Calorimetry for Particle Physics
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Protocol for Use of Differential Scanning Calorimeter (NSF/Epscor Proteomics Facility @ Brown University)
MicroCal VP-DSC Geoff Stetson/ Page Laboratory/ 2007 Protocol for Use of Differential Scanning Calorimeter (NSF/EPSCoR Proteomics Facility @ Brown University) 1. Equipment (photos) 2. Getting Started Degasser - Turn on the degasser. - Make sure the metal valve on the top of the lid is closed. - Set the temperature to 20-25°C. - Place a small stir bar in a couple of plastic vials. - Fill vials 2/3 full with Milli-Q water. - Place vials into slots on top of degasser. - Turn the stirrer speed knob to - 10 or 11 o’clock. - - Place the lid on firmly, and while pressing down turn on the degasser o (Note: If you flip the switch to on, the degasser will run until switched off. If the switch is flipped to timer, the degasser will run for eight minutes). - Degas the sample for 8-15 minutes. o Turn off the vacuum. - Open the metal valve on top of the lid in order to release the vacuum created underneath. - Remove the plastic vials. 1 MicroCal VP-DSC Geoff Stetson/ Page Laboratory/ 2007 DSC - Unscrew top. - Remove contents of of the sample cell and the reference cell using the glass filling syringe. o Insert the funnel into the top of the cell. o Slowly put the syringe into the cell until it gently touches the bar across the top of the funnel, then remove the liquid. Repeat. o (Note: Be careful when putting anything into the cells. The machine is extremely sensitive.) - Fill glass syringe with degassed Milli-Q water. - Rinse out both cells with the Milli-Q water (3x). -
Soda Can Calorimeter
Soda Can Calorimeter Energy Content of Food SCIENTIFIC SCIENCEFAX! Introduction Have you ever noticed the nutrition label located on the packaging of the food you buy? One of the first things listed on the label are the calories per serving. How is the calorie content of food determined? This activity will introduce the concept of calorimetry and investigate the caloric content of snack foods. Concepts •Calorimetry • Conservation of energy • First law of thermodynamics Background The law of conservation of energy states that energy cannot be created or destroyed, only converted from one form to another. This fundamental law was used by scientists to derive new laws in the field of thermodynamics—the study of heat energy, temperature, and heat transfer. The First Law of Thermodynamics states that the heat energy lost by one body is gained by another body. Heat is the energy that is transferred between objects when there is a difference in temperature. Objects contain heat as a result of the small, rapid motion (vibrations, rotational motion, electron spin, etc.) that all atoms experience. The temperature of an object is an indirect measurement of its heat. Particles in a hot object exhibit more rapid motion than particles in a colder object. When a hot and cold object are placed in contact with one another, the faster moving particles in the hot object will begin to bump into the slower moving particles in the colder object making them move faster (vice versa, the faster particles will then move slower). Eventually, the two objects will reach the same equilibrium temperature—the initially cold object will now be warmer, and the initially hot object will now be cooler. -
Followed by a Stretcher That Fits Into the Same
as the booster; the main synchro what cheaper because some ex tunnel (this would require comple tron taking the beam to the final penditure on buildings and general mentary funding beyond the normal energy; followed by a stretcher infrastructure would be saved. CERN budget); and at the Swiss that fits into the same tunnel as In his concluding remarks, SIN Laboratory. Finally he pointed the main ring of circumference 960 F. Scheck of Mainz, chairman of out that it was really one large m (any resemblance to existing the EHF Study Group, pointed out community of future users, not presently empty tunnels is not that the physics case for EHF was three, who were pushing for a unintentional). Bradamante pointed well demonstrated, that there was 'kaon factory'. Whoever would be out that earlier criticisms are no a strong and competent European first to obtain approval, the others longer valid. The price seems un physics community pushing for it, would beat a path to his door. der control, the total investment and that there were good reasons National decisions on the project for a 'green pasture' version for building it in Europe. He also will be taken this year. amounting to about 870 million described three site options: a Deutschmarks. A version using 'green pasture' version in Italy; at By Florian Scheck existing facilities would be some- CERN using the now defunct ISR A ZEUS group meeting, with spokesman Gunter Wolf one step in front of the pack. (Photo DESY) The HERA electron-proton collider now being built at the German DESY Laboratory in Hamburg will be a unique physics tool. -
T E M P E R a T U
THE HIGH TEMPERATURE HEAT CONTENTS OP 0 MOLYBDENUM AND TITANIUM AND THE LOW TEMPERATURE HEAT CAPACITIES OP TITANIUM DISSERTATION Presented In Partial Fulfillment of the Requirements for the Degree Doctor of Philosophy in the Graduate School of The Ohio State University By CHARLES WILLIAM KOTHEN, B.A. // The Ohio State University 1952 Approved By: Adviser i TABLE OF CONTENTS E&gft INTRODUCTION ............................ 1 THEORETICAL ............................. 3 HISTORICAL .............................. 6 PART I The High Temperature Heat Contents of Molybdenum and Titahium ................... 13 Introduction ...................... 13 Apparatus .......................... 14 Measurements and Calculations ........ 32 Errors ... ......................... 45 Experimental Results ............... 49 PART II Low Temperature Heat Capacity of Titanium.. 61 Introduction ...................... 61 Apparatus ........................... 62 Measurements and Calculations ....... 71 Errors ................... 74 Experimental Results ............... 75 ACKNOWLEDGMENTS .......................... 80 APPENDIX I Physical Constants, Drop Calorimeter Data .... 61 APPENDIX II Low Temperature Calorimeter Data ..... 82 APPENDIX III Standard Lamp Calibration ............ 83 3182G G TABLE OF CONTENTS, (cont.) Page APPENDIX IV Bibliography ................. 85 AUTOBIOGRAPHY .......................... 89 iii LIST OF ILLUSTRATIONS 1 Vacuum Furnace 15 2 Dropping Mechanism 19 3 Improved Calorimeter 20 4. Modified Calorimeter, II 21 5 Drop Calorimeter Electrical Circuits -
Accelerator Search of the Magnetic Monopo
Accelerator Based Magnetic Monopole Search Experiments (Overview) Vasily Dzhordzhadze, Praveen Chaudhari∗, Peter Cameron, Nicholas D’Imperio, Veljko Radeka, Pavel Rehak, Margareta Rehak, Sergio Rescia, Yannis Semertzidis, John Sondericker, and Peter Thieberger. Brookhaven National Laboratory ABSTRACT We present an overview of accelerator-based searches for magnetic monopoles and we show why such searches are important for modern particle physics. Possible properties of monopoles are reviewed as well as experimental methods used in the search for them at accelerators. Two types of experimental methods, direct and indirect are discussed. Finally, we describe proposed magnetic monopole search experiments at RHIC and LHC. Content 1. Magnetic Monopole characteristics 2. Experimental techniques 3. Monopole Search experiments 4. Magnetic Monopoles in virtual processes 5. Future experiments 6. Summary 1. Magnetic Monopole characteristics The magnetic monopole puzzle remains one of the fundamental and unsolved problems in physics. This problem has a along history. The military engineer Pierre de Maricourt [1] in1269 was breaking magnets, trying to separate their poles. P. Curie assumed the existence of single magnetic poles [2]. A real breakthrough happened after P. Dirac’s approach to the solution of the electron charge quantization problem [3]. Before Dirac, J. Maxwell postulated his fundamental laws of electrodynamics [4], which represent a complete description of all known classical electromagnetic phenomena. Together with the Lorenz force law and the Newton equations of motion, they describe all the classical dynamics of interacting charged particles and electromagnetic fields. In analogy to electrostatics one can add a magnetic charge, by introducing a magnetic charge density, thus magnetic fields are no longer due solely to the motion of an electric charge and in Maxwell equation a magnetic current will appear in analogy to the electric current. -
Adiabatic Dewar Calorimeter
I.CHEM.E. SYMPOSIUM SERIES NO. 97 ADIABATIC DEWAR CALORIMETER T.K.Wright'and R.L.Rogers* A simple calorimeter has been developed that enables chemical reaction runaway conditions to be directly determined, under the low heat loss conditions found in full scale chemical plants. Since the calorimeter provides temperature time data in the near absence of environmental heat losses the data can be simply analysed to yield heats of reaction and chemical power output. The latter are used either in conjunction with plant natural cooling data to assess reactor stability or at higher temperatures to size reactor vents. If the reaction mechanisms are known or adequate assumptions can be made then the temperature-time data can also be processed to yield reaction kinetics constants for simulation purposes. Keywords: Hazards, Exotherms, Adiabatic Calorimeter, kinetics INTRODUCTION Evaluation of chemical reaction hazards requires the detection of exotherms/gas generation likely to lead to reactor overpressure. Some form of small scale scanning calorimetry is generally used for the initial detection of the exotherm and gas generation and a temperature of onset will be determined which is dependent on the sensitivity of the equipment, but on a 10-20gm scale exothermlcity will generally be detected at self heating rates of 2-10°C/hr - approximately 3-10 watts/lit. Depending on apparent exotherm size and proximity to process temperature or any likely excursions then secondary testing may be required to display more accurately (a) The minimum temperature above which the reactor will be unstable on the scale used. (b) The consequences of the exotherm - heat of reaction/adiabatic rise/ pressure developed/venting requirement. -
Linseis Optical Dilatometer and Heating Microscope Brochure
THERMAL ANALYSIS Optical Dilatometer DIL L74 Heating Microscope Since 1957 LINSEIS Corporation has been deliv- ering outstanding service, know how and lead- ing innovative products in the field of thermal analysis and thermo physical properties. Customer satisfaction, innovation, flexibility and high quality are what LINSEIS represents. Thanks to these fundamentals our company enjoys an exceptional reputation among the leading scientific and industrial organizations. LINSEIS has been offering highly innovative benchmark products for many years. The LINSEIS business unit of thermal analysis is involved in the complete range of thermo Claus Linseis analytical equipment for R&D as well as qual- Managing Director ity control. We support applications in sectors such as polymers, chemical industry, inorganic building materials and environmental analytics. In addition, thermo physical properties of solids, liquids and melts can be analyzed. LINSEIS provides technological leadership. We develop and manufacture thermo analytic and thermo physical testing equipment to the high- est standards and precision. Due to our innova- tive drive and precision, we are a leading manu- facturer of thermal Analysis equipment. The development of thermo analytical testing machines requires significant research and a high degree of precision. LINSEIS Corp. invests in this research to the benefit of our customers. 2 German engineering Innovation The strive for the best due diligence and ac- We want to deliver the latest and best tech- countability is part of our DNA. Our history is af- nology for our customers. LINSEIS continues fected by German engineering and strict quality to innovate and enhance our existing thermal control. analyzers. Our goal is constantly develop new technologies to enable continued discovery in Science. -
An Analysis on Single and Central Diffractive Heavy Flavour Production at Hadron Colliders
416 Brazilian Journal of Physics, vol. 38, no. 3B, September, 2008 An Analysis on Single and Central Diffractive Heavy Flavour Production at Hadron Colliders M. V. T. Machado Universidade Federal do Pampa, Centro de Cienciasˆ Exatas e Tecnologicas´ Campus de Bage,´ Rua Carlos Barbosa, CEP 96400-970, Bage,´ RS, Brazil (Received on 20 March, 2008) In this contribution results from a phenomenological analysis for the diffractive hadroproduction of heavy flavors at high energies are reported. Diffractive production of charm, bottom and top are calculated using the Regge factorization, taking into account recent experimental determination of the diffractive parton density functions in Pomeron by the H1 Collaboration at DESY-HERA. In addition, multiple-Pomeron corrections are considered through the rapidity gap survival probability factor. We give numerical predictions for single diffrac- tive as well as double Pomeron exchange (DPE) cross sections, which agree with the available data for diffractive production of charm and beauty. We make estimates which could be compared to future measurements at the LHC. Keywords: Heavy flavour production; Pomeron physics; Single diffraction; Quantum Chromodynamics 1. INTRODUCTION the diffractive quarkonium production, which is now sensitive to the gluon content of the Pomeron at small-x and may be For a long time, diffractive processes in hadron collisions particularly useful in studying the different mechanisms for have been described by Regge theory in terms of the exchange quarkonium production. of a Pomeron with vacuum quantum numbers [1]. However, the nature of the Pomeron and its reaction mechanisms are In order to do so, we will use the hard diffractive factoriza- not completely known. -
A New Avenue to Parton Distribution Functions Uncertainties: Self-Organizing Maps Abstract
A New Avenue to Parton Distribution Functions Uncertainties: Self-Organizing Maps Abstract Neural network algorithms have been recently applied to construct Parton Distribution Functions (PDFs) parametrizations as an alternative to standard global fitting procedures. We propose a different technique, namely an interactive neural network algorithm using Self-Organizing Maps (SOMs). SOMs enable the user to directly control the data selection procedure at various stages of the process. We use all available data on deep inelastic scattering experiments in the kinematical region of 0:001 ≤ x ≤ 0:75, and 1 ≤ Q2 ≤ 100 GeV2, with a cut on the final state invariant mass, W 2 ≥ 10 GeV2. Our main goal is to provide a fitting procedure that, at variance with standard neural network approaches, allows for an increased control of the systematic bias. Controlling the theoretical uncertainties is crucial for determining the outcome of a variety of high energy physics experiments using hadron beams. In particular, it is a prerequisite for unambigously extracting from experimental data the signal of the Higgs boson, that is considered to be, at present, the key for determining the theory of the masses of all known elementary particles, or the Holy Grail of particle physics. PACS numbers: 13.60.-r, 12.38.-t, 24.85.+p 1 I. DEFINITION OF THE PROBLEM AND GENERAL REMARKS In high energy physics experiments one detects the cross section, σX , for observing a particle X during a given collision process. σX is proportional to the number of counts in the detector. It is, therefore, directly \observable". Consider the collision between two hadrons (a hadron is a more general name to indicate a proton, neutron...or a more exotic particle made of quarks). -
Collider Physics at HERA
ANL-HEP-PR-08-23 Collider Physics at HERA M. Klein1, R. Yoshida2 1University of Liverpool, Physics Department, L69 7ZE, Liverpool, United Kingdom 2Argonne National Laboratory, HEP Division, 9700 South Cass Avenue, Argonne, Illinois, 60439, USA May 21, 2008 Abstract From 1992 to 2007, HERA, the first electron-proton collider, operated at cms energies of about 320 GeV and allowed the investigation of deep-inelastic and photoproduction processes at the highest energy scales accessed thus far. This review is an introduction to, and a summary of, the main results obtained at HERA during its operation. To be published in Progress in Particle and Nuclear Physics arXiv:0805.3334v1 [hep-ex] 21 May 2008 1 Contents 1 Introduction 4 2 Accelerator and Detectors 5 2.1 Introduction.................................... ...... 5 2.2 Accelerator ..................................... ..... 6 2.3 Deep Inelastic Scattering Kinematics . ............. 9 2.4 Detectors ....................................... .... 12 3 Proton Structure Functions 15 3.1 Introduction.................................... ...... 15 3.2 Structure Functions and Parton Distributions . ............... 16 3.3 Measurement Techniques . ........ 18 3.4 Low Q2 and x Results .................................... 19 2 3.4.1 The Discovery of the Rise of F2(x, Q )....................... 19 3.4.2 Remarks on Low x Physics.............................. 20 3.4.3 The Longitudinal Structure Function . .......... 22 3.5 High Q2 Results ....................................... 23 4 QCD Fits 25 4.1 Introduction.................................... ...... 25 4.2 Determinations ofParton Distributions . .............. 26 4.2.1 TheZEUSApproach ............................... .. 27 4.2.2 TheH1Approach................................. .. 28 4.3 Measurements of αs inInclusiveDIS ............................ 29 5 Jet Measurements 32 5.1 TheoreticalConsiderations . ........... 32 5.2 Jet Cross-Section Measurements . ........... 34 5.3 Tests of pQCD and Determination of αs ......................... -
Simple Calorimeter for Heats of Fusion. Data on The
U.S. Department of Commerce, Bureau of Standards RESEARCH PAPER RP607 Part of Bureau of Standards Journal of Research, Vol. 11, October 1933 A SIMPLE CALORIMETER FOR HEATS OF FUSION. DATA ON THE FUSION OF PSEUDOCUMENE, MESITYLENE (« AND 0), HEMIMELLITENE, o- AND m-XYLENE, AND ON TWO TRANSITIONS OF HEMIMELLITENE By Frederick D. Rossini abstract A vacuum flask with a thermoelement serves as a simple calorimeter for measuring heats of fusion quickly and economically, with an accuracy of a few percent. The following heats of fusion (with estimated uncertainties), in k-cal. per mole, were obtained: pseudocumene, — 44.1° C, 2.75±0.06; hemimelli- tene,-25.5° C, 2.00±0.05; mesitylene (a), — 44.8° C, 2.28±0.06; mesitylene (0), -51.7° C., 1.91±0.05; o-xylene,-25.3° C, 3.33±0.07; m-xylene,-47.9° C, 2.76 ±0.05. Hemimellitene was found to have two transitions below the freez- ing point, with the following heats of transition, in A>cal. per mole: hemimelli- tene (7-»0),-58±2° C.,0.28±0.04; hemimellitene (P^a),- 46 ± 1° C.,0.36±0.04. CONTENTS Page I. Introduction 553 II. Apparatus and method 553 III. Materials 554 IV. Standardization experiments 555 V. Experimental data 557 VI. Conclusion 559 I. INTRODUCTION The simple calorimeter described here was assembled in order to provide a means for measuring as quickly and economically as prac- ticable, and with an accuracy of a few percent, the heats of fusion of certain hydrocarbons for which there are no data. -
Deep Inelastic Scattering
Particle Physics Michaelmas Term 2011 Prof Mark Thomson e– p Handout 6 : Deep Inelastic Scattering Prof. M.A. Thomson Michaelmas 2011 176 e– p Elastic Scattering at Very High q2 ,At high q2 the Rosenbluth expression for elastic scattering becomes •From e– p elastic scattering, the proton magnetic form factor is at high q2 Phys. Rev. Lett. 23 (1969) 935 •Due to the finite proton size, elastic scattering M.Breidenbach et al., at high q2 is unlikely and inelastic reactions where the proton breaks up dominate. e– e– q p X Prof. M.A. Thomson Michaelmas 2011 177 Kinematics of Inelastic Scattering e– •For inelastic scattering the mass of the final state hadronic system is no longer the proton mass, M e– •The final state hadronic system must q contain at least one baryon which implies the final state invariant mass MX > M p X For inelastic scattering introduce four new kinematic variables: ,Define: Bjorken x (Lorentz Invariant) where •Here Note: in many text books W is often used in place of MX Proton intact hence inelastic elastic Prof. M.A. Thomson Michaelmas 2011 178 ,Define: e– (Lorentz Invariant) e– •In the Lab. Frame: q p X So y is the fractional energy loss of the incoming particle •In the C.o.M. Frame (neglecting the electron and proton masses): for ,Finally Define: (Lorentz Invariant) •In the Lab. Frame: is the energy lost by the incoming particle Prof. M.A. Thomson Michaelmas 2011 179 Relationships between Kinematic Variables •Can rewrite the new kinematic variables in terms of the squared centre-of-mass energy, s, for the electron-proton collision e– p Neglect mass of electron •For a fixed centre-of-mass energy, it can then be shown that the four kinematic variables are not independent.