SCAN-Lab BT-Lab EC-Lab products Electrochemistry accessories Local probes accessories Connectionaccessories Fuel cell Cellsfor battery testing Rotating electrodes Battery holders Quartz crystal analyzer Spectroelectrochemistry Electrodes Glassware Corrosion cell Analytical cell
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell electrochemistry technology. have beenatthe cutting edgeofscanning probe more than20years, Uniscan Instruments Ltd. Ltd., acompany basedinMacclesfield, UK.For and manufactured byUniscan Instruments tools. Theseproducts are developed, designed to highresolution electrochemical mapping workstations. TheScan-Lab divisionisdedicated instruments to thescanning electrochemical In 2012,Bio-LogicSASextended itschoice of current boosters. systems, integrating EIScapability andhigh from single channelupto 128-channel Lab) andbattery test equipments(BT-Lab) We offer electrochemical workstations (EC- modular andflexible design. Bio-Logic’s product range isbasedona and material testing. electrochemistry, battery testing, fuelcell instruments andsoftware for performance, research laboratory We designandmanufacture high near Grenoble intheFrench Alps. Bio-Logic SAS(founded in1983)islocated Bio-Logic
ELECTROCHEMISTRY ACCESSORIES accessories Local probes accessories Connection cell Fuel accessories Battery crystal analyzer Quartz electrochemistry Spectro- electrodes Rotating Electrodes Glassware cell Corrosion cell Analytical
Video Cells Probes 47 Test Boxes &Dummycells External device connection Transport cases Faraday cages Multi-electrode investigation cables Connectors 44 Specific Educational kit Membrane Electrode Assemblies (MEA) Sense Adapter Module (SAM-50) Current Collector (CC5) Battery (BH-1)&CoinCell Holder(CCH) Rack Dilatometers Test cells Biosensor QCM Quartz resonators EQCM Thin layer spectroelectrochemical cell Flow experiment Static experiment Spectrometer Rotating DiskElectrode (RDE) Working electrode tips Rotating RingDiskElectrode (RRDE) Metallic electrodes Counter electrodes King sizereference electrodes Small sizereference electrodes Working electrodes Bridge tubeswithceramic junction Bridge &purge tubesfor analytical cells Small sizebridgetubes Bridge &purge tubesfor corrosion cells Small &bigvolume cell vials Coating cell Plate material evaluating cell Galvanic cells Flat cells Avesta cell Standard corrosion cells Screen Printed Electrodes (SPE) Ring disktypeelectrodes InterDigitated Array (IDA) electrodes Flow cells Large volume cells Small volume cells 47
Microscope cables 44
System
46 47 46 46 45 45 43 42 41 41 40 40 39 38 36 35 34 32 31 30 28 26 25 24 23 23 22 20 18 18 17 16 16 14 13 13 13 12 11 10 9 8 8 7 6 4 2/3
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell Small volume cells Analytical cell (200 μLinthesample holder) Small amountofsolution microvolume mode SVC-2 modularity: condition...). solution, oxygen free electrode, volume of (specific working specific application is designedfor a Each voltammetry cell I/nA -50 -40 -30 -20 -10 10 20 30 0 -0.5 E we 0
/V
- - - - SVC-2 inthemicrovolume modeisrecommended. If only asmallamountoftheelectroactive compound isavailable, more suitable. For application requiring otherworking electrode shape,SVC-2 is of SVC-3 kitisrecommended. electrode withanouter diameter (OD)of6mmthefixed configuration For example, for voltammetry investigations usingstandard working Bulk electrolysis cell, for avolume of100mL. VC-4, for avolume of1to 3mL,only for working electrode withODof6mm. SVC-3, for avolume of5to 20mL,only for working electrode with OD of6mm. SVC-2, modular with ODof10mm For electrode oxygen free mode 0.5
SVC-2 with ODof6mm For electrode - Note thatacomplete analytical specialkit - - - This kitincludes: electrode hasto bepurchased separately. (A-012763) isalsoproposed, butthereference ID 1.6mm(A-002013)(seepage 18). one platinumelectrode, OD6.0 mm, ID 3.0mm(A-002012)(seepage 18), one glassy carbon electrode, OD6.0mm, PK-3 polishingkit(A-011975)(seepage18), SVC-3 kit(A-012669),
with ODof4mm For microelectrode SVC-3
SK-2
Sample holder Options Additional items 100 mm Products Small volume cells Counter electrode (CE) Cell holder Sample vial Content Purge tube(ETFE), PTFE cap Purge tube(ETFE) Working electrodes Reference electrodes PTFE cap ELECTROCHEMISTRY ACCESSORIES surface area oftheworking electrode. so thesurface area ofthecounter electrode shouldbelarger thanthe The counter shouldnotbethelimitingfactor for theelectron transfer, Working andreference electrodes have to beclose to eachother. The geometryofthecell shouldbeoptimizedto reduce theohmicdrop. Cell geometry
VC-4 9.0 mm (2 pieces) 10 to 6 (7 pieces) adapter SVC-2 57 mm for 20mL 20 mL 1 m
A-012177 - A-001056 - A-012668 A-002222 Catalog n° A-001209 A-012670 A-010537 6.2 mm 1.6 mm 10.2 mm (2 pieces) (7 pieces) 6.0 mm 20 mL SVC-3 50 mm for 20mL 1 m see page18 see page20
- Catalog n° A-012176 A-001056 A-012669 A-012671 A-002222 A-001209 A-010537 1.6 mm 6.2 mm cell holder (7 pieces) 5 mL VC-4 57 mm 1 m see page18 see page20
1.6 mm 6.3 mm 1.65 mm Catalog n° A-011227 - A-011504 A-011224 A-011226 A-002222 A-010537 Bulk electrolysis cell stirrer bar port plug O-ring chamber for CE lid for CE porous carbon electrode (1 piece) 100 mL Bulk electrolysis cell 230 mm 1 m see page20
Catalog n° A-000178 A-009131 A-001236 A-001196 A-001198 A-010530 - A-012632 A-001197 A-0 12551 A-002234 A-010537 4/5
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion AnalyticalAnalytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cellcell - - Two typesofpackagesare offered: applications. for macro electrochemistry from 50to 250mLiswell adapted This analytical cell withvolumes Large volume cells Analytical control andgaspurging). (which allows temperature the complete analytical cell kit the standard analytical cell kit, EL-A-012 cell EL-A-002
250 mLcells are alsoavailable: Set of10porous 4mmglass frit(CoralPor™) withPTFEheatshrink(200mm) Aluminum baseholderfor magneticstirrer without PT100probe Magnetic stirrer &heater, PT100 probe, indicate connector type Bridge tubefor reference electrode ofOD8mm Electrode bridge extension for electroanalytical cell Options Telescopic cell stand Double nut25mmand12diameter Reference electrode Purge tube Platinum counter electrode Bridge tubefor reference electrode, OD6mm Double purge tube Cell collar withclamp PTFE ring,silicon encapsulated, OD102mm PTFE cap 5holes Double jacketed glass cell 150mL Double jacketed glass cell 80mL Glass cell 80mL EL-A-003 EL-A-004
glass cell EL-A-018or double jacketed glass cell EL-A-021 EL-A-005 110 V 220 V EL-ELECTRO-1 cell kit(80 mL) analytical Standard
EL-ELECTRO-2 cell kit(80 mL) analytical Complete EL-A-008 EL-ELECTRO-3 cell kit(150 mL) analytical Complete EL-A-009 092-VYC4 EL-C-018 EL-C-015B EL-C-015A EL-C-014 EL-A-017 EL-A-022 EL-A-012 EL-A-011 A-013430 EL-A-016 EL-A-009 EL-A-008 EL-A-006 EL-A-005 EL-A-004 EL-A-003 EL-A-020 EL-A-002 EL-A-001 Catalog n°
EL-A-022 Flow cells ELECTROCHEMISTRY ACCESSORIES Dual, parallel/cross flow Dual, series/cross flow Single/radial flow diagram Schematic Product Cross/radial Radial flow Cross flow Options dynaseal PEEKfingertight (10pieces) 1/16" PEEKtube 0.04" MMconnector (10pieces) 0.04" single leal connector (2pieces) RE-7VP nonaqueousreference electrode (Ag/Ag RE-3VP Ag/AgClscrew typeelectrode, PEEK resin RE-7V nonaqueousreference electrode (Ag/Ag RE-3V Ag/AgClreference electrode screw type radial flow cell block gasket electrode cross flow cell block gasket electrode Cross flow cell * Gasket, working, reference electrodes andconnectors are soldseparately Cross flow cell* g asket TG-12MR PTFE(4pieces) TG-11MR PTFE(4pieces) TG-8MR PTFE(4pieces) TG-6MR PTFE(4pieces) TG-5MR PTFE(4pieces) TG-2MR PTFE(4pieces) carbon paste PFCE carbon gold platinum glassy carbon glassy carbon TG-12M silicon (4pieces) TG-11M silicon (4pieces) TG-8M PTFE(4pieces) TG-6M PTFE(4pieces) TG-5M PTFE(4pieces) TG-2M PTFE(4pieces) glassy carbon/platinum glassy carbon/gold nickel carbon paste silver platinum gold glassy carbon Cross flow cell INLET OUTLET A-012798 Catalog n° detector + ) screw type,poly acetal resin + ) screw type,PEEKresin screw for pipeconnecting integrated 1/16" ID 0.25mm,length 3.0m size Ø10x48mm material PEEK film thickness 1,000µm film thickness 500µm film thickness 100µm film thickness 50µm film thickness 25µm film thickness 12µm Ø 3mm(single type),size25xmm Ø 3mm(single type),size25xmm Ø 3mm(single type),size25xmm Ø 3mm(single type),size25xmm Ø 3mm(single type),size25xmm Ø 6mm(single type),size25xmm material PEEK film thickness 1,000µm film thickness 500µm film thickness 100µm film thickness 50µm film thickness 25µm film thickness 12µm Ø 3mmx2(dualtype),size25 Ø 3mmx2(dualtype),size25 Ø 3mmx2(dualtype),size25 Ø 3mmx2(dualtype),size25 Ø 3mmx2(dualtype),size25 Ø 3mmx2(dualtype),size25 Ø 3mmx2(dualtype),size25 Ø 3mmx2(dualtype),size25 Radial flow cell Radial flow cell* gasket flow channel OUTLET OUTLET Radial flow cell INLET detector A-012799 Catalog n° A-004130 A-001531 A-013273 A-012912 A-012174 A-012173 A-012170 A-012169 A-001031 A-001193 A-001192 A-012802 A-001148 A-001147 A-001146 A-010251 A-000999 A-011155 A-009908 A-012124 A-001016 A-001032 A-001093 A-001092 A-001049 A-001048 A-001047 A-001046 A-012583 A-001006 A-001009 A-001004 A-001008 A-001012 A-001002 A-001000 6/7
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion AnalyticalAnalytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cellcell Passivation membrane diazido compounds. Novolac resin +naphtoquinore- The passivation membrane isa InterDigitated Array (IDA) electrodes Analytical Working electrode #2 Working electrode #1 Reference electrode thickness =0.5mm Counter electrode Quartz plate,
cell 12 2 20 Ring disktypeelectrodes Gold IDA electrode Carbon ringdiskelectrode (3pieces) Platinum ringdiskelectrode (3pieces) Gold ringdiskelectrode (3pieces) Ring disktypeelectrodes Platinum Gold withoutpassivation membrane Platinum withoutpassivation membrane Gold Platinum Gold withoutpassivation membrane Platinum withoutpassivation membrane Gold Platinum ITO Carbon Gold withoutpassivation membrane Platinum withoutpassivation membrane ITO withoutpassivation membrane Carbon withoutpassivation membrane Ag/AgCl inkfor reference electrode (2.0mL) Cable kitfor IDA electrode Options 3 µm Width 2 µm 2 µm 2 µm 2 µm 3 µm 3 µm 3 µm 3 µm 10 µm 10 µm 10 µm 10 µm 10 µm 10 µm 10 µm 10 µm 10 µm Interval 2 µm 2 µm 2 µm 2 µm 3 µm 3 µm 3 µm 3 µm 5 µm 5 µm 5 µm 5 µm 5 µm 5 µm 5 µm 5 µm 6 mm 6 mm 6 mm Ring OD Length 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm 2 mm N° offeet 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs 65 pairs Ring ID 4 mm 4 mm 4 mm Film thickness 90 nm 90 nm 90 nm 90 nm 90 nm 90 nm 90 nm 90 nm 90 nm 90 nm 100 ±20nm 1200 ±100nm 90 nm 90 nm 100 ±200nm 1200 ±100nm Disk 3 mm 3 mm 3 mm Catalog n° A-002083 A-002082 A-002081 A-012257 Catalog n° A-012258 A-012261 A-012264 A-012129 A-012130 A-012260 A-012263 A-012125 A-012126 A-012128 A-012127 A-012259 A-012262 A-012265 A-012266 A-011464 A-011066 platinum, gold.TheSPEallows users to work with working electrode can bemadeofglassy carbon, electrodes according to thedesignneeded.The one counter electrode andoneorseveral working disposable. They includeonereference electrode, Screen Printed Electrodes (SPE)are low cost and ELECTROCHEMISTRY ACCESSORIES Connector for 3-electrode Screen Printed Electrodes (2mmbananaplug) Option overall dimension: ratio CE/WEsurface area: size ofRE: Ø ofWE: 3-electrode Screen PrintedElectrodes on eachworking electrode ofthearray (upto 16). it ispossible to run simultaneous investigations Note withBio-Logic’s multichannelpotentiostats, and oneshared counter electrode. electrode SPEwithoneshared reference electrode A two–electrode set-upisusedfor multiworking a smallamountofsolution(25-100μL). Screen PrintedElectrodes (SPE) 50 x10mm 4/1 0.5 x1mm 2 mm
Working electrode Working electrode gold gold gold gold gold gold platinum platinum platinum platinum graphite graphite graphite graphite graphite graphite
Counter electrode &ref. electrode Counter electrode graphite graphite graphite graphite graphite graphite graphite graphite graphite graphite graphite graphite graphite graphite graphite graphite
Three-electrode sensor Ref. electrode Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Ag/AgCl Working electrode Reference electrode Counter electrode Substrat Substrat valox FR1 valox FR1 valox FR1 alumina alumina alumina valox FR1 valox FR1 alumina alumina valox FR1 valox FR1 valox FR1 alumina alumina alumina Array of16working electrodes Packaging Packaging 500 pieces 100 pieces 20 pieces 500 pieces 100 pieces 20 pieces 500 pieces 100 pieces 500 pieces 100 pieces 500 pieces 100 pieces 20 pieces 500 pieces 100 pieces 20 pieces 3-electrode SPE connector for U-GEM,
Catalog n° Catalog n° G-AUGP/2 G-AUGP/1 G-AUGP/0 G-AUGA/2 G-AUGA/1 G-AUGA/0 G-PTGP/2 G-PTGP/1 G-PTGA/2 G-PTGA/1 G-GGP/2 G-GGP/1 G-GGP/0 G-GGA/2 G-GGA/1 G-GGA/0 U-GEM
8/9
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion AnalyticalAnalytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cellcell log (|I/nA|) 3 4 5 6 7 8 -0.6 - - i.e. ~1Lare available: two packagesfor large volume For corrosion applications, Standard corrosion cells Corrosion and cell stand). and includessample holder (allows temperature control complete corrosion cell kit basic corrosion cell kit, -0.4 -0.2 E we /V 0 0.2 cell
Glass cell 1L are alsoavailable (EL-C-020andEL-C-021,respectively). PTFE ring,silicon encapsulated, OD102mm PTFE cap Double jacketed glass cell 1L Cell collar withclamp Bridge tubefor 8mmdiameter reference electrode Purge tube Sample holder1cm Telescopic cell stand Double nut25mmand12diameter Graphite counter electrode rod (2pieces) Double purge tube Calomel reference electrode length 80mm,OD8mmscrew cap 12 mmODconical rings for reference electrode of8mm(4pieces) Cable connection for screw cap 100mm,2mmbananaplug 500 mLor2Ldouble jacketed glass cell Set of10porous frit(4mmCoralPor™) withPTFEheatshrink(200mm) Aluminum baseholderfor magneticstirrer Magnetic stirrer &heater, withoutPT100probe PT100 probe (indicate connector type) Bridge tubefor 6mmdiameter reference electrode Options EL-C-002 2 EL-C-003
EL-C-004 110 V 220 V EL-C-005
EL-CORR-1 cell kit Basic corrosion
EL-CORR-2 corrosion cell kit Complete
EL-C-017 092-C-013
EL-C-003 EL-C-002 EL-C-001 Catalog n° EL-C-004 EL-C-016 092-C-013 EL-C-012 EL-C-011 EL-C-009 EL-C-006 EL-C-005 EL-C-017 R-A94L111 R-XR110 EL-C-015B EL-C-015A R-X31M012 092-VYC4 EL-C-018 EL-C-014 EL-C-008 EL-C-009 ELECTROCHEMISTRY ACCESSORIES connector Copper Sampl Principle ofAvesta cell with PTFEheatshrink(200mm) Set of10porous frit(4mmCoralPor™) Temperature probe PT100 Single purge tube with ODof8mm Bridge tubefor reference electrode Peristaltic pumpfor low flow Options Skeleton Telescopic cell stand Double nut Bridge tubefor RE6mm Graphite counter electrode rods (2pieces) Filter paperring(100pieces) Double purge tube Cell collar withclamp O-ring PTFEsilcone encapsulated PTFE cap 5holes Double jacketed cell glass 250mL Content Avesta cell kit Avesta cell (EL-AV-008) whichdelivers 0.5to 5mL/h. The water flow iscontrolled byaperistaltic pump in order to eliminate crevice corrosion. and thegasket isfloodedbydistilled water A filter paperringplaced between thesample gasket atthebottom aperture ofthecell. formed between theworking electrode andthe It isdesignedto avoid microcrevice corrosion for pittingcorrosion testing (ASTMG150). Avesta cell isanelectrochemical cell developed Avesta cell INLET e
Filter paperring External gasket Internal gasket
Catalog n° 092-VYC4 EL-C-014 EL-AV-014 EL-AV-013 EL-AV-008 EL-AV-015 EL-AV-012 EL-C-011 EL-AV-010 EL-C-009 EL-AV-007 EL-AV-006 EL-A-005 EL-AV-004 EL-AV-003 EL-AV-002 EL-AV-001
10/11
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware CorrosionCorrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cellcell cell
Set of10porous frit(4mm CoralPor™) withPTFEheatshrink(200mm) PTFE O-ringsfor 10cm²** PTFE O-ringsfor 1cm²** EPDM O-ringsfor 10cm²** EPDM O-ringsfor 1cm²** PTFE O-ringsfor 10cm²withPEEKferrule for CE** PTFE O-ringsfor 1cm²withPEEKferrule for CE** EPDM O-ringsfor 10cm²withPEEKferrule for CE** EPDM O-ringsfor 1cm²withPEEKferrule for CE** PVDF* body(nondouble jacketed) Temperature Options it ispossible to get abodyoftheflatcell inPVDF*instead ofglass. If theexperiment isperformed inmore agressive mediasuchasfluorhydricacidmedia, Investigation inagressive media inferior to 10mmfitsintheholder. Thanks to itsdesign,anysample withathickness diameter of17.6mmandthe2others of 8.3mm. purge tubeandtemperature probe withinner control andthree holes for reference electrode, This cell hasadouble jacket for temperature on flatspecimenof1cm²or10area. adapted to perform AC orDCexperiments This cell withavolume of250mLis 1 to 10cm²sample area Flat cells, Corrosion PVDF* Borosilicated glass PTFE ** TheO-ringkitsinclude4O-ringsfor theglassware sideand10O-ringsfor thesample side * Polyvinylidenefluoride 20° C acid 48% Fluorhydric
cell 50° C acid 98% Sulfuric 20° C
50° C
acid 85% Phosphoric 20° C
50° C - - glass partfor flat cell (250mL) EL-FLAT-3 includes: Corrosion flat cell 1cm² (6 mmdiameter) Reference electrode bridgetube (54 mmwire/ 80mesh),25x35mm Platinum meshcounter electrode (length: 90mm,OD:6mm) RE-2B calomel reference electrode Content Flat cell kit1cm² Flat cell 1cm² flat cell 1cm² mechanical part for corrosion acid 35% Hydrochloric 20° C 50° C 092-VYC4 EL-SEAL-T10 EL-SEAL-T1 EL-SEAL-10 EL-SEAL-1 EL-SEAL-T10B EL-SEAL-T1B EL-SEAL-10B EL-SEAL-1B EL-F-PVDF Catalog n° acid 70% Nitric 20° C
50° C
EL-FLAT-3H EL-F-002 EL-FLAT-3 EL-F-004 A-702439 A-013430 EL-FLAT Catalog n°
acid Perchlorique 20° C 50° C RE-2B calomel reference electrode Content Flat cell kit10cm² Flat cell 10cm² - - EL-FLAT-4 includes: Corrosion flat cell 10cm² (6 mmdiameter) Reference electrode bridgetube (54 mmwire/ 80mesh),25x35mm Platinum meshcounter electrode (length: 90mm,OD:6mm) flat cell 10cm² mechanical part for corrosion glass partfor flat cell (250mL) hydroxide 50% Sodium 20° C * Polyvinylidenefluoride 50° C notcompatible notrecommended good excellent concentred hydroxide Potassium 20° C
50° C EL-FLAT-4H EL-F-002 EL-FLAT-2 EL-FLAT-4 EL-F-004 A-702439 A-013430 Catalog n° Galvanic cells, O-ring (10pieces) Options Platinum counter electrode (1piece) Purging tube,100mm Screw 20mm(1piece) O-ring (1piece) PTFE cell [body&base](1piece) Content Plate material evaluating cell design oftheflatcell, Thanks to themodular ELECTROCHEMISTRY ACCESSORIES Plate materialevaluating cell The required volume ofsolutionisabout1mL. cell blocks. The sample plate issandwichedbetween thetwo such asametal, semi-conducting plate... This cell wasdeveloped to evaluate aplate material up to 1cm²sample area evaluating cell, Plate material be 1or10cm². The surface area may at eachendofthecell. two different materials it ispossible to place 1 to 10cm²sample area
Galvanic kit1cm² Flat cell kit1cm² Content Galvanic cell kit1cm² Galvanic cell 1cm²
A-012022 A-002222 - - - - A-011951 Catalog n° Mask for 10cm²(20pieces) Mask for 5cm²(20pieces) Mask for 1cm²(20pieces) Bridge tubefor 6mmreference electrode Ag/AgCl reference electrode (OD:6mm) Options (L: 145mm,OD:6mm) Coating cell Catalog n° Coating cell Graphite rod counter electrode O-ring for coating cell Metallic clamp Rubber cupwithtwo holes Nylon basewiththree feets Glass for coating cell Content Coating cell kit 092-FLAT/1 EL-FLAT EL-GAL-1 Galvanic kit10cm² Flat cell kit10cm² Content Galvanic flat cell kit10cm² Galvanic cell 10cm²
EL-P-013 EL-P-012 EL-P-011 EL-P-008 A-012167 EL-P-009 EL-P-006 EL-P-005 EL-P-004 EL-P-003 EL-P-002 EL-COAT Catalog n°
Catalog n° 092-FLAT/10 EL-FLAT-2 EL-GAL-10 12/13
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware CorrosionCorrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cellcell cell Glassware Big volume cell vials cell vials Small volume Small &bigvolume cell vials
cell holderfor 20mLvial cell holderfor kingsizevial (1L) water jacketed-glass vial water jacketed-glass vial sample vial sample vial on request. volumes are available Note thatother offered separately. the cell vialsare also To complete akit, 1 to 100mL Small volume cell vials, A-012672 A-011504 ID 15.6 15,6 40 18 100 mL 20 mL 1,000 mL 5 mL 100 mL 80 mL 1,000 mL 20 mL Volume 80 mL 5 mL 30 40 70 mm 55 mm 120 mm 40 mm 50 mm 90 mm 120 mm 28 mm OD 90 mm 18 mm cell holderfor A-011506 46.4 mm 25.6 mm 90 mm 15.6 mm 46.4 mm 62 mm 90 mm 25.6 mm 62 mm 15.6 mm ID A-001209 80 mm 50 mm 200 mm 40 mm 72 mm 85 mm 175 mm 50 mm 80 mm 30 mm Height A-001051 25.6 55 1 1 1 1 1 1 1 1 1 10 1 10 Quantity
A-001056 ID 25.6 28 RRDE-3A, bulkelectrolysis SVC-2, SVC-3 SVC-2, SVC-3 EL-CORR-2 VC-4 RRDE-3A, bulkelectrolysis EL-CORR-1 EL-ELECTRO-2 EL-CORR-1 SVC-2, SVC-3 EL-ELECTRO-1 VC-4 Purpose 50 50 A-012632 ID 46.4 A-012652 A-001209 A-001051 EL-C-002 A-012672 A-012632 EL-C-019 EL-A-002 EL-C-001 A-001056 EL-A-001 A-011504 Catalog n° A-012652 50 45 70 72 80 cell holderfor EL-C-001 ELECTROCHEMISTRY ACCESSORIES Big volume cell vials, 100 to 2,000mL EL-C-019,
EL-C-001 EL-A-001 120 90 62 90 80
175 EL-A-002 Dimensions inmm EL-C-002 62 90 120 90 85 200 14/15
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes GlasswareGlassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell Glassware for corrosion cells Bridge tubes EL-C-008 10 bridge tubes Small size 250 EL-C-017 10 EL-F-004B 10
60 140 EL-F-004 10 A-012176 6 120 60 65 A-012177 9 65 220 for corrosion cells Purge tubes 10 EL-C-006 ± is approximately each dimension The tolerance of 0.5 mm.
200 100 10
EL-C-016
ELECTROCHEMISTRY ACCESSORIES with ceramic junction for corrosion cells for analytical cells for analytical cells for corrosion cells Small sizebridgetube Glassware for analytical cells Bridge tubes (2) Setof10porous 4mmglass frit(CoralPor™) withPTFEheatshrink(200mm) (1) Setof10porous 2.8mmglass frit(CoralPor™) withPTFEheatshrink(200mm) Options Bridge tube Purge tube Purge tube Bridge tube Bridge tube EL-A-017 10
165 EL-A-008 10
Ø 8mm Ø 6mm single single Ø 8mm Ø 6mm Ø 6mm
standard (non aqueous) short Ref. electrode Ø 9mm double double Ø 6mm standard Ø 9mm with reverse sleeve
200 6 mm 10 mm 10 mm 10 mm 10 mm 10 mm 6 mm OD 8 mm 8 mm 12 mm 9 mm 10 mm 10 mm 10 mm 10 mm 8 mm 9 mm 10 mm Purge tubes for analytical cells
10 EL-A-006 138 mm 68 mm 250 mm 200 mm 165 mm 165 mm 250 mm 68 mm Height 138 mm 70 mm 68 mm 120 mm 220 mm 200 mm 155 mm 250 mm 68 mm 140 mm
1 22 1 1 1 1 1 2 Quantity 1 1 2 1 1 1 1 1 22 1
SVC-2, SVC-3 EL-CORR EL-CORR EL-ELECTRO EL-ELECTRO EL-CORR SVC-2, SVC-3 Purpose SVC-2 EL-FLAT EL-CORR EL-ELECTRO EL-ELECTRO SVC-2 EL-FLAT 165
Vycor typecompatibility 092-VYC4 092-VYC3 100 EL-A-016 10 (2) (1) R-AL210 EL-C-008 A-012176 A-012306 EL-C-017 EL-C-016 EL-A-016 EL-A-017 R-AL120 R-AL100 092-VYC4 092-VYC3 Catalog n° A-012177 EL-F-004 EL-C-006 EL-A-006 EL-A-008 R-AL110 A-012307 EL-F-004B R-AL100 with ceramic junction Bridge tubes
70 R-AL110 10 250 Dimensions inmm R-AL120
138 16/17
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes GlasswareGlassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell each measurement. electrode after recommend polishingthe of theelectrode we To refresh thesurface materials. built withdifferent up to 6mmand from 7 µm diameters ranging is offered with electrodes (WE) range ofworking application, awide To address every Electrodes Working electrode maintenance
6 µmpolishingdiamond(10mL) Coarse polishingpad(20pieces) Emery paperUF800(20pieces) Diamond polishingpad(20pieces) Alumina polishingpad(20pieces) Spare parts Diamond polishingpad(10pieces) Alumina polishingpad(10pieces) Glass plate (1piece) 1 µmpolishingdiamond(10mL) 0.05 µmpolishingalumina(20mL) Content PK-3 electrode polishingkit Working electrodes maintenance Working electrodes Small type 3 55 15 Standard type 6 55 15 Long type 6 Catalog n° A-002053 A-001042 A-012611 A-001041 A-001040 - - A-002249 A-002054 A-001050 A-011975 110 15 4 Micro type 70 Gauze type 35 25 10 23 Dimensions inmm ELECTROCHEMISTRY ACCESSORIES Carbon paste Working electrodes Platinum Gold Silver Palladium Nickel Copper Iron Carbon
Platinum Carbon long glassy carbon electrode standard carbon paste electrode hole depth4mm standard glassy carbon electrode small carbon paste electrode hole depth4mm CPO carbon paste oilbase1g small glassy carbon electrode micro carbon fiberelectrode standard pyrolytic graphite electrode standard PFCE carbon electrode small PFCE carbon electrode platinum gauzeelectrode long platinumelectrode standard platinumelectrode small platinumelectrode micro platinumelectrode gold gauzeelectrode long goldelectrode standard goldelectrode small goldelectrode micro goldelectrode standard silver electrode small silver electrode standard palladiumelectrode small palladiumelectrode standard nickel electrode micro nickel electrode standard copper electrode micro copper electrode standard iron electrode Electroactivity window oftheworking electrodes indifferent media -3 -2 -1 TBAP/DMF edge plane basal plane pH =14 0.1 MKCI TBAP/ACN 0 pH =7 1 MHCIO4 pH =0 PEEK PEEK Isolation PEEK PEEK PEEK PEEK PEEK PEEK PEEK glass glass PEEK PEEK PEEK PEEK PEEK PEEK PEEK PEEK PEEK PEEK PEEK glass glass glass glass PEEK PEEK PEEK PEEK PEEK PEEK glass glass glass PEEK PEEK PEEK PEEK PEEK PEEK PEEK glass PEEK PEEK glass PEEK PEEK 1 OD 6 mm 6 mm 10 mm 3 mm 6 mm 6 mm 6 mm 3 mm 3 mm 4 mm 4 mm 6 mm 6 mm 6 mm 6 mm 3 mm 80 mesh 6 mm 10 mm 6 mm 6 mm 3 mm 4 mm 4 mm 4 mm 4 mm 100 mesh 6 mm 10 mm 6 mm 6 mm 3 mm 4 mm 4 mm 4 mm 10 mm 6 mm 6 mm 3 mm 6 mm 3 mm 6 mm 4 mm 6 mm 6 mm 4 mm 6 mm 6 mm 2 Electrode size 3 mm 3 mm 5 mm 1.6 mm 3 mm 1.6 mm 1 mm 1.6 mm 1 mm 33 µm 7 µm 3 mm 3 mm 3 mm 1 mm 1 mm 25 x35mm 3 mm 5 mm 3 mm 1.6 mm 1.6 mm 100 µm 25 µm 15 µm 10 µm 25 x35mm 3 mm 5 mm 3 mm 1.6 mm 1.6 mm 100 µm 25 µm 10 µm 5 mm 3 mm 1.6 mm 1.6 mm 1.6 mm 1.6 mm 1.5 mm 100 µm 1.6 mm 3 mm 25 µm 1.5 mm 3 mm 3 V vs SCE ± 4% Catalog n° A-012744 A-002210 A-002417 A-001010 A-002223 A-002012 A-012297 A-002411 A-012298 A-002412 A-002002 A-002007 A-002253 A-002252 A-002408 A-002409 A-011854 A-002250 A-012745 A-002420 A-002422 A-002013 A-002313 A-002009 A-002003 A-002015 A-002005 A-002251 A-012746 A-002418 A-002421 A-002014 A-002314 A-002010 A-002004 A-002006 A-002416 A-002419 A-002011 A-002315 A-002019 A-002319 A-002016 A-002273 A-002017 A-012584 A-002271 A-002018 A-012585 18/19
Local probes Connection Fuel Battery Quartz Spectro- Rotating ElectrodesElectrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell of Vycor-based or organic media). immersed (aqueous the electrode is the mediainwhich groups according to are dividedinto two Reference electrodes Electrodes Maintenance Ag/AgCl ink reference electrode
electrode. identical to the fillingsolutionofthereference with solution.Thisstorage solutionshouldbe lifetime isto keep itinasealed preservative vial maintain thereference electrode capability and When itisnotinuse,therecommended wayto immersed intheelectrolyte Store your reference electrode RHE Reversible Hydrogen Electrode kit main bodyinpolyacetal resin RE-61AP Hg/HgOreference electrode free from chloride RE-2CP Hg RE-2BP calomel reference electrode Ag/AgCl ink,2mL PEEK resin RE-3VP Ag/AgClscrew typeelectrode, screw type,poly acetal resin RE-3V silver, silver chloride reference electrode RE-1CP silver, silver chloride reference electrode RE-1S silver, silver chloride reference electrode RE-1B silver, silver chloride reference electrode Small sizereference electrode for aqueousmedia(Ag/AgCl,Hg) for aqueousmedia(Ag/AgCl,Hg) Small sizereference electrodes Double junctionchamberkitfor Bridge tubeØ9.0mm(22pieces) Bridge tubeØ9.0mm(2pieces) RE-PV preservative vialfor reference electrode, 10mL Options (1) Setof10porous 2.8mmglass frit(CoralPor™) withPTFEheatshrink(200mm) Spare parts RE-1B 2.8 2 SO 80 4 reference electrode, RE-1S 2.8 50 RHE
RE-1CP (1) (1)
IPPG* IPPG* Junction - IPPG* ceramic ceramic ceramic - - IPPG* IPPG* ceramic flash point:82°C viscosity: 50,000 surface resistance: 0.2Ω/sq/25.4µm RE-2BP ± 10,000 [email protected]°C compounds into thepores. This iscaused bytheadsorptionoforganic Yellowish discoloration indicates contamination. Replace thevycor when needed electrode, asample holdercan beused. To prevent contamination ofthereference Prevent contamination 3 MNaCl 3 MNaCl Electrolyte HCl orH 1M NaOH saturated K saturated KCl 3 MNaCl 3 MNaCl saturated KCl RE-2CP 2 SO 45 45 2 4 SO
4 SECM electrolysis, RRDE-3A,flat cell SVC-2, SVC-3, VC-4, bulk for alkalinemedia electrolysis, RRDE-3A,flat cell SVC-2, SVC-3, VC-4, bulk for flow cell spectro for flow cell spectroelectrochemcial electrolysis, RRDE-3A,flat cell SVC-2, SVC-3, VC-4, bulk for acidicmedia(pH electrochemcial cell SEC-3F cell SEC-3F Purpose for micro CV cell, IDA measurment RE-3V 40.5 11
RE-61AP < 2) 6 50 40
Catalog n° A-013375 A-012307 A-012177 A-012108 092-VYC3 A-013373 A-013395 A-013431 A-013430 A-011464 A-012170 A-012169 A-013429 A-012168 A-012167
A-012177 the body. Thisgives thepossibility to fillitregularly. during storage ortransport, theelectrolyte isseparated from ELECTROCHEMISTRY ACCESSORIES To RE-7 nonaqueousreference electrode (Ag/Ag Small sizereference electrode for nonaqueousmedia(Ag/Ag Bridge tubeØ9.0mm(22pieces) Bridge tubeØ9.0mm(2pieces) RE-PV preservative vialfor reference electrode, 10mL Options (1) Setof10porous 2.8mmglass frit(CoralPor) withPTFEheatshrink(200mm) Sample holder6mmdiameter (for RE-7)(2pieces) PTFE cap with Ag wire (for RE-7S) PTFE cap with Ag wire (for RE-7) Electrolyte solution(10mL) Spare parts RE-7VP nonaqueousreference electrode (Ag/Ag RE-7V nonaqueousreference electrode (Ag/Ag RE-7S nonaqueousreference electrode (Ag/Ag for nonaqueousmedia(Ag/Ag Small sizereference electrodes RE-7 avoid 9 68 10 Electrolyte 65 solution electrolyte 44 20
A-012108 leakage or Electrolyte RE-7S concentration solution + ) 10 + (1) + ) screw type,poly acetal resin ) + (1) ) screw type,PEEKresin
23 20 due to + ) evaporation Electrolyte RE-7V solution + IPPG* IPPG* IPPG* IPPG* Junction )
5.5 11 30
0.205 V 0.236 V 0.624 V 0.930 V 0.542 V 0.241 V 0.197 V 0.650 V 0.194 V 0.000 V E/V vs NHE at 25 °C 25 at NHE vs E/V
*** Tetra ButylAmmoniumPerchlorate ** * IonPermable Porous Glass Electrolyte Ag/Ag Ag/Ag Ag/Ag Ag/Ag 35 Acetonitrile + + + + /ACN**/TBAP*** /ACN**/TBAP*** /ACN**/TBAP*** /ACN**/TBAP*** Ag/AgCl/ KCl (3.5M) Hg/Hg Fc/Fc Hg/HgO/ NaOH(0.1M) Ag/Ag Hg/Hg Ag/AgCl/ KCl (sat) Hg/Hg Ag/AgCl/ NaCl(sat) NHE NormalHydrogen Electrode Electrolyte RE-7VP solution + + TBAP(0.1M)ACN 2 2 2 TBAP(0.1M)ACN Cl Cl SO 2 2 NaCl(sat) KCl (sat) 4 /K 5.5 11 30
Purpose flow cell flow cell SECM CV 2 SO Dimensions inmm 4 (sat) Catalog n° A-012307 A-012177 A- 012108 092-VYC3 A-012176 A-012058 A-012057 A-012549 A-012174 A-012173 A-012172 A-012171 35 20/21
Local probes Connection Fuel Battery Quartz Spectro- Rotating ElectrodesElectrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell -Im(Z)/Ohm 1,000 2,000 3,000 Electrodes 0 0 Re(Z)/Ohm 2,000 4,000 Conical ringsfor 8mmOD 12mmelectrodes (4pieces) (1) Options Ag/AgCl reference electrode for EIS Hg/HgO reference electrode in1MKOH withfiber rod Hg/HgO reference electrode in0.1MKOH for CV Ag/AgCl reference electrode SatKCl for CV Hg/HgSO Calomel reference electrode inKCl satfor CV, curved Calomel reference electrode inKCl satfor CV, straight Calomel reference electrode nonaqueous(LiCl) Hg/HgSO Salt bridgewithreverse sleeve, nonaqueous King sizereference electrodes for general purpose Red rod reference electrode King sizereference electrodes Salt bridge R-REF621 Cable connection for screw cap electrode, to theBio-Logicinstruments recommended to connect thesereferences electrodes 4 4 reference electrode insat.K reference electrode insatK R-XR110 2 R-XR200 2 SO SO 4 4 for CV , chloride free
R-XR300
screw cap screw cap banana cable screw cap screw cap screw cap screw cap screw cap screw cap Connection type banana cable screw cap banana plugof2mm screw cap banana cable banana plugof2mm banana plugof4mm (1) (1) (1) (1) (1) (1) (1) (1) (1) (1) R-XR400 Junction ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic ceramic 120 103 mm 103 mm 138 mm 103 mm 160 mm 120 mm 120 mm 120 mm 120 mm 120 mm 120 mm 103 mm 103 mm 103 mm Length 250 mm 1 m 138 mm 100 mm 70 mm 1 m R-XR820
12 mm 7.5 mm 8 mm 7.5 mm 8 mm 8 mm 8 mm 8 mm 8 mm 8 mm 8 mm 8 mm 8 mm 8 mm OD 8 mm 8 mm 12 mm
m
e EIS
160 a
R-REF251 R-REF601 R-AL210 R-X31M012 R-REF201 R-XR820 R-XR440 R-XR400 R-XR300 R-XR200 R-XR150 R-XR110 R-REF921 R-REF621 R-REF421 R-AL110 Catalog n° R-AL120 R-CRI9439 R-AL100 R-A94L111 R-CL111 s
u
r e m e nt Gold gauzeelectrode, PEEK Platinum gauzeelectrode, PEEK Stainless steel Nickel Gold ELECTROCHEMISTRY ACCESSORIES Platinum gauzeelectrode, platinumwire of51mm Platinum Counter electrodes Counter electrodes Conical ringsfor 8mmOD 12mmelectrodes (4pieces) Platinum Metallic electrodes (1) Options Glassy carbon A-002222
to theBio-Logicinstruments recommended to connect thesereferences electrodes Cable connection for screw cap electrode, (1) A-012198 (1) A-002233 50 A-002234 A-002254 100 mesh 80 mesh 55 mesh A-002250
35 25 x35mm 25 x35mm 50 mm 230 mm 230 mm 57 mm 25 x35mm Length 230 mm 40 x50mm 50 mm 100 25 10 23
0.07 mm 0.08 mm 1.5 mm 0.5 mm 0.5 mm 0.5 mm 0.08 mm Wire Ø 0.5 mm 0.12 mm 0.5 mm ~ 1cm ~ 1cm ~ 2.35cm ~ 3.6cm ~ 3.6cm ~ 0.7cm ~ 1cm ~ 3.6cm ~ 5.1cm ~ 0.7cm Surf. area R-XM110 1 m,bananaplugof4mm 100 mm,bananaplugof2mm 1 m,bananaplugof2mm 103 mm 80 mm Length 120 mm 120 mm 120 mm Metallic electrodes 2 2 2 2 2 2 2 2 2 2 flat cell flow cell RRDE-3A, bulkelectrolysis, SVC-3 RRDE-3A, bulkelectrolysis, SVC-3 RRDE-3A, bulkelectrolysis, SVC-3 SVC-3 evaluating cell SVC-2, VC-4, plate material Purpose OD 8 mm 8 mm 8 mm 8 mm 12 mm R-XM120 Wire dimension rod Øof3mm Ø 1mm plate 5xmm plate 8xmm disk of10mm R-XM140
Dimensions inmm R-XM150 A-702439 A-012198 A-012639 A-012638 A-002234 A-002233 A-002254 A-002251 A-002250 A-002222 Catalog n° R-CL111 R-A94L111 R-CRI9439 R-X31M012 Catalog n° R-M291C R-XM110 R-XM120 R-XM140 R-XM150 120 22/23
Local probes Connection Fuel Battery Quartz Spectro- Rotating ElectrodesElectrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell Features controlled byBio-Logicelectrochemical workstation. RRDE-3A isable to beoperated asastand-alone unitordirectly It iseasyto remove andreplace thecell vial. is easyfor rinsing,cleaning, andreplacing theelectrodes. purging insidethecell vial.Additionally, theaccess to glass cell The unitalsoprovides anadjustable valve system for inertgas a DCservo-motor. Electrodes are smallandrapidly interchangeable. RRDE-3A iselectronically controlled byaclosed loop circuit driving the modulation. allows theusers to control accurately theelectrode rotation and (RDE orRRDE)measurement. Itsdesign(shortstainless steel shaft) RRDE-3A isasystem thatcan beusedto perform hydrodynamic (RRDE) Rotating RingDiskElectrode Rotating Bandwidth Rotation control type Accuracy Setting resolution Rotational range Weight Dimensions (WxDH) Power Temperature Inlet gaspressure Specifications - - - Open architecture for easyaccess to cell is available, remote andmanualcontrolled purge lines Small sample volume (upto 10-15mL),gas lineconnector Remote- andmanual-controlled rotation electrodes 60 Hzat3,500rpm PLL (phase-locked loop) < 0.1% 1 rpm 100 -8,000rpm 6 kg 185 x(base:230,body:120)400mm 100-240 VAC, 50/60Hz 10-50 °C 5 PSI peak-to-peak modulation base and1,000rpm
Bearing assembly Bipotentiostat cable for two standard channels DB9 cable to control RRDE-3A (100 mL,OD70mm,ID46.4H80mm) Water-jacketed glass cell Options Power cable Instruction manual PTFE cap for RRDE-3A Tygon tubing, OD6.4mmxID3.2(1.3m) Nipple for purge valve Spin coating adapter RRDE-3A glass cell vial100mL Content and counter electrodes (page23)have to bepurchased separately. Working electrodes (page25),reference electrodes (page20) RRDE-3A apparatus Rotating RingDiskElectrode
Catalog n° A-012625 092-22/12 092-22/11 A-012652 - - A-012631 A-010058 A-012065 A-012064 A-012632 A-012180
PK-3 polishingkit Option RDE Working electrode Disk electrode polishing andexchanging tool kit Tool kit RDE ELECTROCHEMISTRY ACCESSORIES RRDE Disk Replaceable Electrode tips RRDE Standard tips RDE Disk electrode RRDE Ring electrode Disk electrode content platinum diskreplaceable electrode kit content gold diskreplaceable electrode kit content glassy carbon diskreplaceable electrode kit content platinum ring/GCdiskreplaceable electrode kit disk assembly PTFE spacer (3pieces) platinum disk disk assembly PTFE spacer (3pieces) gold disk disk assembly PTFE spacer (3pieces) glassy carbon disk PTFE spacer (3pieces) glassy carbon disk platinum ringassembly Ø 12mm Ø 3mm Ø 12mm Ø 7mm Ø 4mm A-011172 carbon paste disk,hole depth4mm tungsten disk titanium disk tantalum disk nickel disk copper disk glassy carbon ring/glassy carbon disk silver disk gold ring/platinumdisk aluminum disk platinum ring/golddisk gold disk gold ring/glassy carbon disk platinum disk platinum ring/glassy carbon disk glassy carbon disk platinum ring/platinumdisk A-011162 A-013340 A-013361 A-013339 A-013367 A-013365 A-013361 A-013339 A-013366 A-013364 A-013361 A-013339 A-013338 A-013362 A-013339 A-013338 A-013337 A-013336 Catalog n° A-011163 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm 25 mm Tips length 25 mm 25 mm Disk electrode polishingandexchanging tool kit RRDE platinumring/GCdiskreplaceable electrode kit 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm 12 mm Tips OD 12 mm 12 mm A-011164 ------5.0 mm - 5.0 mm - 5.0 mm - 5.0 mm - 5.0 mm Ring ID - 5.0 mm A-011170 ------7.0 mm - 7.0 mm - 7.0 mm - 7.0 mm - 7.0 mm - 7.0 mm Ring OD 3.0 mm 3.0 mm 3.0 mm 3.0 mm 3.0 mm 3.0 mm 4.0 mm 3.0 mm 4.0 mm 3.0 mm 4.0 mm 3.0 mm 4.0 mm 3.0 mm 4.0 mm 3.0 mm 4.0 mm Disk Ø A-011171 A-011975 A-011973 A-011972 A-011971 A-011970 A-011969 A-011968 A-012618 A-011967 A-012617 A-011966 A-011164 A-011171 A-011163 A-011170 A-011162 A-011169 A-011172 Catalog n° A-011169 24/25
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell EL-ELECTRO-2 orEL-ELECTRO-3 kit. This RDEcan beusedwiththeEL-ELECTRO-1, and achieve a“Levich” typeexperiment allinonego. the rotation speedfrom onemethodto anothermethod potentiostat/galvanostat. You can program thevariation of The speedcontrol unitcan bedirectly driven from aBio-Logic rotation speedisclearly displayed onafour-digit LCD. fully reproducible experimental conditions. Themeasured speed. Itoffers accuracy better than The CTV101 speedcontrol unitcontrols theEDI101rotation a widerange ofcells. Thanks to itsconic shaftholder,theEDI101can beusedwith standard orcustom materials: platinum,glassy carbon, gold... available withawidechoice ofquick-fitexchangeable tipsin ideal for usewithanyBio-Logicpotentiostat/galvanostat. Itis The EDI101isaversatile andruggedrotating diskelectrode (RDE) Rotating DiskElectrode Rotating Weight Dimensions Consommation Power Temperature Gas inlet for brushcontact purging Material ofEDI101 Setting resolution Eccentricity Accuracy Rotational range Specifications electrodes EDI101: 0.3kg CTV101: 1.5kg EDI101: 255mm(length) CTV101: 80x240230mm(WDH), 12 VA 230 Vac, 47.5-63Hz 5 -40°C Ø 2mm KeI-F 1 rpm < ±0.1mm < 0.1% 100 -5,000rpm ± 0.1% for precise and
DB9 cable to control RDE Adapter EDI(banana4mmfemale, banana2mmmale) EDI tip BEC/EDI electrochemical cell withglassware andelectrodes Options BNC-BNC connector 1m EDI101 RDEwithouttip(10-5,000tr/min) CTV101, controlling unitfor EDI101 Content electrode rotator Rotating DiskElectrode system includingcontrol unitand Rotating DiskElectrode
I/µA 100 200 300 400 500 600 700 0 0 gold, L40mm platinum, L40mm sample holder stainless steel without anymaterial nickel silver graphite copper gold gold platinum platinum glassy carbon glassy carbon 0,2 0,4 E we /V 0,6 0,8 Ø 4mm Ø 5mm Ø 11mm Ø 5mm Ø 5mm Ø 5mm Ø 4mm Ø 5mm Ø 5mm Ø 2mm Ø 5mm Ø 2mm Ø 5mm Ø 3mm 1
Catalog n° 092-22/11 R-X41V001 R-A35T456 R-A35T452 R-A35T450 R-A35T420 R-A35T402 R-A35T160 R-A35T150 R-A35T140 R-A35T130 R-A35T120 R-A35T110 R-A35T105 R-A35T100 R-A35T095 R-A35T090 R-XR51V001 COR28100 R-A35T040 R-R21V035 R-RDE/EDI An example oftheLevich analysis isperformed - - - - - - - Where: I and thephysical parameters asfollows: determination whichisD=6.36x10 analysis leads to thediffusioncoefficient (D) and presented intheimagebelow. TheLevich voltammograms. Theresulting CVs are overlaid from 10rpmto 2000rpm,and 13 twin-cycle cyclic The sequence comprised of13rotational velocities is aglassy carbon diskelectrode. in KCl (0.1M)solution.Theworking electrode on a5.5mMPotassium Hexacyanoferrate (III), limiting current (I proposed therelationship between thevoltammetry A 20 ELECTROCHEMISTRY ACCESSORIES RDE applications Rotating electrodes D = L = C istheelectroactive speciesconcentration v isthekinematicviscosity (cm²/s), D isthediffusioncoefficient (cm²/s), A isthediskarea (cm²), F istheFaraday constant (F=96,485C/mol), (dimensionless), n electrons involved withinthereaction ω istherotational velocity (radian per second), Current/mA (mol/cm 0.08 0.28 0.48 0.68 0.88 ± ( th 0.62 nFAD century electro-chemist, Dr. Levich 0.62 nFAv 3 ). 1 m 2/3 -1/6 L , A)ofarotating diskelectrode ω C 1/2 v ) 3/2 -1/6 ω 7.57 ⁄s C -1/2 -6 cm²/s. 14.1
Of thesetwo options,thelatter ispreferred that isavailable inEC-Lab on theringelectrode. ItistheCV-CA technique disk electrode andaconstant voltage isapplied In atypical experiment, aCV isperformed onthe reduction oroxidation atthering,respectively. potential. Thisnew speciesisdetected by are oxidized orreduced according to theapplied At thediskelectrode, theelectro-active species cyclers) offer suchelectrode connection type. Bio-Logic multichannelpotentiostats (except because theleakage current isless. Allofthe - - This can beachieved intwo different ways: (to avoid anyground loop trouble) isneeded. in thesamesetup,aspecificconnection mode Because ofthepresence oftwo working electrodes appropriate instrument for RRDEapplications. SP-300 equippedwithtwo channelswould bean electrode andtheotherto control thering.An electrodes i.e.onechannelto control thedisk needed. Abipotentiostat controls thetwo working For RRDEmeasurement, abipotentiostat is RRDE techniques folder. instruments provides thisuniquecapability. The “CE-to-ground” modeoftheBio-Logic grounding thecounter electrode. potentiostat infloatingmode), isolating thetwo channels(atleast one ® inthe“bipotentiostat”
26/27
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell spectroscopic measurements. to synchronize electrochemical and The spectrometer isequipped withatrigger cuvette holder). three parts(spectrometer, lightsource and The spectroelectrochemical kitiscomposed of elucidate electrochemical reaction mechanisms. Spectroelectrochemistry (SEC)can beusefulto Spectrometer Spectro -0,2
Absorbance 0,2 0 300 Wa electrochemistry ve le 400 nght 500
270 sec 240 sec 210 sec 180 sec 150 sec 120 sec 90 sec 60 sec 30 sec
Cuvette holder Light source Spectrometer Content combo kittype Spectrometer Connecting cable to synchronize thespectrometer andtheBio-Logicpotentiostat Option Reflectance transmittance Absorbance/ Transmittance Emission Irradiance Fluorescence Fluorescence Scattering Utilization modes
- - - - - - - - - - - - Insitu metal monitoring - - - - - - Textile qualitycontrol Activation energy ofphotocatalytic species Film thickness/composition (qualitycontrol) Freshness testing DNA quantification Polymer extrusion processes Concentration ofchemicals (solution) Astronomy (e.g, spectra ofHale-Bopp, Biology (DNA,protein, Marine organisms Luminescence (PL,EL),LED&laserwavelength plasma monitoring) glasstransition crystallize temperature) Physical transition phenomena(e.g,meltingpoint, Raman spectroscopy Oil concentrations ofoil/water system Tissue diagnosis agronomy, agrochemicals, pollutionstudies, forestry, ecology) Plant efficiency(plantphysiology, plantbreeding, horticulture, trace studies, hydrocarbon detection, dissolved oxygen) Environmental fields(waste water analysis, ground water histamine-analysis, algamonitoring) cell proliferation assay, SEC2000-UV/VIS SEC2000-CUV SEC2000-DH UV SEC2000-UV/VIS SEC2000-UV/VIS
Catalog n° A-012195 A-012193 A-012856 A-012838
SEC2000-CUV with SEC2000-TH visible SEC2000-VIS/NIR SEC2000-VIS/NIR diffusion plate SEC2000-VIS/NIR
A-012194 A-012971 A-012973 Catalog n° 092-22/11 A-012244 Catalog Dimensions (WxDH) ELECTROCHEMISTRY ACCESSORIES Catalog n° Cuvette holder D2 lamp Spectral range (Halogen +D2) Light source Operating system Interface Optical entrance A/D resolution Dark noise Accuracy Resolution Grating Wave length range Detector Spectrometer (2). Value for less than50%power consumption of240nm. Bulb Spare parts (1). Slitcould be selected from: 10,25,100,200μm. Catalog Dimensions (WxDH) Connector lamp Halogen Gamma ra Pic 200 nm ometer 100 (UV-C) n° n° power consumption (240nm) spectral range light source bulb life drift stability bulb life y 280 nm Ultraviol (2) X-ray UV-B Nanomete et ray(UV) 315 nm r Ultraviol UV-A 98 x11835mm < 5x10 200 -400nm 200 -1,100nm Windows USB 2.0 SMA905 14 bit < 2mAbs < 1%ataAbs 1.8 ±0.2nm:slit50µmx1,000(standard) blazed at400nm 220 -800nm 2,048 pixels CCDarray A-012221 (UVbulb) A-012193 < 0.25%/h 1 x10 A-012856 98 x11835mm SMA905 included > 2,000h > 1,000h (deuterium &tungsten halogen) SEC2000-DH Lightsource SEC2000-UV/VIS combo kit 400 nm A-012195 SEC2000-UV/VIS combo kit et ra -3 AU y -8 TM W/nmsr XP Electromagnetic spectrum Micr ometer Infrar Visibl ed e light
Millimeter (1) Micr SEC2000-TH Lightsource SEC2000-VIS/NIR combo kit 98 x11835mm - (tungsten halogen) 1.8 ±0.2nm:slit50µmx1,000(standard) - 360 -2,000nm USB 2.0 SMA905 14 bit < 2mAbs < 1%ataAbs blazed at750nm 500 -1,000nm 2,048 pixels CCDarray A-012222 (TVbulb) A-012194 Windows - - A-012971 98 x11835mm SMA905 notincluded 1,500 h - SEC2000-VIS/NIR combo kit A-012244 700 nm owaves Near IR TM XP 1,400 nm Infrar Mete IR ed (IR) r Radio waves 3,000 nm
F Kilo ar IR mete 10,000 nm (1) r 28/29
Local probes Connection Fuel Battery Quartz Spectro-Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistryelectrochemistry electrodes cell cell Static experiment Spectro electrochemistry Purging tube(ETFE),1m RE-7 nonaqueousreference electrode RE-1B Ag/AgClreference electrode Options Quartz glass spectroelectrochemical cell kit 0.5 mm 1 mm
UA -0.1 0.1 0.2 0.3 0.4 0.5 300 0
350
gauze working electrode purging tube(ETFE,100mm) PTFE cap thin layer quartzglass cell platinum counter electrode Content gauze working electrode purging tube(ETFE,100mm) PTFE cap thin layer quartzglass cell platinum counter electrode Content
vel Wa 400 ength (nm) ength 450
500
550
600 A-012904
650
700
4
6
8
10
12
14 16 Platinum height 5mm height 6mm 80 mesh, 80 mesh, A-012907
45 A-012606 A-011498 - A-011501 A-012815 A-012609 - A-011501 A-012907 A-012906 Catalog n° A-012813 A-012904 A-011498 40 100 mesh, 100 mesh,
Gold height 5mm height 6mm 6 A-012906
39 - A-011501 A-012815 A-012609 - A-011501 A-012907 A-012906 A-012814 A-012905 A-012607 A-010537 A-012171 A-012167 A-012017 Catalog n° A-011501 13 Purging tube 5 mm 0.5 mm 5.5 mm 6 mm 1 mm 6.5 mm 100 Fibre andlens Flow experiment Gasket electrode grid Working ELECTROCHEMISTRY ACCESSORIES cell for flow screw type electrode Reference Options PTFE tube(1m) Silicon tube(300mm) Dynaseal PEEKfingertight Needle adaptor Stainless tubeOD1.59mm(length of50mm) SEC-2F S500silicone gasket SEC-2F flow cell Content SEC-2F spectroelectrochemical flow cell Flow experiment
PTFE silicone Ø 4inchx0.5mm 10 x0.5mm 10 x200.5mm 8 x270.5mm 8 x271mm Ø 10x55mm 400 µmoptical fibre SR,2m 400 moptical fibre SR,250mm T100, 100µmthick(4pieces) T250, 250µmthick(4pieces) T500, 500µmthick(4pieces) S500, 500µmthick(4pieces) ITO electrode (1piece) ITO electrode (30pieces) ITO electrode (10pieces) ITO electrode (12pieces) ITO electrode (4pieces) carbon gridelectrode (1piece) gold (1piece) platinum (1piece) RE-7VP nonaqueous(PEEK) RE-7V nonaqueous RE-3VP aqueous(PEEK) RE-3V aqueous UV/VIS collimating lens, 200-2,000nm block B block A cover base Quantity 1 1 2 1 1 2 1 1 1 1 A-011522 A-012667 A-012666 A-012665 A-012664 A-012661 A-011827 A-011233 A-010887 A-011465 A-012658 A-012657 A-012656 A-012655 A-012174 A-012173 A-012170 A-012169 Catalog n° A-012234 - - - - A-012198 A-012661 - - - - A-012660 Solution volumes Gasket of Reference electrode Collimating Lens Counter electrode Silicone gasket 500µm Working electrode Outlet Gold gridelectrode A-012656 500 µm 250 µm 100 µm Inlet Volume 230 µl 11.5 µl 4.6 µl 30/31
Local probes Connection Fuel Battery Quartz Spectro-Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistryelectrochemistry electrodes cell cell thin-layer spectroelectrochemistry. The UFS setisconceived to perform cell spectroelectrochemical Thin layer Spectro Auxiliary electrode Working electrode electrode Pseudo-reference Spacer PTFE adapter for optical fibres +optical fibre
electrochemistry Full kit+
PTFE adapter for optical fibres withUV/VIS/NIR collimating lenses (200-2500nm), Options Optical fibre: SMA-SMA connector length 1m 1 spacer (goldworking electrode/platinum auxiliaryelectrode/Ag pseudo-reference electrode) electrode) 1 spacer (platinumworking electrode/platinum auxiliaryelectrode/Ag pseudo-reference PTFE cuvette holderto beusedwithUF-OFA andUF-BS Base stand for optical fibres measurements adjustable focus, SMA-905connection Full kit Thin layer spectroelectrochemical cell kit PTFE mask Plug spectrophotometer universally fitthe cell ina XY holder(withmagnets)to Stainless steel bodycell electrode) electrode/Ag pseudo-reference + 1spacer (platinum auxiliary 1 PTFEwindows aligner Content Platinum electrode working platinum UF-Full UF-M UF-P UF-XY - UF-SEC-PT UF-Full-PT Catalog n° Gold electrode gold working
UF-M UF-P UF-XY - UF-SEC-AU UF-Full-AU Catalog n° 092-101 UF-SPA UF-SPP UF-C UF-BS UF-OFA reactant/product concentrations inthecell and necessary bothto ensure homogeneityofthe Small potential sweep rates (2-10mV/s)are may alter thesolution/analyte composition. the presence ofirreversible redox reactions, which condition). Potential driftscan beobserved in constant intimeeachgiven experimental the solutionmedium(butisexpected to remain pseudo-reference electrode, whichissensitive to of interest: infact, theUFspacer hasansilver your SECcell to better localize theredox process A cyclic voltammetry shouldberegistered in to control theresistive effects. in thin-layer electrochemical cells of thecell reactant andminimaldiffusioneffects thin-layer cells, indicating exhaustive electrolysis potential plot isacharacteristic behaviorof current flow following thepeakincurrent electrolyzed. Thedropping to nearzero ofthe the electro-active speciescan beexhaustively the diffusionprocess andtherapidity withwhich of thin-layer cells istheabsence oftheeffect of transfer can beignored. Themost significant virtue is smaller thanthediffusionlayer andthemass confined bythecell walls,sothatthecell thickness layer (≤0.2mm)adjacent to theelectrode is In suchfinite diffusionconditions, athinsolution ELECTROCHEMISTRY ACCESSORIES Finite diffusionconditions applications Spectroelectrochemistry
-80 -40 I/mA 40 80 0 Scan rate:5mV/s Fe 0 rr oc ene inCH 2 0.2 Cl 2 / NBu 4 E PF we /V 4 (0.2M) 0.4 (1) (2) . 0.6
(2): (1): optical path. the experiment itself to avoid changesofthe changing thetightness ofthecell screws during For thesamereason, itisalsoimportant to avoid each Infra-Red spectroelectrochemical experiment. measured background shouldbeobtained before common solvents andelectrolytes, avery carefully Due to thehighInfra-Red absorbance ofmore the concentration can beadapted. most optimizedconcentration, butinsomecases, A milli-molarconcentration appears to bethe with alow molarextinction coefficient. may berequired to study thechanges ofbands of arelatively highconcentration ofthesample due to thenarrowness oftheoptical path,theuse may bepreferred. However, insomecases, low scan rates andlow sample concentrations the current shouldalsobekept low whichmeans To maintain theohmicdrop aslow aspossible, -1 ε/cm-1.M L. Marchetti, P. Zanello, Chem.Eur. J.,2008,14,847 P. Leoni,F. Marchetti, C.Bonaccorsi, F. Fabrizi deBiani, 1991, 317,179. M. Krejčik, M.DanĕkandF. Hartl,J.Electroanal. Chem., 100 200 300 400 0 Step of50mV Starting potential:150mV 400 λ 800 /nm 1,200
32/33
Local probes Connection Fuel Battery Quartz Spectro-Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistryelectrochemistry electrodes cell cell using aDB9-8BNCcable (catalog n°:092-22/1). Analyzer (QCA922) to aBio-Logicpotentiostat It ispossible to connect theQuartzCrystal are alsoreflected onthetwo analog outputs. frequency andtheresonant resistance which The instrument monitors boththeresonant EQCM Quartz
-0.2 /mA 0.2 0.4 0.6 0.8 0 0 crystal analyzer E 0.5 we /V 1 092-QCA-FC
Holder isneededto getafull Options Male BNC/BNCcable (2pieces, length 1m) EQCM 27MHzmainunitandcable Content Quartz crystal microbalance 27MHzkit EQCM Low flow peristaltic pump Connector from QCA to potentiostat QCM orEQCMset-up SE-CL3 EQCM specifications Power consumption Temperature Weight Dimensions (WxDH) Interface Display Gate time Resistance output ∆F output Resonant resistance range Frequency range
100-120 VAC, 230-240VAC, 50-60Hz,(15W) 0 -40°C 3.3 kg 260 x23088mm IEEE-488, RS-232C,USB 40 digitsx2rows variable (0.1,1.0,10.0s) 1 /24816kΩ full scale: 0-10 V(11bit) ±200 Hz/2kHz20 full scale: ±10V(12bit) resolution 0.1Ω 10-16 Ω, resolution 0.1Hz 1 MHz-10MHz, flow cell (90µL)(PEEK) flow cell (90µL)transparent (PTFE) flow cell (90µL)(PTFE) transparent well cell well cell (PEEK) well cell (PTFE) dip cell static andflow QCA cell
Catalog n° COR28100 SE-QCA922A-00 SE-QCA922A SE-CL6PK SE-CL7 SE-CL6 SE-CL5 SE-CL4PK SE-CL4 SE-CL3 092-QCA-FC EL-AV-008 092-22/1 Quartz resonators ELECTROCHEMISTRY ACCESSORIES 5 MHz Quartz resonator Resonators 9MHz,nosputter Resonators lead wire nosputter (50pieces) Others 9 MHz Surface finishing Polish finish Mirror finish Etching finish Standard finish finish finish mirror standard polish finish etching finish 0.06 µm 0.06 µm 0.6 µm 0.6 µm Roughness
(calibration at5MHzfactory withnocharge whenpurchased)
resonator resonator lead wire lead wire and lead wire lead wire and separated separated
vacuum deposition sputtered vacuum deposition sputtered Electrode materials deposition
platinum electrode (25pieces) ITO electrode (25pieces) gold electrode (25pieces) titanium electrode (25pieces) stainless steel (SUS304)electrode (25pieces) silicon electrode (25pieces) platinum electrode (25pieces) nickel electrode (25pieces) ITO electrode (25pieces) copper electrode (25pieces) graphite electrode (25pieces) gold electrode (500pieces) gold electrode (25pieces) aluminum electrode (25pieces) platinum electrode (25pieces) gold electrode (25pieces) stainless steel (SUS304)electrode (25pieces) platinum electrode (25pieces) nickel electrode (25pieces) molybdenum electrode (25pieces) cupper electrode (25pieces) graphite electrode (25pieces) gold electrode (25pieces) aluminum electrode (25pieces) gold electrode (25pieces) mirror finishno lead wire (50pieces) no lead wire (50pieces) gold electrode (100pieces) gold electrode (30pieces) gold electrode (100pieces) gold electrode (30pieces) Catalog n° SE-9PT-MS SE-9IT-MS SE-9AU-MS SE-9TI-M SE-9SS-M SE-9SI-M SE-9PT-M SE-9NI-M SE-9IT-M SE-9CU-M SE-9C-M SE-9AU-M2 SE-9AU-M SE-9AL-M SE-9PT-S SE-9AU-S SE-9SS SE-9PT SE-9NI SE-9MO SE-9CU SE-9C SE-9AU SE-9AL SE-LEAD/2 SE-5AU SE-9Q-M/2 SE-9Q/2 SE-9AU-P/3 SE-9AU-P/1 SE-9AU-E/3 SE-9AU-E/1 electrode steel Stainless electrode Platinum electrode Gold
34/35
Local probes Connection Fuel Battery QuartzQuartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystalcrystal analyzeranalyzer electrochemistry electrodes cell cell Quartz crystal analyzer with QCM934andthecell (seepage35). Resonators of9MHzare compatible - - - - - - suitable inthebio-sensingfield. a smallmass change. QCM934isespecially Microbalance (QCM934)allows users to measure The specification (27MHz)oftheQuartzCrystal Biosensor QCM via USBinterface. Computer control anddata collection Works withflows cell, well cell, dipcell. Expandable upto 4channels. temperature. frequency, resonant resistance and Simultaneous measurement ofresonant for addedstability. Specially designedoscillationcircuit Excellent sensitivityandresolution. Power consumption Temperature Weight Dimensions (WxDH) Interface Display Gate time Max channel Resonant resistance range Frequency range Specifications 50-60 Hz,(60W) 100-120 VAC, 230-240VAC, 10 -40°C 5.5 kg 320 x280133mm USB 2.0 20 digitsx2rows variable (0.1,1.0,10.0s) 4 2 Ω,resolution 0.1Ω 25 MHz-27MHz,resolution 0.01Hz
and “notebook computer” “Batch cell-based system ofQCM934”,“transparent well/dip cell” Additional channel Options Cable for OSCmodule connection control module Cable for oscillator &temperature Oscillator &temperature control module WinQCM software Main unit Content Batch cell kit Batch mode “notebook computer” “Flow cell-based system ofQCM934”,“perista pump”and Low flow peristaltic pump Additional channel Options Flow cell (90µL) Measurement chamber control module Cable for oscillator &temperature Oscillator &temperature control module WinQCM software Main unit Content Flow cell kit Flow mode Po Po we we r r QCM Qu QCM Qu ar ar tz tz
Cr
93 93 Crys ys 4 4 ta tal l Mi Mi cr c robala obalan nc ce e
Os Os c Os Te illator cillat Co Os Te Co mp c. ntro St mp c. ntro .S or at & St ta .S us l & Te Mo at tu l ta Te Mo mp us s tu du mp du s er le er at le at ur ur e e SE-QCM934-1CHB SE-QCM934-300 SE-QCM934-200A SE-QCM934-200 SE-WQCM SE-QCM934-000 SE-QCM934-B Catalog n° Catalog n° EL-AV-008 SE-QCM934-1CHF SE-QCM934-510 SE-QCM934-500 SE-QCM934-200A SE-QCM934-200 SE-WQCM SE-QCM934-000 SE-QCM934-F T ransparent w QA -CL QA -CL5 Dip cell
3 ell cell
µ The Sauerbrey equationisdefinedas: working electrode surface area. the electrode surface andto asaturation ofthe solution inmethylpyrrol speciesinthelayer close to That can bedueto aninterfacial depletion ofthe very regular buttends to slow down inthelast cycles. mode (quasi-reversible inthisexample). Thegrowth is such apolymer filmisoften dependentonthedeposition voltammetry. Thereversibility ofthecharge transfer in quartz electrode duringthesuccessive cycles ofcyclic Fig. 1presents thepolypyrrol filmgrowth onthe working electrode Polypyrrol filmgrowth onthequartz of 1methylpyrrol monomer(0.01mol.L). solution (Bu The quartzelectrode wasimmersed inanacetonitrile (n+2) voltammetry (20cycles). (used astheworking electrode) usingcyclic The polypyrrol filmwascoated onanAuquartz Electropolymerization ofpyrrol ƒ ∆ƒ =∆ to thequartzcrystal resonator relationship between foreign layers firmly attached and experimental verification ofthemass/frequency Sauerbrey wasthefirst whoprovided adescription A mass increase results inafrequency decrease. density, temperature, andcompression waves). solution properties nearthesurface (includingviscosity, is proportional to themass ofthecrystal, aswell as quartz crystal. Theoscillationfrequency ofthecrystal detector basedonfrequency changesofanoscillating The Quartzcrystal microbalance isamass-sensitive ELECTROCHEMISTRY ACCESSORIES applications Quartz crystal analyzer ρ A: change(g) ∆m: mass frequency change(Hz) ∆ƒ: 0 q q resonant frequency (Hz) : : densityofquartz(ρ : (µ (area between electrodes, cm²) piezoelectrically active crystal area shear modulusofquartzfor AT-cut crystal A N R q =2.947x1011g/(cm.s 2ƒ ρ q 0 2 µ 4 q NPF N R 6 m 0.2mol.L)containing asolution N R q =2.648g/cm³) ² N R )) (1)(2) . np + (2n+2)H +
+ +(2n+2+np)e
-
(3): (2): (1): tool ofEC-Lab in theprocess data is doneautomatically versus elapsedtime and thecurrent density the resonant frequency on onecycle showing Fig. 2:graphic zoom time evolution ononecycle. versus potential ononecycle. Thefigure below shows the The interesting pointisto follow thefrequency evolution 0 and1.018V. vs. frequency andcurrent Fig. 1:overlaid This plot can alsobemadeversus potential (seefig.1). frequency andresistance related to thesuccessive cycles. potential sweep resulting inapseudooscillationof growing. Moreover thevariation isdependentonthe resonant resistance increase while thepolymer filmis Fig. 1shows theresonant frequency decrease andthe during thefilmgrowth QCM measurements The mass calculation at 100mV/sbetween film growth. Scanning the application note details can befound in E Application note #13.Section “Apps &literature of EC-Labdivision”. G. Sauerbrey, Z.Phys.,1959,155,206-222. G. Sauerbrey, Phys.Verh., 1957,8,113-114. we ofthepolymer ® . More (3) (3) .
.
∆ƒ/kHz I /mA -200 -100 I /mA 100 120 < > < > 100 200 300 100 150 200 250 300
-50 40 60 80 50 1,000 0 0 0 E we 90 /V vs.Ag/AgCl/KCl(sat’d) 95 Time/s 0.5 Time/s 100 2,000 105 1 110 -120 -100 -80 -60 -40 -12 -10 -8 -6 -4 -2 -0.6 -0.2 -2.6 -2.2 -1.8 -1.4 0 -1 ∆ƒ/kHz ∆m/µg ∆ƒ/kHz 36/37
Local probes Connection Fuel Battery QuartzQuartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystalcrystal analyzeranalyzer electrochemistry electrodes cell cell Battery 3-electrode test cell utilization are alsoavailable. Other cells for specifics 5-lead typeconnection. VMP3 orMPG2thatoffer theunique This can bedonewithaVSP, positive electrode simultaneously. the behaviorofnegative and (Lithium wire) can beusedto follow (E-ECC-REF) areference electrode With theECC-Reftest cell (positive andnegative electrode). characterize theelectrode These cells allow users to Test cells accessories
ECC-AIR
For optical characterization For gasdiffusionelectrodes (pressure test cell) for drawing gassamples gas evolution and For measuring ref electrode electrochemical systems with For bothaqueousandaprotic system other aprotic electrochemical For lithiumIonbattery and Standard test cells ECC to PAT Upgrade kit-ECC1-00-0310-A 2/3 electrode test cell for battery materials (ECCserieswithPAT-core) -ECC-PAT-Core ECC series Docking station for 16electrochemical test cells (PAT-Cell) incl.data logger -PAT-Tray be usedwiththePAT-Tray Leadless 2/3electrode test cell for battery materials (withPAT-core) -PAT-Cell. Ithasto Leadless series PAT-CORE Series • • • • • • • • The advantages ofthePAT-CORE seriesover thestandard test cells are: save timeandspace no cleaning effort easy electrolyte filling better reproducibility better EISmeasurement (noartifact dueto thecell) higher throughput (Tray andsingle useconsumable)/ less cross-contamination. more stable over timethantheprevious version and PAT-TRAY PAT-CORE
ECC SBSsidebyside,complete ECC-Opto Stdface to face ECC-AIR electrochemical test cell ECC-AIR electrochemical test cell (inaprotic media) ECC-press ECC-press-Air ECC-press-Aqu ECC-press-DL 2/3-electrode test cell 2/3-electrode test cell for gasanalysis 2/3-electrode test cell 3-electrode test cell 2-electrode test cell ECC-PAT-CORE Catalog n° E-ECC-PATU E-ECC-PAT* E-ECC-PATT E-ECC-PATC Catalog n° E-ECC-SBS E-ECCOPT-S E-ECCAIR-N E-ECCAIR E-ECCP E-ECCP-A E-ECCP-AQ E-ECCP-DL E-ECCAQU E-ECCDEM E-ECCCOM E-ECC-REF E-ECC-STD 18 mm Cutting pliers Cross hair to reduce cuttingscrap, stop rail, assy Option 18 mm Punching toolfor lithiumfoil Tools Dilatometers organic aswell asaqueouselectrolyte solutions. insertion-type electrodes. Itmaybeusedin the investigation ofLi-ionbattery andother The dilatometers have beendeveloped for electrodes down to thesub-micrometer range. induced strain (expansion andshrinkage)of dedicated to themeasurement ofcharge- The dilatometer isaresearch grade instrument ELECTROCHEMISTRY ACCESSORIES E-ECS18 Catalog n° E-ECCLI18 Catalog n° E /V 2.5 we 3.5 4.5 2 3 4 0 50 Time/h 100 150 3.5 3 2.5 2 1.5 1 0.5 0 E-ECS-R
Displacement/µm Upgrade kitfrom ECD-2Nto ECD-3NorECD-2DLto ECD-3DL Cable to connect Bio-Logicinstrument (DB9connector) to ECD-3-DL Cable to connect Bio-Logicinstrument (DB9connector) to ECD-nano-3DL Options Electro chemical dilatometer ECD-3-DL(complete) Electro chemical dilatometer ECD-nano-DL(complete) Dilatometer Specifications Weight Dimensions (HxWD) DC outputvoltage Electrode configurations Temperature range Cell electrolyte volume Chemical compatibility Load ontest specimen Drift (sample-free) Bandwidth Resolution linearity Dilatation range Displacement sensor metal inotREFbore ofthe E-ECC-REF) REF-load for test cells (allow usto load lithium Load themetallithium Removing tool REF- load REF -cleaning tool set Options ECC CellLoad Electrode alignmentandassembly tool 2.5 kg 230 x100110mm -10 to 10V 2-electrode, 3-electrode (reference), auxiliary -20 to 70°C ≤3 mL(ca. 2mlelectrolyte required) aprotic organic electrolytes, optionalaqueouselectrolytes 1.0 N(fixed) ≤20 nm/h ≥10 Hz ≤5 nm < 0.1%offullrange 250 µm capacitive ECD-nano-DL 0.3 Nor1.0(variable) ≤100 nm/h ≥10 Hz ≤50 nm < 0.15%offullrange 500 µm LVDT ECD-3-DL Catalog n° Catalog n° E-ECCLOADR E-ECC-102 E-ECC-103 E-ECC-104 E-ECCLOAD Catalog n° E-C-UP E-C-3DL E-C-3N E-ECD-3DL E-ECD-3N 38/39
Local probes Connection Fuel BatteryBattery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessoriesaccessories crystal analyzer electrochemistry electrodes cell cell is notpurchased. only iftheslidingoption chassis, HCPandCLB rack for VMP3,booster It ispossible to usethis computer. a lateral tablet for a units inarack with it ispossible to putfive To getacompact setup, Rack Battery accessories power plugs,computer tablet With slidingtablet includingethernetswitch, computer tablet Including ethernetswitch, power plugs, Rack for MPG-2xxseriesupto5units Specifications Temperature range (W xDH) Dimensions Maximum units
shelf withouttheslidingtablet shelf withtheslidingtablet rack
10 -40°C 495 x450295mm 495 x450257mm 600 x7101850mm 5 units 092-85/2 092-85/1 Catalog n° Coin Cell cyclers. compatible withthe BCS-805andBCS-810 whereas theCCH-120/CCH-124are multichannel potentiostat/galvanostat The CCHiscompatible withVMP3andMPG2 No cable isrequired. panel connectors. potentiostat/cycler front directly pluggedto the The coin cell holders are - CCH-124 for BCS-805/810 CCH-120 for BCS-805/810 for VMP3/MPG-2 CCH, dimensions(WxDH)828365mm Coin CellHolder Holder BH-1i, dimensions(WxDH)13479185mm Battery Holder - - - Holder Battery ability to linktogether manybattery holders. (coin cells, 18650or26cells), adaptable to awidevariety ofbattery sizes 15 Amaximumcurrent, 4-point measurement,
096-124 096-120 092-22/14 092-22/15 Catalog n° Catalog n°
SAM-50 Sense AdapterModule boards anda10-element measurement. stack measurements upto 50Vfor 5channel To beaddedto amultichannelsystem to perform for VMP-300/BCS-815 CC8 Current Collector (8channels) for VSP-300/VMP300 CC5Current Collector (5channels) Current Collector for 5boosters A maximumcurrent of60Aand120Acan flow connected inparallel. up to 8channelsofVMP-300orBCS-815can be boosters ofVSP-300orVMP-300andwiththeCC-8 CC5 allows theuserto connect upto five current designed, CC5andCC8. connections, two current collectors have been through thecell. Inorder to simplifythe increase themaximumcurrent thatcan bepassed to connect inparallel several channelsandthen VSP-300/VMP-300 andBCS-815offer thepossibility ELECTROCHEMISTRY ACCESSORIES Module (SAM-50) Sense Adapter Current Collector
096-015 094-201/1 092-26 Catalog n° Catalog n° 40/41
Local probes Connection Fuel BatteryBattery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessoriesaccessories crystal analyzer electrochemistry electrodes cell cell Fuel cell 7-layer MEAs. edges oftheactive layer can beaddedto 5and A subgasket, protecting themembrane andthe - - - catalyst concentration, 70%Pt/C. of 0.5mg/cm²(±0.05),obtained withthestandard perfluoronated membrane, andaplatinumloading These MEAsare basedona50µm-thick Assemblies (MEA) Membrane Electrode around bothelectrodes. a FlatGasket (FG) (fiberglass reinforced silicon) 7 layers MEAcorresponds to a5-layer MEAwith membrane. on theelectroactive area onbothsidesofthe Diffusion Layers (GDL)completing theelectrodes 5 layers MEAcorresponds to aCCMwithGas hydrogen andreformate operations respectively. platinum-Ruthenium alloys are available for catalyst ontheelectroactive area. Platinumand membrane iscovered withaninkcontaining the Membrane (CCM):theproton exchanged 3 layers MEAcorresponds to aCatalyst Covered to bemodified. The other3-layer and5-layer MEAsneed Only the7-layer MEAsisfully active. MEA selection
Assemblies Membrane Electrode (without MEA's) Single cell fixture Membrane Electrode Assemblies(MEA)
I/A
20 30 40 50 10 0
0.4 225 cm² 100 cm² 50 cm² 25 cm² 16 cm² 5 cm² 100 cm² 50 cm² 25 cm² 16 cm² 5 cm² E 0.6 we /V 7 layers 5 layers 3 layers 7 layers 5 layers 3 layers 7 layers 5 layers 3 layers 7 layers 5 layers 3 layers 7 layers 5 layers 3 layers 7 layers 5 layers 3 layers 0.8 Catalog n° 095-09/12 095-09/11 095-09/10 095-09/9 095-09/8 095-09/7 095-09/6 095-09/5 095-09/4 095-09/3 095-09/2 095-09/1 095-09/18 095-09/17 095-09/16 095-09/15 095-09/14 095-09/13 095-08/3 095-08 095-07 095-08/2 095-08/1 surface area ofthemembrane electrode assembly. homogeneous diffusionofhydrogen over thewhole A porous material isplaced insidethekitfor the - ELECTROCHEMISTRY ACCESSORIES - air to produce electricity. let thefuelcell usetheoxygen inthesurrounding to use:just plugthehydrogen tank into thecell and The educational fuelcell kitisvery simple andeasy Educational kit The cell hasonehydrogen gasinputandoneexit. 1 plastic air-breathing fuelcell (25cm²). for closing theunusedgasexit. bottom sideofthecell. Aplastic screw isincluded of thecell viaoneofthegasexits onthetop and reservoir, thehydrogen gasproduced comes out anode sideoftheelectrolyser cell there isawater 7-layer membrane electrode assembly. Atthe 1 plastic electrolyser cell (25cm²)containing a
Power supply bytwo photovoltaic cells 25 cm²air-breathing cell (noMEA) Options 110 V/220Vadapter for 110Vconfiguration Power supply 220V (including connection, data logger, software) PEM kit Content (fuel cell /electrolyzer) Educational kit Educational kit Data acquisition Variable resistance Electrolyzer kit(includinggasline) PEM#1: 25cm²air-breathing cells no possibility to dismantle thecell (MEA S25-7LN212-Pt/C40%), PEM#3: 25cm²air-breathing cells no possibility to dismantle thecell (MEA S25-7LN125-Pt/C70%), PEM#2: 25cm²air-breathing cells no possibility to dismantle thecell (MEA S25-7LN50-Pt/C70%),
220 Velectrical grid 110 Velectrical grid
095-20/B 095-20/A 095-20/8 095-20/6 095-20/10 095-20/9 095-20/7 Catalog n° 095-20/3 095-20/2 095-20/1 095-20/5 095-20/4 42/43
Local probes Connection FuelFuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cellcell accessories crystal analyzer electrochemistry electrodes cell cell Connection accessories cell cables are alsooffered. performed inglove box, hermetic Moreover for applications are offered. length. That’s why,longer cable may needcables withdifferent For someapplications, theuser instruments. 0.8 mlong for VMP3based booster to thepotentiostat is The cable connected from the a cell cable of1.5mlong. the booster are provided with By default, thepotentiostat and Specific cables Connectors For booster board For standard board Connection kits Banana adapter 4mmfemale socket to 2mmmale plug(packof5) Adapter for banana2mmfemale socket to 4mmmale plug(packof5) Banana adapter 2mmfemale socket to 4mm male plug(packof5) Banana plug4mm(packof5) Banana plug2mm(packof10) Socket 4mmfemale (packof10) Socket 2mmfemale (packof10) Alligator clip4mm(packof5) Alligator clipwith2mmconnector (packof10) this section. the accessories offered in optimize theset-upbyusing We recommend theuserto artifact...). stability ofthepotentiostat, measurement (effect onthe induce someeffects onthe Bad connection could Set-up connection - 2sockets of4mm: - 3sockets of2mm: - 2alligator clipsof4mm: - 3alligator clipsof2mm: - 3sockets of2mm: - 4alligator clipsof2mm:
- - - - - (hole diameter to make intheglove box wall:45mm): - (hole diameter to make intheglove box wall:27mm): AJaegerconnector 12pinsensures thehermeticjunction SP-50,SP-150,BiStat, VSP,VMP3,MPG2 Hermetic cell cable for glove box Booster 8A,1020A Booster 2A,45A SP-50, SP-150,VSP,VMP3,MPG2 Longer cable All boosters Connection cable from booster topotentiostat A Jaegerconnector 25pinsensures thehermeticjunction SP-200, SP-240,SP-300,VSP-300,VMP-300 one feedthrough seal connector intheotherside(length 1.5m), cable withDB-25connector inonesideand12pinsJaeger connector intheotherside(length 1m), other dedicated to thechannelboard calibration outsidethebox two feedthrough sealsoneinstalled intheglove box wallthe in theotherside(length: 1.5m) cable withDB-25connector inonesideand25pinsconnector in theotherside(length: 1m) cable withelectrometer inonesideand25pinsconnector cable with2mmconnectors inonesideand12pinsJaeger blue, white blue, white, red red, black blue, white, red blue, white, red blue, white, red, black, Catalog n° 092-1001/28 092-1001/27 092-1001/18 092-1001/9 092-1001/25 092-1001/5 092-1001/13 092-1001/1 Black colour 092-1001/19 092-1001/16 092-1001/10 092-1001/4 092-1001/6 092-1001/14 092-1001/2 Red colour Hermetic cell cable for glove box 092-1001/20 092-1001/15 092-1001/11 092-1001/3 092-1001/7 092-1001/23 092-1001/26 Blue colour
5 m 3 m 2.5 m 5 m 3 m 2.5 m 10 m 5 m 3 m 2.5 m 5 m 3 m Available length Available length
092-1001/21 092-1001/24 092-1001/12 092-1001/8 092-1001/22 White colour 092-1001/31 092-1001/30 092-33/23 092-33/22 092-33/21 092-33/13 092-33/12 092-33/11 092-23/4 092-23/3 092-23/7 092-23/2 092-33/6 092-33/5 Catalog n° Catalog n° Catalog n° 094-101/6 092-23/5 ELECTROCHEMISTRY ACCESSORIES Weight Interface Gas pressure Fuse Power supply Temperature cage specifications Advanced Faraday Advanced Faraday cage 3.8 kg IEEE-488, RS-232C < 34kPa max. 1 A 100 VAC-240 VAC, 50/60Hz 0 -50°C External power supply for theNstat box (thisoptionisneededifmore thanone Option Bipot cable Nstat box isconnected to VMP3oriftheuserusesVSP) (for VSP,BiStat, VMP3) (for VSP,VMP3) Nstat box Multi-electrode investigation cables investigation cables Multi-electrode Nstat box (8channels) instrument). instrument (green plugontherear panelofthe cage hasto beconnected to theground ofthe Please note thatto activate thisprotection, Faraday the Faraday cage. for low current application, we recommend using To avoid anyexternal perturbations,especially Faraday cages
Advanced Faraday cage, 286x230320mm Standard Faraday cage, 400x200600mm Stand for FC-45 FC-45 Faraday cage, 450xmm Faraday cages standard low current standard Channel
Bipot cable: dedicated to RRDEapplications 2 2 2 8 8 4 Nb ofchannels
FC-45 Faraday cage 4 m 3 m 1.5 m 1.5 m 1.5 m 1.5 m Length
A-012033 NS-FAR600 094-084/2 094-084/1 Catalog n° 092-22/12B 092-22/12A 092-22/12 092-22/4 092-22/3 092-16 092-16/1 Catalog n°
44/45
Local probes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell Connection accessories Test Boxes can beboundtogether aswell. The dummycell for booster andDC2 It isprovided whitheachbooster chassis. dedicated to checkperiodically abooster. The dummycell for booster isespecially Dummy cells for booster DC2 Dummy cell Dummy cell Test Box 2 Test Boxes Test Box 3 booster specifications Dummy cell for Test Box 2 Temperature coefficient Standard tolerance Resistance/mΩ DC2
resistors. For calibration andvalidation several circuits withhighprecision For teaching anddemonstration 3 circuits: linear,exponential, non-linear. For standard check 1 power resistor, 5mOhm. 1 R/Ccircuit. For standard check Dummy cell for booster ±50 ppm/°C 1% 5
Test Box 3
092-32/1 094-111/3
092-22/6 092-22/7 Catalog n° Catalog n° SP-240/SP-300 SP-200 Transport cases Transport cases for VSP300basedinstruments IS1 isolationmodule for auxiliaryI/O length ofcable: 2.5m dimensions: 3x20mm, temperature range: -50°Cto 250°C, to beconnected to theauxiliaryI/O, PT100 temperature probe, DB9-8 BNCconnector for auxiliaryI/O External device connection connection External device
Catalog n° 094-091 094-082 Catalog n° 094-081/5 092-22/13 092-22/1 IS1 ELECTROCHEMISTRY ACCESSORIES Scanning products scanning probe electrochemistry techniques. between probe tipandsample surface inmany microscope whichallows users to view thedistance The VCAM3 isalong working distance video Video Microscope System VCAM3 systems. applications are available for theM370andM470 SECM, SVP,SKP,HRSKPandLEISscanning probe A range ofprobes dedicated for usewithour Probes Catalog n° Operation temperature Field ofview Min illumination VCAM3 specifications SECM Shallow μTriCell™ HR SKP U-VCAM3 -30 to +70°C 1.4 mm(x4.5)to 8.6mm(0.7) 0.0003 lux TriCell™ accessories SKP Cells μTriCell to SECMtechniques (dc,acandicmode).TheShallow The μTriCell dedicated to LEIS, SVP,SKP,SDStechniques. than theμTriCell The TriCell Three cells are available : diameter resin cylinder. All cells accomodate samples mounted ina32mm SVP LEIS HR SKP150μmdiameter SKP 500μmdiameter SECM 25μmdiameter Platinumdisk SECM 15μmdiameter Platinumdisk SECM 10μmdiameter Platinumdisk Probes Shallow μTriCell™ μTriCell™ TriCell™ Cells TM contains aslightly smaller volume ofelectrolyte TM TM isalarge volume, widescan range cell, anditsShallow version are dedicated LEIS TM is more accessible. Volume 6 mL 7 mL ~1 L SVP U-SVP370/1 U-LEIS370/1 U-SKP-150 U-SKP370/1 U-23/25 U-23/15 U-23/10 Catalog n° Catalog n° U-SuTRICELL U-uTRICELL U-TRICELL 46/47
LocalLocal probesprobes Connection Fuel Battery Quartz Spectro- Rotating Electrodes Glassware Corrosion Analytical accessoriesaccessories accessories cell accessories crystal analyzer electrochemistry electrodes cell cell Sales & technical contacts
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