressure; working maximum the twice to; tested independently are items We Vacuum& Pressure Testing on today us Contact etc. audits safety glassware repairs, emergency on-site rigs, vacuum assembling as such work on-site for available also are Glassblowers basis. weekly or daily a on provided are glassblowers Skilled help. can we cover temporary need you if so holidays... have to need glassblowers Even call... a us Give ? glassblower back-up or temporary on-site an Need Service Glassblowing On-site on today us Contact 810002. No. Cat item. per £2.50 plus certificate per £12.50 @ numbered, individually item each with certificate single A 810001. No. Cat certificate. per £12.50 @ item each for certificates single or orders complete for certificates Single A Conformity of Certificates • • • • • • • precautions shouldbetaken... If youdowishtosubjectyourglasswarepressureorvacuum,thefollowingsafety therefore beavoidedifpossible. Subjecting laboratoryglasswaretopressurecanbeveryhazardous,andshould Pressure &Vacuum SafetyProcedures-Testing ofGlassware vailable for all standard and custom glassware items... glassware custom and standard all for vailable are likelytoimplode. Generally speaking,flatbottomedvesselsshouldnotbeusedundervacuumasthey Always applyorreleasethepressurevacuumgradually. significantly affect thestrengthofyourglassware. Check glasswarefordamage,suchaschipsorcracks.Eventhesmallestdefectscan A Use safetynettingorplasticcoatings. Always enclosevesselswithsafetyshields. Obtain independentpressure/vacuumcertificationofindividualvessels.

void over-clamping,whichcancausestresswithinthevessel. are pleased to be able to offer this service for all types of vessel. Individual glassware Individual vessel. offerof to types able all be for to service pleased this are +33 4 70 03 88 55 88 03 70 4 +33 55 88 03 70 4 +33 55 88 03 70 4 +33 t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] e: [email protected] e: 60 82 03 70 4 +33 f: 55 88 03 70 4 +33 t: for more information more for information more for information more for +33 4 70 03 88 55 88 03 70 4 +33 Specialist ScientificGlassblowing for more information more for

5 GENERAL GLASSBLOWING INTRODUCTION 6 GENERAL GLASSBLOWING INTRODUCTION Specialist ScientificGlassblowing Sintered GlasswarePorosityGradeGuide OOIYDSGAINPR IEEXAMPLEAPPLICATIONS PORESIZE DESIGNATION POROSITY 2 1 0 B Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com S 73NOMINAL ISO 4793 A 104 10mPreparativefinefiltration,Mercury 40-100µm P100 Coarsefiltration,GasDistribution 100-160µm P160 2010-20mCoarsefiltration,GasDistribution 160-250µm P250 C C B A Stopcock SelectionGuide Contact us today on today us Contact photo-chemicalreactor, we will be pleased to help. chemicalinertness. Whether you require asimple beaker, furnace tube or amore complicated resistance,thermal shock resistance, high electrical insulation, optical transparency and FusedQuartz Glass is aunique material with an unrivalled combination of purity, high temperature Glassware Quartz Fused Clear on today us Contact methods. those with conformance of certification the requested, where and methods of sourcing the includes service Our abroad. and UK the in both methods, test standard of range large a of requirements the meet to systems glassware complete for quote to pleased be will we area specialist your Whatever IP,ASTM, BS, including, EPA, Pharmacopea... British and European FDA, methods test international of requirements the meet to glassware of Manufacture Standard For Glassware request, please call please request, on available are etc keys spare and stopcocks other and these for Prices grained material Extraction apparatusforCoarse precipitate filtration filtration, Gaswashing,Crystalline be lightlylubricatedwithagoodqualitystopcockgreasebeforeuse General purposestopcockwithinterchangeableborosilicateglasskeyandbarrel.Must Glass KeyStopcock or contamination. not stickorseize.Doesneedgreaseandthereforeavoidsproblemofblockage This stopcockhasahighlypolishedborosilicateglassbarrelwithPTFEkeywhichwill PTFE KeyStopcock control. Vacuum capabilityto10 The RotaflostopcockcombinesanallborosilicateglassandPTFEpathwaywithfineflow Rotaflo ® Stopcock +33 4 70 03 88 55 88 03 70 4 +33 +33 4 70 03 88 55 88 03 70 4 +33 55 88 03 70 4 +33 OOIYDSGAINPR IEEXAMPLEAPPLICATIONS PORESIZE DESIGNATION POROSITY 4 3 5 4 Torr. for more information more for T for a FREE quotation FREE a for information more for S 73NOMINAL ISO 4793 est Methods est 1 0-6mAnalyticalworkwithfine 10-16µm P16 1 0mUltrafinefiltration 4-10µm P10 4 6-4µ Analyticalfiltrationofmedium 16-40µm P40 precipitates grained material Extraction apparatusforfine precipitation. Finegasfiltration,

an elastomerPFA sealinglipwith FPM O-ring. of 250˚C.Theblackcapisglass-fibrereinforcedPPS,thehoseconnectorPFA with A thirdGL14connectorisavailable(FigE)whichhasamaximumoperatingtemperature temperature is200˚C. is glassfilledPTFE,thehoseconnectorpurePTFEwithaO-ringsareviton.Maxoperating which demandbetterchemicalresistanceandahighertemperaturerange.Thegreencap An alternativehighperformanceGL14hoseconnector(FigD)isavailableforapplications connector ispolypropyleneandthesealingwashersilicone. (Fig C)hasamaximumoperatingtemperatureof140˚C.ThecapisPBTP, thehose If youhaveusedQuickfit So, whichonetochoose,SQ13orGL14?Theyareactuallyalmostidentical! is, inturn,screwedontothethread–amuchsaferalternative. connectors. Therubbertubingispushedontotheplastichoseconnectorand SQ13 andGL14 when connectingorremovingthetubing. option isconsideredtobetheleastsafedueriskofinjuryglassbreakages This traditionalstyleallowsrubbertubingtobepusheddirectlyontotheglassware. Olive SQ13 screwthreadorGL14screwthread. Radleys glasswareistypicallyofferedwithachoiceofsidearmtypes:11mm olive, Sidearm SelectionGuide from continentalEuropee.g.Buchi Alternatively, youmaybefamiliarwiththeGL14type(Fig3),whichisusedonequipment hose connectorispurePTFEandtheO-ringsareviton.Maxoperatingtemperature200˚C. chemical resistanceandahighertemperaturerange.TheredcapisglassfilledPTFE,the An alternativehoseconnector(FigB)isavailableforapplicationswhichdemandbetter polypropylene, thehoseconnectorispolyacetalandO-ringsaresilicone. (Fig A)hasamaximumoperatingtemperatureof80˚C.Thecapismadefromglassfilled which iscommonlysuppliedonallQuickfitcondensers.ThestandardSQ13hoseconnector • • • • • • • • consider thefollowing... To Handled withcareyourlaboratoryglasswarewilllastalifetime... Safe HandlingofLaboratoryGlassware For more information on any aspects of glassware safety please call please safety glassware of aspects any on information more For • • • • • • The useofRodaviss unsuccessful pleasecallforadvice. A gentletappingorrockingofthetwosidesjointcanoftenreleasethem.Ifyouare If jointedglasswarebecomesstuckorfrozen,donotuseexcessiveforcetofreethejoints. connectors wherepossible. Never forcetubingontosidearms.UsetheGLorSQplasticscrewthreadtypehose A prone toprematurefailure. Never heatglasswarewithscratches,chipsorcracks,assuchdefectscanmaketheglass defects cansignificantlyaffect thestrengthofyourglassware. Check allglasswarefordamage,suchasscratches,chipsorcracks.Eventhesmallest Use safetyshielding,plasticnettingorcoatingstoprotectyouandyourglassware. lab coatsetcwhenundertakingexperimentsusingglassware. Always weartheappropriateprotectiveclothinge.g.cutresistantgloves,eyeprotection, is doneinaslowanduniformmanner. should alwaysbetakenwhenheatingabove150˚Ctoensurethatandcooling The maximumrecommendedworkingtemperatureforborosilicateglassis500˚C.Care temperature changesorthermalshock. Whilst borosilicateglasshasexcellentheatresistance,itshouldnotbesubjectedtosudden When heatingorautoclavingglassbottlesalwaysslightlyloosenthecaptoallowventing. hot phosphoricacidandstrongalkaliesshouldbeavoided. Whilst borosilicateglasswareoffers superiorchemicalresistance,theuse ofhydrofluoricacid, Do notliftorcarryglasswarebytherimsidearm,alwayssupportmainbody. Always heatglasswareslowlyandevenly. ensure themaximumlifeforyourglasswareandtoprotectusersfrominjuryplease void subjectinglaboratoryglasswaretopressureorvacuum(Seepage567forfurtheradvice). - Themostbasicformofconnection(seeFig1).Alsoknownasanippleorhosebarb. - arebothscrewthreads,whichintendedforusewithplastichose ® t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] safety jointswillpreventfrozen(pleaseseepages570&571). ® apparatus, thenyoumayalreadybefamiliarwithSQ13(Fig2) ® or Schott(Duran ® ). ThisstandardGL14hoseconnector Specialist ScientificGlassblowing +33 4 70 03 88 55 88 03 70 4 +33 3 2 1 C B A E D

7 GENERAL GLASSBLOWING INTRODUCTION 8 GENERAL GLASSBLOWING INTRODUCTION Rodaviss Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com ® Interchangeable GlassJoints Remains SecureforTemperatures upto 200°C Grease Free-MaintainingSampleIntegrity Leakproof UnderVacuum andPressure Safe andExtremelyStrong Rodaviss Convenient SealingCaps Will NotStickorJam Competitively Priced Interchangeable glass joint... The alternative ® t: +33470038855f: 470038260e:[email protected]@interchim.fr The combinationofascrewthreadconnectingcapandO-ring Leak-proof undervacuumandpressure jammed, withouttheneedtoapplydangerouspressure. allows youtofreethetwopartsofjointshouldtheybecome male jointandaplasticlooseningring, a smallglassrimontheoutsideof 'frozen' together. Thecombination of and femalejointsfrombecoming jam methodwhichpreventsthemale Rodaviss incorporatesapatentednon- W safety features. the benefitsofRodavissmany laboratory glasswaregivingyouall will haveacomprehensiverangeof new glassware,andverysoonyou all youroldglassware.SimplyspecifyRodavissjointson means thattochangeRodaviss,youdonothavethrowaway will fitperfectlywithanyordinaryglassjointofequalsize.This ground glassjoints.BoththeconeandsocketjointsofRodaviss 0-504/05m 6m 10 10 165mm 10 150mm 50mm 10 140mm 40mm 10 45/40 135mm 34mm Rodaviss 310ConnectingCap 10 34/35 125mm 30mm 29/32 300-4540 125mm 24mm 24/29 300-3435 10 20mm 19/26 300-2932 10 150mm 14/23 300-2429 10 140mm 50mm 300-1926 10 140mm 38mm 300-1423 10 45/40 130mm 34mm Rodaviss 300HeavyWall Sockets 10 34/35 127mm 28mm 29/32 400-4540 120mm 22mm 24/29 400-3435 18mm 19/26 400-2932 14/23 400-2429 400-1926 400-1423 Rodaviss 400MediumWall Sockets 1-4314/23 310-1423 A OSZ DLNT IEPRP A OSZ DLNT IEPRP A OSZ IEPERPK SIZE SIZE CAT NO PERPK SIZE LENGTH OD SIZE CAT NO PERPK SIZE LENGTH OD SIZE CAT NO 1-9619/26 310-1926 1-4924/29 310-2429 1-9229/32 310-2932 1-50 45/40 34/35 310-4540 310-3435 ill notstickorjam ON UETTLPC PRICE PACK TOTAL TUBE JOINT sample integrity. neither, maintainingabsolute Rodaviss patenteddesignrequires a goodsealandtopreventjamming,but either greaseoraPTFEsleevetoensure Ordinary groundglassjointsrequire sample integrity Grease free,maintaining without greaseorPTFEsurfacing. pressure, remainingleak-proofeven seal, idealforworkinvolvingvacuumor gives theRodavissjointaperfectairtight t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] able withordinary1:10tapered Rodaviss iscompletelyinterchange- Interchangeable to 200˚Candiscompetitivelypriced. is extremelystrong,canbeusedup ground joints,willnotstickorjam, able withstandard1:10tapered pressure, greasefree,interchange- Rodaviss issafeundervacuumor for connectinglaboratoryglassware. extra-safe borosilicateglassjoint Rodaviss isarevolutionary, new, Rodaviss thealternativejoint... 10 10 10 10 10 10 2-504/04m 6m 10 10 165mm 10 140mm 40mm 10 140mm 32mm 10 45/40 135mm 26mm 10 34/35 128mm 22mm 425-4540 29/32 125mm 16mm 10 425-3435 24/29 13mm 10 425-2932 19/26 155mm 10 425-2429 14/23 140mm 40mm 10 425-1926 135mm 32mm 10 425-1423 45/40 125mm 26mm 10 34/35 130mm 22mm 420-4540 115mm 29/32 16mm 420-3435 24/29 13mm 420-2932 19/26 420-2429 14/23 420-1926 420-1423 2-4314/23 322-1423 Rodaviss 425MediumWall DripCones 2-9619/26 322-1926 Rodaviss 322SealingCap(withPTFEface) Rodaviss 420MediumWall Cones 2-4924/29 322-2429 2-9229/32 322-2932 2-5045/40 34/35 322-4540 322-3435 Rodaviss ON UETTLPC PRICE PACK TOTAL TUBE JOINT to makesuchconversionsduringtherepairofyourglassware. incorporate Rodavissjoints.Itcanbeparticularlycosteffective We Get youroldglasswaremodified... socket toclosetheapparatusorvessel. A Rodavisssealingcapmaythenbescrewedontothethreaded apart. Thissystemwillreleaseeventhemost'frozen'joints. cap backontothelooseningring,whichwillpushjointseasily because thesurfacesarejammed,simplyunscrewconnecting on themalejoint.Ineventofanydifficulty inundoingthejoint Clip thelooseningringbetweenconnectingcapandglassrim O-ring, thusensuringaperfectseal,andgoodrigidassembly. of thejoint,screwdownconnectingcaptocompress through theO-ring.Aftermatchingupconeandsockethalves Place themaleconethroughconnectingcap,andthen Rodaviss assembly... air-tight seal. an internalPTFEfacefor Rodaviss sealingcapshave screwthread sealingcap.All your vesselwithaRodaviss you toeasilyandsafelyseal Rodaviss femalejointenables design ontheoutsideof The convenientscrewthread Convenient SealingCap particularly usefulforlargerapparatusassemblies. available intwowallthicknesses,withtheheavyoptionbeing there isnoneedforadditionallugsorclips.Rodavisssocketsare and supportsasconventionalconnectingmethods.WithRodaviss stability andrigidity, thusreducingtheneedforasmanyclamps Because Rodavissjointsaresosecure,theyimproveapparatus Extremely Strong 420 &425 Rodaviss Male Joint will bepleasedtoquotemodifyyourexistingglassware ® Rim Glass Interchangeable GlassJoints Ring Rodaviss435 Loosening Connecting Cap Rodaviss 310 10 10 10 10 10 10 1-453/510 312-4540 312-3435 34/35 312 2932 10 312-2429 312-1926 312-1423 14/23 31 10 31 31 311-2429 24/29 31 31 3-431/310 435-1423 14/23 3-961/610 435-1926 19/26 3-492/910 435-2429 24/29 Rodaviss 312Viton O-ring Rodaviss 311 NitrileO-Rings 3-50 54 10 10 45/40 34/35 10 435-4540 435-3435 435-2932 29/32 Rodaviss 435LooseningRing 1-4540 1-3435 1-2932 1-1926 1-1423 Rodaviss 311 &312 O-ring Rodaviss 400&300 Female Joint ON AKPRICE PACK JOINT 54 10 10 45/40 10 10 29/32 24/29 19/26 10 10 10 45/40 34/35 10 29/32 10 19/26 14/23 Rodaviss 322 Sealing Cap www.interchim.com

9 GENERAL GLASSBLOWING INTRODUCTION 10 REACTION SYSTEMS Reaction SystemExamples Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com • • • • • • • • • Reaction Vessel Accessories • • • • • • • • • • • • Scope ofourservices... in projectdevelopment. of highlyskilledglasstechnologistsandproductspecialistshavemanyyearsexperience a singlebenchtopvessel,wewillhappytoassistinallaspectsofthedesignstage.Ourteam cooperation withourcustomers.Whetheryourequirealargemulti-vesselprocesssystemor The vastmajorityofthereactionvesselsthatwemanufacturearecustomdesignedinclose Custom madereactionsystems-toyourspecificdesign... Custom ReactionVessels &Systems • • • • • • • • • • technical support... FREE technical for or Options Vessel Reaction service. design and on specialists our contact please Therefore limitless. almost is systems vessel for variations design and features different of combination The want... you what us tell Simply Please call Tel: call Please help. can we repaired or modified want you glassware of piece existing an have you If repair? or modification vessel a Need NEW Email: on us contact please Thermoregulator and system your selecting with advice For control. temperature offerthey Thermoregulator appropriate an affordable.precise with and conjunction in used When easier much system appropriate an of selection the make reactors laboratory standard These reactors mounted floor Litre 20 large to systems, benchtop We Insulated hosesandconnectors. Ancillary equipment;temperature,pHcontrolandmonitoring,pumps,balances,leveletc. Acrylic andpolycarbonatesafetyshields. Integral baffles; glass,stainlesssteelorPTFE. Overhead stirrers;electrical,airpoweredandEx-rated. Stirrer guides,shafts,propellers,connectors,fittingsandadapters(standardcustom). cupboard installations,includingcustommetalworkdesignandfabrication. A comprehensivedesignserviceforsupportstructuressinglevesselsorcomplexfume Huber Thermoregulators;microprocessortemperaturecontrolfrom-120˚Cto400˚C. Lids withanynumberandstyleofports. sockets, processcouplingsetc. A widerangeofvesselsidearmoptions;olives,SQandGLscrewthreadfittings,Rodaviss V Cylindrical orsphericalvesselshapes,tallsquat. New splitjacketedvessels. With orwithoutstopcockdrainoutlet. Optional vacuumjacket. With orwithoutcooling/heatingjacket. V V Single jacketedreactionvesselsto50litre. Heating/Cooling Thermoregulators;supply, servicingandsupport Scrubbers, condensersanddistillationassemblies. Overhead stirrers;electrical,airpoweredandEx-rated. Benchtop stands/supports. Photochemical andUVreactors. Fermenters andbioreactors. Solid phasereactorswithsinters. Multi-reactor systemsforparallelsynthesis. Custom madePTFEcomponents;lids,probes,adaptersandconnectors. Installation andtraining. Complex processframeworks. Software andsemi-automatedcontrol.

acuum jacketedreactionvesselsto10litre. essel graduations. essel sizesfrom100mlto50litres. are pleased to introduce a new range of standard Reaction Systems. From small 250ml small From Systems. Reaction standard of range new a introduce to pleased are [email protected] Standard Reaction Systems Reaction Standard +33 4 70 03 88 55 88 03 70 4 +33 t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] or Tel: 33 4 70 03 82 60 82 03 70 4 +33 Fax: or +33 4 70 03 88 55 88 03 70 4 +33 [email protected]

- see following pages following see - performance HuberThermoregulators. for a quotation a for Heating andcoolingviahigh for FREE technical advice technical FREE for Reaction SystemsIntroduction

11 REACTION SYSTEMS 12 REACTION SYSTEMS NEW Reaction Systems metal hosesdependingontheapplicationand rubber tubingormoresophisticatedinsulated Hoses andtheirconnectiontothevessel to preventsolventlossduring The stirrershaftisusedtoagitate A refluxcondenserisused via flexiblehoses.Thesemaybesimple Allows introductionofaninertgas Small BenchtopReactionSystems the reactionvesselcontents. The jacketsidearmsareconnected to monitororcontrolthetemperature or theapplicationofvacuum. a heatedreaction. to theheatingcoolingcirculator Stirrer ShaftandBlade The temperatureprobeisused any safetyconsiderations the stirrershaftandprovides Condenser a rotatingsealtoenableuse Gas PurgeAdapter The stirrerglandsupports Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com of thevesselcontents T under vacuumorair emperature Probe free conditions. Stirrer gland An overheadmotorwhich drives thestirrershaft. Stirrer Motor - 250mlto2Litre For technical advice on temperature on advice technical For range, pressure and also for help for also and pressure range, Thermoregulator and thermofluid and Thermoregulator for liquid/solidaddition,sampling,purging Email: in specifying the appropriate the specifying in stirrer orprobe(temperature,pH,UV, from atmosphere,withmultipleports for your application, please application, your for or spargingandtheconnectionofa A flangelidforsealingthevessel vessel butensuresthatallofthecontentsare socket lid.Athermofluid(typicallysiliconeoil) space stopcockprovideseasydrainingofthe The topflangeenablesconnectionofamulti a jacketforheatingorcooling.Azerodead stirred andkeptatthecorrecttemperature. or CLR(controlledlaboratoryreactor)with Securely supportsthevessel measured amountofliquid.Thepressure [email protected] A borosilicateglassreactionvessel equalising armensuresthattheflow This funnelallowstheadditionofa is pumpedthroughthejacketvia Graduated PressureEqualising particle sizing). and stirrermotor on eithersideofthestopcock. by adifference inpressure Support of liquidisnotaffected the jacketsidearms. Lid Dropping Funnel Vessel t: +33470038855f: 470038260e:[email protected]@interchim.fr NEW • • • •V Hose Options: Systems, buthosesneedtobeorderedseparately. Pleasecallforadvice. connector tothevessel.CouplingandhoseconnectionsareincludedinReaction backing flanges,plasticinserts,boltsandPTFEgasketisusedtoconnectthehose NW10 insulatedflexiblemetalhose.Acouplingconsistingofepoxycoated 10mm borestainlesssteelDN15/M16hoseconnectorwhichconnectstoaHuber Standard Systemcomprises: and anysafetyconsiderations sophisticated insulatedmetalhosesdependingontheapplication via flexiblehoses.Thesemaybesimplerubbertubingormore The jacketsidearmsareconnectedtotheheatingcoolingcirculator Hoses andtheirconnectiontothevessel • • Lid Options: and stainlesssteelquickreleaseclamp. Lids haveRodavisssocketsandSchottflangesforusewithanFEPcoatedo-ring Standard Systemcomprises: connection ofastirrerorprobe(temperature,pH,UV, particlesizing). ports forliquid/solidaddition,sampling,purgingorspargingandthe A flangelidforsealingthevesselfromatmosphere,withmultiple Lid • •V •V • V screwthread withsealingcapandPTFEhoseconnector. drain stopcockis15mmzerodead-space.Thebottomrun-off isfittedwithaGL18 steel quick-releaseclamp.ThejacketsidearmsaretangentialDN15flangesandthe V Standard Systemcomprises: silicone oil)ispumpedthroughthejacketviasidearms. flange enablesconnectionofamultisocketlid.Athermofluid(typically contents arestirredandkeptatthecorrecttemperature.Thetop provides easydrainingofthevesselbutensuresthatall with ajacketforheatingorcooling.Azerodeadspacestopcock A borosilicateglassreactionvesselorcontrolledlaboratoryreactor Vessel pressurised reactions. The vesselsaresuitableforuseundervacuum,butnot The temperaturerangeforthesesystemsis+200˚Cto-50˚C. •A Stirrer Options: IKA electricallydrivenstirrermotor. Standard Systemcomprises: An overheadmotorwhichdrivesthestirrershaft. Stirrer Motor • Probe Options: to provideasealthelidsocket. a Huberheatingcoolingcirculator. APTFEjointadapterandRodavissfittingsareused PTFE PT100temperatureprobe,whichisfittedwithaLemoplugforconnectionto Standard Systemcomprises: of thevesselcontents The temperatureprobeisusedtomonitororcontrolthe T essel Options: essels haveagroovedSchottflangeforusewithanFEPcoatedo-ringandstainless emperature Probe By usingLabworldsoftcontrollingsoftwareadegreeofautomationmaybeachieved. Stainless steelcouplingsareavailableforDN15sidearms. be specifiedforthevesseljacketedsidearm. hose connectorisrecommended.AheavywallRodaviss19/26socketshould If rubbertubingistousedwiththelargervesselsinthisrange,10mmborePTFE available. SQ13andGL14maybesuitableforsmallervessels. hose connectorsareobviouslysaferandseveraldifferent typesandsizesare hose barbsonthevesselandpushrubbertubingstraighttothese.Detachable spherical joints. e.g. ordinaryflatflanges,different typeofjointe.g.ordinarysocketsorgreaseless Any numberorconfigurationofneckstomatchtheapplication,different flangetype or position,indentedbaffles, graduation,thermofluidjacketdrain Different typeofflangee.g.ordinaryflatflange,different jacketsidearmtype process development. used whichcanbeconnectedtoadigitalthermometer, recorderordatalogger. If simplemonitoringisrequiredthenaType ‘K’PTFEtemperatureprobemaybe Air drivenmotorsareavailableforuseinhazardousareas. Custom madePTFElids. Different workingvolumee.g.1500ml arious otherformsofhoseconnectionareavailable.Themostbasicistohaveglass ariations inshape,e.g.squatorshapedtomimicalargerplantvesselfor acuum jacketforinsulationandtopreventfrostingduringcoolingbelowambient. vailable withanRS232interfacetomonitororcontrolstirringspeedandviscosity. Small BenchtopReactionSystems t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] - 250mlto2Litre • •A Dropping FunnelOptions: the topoffunnel. to thevesselviaaswanneckadapter. APTFEfacedRodavisssealingcapseals Dropping funnelwithRodavissjointsandaPTFEkeystopcock.Itisconnected Standard Systemcomprises: affected byadifference inpressureoneithersideofthestopcock. The pressureequalisingarmensuresthattheflowofliquidisnot This funnelallowstheadditionofameasuredamountliquid. Graduated PressureEqualisingDroppingFunnel •V Stirrer GlandOptions: are providedtoconnectcentrallidsocket. PTFE stirrerguideshaveaninternalprecisionglassandseal.Rodavissfittings Standard Systemcomprises: seal toenableuseundervacuumorairfreeconditions. The stirrerglandsupportstheshaftandprovidesarotating Stirrer Gland • • Stirrer Shaft&BladeOptions: A PTFEanchororremovablebladestirrerdependingonthevesselsize. Standard Systemcomprises: The stirrershaftisusedtoagitatethereactionvesselcontents. Stirrer Shaft&Blade • • • Support Options: clamp andstirrermotorareheldinplacewithheavydutybossheads. lower supportringandstainlesssteeltopclamp.Thering, A SupportStandconsistingofasturdyH-shape base, 1000mmupright,Viton covered Standard Systemcomprises: Securely supportsthevesselandstirrermotor. Support * PTFE connector. Gas purgeadapterwithRodavisscone,PTFEstopcockandGL14*screwthread Standard Systemcomprises: Allows introductionofaninertgasortheapplicationvacuum. Gas PurgeAdapter • • Condenser Options: * angle adaptercompletewithGL14PTFEhoseconnector. provide thecoolingwaterconnection.Thetopofcondenserisfittedwitharight A jacketedcoilrefluxcondenserwithRodavissjoints.GL14*plastichoseadapters Standard Systemcomprises: Used topreventsolventlossduringaheatedreaction. Condenser SQ13 screwthreadmaybefittedifpreferred.Seepage569forfurtherinformation. 0161LitreJacketedReactionSystem 500116 500mlJacketedReactionSystem 500114 250mlJacketedReactionSystem DESCRIPTION 500112 CAT NO 0182LitreJacketedReactionSystem 500118 stirrer guidesforusewithprecisiongroundglassshafts development work.Custommadestirrersofanyshapeormaterialareavailable Glass isparticularlysuitableforthemanufactureofscaledownstirrersprocess Different materialse.g.glass,PTFEcoatedsteel,stainlesssteelorhastelloy. which maybere-positioned. Different shapesofbladee.g.propellor, turbineorretreatcurve,detachableblades Custom madeframeworksmaysupportmultiplevessels. vessels tobeconnectedanexistinglaboratoryframework. Clamps, supportringsandbossheadsareavailableseparatelytoenablesmall Other typesofcondenserareavailablee.g.Liebigordoublesurface. Dropping funnelsareavailableungraduated,orwithoutthepressureequalisingarm. Polycarbonate oracrylicsafetyscreensmaybeeasilyfitted. Distillation apparatusmaybefittedtoenablesolventevaporationandcollection. arious othertypesofglandareavailableincludingmagneticcoupling,all-glass Rotaflo stopcockmaybeusedifamorecontrolledrateofadditionisrequired. 100ml DroppingFunnel DN60 LidFlange,IKARW16 BasicOverheadStirrer, DN15 Jacketsidearm,M16HoseConnection 50ml DroppingFunnel DN60 LidFlange,IKARW16 BasicOverheadStirrer, DN15 Jacketsidearm,M16HoseConnection 250ml DroppingFunnel DN100 LidFlange,IKARW16 BasicOverheadStirrer, DN15 Jacketsidearm,M16HoseConnection 500ml DroppingFunnel DN100 LidFlange,IKARW16 BasicOverheadStirrer, DN15 Jacketsidearm,M16HoseConnection SQ13 screwthreadmaybefittedifpreferred.Seepage569forfurtherinformation. Reaction Systems KQYPRICEEACH PK QTY 1 1 1 1 www.interchim.com 13 REACTION SYSTEMS 14 REACTION SYSTEMS NEW Reaction Systems hoses. Thesemaybesimplerubbertubing to theheatingcoolingcirculatorviaflexible Hoses andtheirconnectiontovessel or moresophisticatedinsulatedmetal hoses dependingontheapplication The jacketsidearmsareconnected For technical advice on temperature on advice technical For to preventsolventlossduring range, pressure and also for help for also and pressure range, Thermoregulator and thermofluid and Thermoregulator and anysafetyconsiderations Intermediate BenchtopReactionSystems A refluxcondenserisused The stirrershaftisusedtoagitate Email: in specifying the appropriate the specifying in for your application, please application, your for the reactionvesselcontents a heatedreaction Stirrer ShaftandBlade The stirrerglandsupports the stirrershaft,provides a rotatingsealtoenable Condenser Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com or airfreeconditions use undervacuum [email protected] Stirrer Gland application ofvacuum of aninertgasorthe Gas PurgeAdapter Allows introduction

An overheadmotorwhich drives thestirrershaft Stirrer Motor - 2to5Litres Securely supportsthevessel a sturdyframework and stirrermotorin Support at thecorrecttemperature.Thetopflangeenables (typically siliconeoil)ispumpedthroughthejacket connection ofamultisocketlid.Athermofluid The pressureequalisingarmensures easy drainingofthevesselbutensuresthat by adifference inpressureoneither that theflowofliquidisnotaffected (temperature, pH,UV, particlesizing) from atmosphere,withmultipleports of ameasuredamountliquid. A zerodeadspacestopcockprovides all ofthecontentsarestirredandkept or CLR(controlledlaboratoryreactor) This funnelallowstheaddition for liquid/solidaddition,sampling, Equalising DroppingFunnel A flangelidforsealingthevessel A borosilicateglassreactionvessel with ajacketforheatingorcooling. connection ofastirrerorprobe purging orspargingandthe Graduated Pressure side ofthestopcock via thejacketsidearms or controlthetemperature Vessel Lid The temperatureprobe of thevesselcontents T emperature Probe is usedtomonitor NEW * • • Hose Options: Systems, buthosesneedtobeorderedseparately. Pleasecallforadvice. connector tothevessel.CouplingandhoseconnectionsareincludedinReaction backing flanges,plasticinserts,boltsandPTFEgasket,isusedtoconnectthehose NW10 insulatedflexiblemetalhose.Acoupling,consistingofepoxycoated 10mm borestainlesssteelDN15/M16hoseconnectorwhichconnectstoaHuber Standard Systemcomprises: and anysafetyconsiderations sophisticated insulatedmetalhosesdependingontheapplication via flexiblehoses.Thesemaybesimplerubbertubingormore The jacketsidearmsareconnectedtotheheatingcoolingcirculator Hoses andtheirconnectiontovessel • • Lid Options: coated o-ringandstainlesssteelquickreleaseclamp. SchottflangesforusewithanFEP Reaction systemlidshaveRodavisssocketsand Standard Systemcomprises: connection ofastirrerorprobe(temperature,pH,UV, particlesizing). ports forliquid/solidaddition,sampling,purgingorspargingandthe A flangelidforsealingthevesselfromatmosphere,withmultiple Lid •A • V catchpot andPTFEhoseconnector. a 25mmzerodeadspacedrainstopcockandRodaviss24/29heavywallsocket, screwthread onrun-off withsealingcapandPTFEhoseconnector. 5litrevesselhas flanges. 2litrevesselhasa15mmzerodeadspacedrainstopcockandGL18 and stainlesssteelquick-releaseclamp.ThejacketsidearmsaretangentialDN15 V Standard Systemcomprises: silicone oil)ispumpedthroughthejacketviasidearms. flange enablesconnectionofamultisocketlid.Athermofluid(typically contents arestirredandkeptatthecorrecttemperature.Thetop provides easydrainingofthevesselbutensuresthatall with ajacketforheatingorcooling.Azerodeadspacestopcock A borosilicateglassreactionvesselorcontrolledlaboratoryreactor Vessel pressurised reactions. The vesselsaresuitableforuseundervacuum,butnot The temperaturerangeforthesesystemsis+200˚Cto-50˚C. • • Stirrer Options: IKA electricallydrivenstirrermotors. Standard Systemcomprises: An overheadmotorwhichdrivesthestirrershaft. Stirrer Motor • Probe Options: to provideasealthelidsocket. a Huberheatingcoolingcirculator. APTFEjointadapterandRodavissfittingsareused PTFE PT100temperatureprobe,whichisfittedwithaLemoplugforconnectionto Standard Systemcomprises: of thevesselcontents The temperatureprobeisusedtomonitororcontrolthe T Please notethatsomecirculatorsrequireahighflowrate,particularlyduringcooling,and10mmborewouldbeinsufficient. essel Options: essels haveagroovedSchottflangeforusewithanFEPcoatedorsiliconeO-ring emperature Probe 19/26 socketshouldbespecifiedforthevesseljacketsidearm. hose connectorcataloguenumber451010isrecommended.AheavywallRodaviss If rubbertubingandasimplehoseconnectoraretobeused,the10mm*borePTFE spherical joints. e.g. ordinaryflatflanges,different typeofjointe.g.ordinarysocketsorgreaseless Any numberorconfigurationofneckstomatchtheapplication,different flangetype or position,indentedbaffles, graduationsandthermofluidjacketdrain. to mimicalargerplantvesselforprocessdevelopment. frosting duringcoolingbelowambient.Variations inshape,e.g.squatorshaped Different workingvolumee.g.2.2litre,vacuumjacketforinsulationandtoprevent of automationmaybeachieved. speed andviscosity. ByusingLabworldsoftcontrollingsoftwareadegree IKA stirrermotorsareavailablewithRS232interfacetomonitororcontrolstirring used whichcanbeconnectedtoadigitalthermometer, recorderordatalogger. If simplemonitoringisrequiredthenaType ‘K’PTFEtemperatureprobemaybe Stainless SteelcouplingsareavailableforDN15sidearms. Custom madePTFElids. Air drivenmotorsareavailableforuseinhazardousareas. different typeofflangee.g.ordinaryflatflange,different jacketsidearmtype Intermediate BenchtopReactionSystems t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected]

• •A Dropping FunnelOptions: top ofthefunnel. to thevesselviaaswanneckadapter. APTFEfacedRodavisssealingcapsealsthe A droppingfunnelwhichhasRodavissjointsandaPTFEkeystopcock.Itisconnected Standard Systemincludes: affected byadifference inpressureoneithersideofthestopcock. The pressureequalisingarmensuresthattheflowofliquidisnot This funnelallowstheadditionofameasuredamountliquid. Graduated PressureEqualisingDroppingFunnel •V Stirrer GlandOptions: seal. Rodavissfittingsareprovidedtoconnectcentrallidsocket. PTFE stirrerguidesasstandard.Thesehaveaninternalprecisionglassand Standard Systemincludes: to enableuseundervacuumorairfreeconditions. The stirrerglandsupportstheshaft,providesarotatingseal Stirrer Gland • • • • Stirrer Shaft&BladeOptions: A PTFEanchorstirrer. Standard Systemcomprises: The stirrershaftisusedtoagitatethereactionvesselcontents. Stirrer Shaft&Blade • • • • Support Options: upright post. securely belowtheflange.Thestirrermotorissupportedfromanextendedcentral cushioned heavy-dutysupportringandasturdytopclampholdsthevessel 316 stainlesssteeltubingandpowdercoatedclamps.ThevesselsitsonaViton Supported withinabenchtopframeworkconstructedfromheavygauge27mmdiameter Standard Systemcomprises: Securely supportsthevesselandstirrermotor. Support * PTFE connector. Gas purgeadapterwithRodavisscone,PTFEstopcockandGL14*screwthread Standard Systemincludes: Allows introductionofaninertgasortheapplicationvacuum. Gas PurgeAdapter • • Condenser Options: * angle adaptercompletewithGL14*PTFEhoseconnector. provide thecoolingwaterconnection.Thetopofcondenserisfittedwitharight A jacketedcoilrefluxcondenserwithRodavissjoints.GL14*plastichoseadapters Standard Systemincludes: Used topreventsolventlossduringaheatedreaction. Condenser SQ13 screwthreadmaybefittedifpreferred.Seepage569forfurtherinformation. 0282LitreJacketedReactionSystem DESCRIPTION 500218 CAT NO 0145LitreJacketedReactionSystem 500124 Dropping funnelsareavailableungraduated,orwithoutthepressureequalisingarm. stirrer guidesforusewithprecisiongroundglassshafts. development work. Glass isparticularlysuitableforthemanufactureofscaledownstirrersprocess Different materialse.g.glass,PTFEcoatedsteel,stainlesssteelorhastelloy. Polycarbonate oracrylicsafetyscreensmaybeeasilyfitted. receiver vesselsorseparators. Custom madeframeworksmaysupportmultiplevesselse.g.feedervessels, Stainless steeldriptrays/bundsmaybefittedbelowthevessel. or aparticularvesselheightrequirement. Custom frameworkscanbedesignedandmanufacturedtosuitrestrictedspace Custom madestirrersofanyshapeormaterialareavailable Detachable bladeswhichmayberepositioned. Different shapesofbladee.g.propeller, turbineorretreatcurve. Distillation apparatusmaybefittedtoenablesolventevaporationandcollection. Other typesofcondenserareavailablee.g.Liebigordoublesurface. arious othertypesofglandareavailableincludingmagneticcouplings,orall-glass Rotaflo stopcockmaybeusedifamorecontrolledrateofadditionisrequired. - 2to5Litres 500ml DroppingFunnel DN150 LidFlange,IKARW16 BasicOverheadStirrer DN15 Jacketsidearm,M16HoseConnection, 500ml DroppingFunnel DN150 LidFlange,IKARW16 BasicOverheadStirrer DN15 Jacketsidearm,M16HoseConnection, SQ13 screwthreadmaybefittedifpreferred.Seepage569forfurtherinformation. Reaction Systems KQYPRICEEACH PK QTY 1 1 15 REACTION SYSTEMS t: +33470038855f: 470038260e:[email protected]@interchim.fr

16 REACTION SYSTEMS NEW Reaction Systems (typically siliconeoil)ispumpedthroughthejacket that allofthecontentsarestirredandkeptat provides easydrainingofthevesselbutensures heating orcooling.Azerodeadspacestopcock (controlled laboratoryreactor)withajacketfor connection ofamultisocketlid.Athermofluid For technical advice on temperature on advice technical For correct temperature.Thetopflangeenables A borosilicateglassreactionvesselorCLR range, pressure and also for help for also and pressure range, Thermoregulator and thermofluid and Thermoregulator Email: Large MobileReactionSystems in specifying the appropriate the specifying in for your application, please application, your for via thejacketsidearms. The stirrerglandsupportsthe Allows introductionofaninertgas shaft andprovidesarotatingseal Interchim 211 bis avenue JF Kennedy - BP1140 - 03100 Montluçon - Franc - Montluçon 03100 - BP1140 - Kennedy JF avenue bis 211 Interchim to preventsolventlossduring An overheadmotorwhich [email protected] or theapplicationofvacuum. to enableuseundervacuum A refluxcondenserisused drives thestirrershaft. or airfreeconditions. Vessel Gas PurgeAdapter a heatedreaction. Stirrer Motor Stirrer Gland Condenser

- 10to20Litres or probe(temperature,pH,UV, particlesizing). or spargingandtheconnectionofastirrer The stirrershaftisusedtoagitate for liquid/solidaddition,sampling,purging the reactionvesselcontents. from atmosphere,withmultipleports flow ofliquidisnotaffected byadifference A flangelidforsealingthevessel depending ontheapplicationandanysafety or moresophisticatedinsulatedmetalhoses pressure equalisingarmensuresthatthe Stirrer BladeandShaft hoses. Thesemaybesimplerubbertubing to theheatingcoolingcirculatorviaflexible Hoses andtheirconnectiontovessel of ameasuredamountliquid.The e e Graduated PressureEqualising The jacketsidearmsareconnected The temperatureprobeisused This funnelallowstheaddition www.interchim.com in pressureoneitherside to monitororcontrolthe T the vesselandstirrermotor Dropping Funnel temperature ofthe emperature Probe of thestopcock. in amobileframework. vessel contents Lid considerations Securely supports Support www.interchim.com •A •V •V • V socket, acatchpotandPTFEhoseconnector. 25mm zerodead-space.Thebottomrun-off isfittedwithaRodaviss24/29heavywall clamp. ThejacketsidearmsaretangentialDN25flangesandthedrainstopcockis A groovedSchottflangeforusewithanFEPo-ringandstainlesssteelquick-release Standard Systemcomprises: silicone oil)ispumpedthroughthejacketviasidearms. flange enablesconnectionofamultisocketlid.Athermofluid(typically contents arestirredandkeptatthecorrecttemperature.Thetop provides easydrainingofthevessel,whilstensuringthatall with ajacketforheatingorcooling.Azerodeadspacestopcock A borosilicateglassreactionvesselorcontrolledlaboratoryreactor Vessel pressurised reactions. The vesselsaresuitableforuseundervacuum,butnot The temperaturerangeforthesesystemsis+200˚Cto-50˚C. • • Stirrer Options: IKA electricallydrivenstirrermotors. Standard Systemcomprises: An overheadmotorwhichdrivesthestirrershaft. Stirrer Motor • Probe Options: to provideasealthelidsocket. a Huberheatingcoolingcirculator. APTFEjointadapterandRodavissfittingsareused PTFE pt100temperatureprobe,whichisfittedwithaLemoplugforconnectionto Standard Systemcomprises: of thevesselcontents. The temperatureprobeisusedtomonitororcontrolthe T * • • Hose Options: included inReactionSystems,buthosesneedtobeorderedseparately. to connectthehoseconnectorvessel.Couplingandconnectionsare of epoxycoatedmetalbackingflanges,plasticinserts,boltsandPTFEgasket,isused which connectstoaHuberNW20insulatedflexiblemetalhose.Acoupling,consisting Large reactionsystemsusea20mmborestainlesssteelDN25/M30hoseconnector Standard Systemcomprises: and anysafetyconsiderations sophisticated insulatedmetalhosesdependingontheapplication via flexiblehoses.Thesemaybesimplerubbertubingormore The jacketsidearmsareconnectedtotheheatingcoolingcirculator Hoses andtheirconnectiontothevessel • • Lid Options: stainless steelquickreleaseclamp. Lids haveRodavisssocketsandSchottflangesforusewithanFEPcoatedO-ring Standard Systemcomprises: connection ofastirrerorprobe(temperature,pH,UV, particlesizing). ports forliquid/solidaddition,sampling,purgingorspargingandthe A flangelidforsealingthevesselfromatmosphere,withmultiple Lid NEW Please notethatsomecirculatorsrequireahighflowrate,particularlyduringcooling,and10mmborewouldbeinsufficient. essel Options: emperature Probe or position,indentedbaffles, graduationsandthermofluidjacketdrain development. Air drivenmotorsareavailableforuseinhazardousareas. automation maybeachieved. speed andviscosity. ByusingLabworldsoftcontrollingsoftwareadegreeof IKA stirrermotorsareavailablewithRS232interfacetomonitororcontrolstirring used whichcanbeconnectedtoadigitalthermometer, recorderordatalogger. If simplemonitoringisrequiredthenaType ‘K’PTFEtemperatureprobemaybe Stainless SteelcouplingsareavailableforusewithDN25sidearms. socket shouldbespecifiedforthevesseljacketsidearm. hose connectorCatNo.451010isrecommended.AheavywallRodaviss19/26 If rubbertubingandasimplehoseconnectoraretobeused,the10mm*borePTFE Custom madePTFElids. spherical joints. e.g. ordinaryflatflanges,different typeofjointe.g.ordinarysocketsorgreaseless Any numberorconfigurationofneckstomatchtheapplication,different flangetype Different workingvolumee.g.12Litres ariations inshape,e.g.squatorshapedtomimicalargerplantvesselforprocess acuum jacketforinsulationandtopreventfrostingduringcoolingbelowambient. different typeofflangee.g.ordinaryflatflange,different jacketsidearmtype Large MobileReactionSystems t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] - 10to20Litres

• •A Dropping FunnelOptions: of thefunnel. the vesselviaaswanneckadapter. APTFEfacedRodavisssealingcapsealsthetop Dropping funnelwhichhasRodavissjointsandaPTFEkeystopcock.Itisconnectedto Standard Systemcomprises: by adifference inpressureoneithersideofthestopcock. pressure equalisingarmensuresthattheflowofliquidisnotaffected This funnelallowstheadditionofameasuredamountliquid.The Graduated PressureEqualisingDroppingFunnel •V Stirrer GlandOptions: Rodaviss fittingsareprovidedtoconnectcentrallidsocket. PTFE stirrerguidesasstandard.Thesehaveaninternalprecisionglassandseal. Standard Systemcomprises: seal toenableuseundervacuumorairfreeconditions. The stirrerglandsupportstheshaftandprovidesarotating Stirrer Gland • • • • Stirrer Shaft&BladeOptions: PTFE anchorstirrer. Standard Systemcomprises: The stirrershaftisusedtoagitatethereactionvesselcontents. Stirrer Shaft&Blade • • • • Support Options: upright post. securely belowtheflange.Thestirrermotorissupportedfromanextendedcentral cushioned heavy-dutysupportring,andasturdytopclampholdsthevessel two ofwhichhavebrakestoholdtheframeworkinposition.Thevesselsitsonaviton 316 stainlesssteeltubing,andpowdercoatedclamps.Fourcastorsprovidemobility, Supported withinamobileframeworkconstructedfromheavygauge27mmdiameter Standard Systemcomprises: Securely supportsthevesselandstirrermotorinamobileframework. Support with PTFEconnector. A gaspurgeadapterwithRodavisscone,PTFEstopcockandGL18screwthread Standard Systemcomprises: Allows introductionofaninertgasortheapplicationvacuum. Gas PurgeAdapter • • Condenser Options: angle adaptercompletewithGL18PTFEhoseconnector. provide thecoolingwaterconnection.Thetopofcondenserisfittedwitharight Large doublecoilrefluxcondenserwithRodavissjoints,GL18plastichoseadapters Standard Systemcomprises: reaction. A refluxcondenserisusedtopreventsolventlossduringaheated Condenser 01220000mlJacketedReactionSystem 500132 10000mlJacketedReactionSystem DESCRIPTION 500128 CAT NO Dropping funnelsareavailableungraduated,orwithoutthepressureequalisingarm. stirrer guidesforusewithprecisiongroundglassshafts. Custom madestirrersofanyshapeormaterialareavailable. development work. Glass isparticularlysuitableforthemanufactureofscaledownstirrersprocess Different materialse.g.glass,PTFEcoatedsteel,stainlesssteelorhastelloy. Detachable bladeswhichmayberepositioned. Different shapesofbladee.g.propeller, turbineorretreatcurve. Polycarbonate oracrylicsafetyscreensmaybeeasilyfitted. vessels orseparators. Custom madeframeworksmaysupportmultiplevesselse.g.feedervessels,receiver Stainless steeldriptrays/bundsmaybefittedbelowthevessel. or aparticularvesselheightrequirement. Custom frameworkscanbedesignedandmanufacturedtosuitrestrictedspace Distillation apparatusmaybefittedtoenablesolventevaporationandcollection. Other typesofcondenserareavailablee.g.Liebigordoublesurface. arious othertypesofglandareavailableincludingmagneticcouplings,orall-glass Rotaflo stopcockmaybeusedifamorecontrolledrateofadditionisrequired. 1000ml DroppingFunnel DN200 LidFlange,IKAEurostarPowerBasicOverheadStirrer DN25 Jacketsidearm,M30HoseConnection, 1000ml DroppingFunnel DN200 LidFlange,IKAEurostarDigitalOverheadStirrer DN25 Jacketsidearm,M30HoseConnection, Reaction Systems KQYPRICEEACH PK QTY 1 1 17 REACTION SYSTEMS 18 REACTION SYSTEMS Reaction Vessels G E A C I Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com D H F B other. relative toeach but nottoscale, proportion, Images in I H G F E D C B A space stopcock,tangentialDN15Jacketsidearms,heavywallRodaviss24/29socket on run-off. Jacketed ReactionVessel, withDN200ScottflangegrooveforO-ring,25mmzerodead space stopcock,tangentialDN15jacketsidearms,heavywallRodaviss24/29socketon run-off. Jacketed ReactionVessel, withDN200SchottflangegrooveforO-ring,25mmzerodead space stopcock,tangentialDN15jacketsidearms,heavywallRodaviss24/29socketonrun-off. Jacketed ReactionVessel, withDN200 SchottflangewithgrooveforO-ring,25mmzerodead space stopcock,tangentialDN15jacketsidearms,heavywallRodaviss24/29socketonrun-off. Jacketed ReactionVessel, withDN150 SchottflangewithgrooveforO-ring,25mmzerodead PTFE hoseconnectorandsealingscrewcap. zero deadspacestopcock,tangentialDN15jacketsidearms,GL18screwthreadonrun-off with Squat FormJacketedReactionVessel, withDN150SchottflangegrooveforO-ring,15mm space stopcock,tangentialDN15jacketsidearms,GL18screwthreadonrun-off. Jacketed ReactionVessel, withDN100 SchottflangewithgrooveforO-ring,15mmzerodead space stopcock,tangentialDN15jacketsidearms,GL18screwthreadonrun-off. Jacketed ReactionVessel, withDN100SchottflangegrooveforO-ring,15mmzerodead hose connectorandsealingscrewcap. dead spacestopcock,tangentialDN15jacketsidearms,GL18screwthreadonrun-off withPTFE Jacketed BorosilicateReactionVessel, withDN60SchottflangegrooveforO-ring,15mmzero hose connectorandsealingscrewcap. dead spacestopcock,tangentialDN15jacketsidearms,GL18screwthreadonrun-off withPTFE Jacketed BorosilicateReactionVessel, withDN60SchottflangegrooveforO-ring,15mmzero 379028 CAT NO 379024 CAT NO 380018 CAT NO 379018 CAT NO 379016 CAT NO 379014 CAT NO 379012 CAT NO 379034 CAT NO 379032 CAT NO 30 LitreReactionVessel 5 LitreReactionVessel 2 LitreSquatFormReactionVessel 20 LitreReactionVessel 2 LitreReactionVessel 1 LitreReactionVessel 500ml ReactionVessel 250ml ReactionVessel 10 LitreReactionVessel 10 LitreJacketedReactionVessel 5 LitreJacketedReactionVessel 2 LitreSquatJacketedReactionVessel 2 LitreJacketedReactionVessel 1 LitreJacketedReactionVessel 500ml JacketedReactionVessel 250ml JacketedReactionVessel 30 LitreJacketedReactionVessel 20 LitreJacketedReactionVessel DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION PK QTY PK QTY PK QTY PK QTY PK QTY PK QTY PK QTY PK QTY PK QTY 1 1 1 1 1 1 1 1 1 PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH O N M L K J NEW dead spacestopcock,tangentialDN15jacketsidearms,heavywallRodaviss24/29socketonrun-off. V dead spacestopcock,tangentialDN15jacketsidearms,heavywallRodaviss24/29socketonrun-off. V dead spacestopcock,tangentialDN15 V dead spacestopcock,tangentialDN15jacketsidearms,GL18screwthreadonrun-off. V space stopcock,tangentialDN15jacketsidearms,GL18screwthreadonrun-off. V space stopcock,tangentialDN15jacketsidearms,GL18screwthreadonrun-off. V acuum JacketedReactionVessel, with DN200SchottflangegrooveforO-ring.25mmzero acuum JacketedReactionVessel, with DN150SchottflangegrooveforO-ring,25mmzero acuum JacketedReactionVessel, withDN100SchottflangegrooveforO-ring,15mmzero acuum JacketedReactionVessel, withDN60SchottflangegrooveforO-ring,15mmzerodead acuum JacketedReactionVessel, withDN60SchottflangegrooveforO-ring,15mmzerodead acuum JacketedReactionVessel, withDN100SchottflangegrooveforO-ring,15mmzero 706D6 cotFag i 1xB19/26 4 DN60SchottFlangeLid DESCRIPTION 376006 CAT NO 379728 CAT NO 379724 CAT NO 379718 CAT NO 379716 CAT NO 379714 CAT NO 379712 CAT NO 700D20Sht lneLd6 3/51xB93 1xB29/32 1xB29/32 1xB29/32 1xB29/32 1xB34/35 1xB29/32 1xB29/32 1xB34/35 1xB29/32 6 1xB24/29 1xB34/35 1xB29/32 DN200SchottFlangeLid 5 1xB24/29 376020 1xB34/35 2xB19/26 DN200SchottFlangeLid 6 376021 1xB24/29 1xB19/26 DN150SchottFlangeLid 5 1xB24/29 376015 1xB19/26 DN150SchottFlangeLid 6 376016 DN100SchottFlangeLid 5 5 376000 DN100SchottFlangeLid DN60SchottFlangeLid 376001 376005 250ml Vacuum JacketedReactionVessel 1 LitreVacuum JacketedReactionVessel 5 LitreVacuum JacketedReactionVessel 500ml Vacuum JacketedReactionVessel 10 LitreVacuum JacketedReactionVessel 2 LitreVacuum JacketedReactionVessel Reaction Vessel Lids 10 LitreVacuum JacketedReactionVessel 5 LitreVacuum JacketedReactionVessel 2 LitreVacuum JacketedReactionVessel 1 LitreVacuum JacketedReactionVessel 500ml Vacuum JacketedReactionVessel 250ml Vacuum JacketedReactionVessel DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] O EK ETA IEVRIA IEAGE PRICEEACH SIDEANGLED SIDEVERTICAL CENTRAL NO. NECKS jacket - withRodavisssockets sidearms, GL18screwthreadonrun-off. 1/61xB45/40 1xB45/40 1 xB24/29 1 xB19/26 1xB45/40 1 xB19/26 1xB45/40 1 xB24/29 1 xB19/26 1xB29/32 1 xB19/26 1xB29/32 1 xB24/29 1 xB24/29 - - PK QTY PK QTY PK QTY PK QTY PK QTY PK QTY 1 1 1 1 1 1 3 xB19/26 4 xB19/26 PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH N L J Reaction Vessels O M K other. relative toeach but nottoscale, proportion, Images in 19 REACTION SYSTEMS 20 REACTION SYSTEMS Reaction Vessel Lids&Accessories B D A Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com C offer anyitemfromourrangewithordinarygroundjointsinsteadofRodavissatnoextracharge Whilst Rodavissjointsarecompletelyinterchangeablewithordinaryjoints,wewillbepleasedto If youpreferordinaryjoints... O-rings, LooseningRingsandConnectingCapsrequiredforassembly. All apparatuswhichincorporatesaRodavissconewillcomesuppliedwiththeappropriate Complete Rodavissconnections... 378115 378020 complete withallenkeysforpositioningandtighteningofsupports. support clamp(100mmID)areheldinpositionwithanodisedaluminiumbossheads.Stand issupplied platednickel steel upright. The (555250) lower support ring (7 blue acryliccoatedbasewithrubberfeet.Choosefroma700mmor1000mmx18mm diameter This benchtopstandissuitablefor250mlto2000mlreactionvessels.Itincorporatesa castiron, Benchtop SupportStand ReactionVessel Lids Custom D C B A 6. 5. 4. 3. 2. 1. Selecting thelidyourequireissimple:- 378120 378110 378015 378010 376445 376444 376443 376435 376434 376433 376425 376424 378105 CAT NO 378005 CAT NO 378620 378615 378610 378605 CAT NO 376423 376454 376453 CAT NO 555315 555310 CAT NO 378420 378415 378410 378405 CAT NO If youfinditeasier, simplysketchwhatyouwantandwewilldotherest. On receiptofyourinstructionswewillcontactyoutoconfirmrequirements. Attach thisinformationtoyourpurchaseorder. Select thepositionandangleofsockets. Select thenumberandsizeofsockets. Select thelidflangesize. Viton Silicone O-RingsforSchott FEP CoatedO-RingsforSchott Stainless SteelClampsforSchott ® O-Rings forSchott DN 200Viton O-Ring DN 150Viton O-Ring DN 200SiliconeO-Ring DN 100Viton O-Ring DN 150SiliconeO-Ring DN 100SiliconeO-Ring DN 200SchottO-ringFlange DN 200SchottO-ringFlange DN 200SchottO-ringFlange DN 150SchottO-ringFlange DN 150SchottO-ringFlange DN 150SchottO-ringFlange DN 100SchottO-ringFlange DN 100SchottO-ringFlange DN 60Viton O-Ring DN 60SiliconeO-Ring DN 200FEPO-Ring DN 150FEPO-Ring DN 100FEPO-Ring DN 60FEPO-Ring DN 100SchottO-ringFlange DN 60SchottO-ringFlange DN 60SchottO-ringFlange Complete supportstandwith1000mmupright Complete supportstandwith700mmupright DN 200SchottFastReleaseClamp DN 150SchottFastReleaseClamp DN 100SchottFastReleaseClamp DN 60SchottFastReleaseClamp DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION DESCRIPTION - forsmallreactionvessel ® Flanges ® - withRodaviss Flanges ® Flanges 6mm ID)and(555280)stainlesssteeltop ® Flanges NO. OFNECKS PK QTY PK QTY PK QTY PK QTY PK QTY 1 1 5 5 1 5 1 1 5 4 3 5 4 3 5 4 5 1 3 1 1 1 1 1 1 1 1 4 3 - fastrelease PRICE EACH PRICE EACH PRICE PRICE PRICE PRICE dimensions are12.5mmO.D.x200mmlong. This lowersupportringhasanopeningforeasyinsertionofthereactionvessel.Therod Lower SupportRing heat resistantcoveringandissuppliedwithitsownallenkeytotightensecuringbolt. stainless steeltherodis12.5mmO.D.x200mmlong.Theinsideofclampcushionedwith This singlepiecetopsupportclampfitsbelowtheflangeofreactionvessel.Madefrom Single PieceTop SupportClamp O.D. Overalllengthis525mm.Theringcushionedbyheatresistantcovering. This heavydutylowersupportringismadefrom316stainlesssteel.Therodsare27mm Jumbo cushioned withheatresistantcovering. stainless steelthesupportingrodis12.5mmO.D.x200mmlong.Theinsideofclamp This twopiecetopsupportclampfitsbelowtheflangeofsmallerreactionvessels.Madefrom316 NEW clamp iscushionedwithheatresistantcovering. Made from316stainlesssteelthesupportingrodis27mmO.D.x200mmlong.Theinsideof This twopieceheavydutytopsupportclampfitsbelowtheflangeoflargerreactionvessels. Jumbo NEW NEW lid isrestricted. Swan neckadapterisusedtoconnectdroppingfunnelreactionvesselwherespace aroundthe Allows applicationofvacuumorpurginganinertgas. 555220 *This itemisangledtosuitlids376005&376006notverticalaspicture. 1 313000* 1 312000 311000 CAT NO 10mm 10mm GL18 GL14 24/29 19/26 RodavissGasPurgeAdapter RodavissGasPurgeAdapter 386010 386000 CAT NO 76mm Lowersupportringforsmallvessels DESCRIPTION 555250 CAT NO 555280 CAT NO 555210 CAT NO Two piecetopsupportclamptofitDN60flange 555265 CAT NO 1 1 Two pieceheavydutytopsupportclamptofitDN200flange Two pieceheavydutytopsupportclamptofitDN150flange 555240 555230 CAT NO 520Lwrspotrn o ml esl 100mm Lowersupportringforsmallvessels 555260 555290 555300 T Rodaviss SwanNeckAdapter Rodaviss GasPurgeAdapter op SupportClamp ™ ™ Lower SupportRing T DESCRIPTION DESCRIPTION DESCRIPTION op SupportClamp Lower supportring,insideØ190mm oaisSa ekAatr19/26 29/32 24/29 Rodaviss SwanNeckAdapter Rodaviss SwanNeckAdapter Rodaviss SwanNeckAdapter Single piecetopsupportclamptofit100mmflange Lower supportring,insideØ120mm DESCRIPTION DESCRIPTION DESCRIPTION Single piecetopsupportclamptofit150mmflange Single piecetopsupportclamptofit200mmflange t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] - forsmallreactionvessels OESZ IER ITNP T PRICEEACH PKQTY PISTON SIDEARM CONE SIZE - forDN60Flange RING I.D. OESZ OKTSZ PKQTY SOCKETSIZE CONE SIZE - forlargereactionvessels - forlargereactionvessels - forreactionvessels SLOT I.D. - Rodavisscone&socket 38mm 44mm 19/26 24/29 24/29 PK QTY PK QTY PK QTY PK QTY 1 1 1 1 1 1 PK QTY 1 1 1 1 1 Reaction Vessel Accessories PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH PRICE EACH 21 REACTION SYSTEMS Reaction Vessel Accessories

NEW Rodaviss Cone Stopper Rodaviss cone stopper used to blank off unused reaction vessel lid ports. CAT NO DESCRIPTION CONE SIZE PKQTY PRICE EACH 480514 Rodaviss Glass Stopper 14/23 1 480519 Rodaviss Glass Stopper 19/26 1 480524 Rodaviss Glass Stopper 24/29 1 480529 Rodaviss Glass Stopper 29/32 1 480534 Rodaviss Glass Stopper 34/35 1 480545 Rodaviss Glass Stopper 45/40 1

NEW Right Angle Adapter - Rodaviss cone Right angle adapter with a Rodaviss 29/32 cone and GL 18 screwthread.

CAT NO DESCRIPTION PKQTY PRICE EACH 312804 Righi Angle Adapter 1

NEW DN Sidearm Hose Couplings These couplings securely clamp stainless steel DN hose connector to glass DN sidearm on vessel jacket. These couplings ensure boit load applied to joint is sufficient to make an effective seal, whilst not unduly stressing the glass. Couplings include: backing flanges, inserts, sprung boit assembly and PTFE gasket. CAT NO DESCRIPTION PKQTY PRICE EACH 555411 ON 15 Stainless Steel 1 555431 ON 25 Stainless Steel 1 555415 ON 15 Replacement PTFE Gasket 2 555435 ON 25 Replacement PTFE Gasket 2

NEW Stainless Steel DN Hose Connectors Stainless steel hose connectors for use with standard DN vessel sidearms and Huber flexible insulated metal hoses. See Huber Thermoregulators accessories page 470 for hose details.

CAT NO DESCRIPTION PKQTY PRICE EACH 555400 ON 15 to M16 x 1, cone seat, male 1 555401 ON 15 to M24 x 1.5, cane seat, male 555420 ON 25 to M30 x 1.5, cane seat, male 555440 ON 25 to M16 x 1 cane seat, male

NEW Stainless Steel Hose Connector - with drain valve This modified hose connector incorporates a drain valve to aid draining of thermofluid from reaction systems.

CAT NO DESCRIPTION PKQTY PRICE EACH 555405 DN15 to M16 1 555425 DN25 to M30 1

NEW Replacement Zero Dead Space Pistons - PTFE

CATNO DESCRIPTION PK QTY PRICE EACH A 380415 MK4 15mm Replacement Drain Valve Piston for Single Jacket Reaction Vessel 1 A B 380515 MK4 15mm Replacement Drain Valve Piston for Vacuum Jacket Reaction Vessel 1 C 380025/4 MK4 25mm Replacement Drain Valve Piston for Single Jacket Reaction Vessel 1 D 382025/4 MK4 25mm Replacement Drain Valve Piston for Vacuum Jacket Reaction Vessel 1

Please contact your distributor for details of replacement pistons for vessels purchased before B January 2005.

C

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22 Interchim 211 bis avenue JF Kennedy - BP1140 - 03100 Montluçon - France www.interchim.com a quotationtomeetyourexactrequirements.Pleasecallformoreinformation. advantage ofourin-housedesignservice,whichcanprovideyouwithspecificationsand Y Design Service... • • • • equipment (seepage619).Othercustomcomponentsinclude; Heavy dutyJumbosupportringsandclampsaredesignedtocomplimentourrangeofreaction Accessories for improvedprotectionandappearance. Jumbo clampsaresuppliedwithahardwearingblueglosspolyestercoating(asshownbelow) is connectedwithcastironJumboclamps.Hexagonalscrewslocktheclampsfirmlyinposition. Structures areassembledusingheavyduty27mmsteeltubing(316stainlesssteel)which Assembly and bossheadsarenotuptothejob. V Jumbo ou caneitherdesignandbuildyourownstructurebyorderingcomponentslistedbelow, ortake ersatile heavydutyframework,idealforwhenordinarylaboratoryretortstands,rods Custom clampsandsupports. Acrylic orpolycarbonatesafetyshields. Lightproof cabinetsforphotochemicalreactors. Stainless steelspilltrays. Plastic EndStopper Side OutletTee okn olrHo RoundBaseFlange Hook Locking Collar 90° Crossover 0 lo CornerwithCentre 90° Elbow ™ Support Systems t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] 2 SocketCross Stainless Steel Polished 316 with Centre Swivel atrwt wvlCastorwithSwivel Castor withSwivel Sleeve Joint hr e 3Way 90°Elbow Short Tee Reaction Vessel Accessories Long BaseFlange and Brake Long Tee S J upport umbo ™ 23 REACTION SYSTEMS 24 REACTION SYSTEMS Reaction Vessel Accessories is £4.34permetre.Pleaseputcablelength and Type Kflatpinminiplug.Extracable in metresaslastnumberCatNo.e.g. Supplied with1metreofcable 600.201.4 Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com for fourmetres. 1 toBS4937DIN43710andIEC581withaPTFEinsulatedcablePFA over-sheath. +300˚C. Probebodieshaveametalcoreforrigidity, butcanbebent.ThermocoupleisType K,Class Probes willnotcontaminateyoursampleandaresuitableforusefromcryogenictemperatures upto probes whichareinerttovirtuallyallchemicals,andhaveunsurpassednon-stickproperties. technology. Accuracy:+/-1.5˚Cor+/-0.004T˚C.Isostaticmoldingtechniquesareusedtomanufacture Solid PTFEtemperatureprobesbringawholenewdimensiontomeasurement T NEW NEW NEW NEW quotation by return. by quotation [email protected] email by us contact Please probe. this of use enable to lid vessel the on socket 29/32 Rodaviss vertical a specify Please thermoregulator. suitable a to connection for plug Lemo a with fitted cable of metres two and fitting 29/32 Rodaviss a baffle/probewith The standard as supplied is lid. vessel the in space port saving thus tip, the into moulded is which sensor PT100 a with this combines and contents, bafflevessel a the of of insertion agitation the improve allows to item This Supply andfitlemoplugtoPT100temperatureprobesforconnectionHuberthermoregulators. cushioned supportring.Bossheadonbackuprightforsupportingstirrermotor. coated clamps,withtopsupportclampforDN150flangeand120mmøViton Constructed fromheavyduty27mmø316stainlesssteeltubingandpowder Bosshead onbackuprightforsupportingstirrermotor. cushioned supportring.Fittedwith4castors,2ofwhichareabletobebraked. coated clamps,withtopsupportclampforDN200flangeand190mmøViton Constructed fromheavyduty27mmø316stainlesssteeltubingandpowder ype-K ThermocoupleProbes 555600 CAT NO 555800 CAT NO 1 HeavyDutyBenchtopReactionVessel SupportFrame DESCRIPTION 555650 CAT NO 1 HeavyDutyMobileReactionVessel SupportFrame DESCRIPTION 555750 CAT NO 0.0. TETp- hroopePoe9møx70mbd egh1 1 1 1 1 9mmøx700mmbodylength 1 9mmøx600mmbodylength 1 9mmøx500mmbodylength PTFEType-K ThermocoupleProbe 8mmøx400mmbodylength PTFEType-K ThermocoupleProbe 8mmøx300mmbodylength PTFEType-K ThermocoupleProbe 7mmøx200mmbodylength PTFEType-K ThermocoupleProbe 600.701.1 7mmøx100mmbodylength PTFEType-K ThermocoupleProbe 600.601.1 PTFEType-K ThermocoupleProbe 600.501.1 PTFEType-K ThermocoupleProbe 600.401.1 600.301.1 600.201.1 600.101.1 CAT NO Combination PTFE Baffle/TemperaturePTFE Combination Probe Jumbo Lemo PlugFittingService Jumbo DESCRIPTION Lemo PlugFittingService Combination PTFEbaffle/Temperature Probe DESCRIPTION DESCRIPTION ™ ™ Mobile Vessel SupportFrame Benchtop Vessel SupportFrame with the vessel specifications or required length and we will we and length required or specifications vessel the with - PTFE,upto300˚C DIMENSIONS KQYPRICEEACH PK QTY PRICEEACH PK QTY PK QTY PK QTY KQYPRICEEACH PK QTY 1 1 S S

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materials areglassandPTFEonly. glassware. ThebodyispurePTFEandfullyadjustablewithareplaceableViton seal.Contact Enables standardprobesandthermometerstobeassembledintaperlaboratory NEW insulated cable rigidity, butcanbebent.SensorisClassAtoBS1904,DIN43760andIEC751witha4corePTFE suitable forusefromcryogenictemperaturesupto+300˚C.Probebodieshaveametalcore which haveunsurpassednon-stickproperties.Probeswillnotcontaminateyoursampleandare molding techniquesareusedtomanufactureprobeswhichinertvirtuallyallchemicals,and Solid PTFEplatinumresistanceprobesoffer superioraccuracy:+/-0.3˚Cor+/-0.002T˚C.Isostatic Platinum ResistanceTemperature Probes 021.146.1 CAT NO 0.0. TEPaiu eitneTmeauePoe9møx70mbd egh1 1 9mmøx700mmbodylength 1 9mmøx600mmbodylength 1 PTFEPlatinumResistanceTemperature Probe 9mmøx500mmbodylength 1 PTFEPlatinumResistanceTemperature Probe 8mmøx400mmbodylength 1 PTFEPlatinumResistanceTemperature Probe 500.700.1 8mmøx300mmbodylength 1 PTFEPlatinumResistanceTemperature Probe 500.600.1 7mmøx200mmbodylength PTFEPlatinumResistanceTemperature Probe 500.500.1 7mmøx100mmbodylength PTFEPlatinumResistanceTemperature Probe 500.400.1 PTFEPlatinumResistanceTemperature Probe DESCRIPTION 500.300.1 500.200.1 500.100.1 CAT NO 021.147.1 021.148.1 021.149.1 021.196.1 021.197.1 021.198.1 021.199.1 of ChemScienceCatlogueformoreinformation... See theHuberThermoregulatorsection in ourindustry. familiarity, flexibilityandeaseofusethatisunequalled on allproductsexceptUnistats.Thisbringsalevelof Controllers using“PlugandPlay”technologyarenowused at theprocess! Focusing ontheapplication-Huberoffer powerandresponsewherewhenneeded... to keepupspeedwitheverchangingdemands. Three interchangeable,intuitive,easytousecontrollerswithpracticalfeaturesandflexibility and thepossibilitiesincreased.Morepower, widertemperaturerange,easiertouse. 12 yearson,theUnistatsandTango Technology havebeenrefined,therangehasgrown expectations oftheindustry. of controlandresponsetodynamicthermalloads.Ithasraisedthepossibilities The Unistats’lowvolume,hydraulicallysealedsystemhassetahighbenchmarkinthelevel chemical, petrochemicalandsemiconductorindustries. for accurateandresponsivecontrolofawidevarietyapplicationsinthepharmaceutical, Following theirintroductionin1991,HuberUnistatssoonbecamethethermostatofchoice T in itsconceptthatthesameprincipleisusedfromsmallestbenchtopsystem(Unistat Based onpassivecomponentsandthelawsofphysics,“Tango Technology” issosound • • • • and theUnistatrangeofthermostats. a complexproblem.Theresultsare“Tango Technology”, “PlugandPlayTechnology” Huber areworldleadersinthefieldofthermoregulation-findingsimplesolutionsto Huber HighPrecisionThermoregulators ango) toaunitthatdelivers60kW@-40˚C(Unistat1060). Unistats, PolystatsandMinistats Calibration BathEquipment Unichillers Compatible ControlThermostats Probe &ThermometerHolders with PFA over-sheath. 14/23 Cone DESCRIPTION 14/23 Cone 14/23 Cone 14/23 Cone 19/26 Cone 19/26 Cone 19/26 Cone 19/26 Cone t: +33 4 70 03 88 55 f: +33 4 70 03 82 60 e: [email protected] e: [email protected] Connection maybe2,3or4wire. PROBE Ø 6mm 7mm 8mm 9mm 6mm 7mm 8mm 9mm SEAL CAT NO. 021.06S 021.07S 021.08S 021.09S 021.06S 021.07S 021.08S 021.09S IESOSP T PRICEEACH PKQTY DIMENSIONS - PTFE

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e Support Servicing Supply put cablelengthinmetresaslastnumber plug. Extracableis£4.34permetre.Please Supplied with1metreofcable,butwithout Cat No.e.g.500.200.4 for fourmetres. 25 REACTION SYSTEMS 26 REACTION SYSTEMS Reaction Vessel Accessories may berestricted.. where height with apparatus Ideal foruse Stirrer Drive Right Angle Eurostar powerbasic Overhead Stirrer V Stirrer Guide ersion 5PTFE Borosilicate GlassStirring Propeller Stirrer, 4-bladed Shafts andGuides Interchim 211bisavenueJFKennedy -BP114003100MontluçonFrancewww.interchim.com Buddeberg Air Stirrersfrom PLR Compressed Overhead Stirrer RW RW V Mechanical Stirrer Guide ersion 6PTFE 20 DZM.n Suitable forusewherespaceaboveavesselislimited.AcceptsPTFEormetal9.5mmshafts. This unitcombinesarightangledriveandcouplingwhichcompensatesformisalignment. NEW 555320 CAT NO • • A widerangeofPTFE,glassandmetalstirrershaftsguides. NEW For pricesandspecificationsonPTFEStirrersGuidespleaseseeChemScienceCatalogue T or vessel,alwaysensurethatthespeedelectedis‘whipfree’ Note: shaft of6,8,9.5,10,12and16mmdiameter. stirrer shaftsintoreactionorfermentationvessels.Theyaresuitableforalltypesof These PTFEStirrerGuidesaredesignedtoprovideareliableandsafemeansofentryfor NEW For priceson • • • • Compressed AirStirrersareidealforallkindsoflabstirringtasks.Featuresinclude:- NEW For pricesandspecificationsonIKAStirrerspleaseseeChemScienceCatalogue • • • • • up tothe“highviscosity”range.Featuresinclude: IKA overheadstirrersarepowerfulslimline,laboratoryandprocessforstirringtasks NEW For pricesandspecificationsontheseStirrersShaftspleaseseeChemScienceCatalogue • PTFE ScrewPropellerStirrer wo versionsofPTFEstirrerguideareavailable,Version 5andVersion 6. ls Chemicallyinert,easytoclean, Glass - -Chemicallyinert,unbreakable,easytoclean, PTFE W Can beoverloadedtoastandstillwithoutcausingdamage V Explosion proof Push throughstirringshafts Non-locking, overloadcapabilities Slim casing,quietrunning Infinitely adjustablewithoutgearshifting Microprocessor control ea Robustuptohighspeeds,rigid,easyclean, Metal - ery highpowertoweightratio ell suitedtocontinuousoperation Right AngleStirrerDrive All stirrershaftsmaywhipatcertainspeed,thereforetoavoiddamageshaft Stirrer Shafts&Blades PTFE StirrerGuides Compressed AirStirrer IKA Compressed AirStirrers ® Right AngleStirrerDrive DESCRIPTION Overhead Stirrers TECentrifugalStirrer PTFE please seeChemScienceCatalogue non-shedding - for9.5mmdiametershafts - Buddeberg useable upto280˚C non-shedding PK QTY 1 Maxi PropellerStirrerShaft PRICE EACH Prices All Prices are in Pounds Sterling and subject to alteration without prior notice. We reserve the right to invoice goods at prices ruling at the date of despatch. Prices are exclusive of carriage, packing, insurance and VAT. Our preferred minimum order value is £30 net.

Delivery of Goods We will despatch all goods by the most cost effective method of transport unless otherwise specified by the customer. Please advise of any special shipping requirements. For details of carriage, packing and insurance charges please contact our Sales Office on Tel: +44-(0)1799-513320.

Quotations All offers, written or verbal, are valid for 30 days, unless otherwise specified. The right is reserved to amend any accidental errors.

Damage or Shortage of Delivered Goods Within three working days advise the carrier both in writing and verbally. Immediately advise us both in writing and verbally. Retain goods and packaging for inspection. Deliveries offered ex-stock are subject to the goods being unsold at the date of receipt of customer’s order.

Payment of Accounts Our terms of payment are strictly 30 days from date of invoice, subject to approved trade and bankers’ references.

Responsibility Our responsibility is limited to the supply of goods in the kind and quality ordered. All goods should be checked before use as no subsequent liability can be accepted.

Free-Issue Materials and Repairs We are not responsible for damage to articles sent to us for repair or examination, nor for incidental damage to glass apparatus and delicate instruments during the course of repair whilst on our premises, or during transit, to or from our premises. Time involved in the preliminary examination of any article may be charged TERMS & CONDITIONS in the event of no subsequent order being placed. Goods for repair should be sent carriage paid and clearly labelled with the sender’s name and address; at the same time a note should be included detailing the work required. Any goods sent for repair, maintenance or return should be free from physical, chemical and biological hazards.

On-site Work No responsibility can be accepted for any accident, however caused, whilst our employees are on the customer’s premises. Safety precautions are the hirer’s responsibility.

Tools or Moulds Unless otherwise agreed between the purchaser and ourselves, in the case of orders where special tools, moulds, gauges etc, are required for the manufacturer of the parts to be supplied, the purchaser will be charged with a part cost of the manufacture or purchase of such tool, as and when samples for approval are being submitted. We reserve the right to retain possession of all such tools.

Return of Goods Return of correctly supplied goods will not be accepted unless agreed arrangements have been made. A separate advice of despatch should be sent to us for all items. No responsibility will be accepted for items damaged or lost in transit.

Illustrations and Specifications Subject to alteration without notice. They are not binding and are only intended to represent generally the type of goods offered, as owing to improvements and revision of design and/or change of service, apparatus may not conform to them in detail.

Bank Details Lloyds Bank plc, 25 East Gate, Harlow Town Centre, Harlow, Essex. CM20 1LD. United Kingdom Account Name: R. B. Radley & Co. Ltd. Account Number: 0149739. Bank Sort Code: 30-93-89

New Customers For new customers there may be some delay in despatching goods until credit has been approved. To avoid the delay customers may remit on Proforma invoice, where goods will be despatched after remittance is received.

Export Customers Our terms of payment are strictly 30 days from date of invoice, subject to credit approval. All invoices will be in Pounds Sterling and should be remitted in Sterling. Payment should be made by Bankers Draft drawn in Sterling and sent direct to ourselves or by International Money Transfer, direct to our bank. When remitting by IMT please advise us of details in advance.

Pay by Credit Card For your convenience we accept payment by all leading credit or debit cards. Credit card orders are accepted by telephone, fax, post or email. Please provide your card number, card holders name, address and expiry date when placing your order. Payment is debited when your goods are despatched.

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