Speleothem Genesis in Ohio Caverns: How Erosion of Overlying Strata Resulted in Different Speleothem Characteristics

Speleothem Genesis in Ohio Caverns: How Erosion of Overlying Strata Resulted in Different Speleothem Characteristics.

THESIS

Presented in Partial Fulfillment of the Requirements for the Degree Master of Science in

the Graduate School of The Ohio State University

Julie E. Codispoti

Graduate Program in Geological Sciences

The Ohio State University

2011

Master's Examination Committee:

Dr. E. Scott Bair (Advisor)

Dr. Lawrence Krissek

Dr. Berry Lyons

Julie E. Codispoti

2011

Abstract

Ohio Caverns in southern Logan and northern Champaign counties, Ohio, is highly decorated in calcitic speleothems ranging in color from rusty red to white. The cave formed in the Devonian Columbus Limestone and is believed to be more than two million years old, forming before Pleistocene ice advances. Carbon dating of sediment samples in the cave was used to determine if the sediments were deposited in the cave by glacial processes, thus bounding a minimum age of the cave. Some areas of the cave contain a red, rusty colored flowstone that covers the cave walls with a wavy water “sheeting” appearance and does not form the traditional speleothems associated with caves. Other parts of the cave contain white flowstones that have the familiar appearance of speleothems and, in places grow directly from and on the rust colored speleothems indicating a change in mineralization. This change likely occurred from chemical alterations in the overlying strata consisting of the Ohio Shale, the Columbus Limestone, and in the thickness and character of soils prior to and after glaciation. A cave entrance currently being built exposes a cross section of glacial material, Ohio Shale, and

Columbus Limestone. Float and in-situ rocks as well as soil material from a fracture and two ceiling rock cores drilled in the Historical Tour path, were collected for XRD analysis to characterize the mineralogy. The results show the samples are predominantly dolomite and only a few of the minerals are iron or manganese bearing. Well log data and

ii visual observation provide clues that the Ohio Shale is still present over top of the cave.

Sediment collected from Overlook Hole contained very little carbon and pollen for dating and paleoclimate information. It was the goal of this work to determine if changes in overlying strata caused the color change of speleothems in Ohio Caverns.

iii

Dedication

This document is dedicated to my mother for her unwavering kindness and to my father

for his extreme work ethic and never ending tips.

Acknowledgments

This thesis would not have been possible without help from many people. Many thanks go to the employees of Ohio Caverns who took time out of their day to accompany me into the cave and answer questions. Special thanks go to Tim Grissom, manager of Ohio

Caverns, who graciously worked with me in answering questions about the cave and accommodating my visits. My advisor, Dr. E. Scott Bair, who guided me through this process. My committee members, Dr. Berry Lyons and Dr. Lawrence Krissek for their help, input, and guidance. Paul Spahr who helped me with several matters at ODNR.

Thomas Quick and Dr. John Senko from The University of Akron for helping me process my samples for XRD analysis and providing me with results. Dr. Greg Wiles from the

College of Wooster, who lead me through sediment sample processes. Leonid Polyak from Byrd Polar Research Center for the use of his lab and microscopes. Dave Porinchu for his help with sediment samples and directing me to researchers for pollen and carbon analysis. Dr. Owen Davis from University of Arizona for processing sediment samples from Overlook Hole. Thanks to Kevin Crawford for enduring numerous trips to Ohio

Caverns to help me with various aspects of my field work. Lastly, my parents, Tony and

Sharon, for their never-ending love and support.

Vita

September 1982 ...... Born, North Canton, Ohio June 2001 ...... North Canton, Hoover High School August 2006 ...... B.A. Geological Sciences, The Ohio State University March 2011 ...... M.S. Geological Sciences, The Ohio State University

Publications

Grunow, Anne M., Codispoti, Julie E., Elliot, David H., 2009, The United States Polar Rock Repository: A Tool for Antarctic Peninsula Research. Geoscience Information Society Proceedings. Vol. 39, 95-98.

Codispoti, Julie E, Grunow, Anne M., 2008, The Basics of Rocks and Minerals and Polar Geology. Beyond Penguins and Polar Bears: An Online Magazine for k-5 Teachers. Issue 6, September 2008. Available at http://beyondpenguins.nsdl.org/. Professional Learning. Science Content Knowledge.

Grunow, Anne M., Elliot, David H., and Codispoti, Julie E., 2008, The United States Polar Rock Repository: A Geological Resource for the Earth Science Community. U.S. Geological Survey Open-File Report 2007-1047, SRP 068, Alan Cooper, Carol Raymond, and the 10th ISAES Editorial Team, in "Antarctica: A Keystone in a Changing World, Online Proceedings for the 10th International Symposium on Antarctic Earth Sciences".

Fields of Study Major Field: Geological Sciences

Table of Contents

Abstract ...... ii Acknowledgments...... v Vita ...... vi Publications ...... vi Fields of Study ...... vi Table of Contents ...... vii List of Figures ...... ix Chapter 1 ...... 1 Introduction to the Problem ...... 1 Ohio Caverns History and Description ...... 1

Significance of the Research – Purpose and Scope...... 10

Previous Studies ...... 11

Statement of Hypotheses ...... 14

Chapter 2 ...... 17 Background Information ...... 17 Rock Formations of Ohio ...... 17

General Cave Formation ...... 20

Ohio‟s Geologic History ...... 22

Pre-Pleistocene ...... 24

The Pleistocene ...... 27

Chapter 3 ...... 35 Hypotheses Testing ...... 35 Overlying Material ...... 35 vii

Recovered Sediment ...... 36

Chapter 4 ...... 42 Analytical Procedures and Results...... 42 Overlying Material ...... 42

The Ohio Shale ...... 47

Recovered Sediment ...... 49

Chapter 5 ...... 56 Interpretations ...... 56 Overlying Material ...... 56

The Ohio Shale ...... 66

Recovered Sediment ...... 67

Chapter 6 ...... 68 Conclusions ...... 68 Overlying Material ...... 68

The Ohio Shale ...... 68

Recovered Sediment ...... 70

References ...... 71 Appendix A ...... 74 Rock Photos...... 74

Appendix B ...... 88 XRD Data ...... 88

Appendix C ...... 281 XRD Diffractograms ...... 281

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List of Figures

Figure 1. Map of Ohio with the approximate location of Ohio Caverns highlighted in red...... 2

Figure 2. Sediment in Ohio Caverns that appears to have been pushed into place, possibly from glacial advance...... 4

Figure 3. Some of the smaller speleothems within Ohio Caverns measure only centimeters in length and width (Photo courtesy of E. Scott Bair)...... 4

Figure 4. The Crystal King, the largest speleothem in Ohio Caverns and the state of Ohio, measures 4‟10.5‟‟ in length...... 5

Figure 5. An example of the red flowstone that can be found in Ohio Caverns...... 6

Figure 6. An example of white flowstone that can be found in Ohio Caverns ...... 6

Figure 7. Passage in Historical Tour that shows red staining and little amounts of white speleothem deposition ...... 7

Figure 8. Passage near Caveman‟s Couch that has very little to no speleothem deposition...... 8

Figure 9. Cave map of Ohio Caverns showing the location of Caveman‟s Couch where there is very little speleothem deposition...... 9

Figure 10. White speleothems can clearly be seen forming directly from the red stained speleothems. The opening is about 18 inches high...... 10

Figure 11. Flowstone in the ceiling of the Flag Room...... 11

Figure 12. Squeezed sediments found in Ohio Caverns (enlargement of Figure 2)...... 16

Figure 13. Key hole passage morphology that indicates phreatic formation (upper part) changed to vadose formation (lower part)...... 24

Figure 14. The Teays River ...... 25

Figure 15. The hydraulic gradient of the ancestral Mad River ...... 26

Figure 16. Top of bedrock map with the approximate location of the Mad River Valley and its juxtaposition to Ohio Caverns...... 28 ix

Figure 17. Ohio shaded drift thickness map (modified from ODNR – Geological Survey)...... 29

Figure 18. Timeline of Ohio glaciations...... 31

Figure 19. Karst areas of Ohio (modified from ODNR – Geological Survey)...... 32

Figure 20. Geologic map of Ohio with the Bellefontaine Outlier and the approximate location of Ohio Caverns highlighted (modified from ODNR – Geologic Survey)...... 34

Figure 21...... 37

Figure 22. New entrance being built where float and in situ samples were collected for XRD analysis...... 38

Figure 23. Rose diagram showing joint directions within Ohio Caverns...... 39

Figure 24. Combining the rose diagram with the cave map, it becomes easier to see how the cave passages and joints are related. Note the rose diagram has been rotated so that 0° matches north...... 41

Figure 25. New cave entrance being built where in-situ and float samples were collected for XRD analysis...... 43

Figure 26 a and b. In situ sediment collected from fracture near the new entrance being built. Obvious changes in color can be seen...... 44

Figure 27. Graph depicting the contact between the Ohio Shale and Columbus Limestone with approximate topography...... 48

Figure 28. Map of Ohio Caverns with Overlook Hole highlighted in red...... 50

Figure 29. Wire ladder that was used to access different depths of Overlook Hole...... 51

Figure 30. Collecting sediment from Overlook Hole...... 52

Figure 31. A spoon was used to dig out the sediment from Overlook Hole...... 52

Figure 32. The iron staining ends abruptly at the paleo-sediment line which is marked in black...... 59

Figure 33. The black line outlines the paleo-sediment layer and iron staining is clearly seen below this level, which suggests the iron staining was deposited first or material was brought into the cave with the sediment and then oxidized (Photo courtesy of E. Scott Bair)...... 60

Figure 34. The paleo-sediment layer marked by the hand and black line has the iron staining both above and below it (Photo courtesy of E. Scott Bair)...... 61

Figure 35. Speleothems in Ohio Caverns formed in the spaces created after the sediment was emplaced and then eroded or compacted (Photo courtesy of E. Scott Bair)...... 62

Figure 36. White speleothems grew to the top of the sediment layer. The top most layer of sediment is still present and iron staining within can be seen...... 63

Figure 37. Completed Eh-pH diagram for the oxides of Fe and their dominant ions at an activity of 10-6 mol/L and 25°C (modified from Faure, 1998)...... 65

Figure 38. The Ohio Shale is slightly visible looking up to the ceiling at this point in the cave. It is approximately 15 feet from the ground to the shale...... 67

Chapter 1

Introduction to the Problem

Ohio Caverns History and Description

Ohio Caverns in Logan and Champaign counties in western Ohio is the largest known cave system in the state (White, 1925) (Figure 1). It measures approximately

1800 feet in length (White, 1925) and was discovered in August 1897 by Walter

Noffsinger who took notice that water quickly disappeared into a depression in the ground on the property of Abraham Reams (Evans, 1897). Noffsinger dug down 20 - 40 feet (Evans, 1897; Castle, 1898; Piqua Daily, 1924) until he found a crevice large enough to fit through and then crawled a distance of about 8 feet to where he could stand fully erect (Evans, 1897). Without difficulty, Noffsinger explored approximately 860 feet and took notice of cave formations (Evans, 1897).

Mt. Tabor, the local name for the ridge that overlies Ohio Caverns, rises 1278 feet above sea level, lies to the east of the Mad River Valley, and is situated between the Mad

River and a Wisconsinan moraine (Hills, 1916). The cave was initially known as Mt.

Tabor Cave and was later named Reams‟ Cave after the property owners (Castle, 1898;

Richwood Gazette, May 1921). In May 1921, a judge ruled that most of the cave was

Figure 1. Map of Ohio with the approximate location of Ohio Caverns highlighted in red.

2 under the property of Albert H. Smith of Dayton and the Reames family lost the majority of their share of the cave (Richwood Gazette, May 1921). The Reames family had the entrance but little cave, and Smith had most of the cave but no entrance. It wasn‟t until

August 1921, after several failed attempts, that Smith dug down about 20 feet and found a passage into the cave (Richwood Gazette, Sept. 1921). This is the entrance used today.

In 1923, Smith bought the Reames‟ share of the cave and the combined cave was renamed Ohio Caverns (Piqua Daily, Sept. 1924).

Large amounts of sediment had to be extracted from the cave before it could be accessed by the public (Tim Grissom – personal communication). It is possible that the sediments were squeezed into the cave passages under pressure as viscous lodgement till under the ice (Figure 2). This implies that the cave formed prior to or during early

Pleistocene glaciations.

The diversity of speleothems in Ohio Caverns ranges from soda straw stalactites measuring just several inches long and with a diameter “about the size of a cigarette”

(Figure 3) to larger speleothems measuring three to five feet in length (Figure 4) (White,

1925).

Figure 2. Sediment in Ohio Caverns that appears to have been pushed into place, possibly from glacial advance.

Figure 3. Some of the smaller speleothems within Ohio Caverns measure only centimeters in length and width (Photo courtesy of E. Scott Bair). 4

Figure 4. The Crystal King, the largest speleothem in Ohio Caverns and the state of Ohio, measures 4‟10.5‟‟ in length (Photo courtesy of E. Scott Bair).

Flowstone is found throughout the cave in colors ranging “from the purest white to very dark red, with all the variations between the two” (Figures 5 and 6) (White,

1925).

Figure 5. An example of the red flowstone that can be found in Ohio Caverns (Photo courtesy of E. Scott Bair).

Figure 6. An example of white flowstone that can be found in Ohio Caverns (Photo courtesy of E. Scott Bair).

There are at least two levels to Ohio Caverns, however, the tour path remains on the first level (Ohio Caverns Booklet), the uppermost level. Not all areas of the cave contain both red and white speleothems. For example, the Historic Tour path has red staining and little to no white speleothems (Figure 7). The area in the cave known as

Caveman‟s Couch (Figure 9) has neither red nor white speleothems (Figure 8). This is clearly an area that has something impeding infiltrating water.

Figure 7. Passage in Historical Tour that shows red staining and little amounts of white speleothem deposition (Photo courtesy of E. Scott Bair).

Figure 8. Passage near Caveman‟s Couch that has very little to no speleothem deposition.

Figure 9. Cave map of Ohio Caverns showing the location of Caveman‟s Couch where there is very little speleothem deposition.

Significance of the Research – Purpose and Scope

The speleothems in the cave are predominantly red or white in color and in some areas the white speleothems grow directly from or on the red speleothems (Figure 10). It is the goal of this research to determine what altered the color and composition of the speleothems. Learning this can help in understanding the origin of Ohio Caverns and its speleothems.

Figure 10. White speleothems can clearly be seen forming directly from the red stained speleothems. The opening is about 18 inches high.

Previous Studies

Hills (1916) is the first scientific paper written regarding Ohio Caverns, which at that time was known as Reames Cave. Hills (1916) states that the white and red speleothems have been and are being deposited simultaneously. He mentions the “Flag Room”, which is believed to be a reference to the various shades of flowstone shown in the photograph below, which occur along a side passage in the Historic Tour section (Figure 11).

Figure 11. Flowstone in the ceiling of the Flag Room.

From the Olentangy and Scioto rivers to the western border of Ohio, is an area of sinkholes. Hubbard (1911) states that dissolution along joints led to the formation of the sinkholes and must have occurred at least before the last glacial advance and probably before any of the glacial advances recorded in the state. This is because glacial striations are found on top of surrounding rocks and surely the striations would have undergone erosion from so much water, however they remain relatively unaltered (Hubbard, 1911).

Hoy et al., (1995) investigated the source of the fine-grained sediments and iron staining within Ohio Caverns and determined there were two possible sources: the overlying soils or the insoluble residue from the surrounding limestone.

Brayman (pg. 1, 2002) examined the composition of the sediments within the cave including “matrix texture, clay mineralogy, and fine-carbonate analyses”. These findings were then compared to sediment on the surface of the surrounding area to determine if samples were similar and therefore indicate the cave and surface sediment had similar origins, possibly from Pleistocene glaciations. Twenty-six sediment samples were collected from Overlook Hole, which Brayman refers to as Mother In-law Hole

(MILH), and were “analyzed for matrix texture, percent fine carbonates, coarse sand lithology, clay mineralogy, and magnetic properties to establish a positive identification of the material that would determine its sources” (Brayman, 2002, pg. 11).

Surface sediments were collected from five locations in the surrounding area to compare with the sediments from MILH. Knowing that sediment was taken out of the

12 cave to access it and that much of that material was placed in the immediate area,

Brayman chose sample sites with the notion that there was little to no contamination by sediments that had been dug out of the cave, but still close enough to represent the soil and sediment found naturally over the cave (Brayman, 2002).

From the samples collected from MILH, Brayman (2002) found five distinct sediment units, which he labels going up section as units, E-A. The different units are based on grain size and represent different periods of energy intensity. Large sediment grains require more energy to move than small grains. Brayman (2002) also found that the amount of carbonate (7.4% to 9.4% calcite, 21.1% to 30.7% dolomite) included in the sediment increased with increasing sediment size. He determined this could mean the carbonates were eroded from the surrounding limestone during times of higher energy.

By calculating the Diffraction Intensity Ratio (DI) [“calculated by dividing the intensity of the 1.0 nm (illite) peak by the 0.7 nm (kaolinite and chlorite) peak”],

Brayman (2002) concluded that the weathering profile of the sediment that was carried into MILH is the reverse of that on the surface. For example, the erosion of the top of the soil profile was deposited at the bottom of the cave followed by sequential downward erosion of the soil profile and its sequential upward deposition in the cave. Sediment that was first carried into the cave would have initially been the soil at the surface that had been exposed to more intense weathering and for a longer period of time than the soil beneath it.

Brayman (2002) also measured scallops, smooth indentations in the cave wall formed by groundwater flow, to determine paleoflow direction. The measurement of

13 scallops indicates north to south groundwater flow within the cave. Brayman (2002) also estimated the mean velocity of the water through the cave to have been ~0.7 cm/s.

The sediment samples collected from MILH were also analyzed for magnetic declination by Brayman (2002). Despite an anomalous reading from one sample, the data indicated that all the sediments were deposited during a single magnetic time event, the

Brunhes-Matuyama, indicating the sediments had to have been deposited or in place for the last 788,000 years (Brayman, 2002). These findings, along with the sediment profile at the surface being the reverse of the sediments in MILH, are not consistent with my hypothesis of the sediment being pushed into the cave by Pleistocene glaciations.

Brayman (2002) concluded that although the source of the sediments within the cave is from the surrounding area, the present surface sediment is not compositionally similar to the cave sediment. He states this implies the actual source of the sediment has completely eroded away or is farther away than Mt. Tabor.

Statement of Hypotheses

Throughout the cave an iron-red stain is clearly visible and is predominantly isolated in and around vertical joints, while large portions of the ceilings are devoid of iron staining. Overlying material is the likely source for the iron and manganese and at some point in the past was physically removed by erosion or was exhausted of its iron material, causing white speleothems to be deposited on top of and instead of red-stained speleothems. It is possible that the overlying basal remnants of the Ohio Shale were

14 removed by the Pleistocene glaciations, therefore causing the color change in speleothem deposition. It is also possible that portions of the shale remain over top the cave and have been leached of its iron.

Before the cave was used for commercial use, many of the passages were cleared of sediment that was approximately 5 feet thick (Tim Grissom – personal communication). The origin of the sediment and how it accumulated within the cave is not clearly understood. Based on a sedimentary feature found in Ohio Caverns (Figure

12), it is believed sediments were squeezed into the cave with the advance and retreat of

Pleistocene glaciations.

The hypotheses for this research are:

1. Overlying material was the likely source for the iron and manganese and at some

point in the past was changed or removed, causing white speleothems to be

deposited on top of and instead of red-stained speleothems.

a. Some overlying basal remnants of the Ohio Shale were removed by the

Pleistocene glaciations, which caused a change in deposition and lead to white

speleothems.

2. Based on a sedimentary feature (Figure 12) it is believed sediments were

squeezed into the cave with the advance and retreat of Pleistocene glaciations.

Figure 12. Squeezed sediments found in Ohio Caverns (enlargement of Figure 2).

Chapter 2

Background Information

Rock Formations of Ohio

The geologic formations of interest are the Columbus Limestone and the Ohio

Shale, as these formations are present within and above Ohio Caverns (Stout, 1941). In

Champaign County, the Ohio Shale lies unconformably above the Columbus Limestone because the Delaware Limestone is not present in this area (Stout, 1941). Stout (1941) described the Columbus Limestone as follows,

“In general the Columbus strata are massive in bedding, somewhat earthy in

appearance, and light gray to light brown in color. The composition varies not

only with the locality but with the different layers. It changes from a low

magnesian limestone in the upper portion to a limy dolomite in the lower part.

Locally chert is present either in definite layers or as scattered nodules. The

thickness of the formation, where normally developed, changes from 80 to 125

feet.”

Hubbard (1909) breaks down the Columbus Limestone into eight zones, H – A, based on differences in fossil abundance in each layer and differences in limestone

17 lithology. Based on Hubbard‟s description of the limestone zones, it appears that Ohio

Caverns is formed in Zone B (Hills, 1916; Hubbard, 1909), which Hubbard (1909) describes as:

“Brown limestone, exceedingly massive, showing but few irregular bedding

planes, and at places appearing as a solid wall without bedding planes. It contains

much bituminous matter, has a saccharoidal appearance, and often shows a

slightly banded structure. The fresh surface of the rock sometimes glistens with

cleavage faces of calcite and frequently contains pockets of the crystals. It also

contains more or less chert scattered through the upper part. Fossils are usually

rare and poorly preserved. Average thickness…35 [feet]”.

The other zones of the Columbus Limestone that Hubbard (1909) describes are fossiliferous, which does not accurately describe the limestone in which Ohio Caverns formed because there are few fossils to be seen in the cave walls. The description of the chert in the other zones also does match as there are visible chert nodules throughout the cave.

Stout (1941) described the Ohio Shale as having three fairly indistinct members:

Huron, Chagrin, and Cleveland.

“Huron and Cleveland are typically black or brownish black, fissile shales with a

high content of carbonaceous matter in a fine state of division. Pyrite either in fine

crystals or in nodules or flakes is also a common impurity. The Chagrin or

middle unit is a gray, siliceous shale differing from the others through lack of

organic and pyritic matter (Stout, 1941).” The Ohio Shale crops out in three

broad areas across Ohio including the Bellefontaine outlier (Stout, 1941).

The Ohio Shale is approximately 100 feet thick in the Columbus area (Stout,

1941). Using this information and the fact that the beds dip slightly (~2°) thicken and to the east, it is not logical that the amount of Ohio Shale on top of the cave would have been more than 100 feet.

The Ohio Shale member above Ohio Caverns is the Huron Member as the

Cleveland and Chagrin Members do not extend that far west (Mike Hansen, personal communication). In a study done on the Devonian-age shales of Ohio, the Huron

Member was described by Gray et al. (1998) as lithotype 1 and lithotype 6:

Lithotype 1: “Silt and clay laminae…range in thickness from one silt grain up to 2 or 3 millimeters. The may be continuous throughout the slide or occur in short lenses. The silt laminae are generally free from organics and may contain carbonate or more rarely gypsum, anhydrite, or barite and minor amounts of clay. Pyrite is generally present as lenses or disseminated throughout the rock. Burrowing along contacts is common, particularly in the lower part of the Huron Shale Member…Type 1 lithotypes average 9% organics, 3% carbonate, 23% silt (mostly quartz and mica), and 65% clay-size material”.

“Type 6 lithotypes are generally dark-greenish-gray or olive-black to olive-gray silty claystones or clay-shales. They are mottled or more rarely lenticularly laminated, contain (worm?) burrows, which may be pyritized, and moderate to high amounts of carbonate. Type 6 lithotypes average 0% organics, 9% carbonate, 22% silt (quart and mica), and 69% clay-size material”.

General Cave Formation

Gillieson (1996) defines the word “cave” as “a natural cavity in a rock, which acts as a conduit for water flow between input points, such as stream sinks, and output points, such as springs or seeps.”

Most caves are formed in limestone and calcite, which is the main component of limestone, dissociates as follows:

2+ 2- CaCO3(s) ↔ Ca (aq) + CO3 (aq)

Calcium Carbonate ↔ Calcium and Carbonate

Palmer (2007)

However, there commonly is interaction with acids, so a more accurate way to depict calcite dissociation is:

+ 2+ - CaCO3(s) + H ↔ Ca + HCO3 (aq)

Calcium Carbonate + Hydrogen ↔ Calcium + Bicarbonate

Palmer (2007)

When carbon dioxide and water combine, the water becomes slightly acidic and forms carbonic acid.

- CO2(g) + H2O(l) ↔ H2CO3 (aq)

Carbon Dioxide + Water ↔ Carbonic Acid

(Brown et al., 2003)

Carbonic acid slowly disassociates the carbonate ion, freeing the Ca2+ and allows it to be transported away in solution in moving water.

2+ - CaCO3(s) + H2O(l) + CO2(g)  Ca (aq) + 2HCO3 (aq)

Calcium Carbonate + Water + Carbon Dioxide  Calcium + Bicarbonate (Carbonic Acid)

(Brown et al., 2003)

This reaction causes the breakdown of calcium carbonate, which is the beginning stage of cave formation. With the right conditions: sufficient water supply, elevation gradient, soluble rock, and time, cracks and crevices will slowly be widened by this chemical reaction, which eventually can form cave passages.

Caves have a life cycle. The water entrance point will enlarge more rapidly than the passage further into the conduit because the groundwater entering has not yet reached saturation and therefore is still aggressive. As the water continues to flow, it becomes more and more saturated with dissolved solids, diminishing its aggressiveness and reducing its capability to dissolve rock. At this initial stage the groundwater is in laminar flow and travels along many different paths. After a passage or passages become sufficiently widened, flow can become turbulent and the groundwater is able to maintain its chemical aggressiveness further into the cave. This allows for portions of the conduits further in the cave to become enlarged (Palmer, 2007).

When the cave is predominantly air filled, the formation of speleothems can occur

(Palmer, 2007) now that a void has been created within the rock. Speleothems are

21 formed by running the previous equation to the left, causing the Ca2+ to be redeposited within the opened passages (Brown et al., 2003).

2+ - CaCO3(s) + H2O(l) + CO2(g)  Ca (aq) + 2HCO3 (aq)

Calcium Carbonate + Water + Carbon Dioxide  Calcite + Bicarbonate (Carbonic Acid) (Brown et al., 2003)

Stout (1941) describes limestone as, “a rock composed essentially of calcium carbonate, CaCO3, with minor quantities of other basic carbonates, sulfates, sulfides, phosphates and silicates, and of siliceous and clay-like materials. In general, limestone ranges from 80 to 98 percent calcium carbonate.” The limestone in the western portion of Ohio varies in thickness from 2,700 to 4,000 feet (Stout, 1941). However, because the cave is formed in the upper portion of the Columbus Limestone, the variety in thickness would not have had an effect on the formation of Ohio Caverns itself and speleothem genesis within the cave.

Ohio’s Geologic History

As Hills (1916) states, the age of Ohio Caverns is not known but based on comparisons of other solution holes within the Columbus Limestone, it is believed that the cave formed before the Pleistocene glaciations and was then filled with glacial sediments as the glaciers advanced and retreated during the Pleistocene. 22

The passages used for tours at Ohio Caverns began initially as phreatic passages, which can be seen in the morphology of the cave passages (Figure 13). Phreatic passages are identified by their ellipsoidal shape and indicate that the passage formed at or near the water table. At some point, perhaps coinciding with one of the glacial advances, or in relation to the potentiometric gradients created from the Teays River Valley, the water table in the area dropped. This is indicated by the physical weathering of down cutting the passages to what is called a T cross-section or key hole passage. This shape is formed by incoming water to the cave trying to reach the watertable as quickly as possible

(Palmer, 2007).

At one time, Ohio Caverns may have been completely filled with glacial sediments. After deposition, erosion and compaction of sediments by dewatering occurred. After the last of the glacial material was emplaced and any erosion or compaction occurred, the cave had adequate space and moisture to allow speleothem formation.

Figure 13. Key hole passage morphology that indicates phreatic formation (upper part) changed to vadose formation (lower part).

Pre-Pleistocene

The Teays River drainage system existed throughout the Miocene and Pliocene

Epochs (23 to 2.6 mya) and possibly longer (Melhorn and Kempton, 1991). The Teays

River began in western North Carolina and flowed north into Virginia, West Virginia, and southwestern Ohio crossing into Indiana and Illinois, then joining with the ancestral

Mississippi River (Figure 14) (Hansen, 1995). The valley that the Teays River created in

Ohio measured 1.5 to 2.5 miles wide and 200 to 300 feet below the surrounding hill tops

(Goldthwait, 1991). This elevation difference between valley bottom and hills created a significant gradient for groundwater on the upland areas to flow to local base level of

24 streams. This may have helped in the formation of Ohio Caverns, in particular the formation of the vadose passages.

Figure 14. The Teays River flowed northward from North Carolina through Virginia, West Virginia and Ohio, and then west into Indiana and Illinois before joining with the Mississippi Embayment. An advancing glacier impeded the Teays River from flowing north and caused the river water to collect and form Lake Tight (modified from Hansen, 1995).

Precipitation that fell around Ohio Caverns would have been driven downward by potentiometric gradients (Figure 15). These gradients would have caused the groundwater above the cave to descend downward in an attempt to reach the water table.

This descent of groundwater allowed dissolution of the Columbus Limestone to occur, forming Ohio Caverns.

Figure 15. The hydraulic gradient of the ancestral Mad River was greater than the current day. Therefore water had a greater distance to reach base level than it does today. This downward drive helped to form Ohio Caverns.

By analyzing the top of bedrock map (Figure 16) in detail, it appears that the ancestral Mad River, the closest tributary of the Teays River, is approximately 1.4 miles

(2.3 km) directly west of Ohio Caverns. The depth to bedrock in this tributary ranges from 700 to 1,000 feet below the land surface and by analyzing the shaded drift thickness map (Figure 17) the drift thickness filling this valley ranges from 260 to 330 feet.

The Pleistocene

The Pleistocene Epoch began about two million years ago. At this time, Earth‟s climate began to cool and eventually allowed a continental ice sheet, centered on current day Hudson Bay, to form and begin advancing southward (Hansen, 1995). These advancing glaciers from the north caused natural dams to form and forced many rivers to find new paths, predominantly southward (Camp, 2006). The Teays River and its tributaries were stopped from flowing north and, consequently, created a lake known as

Lake Tight (Figure 14).

Lake Tight formed approximately 240,000 years ago glaciers advanced into Ohio.

From lake sediment deposits, it is estimated that Lake Tight existed for more than 6,500 years. The level of Lake Tight eventually raised high enough to flow over local drainage divides and created a new drainage path southward, opposite the original direction of surface water drainage prior to glaciation (Hansen, 1995). The two earliest advances of ice from the north previously were referred to as the Nebraskan and Kansan Stages, but these names have fallen out of favor and the term “pre-Illinoian,”

Figure 16. Top of bedrock map with the approximate location of the Mad River Valley and its juxtaposition to Ohio Caverns.

Figure 17. Ohio shaded drift thickness map (modified from ODNR – Geological Survey).

29 is now used (Hansen, 1997). Pre-Illinoian refers to glacial materials formed between approximately 2 million years ago and 240,000 years ago, at which time the Illinoian glacier began to enter Ohio. The only evidence of the Illinoian glaciation in Ohio is in the

Cincinnati area because subsequent glaciations destroyed much of these older glacial materials (Camp, 2006). With the retreat of the pre-Illinoian glaciers, sediments in-filled much of the Teays River Valley, raising the local base flow levels of streams. Glacial material deposited by subsequent glacial advances also in-filled the Teays River Valley, adding to the sediment deposited within the valleys.

The Illinoian ice sheet lasted until around 125,000 years ago when an interglacial warm period occurred and allowed the then exposed Illinoian sediment to be eroded.

Following a period of cooling the final glacial advance, the Wisconsinan, entered Ohio about 117,000 years ago (Camp, 2006), began retreating around 20,000 years ago (Shane,

1987), and disappeared from Ohio‟s landscape about 14,000 years ago (Hansen, 1997)

(Figure 18). Nearly all of the exposed carbonate rocks of Ohio are within the glacial boundary (Figure 19). Only areas in Pike, Highland, Adams, and Brown counties contain carbonate rocks that were unaffected by the glacial advances.

The Illinoian glacier extended southward through Ohio past the Ohio River, and as far south as the western portion of Kentucky. The Wisconsinan glacier did not reach as far south and is marked by a terminal moraine that extends west from Chillicothe towards the Indiana state line (Stout, 1941).

Figure 18. Timeline of Ohio glaciations.

Figure 19. Karst areas of Ohio (modified from ODNR – Geological Survey).

It is well known that the topographically high Bellefontaine Outlier (Figure 20) impeded Wisconsinan glacial advance and split the continental ice sheet into two sublobes: the Scioto Lobe on the east and the Miami Lobe on the west. Despite its higher topography, the Bellefontaine Outlier was covered by the Wisconsinan ice sheets around

23,000 year ago (Quinn and Goldthwait, 1979). Areas surrounding the Bellefontaine

Outlier lack obvious surficial karst features, such as sinkholes. This is due mainly to the solution holes in the area being completely or partially filled with sediment that was deposited by the glaciers (Hull, 1999). If other solution holes have been filled with sediment from the last ice age, it is certainly plausible that Ohio Caverns was in-filled with sediment as well.

The two sublobes later thinned and began retreating around 19,000 years ago. As they retreated, the outwash deposited at least 15 inches of silt on top of the end moraines in Champaign County (Quinn and Goldthwait, 1979). According to Hansen (1997), the region was devoid of ice as early as 14,000 years ago or perhaps sooner (Figure 18).

Figure 20. Geologic map of Ohio with the Bellefontaine Outlier and the approximate location of Ohio Caverns highlighted (modified from ODNR – Geologic Survey).

Chapter 3

Hypotheses Testing

Overlying Material

Two rock cores, approximately 2 mm in diameter, were drilled into the ceiling in a passage off the Historical Tour path (Figure 21a and 21b). These were analyzed with

XRD for mineral composition and to see if the iron stain leaches down through the ceiling, or if it is simply surficial. A portable, hand-held drill with a rock-core attachment was used. Water was provided from a spigot in the cave and was run through a hose attached to the drill. One core was drilled into the ceiling in an area with no indication of iron staining (Figure 21b). The other core was drilled directly into an area of iron staining (Figure 21a).

Float and in-situ samples were collected from the new entrance being built on the northeastern side of the cave for XRD analysis to determine mineral composition and, specifically, for the presence of iron or manganese bearing minerals (Figure 22).

The Ohio Shale

Well log data were obtained from the Ohio Division of Natural Resources

(ODNR) to determine if the Ohio Shale is still present over the cave and if so, the approximate thickness.

Recovered Sediment

The sediment that was placed into Ohio Caverns, possibly by glaciers, and remains in-situ, was collected from Overlook Hole to obtain carbon and pollen. Both of these materials can provide information as to the age of the sediment and therefore to determine when the material was likely emplaced in the cave and thus provide a minimum age of the cave. Pollen can also be used for paleoclimate information of the area, which could be useful in determining if glaciations had anything to do with the infilling of the cave.

Figure 21. a) Drilling the rock core directly into the iron staining off the Historic Tour path. b) Drilling the rock core into a non-mineralized part of the ceiling off the Historic Tour path.

Figure 22. New entrance being built where float and in situ samples were collected for XRD analysis.

As an aside, the dominant joint directions were measured using a Suunto KB-

14/360 and plotted into a rose diagram using the computer program Grapher (Figure 23).

Figure 23. Rose diagram showing joint directions within Ohio Caverns.

The dominant joint direction in Ohio Caverns is north-northwest and secondary is northeast. This fits with the orientation of the main cave passages in the first level and is more apparent when the rose diagram is placed on top of the cave map (Figure 24).

Perhaps the other level(s) of Ohio Caverns follows the joint patterns that do not match the first level tour paths.

The dominate joint directions in Ohio Caverns are likely the result of continental collisions throughout the Paleozoic and current stress regimes. The NE-SW joints were created as a result of stress from the collisions whereas the NW-SE joints were created within the modern stress regime by progressive erosional unroofing. The joints became areas of weakness, later allowing groundwater easy access to the Columbus Limestone to form the cave.

Figure 24. Combining the rose diagram with the cave map, it becomes easier to see how the cave passages and joints are related. Note the rose diagram has been rotated so that 0° matches north.

Chapter 4

Analytical Procedures and Results

Overlying Material

Five float and seven in-situ samples were collected from a new entrance being built on the northeastern side of the cave for XRD analysis (Figure 25). Three of the in situ samples were drilled, using the same drill to obtain the rock cores, from a fracture with material that had obvious color changes (Figure 26a, 26b). All float and in situ samples were taken to the University of Akron for XRD analysis to determine major mineral composition. Small pieces (approximately 5 to 10 g) were broken from each sample and then crushed using a tungsten carbide ball mill to produce a fine powder. A small portion of powder from each sample was tightly packed into an individual “powder pack”, a small circular piece of equipment, to hold the powder in place while run through the XRD machine. The primary results of the XRD analysis are listed in Table 1. Full results can be found in Appendices B and C.

Figure 25. New cave entrance being built where in-situ and float samples were collected for XRD analysis (Photo courtesy of E. Scott Bair).

b Figure 26 a and b. In situ sediment collected from fracture near the new entrance being built. Obvious changes in color can be seen.

Main Sample Picture Other Minerals Description Mineral(s) JCFloat Float 1 Goethite Hematite, Quartz Easily broken, highly weathered. Red and dark brown in some spots. 1 JCFloat Highly weathered, rusty-red color throughout, with some dark brown Float 2 Quartz Hematite 2 and dark yellow spots. JCFloat Highly weathered, rusty-red, dark brown, dark yellowish orange cave Float 3 Goethite Quartz 3 "popcorn" appearance. JCFloat Float 4 Quartz -- Light colored, tannish rock. Easily broken 4

45 Highly weathered. Not as much rusty-red as other float samples. Dark JCFloat Goethite,

Float 5 -- brown dominates sample with some areas of orangish-yellow color. 5 Quartz Moderately indurated. Not as easy to break as the other float samples.

Shale – one sample, all weathered – there was no unweathered JC1 OC-1 Quartz Muscovite material to analyze. Turquoise JC2 OC-5 Quartz Material from fracture. Tephroite JC3 OC-6 Quartz Kaolinite Material from black fracture in new entrance being built. Goethite, JC4 OC-7 -- Material from red fracture in new entrance being built. Quartz

Table 1. Dominant minerals determined from XRD analysis to be in rocks and sediments collected from entrance being built. Full results can be seen in Appendices B and C. (Continued)

Table 1 Continued JC5 Core-1 Dolomite Calcite Core 1, Section 1. JC6 OC-4 Dolomite Quartz Limestone from shale/limestone contact. Weathered rind of rock. Limestone – not in situ and not from shale/limestone contact. JC7 OC-3 Dolomite Quartz Weathered rind of rock. Sandstone from fracture with iron staining. Weathered rind of rock, JC8 OC-2 Dolomite Variscite (with fresher surface included). Limestone – not in situ and not from shale/limestone contact. JC9 OC-3 Dolomite -- Completely fresh surface. JC10 OC-4 Dolomite Quartz Limestone from shale/limestone contact. Completely fresh surface. JC11 OC-2 Dolomite Humite Sandstone from fracture with iron staining. Completely fresh surface. JC12 Core-1 Dolomite Quartz Core 1, Section 2. JC13 Core-1 Dolomite Quartz Core 1, Section 3. JC14 Core-2 Dolomite -- Core 2, Section 1. JC15 Core-2 Dolomite -- Core 2, Section 2.

46 JC16 Core-2 Dolomite -- Core 2, Section 3.

A description of “sandstone” is given to a few collected samples because this most accurately describes the lithology. However there has been no evidence of sandstone in this area and may simply be a friable limestone.

The Ohio Shale

Well log data were obtained from ODNR (Table 2) and used to extrapolate till, shale, and limestone thicknesses in the area for construction of a generalized geologic cross section (Figure 27). The information from the respective well logs is listed below.

ODNR Well No. Well No. 62-4 28894 From Formations (ft) To (ft) Top Soil 0 2 Red clay 2 6 Shale 6 8.5 Limestone 8.5 122.5 ODNR Well No. Well No. 64-10 160776 From Formations (ft) To (ft) Top Soil 0 2 Red Clay 2 20 Blue Clay 20 40 Brown Clay 40 45 Blue Clay 45 66 Slate 66 140 Limestone 140 193 ODNR Well No. Well No. 64-5 292236 From Formations (ft) To (ft) Clay 0 19 Shale 19 50 Limestone 50 132 Slate 132 153 Limestone 153 160 Slate 160 169

Table 2. Well log information obtained from ODNR. 47

Figure 27. Graph depicting the contact between the Ohio Shale and Columbus Limestone with approximate topography. 48

Recovered Sediment

Overlook Hole, an unofficial name for the one existing (excavated) pit in the cave, was the focus for sediment collection to determine approximate age of emplacement of the sediment into Ohio Caverns (Figure 28). This pit was filled with the same sediment that filled the cave passages and like the passages, was dug out. However, there are still remnants of this sediment along one wall of the pit.

Nine sediment samples (S-1 through S-9) were collected from the bottom to the top of Overlook Hole (Figures 29, 30, 31). This is the same area that Brayman (2002) sampled. Sediment believed to have been placed into Ohio Caverns by glaciers and remains in-situ was collected for carbon dating to determine approximately when the material was emplaced into the cave.

A wire ladder, measuring approximately 6 inches across was lowered into

Overlook Hole (Figures 29, 30, 31). Starting from the bottom, sediment was collected from the wall opposite the wire ladder, using a spoon. The outermost sediment was scraped off and then several spoonfuls of sediment from within the same layer were put into a plastic sandwich bag and labeled (Figure 31). Because of the difficulty using the wire ladder to access the sediment on the opposite side of the wall, regular intervals were not feasible, however, samples were collected approximately 10 to 14 inches apart.

Figure 28. Map of Ohio Caverns with Overlook Hole highlighted in red.

Figure 29. Wire ladder that was used to access different depths of Overlook Hole.

Figure 30. Collecting sediment from Overlook Hole.

Figure 31. A spoon was used to dig out the sediment from Overlook Hole.

A small portion of each sample was freeze dried for a period of 24 hours to remove moisture. The samples were then washed with water through a sieve to separate the sediment into two fractions: <63 µm and >63 µm.

A 63 µm mesh sieve containing the sediment was placed into a container and the sample was washed with tap water squeezed from a plastic bottle to separate the <63 µm sediment into the container. Once the water in the container turned clear, the sieve, containing the >63 µm fraction, was placed into a drier overnight to remove moisture.

Once the >63 µm sediment was dry, it was put into a small, glass, labeled vial(s). The containers of washed sediment were left out overnight to allow the clay material to settle.

The following day water was removed and the container was left in the drier overnight to remove the excess water. Once the clay samples were dry, they were placed into marked plastic bags.

Both size fractions for every sample were analyzed under a microscope to look for the presence of carbon material, which would be used to obtain an approximate age and therefore an approximate date of emplacement. However, no carbon material was found under the microscope.

Three of the nine samples, S-1, S-5, and S-9, were sent to the University of

Arizona to determine if any microscopic carbon and/or pollen spores could be found for dating and paleoclimatology information.

The three sediment samples were analyzed by Dr. Owen Davis from the

University of Arizona. He concluded that there was very little carbon material present and based on other materials found in the sediment, the carbon material is likely from the

Devonian; therefore carbon dating would be useless as this exceeds the limit of carbon dating. He also determined that there was very little pollen and what was present was poorly preserved and therefore unidentifiable. One fungal spore could be identified, however, it is found in sediment that ranges in age from the Devonian to today and, therefore, not useful for this study.

Dr. Davis provided the following information and conclusions based on his analyses of the sediment samples:

“The „acritarcs‟ [sic] are sacks with many small processes similar to the acrticarc Cymatogalea. „Acritarcs‟ are common in Paleozoic sediments but are of unknown origin, but probably planktonic. The „charcoal‟ fragments are opaque and irregular, but the margins are never sharp and likely are not the results of burning, but of slow decay. The „wood fibers‟ are cylindrical, with regular markings, but are light-colored and do not accept the fuschin die. I‟m afraid they may be modern contaminants, but I‟m not completely certain they are wood fragments. None of this is diagnostic. The only identifiable particle is „Concentracystis,‟ it has a very distinctive „thumbprint‟ patter on opposite sides of the spore. Unfortunately it has a very long stratigraphic range – Devonian to present. The spores and acritarcs do not rule out that age, but they do not provide strong support. The fungi likewise have very long diagnostic ranges, particularly the spore forms recovered in these samples” (Table 3).

SAMPLES S-1 S-5 S-9 Deteriorated spores/pollen 0 2 7 Trilete spores 0 1 9 Concentracystis 0 0 1 Fungal spores and hyphae 5 8 20 Thin organic membranes 5 13 27 Acritarcs (spheres) 0 2 0 Charcoal or dark organic matter 6 32 11 “Wood” fibers 7 9 7

Table 3. Results from Dr. Owen Davis, University of Arizona.

Dr. Davis had this to say as to the reason for the lack of datable material:

“Ordinarily fine-grained clastic samples of this volume would produce hundreds

of pollen and spores…What I found indicates that the sediments resulted from

solution of the Devonian limestone, leaving behind mineral clay and silt

particles”.

However, considering the amount of sediment found in the cave (approximately 5 feet thick throughout) the cave would have to be considerably larger in order to account for the amount of “insoluble residue” left behind. Therefore, this explanation does not seem likely.

Chapter 5

Interpretations

Overlying Material

Dolomite dominates the in situ and core rock samples and quartz, goethite, and calcite are major components. Even the different sections of core, including the iron stained tip of Core 2, Section 1 lack significant iron-bearing minerals. Red pieces of the weathered hand samples did not come back with any significant iron minerals either; instead all the samples are predominantly dolomite and quartz.

The possibilities for the lack of iron in the samples are:

1. What appears to be iron staining is in fact not iron staining. This is a possible

topic for future study and outside the scope of my research. Therefore, the idea

that it is iron staining remains the likely explanation.

2. The analysis results from the XRD could have provided false readings leading to

the conclusion that very little iron is present in the hand samples.

3. The iron source is still present but has been leached.

4. The iron source was removed.

The most likely explanation is that there was an iron source for the red speleothems and staining that were deposited, however, the iron source was physically removed or depleted. The Ohio Shale is known for having pyrite, although the XRD analysis did not show any evidence of disseminated pyrite in the shale sample. The shale that is exposed at the new entrance being built and the shale hand sample collected from this exposure are severely weathered, so it‟s possible that pyrite has been leached or is not in enough abundance to be detected by the XRD.

There can be problems associated with XRD analyses and therefore some of my conclusions. For example, the sediment sample needs to have a completely smooth surface, therefore any tiny gaps between sediment grains can cause problems in diffraction, providing erroneous results (Scintag, 1999).

The samples should also be homogeneous and randomly distributed. The diffraction intensity from preferred orientation minerals, such as clays, can cause a different outcome from minerals that are randomly distributed. Preferred orientation causes changes in the intensity and therefore changes the quantative analyses (Scintag,

1999). If high clay content is known or suspected, it is best to separate the clay fraction and have these materials XRD analyzed on a glass plate separately from the rest of the sample (Tom Quick, Research Associate from University of Akron – personal communication).

It should also be noted when analyzing the XRD diffractograms, the scales can differ from one sample readout to the next. This can cause the reader to misinterpret the significance of certain peaks compared to others.

In some areas, the iron staining on the cave walls stretches from the joints in the ceiling down to the current cave floor. However, in some areas red staining does not continue to the floor but appears to end rather abruptly part way down the cave walls

(Figure 32). There are several places throughout the cave where the paleo-sediment line, the remnants of the uppermost sediment layer, can be seen on the cave walls and below this line there is clear evidence of iron discoloration (Figure 33).

This brings into question the timing of the sediment in relation to the iron staining. If the staining reaches the floor this would indicate the staining occurred before sediment infill as the presence of sediment would have impeded iron staining from reaching the current floor. However, as mentioned earlier, there are also areas where there is iron staining below the paleo-sediment line (Figure 33). This could be due to material within the sediment that oxidized once it interacted with water and oxygen in the cave, and therefore stained the walls. The sediment probably contained pieces of the

Ohio Shale and therefore the disseminate pyrite within it. However, this scenario does not seem as likely, especially since in most areas the iron staining can be followed in a direct path from an overhead joint down to the point where it stops on the wall.

The likely explanation to the timing of staining and sediment is that the iron staining began before sediment infill and then continued while an unknown number of sediment influx episodes occurred.

Figure 34 is an example of iron staining both above and below the paleo-sediment layer.

Figure 32. The iron staining ends abruptly at the paleo-sediment line which is marked in black.

Figure 34. The paleo-sediment layer marked by the hand and black line has the iron staining both above and below it (Photo courtesy of E. Scott Bair).

There is an area in the cave where white speleothems were deposited on top of the sediment that was placed into the cave and the top-most layer of the sediment still remains attached to these speleothems (Figure 35). By observing the sediment that remains attached to the white speleothems, it is clear there is iron staining present in the sediment (Figure 36). This is possible evidence that the iron-enriched groundwater staining the walls, which created the iron-red speleothems, continued to enter the cave after the sediment was deposited. Or, that material carried in with the sediment was exposed to the infiltrating groundwater within the cave, which then caused the oxidation, thus leading to the iron staining at the top of the sediment layer. As mentioned earlier, it is possible there was Ohio Shale containing pyrite within the sediment that could have oxidized and caused the iron staining.

Figure 35. Speleothems in Ohio Caverns formed in the spaces created after the sediment was emplaced and then eroded or compacted (Photo courtesy of E. Scott Bair).

Figure 36. White speleothems grew to the top of the sediment layer. The top most layer of sediment is still present and iron staining within can be seen.

When pyrite and oxygen interact, the following reaction occurs:

2- + 4FeS2 + 15O2 + 14H2O  4Fe(OH)3 + 8SO4 + 16H

(Faure, 1998)

This reaction frees H+, which lowers the pH of the water causing an increase in acidity and increasing iron solubility (Bonnissel-Gissinger et al., 1998). Based on the above equation, as groundwater interacted with pyrite in the Ohio Shale, the water would have decreased in pH, thus allowing more iron into solution and causing the water to become more acidic, which could then dissolve more CaCO3 in the limestone. This increase in acidity likely helped create the cave by speeding up the dissolution process.

The dissolved iron was then oxidized and precipitated as Fe3+ on the calcium carbonate of the speleothems. Here the source of the iron staining in the cave is directly related to pyrite oxidation of the shale and/or shale derived sediment within the cave.

The solubility of Fe2+ and Fe3+ depends on the pH and Eh of the water (Figure

37). Fe2+ is more soluble in acidic water with an Eh between -0.4 and approximately

+0.8 Volts. Fe 3+ is soluble only in water that is very acidic and an Eh of only 0.8 to 1.2

Volts (Faure, 1998).

Figure 37. Completed Eh-pH diagram for the oxides of Fe and their dominant ions at an activity of 10-6 mol/L and 25°C (modified from Faure, 1998).

After the cave formed, the Ohio Shale, the iron source, was present and iron speleothems and staining began to form and continued until Pleistocene glaciations removed nearly all the Ohio Shale that was present above Ohio Caverns. The small remaining amount of shale that persists today, had already been or was eventually leached of its iron, therefore infiltrating groundwater had little to no iron to dissolve and deposit on the cave walls or to precipitate as speleothems. Instead, the groundwater contained dissolved calcite and bicarbonate ions from dissolution of the Columbus

Limestone, which turned speleothem formation to the white calcitic ones that make Ohio

Caverns famous.

Brayman‟s (2002) conclusion that the source of the sediment in the cave is not the same as the current surface sediment in the area supports this. He concluded the original

65 material above the cave was removed or the source for the sediment in the cave is further away than Mt. Tabor. It is likely the Ohio Shale was the source of the iron. However, there may have been more Ohio Shale on top of the cave before Pleistocene glaciations and some was removed by glaciations and/or the iron largely removed by depletion.

My data and interpretations corroborate Brayman‟s (2002) hypothesis of removal, which would account for the absence of iron bearing strata.

The Ohio Shale

The Ohio Shale can be seen above the Historic Entrance, the new entrance being built, and one location in the cave looking up through breakdown in the ceiling (Figure

38). The cross section (Figure 28) also indicates that the Ohio Shale, though thin, is still present on Mt. Tabor. Also, any cores that have been dug for electricity, piping or other material have all hit shale (Tim Grissom – personal communication). Because of this evidence it is concluded that the base of the Ohio Shale remains above Ohio Caverns in thicknesses of a few inches to perhaps a foot.

Figure 38. The Ohio Shale is slightly visible looking up to the ceiling at this point in the cave. It is approximately 15 feet from the ground to the shale.

Recovered Sediment

There was not enough carbon material in the sediment to obtain an approximate age. In fact, fungal spores of Concentricyste were the only identifiable material from the sediments from Overlook Hole and unfortunately this spore can be found in sediments ranging from the Paleozoic to today (Dr. Owen Davis – personal communication).

According to Dr. Owen Davis, it is likely that these spores have come from the limestone itself, which renders the spores useless for this study.

Chapter 6

Conclusions

Overlying Material

No major iron minerals were found in the float, in situ, or rock cores collected from above and within the cave. This would initially indicate that the overlying material is not the source for the iron, however this is not the case. Possible explanations for the lack of iron in the samples collected from the newest entrance could be due to false readings from the XRD or it is not iron that stains the walls.

The Ohio Shale

The Ohio Shale is still present over most, and possibly the entire cave, measures only a few inches thick, and was the source for the iron staining on the walls and speleothems in Ohio Caverns. The Ohio Shale which is known to contain disseminated pyrite, a source of iron, could have had the capability to deposit iron speleothems and staining. Pyrite interacted with infiltrating groundwater, which caused the groundwater to become more acidic and therefore capable of holding more iron in solution, helping to form cave passages.

Some of the Ohio Shale was removed with one or more of the Pleistocene glaciations and the remaining shale was eventually leached of its iron minerals. Not only did the shale removal cause the change in speleothem deposition from red to white, but also caused changes in water drainage within the cave. For example, the Historic Tour path has significant red staining, but hardly any white speleothems. When the iron source was removed, material must have been placed over the Historic Tour that makes it difficult for groundwater to penetrate into the cave.

By examining the iron staining and paleo-sediment layer throughout the cave, it appears that iron staining began initially before the sediment influx, and then continued as sediment was deposited into the cave.

A very basic timeline of events for the cave are as follows:

o Paleozoic orogenies created NE-SW fractures.

o Progressive unroofing within modern stress field created NW-SE

fractures.

o Pyrite dissolution occurred, creating initial cave passages probably in

Miocene or Pliocene Epochs  Cave formed before Pleistocene.

o Iron speleothems and staining begin to be deposited.

o Sediment infill – iron deposition continues.

o Some Ohio Shale removed by Pleistocene glaciations.

o White speleothem deposition.

Recovered Sediment

Because no significant carbon material or pollen spores were found in the sediments collected from Overlook Hole, it cannot be proved that the cave sediment was pushed in by Pleistocene glaciations. This also means a minimum age constraint for the cave was not determined. Based on previous findings, such as magnetic information from Brayman (2002), it is not likely that the sediment was pushed into the cave, but may have been the result of glacial outwash and melting.

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Stout, Wilber. Dolomites and Limestones of Western Ohio. Geological Survey of Ohio. Fourth Series, Bulletin 42. 1941.

White, George Willard. The Limestone Caves and Caverns of Ohio. Master‟s thesis. The Ohio State University. 1925.

Chapter 7: Basics of X-ray diffraction. Scintag Inc. Cuptertino, CA. 1999. Found online at http://epswww.unm.edu/xrd/xrdbasics.pdf

“Mt. Tabor Cave Case.” The Richwood Gazette May 12, 1921.

“New Entrance to Mount Tabor Cave.” The Richwood Gazette. Richwood. Union County, OH. No. 7. September 1, 1921

“New Discoveries Made at Ohio Caverns by Excavators Recently.” The Piqua Daily Call Pg. 2. Piqua, OH. May 27, 1924

Appendix A Rock Photos

Appendix B XRD Data

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC1 Data measured at: 24-Jan-2011 11:05:00

Diffractometer type: PW1710 BASED Tube anode: Cu Generator tension [kV]: 40 Generator current [mA]: 35 Wavelength Alpha1 [•]: 1.54056 Wavelength Alpha2 [•]: 1.54439 Intensity ratio (alpha2/alpha1): 0.500 Divergence slit: AUTOMATIC Irradiated length [mm]: 12 Receiving slit: 0.2 Spinner: OFF Monochromator used: YES

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 9350.890 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 184.96 201.64 204.49 174.24 174.24 169.00 2.130 174.24 169.00 166.41 184.96 158.76 156.25 2.250 139.24 148.84 114.49 146.41 141.61 132.25 2.370 144.00 121.00 116.64 116.64 129.96 129.96 2.490 127.69 127.69 118.81 114.49 114.49 116.64 2.610 106.09 98.01 114.49 118.81 84.64 92.16 2.730 92.16 114.49 100.00 110.25 102.01 94.09 2.850 108.16 110.25 88.36 110.25 86.49 106.09 2.970 92.16 88.36 96.04 88.36 98.01 100.00 3.090 86.49 98.01 75.69 82.81 94.09 102.01 3.210 84.64 90.25 72.25 106.09 81.00 86.49 3.330 81.00 108.16 88.36 75.69 94.09 98.01 3.450 72.25 56.25 84.64 84.64 94.09 70.56 3.570 82.81 92.16 77.44 70.56 90.25 65.61 3.690 75.69 81.00 64.00 86.49 77.44 86.49 3.810 73.96 81.00 70.56 59.29 79.21 77.44 3.930 82.81 70.56 77.44 77.44 82.81 86.49 4.050 75.69 73.96 60.84 60.84 77.44 75.69 4.170 84.64 68.89 79.21 88.36 77.44 67.24 4.290 75.69 68.89 77.44 86.49 88.36 75.69 4.410 79.21 75.69 75.69 75.69 67.24 72.25 4.530 65.61 82.81 70.56 79.21 79.21 77.44 4.650 62.41 72.25 65.61 62.41 56.25 70.56 4.770 82.81 79.21 64.00 67.24 62.41 67.24 4.890 73.96 90.25 57.76 70.56 75.69 64.00 5.010 82.81 75.69 77.44 75.69 73.96 67.24 5.130 79.21 77.44 67.24 68.89 75.69 56.25 5.250 67.24 73.96 84.64 79.21 56.25 70.56

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 72.25 59.29 72.25 62.41 75.69 46.24 5.490 65.61 62.41 62.41 82.81 67.24 70.56 5.610 64.00 75.69 72.25 75.69 75.69 70.56 5.730 51.84 54.76 67.24 65.61 77.44 67.24 5.850 77.44 62.41 70.56 68.89 62.41 54.76 5.970 56.25 75.69 62.41 70.56 67.24 70.56 6.090 79.21 65.61 60.84 59.29 65.61 67.24 6.210 72.25 79.21 64.00 62.41 72.25 75.69 6.330 56.25 65.61 72.25 73.96 82.81 53.29 6.450 62.41 62.41 64.00 59.29 65.61 60.84 6.570 65.61 59.29 75.69 67.24 53.29 65.61 6.690 43.56 72.25 60.84 62.41 75.69 75.69 6.810 79.21 81.00 59.29 68.89 67.24 59.29 6.930 70.56 67.24 75.69 65.61 70.56 77.44 7.050 65.61 64.00 65.61 59.29 65.61 86.49 7.170 86.49 82.81 59.29 77.44 62.41 70.56 7.290 70.56 65.61 60.84 68.89 60.84 65.61 7.410 90.25 75.69 64.00 75.69 56.25 84.64 7.530 59.29 70.56 62.41 68.89 51.84 62.41 7.650 68.89 67.24 67.24 62.41 75.69 73.96 7.770 79.21 67.24 70.56 67.24 70.56 56.25 7.890 72.25 77.44 81.00 81.00 73.96 70.56 8.010 77.44 64.00 75.69 77.44 77.44 79.21 8.130 72.25 70.56 68.89 90.25 90.25 86.49 8.250 77.44 86.49 81.00 81.00 75.69 88.36 8.370 88.36 79.21 106.09 94.09 100.00 100.00 8.490 96.04 84.64 92.16 84.64 90.25 108.16 8.610 86.49 102.01 100.00 114.49 132.25 102.01 8.730 114.49 132.25 127.69 118.81 153.76 134.56 8.850 125.44 106.09 94.09 102.01 90.25 68.89 8.970 79.21 79.21 60.84 67.24 60.84 77.44 9.090 60.84 60.84 67.24 59.29 60.84 62.41 9.210 64.00 57.76 82.81 59.29 62.41 44.89 9.330 53.29 67.24 64.00 62.41 73.96 50.41 9.450 72.25 50.41 62.41 62.41 50.41 62.41 9.570 62.41 49.00 53.29 68.89 56.25 62.41 9.690 54.76 47.61 54.76 54.76 59.29 62.41 9.810 47.61 62.41 50.41 72.25 53.29 43.56 9.930 57.76 53.29 50.41 51.84 62.41 59.29 10.050 47.61 46.24 56.25 62.41 60.84 67.24 10.170 47.61 43.56 65.61 59.29 70.56 67.24 10.290 62.41 40.96 53.29 54.76 59.29 54.76 10.410 57.76 62.41 54.76 56.25 44.89 47.61 10.530 43.56 44.89 50.41 43.56 43.56 77.44 10.650 42.25 56.25 50.41 53.29 49.00 53.29 10.770 54.76 50.41 53.29 59.29 65.61 53.29 10.890 60.84 56.25 42.25 56.25 54.76 43.56 11.010 49.00 54.76 50.41 59.29 56.25 47.61 11.130 49.00 56.25 50.41 53.29 44.89 49.00 11.250 62.41 44.89 46.24 65.61 59.29 46.24 11.370 50.41 57.76 57.76 77.44 47.61 50.41 11.490 51.84 50.41 49.00 56.25 51.84 53.29

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 44.89 65.61 53.29 42.25 72.25 43.56 11.730 50.41 53.29 57.76 50.41 42.25 49.00 11.850 62.41 64.00 43.56 60.84 59.29 64.00 11.970 50.41 64.00 56.25 60.84 59.29 62.41 12.090 56.25 47.61 59.29 59.29 56.25 67.24 12.210 62.41 59.29 59.29 79.21 75.69 67.24 12.330 77.44 73.96 65.61 65.61 56.25 67.24 12.450 42.25 65.61 43.56 53.29 47.61 43.56 12.570 51.84 65.61 56.25 50.41 65.61 64.00 12.690 59.29 47.61 56.25 57.76 54.76 54.76 12.810 56.25 54.76 50.41 54.76 51.84 47.61 12.930 47.61 47.61 70.56 60.84 51.84 67.24 13.050 62.41 59.29 57.76 47.61 67.24 59.29 13.170 47.61 57.76 64.00 53.29 59.29 70.56 13.290 62.41 67.24 60.84 57.76 56.25 57.76 13.410 67.24 77.44 72.25 77.44 81.00 72.25 13.530 72.25 62.41 59.29 84.64 62.41 64.00 13.650 72.25 75.69 79.21 50.41 64.00 65.61 13.770 67.24 54.76 65.61 75.69 60.84 70.56 13.890 67.24 64.00 68.89 56.25 65.61 60.84 14.010 65.61 64.00 72.25 68.89 62.41 65.61 14.130 81.00 49.00 73.96 50.41 68.89 53.29 14.250 67.24 54.76 56.25 53.29 62.41 51.84 14.370 65.61 46.24 64.00 56.25 65.61 50.41 14.490 72.25 70.56 56.25 51.84 44.89 51.84 14.610 47.61 43.56 57.76 62.41 57.76 59.29 14.730 60.84 47.61 67.24 65.61 47.61 64.00 14.850 50.41 54.76 65.61 56.25 60.84 81.00 14.970 59.29 67.24 47.61 56.25 49.00 50.41 15.090 46.24 53.29 46.24 53.29 46.24 49.00 15.210 53.29 53.29 51.84 46.24 53.29 47.61 15.330 53.29 56.25 56.25 56.25 56.25 59.29 15.450 54.76 65.61 50.41 50.41 47.61 50.41 15.570 53.29 51.84 57.76 38.44 57.76 53.29 15.690 50.41 44.89 50.41 43.56 47.61 46.24 15.810 46.24 64.00 50.41 60.84 50.41 47.61 15.930 67.24 67.24 50.41 46.24 53.29 44.89 16.050 54.76 56.25 53.29 53.29 53.29 47.61 16.170 39.69 59.29 60.84 56.25 40.96 44.89 16.290 56.25 50.41 54.76 60.84 60.84 47.61 16.410 47.61 53.29 53.29 47.61 64.00 47.61 16.530 57.76 47.61 51.84 42.25 62.41 47.61 16.650 42.25 65.61 53.29 53.29 67.24 51.84 16.770 38.44 47.61 54.76 62.41 46.24 53.29 16.890 57.76 46.24 47.61 47.61 59.29 59.29 17.010 44.89 67.24 47.61 53.29 56.25 56.25 17.130 51.84 65.61 47.61 67.24 53.29 54.76 17.250 75.69 54.76 53.29 65.61 56.25 72.25 17.370 59.29 62.41 70.56 67.24 53.29 75.69 17.490 67.24 77.44 67.24 65.61 57.76 67.24 17.610 67.24 86.49 82.81 82.81 108.16 92.16 17.730 84.64 92.16 90.25 100.00 77.44 92.16

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 84.64 84.64 68.89 86.49 67.24 64.00 17.970 56.25 62.41 56.25 62.41 72.25 64.00 18.090 59.29 53.29 53.29 64.00 56.25 65.61 18.210 50.41 62.41 59.29 62.41 53.29 77.44 18.330 65.61 64.00 51.84 56.25 59.29 47.61 18.450 57.76 44.89 62.41 62.41 62.41 67.24 18.570 62.41 62.41 50.41 50.41 53.29 59.29 18.690 47.61 67.24 62.41 53.29 75.69 62.41 18.810 50.41 54.76 57.76 70.56 53.29 56.25 18.930 65.61 73.96 72.25 73.96 72.25 56.25 19.050 68.89 54.76 73.96 82.81 72.25 86.49 19.170 67.24 72.25 70.56 70.56 62.41 70.56 19.290 73.96 73.96 59.29 75.69 73.96 84.64 19.410 77.44 90.25 90.25 92.16 100.00 96.04 19.530 106.09 132.25 132.25 161.29 136.89 148.84 19.650 169.00 196.00 231.04 207.36 228.01 207.36 19.770 225.00 228.01 234.09 219.04 210.25 204.49 19.890 190.44 198.81 196.00 169.00 158.76 163.84 20.010 141.61 148.84 129.96 139.24 174.24 127.69 20.130 125.44 139.24 110.25 127.69 110.25 116.64 20.250 112.36 77.44 151.29 121.00 134.56 125.44 20.370 127.69 144.00 141.61 108.16 144.00 166.41 20.490 141.61 174.24 176.89 198.81 228.01 243.36 20.610 249.64 334.89 361.00 445.21 542.89 610.09 20.730 761.76 967.21 1102.24 1339.56 1406.25 1459.24 20.850 1346.89 1122.25 800.89 605.16 416.16 316.84 20.970 259.21 228.01 207.36 156.25 139.24 146.41 21.090 125.44 134.56 146.41 112.36 110.25 108.16 21.210 106.09 110.25 104.04 104.04 94.09 92.16 21.330 88.36 86.49 98.01 73.96 90.25 84.64 21.450 84.64 104.04 90.25 88.36 106.09 112.36 21.570 90.25 90.25 79.21 88.36 81.00 90.25 21.690 84.64 84.64 72.25 72.25 82.81 70.56 21.810 84.64 62.41 81.00 79.21 72.25 72.25 21.930 59.29 75.69 88.36 59.29 68.89 73.96 22.050 53.29 75.69 62.41 72.25 81.00 67.24 22.170 56.25 65.61 68.89 72.25 73.96 90.25 22.290 70.56 72.25 81.00 77.44 73.96 62.41 22.410 62.41 82.81 75.69 82.81 65.61 75.69 22.530 79.21 67.24 79.21 96.04 84.64 77.44 22.650 70.56 94.09 90.25 100.00 98.01 98.01 22.770 106.09 94.09 104.04 84.64 84.64 114.49 22.890 112.36 79.21 81.00 86.49 82.81 88.36 23.010 88.36 88.36 67.24 79.21 88.36 72.25 23.130 81.00 92.16 88.36 82.81 94.09 70.56 23.250 82.81 81.00 70.56 98.01 75.69 77.44 23.370 94.09 79.21 72.25 72.25 92.16 81.00 23.490 82.81 81.00 104.04 88.36 77.44 94.09 23.610 90.25 84.64 104.04 104.04 92.16 106.09 23.730 98.01 104.04 100.00 96.04 110.25 100.00 23.850 108.16 114.49 92.16 90.25 106.09 86.49 23.970 88.36 88.36 90.25 94.09 82.81 90.25

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 90.25 79.21 84.64 86.49 98.01 86.49 24.210 86.49 90.25 77.44 86.49 82.81 67.24 24.330 88.36 90.25 86.49 90.25 68.89 88.36 24.450 92.16 86.49 75.69 86.49 84.64 86.49 24.570 82.81 75.69 94.09 79.21 92.16 96.04 24.690 86.49 88.36 104.04 96.04 94.09 106.09 24.810 114.49 102.01 100.00 104.04 112.36 92.16 24.930 108.16 106.09 108.16 88.36 98.01 75.69 25.050 106.09 90.25 106.09 98.01 90.25 84.64 25.170 104.04 125.44 118.81 127.69 153.76 136.89 25.290 166.41 166.41 139.24 125.44 141.61 123.21 25.410 141.61 136.89 163.84 146.41 151.29 146.41 25.530 151.29 136.89 139.24 127.69 134.56 110.25 25.650 132.25 110.25 110.25 141.61 121.00 116.64 25.770 116.64 132.25 129.96 104.04 123.21 127.69 25.890 84.64 132.25 110.25 148.84 139.24 158.76 26.010 156.25 153.76 163.84 182.25 207.36 216.09 26.130 237.16 234.09 275.56 316.84 282.24 376.36 26.250 400.00 408.04 470.89 561.69 655.36 681.21 26.370 835.21 1062.76 1346.89 1624.09 1998.09 2530.09 26.490 3249.00 4147.36 5416.96 6707.61 7744.00 9063.04 26.610 9350.89 8817.21 7499.56 6115.24 4761.00 3600.00 26.730 2440.36 1738.89 1376.41 1056.25 858.49 707.56 26.850 635.04 538.24 453.69 428.49 388.09 345.96 26.970 327.61 313.29 272.25 246.49 259.21 249.64 27.090 225.00 234.09 182.25 198.81 204.49 151.29 27.210 179.56 174.24 148.84 153.76 141.61 166.41 27.330 174.24 187.69 158.76 158.76 161.29 179.56 27.450 187.69 158.76 163.84 139.24 163.84 146.41 27.570 123.21 153.76 136.89 108.16 146.41 136.89 27.690 132.25 153.76 146.41 127.69 132.25 141.61 27.810 163.84 156.25 156.25 151.29 139.24 141.61 27.930 123.21 134.56 110.25 112.36 125.44 90.25 28.050 106.09 98.01 84.64 102.01 94.09 90.25 28.170 100.00 92.16 88.36 102.01 88.36 102.01 28.290 84.64 84.64 94.09 88.36 92.16 86.49 28.410 92.16 84.64 102.01 88.36 92.16 82.81 28.530 96.04 92.16 100.00 98.01 98.01 116.64 28.650 90.25 116.64 102.01 104.04 108.16 108.16 28.770 82.81 92.16 86.49 102.01 94.09 100.00 28.890 94.09 106.09 106.09 118.81 106.09 127.69 29.010 104.04 123.21 110.25 104.04 92.16 108.16 29.130 96.04 98.01 94.09 90.25 100.00 98.01 29.250 81.00 92.16 96.04 86.49 110.25 94.09 29.370 98.01 98.01 94.09 94.09 88.36 88.36 29.490 84.64 79.21 86.49 88.36 84.64 98.01 29.610 110.25 118.81 110.25 106.09 106.09 114.49 29.730 136.89 114.49 132.25 151.29 146.41 148.84 29.850 156.25 129.96 141.61 114.49 110.25 104.04 29.970 118.81 108.16 98.01 94.09 108.16 102.01 30.090 84.64 98.01 92.16 86.49 102.01 96.04 30.210 92.16 84.64 82.81 77.44 84.64 72.25

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 75.69 86.49 72.25 79.21 106.09 79.21 30.450 73.96 77.44 94.09 68.89 77.44 77.44 30.570 79.21 82.81 88.36 72.25 94.09 77.44 30.690 79.21 96.04 75.69 73.96 94.09 88.36 30.810 88.36 94.09 77.44 86.49 79.21 96.04 30.930 108.16 82.81 94.09 86.49 94.09 106.09 31.050 86.49 79.21 96.04 94.09 90.25 98.01 31.170 94.09 96.04 123.21 104.04 96.04 108.16 31.290 98.01 104.04 86.49 90.25 88.36 82.81 31.410 88.36 84.64 96.04 84.64 72.25 70.56 31.530 75.69 73.96 70.56 77.44 72.25 65.61 31.650 84.64 72.25 70.56 70.56 84.64 67.24 31.770 72.25 75.69 94.09 81.00 82.81 75.69 31.890 82.81 90.25 86.49 79.21 106.09 86.49 32.010 86.49 82.81 98.01 88.36 77.44 75.69 32.130 94.09 98.01 77.44 82.81 72.25 75.69 32.250 84.64 77.44 70.56 68.89 81.00 65.61 32.370 65.61 81.00 67.24 54.76 62.41 50.41 32.490 62.41 54.76 53.29 59.29 65.61 73.96 32.610 51.84 67.24 79.21 65.61 47.61 68.89 32.730 56.25 67.24 67.24 60.84 62.41 50.41 32.850 56.25 62.41 53.29 43.56 62.41 62.41 32.970 72.25 65.61 70.56 62.41 75.69 60.84 33.090 72.25 65.61 62.41 75.69 65.61 70.56 33.210 59.29 47.61 62.41 62.41 47.61 62.41 33.330 67.24 70.56 65.61 75.69 62.41 79.21 33.450 62.41 57.76 67.24 82.81 56.25 67.24 33.570 70.56 70.56 79.21 59.29 57.76 67.24 33.690 75.69 56.25 53.29 59.29 53.29 62.41 33.810 60.84 68.89 70.56 65.61 62.41 65.61 33.930 56.25 57.76 60.84 62.41 47.61 62.41 34.050 70.56 92.16 70.56 75.69 70.56 79.21 34.170 79.21 79.21 92.16 88.36 79.21 79.21 34.290 96.04 90.25 104.04 134.56 127.69 139.24 34.410 125.44 144.00 148.84 153.76 146.41 153.76 34.530 174.24 198.81 171.61 166.41 213.16 243.36 34.650 198.81 187.69 196.00 193.21 207.36 231.04 34.770 234.09 231.04 246.49 249.64 231.04 265.69 34.890 316.84 272.25 289.00 309.76 295.84 282.24 35.010 222.01 228.01 228.01 240.25 216.09 193.21 35.130 187.69 176.89 163.84 148.84 161.29 153.76 35.250 129.96 121.00 125.44 118.81 127.69 116.64 35.370 104.04 98.01 104.04 112.36 94.09 104.04 35.490 102.01 96.04 86.49 98.01 90.25 73.96 35.610 75.69 73.96 94.09 96.04 106.09 79.21 35.730 100.00 106.09 88.36 100.00 102.01 94.09 35.850 106.09 104.04 94.09 112.36 104.04 96.04 35.970 106.09 127.69 114.49 102.01 129.96 121.00 36.090 110.25 134.56 125.44 134.56 118.81 129.96 36.210 116.64 144.00 151.29 196.00 179.56 204.49 36.330 222.01 265.69 289.00 396.01 453.69 524.41 36.450 585.64 660.49 823.69 806.56 817.96 745.29

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 670.81 585.64 515.29 470.89 384.16 324.00 36.690 302.76 249.64 225.00 243.36 219.04 207.36 36.810 210.25 240.25 156.25 184.96 169.00 187.69 36.930 204.49 182.25 166.41 148.84 171.61 156.25 37.050 158.76 146.41 169.00 174.24 163.84 153.76 37.170 174.24 146.41 141.61 134.56 136.89 139.24 37.290 134.56 134.56 132.25 134.56 158.76 146.41 37.410 132.25 136.89 151.29 158.76 146.41 163.84 37.530 129.96 148.84 139.24 161.29 174.24 163.84 37.650 176.89 139.24 148.84 153.76 169.00 144.00 37.770 163.84 136.89 121.00 136.89 139.24 144.00 37.890 112.36 112.36 108.16 116.64 118.81 100.00 38.010 112.36 86.49 110.25 86.49 102.01 110.25 38.130 75.69 94.09 102.01 102.01 82.81 90.25 38.250 81.00 81.00 100.00 84.64 98.01 96.04 38.370 82.81 98.01 112.36 94.09 90.25 106.09 38.490 100.00 96.04 94.09 90.25 98.01 84.64 38.610 102.01 84.64 86.49 84.64 79.21 84.64 38.730 72.25 88.36 81.00 86.49 84.64 82.81 38.850 86.49 81.00 96.04 79.21 75.69 86.49 38.970 106.09 88.36 98.01 88.36 118.81 102.01 39.090 121.00 125.44 127.69 144.00 171.61 156.25 39.210 163.84 184.96 201.64 210.25 309.76 345.96 39.330 441.00 529.00 645.16 767.29 876.16 912.04 39.450 876.16 756.25 665.64 630.01 580.81 515.29 39.570 424.36 357.21 275.56 219.04 216.09 207.36 39.690 176.89 228.01 182.25 228.01 228.01 207.36 39.810 187.69 234.09 210.25 234.09 240.25 246.49 39.930 252.81 256.00 201.64 225.00 231.04 256.00 40.050 252.81 252.81 252.81 246.49 289.00 313.29 40.170 324.00 392.04 404.01 428.49 428.49 436.81 40.290 342.25 327.61 331.24 292.41 282.24 240.25 40.410 207.36 176.89 141.61 108.16 127.69 127.69 40.530 114.49 127.69 121.00 108.16 92.16 82.81 40.650 110.25 96.04 84.64 102.01 100.00 86.49 40.770 110.25 96.04 108.16 100.00 100.00 108.16 40.890 108.16 86.49 96.04 100.00 82.81 106.09 41.010 98.01 96.04 104.04 102.01 98.01 92.16 41.130 100.00 100.00 106.09 104.04 92.16 110.25 41.250 96.04 79.21 106.09 110.25 94.09 102.01 41.370 104.04 96.04 86.49 77.44 82.81 86.49 41.490 79.21 64.00 90.25 94.09 75.69 86.49 41.610 72.25 92.16 73.96 94.09 100.00 84.64 41.730 114.49 100.00 100.00 94.09 100.00 106.09 41.850 118.81 110.25 110.25 110.25 112.36 127.69 41.970 121.00 139.24 136.89 144.00 123.21 129.96 42.090 139.24 148.84 163.84 174.24 171.61 187.69 42.210 184.96 216.09 268.96 295.84 342.25 388.09 42.330 449.44 529.00 595.36 702.25 665.64 615.04 42.450 595.36 547.56 488.41 436.81 408.04 313.29 42.570 299.29 243.36 225.00 196.00 136.89 132.25 42.690 148.84 123.21 114.49 94.09 100.00 114.49

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 110.25 102.01 98.01 96.04 90.25 77.44 42.930 86.49 86.49 88.36 96.04 90.25 82.81 43.050 86.49 72.25 84.64 94.09 73.96 106.09 43.170 84.64 84.64 84.64 75.69 88.36 67.24 43.290 75.69 81.00 68.89 82.81 79.21 75.69 43.410 88.36 86.49 79.21 65.61 86.49 67.24 43.530 73.96 64.00 70.56 54.76 70.56 70.56 43.650 84.64 82.81 73.96 56.25 64.00 81.00 43.770 79.21 70.56 70.56 64.00 77.44 70.56 43.890 60.84 81.00 92.16 75.69 75.69 77.44 44.010 70.56 82.81 90.25 92.16 86.49 75.69 44.130 67.24 79.21 70.56 68.89 73.96 65.61 44.250 73.96 84.64 77.44 67.24 82.81 68.89 44.370 62.41 77.44 81.00 72.25 77.44 84.64 44.490 92.16 81.00 84.64 73.96 79.21 73.96 44.610 90.25 75.69 72.25 88.36 88.36 88.36 44.730 81.00 72.25 92.16 90.25 67.24 77.44 44.850 70.56 81.00 70.56 73.96 92.16 77.44 44.970 79.21 92.16 84.64 75.69 108.16 108.16 45.090 98.01 104.04 112.36 108.16 114.49 102.01 45.210 110.25 112.36 129.96 158.76 156.25 158.76 45.330 153.76 156.25 156.25 141.61 176.89 171.61 45.450 161.29 163.84 169.00 198.81 204.49 187.69 45.570 187.69 234.09 256.00 302.76 313.29 349.69 45.690 445.21 484.00 488.41 484.00 457.96 396.01 45.810 334.89 376.36 327.61 316.84 295.84 259.21 45.930 207.36 207.36 146.41 153.76 121.00 163.84 46.050 112.36 127.69 102.01 118.81 112.36 102.01 46.170 129.96 112.36 114.49 102.01 79.21 108.16 46.290 106.09 94.09 102.01 108.16 114.49 112.36 46.410 96.04 104.04 100.00 118.81 110.25 118.81 46.530 98.01 106.09 114.49 118.81 110.25 114.49 46.650 102.01 94.09 112.36 98.01 98.01 116.64 46.770 118.81 90.25 84.64 79.21 102.01 79.21 46.890 90.25 79.21 88.36 75.69 70.56 84.64 47.010 75.69 64.00 65.61 72.25 62.41 65.61 47.130 60.84 72.25 72.25 56.25 70.56 56.25 47.250 62.41 72.25 60.84 56.25 65.61 57.76 47.370 54.76 62.41 56.25 53.29 53.29 67.24 47.490 65.61 62.41 67.24 60.84 79.21 59.29 47.610 73.96 67.24 53.29 56.25 65.61 62.41 47.730 54.76 56.25 64.00 62.41 65.61 57.76 47.850 70.56 59.29 53.29 72.25 67.24 82.81 47.970 88.36 72.25 70.56 81.00 79.21 62.41 48.090 77.44 70.56 67.24 53.29 70.56 53.29 48.210 64.00 67.24 53.29 57.76 68.89 79.21 48.330 70.56 62.41 47.61 70.56 62.41 70.56 48.450 62.41 79.21 65.61 65.61 62.41 59.29 48.570 67.24 59.29 75.69 49.00 50.41 56.25 48.690 49.00 68.89 65.61 70.56 65.61 65.61 48.810 67.24 56.25 67.24 64.00 67.24 65.61 48.930 65.61 53.29 62.41 56.25 68.89 68.89

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 57.76 68.89 67.24 59.29 84.64 82.81 49.170 64.00 73.96 68.89 59.29 70.56 79.21 49.290 88.36 73.96 65.61 77.44 60.84 65.61 49.410 77.44 82.81 73.96 81.00 82.81 82.81 49.530 96.04 94.09 94.09 108.16 114.49 102.01 49.650 134.56 129.96 127.69 161.29 163.84 153.76 49.770 190.44 198.81 225.00 225.00 272.25 334.89 49.890 364.81 424.36 600.25 676.00 789.61 992.25 50.010 1135.69 1332.25 1436.41 1505.44 1608.01 1505.44 50.130 1332.25 1162.81 1089.00 1095.61 979.69 894.01 50.250 778.41 605.16 510.76 388.09 320.41 313.29 50.370 256.00 225.00 198.81 179.56 161.29 136.89 50.490 156.25 163.84 158.76 171.61 134.56 153.76 50.610 136.89 139.24 121.00 129.96 118.81 86.49 50.730 98.01 112.36 94.09 104.04 96.04 82.81 50.850 81.00 92.16 75.69 79.21 67.24 62.41 50.970 72.25 75.69 70.56 67.24 62.41 72.25 51.090 88.36 67.24 72.25 77.44 59.29 75.69 51.210 59.29 73.96 51.84 81.00 56.25 59.29 51.330 53.29 65.61 44.89 68.89 59.29 72.25 51.450 60.84 67.24 59.29 60.84 50.41 56.25 51.570 54.76 67.24 59.29 67.24 56.25 57.76 51.690 59.29 56.25 60.84 72.25 57.76 56.25 51.810 54.76 51.84 57.76 54.76 73.96 72.25 51.930 67.24 53.29 57.76 65.61 65.61 65.61 52.050 44.89 56.25 54.76 53.29 67.24 57.76 52.170 68.89 49.00 67.24 75.69 65.61 62.41 52.290 75.69 67.24 67.24 73.96 57.76 72.25 52.410 56.25 64.00 64.00 64.00 70.56 59.29 52.530 47.61 70.56 79.21 72.25 65.61 90.25 52.650 67.24 73.96 67.24 77.44 79.21 65.61 52.770 75.69 67.24 77.44 62.41 75.69 77.44 52.890 77.44 79.21 70.56 73.96 67.24 65.61 53.010 56.25 70.56 86.49 65.61 67.24 56.25 53.130 64.00 73.96 75.69 92.16 77.44 88.36 53.250 84.64 75.69 70.56 77.44 79.21 77.44 53.370 70.56 75.69 65.61 81.00 96.04 90.25 53.490 82.81 82.81 75.69 88.36 79.21 88.36 53.610 92.16 100.00 100.00 79.21 90.25 92.16 53.730 112.36 90.25 98.01 112.36 104.04 100.00 53.850 96.04 110.25 98.01 123.21 104.04 100.00 53.970 88.36 106.09 92.16 64.00 118.81 96.04 54.090 96.04 90.25 123.21 108.16 116.64 112.36 54.210 100.00 114.49 136.89 136.89 139.24 123.21 54.330 114.49 125.44 118.81 116.64 108.16 104.04 54.450 132.25 129.96 163.84 146.41 174.24 166.41 54.570 166.41 190.44 201.64 176.89 222.01 295.84 54.690 320.41 368.64 445.21 479.61 515.29 519.84 54.810 515.29 515.29 506.25 436.81 453.69 449.44 54.930 384.16 412.09 384.16 338.56 306.25 316.84 55.050 265.69 225.00 234.09 252.81 259.21 262.44 55.170 259.21 272.25 327.61 302.76 331.24 320.41

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 345.96 282.24 265.69 268.96 256.00 252.81 55.410 228.01 275.56 216.09 225.00 184.96 184.96 55.530 169.00 158.76 153.76 148.84 153.76 139.24 55.650 148.84 151.29 156.25 153.76 153.76 151.29 55.770 136.89 153.76 169.00 132.25 118.81 129.96 55.890 139.24 134.56 118.81 125.44 110.25 106.09 56.010 121.00 118.81 118.81 102.01 121.00 98.01 56.130 136.89 114.49 118.81 102.01 123.21 114.49 56.250 127.69 114.49 114.49 112.36 94.09 106.09 56.370 118.81 112.36 104.04 121.00 100.00 98.01 56.490 112.36 100.00 116.64 106.09 112.36 98.01 56.610 102.01 121.00 98.01 100.00 88.36 112.36 56.730 108.16 104.04 106.09 96.04 100.00 82.81 56.850 96.04 94.09 84.64 96.04 98.01 102.01 56.970 92.16 104.04 104.04 110.25 110.25 112.36 57.090 110.25 134.56 118.81 125.44 86.49 118.81 57.210 106.09 110.25 104.04 114.49 100.00 104.04 57.330 114.49 108.16 88.36 100.00 110.25 116.64 57.450 86.49 88.36 100.00 79.21 110.25 92.16 57.570 92.16 75.69 102.01 100.00 86.49 81.00 57.690 57.76 84.64 98.01 77.44 92.16 86.49 57.810 82.81 73.96 92.16 77.44 72.25 92.16 57.930 82.81 82.81 90.25 82.81 62.41 86.49 58.050 86.49 86.49 88.36 84.64 67.24 90.25 58.170 73.96 102.01 75.69 79.21 84.64 90.25 58.290 79.21 70.56 88.36 68.89 70.56 88.36 58.410 90.25 77.44 67.24 94.09 73.96 88.36 58.530 96.04 90.25 90.25 81.00 86.49 75.69 58.650 90.25 100.00 68.89 86.49 96.04 81.00 58.770 82.81 72.25 84.64 81.00 79.21 86.49 58.890 86.49 75.69 102.01 77.44 96.04 96.04 59.010 96.04 98.01 86.49 88.36 100.00 116.64 59.130 102.01 100.00 98.01 114.49 116.64 100.00 59.250 102.01 106.09 125.44 116.64 110.25 121.00 59.370 114.49 134.56 123.21 156.25 136.89 182.25 59.490 153.76 151.29 190.44 190.44 196.00 231.04 59.610 228.01 265.69 249.64 338.56 353.44 432.64 59.730 445.21 538.24 620.01 761.76 806.56 992.25 59.850 1062.76 1142.44 1169.64 1108.89 1030.41 942.49 59.970 841.00 823.69 756.25 745.29 750.76 640.09 60.090 610.09 510.76 445.21 345.96 309.76 259.21 60.210 268.96 228.01 210.25 190.44 201.64 148.84 60.330 161.29 174.24 169.00 136.89 153.76 127.69 60.450 134.56 136.89 127.69 114.49 123.21 121.00 60.570 127.69 112.36 123.21 112.36 125.44 112.36 60.690 102.01 127.69 94.09 127.69 121.00 110.25 60.810 100.00 100.00 112.36 114.49 116.64 102.01 60.930 104.04 96.04 104.04 102.01 102.01 123.21 61.050 106.09 112.36 102.01 102.01 112.36 136.89 61.170 110.25 108.16 125.44 118.81 136.89 136.89 61.290 139.24 129.96 125.44 163.84 156.25 166.41 61.410 153.76 169.00 174.24 158.76 190.44 187.69

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 201.64 182.25 182.25 207.36 204.49 216.09 61.650 216.09 182.25 207.36 228.01 201.64 193.21 61.770 196.00 219.04 213.16 213.16 216.09 193.21 61.890 182.25 166.41 171.61 184.96 139.24 156.25 62.010 158.76 161.29 129.96 158.76 148.84 108.16 62.130 125.44 116.64 112.36 121.00 121.00 132.25 62.250 118.81 125.44 121.00 110.25 123.21 92.16 62.370 114.49 114.49 112.36 132.25 118.81 114.49 62.490 123.21 98.01 114.49 90.25 102.01 112.36 62.610 102.01 102.01 106.09 84.64 84.64 94.09 62.730 96.04 96.04 96.04 77.44 102.01 86.49 62.850 77.44 92.16 86.49 90.25 79.21 102.01 62.970 86.49 82.81 86.49 82.81 72.25 72.25 63.090 88.36 98.01 88.36 75.69 75.69 84.64 63.210 72.25 90.25 88.36 86.49 90.25 94.09 63.330 77.44 49.00 84.64 86.49 96.04 88.36 63.450 88.36 82.81 79.21 70.56 104.04 79.21 63.570 102.01 100.00 81.00 82.81 98.01 100.00 63.690 110.25 116.64 121.00 136.89 121.00 179.56 63.810 139.24 187.69 198.81 204.49 246.49 243.36 63.930 289.00 289.00 268.96 275.56 246.49 228.01 64.050 201.64 198.81 225.00 204.49 198.81 184.96 64.170 169.00 179.56 153.76 127.69 134.56 125.44 64.290 100.00 106.09 94.09 104.04 102.01 77.44 64.410 88.36 90.25 94.09 82.81 79.21 77.44 64.530 88.36 70.56 70.56 72.25 79.21 86.49 64.650 84.64 59.29 65.61 77.44 82.81 77.44 64.770 96.04 75.69 77.44 88.36 82.81 92.16 64.890 72.25 79.21 86.49 88.36 94.09 68.89 65.010 84.64 86.49 96.04 82.81 77.44 73.96 65.130 79.21 92.16 67.24 88.36 82.81 94.09 65.250 88.36 70.56 88.36 86.49 90.25 86.49 65.370 79.21 90.25 102.01 82.81 82.81 96.04 65.490 77.44 86.49 94.09 90.25 90.25 112.36 65.610 94.09 136.89 123.21 118.81 112.36 112.36 65.730 125.44 94.09 125.44 118.81 127.69 98.01 65.850 102.01 116.64 92.16 77.44 108.16 73.96 65.970 104.04 84.64 84.64 73.96 79.21 77.44 66.090 72.25 84.64 86.49 79.21 90.25 88.36 66.210 73.96 88.36 82.81 94.09 81.00 79.21 66.330 73.96 68.89 68.89 92.16 100.00 72.25 66.450 72.25 79.21 79.21 72.25 86.49 86.49 66.570 79.21 86.49 79.21 75.69 94.09 92.16 66.690 79.21 86.49 77.44 84.64 72.25 84.64 66.810 106.09 86.49 79.21 94.09 96.04 84.64 66.930 106.09 102.01 104.04 94.09 110.25 98.01 67.050 118.81 116.64 108.16 108.16 106.09 118.81 67.170 125.44 100.00 121.00 151.29 144.00 144.00 67.290 158.76 171.61 179.56 204.49 201.64 228.01 67.410 228.01 231.04 275.56 306.25 334.89 380.25 67.530 441.00 479.61 561.69 625.00 718.24 778.41 67.650 812.25 800.89 823.69 739.84 681.21 625.00

File: JC1.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 635.04 625.00 681.21 729.00 691.69 702.25 67.890 750.76 756.25 756.25 812.25 900.00 948.64 68.010 1011.24 1102.24 1260.25 1267.36 1204.09 1142.44 68.130 1128.96 1049.76 1095.61 1075.84 1128.96 1169.64 68.250 1149.21 1004.89 967.21 784.00 718.24 670.81 68.370 635.04 590.49 556.96 515.29 479.61 416.16 68.490 364.81 309.76 292.41 285.61 272.25 246.49 68.610 210.25 201.64 187.69 171.61 174.24 158.76 68.730 158.76 134.56 158.76 153.76 136.89 148.84 68.850 146.41 125.44 125.44 116.64 110.25 116.64 68.970 129.96 136.89 118.81 116.64 110.25 112.36 69.090 125.44 141.61 132.25 129.96 127.69 123.21 69.210 127.69 121.00 112.36 118.81 116.64 104.04 69.330 104.04 132.25 116.64 136.89 136.89 136.89 69.450 127.69 118.81 127.69 114.49 132.25 94.09 69.570 118.81 106.09 118.81 110.25 134.56 121.00 69.690 112.36 98.01 116.64 96.04 104.04 96.04 69.810 92.16 106.09 114.49 106.09 121.00 112.36 69.930 112.36 112.36 125.44 106.09 _

100

File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC2 Data measured at: 24-Jan-2011 12:03:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 645.1600 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 645.16 640.09 590.49 635.04 571.21 585.64 2.130 576.00 556.96 590.49 533.61 529.00 552.25 2.250 492.84 510.76 441.00 453.69 457.96 441.00 2.370 449.44 441.00 445.21 412.09 396.01 400.00 2.490 392.04 420.25 384.16 392.04 357.21 404.01 2.610 368.64 404.01 320.41 368.64 334.89 368.64 2.730 324.00 316.84 324.00 306.25 309.76 299.29 2.850 292.41 282.24 306.25 292.41 256.00 272.25 2.970 237.16 262.44 275.56 285.61 285.61 222.01 3.090 262.44 246.49 231.04 228.01 256.00 246.49 3.210 252.81 216.09 222.01 228.01 222.01 268.96 3.330 201.64 228.01 213.16 207.36 210.25 225.00 3.450 176.89 204.49 201.64 174.24 213.16 187.69 3.570 198.81 184.96 231.04 158.76 193.21 187.69 3.690 182.25 176.89 184.96 169.00 184.96 193.21 3.810 187.69 184.96 161.29 166.41 171.61 144.00 3.930 184.96 148.84 174.24 136.89 158.76 151.29 4.050 169.00 179.56 169.00 146.41 151.29 169.00 4.170 139.24 169.00 158.76 121.00 134.56 148.84 4.290 141.61 136.89 134.56 139.24 132.25 166.41 4.410 139.24 125.44 136.89 125.44 114.49 153.76 4.530 144.00 136.89 110.25 123.21 127.69 127.69 4.650 153.76 123.21 139.24 132.25 110.25 146.41 4.770 132.25 129.96 127.69 114.49 110.25 123.21 4.890 118.81 125.44 141.61 121.00 108.16 134.56 5.010 139.24 125.44 132.25 121.00 118.81 144.00 5.130 141.61 118.81 134.56 125.44 116.64 110.25 5.250 129.96 116.64 104.04 121.00 134.56 94.09

101

File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 121.00 114.49 118.81 112.36 98.01 112.36 5.490 110.25 112.36 110.25 118.81 106.09 82.81 5.610 114.49 104.04 90.25 102.01 121.00 112.36 5.730 104.04 116.64 92.16 108.16 94.09 106.09 5.850 104.04 123.21 100.00 118.81 125.44 98.01 5.970 123.21 100.00 88.36 108.16 98.01 94.09 6.090 88.36 94.09 98.01 108.16 100.00 110.25 6.210 106.09 96.04 121.00 92.16 110.25 94.09 6.330 114.49 94.09 86.49 106.09 98.01 98.01 6.450 110.25 84.64 90.25 90.25 112.36 121.00 6.570 102.01 102.01 94.09 84.64 100.00 81.00 6.690 108.16 72.25 110.25 86.49 82.81 84.64 6.810 114.49 81.00 104.04 86.49 92.16 98.01 6.930 94.09 100.00 86.49 100.00 104.04 82.81 7.050 82.81 86.49 100.00 94.09 82.81 86.49 7.170 86.49 88.36 82.81 96.04 72.25 94.09 7.290 108.16 82.81 100.00 79.21 82.81 90.25 7.410 88.36 79.21 92.16 70.56 90.25 79.21 7.530 82.81 86.49 90.25 77.44 98.01 100.00 7.650 86.49 75.69 79.21 100.00 81.00 70.56 7.770 82.81 92.16 96.04 98.01 79.21 79.21 7.890 86.49 79.21 94.09 86.49 84.64 84.64 8.010 81.00 98.01 104.04 75.69 102.01 96.04 8.130 72.25 94.09 86.49 67.24 79.21 86.49 8.250 90.25 94.09 112.36 84.64 75.69 86.49 8.370 94.09 82.81 79.21 81.00 77.44 94.09 8.490 82.81 86.49 88.36 84.64 88.36 82.81 8.610 86.49 96.04 94.09 92.16 92.16 86.49 8.730 100.00 100.00 94.09 82.81 70.56 94.09 8.850 98.01 90.25 94.09 90.25 88.36 96.04 8.970 75.69 86.49 90.25 96.04 90.25 92.16 9.090 100.00 98.01 104.04 96.04 90.25 94.09 9.210 84.64 82.81 96.04 100.00 84.64 90.25 9.330 86.49 90.25 100.00 79.21 90.25 98.01 9.450 88.36 75.69 77.44 84.64 86.49 86.49 9.570 88.36 90.25 79.21 70.56 81.00 73.96 9.690 84.64 75.69 81.00 90.25 72.25 81.00 9.810 92.16 75.69 79.21 86.49 90.25 98.01 9.930 86.49 86.49 75.69 72.25 84.64 90.25 10.050 84.64 70.56 75.69 92.16 82.81 90.25 10.170 72.25 100.00 77.44 82.81 82.81 65.61 10.290 72.25 92.16 79.21 77.44 84.64 79.21 10.410 62.41 77.44 70.56 75.69 73.96 84.64 10.530 92.16 81.00 92.16 64.00 75.69 88.36 10.650 70.56 82.81 84.64 88.36 88.36 86.49 10.770 96.04 84.64 75.69 75.69 96.04 98.01 10.890 98.01 90.25 65.61 72.25 84.64 96.04 11.010 84.64 77.44 84.64 90.25 82.81 98.01 11.130 98.01 86.49 75.69 102.01 90.25 82.81 11.250 92.16 77.44 112.36 82.81 94.09 98.01 11.370 94.09 102.01 86.49 96.04 118.81 92.16 11.490 86.49 94.09 108.16 98.01 92.16 96.04

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File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 106.09 112.36 98.01 106.09 96.04 94.09 11.730 94.09 98.01 86.49 102.01 114.49 86.49 11.850 102.01 90.25 86.49 110.25 106.09 98.01 11.970 108.16 90.25 94.09 90.25 88.36 86.49 12.090 88.36 79.21 96.04 82.81 65.61 75.69 12.210 79.21 92.16 56.25 67.24 88.36 75.69 12.330 77.44 67.24 62.41 68.89 75.69 59.29 12.450 86.49 70.56 65.61 70.56 57.76 59.29 12.570 79.21 67.24 59.29 59.29 67.24 43.56 12.690 73.96 67.24 65.61 51.84 53.29 62.41 12.810 62.41 57.76 64.00 68.89 70.56 60.84 12.930 53.29 56.25 57.76 60.84 59.29 59.29 13.050 56.25 59.29 57.76 54.76 65.61 59.29 13.170 56.25 59.29 65.61 47.61 64.00 62.41 13.290 54.76 67.24 56.25 47.61 77.44 44.89 13.410 56.25 51.84 56.25 53.29 60.84 50.41 13.530 75.69 57.76 59.29 59.29 64.00 62.41 13.650 50.41 59.29 51.84 49.00 50.41 56.25 13.770 44.89 65.61 56.25 46.24 54.76 62.41 13.890 51.84 47.61 50.41 56.25 62.41 53.29 14.010 50.41 53.29 60.84 40.96 56.25 56.25 14.130 72.25 53.29 54.76 60.84 57.76 38.44 14.250 47.61 42.25 65.61 47.61 50.41 46.24 14.370 56.25 50.41 43.56 62.41 44.89 47.61 14.490 57.76 42.25 59.29 56.25 50.41 62.41 14.610 53.29 40.96 51.84 47.61 47.61 46.24 14.730 44.89 51.84 60.84 44.89 49.00 40.96 14.850 43.56 42.25 53.29 53.29 40.96 47.61 14.970 39.69 42.25 50.41 62.41 49.00 53.29 15.090 38.44 44.89 59.29 54.76 56.25 59.29 15.210 65.61 75.69 56.25 56.25 49.00 51.84 15.330 53.29 42.25 47.61 49.00 50.41 57.76 15.450 50.41 42.25 46.24 44.89 49.00 47.61 15.570 53.29 62.41 39.69 50.41 49.00 50.41 15.690 56.25 46.24 60.84 54.76 49.00 46.24 15.810 50.41 57.76 47.61 64.00 42.25 44.89 15.930 53.29 56.25 47.61 47.61 50.41 60.84 16.050 49.00 50.41 42.25 53.29 50.41 38.44 16.170 59.29 49.00 47.61 54.76 50.41 53.29 16.290 42.25 54.76 53.29 49.00 56.25 42.25 16.410 53.29 51.84 36.00 47.61 54.76 53.29 16.530 60.84 47.61 59.29 47.61 53.29 47.61 16.650 54.76 42.25 47.61 62.41 62.41 38.44 16.770 64.00 50.41 50.41 46.24 43.56 59.29 16.890 54.76 65.61 57.76 53.29 49.00 64.00 17.010 43.56 46.24 51.84 62.41 62.41 62.41 17.130 70.56 67.24 59.29 54.76 47.61 59.29 17.250 53.29 42.25 57.76 53.29 56.25 51.84 17.370 49.00 64.00 50.41 59.29 50.41 56.25 17.490 75.69 65.61 50.41 62.41 59.29 56.25 17.610 59.29 51.84 75.69 62.41 68.89 59.29 17.730 72.25 59.29 65.61 79.21 51.84 79.21

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 65.61 77.44 60.84 73.96 60.84 75.69 17.970 67.24 70.56 73.96 77.44 81.00 79.21 18.090 57.76 72.25 70.56 64.00 51.84 59.29 18.210 72.25 53.29 70.56 67.24 54.76 72.25 18.330 79.21 75.69 60.84 77.44 53.29 65.61 18.450 77.44 59.29 75.69 51.84 75.69 73.96 18.570 70.56 46.24 59.29 70.56 64.00 56.25 18.690 57.76 72.25 75.69 70.56 67.24 77.44 18.810 70.56 67.24 70.56 72.25 67.24 62.41 18.930 82.81 53.29 73.96 79.21 72.25 70.56 19.050 73.96 68.89 67.24 77.44 50.41 86.49 19.170 59.29 73.96 62.41 73.96 82.81 82.81 19.290 73.96 75.69 82.81 96.04 88.36 90.25 19.410 70.56 98.01 100.00 102.01 88.36 90.25 19.530 114.49 121.00 88.36 118.81 102.01 106.09 19.650 153.76 116.64 123.21 144.00 161.29 161.29 19.770 169.00 169.00 190.44 179.56 210.25 201.64 19.890 222.01 196.00 204.49 184.96 210.25 225.00 20.010 243.36 207.36 210.25 222.01 219.04 187.69 20.130 207.36 158.76 179.56 196.00 193.21 187.69 20.250 184.96 196.00 193.21 182.25 174.24 176.89 20.370 190.44 166.41 174.24 171.61 153.76 171.61 20.490 144.00 171.61 141.61 171.61 169.00 161.29 20.610 156.25 156.25 171.61 193.21 174.24 153.76 20.730 153.76 174.24 210.25 240.25 216.09 210.25 20.850 213.16 213.16 187.69 187.69 201.64 187.69 20.970 198.81 153.76 184.96 198.81 196.00 176.89 21.090 184.96 179.56 213.16 198.81 196.00 198.81 21.210 201.64 213.16 196.00 201.64 201.64 207.36 21.330 179.56 190.44 187.69 198.81 201.64 198.81 21.450 184.96 190.44 158.76 179.56 169.00 176.89 21.570 169.00 153.76 156.25 153.76 144.00 136.89 21.690 151.29 146.41 141.61 129.96 153.76 134.56 21.810 144.00 136.89 116.64 106.09 134.56 129.96 21.930 134.56 116.64 104.04 139.24 136.89 134.56 22.050 132.25 121.00 112.36 104.04 116.64 106.09 22.170 106.09 125.44 112.36 116.64 114.49 102.01 22.290 94.09 121.00 108.16 100.00 104.04 100.00 22.410 98.01 106.09 106.09 104.04 114.49 102.01 22.530 108.16 102.01 96.04 108.16 121.00 84.64 22.650 118.81 84.64 92.16 100.00 108.16 123.21 22.770 92.16 96.04 82.81 106.09 106.09 88.36 22.890 100.00 106.09 112.36 106.09 96.04 92.16 23.010 110.25 104.04 96.04 104.04 106.09 94.09 23.130 112.36 108.16 104.04 110.25 100.00 90.25 23.250 108.16 100.00 84.64 88.36 112.36 92.16 23.370 96.04 102.01 118.81 98.01 104.04 88.36 23.490 100.00 90.25 121.00 121.00 104.04 94.09 23.610 94.09 123.21 121.00 106.09 106.09 110.25 23.730 102.01 114.49 106.09 104.04 96.04 116.64 23.850 110.25 104.04 102.01 121.00 132.25 108.16 23.970 106.09 110.25 104.04 134.56 114.49 114.49

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File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 132.25 112.36 129.96 116.64 118.81 136.89 24.210 121.00 129.96 106.09 110.25 121.00 123.21 24.330 104.04 121.00 108.16 151.29 118.81 134.56 24.450 116.64 108.16 123.21 121.00 121.00 114.49 24.570 108.16 116.64 108.16 102.01 114.49 127.69 24.690 106.09 121.00 110.25 121.00 123.21 116.64 24.810 121.00 125.44 96.04 121.00 134.56 118.81 24.930 139.24 118.81 118.81 116.64 110.25 125.44 25.050 112.36 114.49 112.36 121.00 118.81 102.01 25.170 106.09 116.64 88.36 90.25 110.25 104.04 25.290 102.01 114.49 114.49 98.01 114.49 114.49 25.410 106.09 104.04 94.09 110.25 112.36 129.96 25.530 106.09 102.01 104.04 98.01 102.01 92.16 25.650 114.49 92.16 86.49 96.04 102.01 84.64 25.770 104.04 104.04 98.01 92.16 121.00 100.00 25.890 92.16 121.00 102.01 100.00 106.09 110.25 26.010 106.09 121.00 94.09 90.25 100.00 121.00 26.130 81.00 100.00 110.25 102.01 104.04 112.36 26.250 112.36 100.00 116.64 110.25 116.64 118.81 26.370 136.89 112.36 121.00 129.96 116.64 161.29 26.490 136.89 163.84 166.41 228.01 278.89 353.44 26.610 364.81 364.81 285.61 265.69 240.25 179.56 26.730 158.76 123.21 98.01 94.09 102.01 110.25 26.850 123.21 112.36 90.25 106.09 70.56 88.36 26.970 98.01 92.16 100.00 106.09 98.01 98.01 27.090 79.21 106.09 98.01 73.96 92.16 88.36 27.210 94.09 82.81 92.16 81.00 79.21 96.04 27.330 104.04 94.09 94.09 88.36 92.16 94.09 27.450 84.64 92.16 86.49 86.49 86.49 92.16 27.570 94.09 88.36 104.04 77.44 82.81 79.21 27.690 84.64 77.44 79.21 79.21 88.36 86.49 27.810 88.36 77.44 82.81 108.16 82.81 86.49 27.930 82.81 75.69 77.44 82.81 92.16 64.00 28.050 81.00 70.56 92.16 81.00 62.41 77.44 28.170 88.36 79.21 84.64 59.29 84.64 65.61 28.290 64.00 84.64 70.56 73.96 72.25 70.56 28.410 75.69 92.16 92.16 75.69 67.24 77.44 28.530 86.49 79.21 88.36 88.36 88.36 79.21 28.650 88.36 56.25 86.49 72.25 70.56 67.24 28.770 96.04 79.21 90.25 73.96 67.24 67.24 28.890 73.96 90.25 84.64 73.96 77.44 84.64 29.010 79.21 75.69 70.56 75.69 67.24 82.81 29.130 73.96 88.36 84.64 67.24 88.36 75.69 29.250 70.56 75.69 77.44 72.25 73.96 68.89 29.370 88.36 56.25 70.56 59.29 70.56 82.81 29.490 86.49 77.44 72.25 84.64 73.96 65.61 29.610 72.25 86.49 67.24 84.64 51.84 79.21 29.730 72.25 75.69 79.21 62.41 68.89 67.24 29.850 70.56 70.56 90.25 53.29 68.89 59.29 29.970 68.89 77.44 62.41 77.44 75.69 72.25 30.090 59.29 75.69 75.69 70.56 86.49 72.25 30.210 67.24 82.81 73.96 59.29 67.24 67.24

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File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 62.41 84.64 67.24 68.89 67.24 65.61 30.450 82.81 88.36 53.29 59.29 67.24 67.24 30.570 65.61 77.44 92.16 68.89 82.81 79.21 30.690 75.69 81.00 65.61 62.41 68.89 67.24 30.810 75.69 62.41 82.81 72.25 59.29 70.56 30.930 73.96 65.61 67.24 67.24 62.41 72.25 31.050 84.64 70.56 68.89 75.69 64.00 67.24 31.170 72.25 72.25 70.56 70.56 72.25 79.21 31.290 68.89 70.56 57.76 75.69 67.24 59.29 31.410 77.44 67.24 75.69 62.41 79.21 67.24 31.530 84.64 77.44 77.44 77.44 82.81 59.29 31.650 72.25 82.81 64.00 67.24 81.00 54.76 31.770 72.25 65.61 94.09 79.21 77.44 60.84 31.890 67.24 77.44 77.44 79.21 81.00 72.25 32.010 70.56 70.56 75.69 84.64 86.49 60.84 32.130 72.25 96.04 92.16 90.25 84.64 92.16 32.250 77.44 81.00 70.56 86.49 72.25 86.49 32.370 86.49 79.21 81.00 75.69 79.21 75.69 32.490 100.00 96.04 92.16 96.04 96.04 112.36 32.610 86.49 79.21 98.01 110.25 79.21 86.49 32.730 94.09 114.49 100.00 86.49 90.25 108.16 32.850 106.09 108.16 112.36 96.04 114.49 112.36 32.970 86.49 118.81 102.01 108.16 118.81 129.96 33.090 121.00 132.25 121.00 136.89 112.36 129.96 33.210 108.16 100.00 129.96 114.49 102.01 121.00 33.330 125.44 121.00 110.25 125.44 114.49 121.00 33.450 118.81 123.21 116.64 116.64 108.16 102.01 33.570 132.25 129.96 116.64 106.09 110.25 110.25 33.690 112.36 104.04 102.01 106.09 114.49 92.16 33.810 110.25 106.09 108.16 110.25 102.01 106.09 33.930 118.81 121.00 114.49 110.25 102.01 90.25 34.050 106.09 114.49 96.04 92.16 88.36 108.16 34.170 94.09 106.09 104.04 116.64 100.00 106.09 34.290 112.36 100.00 96.04 121.00 102.01 112.36 34.410 108.16 136.89 114.49 116.64 125.44 112.36 34.530 136.89 144.00 129.96 129.96 146.41 136.89 34.650 151.29 132.25 176.89 153.76 182.25 174.24 34.770 176.89 176.89 163.84 161.29 174.24 182.25 34.890 174.24 163.84 148.84 176.89 196.00 184.96 35.010 190.44 176.89 210.25 153.76 166.41 174.24 35.130 179.56 148.84 166.41 169.00 187.69 156.25 35.250 163.84 153.76 174.24 163.84 161.29 163.84 35.370 158.76 190.44 166.41 146.41 158.76 153.76 35.490 163.84 144.00 169.00 182.25 184.96 153.76 35.610 158.76 190.44 146.41 153.76 169.00 174.24 35.730 184.96 187.69 153.76 184.96 174.24 184.96 35.850 156.25 182.25 184.96 169.00 174.24 184.96 35.970 176.89 174.24 174.24 182.25 187.69 179.56 36.090 184.96 176.89 182.25 174.24 187.69 210.25 36.210 198.81 187.69 182.25 190.44 219.04 190.44 36.330 201.64 210.25 222.01 219.04 210.25 228.01 36.450 231.04 216.09 272.25 268.96 278.89 285.61

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File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 252.81 272.25 275.56 262.44 302.76 278.89 36.690 285.61 262.44 292.41 299.29 282.24 313.29 36.810 334.89 282.24 338.56 278.89 302.76 299.29 36.930 316.84 278.89 334.89 282.24 309.76 289.00 37.050 275.56 289.00 299.29 268.96 262.44 262.44 37.170 259.21 243.36 225.00 225.00 246.49 222.01 37.290 240.25 216.09 204.49 193.21 174.24 184.96 37.410 216.09 193.21 187.69 193.21 184.96 182.25 37.530 158.76 153.76 161.29 174.24 184.96 179.56 37.650 193.21 176.89 193.21 174.24 171.61 176.89 37.770 153.76 158.76 184.96 161.29 169.00 176.89 37.890 174.24 151.29 153.76 182.25 163.84 169.00 38.010 146.41 163.84 141.61 151.29 144.00 146.41 38.130 136.89 129.96 146.41 148.84 153.76 127.69 38.250 146.41 136.89 132.25 136.89 129.96 139.24 38.370 136.89 151.29 129.96 134.56 148.84 134.56 38.490 121.00 121.00 136.89 121.00 139.24 118.81 38.610 127.69 136.89 136.89 153.76 146.41 129.96 38.730 139.24 123.21 121.00 127.69 127.69 118.81 38.850 136.89 121.00 129.96 127.69 118.81 121.00 38.970 118.81 127.69 116.64 127.69 127.69 134.56 39.090 132.25 132.25 139.24 156.25 112.36 116.64 39.210 146.41 141.61 146.41 123.21 141.61 146.41 39.330 134.56 146.41 134.56 144.00 171.61 179.56 39.450 158.76 156.25 176.89 153.76 174.24 193.21 39.570 187.69 184.96 207.36 204.49 193.21 196.00 39.690 201.64 198.81 187.69 204.49 213.16 222.01 39.810 219.04 216.09 216.09 216.09 201.64 228.01 39.930 246.49 234.09 222.01 228.01 201.64 237.16 40.050 187.69 171.61 237.16 207.36 166.41 196.00 40.170 184.96 161.29 161.29 169.00 146.41 179.56 40.290 166.41 169.00 161.29 151.29 163.84 144.00 40.410 163.84 118.81 144.00 146.41 136.89 125.44 40.530 129.96 153.76 151.29 129.96 129.96 127.69 40.650 127.69 139.24 121.00 118.81 121.00 139.24 40.770 141.61 102.01 136.89 116.64 116.64 118.81 40.890 139.24 132.25 104.04 106.09 112.36 114.49 41.010 136.89 129.96 127.69 144.00 118.81 136.89 41.130 121.00 114.49 127.69 141.61 129.96 127.69 41.250 116.64 132.25 116.64 114.49 121.00 121.00 41.370 127.69 123.21 125.44 141.61 144.00 125.44 41.490 121.00 139.24 125.44 114.49 123.21 134.56 41.610 106.09 104.04 108.16 125.44 125.44 114.49 41.730 112.36 102.01 116.64 106.09 116.64 114.49 41.850 106.09 106.09 110.25 81.00 90.25 94.09 41.970 94.09 102.01 104.04 94.09 84.64 94.09 42.090 106.09 112.36 96.04 88.36 79.21 94.09 42.210 104.04 72.25 94.09 104.04 123.21 98.01 42.330 104.04 116.64 90.25 112.36 110.25 98.01 42.450 96.04 114.49 104.04 94.09 104.04 116.64 42.570 77.44 90.25 110.25 94.09 92.16 94.09 42.690 86.49 90.25 88.36 86.49 94.09 100.00

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File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 81.00 84.64 96.04 75.69 94.09 90.25 42.930 88.36 82.81 102.01 84.64 98.01 79.21 43.050 94.09 77.44 94.09 106.09 90.25 104.04 43.170 100.00 98.01 96.04 82.81 77.44 84.64 43.290 94.09 92.16 96.04 77.44 82.81 84.64 43.410 73.96 94.09 98.01 82.81 72.25 75.69 43.530 79.21 81.00 79.21 90.25 82.81 81.00 43.650 92.16 92.16 96.04 73.96 77.44 88.36 43.770 96.04 90.25 70.56 88.36 86.49 86.49 43.890 96.04 77.44 67.24 96.04 90.25 79.21 44.010 72.25 98.01 81.00 68.89 72.25 79.21 44.130 77.44 70.56 62.41 75.69 82.81 98.01 44.250 67.24 75.69 86.49 96.04 88.36 67.24 44.370 75.69 86.49 82.81 90.25 65.61 86.49 44.490 72.25 64.00 82.81 88.36 77.44 104.04 44.610 81.00 67.24 79.21 72.25 77.44 79.21 44.730 77.44 75.69 82.81 75.69 70.56 65.61 44.850 79.21 67.24 88.36 81.00 77.44 82.81 44.970 59.29 81.00 88.36 92.16 86.49 77.44 45.090 68.89 70.56 73.96 96.04 84.64 90.25 45.210 79.21 75.69 92.16 73.96 92.16 90.25 45.330 70.56 84.64 98.01 82.81 90.25 77.44 45.450 79.21 84.64 72.25 75.69 88.36 84.64 45.570 75.69 88.36 79.21 90.25 88.36 79.21 45.690 88.36 67.24 100.00 118.81 114.49 77.44 45.810 75.69 96.04 88.36 88.36 82.81 72.25 45.930 77.44 82.81 92.16 75.69 86.49 75.69 46.050 72.25 94.09 77.44 81.00 90.25 82.81 46.170 86.49 56.25 86.49 84.64 96.04 72.25 46.290 79.21 77.44 100.00 88.36 114.49 88.36 46.410 79.21 100.00 94.09 106.09 98.01 100.00 46.530 102.01 96.04 79.21 90.25 108.16 79.21 46.650 96.04 98.01 96.04 86.49 100.00 92.16 46.770 86.49 84.64 94.09 94.09 102.01 98.01 46.890 94.09 82.81 81.00 67.24 86.49 77.44 47.010 73.96 86.49 86.49 65.61 92.16 77.44 47.130 56.25 82.81 90.25 82.81 79.21 75.69 47.250 70.56 77.44 65.61 79.21 82.81 68.89 47.370 86.49 81.00 79.21 72.25 82.81 72.25 47.490 92.16 73.96 72.25 64.00 81.00 82.81 47.610 56.25 77.44 88.36 72.25 72.25 82.81 47.730 82.81 70.56 67.24 70.56 70.56 82.81 47.850 82.81 67.24 65.61 75.69 84.64 82.81 47.970 56.25 62.41 75.69 56.25 62.41 65.61 48.090 88.36 67.24 67.24 75.69 77.44 77.44 48.210 72.25 68.89 82.81 77.44 64.00 73.96 48.330 77.44 65.61 68.89 62.41 77.44 60.84 48.450 67.24 65.61 67.24 70.56 68.89 79.21 48.570 77.44 67.24 73.96 65.61 84.64 70.56 48.690 59.29 70.56 70.56 62.41 72.25 65.61 48.810 77.44 84.64 72.25 56.25 77.44 79.21 48.930 53.29 67.24 79.21 82.81 86.49 77.44

108

File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 75.69 86.49 82.81 73.96 75.69 62.41 49.170 75.69 67.24 68.89 72.25 62.41 82.81 49.290 70.56 68.89 75.69 82.81 86.49 84.64 49.410 67.24 79.21 67.24 72.25 65.61 75.69 49.530 72.25 86.49 72.25 64.00 64.00 79.21 49.650 75.69 72.25 72.25 73.96 75.69 82.81 49.770 88.36 70.56 79.21 79.21 81.00 75.69 49.890 67.24 84.64 79.21 98.01 96.04 100.00 50.010 108.16 123.21 121.00 114.49 125.44 118.81 50.130 108.16 100.00 116.64 108.16 123.21 88.36 50.250 92.16 108.16 96.04 92.16 82.81 72.25 50.370 88.36 86.49 70.56 86.49 64.00 77.44 50.490 73.96 102.01 88.36 98.01 77.44 79.21 50.610 108.16 75.69 88.36 88.36 82.81 81.00 50.730 88.36 90.25 94.09 98.01 98.01 86.49 50.850 82.81 102.01 98.01 84.64 96.04 86.49 50.970 82.81 92.16 86.49 86.49 104.04 90.25 51.090 92.16 84.64 96.04 86.49 84.64 79.21 51.210 92.16 90.25 90.25 84.64 72.25 96.04 51.330 72.25 86.49 98.01 79.21 96.04 94.09 51.450 96.04 79.21 73.96 79.21 92.16 75.69 51.570 79.21 79.21 86.49 79.21 72.25 88.36 51.690 79.21 72.25 88.36 94.09 81.00 82.81 51.810 94.09 82.81 65.61 82.81 77.44 81.00 51.930 67.24 92.16 86.49 102.01 77.44 75.69 52.050 90.25 79.21 82.81 90.25 84.64 96.04 52.170 79.21 73.96 88.36 84.64 75.69 92.16 52.290 82.81 86.49 79.21 84.64 96.04 98.01 52.410 94.09 79.21 86.49 96.04 100.00 96.04 52.530 114.49 88.36 92.16 110.25 92.16 84.64 52.650 98.01 106.09 90.25 106.09 88.36 98.01 52.770 98.01 121.00 100.00 125.44 125.44 141.61 52.890 104.04 114.49 132.25 104.04 125.44 110.25 53.010 108.16 141.61 132.25 114.49 141.61 158.76 53.130 146.41 141.61 146.41 144.00 129.96 148.84 53.250 134.56 139.24 153.76 134.56 161.29 139.24 53.370 174.24 158.76 156.25 179.56 146.41 141.61 53.490 174.24 161.29 139.24 163.84 146.41 146.41 53.610 161.29 151.29 148.84 158.76 158.76 156.25 53.730 141.61 158.76 141.61 158.76 136.89 132.25 53.850 123.21 136.89 158.76 161.29 163.84 148.84 53.970 151.29 161.29 125.44 151.29 141.61 151.29 54.090 127.69 146.41 141.61 127.69 158.76 129.96 54.210 141.61 151.29 151.29 151.29 141.61 136.89 54.330 144.00 136.89 148.84 121.00 134.56 127.69 54.450 141.61 139.24 136.89 151.29 136.89 136.89 54.570 148.84 112.36 125.44 148.84 118.81 114.49 54.690 148.84 141.61 121.00 132.25 100.00 136.89 54.810 144.00 127.69 163.84 123.21 141.61 132.25 54.930 121.00 121.00 123.21 139.24 136.89 121.00 55.050 125.44 114.49 121.00 114.49 118.81 102.01 55.170 104.04 110.25 104.04 116.64 110.25 112.36

109

File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 129.96 123.21 123.21 104.04 102.01 125.44 55.410 112.36 100.00 104.04 129.96 110.25 108.16 55.530 96.04 102.01 110.25 106.09 108.16 92.16 55.650 118.81 100.00 121.00 98.01 114.49 98.01 55.770 110.25 98.01 100.00 116.64 110.25 92.16 55.890 116.64 98.01 102.01 96.04 96.04 81.00 56.010 88.36 106.09 112.36 90.25 90.25 96.04 56.130 102.01 108.16 112.36 92.16 100.00 84.64 56.250 94.09 110.25 110.25 98.01 114.49 86.49 56.370 94.09 88.36 86.49 100.00 88.36 92.16 56.490 75.69 88.36 86.49 98.01 96.04 96.04 56.610 110.25 106.09 92.16 88.36 102.01 108.16 56.730 106.09 96.04 90.25 90.25 102.01 84.64 56.850 92.16 82.81 102.01 96.04 106.09 96.04 56.970 90.25 90.25 90.25 98.01 86.49 82.81 57.090 81.00 84.64 98.01 94.09 84.64 102.01 57.210 104.04 116.64 100.00 100.00 104.04 84.64 57.330 121.00 88.36 79.21 100.00 104.04 108.16 57.450 84.64 110.25 94.09 108.16 108.16 94.09 57.570 86.49 94.09 110.25 110.25 106.09 90.25 57.690 102.01 104.04 114.49 106.09 94.09 102.01 57.810 92.16 72.25 82.81 108.16 100.00 100.00 57.930 106.09 84.64 90.25 96.04 112.36 116.64 58.050 96.04 100.00 90.25 96.04 86.49 102.01 58.170 88.36 94.09 100.00 106.09 88.36 79.21 58.290 98.01 112.36 92.16 98.01 94.09 86.49 58.410 92.16 84.64 118.81 106.09 88.36 98.01 58.530 118.81 108.16 106.09 98.01 96.04 114.49 58.650 88.36 108.16 96.04 100.00 110.25 104.04 58.770 116.64 110.25 110.25 121.00 110.25 98.01 58.890 102.01 108.16 90.25 104.04 125.44 106.09 59.010 108.16 116.64 134.56 123.21 110.25 132.25 59.130 121.00 114.49 116.64 112.36 125.44 123.21 59.250 114.49 127.69 136.89 125.44 139.24 129.96 59.370 100.00 132.25 98.01 129.96 129.96 136.89 59.490 116.64 114.49 118.81 121.00 116.64 121.00 59.610 127.69 136.89 108.16 123.21 123.21 100.00 59.730 121.00 125.44 127.69 127.69 110.25 139.24 59.850 161.29 169.00 132.25 144.00 136.89 106.09 59.970 112.36 102.01 125.44 141.61 129.96 127.69 60.090 121.00 104.04 108.16 106.09 106.09 86.49 60.210 96.04 98.01 104.04 116.64 100.00 79.21 60.330 96.04 84.64 96.04 94.09 88.36 94.09 60.450 94.09 92.16 96.04 88.36 94.09 90.25 60.570 88.36 92.16 90.25 114.49 106.09 108.16 60.690 98.01 108.16 104.04 88.36 108.16 88.36 60.810 118.81 102.01 102.01 116.64 90.25 108.16 60.930 129.96 106.09 114.49 90.25 102.01 110.25 61.050 123.21 108.16 116.64 123.21 112.36 118.81 61.170 121.00 118.81 139.24 106.09 102.01 125.44 61.290 129.96 121.00 121.00 116.64 121.00 141.61 61.410 136.89 125.44 112.36 125.44 151.29 158.76

110

File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 146.41 134.56 134.56 139.24 144.00 139.24 61.650 134.56 148.84 161.29 163.84 163.84 153.76 61.770 129.96 158.76 156.25 146.41 132.25 144.00 61.890 174.24 161.29 166.41 158.76 153.76 148.84 62.010 151.29 169.00 158.76 144.00 153.76 171.61 62.130 169.00 176.89 148.84 166.41 161.29 179.56 62.250 182.25 125.44 163.84 163.84 153.76 158.76 62.370 166.41 169.00 169.00 174.24 151.29 169.00 62.490 158.76 176.89 196.00 179.56 196.00 174.24 62.610 169.00 166.41 163.84 148.84 163.84 156.25 62.730 158.76 171.61 169.00 166.41 163.84 151.29 62.850 148.84 146.41 144.00 144.00 158.76 156.25 62.970 148.84 158.76 153.76 156.25 158.76 158.76 63.090 132.25 161.29 148.84 141.61 148.84 141.61 63.210 156.25 129.96 136.89 158.76 148.84 146.41 63.330 134.56 129.96 129.96 148.84 148.84 132.25 63.450 148.84 148.84 134.56 110.25 146.41 125.44 63.570 129.96 114.49 127.69 136.89 123.21 139.24 63.690 125.44 127.69 141.61 118.81 136.89 121.00 63.810 123.21 123.21 129.96 151.29 144.00 146.41 63.930 134.56 136.89 127.69 134.56 134.56 123.21 64.050 141.61 106.09 146.41 127.69 144.00 141.61 64.170 121.00 127.69 121.00 127.69 125.44 123.21 64.290 123.21 125.44 114.49 125.44 112.36 121.00 64.410 112.36 127.69 121.00 129.96 102.01 116.64 64.530 121.00 125.44 121.00 123.21 102.01 100.00 64.650 92.16 121.00 121.00 96.04 92.16 114.49 64.770 108.16 104.04 77.44 114.49 94.09 108.16 64.890 94.09 106.09 104.04 90.25 92.16 84.64 65.010 92.16 98.01 92.16 90.25 96.04 104.04 65.130 82.81 90.25 92.16 106.09 106.09 94.09 65.250 96.04 77.44 84.64 100.00 104.04 98.01 65.370 102.01 92.16 82.81 90.25 104.04 86.49 65.490 92.16 94.09 79.21 98.01 86.49 96.04 65.610 94.09 100.00 100.00 98.01 112.36 121.00 65.730 104.04 116.64 104.04 79.21 96.04 86.49 65.850 92.16 110.25 102.01 96.04 104.04 92.16 65.970 90.25 84.64 92.16 92.16 94.09 110.25 66.090 94.09 108.16 108.16 114.49 104.04 82.81 66.210 108.16 94.09 104.04 92.16 84.64 98.01 66.330 79.21 98.01 102.01 88.36 92.16 100.00 66.450 102.01 86.49 88.36 94.09 100.00 82.81 66.570 98.01 94.09 86.49 86.49 98.01 77.44 66.690 88.36 94.09 100.00 88.36 82.81 77.44 66.810 86.49 94.09 96.04 77.44 106.09 90.25 66.930 98.01 100.00 112.36 81.00 88.36 102.01 67.050 100.00 82.81 86.49 88.36 94.09 84.64 67.170 72.25 98.01 86.49 96.04 90.25 102.01 67.290 106.09 104.04 92.16 90.25 90.25 82.81 67.410 86.49 92.16 84.64 81.00 90.25 90.25 67.530 88.36 86.49 104.04 92.16 102.01 100.00 67.650 100.00 104.04 102.01 92.16 100.00 100.00

111

File: JC2.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 77.44 96.04 100.00 106.09 92.16 121.00 67.890 108.16 98.01 104.04 114.49 98.01 112.36 68.010 102.01 94.09 116.64 123.21 134.56 104.04 68.130 110.25 88.36 108.16 92.16 116.64 106.09 68.250 134.56 129.96 110.25 102.01 94.09 88.36 68.370 100.00 100.00 102.01 106.09 108.16 98.01 68.490 88.36 81.00 100.00 90.25 94.09 102.01 68.610 79.21 114.49 102.01 102.01 108.16 84.64 68.730 100.00 102.01 106.09 100.00 92.16 100.00 68.850 102.01 104.04 110.25 96.04 88.36 100.00 68.970 96.04 96.04 108.16 86.49 90.25 90.25 69.090 86.49 96.04 92.16 96.04 86.49 90.25 69.210 82.81 98.01 98.01 84.64 81.00 92.16 69.330 106.09 96.04 96.04 100.00 88.36 96.04 69.450 108.16 106.09 106.09 114.49 114.49 112.36 69.570 96.04 92.16 86.49 94.09 94.09 88.36 69.690 96.04 82.81 100.00 92.16 96.04 90.25 69.810 94.09 98.01 96.04 88.36 94.09 77.44 69.930 92.16 86.49 86.49 84.64 _

112

File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC3 Data measured at: 24-Jan-2011 13:01:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 772.8400 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 750.76 686.44 691.69 650.25 590.49 620.01 2.130 610.09 635.04 566.44 605.16 561.69 533.61 2.250 524.41 529.00 533.61 519.84 519.84 470.89 2.370 488.41 492.84 420.25 453.69 445.21 445.21 2.490 441.00 424.36 424.36 396.01 404.01 400.00 2.610 392.04 364.81 396.01 368.64 349.69 349.69 2.730 396.01 357.21 342.25 342.25 345.96 342.25 2.850 316.84 349.69 338.56 327.61 316.84 316.84 2.970 302.76 313.29 292.41 302.76 292.41 306.25 3.090 268.96 289.00 282.24 285.61 275.56 262.44 3.210 275.56 262.44 259.21 262.44 256.00 282.24 3.330 265.69 246.49 240.25 243.36 249.64 231.04 3.450 246.49 228.01 240.25 240.25 225.00 228.01 3.570 225.00 234.09 231.04 176.89 204.49 207.36 3.690 237.16 222.01 228.01 190.44 196.00 204.49 3.810 210.25 213.16 163.84 190.44 222.01 198.81 3.930 198.81 182.25 201.64 171.61 201.64 182.25 4.050 182.25 179.56 190.44 187.69 176.89 176.89 4.170 182.25 198.81 163.84 187.69 156.25 182.25 4.290 176.89 161.29 184.96 169.00 141.61 201.64 4.410 196.00 169.00 144.00 184.96 166.41 161.29 4.530 179.56 187.69 163.84 174.24 146.41 163.84 4.650 163.84 144.00 158.76 144.00 161.29 174.24 4.770 166.41 144.00 148.84 141.61 144.00 136.89 4.890 153.76 116.64 166.41 141.61 153.76 161.29 5.010 132.25 129.96 141.61 139.24 169.00 144.00 5.130 158.76 129.96 153.76 139.24 156.25 148.84 5.250 156.25 141.61 153.76 136.89 158.76 129.96

113

File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 134.56 121.00 151.29 121.00 146.41 169.00 5.490 148.84 134.56 144.00 136.89 123.21 121.00 5.610 141.61 141.61 141.61 141.61 136.89 127.69 5.730 141.61 136.89 127.69 144.00 141.61 141.61 5.850 134.56 136.89 104.04 121.00 121.00 118.81 5.970 136.89 114.49 129.96 116.64 121.00 136.89 6.090 144.00 134.56 123.21 114.49 121.00 129.96 6.210 127.69 129.96 116.64 136.89 141.61 134.56 6.330 123.21 141.61 116.64 108.16 121.00 134.56 6.450 129.96 123.21 118.81 123.21 148.84 127.69 6.570 125.44 121.00 121.00 121.00 108.16 114.49 6.690 102.01 104.04 114.49 121.00 121.00 112.36 6.810 118.81 88.36 121.00 90.25 116.64 104.04 6.930 116.64 114.49 110.25 106.09 129.96 125.44 7.050 129.96 112.36 102.01 108.16 116.64 114.49 7.170 96.04 100.00 110.25 110.25 129.96 112.36 7.290 110.25 86.49 112.36 84.64 104.04 100.00 7.410 118.81 98.01 116.64 110.25 106.09 127.69 7.530 108.16 106.09 98.01 102.01 112.36 100.00 7.650 118.81 98.01 114.49 94.09 82.81 118.81 7.770 106.09 134.56 98.01 121.00 116.64 114.49 7.890 106.09 108.16 102.01 84.64 102.01 116.64 8.010 112.36 118.81 98.01 116.64 84.64 125.44 8.130 92.16 92.16 102.01 104.04 112.36 106.09 8.250 116.64 112.36 100.00 100.00 94.09 110.25 8.370 108.16 98.01 112.36 104.04 123.21 100.00 8.490 92.16 114.49 102.01 108.16 123.21 94.09 8.610 116.64 104.04 110.25 98.01 110.25 98.01 8.730 104.04 102.01 100.00 104.04 110.25 116.64 8.850 112.36 121.00 121.00 92.16 94.09 98.01 8.970 100.00 98.01 100.00 106.09 100.00 102.01 9.090 104.04 84.64 81.00 96.04 77.44 112.36 9.210 114.49 114.49 92.16 92.16 110.25 100.00 9.330 100.00 92.16 100.00 98.01 123.21 106.09 9.450 110.25 90.25 114.49 98.01 94.09 114.49 9.570 98.01 108.16 88.36 127.69 106.09 104.04 9.690 104.04 86.49 104.04 110.25 123.21 112.36 9.810 123.21 108.16 98.01 104.04 100.00 118.81 9.930 118.81 108.16 100.00 96.04 125.44 94.09 10.050 106.09 134.56 141.61 114.49 98.01 123.21 10.170 127.69 92.16 106.09 110.25 114.49 100.00 10.290 121.00 100.00 112.36 121.00 116.64 136.89 10.410 106.09 132.25 123.21 116.64 118.81 129.96 10.530 118.81 116.64 123.21 121.00 132.25 132.25 10.650 118.81 125.44 127.69 139.24 134.56 114.49 10.770 134.56 139.24 141.61 139.24 148.84 134.56 10.890 132.25 151.29 141.61 153.76 132.25 153.76 11.010 158.76 153.76 153.76 163.84 163.84 182.25 11.130 158.76 182.25 198.81 148.84 184.96 166.41 11.250 196.00 163.84 179.56 176.89 231.04 182.25 11.370 210.25 210.25 246.49 225.00 243.36 228.01 11.490 231.04 213.16 246.49 231.04 237.16 268.96

114

File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 240.25 282.24 246.49 306.25 295.84 309.76 11.730 275.56 302.76 302.76 309.76 292.41 327.61 11.850 313.29 320.41 309.76 262.44 282.24 353.44 11.970 334.89 275.56 268.96 278.89 299.29 265.69 12.090 256.00 275.56 252.81 243.36 240.25 216.09 12.210 231.04 196.00 198.81 187.69 184.96 182.25 12.330 198.81 161.29 158.76 158.76 148.84 134.56 12.450 132.25 146.41 125.44 146.41 125.44 110.25 12.570 121.00 112.36 106.09 108.16 88.36 96.04 12.690 121.00 100.00 102.01 114.49 86.49 79.21 12.810 94.09 102.01 94.09 94.09 102.01 110.25 12.930 70.56 102.01 94.09 94.09 81.00 84.64 13.050 84.64 72.25 84.64 86.49 86.49 96.04 13.170 82.81 77.44 70.56 86.49 86.49 77.44 13.290 65.61 54.76 75.69 79.21 68.89 68.89 13.410 75.69 65.61 62.41 75.69 70.56 65.61 13.530 72.25 75.69 77.44 86.49 73.96 62.41 13.650 79.21 79.21 59.29 72.25 73.96 82.81 13.770 65.61 75.69 70.56 64.00 57.76 59.29 13.890 65.61 67.24 64.00 72.25 75.69 65.61 14.010 72.25 57.76 84.64 47.61 67.24 59.29 14.130 67.24 72.25 53.29 75.69 62.41 60.84 14.250 60.84 72.25 77.44 67.24 49.00 62.41 14.370 65.61 67.24 56.25 65.61 56.25 59.29 14.490 53.29 53.29 65.61 67.24 59.29 60.84 14.610 54.76 65.61 56.25 59.29 65.61 49.00 14.730 70.56 59.29 47.61 47.61 65.61 53.29 14.850 82.81 56.25 56.25 72.25 57.76 54.76 14.970 59.29 67.24 53.29 60.84 59.29 43.56 15.090 70.56 51.84 57.76 73.96 73.96 51.84 15.210 60.84 53.29 56.25 65.61 59.29 46.24 15.330 67.24 65.61 68.89 47.61 57.76 38.44 15.450 64.00 57.76 51.84 67.24 56.25 54.76 15.570 73.96 47.61 47.61 56.25 59.29 46.24 15.690 65.61 59.29 67.24 44.89 70.56 65.61 15.810 59.29 56.25 67.24 51.84 49.00 72.25 15.930 72.25 53.29 53.29 50.41 53.29 56.25 16.050 47.61 47.61 56.25 64.00 62.41 72.25 16.170 49.00 64.00 64.00 60.84 40.96 47.61 16.290 49.00 65.61 57.76 47.61 53.29 54.76 16.410 70.56 46.24 51.84 59.29 54.76 56.25 16.530 62.41 65.61 59.29 50.41 65.61 64.00 16.650 57.76 60.84 65.61 54.76 64.00 65.61 16.770 47.61 59.29 50.41 68.89 47.61 56.25 16.890 64.00 59.29 56.25 56.25 50.41 51.84 17.010 62.41 70.56 56.25 62.41 53.29 62.41 17.130 75.69 59.29 64.00 65.61 68.89 70.56 17.250 56.25 67.24 59.29 56.25 67.24 73.96 17.370 57.76 68.89 53.29 60.84 59.29 75.69 17.490 62.41 67.24 65.61 57.76 64.00 53.29 17.610 60.84 67.24 75.69 75.69 70.56 65.61 17.730 67.24 67.24 56.25 72.25 79.21 70.56

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File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 70.56 82.81 65.61 49.00 75.69 75.69 17.970 62.41 62.41 92.16 82.81 72.25 72.25 18.090 84.64 65.61 79.21 67.24 84.64 70.56 18.210 59.29 79.21 62.41 73.96 77.44 79.21 18.330 65.61 70.56 62.41 68.89 79.21 50.41 18.450 72.25 75.69 67.24 88.36 84.64 77.44 18.570 82.81 81.00 62.41 79.21 88.36 72.25 18.690 60.84 67.24 72.25 84.64 77.44 70.56 18.810 86.49 96.04 96.04 86.49 90.25 75.69 18.930 92.16 86.49 86.49 62.41 86.49 79.21 19.050 96.04 77.44 79.21 86.49 100.00 92.16 19.170 112.36 116.64 100.00 81.00 100.00 96.04 19.290 121.00 112.36 121.00 118.81 118.81 125.44 19.410 112.36 134.56 129.96 144.00 146.41 136.89 19.530 169.00 190.44 196.00 184.96 210.25 228.01 19.650 204.49 243.36 256.00 265.69 313.29 349.69 19.770 364.81 408.04 396.01 420.25 475.24 470.89 19.890 547.56 538.24 529.00 510.76 510.76 561.69 20.010 533.61 510.76 519.84 519.84 492.84 488.41 20.130 462.25 501.76 420.25 416.16 466.56 396.01 20.250 400.00 424.36 368.64 404.01 396.01 396.01 20.370 376.36 357.21 342.25 357.21 376.36 316.84 20.490 338.56 316.84 324.00 324.00 324.00 309.76 20.610 316.84 313.29 316.84 299.29 320.41 302.76 20.730 331.24 412.09 475.24 488.41 501.76 445.21 20.850 424.36 384.16 384.16 313.29 324.00 265.69 20.970 289.00 252.81 262.44 292.41 252.81 285.61 21.090 262.44 265.69 246.49 249.64 237.16 237.16 21.210 262.44 240.25 216.09 256.00 262.44 228.01 21.330 196.00 256.00 246.49 231.04 201.64 240.25 21.450 237.16 237.16 193.21 216.09 231.04 210.25 21.570 213.16 216.09 231.04 204.49 225.00 187.69 21.690 210.25 222.01 213.16 190.44 225.00 176.89 21.810 204.49 201.64 213.16 196.00 204.49 216.09 21.930 196.00 213.16 184.96 216.09 196.00 198.81 22.050 193.21 201.64 198.81 213.16 196.00 190.44 22.170 196.00 174.24 201.64 222.01 219.04 207.36 22.290 174.24 196.00 193.21 190.44 198.81 196.00 22.410 196.00 184.96 193.21 187.69 184.96 174.24 22.530 201.64 198.81 219.04 166.41 196.00 184.96 22.650 207.36 179.56 190.44 176.89 179.56 222.01 22.770 182.25 182.25 201.64 190.44 213.16 182.25 22.890 198.81 196.00 240.25 207.36 198.81 196.00 23.010 225.00 204.49 198.81 222.01 222.01 207.36 23.130 219.04 171.61 204.49 198.81 198.81 201.64 23.250 234.09 213.16 234.09 210.25 198.81 187.69 23.370 210.25 219.04 219.04 225.00 210.25 234.09 23.490 240.25 219.04 204.49 231.04 234.09 243.36 23.610 259.21 222.01 234.09 240.25 237.16 268.96 23.730 228.01 249.64 268.96 256.00 243.36 278.89 23.850 275.56 289.00 282.24 306.25 256.00 302.76 23.970 275.56 285.61 292.41 289.00 342.25 309.76

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File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 376.36 338.56 292.41 309.76 306.25 320.41 24.210 331.24 324.00 353.44 342.25 324.00 342.25 24.330 342.25 353.44 331.24 349.69 345.96 345.96 24.450 361.00 331.24 364.81 334.89 327.61 384.16 24.570 302.76 380.25 306.25 324.00 361.00 331.24 24.690 338.56 289.00 342.25 285.61 320.41 285.61 24.810 338.56 278.89 299.29 289.00 265.69 278.89 24.930 252.81 256.00 285.61 268.96 285.61 256.00 25.050 243.36 268.96 237.16 234.09 256.00 225.00 25.170 237.16 234.09 249.64 219.04 213.16 240.25 25.290 213.16 237.16 231.04 201.64 210.25 219.04 25.410 216.09 216.09 201.64 240.25 184.96 198.81 25.530 193.21 198.81 193.21 222.01 210.25 187.69 25.650 187.69 193.21 190.44 193.21 213.16 196.00 25.770 196.00 187.69 163.84 166.41 179.56 182.25 25.890 174.24 153.76 171.61 196.00 187.69 176.89 26.010 169.00 187.69 210.25 179.56 169.00 190.44 26.130 204.49 193.21 158.76 174.24 204.49 163.84 26.250 156.25 187.69 196.00 179.56 176.89 198.81 26.370 207.36 213.16 190.44 231.04 275.56 259.21 26.490 349.69 479.61 585.64 660.49 723.61 772.84 26.610 734.41 772.84 625.00 492.84 408.04 327.61 26.730 246.49 184.96 196.00 196.00 176.89 207.36 26.850 201.64 193.21 187.69 166.41 163.84 193.21 26.970 161.29 141.61 169.00 182.25 151.29 161.29 27.090 161.29 132.25 163.84 148.84 153.76 176.89 27.210 166.41 174.24 132.25 136.89 148.84 153.76 27.330 161.29 144.00 139.24 161.29 146.41 132.25 27.450 153.76 144.00 144.00 136.89 144.00 169.00 27.570 151.29 163.84 146.41 134.56 125.44 141.61 27.690 144.00 144.00 144.00 156.25 153.76 136.89 27.810 156.25 127.69 136.89 148.84 136.89 132.25 27.930 134.56 158.76 132.25 132.25 136.89 141.61 28.050 127.69 151.29 141.61 158.76 144.00 136.89 28.170 153.76 144.00 123.21 139.24 148.84 121.00 28.290 125.44 127.69 127.69 141.61 132.25 144.00 28.410 153.76 148.84 118.81 139.24 116.64 134.56 28.530 146.41 129.96 132.25 118.81 129.96 134.56 28.650 129.96 127.69 125.44 121.00 136.89 132.25 28.770 132.25 121.00 116.64 121.00 134.56 106.09 28.890 114.49 136.89 125.44 116.64 121.00 112.36 29.010 134.56 112.36 112.36 108.16 132.25 125.44 29.130 148.84 118.81 134.56 123.21 108.16 102.01 29.250 118.81 110.25 116.64 114.49 121.00 125.44 29.370 144.00 127.69 110.25 110.25 127.69 134.56 29.490 114.49 121.00 108.16 134.56 118.81 118.81 29.610 108.16 110.25 110.25 132.25 110.25 121.00 29.730 121.00 125.44 123.21 118.81 118.81 123.21 29.850 123.21 108.16 144.00 125.44 102.01 118.81 29.970 118.81 118.81 121.00 100.00 102.01 129.96 30.090 110.25 129.96 100.00 123.21 104.04 104.04 30.210 116.64 112.36 118.81 136.89 92.16 123.21

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File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 125.44 104.04 123.21 94.09 118.81 94.09 30.450 118.81 125.44 116.64 112.36 108.16 104.04 30.570 110.25 112.36 125.44 108.16 110.25 112.36 30.690 116.64 118.81 100.00 121.00 108.16 116.64 30.810 100.00 106.09 144.00 121.00 114.49 134.56 30.930 116.64 116.64 104.04 129.96 123.21 123.21 31.050 98.01 118.81 108.16 106.09 110.25 96.04 31.170 104.04 132.25 121.00 102.01 81.00 98.01 31.290 98.01 112.36 106.09 112.36 100.00 118.81 31.410 123.21 114.49 110.25 92.16 114.49 90.25 31.530 96.04 104.04 108.16 112.36 100.00 118.81 31.650 98.01 118.81 100.00 92.16 110.25 108.16 31.770 114.49 112.36 98.01 112.36 106.09 75.69 31.890 98.01 98.01 106.09 106.09 108.16 100.00 32.010 108.16 96.04 106.09 108.16 86.49 110.25 32.130 98.01 96.04 100.00 104.04 82.81 79.21 32.250 86.49 116.64 110.25 102.01 96.04 67.24 32.370 106.09 110.25 90.25 90.25 86.49 104.04 32.490 92.16 98.01 94.09 100.00 86.49 90.25 32.610 90.25 98.01 94.09 84.64 108.16 88.36 32.730 84.64 108.16 84.64 94.09 75.69 106.09 32.850 98.01 96.04 106.09 90.25 90.25 98.01 32.970 86.49 100.00 96.04 98.01 81.00 98.01 33.090 114.49 108.16 96.04 118.81 116.64 106.09 33.210 110.25 96.04 98.01 100.00 106.09 116.64 33.330 90.25 110.25 100.00 106.09 114.49 94.09 33.450 96.04 96.04 96.04 98.01 108.16 110.25 33.570 100.00 98.01 98.01 98.01 94.09 110.25 33.690 90.25 104.04 94.09 96.04 104.04 110.25 33.810 106.09 96.04 96.04 112.36 112.36 102.01 33.930 96.04 116.64 116.64 110.25 110.25 116.64 34.050 114.49 94.09 114.49 112.36 118.81 123.21 34.170 110.25 123.21 139.24 125.44 127.69 134.56 34.290 153.76 153.76 121.00 132.25 156.25 148.84 34.410 148.84 148.84 166.41 169.00 153.76 176.89 34.530 163.84 169.00 166.41 201.64 182.25 213.16 34.650 182.25 222.01 219.04 252.81 246.49 246.49 34.770 243.36 265.69 240.25 256.00 259.21 272.25 34.890 289.00 246.49 302.76 268.96 285.61 285.61 35.010 282.24 256.00 275.56 289.00 268.96 299.29 35.130 272.25 299.29 295.84 299.29 285.61 282.24 35.250 313.29 249.64 259.21 256.00 262.44 249.64 35.370 246.49 259.21 243.36 268.96 278.89 259.21 35.490 252.81 252.81 249.64 249.64 249.64 275.56 35.610 272.25 262.44 262.44 246.49 234.09 285.61 35.730 282.24 275.56 289.00 265.69 292.41 292.41 35.850 272.25 295.84 262.44 309.76 289.00 262.44 35.970 256.00 285.61 275.56 292.41 313.29 295.84 36.090 302.76 289.00 285.61 306.25 299.29 285.61 36.210 299.29 316.84 252.81 289.00 282.24 292.41 36.330 299.29 302.76 327.61 302.76 349.69 327.61 36.450 342.25 376.36 404.01 388.09 392.04 372.49

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File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 349.69 353.44 376.36 349.69 331.24 364.81 36.690 324.00 316.84 342.25 338.56 313.29 368.64 36.810 306.25 334.89 380.25 364.81 313.29 327.61 36.930 338.56 306.25 368.64 357.21 364.81 380.25 37.050 345.96 392.04 327.61 334.89 299.29 331.24 37.170 342.25 320.41 327.61 331.24 342.25 327.61 37.290 320.41 338.56 334.89 306.25 313.29 316.84 37.410 357.21 316.84 327.61 324.00 334.89 327.61 37.530 289.00 306.25 299.29 316.84 306.25 327.61 37.650 285.61 285.61 342.25 320.41 334.89 282.24 37.770 334.89 299.29 285.61 289.00 327.61 292.41 37.890 295.84 278.89 309.76 309.76 342.25 316.84 38.010 334.89 302.76 282.24 268.96 331.24 268.96 38.130 292.41 282.24 262.44 302.76 249.64 275.56 38.250 275.56 299.29 292.41 259.21 265.69 285.61 38.370 268.96 292.41 256.00 246.49 265.69 262.44 38.490 275.56 246.49 265.69 282.24 278.89 272.25 38.610 252.81 289.00 246.49 268.96 259.21 256.00 38.730 282.24 246.49 225.00 240.25 262.44 259.21 38.850 246.49 243.36 249.64 262.44 249.64 228.01 38.970 249.64 256.00 231.04 240.25 243.36 272.25 39.090 237.16 256.00 225.00 256.00 272.25 225.00 39.210 262.44 275.56 262.44 246.49 275.56 249.64 39.330 237.16 249.64 302.76 278.89 295.84 327.61 39.450 289.00 289.00 285.61 289.00 272.25 262.44 39.570 295.84 285.61 249.64 282.24 285.61 282.24 39.690 252.81 299.29 265.69 295.84 256.00 272.25 39.810 282.24 278.89 292.41 299.29 289.00 262.44 39.930 320.41 259.21 234.09 243.36 282.24 252.81 40.050 265.69 249.64 237.16 249.64 256.00 201.64 40.170 246.49 262.44 240.25 243.36 246.49 234.09 40.290 213.16 222.01 237.16 228.01 210.25 207.36 40.410 222.01 213.16 196.00 225.00 210.25 196.00 40.530 176.89 198.81 225.00 207.36 187.69 207.36 40.650 166.41 201.64 216.09 174.24 182.25 182.25 40.770 184.96 184.96 216.09 174.24 153.76 184.96 40.890 193.21 184.96 179.56 190.44 161.29 184.96 41.010 163.84 174.24 158.76 190.44 176.89 179.56 41.130 161.29 225.00 216.09 198.81 187.69 204.49 41.250 187.69 184.96 196.00 182.25 193.21 184.96 41.370 176.89 179.56 213.16 187.69 169.00 179.56 41.490 161.29 176.89 174.24 179.56 134.56 169.00 41.610 169.00 169.00 166.41 176.89 171.61 179.56 41.730 176.89 161.29 163.84 163.84 201.64 161.29 41.850 153.76 174.24 156.25 166.41 169.00 136.89 41.970 158.76 187.69 166.41 174.24 156.25 176.89 42.090 174.24 158.76 179.56 169.00 182.25 158.76 42.210 148.84 153.76 187.69 151.29 193.21 204.49 42.330 198.81 187.69 207.36 207.36 184.96 198.81 42.450 204.49 196.00 187.69 196.00 179.56 174.24 42.570 179.56 184.96 169.00 187.69 158.76 156.25 42.690 163.84 151.29 176.89 151.29 144.00 161.29

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File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 136.89 153.76 136.89 169.00 163.84 161.29 42.930 148.84 139.24 166.41 156.25 163.84 179.56 43.050 153.76 169.00 163.84 166.41 166.41 148.84 43.170 163.84 148.84 161.29 187.69 174.24 161.29 43.290 144.00 174.24 151.29 169.00 158.76 161.29 43.410 174.24 148.84 187.69 169.00 153.76 166.41 43.530 156.25 156.25 161.29 151.29 158.76 161.29 43.650 144.00 139.24 144.00 144.00 156.25 151.29 43.770 171.61 166.41 179.56 139.24 153.76 158.76 43.890 153.76 139.24 146.41 166.41 123.21 139.24 44.010 127.69 190.44 176.89 163.84 141.61 141.61 44.130 153.76 171.61 158.76 144.00 182.25 158.76 44.250 184.96 132.25 163.84 144.00 156.25 163.84 44.370 151.29 161.29 156.25 148.84 161.29 182.25 44.490 161.29 161.29 129.96 174.24 136.89 136.89 44.610 156.25 139.24 153.76 161.29 158.76 146.41 44.730 156.25 146.41 163.84 158.76 141.61 148.84 44.850 148.84 139.24 158.76 144.00 151.29 171.61 44.970 144.00 174.24 136.89 146.41 141.61 158.76 45.090 171.61 141.61 144.00 156.25 136.89 153.76 45.210 158.76 166.41 161.29 148.84 136.89 148.84 45.330 139.24 166.41 139.24 156.25 153.76 163.84 45.450 187.69 158.76 144.00 148.84 163.84 148.84 45.570 148.84 161.29 136.89 153.76 158.76 176.89 45.690 171.61 187.69 207.36 187.69 187.69 184.96 45.810 158.76 151.29 148.84 163.84 174.24 158.76 45.930 169.00 118.81 158.76 166.41 134.56 136.89 46.050 141.61 121.00 144.00 136.89 148.84 146.41 46.170 176.89 153.76 136.89 148.84 146.41 153.76 46.290 134.56 136.89 151.29 144.00 163.84 151.29 46.410 136.89 148.84 148.84 148.84 158.76 156.25 46.530 134.56 179.56 163.84 153.76 158.76 153.76 46.650 136.89 174.24 139.24 136.89 151.29 136.89 46.770 136.89 158.76 163.84 136.89 163.84 129.96 46.890 148.84 144.00 163.84 146.41 134.56 148.84 47.010 139.24 144.00 127.69 139.24 132.25 118.81 47.130 121.00 127.69 136.89 139.24 141.61 121.00 47.250 125.44 153.76 146.41 118.81 112.36 136.89 47.370 129.96 118.81 102.01 136.89 125.44 125.44 47.490 139.24 151.29 146.41 108.16 169.00 141.61 47.610 121.00 146.41 121.00 125.44 121.00 118.81 47.730 136.89 146.41 141.61 129.96 127.69 146.41 47.850 129.96 134.56 127.69 125.44 163.84 121.00 47.970 114.49 161.29 148.84 127.69 127.69 136.89 48.090 125.44 134.56 132.25 139.24 141.61 129.96 48.210 144.00 132.25 121.00 129.96 125.44 148.84 48.330 112.36 125.44 127.69 139.24 123.21 132.25 48.450 132.25 121.00 129.96 144.00 123.21 118.81 48.570 139.24 127.69 121.00 118.81 144.00 114.49 48.690 153.76 136.89 134.56 123.21 127.69 148.84 48.810 156.25 153.76 121.00 146.41 153.76 132.25 48.930 151.29 121.00 125.44 125.44 136.89 114.49

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File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 134.56 121.00 161.29 156.25 136.89 166.41 49.170 153.76 148.84 136.89 136.89 132.25 141.61 49.290 139.24 125.44 151.29 125.44 141.61 146.41 49.410 141.61 141.61 134.56 136.89 151.29 110.25 49.530 163.84 136.89 125.44 136.89 148.84 136.89 49.650 139.24 108.16 134.56 141.61 136.89 146.41 49.770 134.56 129.96 144.00 153.76 151.29 158.76 49.890 141.61 163.84 169.00 163.84 184.96 169.00 50.010 225.00 207.36 216.09 213.16 246.49 222.01 50.130 228.01 237.16 198.81 184.96 204.49 198.81 50.250 184.96 166.41 174.24 174.24 146.41 129.96 50.370 176.89 144.00 156.25 153.76 171.61 151.29 50.490 134.56 158.76 158.76 148.84 153.76 129.96 50.610 125.44 141.61 153.76 148.84 146.41 158.76 50.730 136.89 110.25 144.00 125.44 146.41 125.44 50.850 134.56 136.89 141.61 132.25 156.25 129.96 50.970 153.76 123.21 134.56 114.49 127.69 118.81 51.090 121.00 141.61 127.69 148.84 129.96 127.69 51.210 144.00 141.61 121.00 132.25 123.21 121.00 51.330 151.29 156.25 144.00 134.56 136.89 123.21 51.450 123.21 151.29 144.00 121.00 148.84 156.25 51.570 132.25 134.56 132.25 123.21 132.25 125.44 51.690 114.49 139.24 127.69 125.44 139.24 139.24 51.810 141.61 121.00 121.00 141.61 123.21 141.61 51.930 146.41 139.24 129.96 148.84 134.56 134.56 52.050 148.84 129.96 114.49 139.24 153.76 134.56 52.170 148.84 134.56 136.89 148.84 116.64 127.69 52.290 148.84 132.25 148.84 118.81 136.89 125.44 52.410 121.00 121.00 121.00 108.16 169.00 121.00 52.530 139.24 146.41 144.00 156.25 141.61 132.25 52.650 144.00 114.49 146.41 127.69 136.89 158.76 52.770 166.41 139.24 136.89 127.69 127.69 125.44 52.890 129.96 121.00 148.84 132.25 146.41 151.29 53.010 139.24 144.00 136.89 158.76 153.76 136.89 53.130 151.29 141.61 151.29 166.41 129.96 169.00 53.250 129.96 151.29 153.76 161.29 139.24 139.24 53.370 127.69 169.00 132.25 136.89 151.29 158.76 53.490 153.76 163.84 148.84 136.89 146.41 161.29 53.610 144.00 169.00 158.76 144.00 151.29 158.76 53.730 156.25 163.84 176.89 161.29 166.41 169.00 53.850 163.84 174.24 184.96 169.00 169.00 156.25 53.970 187.69 193.21 171.61 196.00 190.44 184.96 54.090 176.89 187.69 174.24 213.16 201.64 196.00 54.210 216.09 228.01 198.81 184.96 240.25 187.69 54.330 243.36 201.64 237.16 207.36 216.09 225.00 54.450 234.09 246.49 213.16 240.25 240.25 234.09 54.570 246.49 231.04 219.04 222.01 234.09 234.09 54.690 219.04 228.01 262.44 262.44 252.81 246.49 54.810 243.36 231.04 234.09 243.36 256.00 246.49 54.930 243.36 252.81 249.64 207.36 204.49 259.21 55.050 246.49 243.36 198.81 225.00 219.04 204.49 55.170 213.16 216.09 243.36 219.04 198.81 219.04

121

File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 252.81 252.81 231.04 193.21 196.00 219.04 55.410 234.09 210.25 201.64 228.01 207.36 207.36 55.530 213.16 207.36 225.00 216.09 210.25 210.25 55.650 204.49 187.69 193.21 210.25 193.21 201.64 55.770 222.01 184.96 190.44 182.25 204.49 193.21 55.890 198.81 196.00 201.64 184.96 196.00 190.44 56.010 213.16 169.00 193.21 190.44 219.04 166.41 56.130 166.41 222.01 207.36 193.21 171.61 184.96 56.250 163.84 187.69 193.21 174.24 201.64 166.41 56.370 196.00 190.44 210.25 169.00 179.56 201.64 56.490 196.00 190.44 171.61 174.24 166.41 210.25 56.610 158.76 176.89 182.25 169.00 163.84 176.89 56.730 179.56 171.61 196.00 161.29 184.96 153.76 56.850 179.56 179.56 151.29 156.25 169.00 179.56 56.970 158.76 204.49 176.89 161.29 166.41 176.89 57.090 193.21 153.76 182.25 166.41 169.00 176.89 57.210 182.25 207.36 166.41 171.61 190.44 148.84 57.330 179.56 182.25 190.44 166.41 156.25 196.00 57.450 174.24 151.29 148.84 148.84 144.00 184.96 57.570 193.21 144.00 174.24 184.96 158.76 174.24 57.690 166.41 196.00 151.29 171.61 148.84 144.00 57.810 198.81 158.76 184.96 163.84 166.41 169.00 57.930 121.00 144.00 169.00 176.89 144.00 156.25 58.050 141.61 163.84 151.29 161.29 146.41 169.00 58.170 144.00 158.76 158.76 153.76 144.00 153.76 58.290 166.41 158.76 148.84 151.29 141.61 136.89 58.410 158.76 163.84 174.24 161.29 156.25 146.41 58.530 141.61 153.76 129.96 141.61 144.00 144.00 58.650 144.00 166.41 187.69 161.29 187.69 156.25 58.770 148.84 153.76 148.84 134.56 174.24 146.41 58.890 148.84 161.29 182.25 163.84 146.41 148.84 59.010 153.76 156.25 158.76 153.76 144.00 174.24 59.130 174.24 156.25 153.76 146.41 163.84 148.84 59.250 156.25 148.84 146.41 161.29 148.84 171.61 59.370 153.76 163.84 148.84 163.84 153.76 161.29 59.490 176.89 136.89 169.00 174.24 153.76 148.84 59.610 153.76 148.84 176.89 139.24 174.24 176.89 59.730 171.61 198.81 210.25 213.16 234.09 268.96 59.850 275.56 275.56 334.89 292.41 246.49 222.01 59.970 219.04 207.36 216.09 237.16 231.04 237.16 60.090 207.36 158.76 182.25 166.41 166.41 171.61 60.210 156.25 166.41 153.76 169.00 179.56 153.76 60.330 171.61 158.76 166.41 151.29 161.29 132.25 60.450 156.25 158.76 163.84 193.21 139.24 171.61 60.570 169.00 174.24 144.00 153.76 166.41 166.41 60.690 176.89 184.96 166.41 161.29 156.25 196.00 60.810 182.25 163.84 139.24 148.84 151.29 163.84 60.930 156.25 182.25 151.29 184.96 176.89 148.84 61.050 156.25 169.00 176.89 156.25 163.84 174.24 61.170 169.00 163.84 201.64 171.61 169.00 187.69 61.290 198.81 193.21 179.56 166.41 148.84 171.61 61.410 193.21 201.64 184.96 174.24 196.00 190.44

122

File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 171.61 213.16 187.69 201.64 213.16 222.01 61.650 219.04 198.81 231.04 222.01 231.04 210.25 61.770 207.36 219.04 207.36 231.04 231.04 231.04 61.890 262.44 246.49 265.69 246.49 249.64 262.44 62.010 272.25 272.25 265.69 275.56 278.89 331.24 62.130 313.29 289.00 285.61 295.84 309.76 345.96 62.250 342.25 338.56 357.21 364.81 327.61 357.21 62.370 388.09 392.04 404.01 364.81 353.44 392.04 62.490 380.25 384.16 349.69 353.44 412.09 364.81 62.610 368.64 368.64 400.00 364.81 361.00 324.00 62.730 345.96 372.49 357.21 372.49 338.56 368.64 62.850 353.44 345.96 324.00 349.69 324.00 342.25 62.970 338.56 282.24 306.25 320.41 320.41 331.24 63.090 309.76 316.84 278.89 338.56 278.89 292.41 63.210 275.56 302.76 278.89 278.89 292.41 295.84 63.330 272.25 275.56 237.16 252.81 265.69 259.21 63.450 243.36 246.49 237.16 278.89 249.64 240.25 63.570 225.00 256.00 249.64 234.09 243.36 228.01 63.690 256.00 240.25 231.04 237.16 265.69 240.25 63.810 243.36 210.25 225.00 216.09 237.16 259.21 63.930 231.04 237.16 231.04 259.21 210.25 228.01 64.050 237.16 246.49 213.16 216.09 216.09 234.09 64.170 196.00 225.00 201.64 196.00 187.69 193.21 64.290 196.00 171.61 174.24 176.89 187.69 193.21 64.410 174.24 182.25 184.96 196.00 158.76 196.00 64.530 201.64 184.96 184.96 174.24 193.21 163.84 64.650 187.69 184.96 187.69 153.76 158.76 196.00 64.770 182.25 184.96 190.44 163.84 163.84 144.00 64.890 184.96 156.25 171.61 182.25 161.29 176.89 65.010 169.00 184.96 176.89 161.29 174.24 169.00 65.130 148.84 156.25 158.76 182.25 151.29 174.24 65.250 158.76 163.84 146.41 148.84 169.00 148.84 65.370 169.00 156.25 169.00 146.41 184.96 187.69 65.490 158.76 163.84 139.24 169.00 171.61 136.89 65.610 148.84 176.89 169.00 163.84 190.44 161.29 65.730 174.24 166.41 169.00 166.41 153.76 158.76 65.850 148.84 153.76 169.00 161.29 148.84 153.76 65.970 139.24 148.84 171.61 163.84 156.25 163.84 66.090 134.56 158.76 148.84 156.25 146.41 146.41 66.210 174.24 163.84 163.84 123.21 148.84 176.89 66.330 136.89 141.61 169.00 158.76 158.76 158.76 66.450 158.76 151.29 174.24 174.24 163.84 156.25 66.570 144.00 176.89 161.29 139.24 148.84 166.41 66.690 153.76 169.00 163.84 169.00 132.25 141.61 66.810 187.69 161.29 144.00 166.41 144.00 146.41 66.930 174.24 184.96 141.61 129.96 148.84 161.29 67.050 161.29 134.56 156.25 151.29 171.61 169.00 67.170 184.96 163.84 161.29 174.24 129.96 146.41 67.290 166.41 176.89 166.41 171.61 153.76 174.24 67.410 134.56 161.29 174.24 171.61 174.24 158.76 67.530 161.29 176.89 187.69 184.96 204.49 256.00 67.650 228.01 201.64 246.49 216.09 246.49 259.21

123

File: JC3.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 196.00 207.36 207.36 182.25 207.36 204.49 67.890 240.25 207.36 187.69 213.16 210.25 216.09 68.010 252.81 243.36 265.69 278.89 252.81 268.96 68.130 327.61 353.44 404.01 404.01 408.04 376.36 68.250 320.41 313.29 231.04 234.09 243.36 275.56 68.370 302.76 302.76 268.96 240.25 198.81 207.36 68.490 182.25 156.25 169.00 171.61 158.76 144.00 68.610 166.41 163.84 171.61 182.25 169.00 129.96 68.730 146.41 144.00 161.29 158.76 163.84 136.89 68.850 148.84 153.76 139.24 169.00 144.00 174.24 68.970 153.76 144.00 158.76 187.69 148.84 148.84 69.090 136.89 141.61 134.56 166.41 151.29 136.89 69.210 146.41 151.29 163.84 144.00 153.76 151.29 69.330 139.24 144.00 144.00 156.25 176.89 161.29 69.450 174.24 169.00 141.61 158.76 156.25 144.00 69.570 158.76 153.76 151.29 146.41 153.76 153.76 69.690 158.76 148.84 132.25 118.81 116.64 144.00 69.810 153.76 146.41 136.89 144.00 153.76 146.41 69.930 166.41 151.29 169.00 166.41 _

124

File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC4 Data measured at: 24-Jan-2011 13:59:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 702.2500 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 702.25 650.25 605.16 580.81 542.89 580.81 2.130 571.21 561.69 556.96 542.89 547.56 524.41 2.250 457.96 519.84 492.84 488.41 492.84 412.09 2.370 404.01 404.01 428.49 404.01 372.49 372.49 2.490 388.09 364.81 361.00 349.69 353.44 372.49 2.610 331.24 338.56 345.96 349.69 327.61 331.24 2.730 327.61 313.29 309.76 306.25 302.76 289.00 2.850 282.24 256.00 262.44 256.00 289.00 278.89 2.970 268.96 268.96 234.09 231.04 240.25 237.16 3.090 231.04 249.64 231.04 240.25 222.01 213.16 3.210 249.64 207.36 187.69 222.01 201.64 219.04 3.330 184.96 198.81 182.25 210.25 196.00 219.04 3.450 204.49 190.44 193.21 198.81 169.00 171.61 3.570 187.69 184.96 153.76 153.76 174.24 201.64 3.690 174.24 176.89 182.25 179.56 184.96 158.76 3.810 169.00 176.89 151.29 161.29 176.89 139.24 3.930 158.76 153.76 139.24 153.76 153.76 151.29 4.050 144.00 132.25 166.41 148.84 139.24 123.21 4.170 148.84 136.89 151.29 169.00 156.25 144.00 4.290 146.41 132.25 134.56 132.25 134.56 129.96 4.410 158.76 136.89 129.96 121.00 127.69 125.44 4.530 116.64 112.36 121.00 121.00 141.61 136.89 4.650 114.49 153.76 141.61 129.96 106.09 108.16 4.770 129.96 110.25 112.36 116.64 94.09 136.89 4.890 118.81 118.81 110.25 106.09 129.96 106.09 5.010 121.00 92.16 116.64 102.01 127.69 116.64 5.130 116.64 114.49 94.09 121.00 132.25 127.69 5.250 116.64 116.64 106.09 114.49 110.25 121.00

125

File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 112.36 125.44 114.49 102.01 102.01 129.96 5.490 98.01 118.81 110.25 114.49 146.41 110.25 5.610 118.81 123.21 106.09 100.00 114.49 104.04 5.730 106.09 118.81 98.01 102.01 116.64 106.09 5.850 121.00 104.04 96.04 134.56 114.49 86.49 5.970 108.16 110.25 104.04 110.25 112.36 92.16 6.090 112.36 92.16 102.01 94.09 100.00 102.01 6.210 104.04 104.04 116.64 98.01 112.36 110.25 6.330 90.25 98.01 79.21 121.00 100.00 77.44 6.450 82.81 88.36 88.36 108.16 90.25 84.64 6.570 90.25 106.09 108.16 86.49 86.49 79.21 6.690 72.25 96.04 106.09 79.21 100.00 84.64 6.810 94.09 98.01 82.81 90.25 98.01 98.01 6.930 72.25 86.49 106.09 70.56 82.81 100.00 7.050 94.09 79.21 96.04 81.00 77.44 88.36 7.170 77.44 77.44 86.49 98.01 81.00 77.44 7.290 94.09 92.16 94.09 86.49 86.49 81.00 7.410 84.64 75.69 90.25 86.49 65.61 79.21 7.530 77.44 90.25 94.09 79.21 88.36 86.49 7.650 106.09 79.21 81.00 75.69 59.29 92.16 7.770 65.61 84.64 79.21 65.61 96.04 88.36 7.890 88.36 84.64 98.01 75.69 64.00 75.69 8.010 72.25 72.25 79.21 77.44 94.09 100.00 8.130 79.21 81.00 72.25 82.81 86.49 79.21 8.250 77.44 79.21 72.25 77.44 92.16 67.24 8.370 81.00 84.64 70.56 84.64 81.00 75.69 8.490 68.89 86.49 77.44 65.61 90.25 60.84 8.610 86.49 77.44 72.25 67.24 79.21 67.24 8.730 65.61 88.36 72.25 67.24 72.25 79.21 8.850 75.69 65.61 75.69 70.56 72.25 62.41 8.970 75.69 79.21 79.21 65.61 75.69 82.81 9.090 73.96 73.96 82.81 70.56 56.25 75.69 9.210 75.69 67.24 67.24 73.96 79.21 70.56 9.330 70.56 65.61 73.96 81.00 77.44 70.56 9.450 77.44 84.64 67.24 79.21 65.61 65.61 9.570 79.21 90.25 79.21 88.36 67.24 75.69 9.690 77.44 77.44 77.44 82.81 68.89 68.89 9.810 70.56 64.00 75.69 72.25 77.44 56.25 9.930 70.56 75.69 65.61 90.25 81.00 68.89 10.050 67.24 64.00 81.00 62.41 84.64 94.09 10.170 77.44 84.64 67.24 82.81 79.21 67.24 10.290 68.89 82.81 75.69 84.64 70.56 72.25 10.410 82.81 72.25 70.56 77.44 88.36 68.89 10.530 79.21 79.21 86.49 70.56 65.61 72.25 10.650 81.00 79.21 82.81 70.56 72.25 75.69 10.770 70.56 54.76 67.24 86.49 70.56 75.69 10.890 79.21 96.04 88.36 75.69 67.24 100.00 11.010 86.49 67.24 75.69 79.21 79.21 68.89 11.130 84.64 90.25 82.81 104.04 79.21 102.01 11.250 82.81 84.64 96.04 90.25 77.44 102.01 11.370 70.56 84.64 77.44 82.81 102.01 96.04 11.490 96.04 116.64 100.00 96.04 88.36 104.04

126

File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 102.01 100.00 94.09 102.01 77.44 94.09 11.730 96.04 94.09 110.25 82.81 112.36 96.04 11.850 98.01 104.04 100.00 110.25 84.64 106.09 11.970 90.25 88.36 121.00 79.21 96.04 92.16 12.090 98.01 86.49 102.01 72.25 88.36 92.16 12.210 81.00 92.16 70.56 79.21 90.25 73.96 12.330 77.44 72.25 70.56 75.69 70.56 86.49 12.450 67.24 75.69 70.56 67.24 73.96 70.56 12.570 57.76 65.61 59.29 65.61 60.84 59.29 12.690 75.69 62.41 65.61 65.61 54.76 59.29 12.810 56.25 68.89 59.29 56.25 62.41 50.41 12.930 67.24 53.29 62.41 49.00 47.61 56.25 13.050 44.89 47.61 60.84 56.25 53.29 57.76 13.170 53.29 67.24 59.29 51.84 67.24 60.84 13.290 62.41 51.84 57.76 47.61 50.41 53.29 13.410 50.41 43.56 51.84 53.29 51.84 44.89 13.530 59.29 51.84 44.89 47.61 53.29 60.84 13.650 62.41 47.61 54.76 65.61 50.41 44.89 13.770 46.24 51.84 65.61 51.84 53.29 56.25 13.890 43.56 47.61 43.56 56.25 62.41 42.25 14.010 60.84 53.29 51.84 50.41 56.25 53.29 14.130 38.44 39.69 42.25 40.96 57.76 59.29 14.250 46.24 47.61 49.00 42.25 47.61 51.84 14.370 50.41 50.41 59.29 53.29 47.61 37.21 14.490 44.89 60.84 44.89 53.29 49.00 50.41 14.610 43.56 53.29 49.00 53.29 50.41 43.56 14.730 40.96 36.00 47.61 37.21 56.25 49.00 14.850 51.84 59.29 43.56 47.61 54.76 43.56 14.970 53.29 44.89 50.41 50.41 47.61 50.41 15.090 59.29 49.00 50.41 46.24 56.25 47.61 15.210 42.25 47.61 49.00 38.44 53.29 44.89 15.330 38.44 59.29 46.24 54.76 56.25 36.00 15.450 50.41 47.61 49.00 59.29 40.96 40.96 15.570 46.24 44.89 42.25 46.24 59.29 46.24 15.690 46.24 56.25 46.24 38.44 47.61 39.69 15.810 60.84 50.41 56.25 53.29 44.89 43.56 15.930 50.41 30.25 47.61 50.41 50.41 50.41 16.050 43.56 46.24 47.61 51.84 39.69 56.25 16.170 42.25 38.44 43.56 46.24 44.89 40.96 16.290 44.89 47.61 38.44 46.24 47.61 47.61 16.410 57.76 46.24 38.44 49.00 50.41 51.84 16.530 54.76 53.29 47.61 38.44 40.96 43.56 16.650 49.00 49.00 53.29 39.69 47.61 43.56 16.770 56.25 40.96 43.56 56.25 50.41 43.56 16.890 59.29 49.00 62.41 50.41 54.76 50.41 17.010 50.41 53.29 40.96 60.84 54.76 44.89 17.130 60.84 50.41 47.61 65.61 42.25 37.21 17.250 44.89 47.61 56.25 53.29 53.29 67.24 17.370 47.61 49.00 59.29 56.25 53.29 50.41 17.490 53.29 50.41 54.76 57.76 65.61 70.56 17.610 56.25 46.24 53.29 49.00 59.29 54.76 17.730 57.76 54.76 62.41 54.76 65.61 59.29

127

File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 56.25 59.29 72.25 57.76 53.29 67.24 17.970 62.41 64.00 59.29 77.44 47.61 57.76 18.090 59.29 65.61 72.25 62.41 70.56 72.25 18.210 68.89 50.41 62.41 62.41 75.69 51.84 18.330 67.24 64.00 59.29 53.29 75.69 56.25 18.450 68.89 56.25 62.41 47.61 60.84 65.61 18.570 56.25 56.25 59.29 54.76 44.89 60.84 18.690 75.69 64.00 56.25 67.24 64.00 59.29 18.810 60.84 53.29 53.29 67.24 64.00 59.29 18.930 54.76 81.00 65.61 70.56 60.84 67.24 19.050 51.84 67.24 77.44 82.81 68.89 70.56 19.170 75.69 65.61 72.25 70.56 73.96 72.25 19.290 72.25 77.44 70.56 102.01 112.36 84.64 19.410 88.36 98.01 90.25 112.36 94.09 118.81 19.530 118.81 104.04 144.00 132.25 144.00 141.61 19.650 144.00 127.69 151.29 158.76 163.84 166.41 19.770 179.56 196.00 204.49 210.25 225.00 213.16 19.890 237.16 213.16 216.09 225.00 228.01 219.04 20.010 222.01 222.01 213.16 193.21 182.25 219.04 20.130 193.21 179.56 210.25 207.36 204.49 184.96 20.250 158.76 163.84 153.76 193.21 158.76 151.29 20.370 169.00 166.41 193.21 184.96 169.00 163.84 20.490 161.29 163.84 163.84 174.24 153.76 169.00 20.610 184.96 182.25 163.84 176.89 187.69 166.41 20.730 187.69 174.24 204.49 210.25 272.25 295.84 20.850 295.84 285.61 256.00 234.09 184.96 182.25 20.970 174.24 179.56 163.84 176.89 179.56 184.96 21.090 204.49 216.09 184.96 166.41 193.21 204.49 21.210 184.96 184.96 219.04 184.96 198.81 190.44 21.330 158.76 163.84 184.96 174.24 193.21 166.41 21.450 169.00 156.25 156.25 156.25 158.76 156.25 21.570 166.41 148.84 156.25 148.84 148.84 151.29 21.690 144.00 139.24 125.44 116.64 148.84 129.96 21.810 129.96 108.16 139.24 132.25 102.01 127.69 21.930 112.36 129.96 108.16 118.81 110.25 108.16 22.050 100.00 108.16 106.09 116.64 136.89 100.00 22.170 116.64 106.09 108.16 112.36 118.81 102.01 22.290 88.36 104.04 106.09 100.00 104.04 102.01 22.410 96.04 100.00 110.25 112.36 94.09 112.36 22.530 104.04 118.81 94.09 82.81 96.04 106.09 22.650 94.09 104.04 96.04 84.64 102.01 92.16 22.770 96.04 88.36 102.01 94.09 98.01 94.09 22.890 92.16 77.44 90.25 100.00 118.81 108.16 23.010 100.00 110.25 92.16 112.36 98.01 104.04 23.130 108.16 98.01 88.36 98.01 108.16 104.04 23.250 94.09 102.01 96.04 88.36 121.00 96.04 23.370 92.16 102.01 92.16 104.04 88.36 102.01 23.490 110.25 102.01 84.64 86.49 110.25 100.00 23.610 102.01 98.01 92.16 90.25 102.01 100.00 23.730 104.04 100.00 132.25 96.04 123.21 102.01 23.850 118.81 98.01 98.01 118.81 118.81 121.00 23.970 112.36 104.04 98.01 106.09 100.00 127.69

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 125.44 118.81 110.25 118.81 106.09 116.64 24.210 129.96 106.09 118.81 139.24 125.44 123.21 24.330 100.00 123.21 121.00 106.09 123.21 127.69 24.450 94.09 114.49 127.69 112.36 118.81 118.81 24.570 127.69 114.49 144.00 116.64 116.64 129.96 24.690 118.81 116.64 116.64 121.00 121.00 118.81 24.810 127.69 118.81 90.25 116.64 104.04 114.49 24.930 108.16 104.04 118.81 125.44 96.04 90.25 25.050 94.09 108.16 106.09 118.81 102.01 90.25 25.170 114.49 96.04 108.16 96.04 100.00 106.09 25.290 100.00 94.09 88.36 100.00 100.00 96.04 25.410 102.01 98.01 121.00 108.16 88.36 75.69 25.530 98.01 94.09 102.01 84.64 96.04 94.09 25.650 94.09 72.25 86.49 92.16 102.01 77.44 25.770 100.00 98.01 92.16 86.49 88.36 84.64 25.890 94.09 84.64 108.16 104.04 92.16 88.36 26.010 82.81 88.36 92.16 94.09 81.00 106.09 26.130 94.09 94.09 73.96 102.01 108.16 92.16 26.250 94.09 90.25 96.04 90.25 96.04 81.00 26.370 88.36 98.01 96.04 94.09 102.01 114.49 26.490 127.69 121.00 153.76 196.00 213.16 237.16 26.610 285.61 272.25 262.44 204.49 161.29 153.76 26.730 112.36 108.16 96.04 96.04 98.01 86.49 26.850 67.24 94.09 88.36 77.44 72.25 75.69 26.970 72.25 94.09 75.69 88.36 86.49 82.81 27.090 88.36 75.69 75.69 72.25 86.49 81.00 27.210 79.21 77.44 75.69 75.69 79.21 86.49 27.330 90.25 90.25 86.49 70.56 77.44 75.69 27.450 77.44 75.69 84.64 77.44 60.84 77.44 27.570 75.69 77.44 59.29 79.21 72.25 65.61 27.690 77.44 62.41 56.25 68.89 73.96 67.24 27.810 73.96 65.61 67.24 70.56 86.49 67.24 27.930 82.81 65.61 82.81 73.96 65.61 72.25 28.050 82.81 65.61 72.25 72.25 70.56 50.41 28.170 62.41 60.84 75.69 56.25 65.61 70.56 28.290 82.81 56.25 82.81 67.24 77.44 67.24 28.410 65.61 65.61 65.61 75.69 59.29 84.64 28.530 82.81 79.21 75.69 72.25 62.41 79.21 28.650 77.44 65.61 82.81 72.25 72.25 54.76 28.770 59.29 70.56 59.29 54.76 59.29 70.56 28.890 59.29 60.84 67.24 67.24 68.89 75.69 29.010 62.41 59.29 62.41 92.16 72.25 75.69 29.130 67.24 47.61 62.41 75.69 67.24 43.56 29.250 70.56 59.29 62.41 59.29 72.25 62.41 29.370 65.61 62.41 56.25 67.24 67.24 68.89 29.490 70.56 82.81 62.41 67.24 59.29 67.24 29.610 72.25 53.29 67.24 67.24 62.41 67.24 29.730 67.24 59.29 56.25 56.25 67.24 75.69 29.850 67.24 65.61 50.41 79.21 75.69 64.00 29.970 70.56 59.29 53.29 67.24 64.00 53.29 30.090 56.25 53.29 57.76 53.29 57.76 62.41 30.210 68.89 59.29 56.25 65.61 59.29 68.89

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File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 65.61 73.96 65.61 60.84 65.61 54.76 30.450 64.00 51.84 59.29 57.76 62.41 65.61 30.570 72.25 84.64 54.76 56.25 72.25 49.00 30.690 68.89 75.69 60.84 67.24 43.56 57.76 30.810 65.61 72.25 64.00 53.29 67.24 62.41 30.930 46.24 72.25 72.25 67.24 67.24 62.41 31.050 53.29 50.41 77.44 64.00 54.76 54.76 31.170 59.29 56.25 65.61 56.25 75.69 65.61 31.290 53.29 65.61 56.25 60.84 62.41 62.41 31.410 68.89 62.41 84.64 72.25 73.96 72.25 31.530 81.00 56.25 64.00 62.41 64.00 72.25 31.650 59.29 82.81 79.21 57.76 70.56 84.64 31.770 72.25 43.56 72.25 68.89 64.00 57.76 31.890 62.41 77.44 70.56 73.96 75.69 68.89 32.010 65.61 70.56 70.56 70.56 60.84 72.25 32.130 60.84 79.21 59.29 59.29 67.24 90.25 32.250 56.25 67.24 65.61 70.56 75.69 77.44 32.370 65.61 77.44 65.61 70.56 72.25 82.81 32.490 64.00 77.44 77.44 86.49 88.36 75.69 32.610 79.21 77.44 86.49 86.49 75.69 88.36 32.730 82.81 79.21 86.49 82.81 90.25 96.04 32.850 86.49 94.09 110.25 94.09 90.25 98.01 32.970 106.09 72.25 92.16 106.09 90.25 118.81 33.090 112.36 98.01 102.01 108.16 98.01 102.01 33.210 110.25 116.64 110.25 116.64 121.00 102.01 33.330 125.44 112.36 104.04 121.00 116.64 121.00 33.450 106.09 108.16 114.49 100.00 90.25 106.09 33.570 110.25 108.16 118.81 106.09 96.04 92.16 33.690 100.00 127.69 112.36 112.36 86.49 112.36 33.810 102.01 92.16 100.00 98.01 102.01 102.01 33.930 100.00 98.01 108.16 98.01 86.49 92.16 34.050 92.16 102.01 106.09 104.04 108.16 118.81 34.170 94.09 106.09 106.09 88.36 112.36 104.04 34.290 108.16 110.25 114.49 116.64 118.81 100.00 34.410 127.69 141.61 116.64 141.61 136.89 144.00 34.530 153.76 136.89 141.61 134.56 153.76 153.76 34.650 144.00 144.00 166.41 158.76 158.76 156.25 34.770 176.89 158.76 169.00 169.00 169.00 151.29 34.890 179.56 204.49 176.89 169.00 182.25 198.81 35.010 182.25 158.76 163.84 158.76 156.25 171.61 35.130 174.24 144.00 136.89 144.00 166.41 171.61 35.250 182.25 146.41 158.76 166.41 156.25 141.61 35.370 169.00 166.41 166.41 169.00 141.61 179.56 35.490 182.25 153.76 169.00 158.76 176.89 148.84 35.610 161.29 158.76 146.41 174.24 161.29 134.56 35.730 176.89 151.29 169.00 184.96 171.61 158.76 35.850 174.24 169.00 166.41 182.25 161.29 158.76 35.970 158.76 161.29 193.21 198.81 171.61 176.89 36.090 182.25 222.01 182.25 176.89 179.56 193.21 36.210 210.25 198.81 210.25 193.21 190.44 176.89 36.330 196.00 207.36 216.09 193.21 237.16 198.81 36.450 207.36 222.01 237.16 246.49 243.36 302.76

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File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 252.81 222.01 268.96 299.29 268.96 259.21 36.690 259.21 259.21 256.00 243.36 240.25 249.64 36.810 252.81 246.49 228.01 249.64 246.49 228.01 36.930 249.64 272.25 249.64 256.00 237.16 219.04 37.050 231.04 234.09 222.01 228.01 222.01 222.01 37.170 240.25 216.09 222.01 207.36 210.25 198.81 37.290 179.56 196.00 198.81 184.96 184.96 158.76 37.410 182.25 158.76 184.96 163.84 148.84 151.29 37.530 153.76 158.76 176.89 156.25 158.76 141.61 37.650 146.41 127.69 153.76 158.76 174.24 139.24 37.770 134.56 141.61 161.29 127.69 153.76 156.25 37.890 129.96 158.76 146.41 151.29 129.96 134.56 38.010 116.64 148.84 148.84 125.44 151.29 129.96 38.130 123.21 125.44 139.24 134.56 110.25 121.00 38.250 123.21 139.24 132.25 129.96 148.84 121.00 38.370 134.56 118.81 134.56 116.64 104.04 134.56 38.490 134.56 108.16 100.00 100.00 121.00 123.21 38.610 110.25 139.24 132.25 118.81 110.25 98.01 38.730 123.21 110.25 127.69 116.64 121.00 110.25 38.850 123.21 141.61 112.36 125.44 121.00 106.09 38.970 134.56 123.21 121.00 129.96 112.36 108.16 39.090 121.00 110.25 102.01 118.81 118.81 134.56 39.210 125.44 116.64 125.44 118.81 108.16 125.44 39.330 108.16 104.04 127.69 158.76 132.25 148.84 39.450 127.69 123.21 153.76 146.41 132.25 151.29 39.570 141.61 121.00 132.25 125.44 127.69 148.84 39.690 139.24 134.56 148.84 158.76 144.00 136.89 39.810 158.76 134.56 156.25 134.56 139.24 118.81 39.930 153.76 141.61 169.00 148.84 156.25 153.76 40.050 158.76 156.25 132.25 148.84 144.00 144.00 40.170 146.41 148.84 141.61 163.84 153.76 136.89 40.290 153.76 151.29 123.21 146.41 141.61 136.89 40.410 144.00 127.69 136.89 121.00 127.69 110.25 40.530 136.89 118.81 125.44 146.41 121.00 129.96 40.650 116.64 123.21 123.21 125.44 110.25 114.49 40.770 114.49 118.81 94.09 104.04 127.69 106.09 40.890 129.96 112.36 125.44 102.01 114.49 108.16 41.010 121.00 110.25 106.09 114.49 125.44 121.00 41.130 104.04 114.49 118.81 121.00 136.89 92.16 41.250 132.25 123.21 106.09 110.25 100.00 110.25 41.370 98.01 108.16 123.21 88.36 127.69 104.04 41.490 102.01 106.09 104.04 118.81 121.00 132.25 41.610 118.81 100.00 102.01 90.25 102.01 118.81 41.730 88.36 92.16 84.64 88.36 104.04 102.01 41.850 84.64 98.01 104.04 84.64 100.00 94.09 41.970 86.49 96.04 98.01 94.09 92.16 102.01 42.090 92.16 88.36 96.04 84.64 90.25 82.81 42.210 79.21 77.44 84.64 98.01 100.00 123.21 42.330 151.29 153.76 210.25 161.29 161.29 184.96 42.450 144.00 148.84 136.89 132.25 114.49 110.25 42.570 98.01 82.81 100.00 79.21 79.21 86.49 42.690 77.44 88.36 84.64 70.56 67.24 88.36

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File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 84.64 90.25 62.41 86.49 72.25 94.09 42.930 79.21 86.49 70.56 72.25 90.25 79.21 43.050 100.00 84.64 65.61 73.96 94.09 108.16 43.170 72.25 72.25 75.69 77.44 92.16 60.84 43.290 88.36 72.25 79.21 62.41 81.00 77.44 43.410 90.25 73.96 88.36 75.69 88.36 96.04 43.530 75.69 67.24 70.56 70.56 75.69 72.25 43.650 84.64 59.29 82.81 73.96 70.56 65.61 43.770 77.44 62.41 72.25 70.56 64.00 72.25 43.890 75.69 67.24 51.84 60.84 75.69 70.56 44.010 75.69 72.25 79.21 77.44 72.25 81.00 44.130 82.81 86.49 62.41 82.81 70.56 70.56 44.250 77.44 75.69 77.44 65.61 64.00 64.00 44.370 75.69 68.89 79.21 75.69 79.21 70.56 44.490 70.56 88.36 67.24 59.29 72.25 65.61 44.610 72.25 67.24 84.64 56.25 70.56 67.24 44.730 59.29 72.25 75.69 67.24 77.44 79.21 44.850 84.64 88.36 65.61 72.25 64.00 86.49 44.970 50.41 67.24 75.69 79.21 77.44 64.00 45.090 70.56 70.56 75.69 81.00 81.00 77.44 45.210 50.41 73.96 56.25 56.25 82.81 72.25 45.330 70.56 68.89 56.25 73.96 65.61 67.24 45.450 59.29 62.41 67.24 75.69 67.24 75.69 45.570 57.76 70.56 77.44 77.44 82.81 67.24 45.690 82.81 75.69 92.16 86.49 79.21 88.36 45.810 67.24 70.56 100.00 86.49 67.24 72.25 45.930 65.61 77.44 65.61 60.84 64.00 59.29 46.050 75.69 77.44 62.41 75.69 75.69 57.76 46.170 77.44 70.56 75.69 53.29 79.21 70.56 46.290 62.41 56.25 72.25 73.96 72.25 70.56 46.410 64.00 60.84 77.44 53.29 75.69 79.21 46.530 70.56 67.24 67.24 67.24 59.29 75.69 46.650 70.56 67.24 79.21 62.41 75.69 77.44 46.770 65.61 64.00 73.96 62.41 65.61 70.56 46.890 67.24 67.24 64.00 73.96 57.76 75.69 47.010 70.56 77.44 57.76 67.24 84.64 65.61 47.130 62.41 77.44 68.89 70.56 59.29 70.56 47.250 65.61 57.76 79.21 81.00 65.61 77.44 47.370 70.56 82.81 79.21 70.56 59.29 79.21 47.490 50.41 72.25 75.69 75.69 53.29 72.25 47.610 67.24 79.21 72.25 68.89 60.84 64.00 47.730 65.61 70.56 70.56 70.56 77.44 84.64 47.850 62.41 86.49 65.61 62.41 62.41 77.44 47.970 73.96 65.61 67.24 50.41 67.24 77.44 48.090 70.56 65.61 62.41 65.61 79.21 60.84 48.210 59.29 72.25 65.61 57.76 56.25 67.24 48.330 68.89 73.96 65.61 53.29 67.24 59.29 48.450 84.64 67.24 77.44 60.84 64.00 56.25 48.570 59.29 62.41 56.25 59.29 81.00 84.64 48.690 70.56 65.61 59.29 60.84 64.00 62.41 48.810 70.56 67.24 84.64 65.61 62.41 53.29 48.930 56.25 73.96 53.29 56.25 59.29 56.25

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File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 75.69 56.25 65.61 65.61 64.00 81.00 49.170 46.24 62.41 70.56 62.41 75.69 68.89 49.290 62.41 57.76 62.41 59.29 53.29 79.21 49.410 72.25 73.96 64.00 65.61 62.41 51.84 49.530 67.24 60.84 81.00 62.41 62.41 70.56 49.650 73.96 77.44 72.25 68.89 62.41 59.29 49.770 65.61 59.29 70.56 65.61 72.25 67.24 49.890 79.21 88.36 79.21 72.25 94.09 102.01 50.010 92.16 100.00 110.25 108.16 112.36 118.81 50.130 118.81 82.81 96.04 112.36 98.01 86.49 50.250 102.01 82.81 100.00 75.69 82.81 86.49 50.370 81.00 81.00 81.00 98.01 108.16 108.16 50.490 110.25 100.00 75.69 92.16 88.36 118.81 50.610 88.36 90.25 84.64 75.69 73.96 77.44 50.730 84.64 90.25 70.56 79.21 104.04 88.36 50.850 79.21 98.01 90.25 67.24 75.69 68.89 50.970 79.21 79.21 88.36 82.81 65.61 73.96 51.090 84.64 70.56 84.64 77.44 67.24 77.44 51.210 79.21 59.29 68.89 82.81 81.00 84.64 51.330 88.36 67.24 90.25 70.56 79.21 62.41 51.450 86.49 79.21 75.69 77.44 98.01 70.56 51.570 84.64 68.89 86.49 79.21 67.24 82.81 51.690 82.81 92.16 88.36 73.96 79.21 86.49 51.810 94.09 81.00 75.69 90.25 86.49 86.49 51.930 77.44 77.44 67.24 86.49 79.21 86.49 52.050 77.44 75.69 67.24 94.09 86.49 84.64 52.170 104.04 73.96 84.64 73.96 86.49 77.44 52.290 90.25 79.21 77.44 79.21 86.49 98.01 52.410 77.44 72.25 77.44 96.04 70.56 88.36 52.530 94.09 96.04 73.96 79.21 88.36 90.25 52.650 106.09 102.01 102.01 100.00 86.49 102.01 52.770 90.25 94.09 98.01 112.36 108.16 118.81 52.890 96.04 108.16 127.69 110.25 136.89 118.81 53.010 100.00 146.41 110.25 148.84 121.00 141.61 53.130 141.61 146.41 132.25 163.84 121.00 136.89 53.250 144.00 153.76 158.76 161.29 158.76 144.00 53.370 174.24 163.84 151.29 151.29 129.96 151.29 53.490 139.24 141.61 153.76 151.29 146.41 163.84 53.610 158.76 148.84 144.00 136.89 144.00 169.00 53.730 153.76 174.24 141.61 146.41 139.24 163.84 53.850 141.61 153.76 156.25 139.24 134.56 134.56 53.970 125.44 127.69 153.76 146.41 136.89 129.96 54.090 144.00 129.96 144.00 118.81 125.44 179.56 54.210 123.21 139.24 144.00 132.25 132.25 148.84 54.330 134.56 139.24 146.41 139.24 129.96 146.41 54.450 129.96 136.89 166.41 129.96 123.21 144.00 54.570 123.21 129.96 139.24 144.00 121.00 129.96 54.690 132.25 123.21 134.56 132.25 134.56 158.76 54.810 141.61 141.61 123.21 139.24 129.96 134.56 54.930 94.09 98.01 112.36 125.44 104.04 114.49 55.050 118.81 114.49 121.00 98.01 110.25 108.16 55.170 121.00 112.36 94.09 102.01 116.64 106.09

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File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 82.81 114.49 102.01 110.25 102.01 90.25 55.410 98.01 104.04 98.01 112.36 116.64 100.00 55.530 116.64 123.21 96.04 114.49 106.09 86.49 55.650 116.64 100.00 84.64 94.09 84.64 88.36 55.770 77.44 102.01 75.69 102.01 96.04 116.64 55.890 110.25 98.01 92.16 110.25 96.04 110.25 56.010 94.09 96.04 104.04 100.00 108.16 110.25 56.130 84.64 106.09 90.25 92.16 102.01 102.01 56.250 94.09 88.36 84.64 77.44 86.49 90.25 56.370 98.01 98.01 84.64 75.69 102.01 75.69 56.490 96.04 98.01 90.25 104.04 86.49 86.49 56.610 104.04 77.44 70.56 77.44 84.64 104.04 56.730 86.49 94.09 86.49 75.69 104.04 84.64 56.850 108.16 90.25 84.64 88.36 68.89 110.25 56.970 94.09 98.01 70.56 88.36 102.01 75.69 57.090 98.01 82.81 92.16 98.01 102.01 82.81 57.210 94.09 90.25 77.44 79.21 82.81 92.16 57.330 86.49 102.01 98.01 86.49 90.25 75.69 57.450 88.36 108.16 75.69 92.16 96.04 90.25 57.570 98.01 96.04 86.49 114.49 84.64 98.01 57.690 108.16 96.04 86.49 100.00 100.00 98.01 57.810 82.81 102.01 94.09 106.09 102.01 102.01 57.930 110.25 92.16 106.09 94.09 110.25 116.64 58.050 92.16 94.09 88.36 96.04 75.69 88.36 58.170 98.01 94.09 96.04 70.56 98.01 102.01 58.290 94.09 84.64 88.36 90.25 98.01 84.64 58.410 96.04 90.25 92.16 94.09 110.25 90.25 58.530 79.21 94.09 98.01 102.01 90.25 86.49 58.650 94.09 100.00 110.25 118.81 118.81 98.01 58.770 112.36 100.00 112.36 125.44 98.01 110.25 58.890 110.25 123.21 110.25 104.04 110.25 114.49 59.010 110.25 118.81 108.16 139.24 100.00 129.96 59.130 144.00 102.01 116.64 114.49 118.81 125.44 59.250 121.00 118.81 116.64 127.69 125.44 121.00 59.370 121.00 125.44 134.56 121.00 129.96 116.64 59.490 102.01 132.25 104.04 121.00 112.36 123.21 59.610 106.09 114.49 94.09 121.00 110.25 108.16 59.730 116.64 106.09 98.01 125.44 108.16 125.44 59.850 153.76 132.25 139.24 134.56 136.89 129.96 59.970 116.64 110.25 127.69 136.89 121.00 100.00 60.090 121.00 121.00 114.49 121.00 100.00 94.09 60.210 102.01 110.25 100.00 100.00 108.16 94.09 60.330 86.49 108.16 110.25 110.25 108.16 96.04 60.450 90.25 118.81 102.01 94.09 106.09 92.16 60.570 110.25 110.25 112.36 114.49 96.04 116.64 60.690 104.04 110.25 104.04 116.64 100.00 96.04 60.810 96.04 110.25 96.04 132.25 121.00 123.21 60.930 114.49 125.44 123.21 100.00 121.00 127.69 61.050 132.25 123.21 118.81 141.61 104.04 121.00 61.170 129.96 127.69 94.09 108.16 125.44 136.89 61.290 112.36 141.61 132.25 118.81 132.25 136.89 61.410 127.69 100.00 139.24 144.00 123.21 129.96

134

File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 136.89 139.24 125.44 148.84 116.64 121.00 61.650 151.29 151.29 158.76 153.76 134.56 158.76 61.770 139.24 139.24 156.25 148.84 129.96 132.25 61.890 158.76 151.29 148.84 151.29 158.76 158.76 62.010 158.76 141.61 153.76 163.84 158.76 158.76 62.130 129.96 158.76 158.76 169.00 166.41 158.76 62.250 153.76 144.00 176.89 153.76 182.25 136.89 62.370 136.89 134.56 166.41 161.29 139.24 184.96 62.490 176.89 171.61 148.84 184.96 166.41 158.76 62.610 187.69 171.61 148.84 179.56 161.29 153.76 62.730 166.41 169.00 144.00 144.00 153.76 139.24 62.850 169.00 151.29 144.00 158.76 161.29 146.41 62.970 161.29 171.61 156.25 144.00 146.41 153.76 63.090 136.89 139.24 129.96 125.44 144.00 144.00 63.210 134.56 163.84 158.76 123.21 132.25 121.00 63.330 129.96 129.96 158.76 123.21 125.44 153.76 63.450 132.25 112.36 136.89 158.76 141.61 118.81 63.570 127.69 106.09 123.21 125.44 112.36 106.09 63.690 123.21 129.96 125.44 125.44 102.01 129.96 63.810 123.21 136.89 136.89 139.24 136.89 129.96 63.930 134.56 127.69 118.81 121.00 132.25 141.61 64.050 114.49 125.44 136.89 136.89 125.44 129.96 64.170 141.61 132.25 123.21 110.25 116.64 114.49 64.290 94.09 104.04 108.16 104.04 108.16 125.44 64.410 112.36 118.81 84.64 110.25 112.36 102.01 64.530 108.16 98.01 110.25 106.09 86.49 86.49 64.650 98.01 108.16 96.04 110.25 96.04 106.09 64.770 90.25 112.36 108.16 90.25 98.01 102.01 64.890 94.09 79.21 98.01 90.25 98.01 90.25 65.010 77.44 90.25 104.04 88.36 79.21 75.69 65.130 88.36 84.64 96.04 82.81 102.01 82.81 65.250 96.04 98.01 94.09 92.16 84.64 96.04 65.370 84.64 102.01 104.04 90.25 86.49 86.49 65.490 94.09 90.25 94.09 90.25 92.16 98.01 65.610 79.21 96.04 84.64 88.36 92.16 84.64 65.730 108.16 102.01 92.16 92.16 88.36 86.49 65.850 106.09 94.09 90.25 90.25 98.01 84.64 65.970 90.25 90.25 75.69 90.25 88.36 90.25 66.090 102.01 96.04 75.69 75.69 82.81 84.64 66.210 94.09 92.16 100.00 86.49 84.64 86.49 66.330 86.49 92.16 92.16 81.00 75.69 73.96 66.450 84.64 79.21 72.25 84.64 81.00 70.56 66.570 84.64 70.56 62.41 96.04 86.49 96.04 66.690 70.56 79.21 77.44 86.49 81.00 77.44 66.810 102.01 100.00 79.21 90.25 72.25 81.00 66.930 79.21 88.36 73.96 77.44 77.44 72.25 67.050 84.64 79.21 72.25 94.09 65.61 86.49 67.170 81.00 77.44 88.36 70.56 75.69 67.24 67.290 90.25 81.00 90.25 70.56 75.69 94.09 67.410 65.61 86.49 81.00 84.64 94.09 82.81 67.530 96.04 98.01 79.21 98.01 84.64 102.01 67.650 94.09 90.25 100.00 96.04 108.16 82.81

135

File: JC4.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 94.09 94.09 84.64 106.09 82.81 112.36 67.890 94.09 98.01 81.00 79.21 96.04 104.04 68.010 108.16 112.36 118.81 106.09 108.16 108.16 68.130 112.36 104.04 108.16 110.25 114.49 92.16 68.250 108.16 94.09 112.36 96.04 104.04 98.01 68.370 82.81 84.64 96.04 104.04 100.00 100.00 68.490 100.00 90.25 96.04 81.00 79.21 88.36 68.610 92.16 92.16 84.64 72.25 79.21 65.61 68.730 79.21 82.81 96.04 81.00 88.36 90.25 68.850 92.16 84.64 81.00 108.16 96.04 90.25 68.970 92.16 98.01 79.21 102.01 77.44 79.21 69.090 82.81 102.01 72.25 84.64 94.09 84.64 69.210 100.00 79.21 94.09 86.49 98.01 104.04 69.330 88.36 81.00 92.16 108.16 67.24 88.36 69.450 104.04 79.21 98.01 82.81 82.81 94.09 69.570 102.01 104.04 86.49 88.36 77.44 86.49 69.690 86.49 86.49 88.36 79.21 92.16 98.01 69.810 68.89 84.64 102.01 82.81 108.16 81.00 69.930 90.25 82.81 72.25 67.24 _

136

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC5 Data measured at: 24-Jan-2011 14:56:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 6021.760 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 121.00 127.69 100.00 96.04 108.16 94.09 2.130 108.16 94.09 98.01 90.25 98.01 98.01 2.250 86.49 98.01 92.16 84.64 81.00 73.96 2.370 79.21 96.04 62.41 81.00 79.21 90.25 2.490 73.96 90.25 86.49 70.56 70.56 81.00 2.610 62.41 70.56 72.25 62.41 67.24 65.61 2.730 86.49 75.69 75.69 72.25 56.25 70.56 2.850 59.29 72.25 53.29 75.69 75.69 70.56 2.970 57.76 65.61 72.25 64.00 56.25 59.29 3.090 53.29 56.25 72.25 72.25 70.56 53.29 3.210 70.56 65.61 67.24 75.69 54.76 70.56 3.330 56.25 59.29 62.41 65.61 77.44 56.25 3.450 50.41 59.29 56.25 72.25 70.56 60.84 3.570 70.56 75.69 54.76 60.84 56.25 62.41 3.690 51.84 70.56 57.76 60.84 62.41 59.29 3.810 56.25 53.29 50.41 50.41 47.61 50.41 3.930 60.84 56.25 54.76 46.24 75.69 56.25 4.050 64.00 65.61 65.61 53.29 60.84 62.41 4.170 65.61 56.25 53.29 43.56 56.25 60.84 4.290 62.41 50.41 50.41 56.25 47.61 50.41 4.410 51.84 51.84 75.69 68.89 53.29 60.84 4.530 50.41 56.25 62.41 47.61 62.41 65.61 4.650 59.29 72.25 50.41 70.56 51.84 67.24 4.770 59.29 51.84 72.25 53.29 62.41 65.61 4.890 53.29 51.84 53.29 40.96 56.25 56.25 5.010 53.29 59.29 72.25 56.25 70.56 57.76 5.130 50.41 64.00 59.29 38.44 62.41 43.56 5.250 59.29 54.76 56.25 56.25 54.76 62.41

137

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 70.56 59.29 72.25 53.29 62.41 57.76 5.490 47.61 56.25 50.41 50.41 50.41 64.00 5.610 54.76 59.29 49.00 59.29 43.56 50.41 5.730 51.84 54.76 70.56 56.25 56.25 56.25 5.850 56.25 59.29 57.76 47.61 65.61 56.25 5.970 62.41 56.25 47.61 51.84 53.29 59.29 6.090 37.21 62.41 46.24 47.61 65.61 53.29 6.210 56.25 53.29 62.41 56.25 57.76 59.29 6.330 53.29 47.61 65.61 62.41 49.00 51.84 6.450 51.84 60.84 46.24 60.84 64.00 50.41 6.570 50.41 59.29 50.41 53.29 62.41 54.76 6.690 33.64 65.61 65.61 59.29 60.84 64.00 6.810 50.41 50.41 79.21 57.76 62.41 49.00 6.930 53.29 43.56 56.25 59.29 54.76 62.41 7.050 53.29 50.41 56.25 54.76 56.25 46.24 7.170 43.56 49.00 59.29 59.29 70.56 49.00 7.290 60.84 39.69 44.89 50.41 50.41 57.76 7.410 59.29 54.76 53.29 36.00 53.29 43.56 7.530 56.25 44.89 42.25 77.44 51.84 44.89 7.650 53.29 43.56 44.89 59.29 50.41 54.76 7.770 54.76 62.41 54.76 51.84 59.29 56.25 7.890 50.41 59.29 46.24 47.61 53.29 56.25 8.010 53.29 56.25 43.56 51.84 59.29 50.41 8.130 32.49 65.61 46.24 65.61 44.89 47.61 8.250 50.41 57.76 44.89 53.29 43.56 64.00 8.370 47.61 56.25 43.56 49.00 56.25 50.41 8.490 43.56 49.00 62.41 62.41 42.25 42.25 8.610 57.76 50.41 57.76 62.41 43.56 53.29 8.730 53.29 46.24 53.29 51.84 53.29 56.25 8.850 39.69 51.84 47.61 56.25 40.96 47.61 8.970 56.25 53.29 56.25 43.56 50.41 38.44 9.090 42.25 42.25 56.25 46.24 44.89 46.24 9.210 59.29 47.61 39.69 49.00 70.56 46.24 9.330 38.44 49.00 59.29 49.00 47.61 59.29 9.450 37.21 43.56 42.25 42.25 50.41 53.29 9.570 50.41 43.56 54.76 49.00 54.76 42.25 9.690 43.56 50.41 47.61 53.29 47.61 50.41 9.810 49.00 56.25 40.96 47.61 44.89 47.61 9.930 43.56 38.44 47.61 39.69 43.56 50.41 10.050 50.41 39.69 43.56 42.25 30.25 36.00 10.170 38.44 43.56 37.21 51.84 53.29 43.56 10.290 37.21 49.00 40.96 51.84 43.56 42.25 10.410 43.56 49.00 44.89 38.44 47.61 32.49 10.530 42.25 56.25 43.56 49.00 38.44 51.84 10.650 44.89 43.56 43.56 46.24 46.24 42.25 10.770 43.56 36.00 37.21 43.56 47.61 43.56 10.890 43.56 44.89 50.41 42.25 38.44 43.56 11.010 44.89 42.25 43.56 44.89 38.44 47.61 11.130 38.44 47.61 38.44 49.00 42.25 32.49 11.250 36.00 36.00 47.61 42.25 51.84 47.61 11.370 42.25 38.44 47.61 50.41 40.96 37.21 11.490 44.89 47.61 47.61 42.25 53.29 40.96

138

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 38.44 50.41 37.21 24.01 37.21 40.96 11.730 46.24 49.00 50.41 53.29 44.89 40.96 11.850 46.24 53.29 47.61 47.61 37.21 39.69 11.970 38.44 59.29 29.16 43.56 32.49 53.29 12.090 43.56 50.41 60.84 47.61 43.56 51.84 12.210 46.24 50.41 39.69 31.36 37.21 51.84 12.330 50.41 43.56 37.21 31.36 47.61 47.61 12.450 47.61 38.44 43.56 36.00 47.61 39.69 12.570 56.25 53.29 38.44 38.44 46.24 42.25 12.690 32.49 43.56 49.00 43.56 43.56 53.29 12.810 32.49 42.25 49.00 39.69 39.69 39.69 12.930 59.29 50.41 42.25 50.41 30.25 44.89 13.050 38.44 47.61 42.25 56.25 34.81 43.56 13.170 43.56 54.76 30.25 46.24 44.89 39.69 13.290 42.25 33.64 42.25 47.61 38.44 38.44 13.410 33.64 44.89 31.36 37.21 44.89 43.56 13.530 38.44 43.56 47.61 36.00 34.81 37.21 13.650 38.44 40.96 32.49 36.00 44.89 39.69 13.770 39.69 38.44 32.49 30.25 42.25 43.56 13.890 42.25 37.21 38.44 51.84 38.44 32.49 14.010 43.56 44.89 33.64 44.89 50.41 31.36 14.130 39.69 50.41 51.84 40.96 36.00 38.44 14.250 42.25 51.84 33.64 64.00 32.49 38.44 14.370 38.44 42.25 44.89 40.96 36.00 51.84 14.490 46.24 47.61 37.21 43.56 49.00 43.56 14.610 53.29 30.25 43.56 37.21 46.24 40.96 14.730 53.29 47.61 36.00 42.25 47.61 34.81 14.850 51.84 37.21 43.56 34.81 43.56 43.56 14.970 56.25 47.61 50.41 56.25 54.76 49.00 15.090 57.76 53.29 38.44 56.25 38.44 44.89 15.210 43.56 53.29 47.61 59.29 50.41 50.41 15.330 59.29 47.61 57.76 53.29 59.29 59.29 15.450 60.84 53.29 53.29 53.29 51.84 51.84 15.570 42.25 47.61 47.61 47.61 54.76 53.29 15.690 46.24 53.29 65.61 53.29 50.41 50.41 15.810 57.76 38.44 56.25 53.29 47.61 40.96 15.930 53.29 60.84 49.00 43.56 50.41 65.61 16.050 47.61 50.41 59.29 51.84 51.84 47.61 16.170 46.24 51.84 50.41 44.89 39.69 44.89 16.290 53.29 47.61 44.89 47.61 32.49 53.29 16.410 46.24 44.89 46.24 38.44 53.29 34.81 16.530 43.56 59.29 40.96 43.56 49.00 46.24 16.650 36.00 42.25 43.56 46.24 47.61 47.61 16.770 38.44 36.00 43.56 54.76 39.69 47.61 16.890 56.25 36.00 46.24 43.56 44.89 40.96 17.010 46.24 38.44 38.44 43.56 40.96 38.44 17.130 43.56 44.89 47.61 43.56 49.00 38.44 17.250 38.44 36.00 32.49 43.56 31.36 37.21 17.370 44.89 46.24 31.36 32.49 43.56 42.25 17.490 50.41 34.81 32.49 43.56 34.81 44.89 17.610 36.00 37.21 39.69 32.49 38.44 36.00 17.730 31.36 43.56 32.49 37.21 49.00 29.16

139

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 43.56 40.96 37.21 43.56 38.44 37.21 17.970 43.56 33.64 38.44 38.44 38.44 30.25 18.090 29.16 32.49 43.56 43.56 43.56 36.00 18.210 40.96 32.49 33.64 39.69 46.24 43.56 18.330 36.00 38.44 37.21 32.49 39.69 36.00 18.450 30.25 37.21 36.00 38.44 28.09 50.41 18.570 27.04 38.44 43.56 38.44 47.61 53.29 18.690 37.21 38.44 39.69 43.56 38.44 56.25 18.810 50.41 46.24 33.64 46.24 44.89 37.21 18.930 44.89 39.69 53.29 44.89 43.56 36.00 19.050 38.44 33.64 33.64 43.56 43.56 38.44 19.170 32.49 31.36 28.09 37.21 46.24 34.81 19.290 38.44 53.29 46.24 47.61 37.21 28.09 19.410 32.49 34.81 38.44 40.96 56.25 43.56 19.530 50.41 43.56 40.96 37.21 36.00 47.61 19.650 38.44 49.00 44.89 44.89 30.25 50.41 19.770 44.89 39.69 49.00 43.56 47.61 57.76 19.890 43.56 46.24 44.89 40.96 37.21 46.24 20.010 38.44 43.56 27.04 38.44 38.44 42.25 20.130 42.25 39.69 37.21 36.00 36.00 36.00 20.250 33.64 40.96 38.44 40.96 40.96 39.69 20.370 43.56 46.24 43.56 40.96 38.44 51.84 20.490 29.16 36.00 44.89 36.00 37.21 39.69 20.610 46.24 34.81 32.49 38.44 34.81 34.81 20.730 43.56 39.69 62.41 51.84 50.41 51.84 20.850 49.00 50.41 72.25 46.24 42.25 38.44 20.970 36.00 28.09 39.69 40.96 37.21 33.64 21.090 50.41 32.49 30.25 49.00 39.69 44.89 21.210 40.96 49.00 46.24 50.41 33.64 29.16 21.330 38.44 43.56 43.56 39.69 38.44 38.44 21.450 40.96 32.49 44.89 32.49 43.56 37.21 21.570 40.96 38.44 44.89 33.64 38.44 43.56 21.690 39.69 47.61 51.84 47.61 47.61 50.41 21.810 38.44 57.76 49.00 43.56 38.44 54.76 21.930 49.00 59.29 59.29 68.89 72.25 86.49 22.050 82.81 86.49 64.00 59.29 53.29 51.84 22.170 49.00 56.25 50.41 43.56 43.56 56.25 22.290 54.76 49.00 38.44 46.24 36.00 39.69 22.410 37.21 44.89 46.24 43.56 43.56 43.56 22.530 44.89 47.61 38.44 40.96 39.69 56.25 22.650 42.25 50.41 43.56 62.41 50.41 50.41 22.770 54.76 54.76 50.41 53.29 67.24 77.44 22.890 59.29 77.44 94.09 75.69 96.04 92.16 23.010 110.25 106.09 114.49 139.24 151.29 108.16 23.130 104.04 110.25 110.25 96.04 86.49 82.81 23.250 65.61 62.41 56.25 59.29 67.24 47.61 23.370 70.56 50.41 51.84 60.84 47.61 46.24 23.490 59.29 56.25 67.24 39.69 47.61 49.00 23.610 43.56 57.76 46.24 50.41 60.84 50.41 23.730 43.56 47.61 62.41 56.25 56.25 53.29 23.850 56.25 57.76 82.81 79.21 79.21 94.09 23.970 108.16 125.44 96.04 121.00 123.21 134.56

140

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 148.84 108.16 102.01 88.36 75.69 77.44 24.210 72.25 59.29 42.25 49.00 65.61 47.61 24.330 38.44 38.44 54.76 49.00 36.00 39.69 24.450 33.64 43.56 39.69 44.89 27.04 33.64 24.570 34.81 36.00 43.56 28.09 32.49 30.25 24.690 44.89 31.36 34.81 38.44 32.49 31.36 24.810 32.49 40.96 43.56 31.36 46.24 23.04 24.930 38.44 38.44 26.01 38.44 32.49 28.09 25.050 32.49 37.21 37.21 46.24 32.49 39.69 25.170 34.81 44.89 42.25 33.64 43.56 34.81 25.290 38.44 39.69 39.69 40.96 28.09 38.44 25.410 33.64 32.49 39.69 39.69 36.00 32.49 25.530 34.81 39.69 32.49 40.96 24.01 25.00 25.650 46.24 38.44 34.81 29.16 33.64 39.69 25.770 50.41 44.89 51.84 43.56 37.21 39.69 25.890 38.44 38.44 47.61 37.21 43.56 34.81 26.010 38.44 40.96 53.29 34.81 33.64 37.21 26.130 46.24 43.56 43.56 38.44 31.36 42.25 26.250 47.61 39.69 43.56 32.49 29.16 42.25 26.370 40.96 38.44 39.69 51.84 43.56 60.84 26.490 62.41 56.25 53.29 67.24 110.25 193.21 26.610 228.01 234.09 216.09 179.56 163.84 127.69 26.730 92.16 75.69 60.84 54.76 34.81 57.76 26.850 43.56 33.64 44.89 38.44 39.69 43.56 26.970 46.24 43.56 36.00 49.00 36.00 28.09 27.090 37.21 38.44 43.56 42.25 43.56 32.49 27.210 43.56 24.01 38.44 33.64 38.44 40.96 27.330 43.56 34.81 38.44 34.81 47.61 36.00 27.450 42.25 33.64 44.89 38.44 46.24 33.64 27.570 46.24 29.16 32.49 38.44 51.84 50.41 27.690 34.81 46.24 37.21 31.36 34.81 37.21 27.810 42.25 43.56 50.41 39.69 32.49 27.04 27.930 36.00 40.96 36.00 33.64 29.16 34.81 28.050 37.21 40.96 32.49 47.61 32.49 46.24 28.170 36.00 46.24 47.61 44.89 38.44 53.29 28.290 53.29 38.44 42.25 36.00 46.24 42.25 28.410 49.00 46.24 53.29 51.84 49.00 53.29 28.530 54.76 56.25 43.56 54.76 57.76 54.76 28.650 68.89 56.25 59.29 54.76 88.36 72.25 28.770 70.56 70.56 72.25 98.01 82.81 98.01 28.890 104.04 104.04 129.96 112.36 144.00 146.41 29.010 169.00 184.96 182.25 216.09 246.49 231.04 29.130 265.69 306.25 331.24 420.25 441.00 506.25 29.250 585.64 615.04 745.29 858.49 1049.76 1239.04 29.370 1632.16 2043.04 2391.21 2401.00 2342.56 2106.81 29.490 1953.64 1672.81 1413.76 1069.29 876.16 681.21 29.610 615.04 547.56 488.41 420.25 384.16 338.56 29.730 313.29 252.81 262.44 256.00 252.81 222.01 29.850 222.01 190.44 169.00 153.76 166.41 132.25 29.970 129.96 144.00 127.69 153.76 136.89 136.89 30.090 129.96 121.00 123.21 123.21 108.16 118.81 30.210 121.00 129.96 118.81 132.25 116.64 129.96

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 134.56 148.84 148.84 139.24 153.76 153.76 30.450 190.44 182.25 204.49 228.01 216.09 272.25 30.570 275.56 320.41 334.89 327.61 408.04 453.69 30.690 510.76 595.36 712.89 800.89 979.69 1190.25 30.810 1536.64 1998.09 2809.00 3868.84 4914.01 5760.81 30.930 6021.76 5975.29 5913.61 5227.29 4356.00 3684.49 31.050 3036.01 2190.24 1780.84 1310.44 1017.61 823.69 31.170 729.00 590.49 533.61 457.96 368.64 316.84 31.290 320.41 275.56 259.21 246.49 204.49 196.00 31.410 182.25 174.24 184.96 163.84 169.00 144.00 31.530 158.76 141.61 123.21 127.69 116.64 96.04 31.650 84.64 106.09 108.16 77.44 88.36 96.04 31.770 90.25 77.44 90.25 64.00 65.61 65.61 31.890 77.44 81.00 79.21 59.29 67.24 84.64 32.010 56.25 59.29 65.61 59.29 49.00 51.84 32.130 43.56 57.76 67.24 65.61 65.61 54.76 32.250 53.29 46.24 57.76 47.61 43.56 39.69 32.370 43.56 53.29 57.76 59.29 62.41 32.49 32.490 54.76 60.84 47.61 50.41 32.49 53.29 32.610 39.69 33.64 44.89 40.96 44.89 50.41 32.730 56.25 50.41 43.56 47.61 46.24 34.81 32.850 40.96 38.44 43.56 53.29 51.84 43.56 32.970 37.21 44.89 46.24 42.25 50.41 57.76 33.090 62.41 50.41 47.61 53.29 53.29 38.44 33.210 43.56 51.84 64.00 67.24 65.61 72.25 33.330 67.24 88.36 102.01 88.36 114.49 108.16 33.450 136.89 148.84 166.41 176.89 207.36 193.21 33.570 213.16 179.56 146.41 144.00 121.00 104.04 33.690 100.00 84.64 79.21 75.69 67.24 53.29 33.810 54.76 65.61 50.41 44.89 50.41 60.84 33.930 59.29 43.56 37.21 30.25 50.41 53.29 34.050 50.41 56.25 43.56 43.56 40.96 32.49 34.170 51.84 29.16 43.56 32.49 43.56 33.64 34.290 39.69 42.25 38.44 39.69 36.00 43.56 34.410 46.24 40.96 33.64 40.96 36.00 44.89 34.530 37.21 32.49 39.69 46.24 38.44 38.44 34.650 34.81 31.36 36.00 47.61 43.56 51.84 34.770 54.76 53.29 43.56 38.44 50.41 53.29 34.890 42.25 43.56 56.25 50.41 59.29 53.29 35.010 53.29 64.00 59.29 62.41 59.29 77.44 35.130 94.09 98.01 116.64 125.44 148.84 118.81 35.250 136.89 158.76 161.29 136.89 132.25 151.29 35.370 144.00 129.96 125.44 123.21 96.04 112.36 35.490 112.36 112.36 86.49 90.25 75.69 75.69 35.610 84.64 79.21 86.49 90.25 86.49 82.81 35.730 64.00 100.00 102.01 94.09 102.01 129.96 35.850 132.25 144.00 163.84 174.24 187.69 196.00 35.970 275.56 268.96 302.76 262.44 246.49 275.56 36.090 243.36 237.16 193.21 166.41 144.00 141.61 36.210 127.69 129.96 121.00 108.16 100.00 94.09 36.330 77.44 84.64 92.16 82.81 73.96 88.36 36.450 56.25 79.21 75.69 79.21 84.64 65.61

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File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 70.56 86.49 81.00 81.00 81.00 86.49 36.690 72.25 84.64 88.36 90.25 77.44 62.41 36.810 84.64 114.49 86.49 88.36 77.44 88.36 36.930 86.49 114.49 98.01 102.01 114.49 118.81 37.050 112.36 148.84 94.09 110.25 144.00 132.25 37.170 136.89 144.00 156.25 153.76 169.00 193.21 37.290 182.25 216.09 231.04 268.96 259.21 272.25 37.410 249.64 219.04 213.16 207.36 169.00 146.41 37.530 153.76 132.25 112.36 106.09 102.01 92.16 37.650 77.44 75.69 82.81 98.01 57.76 73.96 37.770 65.61 57.76 64.00 62.41 62.41 65.61 37.890 65.61 75.69 59.29 53.29 51.84 47.61 38.010 47.61 67.24 51.84 53.29 49.00 43.56 38.130 70.56 59.29 70.56 40.96 65.61 43.56 38.250 60.84 53.29 64.00 51.84 47.61 50.41 38.370 49.00 53.29 43.56 44.89 51.84 47.61 38.490 53.29 46.24 59.29 47.61 62.41 50.41 38.610 57.76 50.41 50.41 47.61 53.29 75.69 38.730 53.29 57.76 59.29 51.84 57.76 59.29 38.850 68.89 77.44 73.96 62.41 60.84 64.00 38.970 65.61 75.69 92.16 86.49 90.25 96.04 39.090 86.49 94.09 84.64 88.36 121.00 129.96 39.210 132.25 148.84 118.81 163.84 190.44 182.25 39.330 252.81 262.44 252.81 324.00 357.21 400.00 39.450 466.56 428.49 441.00 376.36 345.96 353.44 39.570 345.96 292.41 272.25 262.44 216.09 204.49 39.690 179.56 228.01 198.81 187.69 210.25 201.64 39.810 193.21 210.25 182.25 196.00 198.81 171.61 39.930 169.00 179.56 187.69 166.41 144.00 163.84 40.050 125.44 136.89 123.21 104.04 84.64 92.16 40.170 82.81 84.64 86.49 68.89 75.69 75.69 40.290 59.29 70.56 67.24 60.84 62.41 75.69 40.410 54.76 51.84 62.41 65.61 47.61 51.84 40.530 92.16 62.41 62.41 70.56 82.81 86.49 40.650 82.81 82.81 73.96 104.04 96.04 108.16 40.770 108.16 112.36 123.21 151.29 129.96 158.76 40.890 174.24 216.09 213.16 265.69 282.24 327.61 41.010 388.09 484.00 571.21 756.25 806.56 985.96 41.130 942.49 912.04 835.21 756.25 729.00 670.81 41.250 676.00 552.25 416.16 349.69 282.24 249.64 41.370 234.09 204.49 171.61 144.00 148.84 132.25 41.490 110.25 106.09 90.25 84.64 86.49 88.36 41.610 84.64 86.49 82.81 65.61 60.84 67.24 41.730 65.61 62.41 70.56 51.84 59.29 42.25 41.850 44.89 43.56 57.76 51.84 60.84 50.41 41.970 54.76 51.84 62.41 47.61 47.61 51.84 42.090 47.61 44.89 56.25 43.56 54.76 38.44 42.210 39.69 38.44 50.41 51.84 39.69 51.84 42.330 57.76 67.24 51.84 57.76 59.29 64.00 42.450 56.25 54.76 54.76 60.84 62.41 50.41 42.570 50.41 49.00 64.00 53.29 70.56 60.84 42.690 51.84 65.61 62.41 67.24 54.76 65.61

143

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 59.29 81.00 75.69 75.69 84.64 102.01 42.930 104.04 108.16 108.16 134.56 112.36 151.29 43.050 176.89 201.64 262.44 292.41 320.41 376.36 43.170 436.81 392.04 400.00 400.00 364.81 338.56 43.290 345.96 324.00 292.41 249.64 228.01 193.21 43.410 182.25 176.89 163.84 125.44 148.84 139.24 43.530 129.96 139.24 112.36 129.96 114.49 116.64 43.650 123.21 129.96 139.24 151.29 139.24 156.25 43.770 136.89 146.41 153.76 141.61 148.84 136.89 43.890 134.56 136.89 102.01 104.04 100.00 96.04 44.010 90.25 96.04 77.44 73.96 86.49 73.96 44.130 72.25 70.56 65.61 64.00 70.56 67.24 44.250 65.61 75.69 75.69 62.41 62.41 67.24 44.370 62.41 51.84 70.56 84.64 72.25 62.41 44.490 67.24 70.56 88.36 88.36 81.00 108.16 44.610 86.49 96.04 108.16 108.16 116.64 146.41 44.730 139.24 148.84 216.09 228.01 243.36 292.41 44.850 349.69 408.04 470.89 424.36 449.44 396.01 44.970 364.81 384.16 392.04 349.69 295.84 285.61 45.090 237.16 216.09 196.00 174.24 161.29 136.89 45.210 123.21 127.69 108.16 98.01 86.49 79.21 45.330 94.09 60.84 65.61 68.89 62.41 67.24 45.450 62.41 59.29 84.64 57.76 62.41 53.29 45.570 67.24 77.44 40.96 62.41 53.29 65.61 45.690 50.41 51.84 54.76 60.84 65.61 57.76 45.810 59.29 51.84 54.76 53.29 53.29 64.00 45.930 65.61 49.00 53.29 50.41 56.25 50.41 46.050 47.61 59.29 70.56 57.76 59.29 54.76 46.170 54.76 64.00 62.41 67.24 62.41 65.61 46.290 62.41 50.41 84.64 72.25 70.56 72.25 46.410 82.81 84.64 70.56 88.36 86.49 96.04 46.530 84.64 84.64 88.36 98.01 88.36 104.04 46.650 86.49 90.25 94.09 90.25 102.01 88.36 46.770 92.16 88.36 118.81 129.96 100.00 100.00 46.890 108.16 123.21 104.04 114.49 125.44 144.00 47.010 132.25 151.29 174.24 176.89 179.56 176.89 47.130 204.49 184.96 201.64 190.44 228.01 207.36 47.250 213.16 240.25 237.16 246.49 252.81 246.49 47.370 272.25 282.24 327.61 368.64 484.00 696.96 47.490 800.89 800.89 630.01 566.44 524.41 533.61 47.610 576.00 538.24 466.56 368.64 361.00 292.41 47.730 272.25 262.44 234.09 225.00 225.00 184.96 47.850 196.00 187.69 176.89 174.24 153.76 163.84 47.970 166.41 158.76 146.41 161.29 153.76 174.24 48.090 169.00 153.76 187.69 163.84 156.25 184.96 48.210 169.00 179.56 184.96 184.96 171.61 182.25 48.330 204.49 231.04 246.49 278.89 275.56 334.89 48.450 436.81 506.25 510.76 424.36 428.49 432.64 48.570 457.96 479.61 400.00 364.81 324.00 285.61 48.690 309.76 268.96 231.04 225.00 228.01 207.36 48.810 174.24 237.16 193.21 161.29 190.44 179.56 48.930 171.61 144.00 141.61 151.29 169.00 153.76

144

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 141.61 141.61 158.76 146.41 158.76 169.00 49.170 136.89 169.00 187.69 187.69 144.00 161.29 49.290 171.61 174.24 158.76 151.29 169.00 139.24 49.410 171.61 134.56 136.89 123.21 121.00 112.36 49.530 106.09 102.01 100.00 90.25 90.25 134.56 49.650 100.00 84.64 92.16 88.36 90.25 79.21 49.770 88.36 92.16 98.01 92.16 102.01 108.16 49.890 108.16 88.36 88.36 114.49 90.25 106.09 50.010 118.81 127.69 132.25 127.69 156.25 132.25 50.130 158.76 141.61 184.96 161.29 156.25 171.61 50.250 204.49 231.04 225.00 243.36 237.16 285.61 50.370 327.61 334.89 420.25 479.61 580.81 610.09 50.490 630.01 676.00 723.61 645.16 645.16 571.21 50.610 630.01 580.81 529.00 492.84 484.00 424.36 50.730 380.25 388.09 361.00 338.56 338.56 338.56 50.850 342.25 327.61 368.64 396.01 441.00 436.81 50.970 506.25 556.96 615.04 625.00 655.36 665.64 51.090 650.25 585.64 620.01 519.84 547.56 501.76 51.210 524.41 484.00 428.49 408.04 334.89 306.25 51.330 275.56 246.49 246.49 196.00 222.01 174.24 51.450 169.00 176.89 144.00 136.89 129.96 118.81 51.570 100.00 96.04 106.09 86.49 75.69 96.04 51.690 96.04 106.09 82.81 64.00 62.41 67.24 51.810 65.61 68.89 67.24 62.41 62.41 59.29 51.930 53.29 51.84 67.24 59.29 59.29 53.29 52.050 59.29 62.41 56.25 54.76 44.89 49.00 52.170 54.76 51.84 65.61 65.61 54.76 59.29 52.290 64.00 53.29 56.25 59.29 65.61 51.84 52.410 67.24 56.25 50.41 44.89 88.36 40.96 52.530 64.00 56.25 50.41 46.24 40.96 64.00 52.650 38.44 46.24 46.24 36.00 37.21 53.29 52.770 50.41 42.25 42.25 38.44 40.96 44.89 52.890 47.61 46.24 38.44 30.25 43.56 47.61 53.010 39.69 56.25 59.29 49.00 43.56 44.89 53.130 54.76 42.25 42.25 53.29 29.16 39.69 53.250 37.21 49.00 40.96 43.56 43.56 38.44 53.370 38.44 28.09 42.25 27.04 37.21 38.44 53.490 40.96 49.00 36.00 33.64 44.89 51.84 53.610 43.56 37.21 43.56 38.44 34.81 40.96 53.730 32.49 33.64 51.84 38.44 42.25 37.21 53.850 38.44 40.96 38.44 50.41 36.00 38.44 53.970 47.61 43.56 46.24 47.61 37.21 33.64 54.090 30.25 43.56 47.61 29.16 43.56 34.81 54.210 34.81 44.89 36.00 36.00 46.24 36.00 54.330 50.41 34.81 33.64 30.25 47.61 49.00 54.450 39.69 24.01 47.61 43.56 44.89 42.25 54.570 34.81 29.16 32.49 38.44 36.00 42.25 54.690 33.64 33.64 39.69 47.61 50.41 46.24 54.810 32.49 46.24 43.56 32.49 42.25 37.21 54.930 33.64 39.69 40.96 38.44 34.81 22.09 55.050 33.64 43.56 38.44 38.44 43.56 43.56 55.170 46.24 37.21 56.25 36.00 42.25 40.96

145

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 43.56 34.81 36.00 38.44 36.00 43.56 55.410 30.25 36.00 43.56 32.49 43.56 46.24 55.530 43.56 28.09 38.44 38.44 42.25 38.44 55.650 39.69 39.69 40.96 46.24 43.56 43.56 55.770 30.25 38.44 40.96 49.00 49.00 43.56 55.890 44.89 59.29 37.21 40.96 50.41 47.61 56.010 42.25 46.24 30.25 43.56 42.25 38.44 56.130 39.69 42.25 50.41 47.61 47.61 47.61 56.250 54.76 53.29 49.00 56.25 70.56 65.61 56.370 50.41 72.25 56.25 59.29 59.29 75.69 56.490 88.36 77.44 102.01 108.16 116.64 136.89 56.610 108.16 116.64 127.69 96.04 102.01 86.49 56.730 108.16 92.16 106.09 96.04 94.09 81.00 56.850 81.00 70.56 72.25 82.81 88.36 81.00 56.970 62.41 72.25 77.44 75.69 72.25 82.81 57.090 90.25 106.09 86.49 102.01 82.81 112.36 57.210 114.49 96.04 127.69 123.21 136.89 136.89 57.330 166.41 201.64 210.25 228.01 225.00 256.00 57.450 204.49 225.00 210.25 187.69 210.25 213.16 57.570 198.81 190.44 161.29 146.41 141.61 116.64 57.690 121.00 86.49 98.01 86.49 112.36 88.36 57.810 110.25 94.09 90.25 77.44 73.96 86.49 57.930 92.16 82.81 100.00 94.09 84.64 86.49 58.050 86.49 92.16 90.25 82.81 75.69 72.25 58.170 75.69 79.21 94.09 86.49 65.61 72.25 58.290 64.00 84.64 81.00 67.24 84.64 73.96 58.410 72.25 54.76 68.89 60.84 70.56 72.25 58.530 65.61 68.89 88.36 75.69 75.69 75.69 58.650 81.00 90.25 84.64 75.69 94.09 88.36 58.770 108.16 106.09 112.36 139.24 148.84 163.84 58.890 139.24 134.56 136.89 127.69 136.89 108.16 59.010 132.25 98.01 106.09 102.01 92.16 106.09 59.130 92.16 75.69 96.04 88.36 65.61 75.69 59.250 72.25 64.00 72.25 65.61 81.00 62.41 59.370 81.00 84.64 92.16 90.25 86.49 73.96 59.490 82.81 100.00 90.25 114.49 125.44 127.69 59.610 106.09 144.00 151.29 176.89 207.36 213.16 59.730 234.09 210.25 240.25 234.09 213.16 219.04 59.850 204.49 216.09 216.09 176.89 193.21 204.49 59.970 184.96 148.84 176.89 166.41 144.00 132.25 60.090 132.25 100.00 102.01 82.81 108.16 98.01 60.210 84.64 100.00 77.44 82.81 81.00 100.00 60.330 75.69 72.25 90.25 79.21 75.69 100.00 60.450 79.21 70.56 82.81 96.04 92.16 86.49 60.570 118.81 129.96 121.00 139.24 151.29 148.84 60.690 158.76 169.00 156.25 136.89 144.00 148.84 60.810 136.89 136.89 153.76 136.89 166.41 153.76 60.930 169.00 153.76 156.25 182.25 151.29 158.76 61.050 125.44 144.00 144.00 136.89 169.00 129.96 61.170 123.21 136.89 125.44 129.96 127.69 121.00 61.290 106.09 121.00 116.64 129.96 144.00 118.81 61.410 144.00 112.36 116.64 100.00 112.36 104.04

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File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 108.16 98.01 79.21 98.01 77.44 92.16 61.650 96.04 72.25 88.36 72.25 70.56 88.36 61.770 62.41 64.00 65.61 72.25 72.25 75.69 61.890 72.25 77.44 75.69 86.49 72.25 79.21 62.010 72.25 73.96 79.21 53.29 84.64 72.25 62.130 75.69 65.61 81.00 75.69 65.61 72.25 62.250 60.84 62.41 50.41 50.41 49.00 75.69 62.370 47.61 57.76 42.25 56.25 50.41 53.29 62.490 67.24 59.29 57.76 51.84 49.00 47.61 62.610 53.29 59.29 49.00 64.00 67.24 50.41 62.730 64.00 64.00 56.25 59.29 72.25 86.49 62.850 62.41 62.41 62.41 88.36 77.44 96.04 62.970 67.24 84.64 96.04 100.00 100.00 100.00 63.090 108.16 106.09 108.16 100.00 125.44 132.25 63.210 129.96 151.29 153.76 171.61 158.76 163.84 63.330 179.56 210.25 210.25 210.25 207.36 222.01 63.450 213.16 187.69 198.81 198.81 176.89 156.25 63.570 153.76 174.24 144.00 129.96 144.00 96.04 63.690 127.69 106.09 106.09 92.16 98.01 86.49 63.810 79.21 86.49 79.21 94.09 88.36 62.41 63.930 106.09 81.00 86.49 86.49 84.64 79.21 64.050 82.81 88.36 77.44 86.49 82.81 92.16 64.170 94.09 84.64 104.04 94.09 110.25 96.04 64.290 121.00 123.21 139.24 182.25 156.25 213.16 64.410 216.09 219.04 228.01 225.00 249.64 219.04 64.530 243.36 201.64 210.25 262.44 237.16 246.49 64.650 240.25 231.04 252.81 225.00 225.00 225.00 64.770 196.00 207.36 179.56 182.25 201.64 176.89 64.890 174.24 187.69 158.76 174.24 158.76 174.24 65.010 184.96 182.25 193.21 210.25 198.81 179.56 65.130 198.81 198.81 196.00 163.84 176.89 169.00 65.250 176.89 196.00 187.69 158.76 156.25 166.41 65.370 153.76 141.61 139.24 144.00 123.21 134.56 65.490 125.44 123.21 134.56 125.44 129.96 136.89 65.610 136.89 146.41 134.56 156.25 139.24 144.00 65.730 144.00 127.69 108.16 108.16 129.96 125.44 65.850 116.64 136.89 123.21 116.64 100.00 132.25 65.970 116.64 139.24 141.61 112.36 144.00 129.96 66.090 144.00 116.64 116.64 116.64 110.25 108.16 66.210 112.36 108.16 108.16 102.01 98.01 94.09 66.330 79.21 98.01 82.81 68.89 86.49 70.56 66.450 73.96 68.89 75.69 56.25 62.41 70.56 66.570 70.56 65.61 50.41 67.24 56.25 56.25 66.690 60.84 62.41 54.76 72.25 59.29 68.89 66.810 50.41 54.76 77.44 59.29 82.81 67.24 66.930 77.44 70.56 72.25 75.69 72.25 84.64 67.050 84.64 90.25 86.49 104.04 96.04 102.01 67.170 134.56 108.16 139.24 134.56 158.76 163.84 67.290 204.49 184.96 219.04 246.49 234.09 252.81 67.410 216.09 240.25 198.81 171.61 182.25 174.24 67.530 158.76 148.84 174.24 174.24 153.76 153.76 67.650 123.21 108.16 104.04 112.36 88.36 102.01

147

File: JC5.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 79.21 104.04 70.56 77.44 72.25 82.81 67.890 65.61 67.24 62.41 64.00 62.41 70.56 68.010 60.84 57.76 57.76 64.00 70.56 62.41 68.130 60.84 62.41 68.89 67.24 57.76 47.61 68.250 54.76 56.25 59.29 53.29 49.00 50.41 68.370 65.61 59.29 54.76 38.44 56.25 62.41 68.490 53.29 39.69 53.29 47.61 38.44 62.41 68.610 47.61 32.49 56.25 56.25 51.84 42.25 68.730 38.44 47.61 51.84 50.41 39.69 39.69 68.850 42.25 43.56 43.56 56.25 50.41 47.61 68.970 57.76 62.41 44.89 50.41 54.76 44.89 69.090 53.29 62.41 68.89 56.25 50.41 72.25 69.210 70.56 53.29 64.00 75.69 53.29 60.84 69.330 53.29 67.24 70.56 65.61 70.56 65.61 69.450 56.25 59.29 64.00 68.89 62.41 79.21 69.570 51.84 62.41 65.61 56.25 60.84 50.41 69.690 64.00 53.29 65.61 53.29 60.84 62.41 69.810 75.69 59.29 79.21 79.21 68.89 57.76 69.930 84.64 82.81 70.56 79.21 _

148

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC6 Data measured at: 24-Jan-2011 15:54:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 11214.81 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 123.21 118.81 123.21 112.36 129.96 104.04 2.130 112.36 98.01 100.00 104.04 92.16 106.09 2.250 106.09 96.04 102.01 104.04 96.04 86.49 2.370 75.69 92.16 72.25 72.25 88.36 70.56 2.490 77.44 72.25 84.64 79.21 86.49 75.69 2.610 75.69 72.25 68.89 70.56 75.69 79.21 2.730 72.25 75.69 62.41 70.56 70.56 60.84 2.850 86.49 67.24 72.25 64.00 77.44 64.00 2.970 62.41 70.56 64.00 67.24 65.61 65.61 3.090 67.24 67.24 62.41 75.69 68.89 72.25 3.210 67.24 53.29 54.76 62.41 54.76 72.25 3.330 62.41 72.25 59.29 77.44 75.69 67.24 3.450 60.84 67.24 82.81 53.29 70.56 59.29 3.570 62.41 59.29 84.64 50.41 50.41 56.25 3.690 56.25 65.61 56.25 57.76 72.25 62.41 3.810 47.61 59.29 53.29 62.41 50.41 62.41 3.930 59.29 65.61 65.61 56.25 50.41 65.61 4.050 70.56 53.29 47.61 62.41 59.29 50.41 4.170 56.25 65.61 64.00 64.00 50.41 56.25 4.290 59.29 65.61 43.56 62.41 50.41 64.00 4.410 59.29 59.29 56.25 59.29 59.29 62.41 4.530 50.41 60.84 59.29 70.56 46.24 67.24 4.650 65.61 62.41 65.61 56.25 68.89 54.76 4.770 53.29 65.61 54.76 57.76 50.41 59.29 4.890 56.25 46.24 60.84 59.29 51.84 77.44 5.010 62.41 65.61 56.25 50.41 51.84 56.25 5.130 53.29 43.56 64.00 59.29 59.29 50.41 5.250 46.24 67.24 54.76 59.29 56.25 59.29

149

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 56.25 54.76 65.61 53.29 53.29 65.61 5.490 73.96 54.76 73.96 54.76 56.25 72.25 5.610 53.29 65.61 50.41 53.29 67.24 50.41 5.730 43.56 53.29 53.29 54.76 49.00 56.25 5.850 59.29 60.84 56.25 62.41 43.56 56.25 5.970 59.29 49.00 68.89 50.41 62.41 51.84 6.090 54.76 53.29 62.41 50.41 59.29 57.76 6.210 49.00 56.25 53.29 47.61 47.61 59.29 6.330 59.29 49.00 50.41 53.29 49.00 43.56 6.450 44.89 60.84 44.89 47.61 65.61 53.29 6.570 59.29 56.25 72.25 49.00 50.41 38.44 6.690 59.29 59.29 54.76 40.96 56.25 50.41 6.810 50.41 44.89 47.61 50.41 57.76 53.29 6.930 38.44 50.41 53.29 50.41 54.76 70.56 7.050 59.29 56.25 75.69 54.76 47.61 46.24 7.170 38.44 56.25 50.41 49.00 51.84 42.25 7.290 50.41 49.00 62.41 56.25 53.29 65.61 7.410 53.29 67.24 54.76 50.41 57.76 37.21 7.530 51.84 53.29 39.69 51.84 51.84 44.89 7.650 53.29 59.29 53.29 59.29 53.29 47.61 7.770 49.00 36.00 54.76 53.29 67.24 47.61 7.890 47.61 53.29 46.24 60.84 54.76 64.00 8.010 39.69 67.24 56.25 57.76 49.00 53.29 8.130 62.41 37.21 53.29 50.41 44.89 47.61 8.250 47.61 46.24 37.21 40.96 47.61 49.00 8.370 50.41 59.29 47.61 51.84 46.24 53.29 8.490 39.69 59.29 50.41 43.56 65.61 54.76 8.610 43.56 62.41 57.76 54.76 53.29 37.21 8.730 51.84 43.56 67.24 67.24 49.00 56.25 8.850 47.61 38.44 53.29 47.61 39.69 47.61 8.970 47.61 59.29 38.44 37.21 34.81 53.29 9.090 43.56 38.44 50.41 50.41 57.76 50.41 9.210 46.24 57.76 56.25 53.29 43.56 50.41 9.330 49.00 46.24 47.61 56.25 59.29 60.84 9.450 34.81 49.00 57.76 62.41 43.56 57.76 9.570 51.84 50.41 40.96 59.29 51.84 51.84 9.690 46.24 43.56 47.61 43.56 46.24 42.25 9.810 40.96 39.69 47.61 43.56 56.25 44.89 9.930 59.29 43.56 39.69 50.41 56.25 40.96 10.050 49.00 49.00 46.24 46.24 57.76 50.41 10.170 62.41 46.24 57.76 50.41 57.76 53.29 10.290 67.24 54.76 42.25 47.61 47.61 47.61 10.410 51.84 60.84 46.24 43.56 43.56 39.69 10.530 59.29 34.81 44.89 44.89 47.61 31.36 10.650 53.29 40.96 53.29 50.41 56.25 39.69 10.770 47.61 42.25 47.61 54.76 56.25 56.25 10.890 56.25 60.84 134.56 46.24 38.44 51.84 11.010 49.00 53.29 47.61 47.61 50.41 39.69 11.130 50.41 46.24 53.29 46.24 53.29 38.44 11.250 50.41 50.41 43.56 47.61 40.96 53.29 11.370 38.44 44.89 49.00 32.49 47.61 43.56 11.490 59.29 44.89 49.00 44.89 51.84 46.24

150

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 59.29 67.24 39.69 46.24 38.44 50.41 11.730 43.56 49.00 46.24 37.21 38.44 47.61 11.850 57.76 57.76 49.00 42.25 50.41 50.41 11.970 43.56 57.76 50.41 50.41 53.29 44.89 12.090 36.00 43.56 44.89 46.24 47.61 43.56 12.210 39.69 46.24 56.25 46.24 50.41 46.24 12.330 53.29 51.84 47.61 43.56 43.56 50.41 12.450 34.81 34.81 43.56 40.96 34.81 34.81 12.570 50.41 49.00 46.24 39.69 32.49 43.56 12.690 42.25 47.61 50.41 50.41 42.25 46.24 12.810 54.76 43.56 51.84 33.64 43.56 25.00 12.930 47.61 38.44 47.61 47.61 43.56 43.56 13.050 38.44 40.96 43.56 38.44 32.49 39.69 13.170 53.29 33.64 38.44 47.61 38.44 46.24 13.290 42.25 53.29 43.56 39.69 53.29 43.56 13.410 37.21 38.44 50.41 39.69 38.44 38.44 13.530 38.44 34.81 42.25 32.49 31.36 50.41 13.650 43.56 43.56 38.44 30.25 39.69 42.25 13.770 51.84 47.61 37.21 38.44 46.24 39.69 13.890 50.41 40.96 50.41 40.96 36.00 46.24 14.010 42.25 36.00 56.25 47.61 37.21 47.61 14.130 43.56 47.61 31.36 39.69 43.56 34.81 14.250 44.89 44.89 46.24 29.16 42.25 32.49 14.370 29.16 50.41 50.41 47.61 43.56 43.56 14.490 42.25 34.81 54.76 27.04 38.44 56.25 14.610 39.69 47.61 38.44 34.81 40.96 32.49 14.730 37.21 49.00 47.61 36.00 42.25 47.61 14.850 37.21 43.56 33.64 43.56 33.64 38.44 14.970 53.29 47.61 40.96 44.89 42.25 43.56 15.090 38.44 54.76 54.76 47.61 43.56 50.41 15.210 50.41 51.84 44.89 50.41 49.00 44.89 15.330 46.24 44.89 43.56 50.41 43.56 50.41 15.450 59.29 47.61 53.29 57.76 62.41 56.25 15.570 42.25 56.25 50.41 47.61 56.25 49.00 15.690 47.61 53.29 53.29 40.96 53.29 59.29 15.810 67.24 50.41 57.76 53.29 57.76 62.41 15.930 67.24 47.61 47.61 62.41 44.89 60.84 16.050 51.84 54.76 44.89 59.29 70.56 65.61 16.170 53.29 53.29 56.25 59.29 51.84 57.76 16.290 50.41 53.29 40.96 44.89 56.25 47.61 16.410 47.61 59.29 49.00 56.25 56.25 44.89 16.530 42.25 59.29 56.25 54.76 44.89 37.21 16.650 51.84 43.56 40.96 51.84 39.69 44.89 16.770 29.16 50.41 39.69 44.89 50.41 56.25 16.890 34.81 47.61 57.76 46.24 53.29 40.96 17.010 56.25 44.89 34.81 37.21 44.89 42.25 17.130 37.21 29.16 37.21 53.29 47.61 53.29 17.250 56.25 50.41 40.96 43.56 37.21 30.25 17.370 36.00 60.84 46.24 46.24 36.00 46.24 17.490 40.96 47.61 38.44 36.00 38.44 50.41 17.610 43.56 44.89 47.61 49.00 47.61 57.76 17.730 46.24 49.00 51.84 39.69 34.81 42.25

151

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 53.29 47.61 47.61 37.21 40.96 31.36 17.970 50.41 46.24 43.56 43.56 43.56 43.56 18.090 44.89 38.44 33.64 38.44 38.44 53.29 18.210 51.84 40.96 33.64 36.00 32.49 39.69 18.330 43.56 39.69 43.56 36.00 31.36 38.44 18.450 46.24 42.25 33.64 37.21 49.00 47.61 18.570 28.09 42.25 40.96 30.25 49.00 30.25 18.690 38.44 34.81 47.61 29.16 38.44 53.29 18.810 49.00 53.29 42.25 34.81 59.29 36.00 18.930 34.81 34.81 47.61 39.69 46.24 39.69 19.050 46.24 36.00 47.61 43.56 47.61 36.00 19.170 33.64 64.00 43.56 39.69 46.24 47.61 19.290 31.36 29.16 37.21 38.44 28.09 51.84 19.410 38.44 32.49 43.56 33.64 34.81 38.44 19.530 38.44 43.56 44.89 36.00 43.56 40.96 19.650 47.61 38.44 50.41 38.44 47.61 39.69 19.770 50.41 32.49 32.49 46.24 36.00 46.24 19.890 33.64 32.49 47.61 38.44 32.49 47.61 20.010 44.89 50.41 38.44 49.00 33.64 43.56 20.130 47.61 47.61 43.56 38.44 38.44 39.69 20.250 47.61 46.24 42.25 38.44 39.69 47.61 20.370 46.24 47.61 46.24 37.21 43.56 32.49 20.490 50.41 44.89 34.81 32.49 53.29 49.00 20.610 42.25 43.56 51.84 47.61 47.61 34.81 20.730 68.89 67.24 75.69 82.81 82.81 98.01 20.850 112.36 110.25 88.36 72.25 59.29 56.25 20.970 59.29 54.76 82.81 57.76 70.56 59.29 21.090 64.00 70.56 72.25 79.21 62.41 77.44 21.210 84.64 82.81 64.00 65.61 79.21 64.00 21.330 60.84 67.24 65.61 46.24 56.25 47.61 21.450 56.25 46.24 47.61 47.61 49.00 42.25 21.570 57.76 53.29 50.41 36.00 50.41 50.41 21.690 47.61 60.84 51.84 49.00 56.25 50.41 21.810 50.41 54.76 62.41 77.44 64.00 62.41 21.930 86.49 86.49 96.04 98.01 121.00 110.25 22.050 94.09 82.81 59.29 57.76 65.61 46.24 22.170 54.76 62.41 57.76 33.64 40.96 44.89 22.290 50.41 46.24 32.49 38.44 50.41 43.56 22.410 36.00 42.25 36.00 43.56 30.25 37.21 22.530 34.81 31.36 51.84 40.96 43.56 39.69 22.650 37.21 36.00 34.81 38.44 33.64 39.69 22.770 50.41 43.56 53.29 42.25 47.61 33.64 22.890 44.89 53.29 42.25 38.44 30.25 42.25 23.010 32.49 39.69 43.56 47.61 51.84 33.64 23.130 43.56 33.64 29.16 38.44 42.25 32.49 23.250 32.49 33.64 56.25 34.81 38.44 34.81 23.370 43.56 36.00 43.56 42.25 42.25 33.64 23.490 46.24 37.21 32.49 39.69 34.81 47.61 23.610 38.44 51.84 39.69 39.69 37.21 47.61 23.730 33.64 53.29 50.41 50.41 60.84 54.76 23.850 59.29 67.24 86.49 88.36 108.16 110.25 23.970 174.24 204.49 213.16 225.00 249.64 213.16

152

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 153.76 127.69 127.69 84.64 70.56 75.69 24.210 42.25 67.24 47.61 54.76 39.69 54.76 24.330 50.41 42.25 43.56 43.56 43.56 39.69 24.450 38.44 38.44 44.89 37.21 43.56 33.64 24.570 30.25 40.96 57.76 49.00 19.36 32.49 24.690 36.00 46.24 37.21 38.44 51.84 31.36 24.810 37.21 46.24 47.61 32.49 43.56 31.36 24.930 27.04 46.24 37.21 32.49 39.69 44.89 25.050 36.00 50.41 47.61 34.81 32.49 40.96 25.170 33.64 39.69 32.49 44.89 30.25 28.09 25.290 47.61 47.61 47.61 42.25 47.61 39.69 25.410 38.44 47.61 43.56 38.44 50.41 29.16 25.530 32.49 38.44 57.76 36.00 38.44 30.25 25.650 33.64 32.49 42.25 33.64 38.44 40.96 25.770 38.44 40.96 42.25 50.41 37.21 44.89 25.890 36.00 43.56 38.44 42.25 50.41 24.01 26.010 39.69 43.56 39.69 47.61 38.44 38.44 26.130 43.56 42.25 28.09 38.44 40.96 40.96 26.250 50.41 50.41 46.24 43.56 50.41 32.49 26.370 43.56 44.89 43.56 37.21 43.56 59.29 26.490 77.44 86.49 90.25 102.01 123.21 161.29 26.610 166.41 141.61 129.96 116.64 86.49 72.25 26.730 53.29 60.84 42.25 42.25 43.56 38.44 26.850 28.09 34.81 44.89 39.69 43.56 37.21 26.970 40.96 33.64 53.29 36.00 38.44 47.61 27.090 33.64 28.09 37.21 38.44 34.81 34.81 27.210 42.25 36.00 43.56 38.44 36.00 38.44 27.330 30.25 31.36 34.81 33.64 36.00 32.49 27.450 31.36 40.96 37.21 38.44 33.64 36.00 27.570 38.44 32.49 38.44 32.49 38.44 32.49 27.690 32.49 36.00 47.61 40.96 42.25 42.25 27.810 33.64 37.21 37.21 30.25 49.00 33.64 27.930 34.81 30.25 27.04 49.00 38.44 39.69 28.050 50.41 51.84 29.16 33.64 33.64 33.64 28.170 31.36 38.44 42.25 43.56 42.25 33.64 28.290 22.09 29.16 37.21 40.96 38.44 38.44 28.410 29.16 34.81 38.44 47.61 40.96 39.69 28.530 39.69 50.41 42.25 31.36 32.49 34.81 28.650 37.21 32.49 34.81 51.84 34.81 31.36 28.770 33.64 36.00 24.01 51.84 42.25 43.56 28.890 39.69 43.56 51.84 44.89 38.44 30.25 29.010 44.89 50.41 42.25 40.96 44.89 42.25 29.130 50.41 50.41 43.56 56.25 59.29 59.29 29.250 56.25 59.29 75.69 94.09 98.01 110.25 29.370 129.96 169.00 153.76 187.69 139.24 129.96 29.490 125.44 104.04 81.00 62.41 67.24 65.61 29.610 56.25 62.41 50.41 36.00 47.61 75.69 29.730 59.29 47.61 65.61 47.61 60.84 53.29 29.850 62.41 64.00 50.41 54.76 62.41 72.25 29.970 62.41 72.25 65.61 65.61 59.29 65.61 30.090 59.29 68.89 75.69 72.25 75.69 92.16 30.210 92.16 82.81 106.09 96.04 98.01 108.16

153

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 125.44 141.61 156.25 153.76 174.24 193.21 30.450 225.00 256.00 278.89 252.81 292.41 361.00 30.570 357.21 432.64 466.56 576.00 635.04 739.84 30.690 870.25 1024.00 1274.49 1722.25 2209.00 3003.04 30.810 3906.25 5227.29 6889.00 8519.29 10000.00 11214.81 30.930 11193.64 10774.44 9120.25 7832.25 6384.01 4900.00 31.050 3684.49 2570.49 1755.61 1339.56 1056.25 812.25 31.170 655.36 625.00 529.00 441.00 380.25 316.84 31.290 309.76 292.41 246.49 204.49 193.21 193.21 31.410 163.84 174.24 153.76 151.29 141.61 112.36 31.530 90.25 98.01 110.25 96.04 100.00 106.09 31.650 96.04 88.36 88.36 96.04 94.09 77.44 31.770 86.49 88.36 75.69 72.25 68.89 75.69 31.890 81.00 70.56 88.36 68.89 73.96 79.21 32.010 82.81 81.00 70.56 65.61 67.24 64.00 32.130 72.25 62.41 62.41 65.61 64.00 65.61 32.250 56.25 68.89 59.29 50.41 53.29 53.29 32.370 56.25 60.84 56.25 56.25 49.00 47.61 32.490 42.25 62.41 47.61 50.41 60.84 47.61 32.610 47.61 43.56 42.25 56.25 53.29 57.76 32.730 59.29 44.89 70.56 46.24 67.24 47.61 32.850 54.76 65.61 60.84 60.84 59.29 67.24 32.970 62.41 47.61 70.56 88.36 67.24 73.96 33.090 77.44 77.44 104.04 82.81 86.49 102.01 33.210 98.01 79.21 112.36 96.04 102.01 125.44 33.330 121.00 127.69 163.84 196.00 187.69 249.64 33.450 289.00 295.84 338.56 306.25 357.21 306.25 33.570 285.61 259.21 219.04 141.61 158.76 123.21 33.690 96.04 94.09 81.00 79.21 54.76 46.24 33.810 50.41 47.61 51.84 40.96 56.25 47.61 33.930 51.84 67.24 49.00 62.41 59.29 43.56 34.050 47.61 43.56 39.69 36.00 39.69 50.41 34.170 43.56 53.29 43.56 42.25 50.41 46.24 34.290 32.49 37.21 31.36 38.44 50.41 40.96 34.410 42.25 43.56 49.00 46.24 59.29 53.29 34.530 56.25 56.25 39.69 36.00 62.41 64.00 34.650 43.56 53.29 47.61 56.25 53.29 57.76 34.770 54.76 64.00 53.29 65.61 49.00 67.24 34.890 56.25 56.25 50.41 65.61 54.76 56.25 35.010 59.29 72.25 72.25 90.25 88.36 92.16 35.130 129.96 129.96 176.89 174.24 204.49 249.64 35.250 275.56 299.29 338.56 327.61 306.25 265.69 35.370 228.01 210.25 198.81 179.56 146.41 127.69 35.490 82.81 92.16 84.64 92.16 79.21 70.56 35.610 65.61 72.25 65.61 59.29 56.25 62.41 35.730 51.84 51.84 64.00 56.25 47.61 53.29 35.850 53.29 59.29 56.25 59.29 38.44 53.29 35.970 60.84 49.00 57.76 68.89 53.29 51.84 36.090 62.41 57.76 60.84 64.00 59.29 51.84 36.210 56.25 53.29 53.29 64.00 47.61 53.29 36.330 47.61 56.25 67.24 62.41 77.44 82.81 36.450 84.64 96.04 102.01 98.01 114.49 136.89

154

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 106.09 112.36 79.21 96.04 102.01 106.09 36.690 98.01 92.16 90.25 88.36 84.64 96.04 36.810 84.64 92.16 108.16 84.64 90.25 84.64 36.930 82.81 82.81 75.69 70.56 88.36 88.36 37.050 92.16 102.01 92.16 96.04 112.36 139.24 37.170 121.00 182.25 182.25 193.21 275.56 342.25 37.290 408.04 462.25 436.81 488.41 432.64 392.04 37.410 364.81 331.24 268.96 216.09 153.76 129.96 37.530 112.36 92.16 96.04 64.00 67.24 56.25 37.650 68.89 60.84 57.76 59.29 49.00 53.29 37.770 47.61 50.41 47.61 40.96 40.96 44.89 37.890 38.44 34.81 44.89 47.61 39.69 39.69 38.010 43.56 50.41 50.41 39.69 47.61 33.64 38.130 38.44 38.44 42.25 32.49 53.29 32.49 38.250 39.69 21.16 46.24 38.44 40.96 33.64 38.370 38.44 42.25 43.56 43.56 37.21 32.49 38.490 33.64 39.69 38.44 36.00 36.00 38.44 38.610 33.64 38.44 38.44 37.21 39.69 37.21 38.730 38.44 47.61 32.49 32.49 33.64 38.44 38.850 47.61 42.25 42.25 34.81 44.89 46.24 38.970 49.00 44.89 46.24 49.00 43.56 43.56 39.090 31.36 39.69 47.61 32.49 38.44 34.81 39.210 36.00 49.00 47.61 38.44 60.84 53.29 39.330 49.00 53.29 70.56 49.00 67.24 75.69 39.450 79.21 79.21 60.84 65.61 65.61 75.69 39.570 65.61 65.61 70.56 51.84 51.84 75.69 39.690 62.41 70.56 90.25 73.96 72.25 90.25 39.810 79.21 88.36 94.09 77.44 84.64 88.36 39.930 100.00 72.25 79.21 84.64 82.81 79.21 40.050 81.00 67.24 72.25 60.84 79.21 70.56 40.170 64.00 62.41 62.41 72.25 92.16 90.25 40.290 77.44 88.36 84.64 73.96 62.41 79.21 40.410 70.56 70.56 44.89 59.29 49.00 56.25 40.530 60.84 67.24 72.25 59.29 77.44 75.69 40.650 72.25 112.36 108.16 100.00 121.00 114.49 40.770 121.00 121.00 139.24 174.24 198.81 193.21 40.890 259.21 278.89 384.16 441.00 566.44 734.41 41.010 906.01 1089.00 1274.49 1451.61 1482.25 1482.25 41.130 1451.61 1303.21 1142.44 1024.00 894.01 800.89 41.250 645.16 501.76 404.01 320.41 256.00 240.25 41.370 196.00 182.25 158.76 146.41 121.00 116.64 41.490 90.25 86.49 88.36 77.44 72.25 73.96 41.610 67.24 68.89 62.41 68.89 56.25 62.41 41.730 50.41 47.61 51.84 57.76 54.76 67.24 41.850 43.56 47.61 50.41 39.69 39.69 53.29 41.970 50.41 33.64 56.25 37.21 44.89 50.41 42.090 38.44 38.44 36.00 42.25 32.49 40.96 42.210 49.00 47.61 50.41 50.41 47.61 38.44 42.330 59.29 56.25 53.29 67.24 62.41 68.89 42.450 75.69 47.61 54.76 53.29 50.41 46.24 42.570 65.61 33.64 44.89 34.81 38.44 56.25 42.690 49.00 33.64 38.44 28.09 40.96 38.44

155

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 32.49 25.00 38.44 43.56 46.24 47.61 42.930 39.69 53.29 50.41 56.25 47.61 60.84 43.050 77.44 53.29 60.84 67.24 75.69 62.41 43.170 70.56 57.76 62.41 62.41 82.81 73.96 43.290 59.29 59.29 67.24 62.41 79.21 65.61 43.410 68.89 72.25 59.29 51.84 62.41 62.41 43.530 77.44 70.56 92.16 77.44 88.36 94.09 43.650 129.96 158.76 182.25 174.24 204.49 219.04 43.770 246.49 234.09 222.01 174.24 182.25 166.41 43.890 146.41 114.49 129.96 94.09 82.81 57.76 44.010 81.00 70.56 64.00 70.56 50.41 57.76 44.130 53.29 47.61 67.24 43.56 53.29 47.61 44.250 47.61 44.89 56.25 59.29 62.41 67.24 44.370 51.84 65.61 59.29 67.24 60.84 62.41 44.490 64.00 73.96 73.96 60.84 75.69 92.16 44.610 92.16 94.09 102.01 121.00 151.29 166.41 44.730 198.81 289.00 349.69 408.04 510.76 640.09 44.850 718.24 870.25 882.09 918.09 817.96 665.64 44.970 650.25 580.81 561.69 484.00 392.04 338.56 45.090 252.81 222.01 176.89 161.29 151.29 134.56 45.210 112.36 123.21 112.36 86.49 75.69 73.96 45.330 67.24 62.41 59.29 67.24 59.29 46.24 45.450 49.00 60.84 50.41 50.41 47.61 50.41 45.570 50.41 54.76 34.81 43.56 49.00 40.96 45.690 53.29 53.29 53.29 50.41 62.41 64.00 45.810 46.24 42.25 46.24 57.76 49.00 47.61 45.930 49.00 50.41 50.41 43.56 54.76 38.44 46.050 38.44 56.25 64.00 65.61 54.76 56.25 46.170 44.89 59.29 47.61 50.41 59.29 73.96 46.290 62.41 62.41 59.29 72.25 86.49 86.49 46.410 225.00 86.49 68.89 82.81 88.36 88.36 46.530 90.25 106.09 96.04 88.36 100.00 92.16 46.650 98.01 92.16 96.04 92.16 90.25 92.16 46.770 90.25 79.21 92.16 79.21 67.24 77.44 46.890 72.25 62.41 62.41 56.25 54.76 49.00 47.010 64.00 44.89 42.25 67.24 46.24 60.84 47.130 53.29 67.24 50.41 46.24 49.00 56.25 47.250 43.56 50.41 51.84 49.00 43.56 51.84 47.370 43.56 57.76 51.84 60.84 47.61 72.25 47.490 56.25 53.29 46.24 70.56 54.76 53.29 47.610 54.76 62.41 62.41 49.00 47.61 49.00 47.730 51.84 50.41 38.44 40.96 28.09 39.69 47.850 38.44 44.89 44.89 42.25 40.96 30.25 47.970 44.89 43.56 33.64 33.64 46.24 43.56 48.090 50.41 49.00 50.41 53.29 43.56 49.00 48.210 42.25 54.76 43.56 53.29 51.84 51.84 48.330 51.84 59.29 62.41 42.25 42.25 53.29 48.450 50.41 54.76 59.29 65.61 50.41 57.76 48.570 70.56 60.84 62.41 56.25 53.29 56.25 48.690 62.41 59.29 46.24 53.29 53.29 59.29 48.810 65.61 54.76 53.29 62.41 59.29 65.61 48.930 70.56 65.61 75.69 96.04 90.25 86.49

156

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 96.04 114.49 146.41 153.76 148.84 184.96 49.170 187.69 225.00 240.25 237.16 252.81 249.64 49.290 222.01 234.09 182.25 169.00 153.76 129.96 49.410 148.84 129.96 144.00 100.00 100.00 90.25 49.530 98.01 96.04 94.09 79.21 84.64 68.89 49.650 77.44 62.41 53.29 65.61 92.16 72.25 49.770 75.69 82.81 100.00 79.21 82.81 98.01 49.890 86.49 98.01 96.04 94.09 112.36 123.21 50.010 134.56 123.21 169.00 176.89 174.24 198.81 50.130 174.24 187.69 179.56 243.36 256.00 289.00 50.250 327.61 327.61 400.00 466.56 524.41 650.25 50.370 772.84 858.49 1011.24 1142.44 1346.89 1459.24 50.490 1428.84 1398.76 1281.64 1253.16 1162.81 1135.69 50.610 1036.84 930.25 812.25 756.25 620.01 576.00 50.730 506.25 475.24 432.64 466.56 441.00 470.89 50.850 576.00 600.25 676.00 829.44 823.69 1030.41 50.970 1075.84 1183.36 1260.25 1324.96 1253.16 1149.21 51.090 1062.76 1056.25 992.25 918.09 864.36 778.41 51.210 681.21 630.01 524.41 466.56 384.16 349.69 51.330 306.25 265.69 272.25 243.36 225.00 182.25 51.450 187.69 129.96 134.56 114.49 123.21 98.01 51.570 108.16 92.16 106.09 98.01 81.00 84.64 51.690 79.21 59.29 75.69 67.24 54.76 50.41 51.810 72.25 67.24 68.89 65.61 59.29 53.29 51.930 60.84 64.00 77.44 46.24 56.25 54.76 52.050 62.41 65.61 62.41 60.84 72.25 47.61 52.170 50.41 51.84 51.84 43.56 59.29 57.76 52.290 68.89 65.61 72.25 59.29 65.61 59.29 52.410 62.41 64.00 60.84 56.25 47.61 50.41 52.530 49.00 53.29 54.76 53.29 43.56 56.25 52.650 56.25 50.41 47.61 50.41 32.49 47.61 52.770 60.84 49.00 62.41 59.29 53.29 59.29 52.890 56.25 59.29 67.24 56.25 46.24 73.96 53.010 64.00 47.61 70.56 64.00 62.41 79.21 53.130 75.69 90.25 60.84 64.00 81.00 56.25 53.250 53.29 70.56 38.44 56.25 67.24 77.44 53.370 60.84 59.29 56.25 54.76 54.76 53.29 53.490 56.25 47.61 54.76 50.41 44.89 64.00 53.610 47.61 56.25 59.29 60.84 40.96 50.41 53.730 56.25 47.61 43.56 51.84 47.61 54.76 53.850 56.25 47.61 50.41 68.89 59.29 53.29 53.970 51.84 50.41 70.56 56.25 56.25 53.29 54.090 43.56 40.96 57.76 50.41 51.84 51.84 54.210 53.29 33.64 54.76 40.96 56.25 54.76 54.330 46.24 39.69 65.61 33.64 47.61 43.56 54.450 40.96 40.96 54.76 40.96 47.61 32.49 54.570 47.61 37.21 43.56 43.56 36.00 44.89 54.690 43.56 46.24 44.89 42.25 46.24 47.61 54.810 37.21 29.16 32.49 43.56 43.56 40.96 54.930 28.09 51.84 36.00 42.25 38.44 39.69 55.050 38.44 40.96 38.44 50.41 39.69 42.25 55.170 38.44 49.00 42.25 42.25 56.25 43.56

157

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 49.00 44.89 33.64 38.44 40.96 38.44 55.410 40.96 47.61 49.00 34.81 33.64 38.44 55.530 46.24 36.00 38.44 33.64 34.81 23.04 55.650 34.81 26.01 43.56 40.96 54.76 26.01 55.770 38.44 40.96 29.16 32.49 36.00 37.21 55.890 28.09 39.69 38.44 37.21 34.81 42.25 56.010 33.64 37.21 34.81 38.44 43.56 37.21 56.130 37.21 39.69 44.89 43.56 53.29 42.25 56.250 47.61 53.29 39.69 42.25 47.61 36.00 56.370 32.49 43.56 47.61 54.76 37.21 36.00 56.490 31.36 40.96 38.44 36.00 42.25 32.49 56.610 30.25 36.00 38.44 38.44 28.09 40.96 56.730 38.44 39.69 32.49 29.16 43.56 42.25 56.850 33.64 39.69 36.00 44.89 30.25 47.61 56.970 43.56 32.49 37.21 38.44 44.89 44.89 57.090 39.69 37.21 37.21 31.36 37.21 46.24 57.210 43.56 44.89 37.21 40.96 46.24 43.56 57.330 43.56 59.29 43.56 43.56 43.56 38.44 57.450 43.56 39.69 54.76 42.25 31.36 51.84 57.570 38.44 43.56 59.29 37.21 31.36 51.84 57.690 47.61 33.64 32.49 49.00 36.00 42.25 57.810 40.96 37.21 46.24 38.44 42.25 47.61 57.930 47.61 40.96 44.89 34.81 37.21 46.24 58.050 36.00 47.61 50.41 46.24 37.21 40.96 58.170 38.44 50.41 36.00 47.61 43.56 28.09 58.290 42.25 44.89 46.24 51.84 49.00 54.76 58.410 50.41 51.84 53.29 50.41 56.25 64.00 58.530 68.89 73.96 59.29 86.49 67.24 79.21 58.650 96.04 106.09 112.36 141.61 156.25 161.29 58.770 222.01 213.16 265.69 262.44 225.00 243.36 58.890 240.25 213.16 184.96 210.25 193.21 146.41 59.010 179.56 132.25 136.89 127.69 114.49 98.01 59.130 79.21 86.49 88.36 65.61 96.04 62.41 59.250 75.69 72.25 77.44 82.81 79.21 79.21 59.370 75.69 70.56 114.49 86.49 102.01 98.01 59.490 108.16 118.81 136.89 163.84 171.61 174.24 59.610 201.64 213.16 272.25 285.61 342.25 388.09 59.730 436.81 441.00 449.44 420.25 384.16 408.04 59.850 376.36 342.25 327.61 338.56 272.25 272.25 59.970 216.09 169.00 163.84 156.25 144.00 148.84 60.090 116.64 94.09 94.09 96.04 72.25 75.69 60.210 64.00 64.00 70.56 72.25 68.89 62.41 60.330 54.76 47.61 44.89 44.89 43.56 60.84 60.450 46.24 43.56 53.29 53.29 59.29 53.29 60.570 53.29 59.29 46.24 51.84 47.61 46.24 60.690 40.96 39.69 46.24 49.00 38.44 49.00 60.810 46.24 56.25 44.89 38.44 43.56 50.41 60.930 44.89 42.25 50.41 47.61 43.56 47.61 61.050 47.61 59.29 47.61 50.41 72.25 56.25 61.170 50.41 47.61 62.41 59.29 49.00 54.76 61.290 51.84 57.76 51.84 53.29 53.29 56.25 61.410 65.61 60.84 53.29 65.61 43.56 50.41

158

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 62.41 51.84 62.41 59.29 47.61 47.61 61.650 38.44 53.29 75.69 68.89 70.56 49.00 61.770 59.29 68.89 75.69 64.00 81.00 82.81 61.890 90.25 84.64 92.16 116.64 100.00 98.01 62.010 112.36 86.49 82.81 73.96 73.96 81.00 62.130 90.25 86.49 79.21 72.25 59.29 47.61 62.250 60.84 49.00 65.61 49.00 62.41 50.41 62.370 50.41 64.00 50.41 37.21 53.29 53.29 62.490 38.44 57.76 56.25 43.56 54.76 49.00 62.610 43.56 50.41 53.29 34.81 56.25 56.25 62.730 57.76 47.61 50.41 44.89 59.29 54.76 62.850 67.24 53.29 77.44 72.25 65.61 77.44 62.970 77.44 75.69 65.61 92.16 94.09 86.49 63.090 88.36 106.09 114.49 125.44 132.25 132.25 63.210 163.84 210.25 216.09 285.61 302.76 357.21 63.330 376.36 404.01 449.44 424.36 449.44 357.21 63.450 364.81 331.24 364.81 292.41 282.24 292.41 63.570 268.96 222.01 196.00 179.56 136.89 161.29 63.690 121.00 114.49 114.49 108.16 102.01 94.09 63.810 94.09 88.36 94.09 94.09 88.36 102.01 63.930 82.81 88.36 90.25 75.69 84.64 84.64 64.050 94.09 82.81 108.16 98.01 112.36 86.49 64.170 125.44 112.36 129.96 127.69 144.00 151.29 64.290 156.25 196.00 228.01 246.49 324.00 302.76 64.410 353.44 345.96 368.64 361.00 345.96 327.61 64.530 278.89 295.84 265.69 228.01 243.36 265.69 64.650 252.81 213.16 193.21 179.56 163.84 144.00 64.770 144.00 146.41 125.44 116.64 134.56 118.81 64.890 132.25 156.25 169.00 182.25 184.96 201.64 65.010 210.25 246.49 246.49 272.25 272.25 272.25 65.130 285.61 265.69 262.44 246.49 249.64 207.36 65.250 219.04 187.69 190.44 182.25 184.96 169.00 65.370 139.24 134.56 102.01 112.36 114.49 98.01 65.490 92.16 79.21 79.21 70.56 86.49 96.04 65.610 92.16 88.36 104.04 75.69 94.09 88.36 65.730 92.16 67.24 94.09 79.21 84.64 98.01 65.850 110.25 136.89 123.21 132.25 129.96 161.29 65.970 129.96 153.76 144.00 174.24 169.00 127.69 66.090 134.56 139.24 125.44 144.00 121.00 96.04 66.210 127.69 88.36 88.36 96.04 102.01 77.44 66.330 72.25 79.21 62.41 59.29 70.56 62.41 66.450 68.89 72.25 60.84 50.41 53.29 50.41 66.570 54.76 59.29 65.61 62.41 56.25 65.61 66.690 57.76 60.84 54.76 60.84 65.61 67.24 66.810 56.25 60.84 59.29 62.41 84.64 65.61 66.930 77.44 70.56 100.00 82.81 72.25 79.21 67.050 82.81 104.04 112.36 136.89 139.24 146.41 67.170 158.76 207.36 278.89 299.29 353.44 357.21 67.290 400.00 466.56 470.89 506.25 400.00 357.21 67.410 357.21 313.29 324.00 327.61 316.84 327.61 67.530 306.25 268.96 246.49 228.01 176.89 148.84 67.650 141.61 104.04 108.16 96.04 102.01 110.25

159

File: JC6.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 82.81 82.81 75.69 75.69 79.21 70.56 67.890 67.24 73.96 65.61 65.61 70.56 72.25 68.010 70.56 70.56 77.44 82.81 88.36 60.84 68.130 70.56 77.44 56.25 73.96 86.49 59.29 68.250 67.24 75.69 75.69 56.25 62.41 53.29 68.370 59.29 56.25 54.76 56.25 56.25 56.25 68.490 54.76 38.44 38.44 53.29 34.81 50.41 68.610 47.61 44.89 43.56 50.41 34.81 56.25 68.730 53.29 44.89 44.89 53.29 49.00 47.61 68.850 42.25 56.25 53.29 56.25 46.24 49.00 68.970 51.84 46.24 31.36 38.44 47.61 47.61 69.090 47.61 64.00 47.61 49.00 44.89 43.56 69.210 46.24 50.41 49.00 51.84 40.96 50.41 69.330 60.84 39.69 54.76 44.89 33.64 56.25 69.450 51.84 42.25 50.41 68.89 53.29 50.41 69.570 44.89 44.89 42.25 59.29 46.24 62.41 69.690 47.61 57.76 47.61 53.29 49.00 62.41 69.810 62.41 47.61 72.25 67.24 72.25 56.25 69.930 54.76 70.56 67.24 77.44 _

160

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC7 Data measured at: 25-Jan-2011 8:07:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 19544.04 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 98.01 108.16 92.16 98.01 92.16 104.04 2.130 94.09 82.81 81.00 82.81 79.21 82.81 2.250 77.44 82.81 86.49 81.00 77.44 65.61 2.370 65.61 70.56 82.81 98.01 72.25 84.64 2.490 60.84 64.00 67.24 67.24 53.29 67.24 2.610 60.84 56.25 56.25 67.24 57.76 70.56 2.730 75.69 62.41 62.41 53.29 53.29 59.29 2.850 75.69 54.76 62.41 57.76 50.41 75.69 2.970 67.24 73.96 59.29 59.29 65.61 65.61 3.090 56.25 72.25 54.76 64.00 54.76 51.84 3.210 59.29 50.41 64.00 47.61 62.41 60.84 3.330 62.41 53.29 50.41 50.41 59.29 73.96 3.450 54.76 53.29 59.29 67.24 50.41 65.61 3.570 43.56 57.76 38.44 59.29 62.41 62.41 3.690 65.61 49.00 54.76 50.41 54.76 62.41 3.810 60.84 59.29 53.29 70.56 62.41 70.56 3.930 62.41 64.00 68.89 47.61 70.56 62.41 4.050 62.41 56.25 47.61 60.84 50.41 53.29 4.170 53.29 47.61 56.25 57.76 56.25 59.29 4.290 59.29 53.29 44.89 51.84 57.76 54.76 4.410 47.61 65.61 62.41 62.41 67.24 50.41 4.530 64.00 56.25 62.41 39.69 44.89 53.29 4.650 59.29 60.84 57.76 56.25 60.84 67.24 4.770 65.61 47.61 59.29 51.84 50.41 50.41 4.890 49.00 56.25 54.76 60.84 62.41 57.76 5.010 65.61 59.29 53.29 67.24 50.41 50.41 5.130 46.24 67.24 65.61 64.00 50.41 53.29 5.250 68.89 57.76 59.29 67.24 67.24 57.76

161

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 67.24 39.69 44.89 59.29 54.76 54.76 5.490 65.61 43.56 64.00 57.76 67.24 75.69 5.610 59.29 62.41 53.29 56.25 53.29 67.24 5.730 50.41 62.41 49.00 53.29 49.00 59.29 5.850 50.41 56.25 57.76 56.25 53.29 65.61 5.970 50.41 50.41 47.61 57.76 59.29 51.84 6.090 47.61 43.56 70.56 43.56 51.84 57.76 6.210 56.25 59.29 54.76 42.25 62.41 60.84 6.330 62.41 43.56 51.84 68.89 62.41 51.84 6.450 49.00 73.96 62.41 57.76 50.41 60.84 6.570 62.41 50.41 56.25 57.76 50.41 56.25 6.690 51.84 50.41 50.41 53.29 53.29 54.76 6.810 53.29 53.29 50.41 43.56 43.56 56.25 6.930 56.25 64.00 51.84 59.29 56.25 56.25 7.050 47.61 44.89 50.41 46.24 62.41 40.96 7.170 50.41 53.29 53.29 43.56 47.61 31.36 7.290 62.41 56.25 54.76 56.25 60.84 56.25 7.410 54.76 56.25 51.84 62.41 53.29 56.25 7.530 47.61 47.61 47.61 59.29 53.29 53.29 7.650 46.24 56.25 77.44 51.84 64.00 51.84 7.770 38.44 62.41 49.00 59.29 60.84 56.25 7.890 47.61 50.41 54.76 50.41 67.24 43.56 8.010 60.84 54.76 51.84 49.00 59.29 54.76 8.130 54.76 51.84 53.29 56.25 56.25 44.89 8.250 51.84 50.41 47.61 39.69 53.29 51.84 8.370 44.89 38.44 53.29 40.96 53.29 38.44 8.490 43.56 56.25 51.84 46.24 54.76 47.61 8.610 70.56 59.29 50.41 53.29 60.84 57.76 8.730 54.76 47.61 57.76 47.61 42.25 36.00 8.850 51.84 47.61 42.25 59.29 50.41 47.61 8.970 42.25 39.69 53.29 43.56 59.29 40.96 9.090 49.00 51.84 49.00 42.25 46.24 53.29 9.210 62.41 49.00 49.00 43.56 50.41 47.61 9.330 50.41 46.24 46.24 54.76 43.56 54.76 9.450 59.29 56.25 40.96 51.84 60.84 37.21 9.570 47.61 47.61 36.00 53.29 47.61 50.41 9.690 53.29 56.25 62.41 47.61 43.56 33.64 9.810 46.24 37.21 59.29 44.89 50.41 64.00 9.930 40.96 56.25 38.44 43.56 53.29 47.61 10.050 51.84 50.41 53.29 56.25 38.44 50.41 10.170 44.89 53.29 42.25 42.25 59.29 47.61 10.290 62.41 59.29 47.61 46.24 39.69 53.29 10.410 46.24 43.56 44.89 59.29 39.69 53.29 10.530 53.29 42.25 59.29 43.56 37.21 49.00 10.650 51.84 50.41 47.61 46.24 56.25 44.89 10.770 56.25 44.89 42.25 47.61 50.41 51.84 10.890 47.61 53.29 53.29 37.21 40.96 51.84 11.010 53.29 43.56 54.76 49.00 42.25 47.61 11.130 39.69 42.25 49.00 47.61 44.89 39.69 11.250 46.24 51.84 49.00 50.41 44.89 51.84 11.370 40.96 50.41 34.81 46.24 47.61 50.41 11.490 60.84 49.00 30.25 43.56 47.61 49.00

162

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 42.25 46.24 64.00 43.56 44.89 72.25 11.730 53.29 46.24 44.89 50.41 47.61 50.41 11.850 43.56 43.56 47.61 50.41 46.24 43.56 11.970 43.56 37.21 43.56 31.36 38.44 53.29 12.090 51.84 47.61 40.96 44.89 40.96 47.61 12.210 43.56 43.56 32.49 46.24 39.69 40.96 12.330 44.89 42.25 50.41 37.21 56.25 38.44 12.450 34.81 44.89 39.69 47.61 47.61 47.61 12.570 50.41 56.25 38.44 47.61 27.04 47.61 12.690 34.81 47.61 43.56 34.81 43.56 39.69 12.810 56.25 38.44 37.21 44.89 59.29 39.69 12.930 43.56 47.61 42.25 42.25 42.25 38.44 13.050 34.81 50.41 53.29 47.61 38.44 47.61 13.170 50.41 47.61 50.41 43.56 39.69 38.44 13.290 32.49 46.24 43.56 40.96 40.96 53.29 13.410 42.25 44.89 33.64 38.44 31.36 40.96 13.530 40.96 39.69 47.61 43.56 47.61 38.44 13.650 38.44 31.36 33.64 40.96 33.64 47.61 13.770 38.44 40.96 36.00 43.56 46.24 47.61 13.890 40.96 37.21 46.24 32.49 30.25 44.89 14.010 42.25 50.41 38.44 38.44 43.56 44.89 14.130 32.49 44.89 38.44 46.24 47.61 38.44 14.250 42.25 53.29 40.96 47.61 43.56 40.96 14.370 47.61 50.41 56.25 47.61 43.56 36.00 14.490 32.49 39.69 36.00 44.89 39.69 34.81 14.610 34.81 37.21 39.69 36.00 36.00 39.69 14.730 39.69 34.81 38.44 56.25 43.56 39.69 14.850 38.44 36.00 49.00 46.24 43.56 53.29 14.970 50.41 32.49 53.29 33.64 34.81 67.24 15.090 46.24 46.24 56.25 56.25 47.61 59.29 15.210 56.25 64.00 57.76 59.29 47.61 59.29 15.330 57.76 62.41 65.61 50.41 70.56 44.89 15.450 62.41 62.41 62.41 67.24 59.29 47.61 15.570 54.76 75.69 79.21 62.41 56.25 60.84 15.690 62.41 62.41 53.29 77.44 62.41 62.41 15.810 62.41 56.25 56.25 70.56 67.24 59.29 15.930 50.41 72.25 68.89 56.25 72.25 56.25 16.050 59.29 56.25 53.29 54.76 59.29 56.25 16.170 67.24 53.29 75.69 67.24 57.76 53.29 16.290 59.29 53.29 51.84 59.29 59.29 54.76 16.410 32.49 34.81 65.61 50.41 47.61 62.41 16.530 62.41 47.61 56.25 50.41 54.76 65.61 16.650 43.56 60.84 46.24 40.96 46.24 42.25 16.770 50.41 59.29 53.29 47.61 43.56 42.25 16.890 49.00 39.69 43.56 46.24 38.44 49.00 17.010 50.41 50.41 53.29 56.25 47.61 39.69 17.130 40.96 49.00 46.24 38.44 47.61 43.56 17.250 43.56 43.56 38.44 50.41 38.44 53.29 17.370 54.76 46.24 46.24 54.76 42.25 34.81 17.490 56.25 33.64 43.56 29.16 37.21 43.56 17.610 47.61 50.41 40.96 42.25 42.25 43.56 17.730 46.24 40.96 44.89 39.69 38.44 43.56

163

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 39.69 43.56 36.00 49.00 28.09 43.56 17.970 38.44 40.96 50.41 46.24 49.00 50.41 18.090 38.44 42.25 49.00 43.56 40.96 39.69 18.210 47.61 39.69 43.56 34.81 43.56 46.24 18.330 50.41 40.96 34.81 42.25 53.29 42.25 18.450 46.24 26.01 30.25 39.69 34.81 56.25 18.570 38.44 43.56 43.56 44.89 32.49 33.64 18.690 49.00 37.21 36.00 32.49 44.89 38.44 18.810 38.44 40.96 42.25 43.56 47.61 46.24 18.930 30.25 50.41 40.96 40.96 38.44 42.25 19.050 50.41 38.44 42.25 43.56 43.56 56.25 19.170 38.44 42.25 49.00 36.00 32.49 40.96 19.290 51.84 53.29 38.44 43.56 51.84 44.89 19.410 47.61 47.61 40.96 57.76 43.56 59.29 19.530 33.64 47.61 38.44 46.24 44.89 53.29 19.650 50.41 50.41 47.61 43.56 43.56 43.56 19.770 38.44 46.24 51.84 34.81 44.89 50.41 19.890 43.56 50.41 43.56 43.56 46.24 44.89 20.010 62.41 38.44 43.56 34.81 49.00 40.96 20.130 36.00 38.44 36.00 44.89 39.69 56.25 20.250 31.36 31.36 32.49 43.56 47.61 38.44 20.370 33.64 43.56 38.44 44.89 49.00 37.21 20.490 51.84 49.00 39.69 40.96 32.49 64.00 20.610 50.41 36.00 32.49 53.29 56.25 54.76 20.730 81.00 75.69 106.09 156.25 166.41 166.41 20.850 148.84 121.00 81.00 65.61 72.25 53.29 20.970 47.61 46.24 42.25 50.41 50.41 54.76 21.090 59.29 50.41 56.25 50.41 56.25 47.61 21.210 54.76 38.44 62.41 43.56 50.41 51.84 21.330 43.56 34.81 37.21 43.56 49.00 43.56 21.450 57.76 34.81 33.64 50.41 32.49 47.61 21.570 38.44 47.61 50.41 53.29 44.89 27.04 21.690 53.29 54.76 38.44 38.44 50.41 47.61 21.810 59.29 53.29 56.25 59.29 72.25 90.25 21.930 94.09 114.49 127.69 116.64 123.21 112.36 22.050 100.00 96.04 79.21 56.25 56.25 44.89 22.170 53.29 56.25 43.56 47.61 33.64 53.29 22.290 40.96 38.44 47.61 43.56 33.64 40.96 22.410 32.49 39.69 44.89 39.69 40.96 36.00 22.530 43.56 40.96 49.00 32.49 33.64 36.00 22.650 46.24 40.96 31.36 47.61 36.00 39.69 22.770 38.44 38.44 39.69 54.76 47.61 32.49 22.890 49.00 43.56 47.61 40.96 44.89 32.49 23.010 44.89 42.25 36.00 27.04 62.41 37.21 23.130 44.89 40.96 36.00 31.36 33.64 47.61 23.250 44.89 32.49 43.56 37.21 32.49 38.44 23.370 32.49 46.24 39.69 32.49 38.44 42.25 23.490 33.64 37.21 39.69 39.69 49.00 46.24 23.610 47.61 38.44 50.41 54.76 50.41 47.61 23.730 50.41 36.00 57.76 51.84 68.89 62.41 23.850 62.41 68.89 88.36 102.01 125.44 148.84 23.970 182.25 222.01 246.49 225.00 216.09 190.44

164

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 144.00 121.00 121.00 72.25 62.41 59.29 24.210 54.76 59.29 56.25 43.56 53.29 37.21 24.330 40.96 43.56 44.89 50.41 38.44 37.21 24.450 32.49 44.89 44.89 42.25 38.44 34.81 24.570 31.36 33.64 43.56 39.69 47.61 32.49 24.690 32.49 43.56 50.41 38.44 38.44 29.16 24.810 37.21 53.29 50.41 32.49 40.96 43.56 24.930 34.81 38.44 46.24 43.56 38.44 43.56 25.050 43.56 38.44 43.56 37.21 47.61 44.89 25.170 38.44 43.56 44.89 33.64 51.84 32.49 25.290 47.61 46.24 56.25 39.69 31.36 31.36 25.410 31.36 33.64 57.76 32.49 36.00 38.44 25.530 32.49 38.44 32.49 38.44 37.21 46.24 25.650 34.81 40.96 47.61 33.64 54.76 31.36 25.770 38.44 38.44 53.29 40.96 38.44 42.25 25.890 40.96 43.56 39.69 49.00 38.44 43.56 26.010 33.64 38.44 37.21 46.24 43.56 47.61 26.130 32.49 47.61 65.61 50.41 43.56 39.69 26.250 47.61 40.96 59.29 51.84 56.25 47.61 26.370 59.29 65.61 56.25 68.89 75.69 70.56 26.490 98.01 102.01 125.44 184.96 234.09 313.29 26.610 364.81 338.56 249.64 228.01 196.00 134.56 26.730 90.25 56.25 67.24 56.25 53.29 46.24 26.850 47.61 40.96 43.56 49.00 36.00 37.21 26.970 37.21 42.25 42.25 46.24 40.96 50.41 27.090 43.56 32.49 53.29 36.00 40.96 31.36 27.210 47.61 38.44 40.96 36.00 33.64 40.96 27.330 43.56 44.89 38.44 43.56 40.96 51.84 27.450 37.21 37.21 32.49 37.21 43.56 34.81 27.570 42.25 28.09 37.21 31.36 38.44 43.56 27.690 28.09 43.56 30.25 46.24 44.89 50.41 27.810 44.89 42.25 37.21 36.00 36.00 36.00 27.930 36.00 34.81 38.44 39.69 43.56 40.96 28.050 39.69 47.61 38.44 31.36 37.21 33.64 28.170 34.81 40.96 43.56 38.44 37.21 33.64 28.290 37.21 32.49 42.25 57.76 39.69 34.81 28.410 34.81 43.56 50.41 38.44 46.24 46.24 28.530 43.56 44.89 43.56 43.56 37.21 50.41 28.650 47.61 53.29 37.21 49.00 51.84 50.41 28.770 54.76 56.25 50.41 38.44 49.00 53.29 28.890 67.24 47.61 44.89 32.49 47.61 50.41 29.010 64.00 47.61 50.41 50.41 56.25 56.25 29.130 50.41 56.25 62.41 60.84 56.25 60.84 29.250 51.84 62.41 77.44 75.69 90.25 106.09 29.370 92.16 94.09 112.36 127.69 92.16 86.49 29.490 98.01 59.29 65.61 56.25 62.41 86.49 29.610 73.96 82.81 59.29 60.84 75.69 72.25 29.730 68.89 70.56 73.96 67.24 82.81 82.81 29.850 75.69 82.81 90.25 86.49 94.09 100.00 29.970 114.49 100.00 88.36 77.44 86.49 108.16 30.090 94.09 106.09 112.36 110.25 114.49 112.36 30.210 139.24 141.61 148.84 158.76 176.89 184.96

165

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 190.44 216.09 225.00 268.96 313.29 313.29 30.450 306.25 361.00 372.49 492.84 519.84 542.89 30.570 590.49 676.00 789.61 846.81 948.64 1176.49 30.690 1421.29 1789.29 2227.84 2905.21 3844.00 5299.84 30.810 7174.09 9801.00 13409.64 16512.25 18686.89 19544.04 30.930 18306.09 16281.76 13853.29 11257.21 8742.25 6416.01 31.050 4678.56 3283.29 2450.25 1866.24 1536.64 1361.61 31.170 1169.64 979.69 817.96 676.00 605.16 556.96 31.290 420.25 408.04 400.00 316.84 292.41 316.84 31.410 285.61 246.49 219.04 207.36 182.25 201.64 31.530 196.00 174.24 156.25 153.76 144.00 136.89 31.650 139.24 106.09 112.36 116.64 134.56 125.44 31.770 96.04 112.36 116.64 114.49 100.00 123.21 31.890 108.16 96.04 96.04 84.64 86.49 96.04 32.010 77.44 94.09 72.25 79.21 86.49 86.49 32.130 64.00 73.96 70.56 86.49 72.25 77.44 32.250 75.69 65.61 70.56 53.29 59.29 54.76 32.370 64.00 47.61 67.24 54.76 50.41 59.29 32.490 62.41 51.84 53.29 50.41 53.29 51.84 32.610 62.41 51.84 59.29 60.84 47.61 62.41 32.730 56.25 54.76 47.61 47.61 50.41 53.29 32.850 47.61 62.41 43.56 53.29 47.61 56.25 32.970 57.76 53.29 67.24 70.56 57.76 50.41 33.090 68.89 54.76 62.41 62.41 59.29 73.96 33.210 67.24 75.69 81.00 77.44 92.16 94.09 33.330 116.64 151.29 176.89 193.21 219.04 216.09 33.450 299.29 320.41 342.25 327.61 331.24 259.21 33.570 243.36 210.25 196.00 158.76 118.81 121.00 33.690 96.04 79.21 62.41 82.81 59.29 67.24 33.810 57.76 51.84 50.41 51.84 46.24 59.29 33.930 50.41 50.41 56.25 49.00 49.00 38.44 34.050 43.56 46.24 40.96 56.25 39.69 47.61 34.170 53.29 51.84 49.00 38.44 44.89 44.89 34.290 28.09 40.96 40.96 46.24 65.61 40.96 34.410 42.25 36.00 53.29 38.44 46.24 57.76 34.530 33.64 44.89 39.69 50.41 43.56 59.29 34.650 51.84 44.89 54.76 56.25 51.84 51.84 34.770 47.61 53.29 53.29 50.41 51.84 46.24 34.890 64.00 54.76 38.44 62.41 75.69 77.44 35.010 72.25 65.61 84.64 84.64 88.36 108.16 35.130 132.25 156.25 184.96 222.01 252.81 309.76 35.250 320.41 361.00 320.41 299.29 299.29 252.81 35.370 176.89 198.81 166.41 156.25 123.21 121.00 35.490 88.36 75.69 79.21 72.25 59.29 57.76 35.610 59.29 53.29 59.29 53.29 38.44 47.61 35.730 56.25 37.21 53.29 53.29 59.29 47.61 35.850 50.41 39.69 40.96 50.41 57.76 56.25 35.970 44.89 46.24 57.76 37.21 62.41 56.25 36.090 43.56 50.41 43.56 51.84 43.56 40.96 36.210 54.76 59.29 37.21 54.76 57.76 34.81 36.330 49.00 43.56 60.84 53.29 54.76 67.24 36.450 60.84 65.61 68.89 82.81 77.44 82.81

166

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 77.44 68.89 70.56 70.56 84.64 79.21 36.690 86.49 82.81 82.81 92.16 82.81 90.25 36.810 77.44 92.16 102.01 84.64 77.44 98.01 36.930 92.16 88.36 75.69 98.01 104.04 108.16 37.050 92.16 121.00 104.04 102.01 134.56 132.25 37.170 158.76 171.61 201.64 262.44 309.76 408.04 37.290 445.21 501.76 475.24 466.56 420.25 380.25 37.410 327.61 313.29 228.01 213.16 136.89 108.16 37.530 98.01 106.09 65.61 82.81 56.25 57.76 37.650 65.61 67.24 53.29 59.29 60.84 62.41 37.770 51.84 49.00 49.00 70.56 53.29 51.84 37.890 44.89 47.61 46.24 50.41 56.25 43.56 38.010 38.44 62.41 50.41 46.24 47.61 49.00 38.130 47.61 39.69 38.44 44.89 38.44 40.96 38.250 43.56 56.25 44.89 39.69 43.56 43.56 38.370 42.25 43.56 37.21 40.96 47.61 38.44 38.490 46.24 42.25 31.36 42.25 43.56 51.84 38.610 47.61 51.84 42.25 60.84 51.84 43.56 38.730 39.69 43.56 53.29 38.44 42.25 42.25 38.850 50.41 40.96 59.29 64.00 36.00 42.25 38.970 44.89 49.00 47.61 46.24 59.29 46.24 39.090 38.44 49.00 40.96 49.00 47.61 56.25 39.210 51.84 60.84 57.76 62.41 70.56 62.41 39.330 67.24 67.24 77.44 104.04 94.09 108.16 39.450 108.16 110.25 116.64 84.64 90.25 100.00 39.570 84.64 82.81 90.25 110.25 106.09 106.09 39.690 96.04 112.36 108.16 112.36 102.01 118.81 39.810 125.44 127.69 112.36 106.09 127.69 141.61 39.930 118.81 123.21 112.36 104.04 94.09 100.00 40.050 92.16 90.25 90.25 70.56 84.64 79.21 40.170 50.41 65.61 68.89 68.89 57.76 56.25 40.290 56.25 51.84 64.00 53.29 42.25 57.76 40.410 60.84 59.29 53.29 43.56 49.00 60.84 40.530 53.29 59.29 65.61 65.61 70.56 77.44 40.650 72.25 90.25 82.81 104.04 104.04 90.25 40.770 118.81 132.25 156.25 151.29 182.25 216.09 40.890 246.49 313.29 380.25 488.41 605.16 876.16 41.010 1115.56 1339.56 1616.04 1780.84 1730.56 1616.04 41.130 1536.64 1346.89 1246.09 1089.00 1004.89 745.29 41.250 580.81 420.25 331.24 278.89 240.25 169.00 41.370 146.41 156.25 166.41 112.36 100.00 104.04 41.490 88.36 84.64 77.44 56.25 70.56 73.96 41.610 57.76 62.41 53.29 56.25 60.84 43.56 41.730 54.76 59.29 59.29 72.25 44.89 42.25 41.850 67.24 39.69 43.56 40.96 59.29 47.61 41.970 43.56 51.84 56.25 39.69 44.89 42.25 42.090 57.76 37.21 50.41 43.56 40.96 49.00 42.210 50.41 47.61 38.44 53.29 59.29 56.25 42.330 65.61 86.49 88.36 96.04 100.00 84.64 42.450 59.29 82.81 57.76 72.25 53.29 54.76 42.570 40.96 47.61 50.41 49.00 42.25 43.56 42.690 36.00 38.44 49.00 50.41 43.56 38.44

167

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 43.56 40.96 44.89 40.96 38.44 40.96 42.930 39.69 53.29 43.56 37.21 43.56 39.69 43.050 38.44 47.61 43.56 46.24 47.61 62.41 43.170 39.69 50.41 44.89 43.56 43.56 56.25 43.290 47.61 39.69 49.00 40.96 65.61 57.76 43.410 60.84 65.61 57.76 43.56 56.25 50.41 43.530 59.29 64.00 70.56 70.56 100.00 136.89 43.650 123.21 182.25 207.36 252.81 237.16 201.64 43.770 240.25 198.81 182.25 153.76 158.76 148.84 43.890 121.00 108.16 92.16 75.69 72.25 59.29 44.010 62.41 42.25 56.25 59.29 75.69 50.41 44.130 50.41 67.24 39.69 53.29 67.24 53.29 44.250 56.25 37.21 59.29 53.29 51.84 57.76 44.370 64.00 53.29 39.69 70.56 59.29 77.44 44.490 64.00 75.69 88.36 81.00 79.21 84.64 44.610 86.49 110.25 118.81 129.96 158.76 184.96 44.730 228.01 268.96 376.36 497.29 660.49 795.24 44.850 936.36 936.36 936.36 852.64 789.61 729.00 44.970 670.81 600.25 524.41 453.69 338.56 259.21 45.090 213.16 190.44 163.84 139.24 129.96 125.44 45.210 106.09 106.09 108.16 96.04 70.56 82.81 45.330 79.21 75.69 77.44 62.41 59.29 43.56 45.450 50.41 54.76 53.29 64.00 62.41 56.25 45.570 49.00 37.21 43.56 53.29 51.84 47.61 45.690 50.41 57.76 56.25 65.61 49.00 47.61 45.810 59.29 53.29 62.41 53.29 50.41 40.96 45.930 59.29 49.00 70.56 56.25 59.29 44.89 46.050 42.25 44.89 50.41 51.84 47.61 59.29 46.170 47.61 53.29 49.00 47.61 51.84 44.89 46.290 54.76 49.00 57.76 50.41 56.25 62.41 46.410 43.56 50.41 47.61 56.25 59.29 47.61 46.530 56.25 67.24 53.29 60.84 65.61 47.61 46.650 53.29 59.29 56.25 72.25 53.29 65.61 46.770 51.84 50.41 59.29 72.25 51.84 46.24 46.890 65.61 53.29 38.44 49.00 50.41 51.84 47.010 32.49 36.00 44.89 43.56 39.69 38.44 47.130 50.41 43.56 39.69 54.76 42.25 54.76 47.250 59.29 46.24 39.69 38.44 42.25 42.25 47.370 39.69 50.41 49.00 50.41 40.96 37.21 47.490 65.61 43.56 56.25 53.29 43.56 50.41 47.610 53.29 39.69 32.49 50.41 40.96 53.29 47.730 44.89 49.00 43.56 51.84 46.24 44.89 47.850 50.41 44.89 43.56 50.41 47.61 43.56 47.970 53.29 39.69 47.61 40.96 43.56 51.84 48.090 47.61 56.25 43.56 50.41 53.29 56.25 48.210 49.00 53.29 50.41 49.00 50.41 46.24 48.330 46.24 56.25 56.25 50.41 50.41 59.29 48.450 53.29 64.00 64.00 56.25 47.61 53.29 48.570 54.76 47.61 43.56 44.89 51.84 53.29 48.690 50.41 53.29 53.29 56.25 59.29 53.29 48.810 59.29 62.41 59.29 56.25 73.96 62.41 48.930 65.61 84.64 60.84 77.44 100.00 86.49

168

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 90.25 121.00 148.84 179.56 216.09 210.25 49.170 243.36 243.36 285.61 240.25 222.01 219.04 49.290 190.44 204.49 219.04 161.29 176.89 174.24 49.410 148.84 129.96 123.21 100.00 86.49 102.01 49.530 84.64 92.16 82.81 88.36 70.56 67.24 49.650 70.56 90.25 96.04 81.00 86.49 75.69 49.770 82.81 72.25 84.64 82.81 75.69 84.64 49.890 79.21 81.00 102.01 96.04 96.04 112.36 50.010 129.96 139.24 153.76 171.61 163.84 176.89 50.130 190.44 196.00 249.64 213.16 231.04 268.96 50.250 306.25 324.00 436.81 470.89 561.69 655.36 50.370 806.56 924.16 1095.61 1149.21 1197.16 1246.09 50.490 1218.01 1211.04 1135.69 1135.69 1024.00 961.00 50.610 882.09 817.96 729.00 650.25 547.56 590.49 50.730 501.76 492.84 432.64 475.24 542.89 556.96 50.850 620.01 772.84 936.36 1082.41 1232.01 1513.21 50.970 1436.41 1689.21 1656.49 1632.16 1592.01 1406.25 51.090 1376.41 1281.64 1267.36 1108.89 992.25 882.09 51.210 789.61 635.04 576.00 453.69 384.16 338.56 51.330 320.41 275.56 265.69 228.01 190.44 193.21 51.450 174.24 169.00 144.00 136.89 116.64 114.49 51.570 106.09 100.00 84.64 96.04 77.44 84.64 51.690 96.04 62.41 70.56 77.44 102.01 75.69 51.810 77.44 64.00 56.25 56.25 70.56 68.89 51.930 53.29 62.41 67.24 44.89 37.21 84.64 52.050 46.24 62.41 53.29 57.76 50.41 59.29 52.170 64.00 67.24 67.24 68.89 57.76 82.81 52.290 75.69 81.00 75.69 62.41 70.56 60.84 52.410 64.00 59.29 67.24 53.29 42.25 51.84 52.530 59.29 49.00 40.96 47.61 43.56 47.61 52.650 43.56 56.25 50.41 62.41 43.56 43.56 52.770 49.00 53.29 47.61 43.56 38.44 43.56 52.890 60.84 39.69 50.41 40.96 42.25 50.41 53.010 65.61 47.61 50.41 54.76 43.56 43.56 53.130 44.89 47.61 49.00 53.29 51.84 53.29 53.250 44.89 51.84 40.96 47.61 65.61 46.24 53.370 46.24 34.81 42.25 51.84 46.24 46.24 53.490 39.69 37.21 37.21 40.96 54.76 32.49 53.610 42.25 42.25 39.69 49.00 40.96 47.61 53.730 47.61 38.44 38.44 32.49 44.89 53.29 53.850 43.56 44.89 37.21 39.69 51.84 38.44 53.970 31.36 50.41 47.61 38.44 31.36 36.00 54.090 39.69 43.56 43.56 38.44 43.56 43.56 54.210 36.00 36.00 43.56 39.69 32.49 34.81 54.330 38.44 32.49 30.25 43.56 38.44 39.69 54.450 25.00 38.44 39.69 47.61 44.89 37.21 54.570 42.25 38.44 33.64 37.21 38.44 37.21 54.690 46.24 56.25 43.56 46.24 65.61 65.61 54.810 88.36 84.64 75.69 77.44 62.41 50.41 54.930 53.29 46.24 73.96 68.89 60.84 50.41 55.050 49.00 43.56 43.56 32.49 47.61 29.16 55.170 34.81 42.25 40.96 32.49 43.56 44.89

169

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 36.00 47.61 57.76 30.25 43.56 39.69 55.410 32.49 30.25 32.49 38.44 38.44 38.44 55.530 44.89 36.00 38.44 32.49 32.49 39.69 55.650 38.44 32.49 31.36 40.96 29.16 43.56 55.770 38.44 38.44 38.44 29.16 50.41 43.56 55.890 39.69 34.81 31.36 38.44 33.64 50.41 56.010 38.44 38.44 43.56 38.44 44.89 38.44 56.130 40.96 38.44 42.25 51.84 32.49 38.44 56.250 40.96 33.64 42.25 36.00 36.00 39.69 56.370 34.81 40.96 30.25 33.64 32.49 34.81 56.490 38.44 28.09 33.64 43.56 38.44 31.36 56.610 38.44 43.56 33.64 29.16 38.44 40.96 56.730 38.44 33.64 44.89 32.49 51.84 31.36 56.850 36.00 30.25 40.96 33.64 46.24 39.69 56.970 33.64 32.49 38.44 56.25 27.04 42.25 57.090 39.69 37.21 31.36 47.61 56.25 38.44 57.210 39.69 31.36 40.96 34.81 44.89 40.96 57.330 31.36 43.56 40.96 43.56 39.69 40.96 57.450 44.89 38.44 36.00 43.56 46.24 38.44 57.570 44.89 38.44 40.96 36.00 33.64 31.36 57.690 38.44 42.25 34.81 37.21 33.64 32.49 57.810 38.44 43.56 39.69 32.49 32.49 25.00 57.930 36.00 38.44 46.24 40.96 33.64 31.36 58.050 34.81 38.44 46.24 44.89 39.69 39.69 58.170 44.89 36.00 44.89 34.81 50.41 56.25 58.290 43.56 36.00 43.56 44.89 46.24 38.44 58.410 40.96 47.61 44.89 60.84 51.84 64.00 58.530 47.61 56.25 70.56 75.69 72.25 75.69 58.650 94.09 106.09 118.81 134.56 163.84 184.96 58.770 222.01 237.16 302.76 262.44 246.49 237.16 58.890 204.49 187.69 210.25 179.56 176.89 190.44 59.010 174.24 144.00 118.81 106.09 88.36 75.69 59.130 70.56 73.96 62.41 64.00 65.61 50.41 59.250 90.25 67.24 59.29 64.00 72.25 72.25 59.370 47.61 67.24 84.64 82.81 75.69 102.01 59.490 82.81 94.09 112.36 129.96 166.41 184.96 59.610 222.01 268.96 302.76 342.25 432.64 492.84 59.730 416.16 466.56 428.49 453.69 396.01 368.64 59.850 384.16 357.21 357.21 320.41 282.24 243.36 59.970 207.36 182.25 163.84 139.24 121.00 108.16 60.090 94.09 104.04 65.61 72.25 57.76 77.44 60.210 50.41 53.29 59.29 50.41 62.41 49.00 60.330 62.41 39.69 54.76 38.44 42.25 43.56 60.450 47.61 33.64 47.61 70.56 32.49 38.44 60.570 47.61 38.44 56.25 43.56 47.61 46.24 60.690 39.69 40.96 59.29 56.25 34.81 51.84 60.810 42.25 46.24 49.00 51.84 44.89 50.41 60.930 43.56 53.29 39.69 60.84 44.89 50.41 61.050 39.69 51.84 44.89 47.61 50.41 43.56 61.170 43.56 53.29 54.76 46.24 53.29 47.61 61.290 47.61 51.84 59.29 57.76 51.84 57.76 61.410 42.25 50.41 53.29 47.61 39.69 40.96

170

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 70.56 39.69 57.76 50.41 51.84 54.76 61.650 72.25 59.29 56.25 67.24 59.29 53.29 61.770 82.81 77.44 82.81 84.64 90.25 88.36 61.890 84.64 110.25 100.00 106.09 108.16 94.09 62.010 86.49 98.01 100.00 75.69 86.49 88.36 62.130 82.81 82.81 92.16 72.25 57.76 54.76 62.250 67.24 59.29 46.24 32.49 56.25 53.29 62.370 50.41 40.96 56.25 53.29 57.76 47.61 62.490 38.44 59.29 53.29 46.24 42.25 59.29 62.610 50.41 57.76 50.41 53.29 53.29 56.25 62.730 49.00 47.61 56.25 59.29 65.61 53.29 62.850 42.25 62.41 70.56 53.29 75.69 56.25 62.970 82.81 72.25 59.29 88.36 82.81 88.36 63.090 90.25 100.00 116.64 127.69 151.29 161.29 63.210 176.89 252.81 282.24 320.41 392.04 462.25 63.330 488.41 484.00 470.89 441.00 408.04 424.36 63.450 364.81 338.56 353.44 342.25 331.24 302.76 63.570 252.81 198.81 213.16 153.76 139.24 125.44 63.690 108.16 108.16 81.00 88.36 96.04 88.36 63.810 79.21 84.64 67.24 65.61 77.44 79.21 63.930 88.36 84.64 77.44 92.16 84.64 84.64 64.050 92.16 86.49 92.16 96.04 114.49 129.96 64.170 129.96 129.96 174.24 146.41 187.69 243.36 64.290 285.61 331.24 400.00 445.21 466.56 519.84 64.410 595.36 590.49 576.00 566.44 542.89 547.56 64.530 542.89 479.61 462.25 420.25 445.21 416.16 64.650 364.81 331.24 299.29 252.81 216.09 193.21 64.770 182.25 179.56 171.61 171.61 148.84 174.24 64.890 187.69 207.36 193.21 237.16 256.00 282.24 65.010 275.56 299.29 302.76 324.00 349.69 299.29 65.130 306.25 256.00 249.64 282.24 262.44 259.21 65.250 204.49 207.36 201.64 187.69 171.61 169.00 65.370 139.24 134.56 123.21 100.00 86.49 96.04 65.490 86.49 86.49 70.56 70.56 82.81 65.61 65.610 90.25 75.69 77.44 73.96 67.24 100.00 65.730 102.01 104.04 84.64 88.36 81.00 125.44 65.850 110.25 129.96 127.69 121.00 169.00 184.96 65.970 190.44 171.61 176.89 174.24 182.25 161.29 66.090 151.29 151.29 144.00 136.89 125.44 116.64 66.210 114.49 90.25 118.81 104.04 96.04 84.64 66.330 75.69 64.00 67.24 62.41 50.41 67.24 66.450 59.29 59.29 64.00 54.76 53.29 56.25 66.570 73.96 38.44 60.84 56.25 43.56 50.41 66.690 59.29 46.24 64.00 60.84 51.84 67.24 66.810 42.25 59.29 47.61 68.89 59.29 88.36 66.930 73.96 79.21 77.44 77.44 73.96 79.21 67.050 86.49 104.04 88.36 106.09 104.04 153.76 67.170 198.81 216.09 265.69 327.61 364.81 462.25 67.290 510.76 466.56 408.04 416.16 338.56 338.56 67.410 306.25 309.76 292.41 306.25 316.84 292.41 67.530 262.44 231.04 193.21 163.84 153.76 151.29 67.650 129.96 132.25 125.44 100.00 102.01 86.49

171

File: JC7.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 70.56 81.00 79.21 72.25 62.41 68.89 67.890 67.24 65.61 75.69 62.41 56.25 65.61 68.010 84.64 81.00 79.21 84.64 75.69 62.41 68.130 82.81 64.00 62.41 67.24 88.36 72.25 68.250 75.69 81.00 59.29 68.89 75.69 43.56 68.370 56.25 59.29 49.00 54.76 47.61 50.41 68.490 53.29 50.41 50.41 56.25 43.56 50.41 68.610 42.25 44.89 31.36 38.44 51.84 43.56 68.730 40.96 33.64 47.61 53.29 43.56 47.61 68.850 43.56 50.41 56.25 46.24 44.89 42.25 68.970 43.56 47.61 56.25 42.25 56.25 32.49 69.090 53.29 36.00 44.89 42.25 51.84 46.24 69.210 42.25 50.41 36.00 42.25 34.81 43.56 69.330 50.41 34.81 49.00 37.21 44.89 54.76 69.450 43.56 53.29 47.61 39.69 49.00 50.41 69.570 38.44 39.69 42.25 34.81 47.61 47.61 69.690 50.41 49.00 53.29 53.29 56.25 50.41 69.810 59.29 56.25 62.41 56.25 62.41 67.24 69.930 68.89 64.00 65.61 65.61 _

172

File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC8 Data measured at: 25-Jan-2011 9:04:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 8968.090 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 77.44 65.61 65.61 73.96 60.84 67.24 2.130 73.96 57.76 57.76 79.21 60.84 64.00 2.250 51.84 65.61 51.84 54.76 62.41 70.56 2.370 75.69 57.76 56.25 49.00 59.29 67.24 2.490 46.24 62.41 56.25 51.84 56.25 51.84 2.610 50.41 59.29 51.84 47.61 38.44 50.41 2.730 47.61 44.89 50.41 50.41 60.84 46.24 2.850 50.41 53.29 50.41 49.00 42.25 40.96 2.970 65.61 40.96 50.41 67.24 56.25 56.25 3.090 51.84 62.41 62.41 39.69 65.61 47.61 3.210 38.44 51.84 42.25 40.96 50.41 47.61 3.330 49.00 51.84 53.29 65.61 42.25 65.61 3.450 38.44 56.25 53.29 53.29 49.00 65.61 3.570 62.41 51.84 44.89 43.56 56.25 57.76 3.690 56.25 56.25 62.41 39.69 57.76 60.84 3.810 53.29 49.00 47.61 43.56 46.24 50.41 3.930 47.61 59.29 62.41 67.24 56.25 47.61 4.050 53.29 56.25 43.56 51.84 43.56 50.41 4.170 47.61 44.89 59.29 56.25 47.61 53.29 4.290 44.89 56.25 62.41 62.41 38.44 44.89 4.410 47.61 38.44 50.41 59.29 53.29 38.44 4.530 49.00 51.84 56.25 53.29 50.41 46.24 4.650 38.44 47.61 60.84 53.29 51.84 38.44 4.770 62.41 57.76 51.84 51.84 56.25 49.00 4.890 39.69 65.61 59.29 49.00 46.24 67.24 5.010 50.41 56.25 65.61 50.41 50.41 43.56 5.130 60.84 54.76 51.84 50.41 46.24 50.41 5.250 53.29 50.41 50.41 51.84 51.84 56.25

173

File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 53.29 36.00 50.41 68.89 59.29 44.89 5.490 47.61 62.41 56.25 53.29 62.41 56.25 5.610 59.29 50.41 49.00 54.76 65.61 62.41 5.730 53.29 47.61 50.41 53.29 47.61 46.24 5.850 47.61 44.89 53.29 60.84 53.29 44.89 5.970 53.29 59.29 54.76 43.56 53.29 64.00 6.090 53.29 47.61 60.84 49.00 56.25 32.49 6.210 64.00 53.29 59.29 43.56 62.41 53.29 6.330 50.41 47.61 65.61 46.24 46.24 47.61 6.450 62.41 47.61 50.41 50.41 56.25 50.41 6.570 59.29 59.29 44.89 65.61 43.56 53.29 6.690 32.49 53.29 47.61 46.24 43.56 56.25 6.810 64.00 47.61 59.29 34.81 46.24 44.89 6.930 47.61 53.29 38.44 43.56 56.25 50.41 7.050 51.84 47.61 62.41 56.25 59.29 51.84 7.170 47.61 53.29 50.41 47.61 54.76 53.29 7.290 47.61 59.29 62.41 56.25 47.61 47.61 7.410 44.89 42.25 50.41 43.56 53.29 47.61 7.530 49.00 50.41 47.61 56.25 47.61 43.56 7.650 42.25 53.29 53.29 46.24 50.41 54.76 7.770 47.61 57.76 54.76 44.89 47.61 46.24 7.890 54.76 53.29 50.41 54.76 50.41 64.00 8.010 49.00 49.00 46.24 53.29 60.84 38.44 8.130 51.84 38.44 59.29 46.24 43.56 49.00 8.250 43.56 43.56 43.56 53.29 46.24 44.89 8.370 46.24 26.01 40.96 47.61 38.44 46.24 8.490 42.25 49.00 56.25 38.44 47.61 43.56 8.610 51.84 50.41 47.61 39.69 62.41 46.24 8.730 57.76 46.24 38.44 37.21 67.24 50.41 8.850 56.25 54.76 44.89 40.96 34.81 50.41 8.970 42.25 43.56 38.44 54.76 38.44 65.61 9.090 42.25 37.21 47.61 40.96 42.25 44.89 9.210 39.69 53.29 43.56 49.00 37.21 56.25 9.330 38.44 62.41 53.29 50.41 47.61 47.61 9.450 46.24 42.25 53.29 43.56 46.24 40.96 9.570 51.84 39.69 54.76 56.25 54.76 38.44 9.690 25.00 62.41 39.69 46.24 39.69 46.24 9.810 59.29 40.96 53.29 37.21 49.00 44.89 9.930 47.61 53.29 47.61 39.69 42.25 39.69 10.050 49.00 57.76 43.56 53.29 38.44 37.21 10.170 39.69 47.61 57.76 54.76 39.69 38.44 10.290 43.56 34.81 53.29 43.56 36.00 56.25 10.410 38.44 32.49 43.56 42.25 59.29 38.44 10.530 37.21 54.76 34.81 53.29 43.56 38.44 10.650 43.56 40.96 50.41 43.56 47.61 49.00 10.770 54.76 40.96 53.29 47.61 50.41 43.56 10.890 38.44 38.44 56.25 43.56 46.24 53.29 11.010 50.41 43.56 47.61 43.56 50.41 47.61 11.130 43.56 33.64 43.56 43.56 38.44 38.44 11.250 36.00 43.56 39.69 39.69 46.24 53.29 11.370 50.41 49.00 54.76 37.21 44.89 42.25 11.490 42.25 47.61 56.25 43.56 53.29 43.56

174

File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 32.49 50.41 39.69 47.61 57.76 37.21 11.730 37.21 34.81 46.24 38.44 47.61 37.21 11.850 38.44 50.41 28.09 36.00 43.56 43.56 11.970 39.69 49.00 32.49 39.69 33.64 56.25 12.090 38.44 47.61 38.44 47.61 49.00 51.84 12.210 43.56 38.44 30.25 37.21 56.25 47.61 12.330 38.44 39.69 43.56 49.00 38.44 50.41 12.450 43.56 40.96 44.89 50.41 50.41 50.41 12.570 38.44 47.61 43.56 47.61 37.21 51.84 12.690 42.25 47.61 38.44 38.44 36.00 33.64 12.810 32.49 42.25 38.44 49.00 47.61 32.49 12.930 38.44 39.69 56.25 36.00 42.25 39.69 13.050 43.56 37.21 47.61 47.61 30.25 50.41 13.170 50.41 46.24 49.00 30.25 28.09 44.89 13.290 40.96 29.16 50.41 40.96 44.89 38.44 13.410 49.00 43.56 31.36 47.61 40.96 32.49 13.530 33.64 47.61 54.76 40.96 39.69 54.76 13.650 44.89 47.61 39.69 42.25 40.96 38.44 13.770 26.01 24.01 40.96 43.56 50.41 46.24 13.890 32.49 43.56 50.41 39.69 47.61 36.00 14.010 53.29 50.41 47.61 43.56 42.25 38.44 14.130 49.00 37.21 42.25 39.69 50.41 32.49 14.250 51.84 43.56 43.56 43.56 36.00 54.76 14.370 34.81 53.29 44.89 26.01 43.56 40.96 14.490 49.00 34.81 38.44 47.61 36.00 50.41 14.610 33.64 46.24 37.21 49.00 43.56 44.89 14.730 43.56 46.24 44.89 50.41 47.61 43.56 14.850 43.56 42.25 62.41 50.41 36.00 44.89 14.970 34.81 40.96 47.61 43.56 47.61 49.00 15.090 43.56 50.41 44.89 43.56 50.41 43.56 15.210 59.29 53.29 62.41 54.76 56.25 44.89 15.330 59.29 60.84 56.25 59.29 50.41 47.61 15.450 51.84 47.61 62.41 59.29 62.41 53.29 15.570 59.29 53.29 59.29 68.89 67.24 62.41 15.690 65.61 49.00 56.25 53.29 46.24 60.84 15.810 59.29 53.29 67.24 62.41 47.61 67.24 15.930 47.61 56.25 50.41 51.84 40.96 60.84 16.050 57.76 43.56 59.29 50.41 60.84 47.61 16.170 50.41 47.61 59.29 56.25 47.61 67.24 16.290 37.21 57.76 62.41 44.89 56.25 57.76 16.410 51.84 47.61 51.84 57.76 64.00 43.56 16.530 65.61 53.29 51.84 39.69 56.25 50.41 16.650 37.21 54.76 53.29 53.29 51.84 47.61 16.770 47.61 47.61 42.25 53.29 50.41 50.41 16.890 50.41 43.56 43.56 50.41 47.61 47.61 17.010 39.69 46.24 38.44 43.56 46.24 39.69 17.130 49.00 44.89 49.00 33.64 62.41 53.29 17.250 46.24 40.96 37.21 34.81 43.56 31.36 17.370 47.61 57.76 43.56 43.56 42.25 38.44 17.490 38.44 44.89 42.25 51.84 53.29 38.44 17.610 29.16 38.44 47.61 40.96 40.96 43.56 17.730 33.64 47.61 43.56 38.44 47.61 40.96

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 39.69 38.44 42.25 38.44 36.00 38.44 17.970 31.36 44.89 43.56 38.44 32.49 39.69 18.090 53.29 56.25 43.56 40.96 32.49 39.69 18.210 50.41 34.81 42.25 40.96 37.21 31.36 18.330 43.56 42.25 39.69 47.61 44.89 42.25 18.450 53.29 40.96 37.21 38.44 46.24 43.56 18.570 49.00 43.56 50.41 49.00 43.56 54.76 18.690 34.81 50.41 32.49 39.69 44.89 34.81 18.810 43.56 43.56 40.96 50.41 42.25 43.56 18.930 27.04 47.61 43.56 40.96 50.41 43.56 19.050 43.56 32.49 39.69 34.81 43.56 29.16 19.170 47.61 47.61 34.81 43.56 38.44 50.41 19.290 50.41 32.49 47.61 53.29 37.21 44.89 19.410 46.24 47.61 39.69 42.25 32.49 47.61 19.530 38.44 42.25 42.25 50.41 44.89 40.96 19.650 40.96 50.41 51.84 43.56 51.84 30.25 19.770 43.56 50.41 40.96 38.44 44.89 38.44 19.890 49.00 49.00 50.41 38.44 27.04 43.56 20.010 24.01 40.96 28.09 47.61 42.25 39.69 20.130 32.49 44.89 44.89 49.00 38.44 37.21 20.250 54.76 51.84 43.56 31.36 42.25 38.44 20.370 33.64 47.61 40.96 49.00 56.25 46.24 20.490 60.84 38.44 43.56 43.56 42.25 47.61 20.610 38.44 40.96 50.41 43.56 43.56 65.61 20.730 44.89 47.61 56.25 79.21 75.69 166.41 20.850 219.04 249.64 207.36 163.84 116.64 96.04 20.970 49.00 50.41 47.61 49.00 50.41 40.96 21.090 47.61 42.25 39.69 37.21 42.25 37.21 21.210 32.49 46.24 46.24 36.00 37.21 42.25 21.330 47.61 36.00 38.44 40.96 27.04 43.56 21.450 43.56 32.49 38.44 47.61 25.00 56.25 21.570 38.44 26.01 34.81 42.25 27.04 40.96 21.690 53.29 42.25 53.29 43.56 44.89 44.89 21.810 47.61 44.89 47.61 50.41 46.24 62.41 21.930 67.24 53.29 50.41 62.41 77.44 70.56 22.050 82.81 88.36 88.36 65.61 59.29 57.76 22.170 47.61 49.00 38.44 50.41 38.44 32.49 22.290 53.29 47.61 47.61 32.49 32.49 37.21 22.410 36.00 32.49 47.61 39.69 33.64 36.00 22.530 38.44 42.25 44.89 42.25 38.44 33.64 22.650 43.56 56.25 38.44 44.89 50.41 38.44 22.770 28.09 47.61 31.36 37.21 53.29 37.21 22.890 34.81 32.49 38.44 37.21 40.96 38.44 23.010 50.41 43.56 42.25 39.69 43.56 32.49 23.130 38.44 42.25 36.00 40.96 47.61 47.61 23.250 34.81 34.81 27.04 29.16 30.25 33.64 23.370 42.25 37.21 43.56 39.69 32.49 44.89 23.490 43.56 36.00 32.49 39.69 29.16 25.00 23.610 38.44 39.69 37.21 33.64 43.56 49.00 23.730 50.41 47.61 33.64 43.56 60.84 47.61 23.850 44.89 43.56 56.25 70.56 56.25 86.49 23.970 59.29 67.24 92.16 92.16 141.61 146.41

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 179.56 171.61 184.96 139.24 129.96 112.36 24.210 60.84 57.76 51.84 32.49 34.81 47.61 24.330 44.89 36.00 47.61 43.56 46.24 38.44 24.450 37.21 43.56 30.25 47.61 38.44 32.49 24.570 50.41 38.44 46.24 46.24 28.09 37.21 24.690 38.44 43.56 38.44 46.24 26.01 32.49 24.810 38.44 40.96 40.96 34.81 50.41 29.16 24.930 38.44 33.64 44.89 33.64 37.21 43.56 25.050 39.69 50.41 31.36 46.24 30.25 46.24 25.170 43.56 32.49 36.00 51.84 42.25 43.56 25.290 36.00 44.89 50.41 53.29 32.49 53.29 25.410 47.61 32.49 43.56 43.56 44.89 38.44 25.530 32.49 38.44 30.25 42.25 38.44 43.56 25.650 34.81 40.96 47.61 38.44 34.81 36.00 25.770 49.00 42.25 34.81 31.36 42.25 39.69 25.890 32.49 36.00 46.24 38.44 32.49 32.49 26.010 32.49 39.69 40.96 31.36 32.49 36.00 26.130 43.56 34.81 37.21 43.56 43.56 51.84 26.250 43.56 39.69 49.00 60.84 49.00 50.41 26.370 37.21 47.61 46.24 57.76 56.25 77.44 26.490 92.16 102.01 134.56 196.00 234.09 231.04 26.610 225.00 207.36 222.01 184.96 144.00 151.29 26.730 112.36 102.01 90.25 72.25 54.76 47.61 26.850 37.21 54.76 38.44 47.61 34.81 50.41 26.970 30.25 43.56 40.96 43.56 50.41 30.25 27.090 32.49 46.24 32.49 53.29 32.49 29.16 27.210 32.49 29.16 53.29 38.44 28.09 32.49 27.330 36.00 27.04 32.49 43.56 31.36 33.64 27.450 34.81 37.21 33.64 46.24 37.21 33.64 27.570 37.21 40.96 32.49 47.61 31.36 32.49 27.690 42.25 44.89 43.56 37.21 38.44 42.25 27.810 37.21 47.61 37.21 47.61 30.25 31.36 27.930 22.09 32.49 34.81 30.25 33.64 42.25 28.050 36.00 47.61 32.49 36.00 34.81 39.69 28.170 32.49 42.25 32.49 46.24 37.21 39.69 28.290 40.96 43.56 36.00 33.64 39.69 37.21 28.410 47.61 31.36 40.96 43.56 42.25 38.44 28.530 27.04 32.49 26.01 34.81 32.49 37.21 28.650 37.21 37.21 27.04 31.36 28.09 43.56 28.770 47.61 38.44 40.96 40.96 43.56 32.49 28.890 46.24 42.25 43.56 31.36 39.69 42.25 29.010 37.21 43.56 51.84 43.56 49.00 43.56 29.130 47.61 43.56 42.25 44.89 56.25 53.29 29.250 54.76 56.25 46.24 53.29 60.84 53.29 29.370 73.96 77.44 86.49 102.01 104.04 116.64 29.490 116.64 104.04 84.64 59.29 73.96 68.89 29.610 62.41 43.56 50.41 59.29 43.56 42.25 29.730 43.56 67.24 47.61 43.56 62.41 47.61 29.850 47.61 75.69 51.84 60.84 56.25 60.84 29.970 68.89 56.25 64.00 43.56 57.76 73.96 30.090 75.69 70.56 59.29 90.25 90.25 75.69 30.210 98.01 84.64 100.00 92.16 116.64 132.25

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 127.69 139.24 198.81 174.24 216.09 207.36 30.450 272.25 292.41 345.96 376.36 428.49 453.69 30.570 519.84 561.69 630.01 691.69 756.25 894.01 30.690 1122.25 1421.29 1918.44 2440.36 3025.00 3329.29 30.810 3660.25 4096.00 4529.29 5299.84 6162.25 7157.16 30.930 7691.29 8519.29 8968.09 8611.84 7779.24 6707.61 31.050 5550.25 4251.04 3340.84 2440.36 1722.25 1332.25 31.170 967.21 829.44 665.64 600.25 529.00 457.96 31.290 364.81 278.89 306.25 278.89 237.16 201.64 31.410 210.25 171.61 182.25 163.84 139.24 129.96 31.530 106.09 110.25 123.21 106.09 114.49 108.16 31.650 84.64 90.25 84.64 77.44 88.36 73.96 31.770 72.25 88.36 73.96 86.49 72.25 75.69 31.890 72.25 79.21 65.61 62.41 70.56 72.25 32.010 50.41 65.61 65.61 56.25 51.84 53.29 32.130 56.25 56.25 54.76 62.41 62.41 56.25 32.250 54.76 56.25 46.24 42.25 54.76 49.00 32.370 49.00 54.76 42.25 50.41 51.84 46.24 32.490 43.56 44.89 39.69 42.25 43.56 44.89 32.610 50.41 53.29 50.41 40.96 47.61 43.56 32.730 53.29 43.56 37.21 46.24 44.89 47.61 32.850 38.44 42.25 43.56 46.24 47.61 47.61 32.970 44.89 44.89 43.56 42.25 51.84 47.61 33.090 51.84 56.25 54.76 70.56 88.36 84.64 33.210 79.21 92.16 98.01 116.64 127.69 132.25 33.330 158.76 171.61 179.56 163.84 196.00 210.25 33.450 262.44 334.89 384.16 457.96 538.24 552.25 33.570 547.56 538.24 470.89 376.36 361.00 282.24 33.690 256.00 210.25 169.00 146.41 110.25 110.25 33.810 86.49 64.00 68.89 72.25 64.00 47.61 33.930 53.29 57.76 53.29 46.24 47.61 44.89 34.050 53.29 59.29 47.61 46.24 51.84 43.56 34.170 46.24 37.21 47.61 43.56 44.89 40.96 34.290 28.09 43.56 28.09 43.56 47.61 38.44 34.410 50.41 43.56 43.56 36.00 36.00 32.49 34.530 36.00 40.96 47.61 28.09 47.61 42.25 34.650 36.00 40.96 40.96 49.00 43.56 56.25 34.770 38.44 46.24 38.44 47.61 50.41 43.56 34.890 59.29 56.25 53.29 62.41 56.25 68.89 35.010 56.25 62.41 77.44 106.09 90.25 108.16 35.130 121.00 151.29 163.84 201.64 228.01 262.44 35.250 275.56 324.00 388.09 380.25 428.49 424.36 35.370 357.21 292.41 285.61 275.56 207.36 174.24 35.490 153.76 123.21 98.01 88.36 98.01 77.44 35.610 72.25 57.76 47.61 42.25 53.29 47.61 35.730 53.29 47.61 37.21 42.25 33.64 47.61 35.850 38.44 34.81 42.25 47.61 50.41 32.49 35.970 47.61 44.89 36.00 51.84 43.56 38.44 36.090 39.69 43.56 46.24 32.49 38.44 33.64 36.210 34.81 32.49 33.64 53.29 42.25 38.44 36.330 34.81 37.21 50.41 49.00 50.41 39.69 36.450 49.00 54.76 50.41 56.25 43.56 59.29

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File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 57.76 59.29 49.00 50.41 70.56 62.41 36.690 47.61 51.84 56.25 50.41 65.61 50.41 36.810 59.29 50.41 53.29 56.25 51.84 62.41 36.930 59.29 47.61 62.41 51.84 53.29 56.25 37.050 65.61 68.89 53.29 56.25 67.24 53.29 37.170 70.56 70.56 84.64 86.49 90.25 110.25 37.290 123.21 146.41 144.00 176.89 166.41 193.21 37.410 196.00 166.41 158.76 125.44 96.04 94.09 37.530 90.25 62.41 67.24 57.76 42.25 40.96 37.650 42.25 47.61 38.44 33.64 43.56 47.61 37.770 33.64 32.49 38.44 33.64 43.56 43.56 37.890 34.81 39.69 51.84 32.49 37.21 38.44 38.010 32.49 30.25 50.41 34.81 31.36 32.49 38.130 37.21 31.36 29.16 27.04 27.04 36.00 38.250 38.44 33.64 40.96 33.64 36.00 42.25 38.370 44.89 47.61 38.44 27.04 38.44 38.44 38.490 38.44 30.25 32.49 44.89 25.00 39.69 38.610 34.81 33.64 34.81 37.21 22.09 33.64 38.730 25.00 40.96 36.00 38.44 43.56 32.49 38.850 32.49 37.21 32.49 31.36 32.49 31.36 38.970 34.81 36.00 44.89 42.25 38.44 43.56 39.090 43.56 38.44 44.89 32.49 43.56 47.61 39.210 36.00 42.25 34.81 42.25 49.00 33.64 39.330 43.56 53.29 34.81 51.84 39.69 43.56 39.450 50.41 62.41 79.21 70.56 70.56 67.24 39.570 62.41 64.00 51.84 56.25 59.29 53.29 39.690 56.25 70.56 54.76 50.41 62.41 54.76 39.810 68.89 62.41 72.25 59.29 79.21 62.41 39.930 62.41 68.89 75.69 70.56 54.76 54.76 40.050 50.41 53.29 57.76 53.29 40.96 37.21 40.170 44.89 62.41 43.56 44.89 47.61 47.61 40.290 46.24 33.64 50.41 43.56 47.61 32.49 40.410 39.69 31.36 43.56 37.21 32.49 32.49 40.530 43.56 38.44 36.00 34.81 65.61 34.81 40.650 56.25 59.29 72.25 72.25 67.24 70.56 40.770 72.25 79.21 96.04 90.25 102.01 156.25 40.890 148.84 184.96 246.49 320.41 420.25 590.49 41.010 745.29 852.64 979.69 1062.76 1102.24 1218.01 41.130 1239.04 1197.16 1108.89 967.21 852.64 750.76 41.250 665.64 542.89 400.00 320.41 219.04 184.96 41.370 153.76 139.24 98.01 94.09 96.04 65.61 41.490 67.24 64.00 59.29 57.76 57.76 53.29 41.610 56.25 50.41 53.29 42.25 38.44 50.41 41.730 36.00 32.49 38.44 36.00 43.56 34.81 41.850 42.25 40.96 40.96 26.01 31.36 38.44 41.970 32.49 32.49 32.49 38.44 46.24 32.49 42.090 36.00 43.56 32.49 36.00 30.25 30.25 42.210 39.69 39.69 39.69 33.64 57.76 67.24 42.330 68.89 77.44 57.76 60.84 53.29 60.84 42.450 43.56 54.76 40.96 50.41 32.49 32.49 42.570 54.76 38.44 36.00 37.21 39.69 51.84 42.690 28.09 42.25 32.49 33.64 43.56 36.00

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File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 38.44 38.44 38.44 39.69 34.81 28.09 42.930 49.00 42.25 38.44 36.00 37.21 33.64 43.050 38.44 27.04 37.21 36.00 43.56 42.25 43.170 38.44 44.89 38.44 51.84 42.25 47.61 43.290 43.56 42.25 38.44 40.96 31.36 36.00 43.410 27.04 30.25 36.00 44.89 56.25 50.41 43.530 53.29 57.76 56.25 53.29 67.24 77.44 43.650 94.09 106.09 106.09 127.69 118.81 129.96 43.770 116.64 129.96 108.16 112.36 127.69 94.09 43.890 104.04 72.25 75.69 64.00 53.29 57.76 44.010 56.25 54.76 32.49 43.56 47.61 49.00 44.130 36.00 50.41 34.81 38.44 33.64 53.29 44.250 50.41 49.00 42.25 51.84 50.41 33.64 44.370 38.44 46.24 54.76 42.25 51.84 50.41 44.490 42.25 50.41 65.61 59.29 60.84 81.00 44.610 70.56 92.16 86.49 129.96 139.24 198.81 44.730 268.96 353.44 392.04 420.25 404.01 441.00 44.850 492.84 515.29 571.21 605.16 676.00 620.01 44.970 529.00 428.49 396.01 361.00 345.96 302.76 45.090 299.29 201.64 176.89 144.00 118.81 106.09 45.210 98.01 88.36 88.36 79.21 59.29 73.96 45.330 53.29 72.25 70.56 49.00 49.00 50.41 45.450 47.61 51.84 46.24 47.61 47.61 47.61 45.570 44.89 37.21 47.61 49.00 49.00 40.96 45.690 42.25 40.96 36.00 47.61 54.76 50.41 45.810 38.44 39.69 44.89 53.29 34.81 50.41 45.930 37.21 32.49 39.69 44.89 33.64 44.89 46.050 46.24 43.56 40.96 32.49 38.44 57.76 46.170 33.64 27.04 42.25 46.24 44.89 50.41 46.290 49.00 38.44 49.00 46.24 43.56 46.24 46.410 32.49 47.61 43.56 50.41 51.84 54.76 46.530 62.41 54.76 54.76 59.29 50.41 50.41 46.650 59.29 47.61 46.24 62.41 51.84 44.89 46.770 46.24 40.96 43.56 46.24 46.24 46.24 46.890 50.41 50.41 50.41 36.00 46.24 43.56 47.010 32.49 43.56 42.25 38.44 42.25 33.64 47.130 38.44 42.25 36.00 34.81 47.61 39.69 47.250 50.41 43.56 44.89 47.61 42.25 38.44 47.370 38.44 43.56 43.56 38.44 50.41 49.00 47.490 50.41 42.25 54.76 50.41 33.64 42.25 47.610 50.41 47.61 34.81 37.21 42.25 44.89 47.730 32.49 34.81 39.69 37.21 39.69 37.21 47.850 44.89 38.44 40.96 59.29 43.56 38.44 47.970 44.89 24.01 47.61 40.96 36.00 33.64 48.090 47.61 49.00 40.96 38.44 53.29 43.56 48.210 46.24 47.61 50.41 49.00 43.56 46.24 48.330 40.96 40.96 43.56 51.84 36.00 57.76 48.450 39.69 38.44 47.61 56.25 43.56 51.84 48.570 57.76 42.25 53.29 49.00 49.00 43.56 48.690 47.61 50.41 34.81 62.41 53.29 47.61 48.810 42.25 42.25 50.41 67.24 59.29 59.29 48.930 57.76 75.69 77.44 65.61 70.56 84.64

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File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 92.16 114.49 114.49 106.09 132.25 146.41 49.170 148.84 196.00 213.16 228.01 259.21 228.01 49.290 240.25 237.16 225.00 169.00 207.36 166.41 49.410 161.29 190.44 134.56 127.69 110.25 94.09 49.530 96.04 72.25 75.69 70.56 60.84 68.89 49.650 62.41 72.25 70.56 67.24 84.64 64.00 49.770 67.24 72.25 72.25 77.44 81.00 79.21 49.890 72.25 81.00 108.16 106.09 118.81 108.16 50.010 110.25 121.00 110.25 153.76 187.69 182.25 50.130 198.81 231.04 282.24 285.61 295.84 361.00 50.250 388.09 470.89 552.25 605.16 707.56 795.24 50.370 858.49 973.44 1075.84 1296.00 1376.41 1428.84 50.490 1616.04 1600.00 1681.00 1705.69 1592.01 1497.69 50.610 1521.00 1406.25 1246.09 1169.64 1017.61 924.16 50.730 852.64 745.29 712.89 635.04 665.64 665.64 50.850 660.49 718.24 772.84 812.25 864.36 948.64 50.970 1062.76 1102.24 1142.44 1218.01 1303.21 1332.25 51.090 1218.01 1197.16 1122.25 1108.89 992.25 967.21 51.210 858.49 789.61 750.76 660.49 600.25 510.76 51.330 470.89 428.49 396.01 353.44 285.61 285.61 51.450 213.16 210.25 179.56 163.84 163.84 136.89 51.570 127.69 112.36 108.16 88.36 84.64 94.09 51.690 70.56 67.24 79.21 60.84 92.16 68.89 51.810 51.84 65.61 64.00 65.61 54.76 50.41 51.930 53.29 51.84 62.41 53.29 47.61 50.41 52.050 46.24 54.76 50.41 64.00 59.29 40.96 52.170 50.41 64.00 43.56 49.00 59.29 62.41 52.290 62.41 51.84 70.56 70.56 50.41 54.76 52.410 72.25 65.61 56.25 53.29 56.25 57.76 52.530 44.89 68.89 34.81 43.56 38.44 43.56 52.650 37.21 40.96 47.61 39.69 33.64 43.56 52.770 39.69 36.00 43.56 42.25 34.81 36.00 52.890 43.56 33.64 33.64 37.21 47.61 43.56 53.010 40.96 44.89 44.89 43.56 43.56 31.36 53.130 47.61 49.00 36.00 40.96 53.29 38.44 53.250 36.00 33.64 37.21 47.61 36.00 38.44 53.370 36.00 31.36 36.00 39.69 29.16 32.49 53.490 38.44 40.96 50.41 33.64 37.21 38.44 53.610 42.25 25.00 38.44 32.49 36.00 37.21 53.730 39.69 27.04 46.24 47.61 38.44 38.44 53.850 38.44 36.00 31.36 29.16 42.25 32.49 53.970 38.44 25.00 25.00 34.81 43.56 34.81 54.090 26.01 28.09 38.44 31.36 32.49 38.44 54.210 37.21 30.25 30.25 31.36 38.44 29.16 54.330 33.64 25.00 43.56 36.00 32.49 31.36 54.450 28.09 39.69 36.00 25.00 42.25 43.56 54.570 31.36 32.49 31.36 30.25 33.64 31.36 54.690 28.09 36.00 34.81 53.29 42.25 50.41 54.810 36.00 57.76 38.44 53.29 43.56 30.25 54.930 37.21 34.81 32.49 38.44 33.64 37.21 55.050 50.41 40.96 30.25 28.09 42.25 39.69 55.170 36.00 38.44 36.00 37.21 30.25 36.00

181

File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 42.25 44.89 34.81 30.25 47.61 26.01 55.410 36.00 28.09 31.36 33.64 25.00 34.81 55.530 34.81 29.16 29.16 34.81 30.25 34.81 55.650 29.16 31.36 32.49 37.21 36.00 33.64 55.770 31.36 39.69 36.00 29.16 42.25 39.69 55.890 46.24 47.61 38.44 32.49 34.81 33.64 56.010 31.36 32.49 32.49 29.16 34.81 27.04 56.130 43.56 38.44 23.04 21.16 38.44 38.44 56.250 29.16 38.44 36.00 36.00 30.25 31.36 56.370 40.96 26.01 44.89 25.00 38.44 32.49 56.490 29.16 39.69 31.36 43.56 40.96 38.44 56.610 39.69 30.25 28.09 36.00 34.81 32.49 56.730 30.25 29.16 29.16 42.25 33.64 36.00 56.850 33.64 31.36 24.01 29.16 36.00 21.16 56.970 43.56 39.69 37.21 30.25 32.49 28.09 57.090 32.49 19.36 26.01 31.36 37.21 30.25 57.210 31.36 30.25 32.49 31.36 33.64 33.64 57.330 47.61 37.21 28.09 29.16 32.49 36.00 57.450 43.56 32.49 34.81 30.25 42.25 32.49 57.570 38.44 36.00 38.44 42.25 25.00 33.64 57.690 26.01 38.44 34.81 21.16 47.61 38.44 57.810 36.00 42.25 26.01 29.16 36.00 24.01 57.930 38.44 37.21 38.44 30.25 23.04 33.64 58.050 38.44 34.81 38.44 38.44 36.00 37.21 58.170 38.44 22.09 34.81 22.09 24.01 31.36 58.290 32.49 38.44 32.49 38.44 31.36 38.44 58.410 29.16 42.25 43.56 30.25 28.09 47.61 58.530 44.89 38.44 50.41 49.00 54.76 60.84 58.650 56.25 67.24 68.89 96.04 121.00 100.00 58.770 121.00 187.69 179.56 207.36 231.04 225.00 58.890 196.00 196.00 176.89 182.25 151.29 169.00 59.010 151.29 144.00 121.00 123.21 123.21 102.01 59.130 82.81 62.41 62.41 51.84 40.96 53.29 59.250 49.00 46.24 47.61 53.29 42.25 59.29 59.370 59.29 54.76 51.84 46.24 64.00 57.76 59.490 81.00 65.61 86.49 100.00 121.00 156.25 59.610 193.21 198.81 246.49 240.25 256.00 292.41 59.730 268.96 289.00 275.56 265.69 265.69 285.61 59.850 249.64 219.04 213.16 210.25 176.89 166.41 59.970 146.41 136.89 121.00 106.09 94.09 84.64 60.090 88.36 62.41 53.29 62.41 49.00 53.29 60.210 59.29 36.00 50.41 40.96 33.64 43.56 60.330 49.00 46.24 36.00 33.64 42.25 43.56 60.450 33.64 49.00 32.49 36.00 43.56 32.49 60.570 32.49 34.81 38.44 43.56 33.64 39.69 60.690 26.01 37.21 43.56 46.24 51.84 37.21 60.810 50.41 36.00 37.21 32.49 38.44 37.21 60.930 32.49 42.25 43.56 42.25 38.44 33.64 61.050 29.16 42.25 31.36 39.69 32.49 28.09 61.170 29.16 43.56 40.96 47.61 50.41 39.69 61.290 31.36 38.44 31.36 43.56 36.00 46.24 61.410 38.44 38.44 36.00 49.00 19.36 34.81

182

File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 40.96 32.49 47.61 44.89 51.84 44.89 61.650 62.41 47.61 62.41 49.00 47.61 47.61 61.770 65.61 75.69 72.25 68.89 65.61 86.49 61.890 79.21 92.16 96.04 79.21 112.36 82.81 62.010 94.09 108.16 102.01 90.25 116.64 88.36 62.130 98.01 90.25 86.49 75.69 84.64 57.76 62.250 70.56 62.41 51.84 60.84 53.29 65.61 62.370 42.25 38.44 54.76 47.61 39.69 40.96 62.490 37.21 43.56 46.24 56.25 27.04 17.64 62.610 38.44 50.41 37.21 36.00 43.56 37.21 62.730 42.25 47.61 59.29 38.44 47.61 59.29 62.850 32.49 44.89 44.89 39.69 56.25 59.29 62.970 51.84 67.24 49.00 62.41 73.96 75.69 63.090 67.24 75.69 77.44 96.04 90.25 106.09 63.210 116.64 129.96 129.96 179.56 210.25 216.09 63.330 275.56 295.84 368.64 338.56 384.16 380.25 63.450 388.09 342.25 309.76 285.61 278.89 249.64 63.570 246.49 249.64 204.49 182.25 187.69 161.29 63.690 125.44 121.00 102.01 68.89 67.24 90.25 63.810 84.64 72.25 65.61 62.41 59.29 65.61 63.930 65.61 70.56 62.41 67.24 70.56 77.44 64.050 77.44 70.56 84.64 77.44 84.64 84.64 64.170 86.49 102.01 108.16 125.44 127.69 158.76 64.290 129.96 193.21 210.25 234.09 302.76 320.41 64.410 353.44 361.00 380.25 428.49 424.36 466.56 64.530 449.44 424.36 342.25 384.16 316.84 316.84 64.650 320.41 285.61 268.96 249.64 231.04 225.00 64.770 190.44 179.56 148.84 171.61 169.00 161.29 64.890 174.24 161.29 179.56 176.89 213.16 207.36 65.010 234.09 243.36 243.36 282.24 292.41 292.41 65.130 285.61 292.41 256.00 268.96 295.84 265.69 65.250 222.01 225.00 210.25 204.49 161.29 182.25 65.370 146.41 139.24 129.96 129.96 98.01 92.16 65.490 100.00 86.49 73.96 81.00 72.25 68.89 65.610 72.25 70.56 59.29 70.56 62.41 70.56 65.730 70.56 59.29 65.61 70.56 64.00 98.01 65.850 96.04 98.01 121.00 125.44 127.69 136.89 65.970 161.29 141.61 161.29 146.41 146.41 144.00 66.090 136.89 134.56 116.64 102.01 104.04 100.00 66.210 90.25 104.04 75.69 88.36 56.25 64.00 66.330 77.44 67.24 67.24 62.41 53.29 53.29 66.450 54.76 43.56 43.56 36.00 33.64 33.64 66.570 49.00 50.41 33.64 43.56 43.56 29.16 66.690 38.44 46.24 44.89 34.81 36.00 46.24 66.810 43.56 43.56 42.25 62.41 53.29 50.41 66.930 47.61 47.61 50.41 59.29 60.84 68.89 67.050 65.61 70.56 75.69 84.64 79.21 104.04 67.170 102.01 112.36 134.56 158.76 193.21 249.64 67.290 246.49 292.41 299.29 331.24 313.29 306.25 67.410 302.76 309.76 285.61 237.16 256.00 234.09 67.530 196.00 228.01 196.00 182.25 161.29 132.25 67.650 104.04 102.01 116.64 84.64 72.25 72.25

183

File: JC8.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 65.61 56.25 70.56 59.29 64.00 65.61 67.890 57.76 43.56 47.61 54.76 53.29 49.00 68.010 67.24 50.41 49.00 67.24 53.29 42.25 68.130 79.21 43.56 57.76 56.25 56.25 50.41 68.250 56.25 56.25 43.56 62.41 75.69 54.76 68.370 54.76 50.41 53.29 40.96 49.00 57.76 68.490 42.25 46.24 43.56 50.41 47.61 54.76 68.610 36.00 38.44 56.25 51.84 33.64 47.61 68.730 40.96 43.56 44.89 44.89 43.56 34.81 68.850 37.21 43.56 36.00 32.49 32.49 37.21 68.970 44.89 47.61 38.44 39.69 43.56 31.36 69.090 43.56 34.81 39.69 43.56 49.00 38.44 69.210 43.56 34.81 38.44 47.61 57.76 42.25 69.330 38.44 59.29 44.89 50.41 46.24 47.61 69.450 44.89 46.24 43.56 38.44 53.29 44.89 69.570 40.96 47.61 43.56 47.61 50.41 57.76 69.690 56.25 49.00 53.29 47.61 42.25 70.56 69.810 67.24 62.41 57.76 59.29 50.41 79.21 69.930 75.69 75.69 82.81 84.64 _

184

File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC9 Data measured at: 25-Jan-2011 10:02:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 6609.690 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 129.96 121.00 100.00 100.00 118.81 106.09 2.130 88.36 110.25 82.81 90.25 102.01 86.49 2.250 81.00 94.09 96.04 67.24 82.81 72.25 2.370 68.89 72.25 72.25 65.61 82.81 75.69 2.490 94.09 62.41 75.69 108.16 68.89 57.76 2.610 70.56 86.49 72.25 84.64 88.36 65.61 2.730 67.24 79.21 56.25 70.56 53.29 62.41 2.850 51.84 57.76 62.41 70.56 67.24 67.24 2.970 65.61 68.89 60.84 54.76 59.29 50.41 3.090 70.56 70.56 59.29 59.29 50.41 75.69 3.210 57.76 67.24 59.29 60.84 65.61 64.00 3.330 75.69 56.25 65.61 59.29 56.25 67.24 3.450 70.56 67.24 60.84 62.41 62.41 62.41 3.570 65.61 50.41 53.29 57.76 67.24 39.69 3.690 72.25 60.84 57.76 62.41 65.61 57.76 3.810 77.44 59.29 72.25 56.25 56.25 53.29 3.930 65.61 53.29 54.76 62.41 59.29 54.76 4.050 59.29 49.00 56.25 47.61 68.89 53.29 4.170 62.41 70.56 56.25 75.69 43.56 60.84 4.290 49.00 59.29 60.84 72.25 57.76 65.61 4.410 53.29 72.25 57.76 53.29 51.84 75.69 4.530 65.61 65.61 62.41 50.41 62.41 59.29 4.650 59.29 65.61 51.84 62.41 62.41 70.56 4.770 49.00 57.76 65.61 56.25 56.25 60.84 4.890 60.84 50.41 65.61 56.25 57.76 57.76 5.010 62.41 60.84 59.29 51.84 59.29 62.41 5.130 56.25 56.25 54.76 72.25 56.25 64.00 5.250 62.41 65.61 62.41 81.00 53.29 62.41

185

File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 54.76 57.76 46.24 60.84 75.69 62.41 5.490 72.25 50.41 49.00 62.41 56.25 77.44 5.610 56.25 46.24 56.25 67.24 56.25 65.61 5.730 65.61 47.61 59.29 64.00 59.29 53.29 5.850 50.41 56.25 59.29 44.89 67.24 50.41 5.970 65.61 70.56 64.00 44.89 54.76 56.25 6.090 42.25 56.25 59.29 59.29 65.61 54.76 6.210 46.24 44.89 49.00 64.00 56.25 59.29 6.330 53.29 46.24 60.84 47.61 46.24 42.25 6.450 60.84 42.25 40.96 56.25 57.76 54.76 6.570 50.41 64.00 50.41 59.29 50.41 57.76 6.690 59.29 38.44 60.84 51.84 56.25 49.00 6.810 51.84 49.00 50.41 38.44 56.25 43.56 6.930 57.76 75.69 47.61 53.29 59.29 51.84 7.050 43.56 49.00 59.29 56.25 50.41 53.29 7.170 46.24 49.00 50.41 54.76 65.61 53.29 7.290 49.00 50.41 50.41 53.29 62.41 38.44 7.410 50.41 43.56 49.00 54.76 47.61 53.29 7.530 62.41 56.25 56.25 57.76 56.25 46.24 7.650 38.44 47.61 49.00 56.25 50.41 50.41 7.770 44.89 59.29 47.61 59.29 46.24 47.61 7.890 50.41 47.61 49.00 43.56 59.29 47.61 8.010 49.00 50.41 53.29 56.25 56.25 62.41 8.130 60.84 50.41 53.29 50.41 49.00 47.61 8.250 53.29 51.84 47.61 62.41 53.29 57.76 8.370 42.25 47.61 62.41 62.41 43.56 53.29 8.490 53.29 59.29 50.41 38.44 59.29 43.56 8.610 39.69 43.56 44.89 50.41 54.76 53.29 8.730 44.89 53.29 44.89 50.41 51.84 70.56 8.850 50.41 47.61 50.41 43.56 57.76 50.41 8.970 56.25 50.41 54.76 39.69 62.41 49.00 9.090 53.29 62.41 38.44 50.41 44.89 50.41 9.210 56.25 43.56 50.41 59.29 40.96 65.61 9.330 47.61 49.00 50.41 32.49 62.41 34.81 9.450 38.44 53.29 47.61 53.29 33.64 53.29 9.570 53.29 50.41 67.24 44.89 47.61 42.25 9.690 50.41 40.96 46.24 53.29 50.41 53.29 9.810 54.76 53.29 56.25 47.61 56.25 42.25 9.930 53.29 53.29 53.29 44.89 56.25 44.89 10.050 47.61 38.44 56.25 43.56 62.41 43.56 10.170 47.61 51.84 47.61 50.41 46.24 47.61 10.290 50.41 47.61 47.61 57.76 56.25 51.84 10.410 46.24 37.21 47.61 42.25 50.41 50.41 10.530 59.29 50.41 53.29 47.61 47.61 47.61 10.650 53.29 42.25 50.41 59.29 44.89 49.00 10.770 62.41 38.44 50.41 47.61 49.00 47.61 10.890 50.41 29.16 39.69 64.00 37.21 43.56 11.010 38.44 30.25 50.41 44.89 43.56 56.25 11.130 46.24 43.56 43.56 39.69 36.00 49.00 11.250 53.29 51.84 59.29 40.96 47.61 44.89 11.370 38.44 56.25 44.89 38.44 56.25 49.00 11.490 38.44 42.25 59.29 54.76 47.61 60.84

186

File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 47.61 47.61 36.00 32.49 34.81 44.89 11.730 54.76 51.84 50.41 50.41 39.69 38.44 11.850 38.44 50.41 49.00 39.69 54.76 53.29 11.970 49.00 51.84 50.41 38.44 30.25 47.61 12.090 49.00 51.84 32.49 46.24 39.69 38.44 12.210 46.24 36.00 47.61 54.76 49.00 53.29 12.330 43.56 43.56 43.56 46.24 54.76 34.81 12.450 47.61 43.56 46.24 46.24 43.56 53.29 12.570 38.44 59.29 32.49 54.76 39.69 53.29 12.690 49.00 39.69 49.00 42.25 47.61 49.00 12.810 47.61 38.44 32.49 40.96 49.00 43.56 12.930 42.25 50.41 43.56 47.61 44.89 33.64 13.050 37.21 47.61 53.29 56.25 42.25 56.25 13.170 43.56 47.61 51.84 51.84 44.89 43.56 13.290 49.00 51.84 32.49 42.25 47.61 42.25 13.410 47.61 39.69 38.44 44.89 49.00 50.41 13.530 56.25 39.69 53.29 38.44 38.44 37.21 13.650 39.69 38.44 31.36 49.00 37.21 46.24 13.770 37.21 42.25 37.21 39.69 38.44 43.56 13.890 36.00 31.36 44.89 32.49 51.84 34.81 14.010 30.25 42.25 40.96 43.56 38.44 38.44 14.130 49.00 43.56 49.00 43.56 37.21 43.56 14.250 42.25 32.49 38.44 36.00 40.96 44.89 14.370 47.61 39.69 42.25 38.44 38.44 50.41 14.490 53.29 32.49 42.25 39.69 38.44 53.29 14.610 36.00 38.44 38.44 43.56 43.56 43.56 14.730 38.44 39.69 37.21 51.84 50.41 33.64 14.850 43.56 40.96 39.69 36.00 47.61 33.64 14.970 32.49 49.00 42.25 54.76 43.56 34.81 15.090 47.61 57.76 50.41 39.69 47.61 37.21 15.210 59.29 47.61 51.84 44.89 57.76 47.61 15.330 51.84 46.24 47.61 56.25 56.25 53.29 15.450 60.84 49.00 53.29 53.29 40.96 50.41 15.570 64.00 54.76 57.76 42.25 38.44 51.84 15.690 60.84 43.56 53.29 64.00 65.61 70.56 15.810 59.29 47.61 43.56 59.29 59.29 56.25 15.930 56.25 53.29 56.25 50.41 44.89 50.41 16.050 46.24 32.49 51.84 43.56 67.24 62.41 16.170 50.41 39.69 43.56 43.56 56.25 56.25 16.290 46.24 59.29 49.00 53.29 47.61 54.76 16.410 43.56 53.29 40.96 54.76 49.00 44.89 16.530 47.61 64.00 65.61 40.96 38.44 59.29 16.650 47.61 65.61 56.25 42.25 43.56 50.41 16.770 50.41 42.25 38.44 39.69 47.61 43.56 16.890 47.61 53.29 47.61 39.69 38.44 39.69 17.010 43.56 43.56 38.44 42.25 47.61 32.49 17.130 43.56 37.21 36.00 43.56 49.00 40.96 17.250 34.81 36.00 46.24 40.96 38.44 42.25 17.370 47.61 46.24 47.61 47.61 29.16 36.00 17.490 36.00 40.96 30.25 32.49 40.96 43.56 17.610 38.44 29.16 44.89 50.41 38.44 43.56 17.730 43.56 33.64 44.89 32.49 42.25 32.49

187

File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 46.24 46.24 44.89 32.49 42.25 43.56 17.970 28.09 32.49 28.09 46.24 39.69 39.69 18.090 43.56 50.41 38.44 24.01 47.61 47.61 18.210 44.89 47.61 39.69 38.44 39.69 39.69 18.330 51.84 38.44 43.56 36.00 34.81 33.64 18.450 34.81 43.56 42.25 53.29 39.69 38.44 18.570 42.25 51.84 32.49 42.25 47.61 47.61 18.690 36.00 42.25 38.44 40.96 46.24 47.61 18.810 37.21 44.89 37.21 53.29 42.25 34.81 18.930 56.25 38.44 40.96 47.61 62.41 50.41 19.050 39.69 54.76 39.69 43.56 39.69 50.41 19.170 51.84 50.41 44.89 51.84 44.89 47.61 19.290 42.25 40.96 53.29 34.81 36.00 53.29 19.410 37.21 40.96 40.96 43.56 42.25 47.61 19.530 49.00 43.56 49.00 54.76 40.96 39.69 19.650 29.16 47.61 34.81 38.44 50.41 46.24 19.770 47.61 43.56 39.69 53.29 34.81 34.81 19.890 50.41 47.61 57.76 34.81 50.41 43.56 20.010 39.69 43.56 30.25 38.44 34.81 40.96 20.130 38.44 49.00 38.44 51.84 37.21 38.44 20.250 56.25 38.44 38.44 43.56 44.89 56.25 20.370 43.56 44.89 47.61 47.61 46.24 47.61 20.490 43.56 62.41 36.00 59.29 39.69 47.61 20.610 42.25 46.24 56.25 50.41 56.25 44.89 20.730 51.84 59.29 70.56 62.41 56.25 65.61 20.850 51.84 59.29 56.25 40.96 43.56 50.41 20.970 49.00 34.81 53.29 42.25 39.69 46.24 21.090 43.56 42.25 36.00 47.61 46.24 38.44 21.210 59.29 51.84 42.25 44.89 33.64 40.96 21.330 39.69 43.56 36.00 38.44 47.61 49.00 21.450 43.56 46.24 43.56 34.81 46.24 33.64 21.570 38.44 46.24 39.69 44.89 39.69 33.64 21.690 59.29 44.89 40.96 56.25 42.25 51.84 21.810 47.61 53.29 65.61 68.89 84.64 94.09 21.930 67.24 112.36 96.04 106.09 136.89 104.04 22.050 90.25 110.25 67.24 64.00 79.21 47.61 22.170 56.25 49.00 37.21 46.24 50.41 22.09 22.290 42.25 42.25 32.49 47.61 43.56 49.00 22.410 38.44 50.41 38.44 43.56 43.56 36.00 22.530 37.21 49.00 40.96 34.81 38.44 38.44 22.650 39.69 50.41 33.64 43.56 42.25 39.69 22.770 51.84 26.01 34.81 37.21 43.56 46.24 22.890 47.61 49.00 37.21 50.41 46.24 34.81 23.010 47.61 53.29 42.25 43.56 43.56 29.16 23.130 42.25 39.69 39.69 44.89 40.96 43.56 23.250 39.69 28.09 40.96 34.81 38.44 32.49 23.370 42.25 44.89 44.89 47.61 38.44 50.41 23.490 34.81 38.44 53.29 43.56 50.41 49.00 23.610 44.89 47.61 42.25 60.84 53.29 59.29 23.730 56.25 72.25 68.89 79.21 88.36 98.01 23.850 88.36 112.36 129.96 144.00 184.96 179.56 23.970 210.25 219.04 219.04 237.16 182.25 184.96

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File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 182.25 141.61 161.29 125.44 100.00 77.44 24.210 82.81 77.44 70.56 75.69 49.00 57.76 24.330 36.00 50.41 49.00 51.84 56.25 51.84 24.450 42.25 37.21 40.96 38.44 46.24 34.81 24.570 38.44 46.24 49.00 44.89 38.44 40.96 24.690 47.61 36.00 42.25 39.69 32.49 42.25 24.810 39.69 38.44 36.00 32.49 37.21 51.84 24.930 42.25 44.89 36.00 44.89 39.69 30.25 25.050 39.69 39.69 34.81 39.69 38.44 33.64 25.170 49.00 53.29 39.69 38.44 42.25 38.44 25.290 38.44 39.69 46.24 46.24 38.44 38.44 25.410 40.96 34.81 53.29 34.81 38.44 44.89 25.530 42.25 40.96 40.96 38.44 30.25 44.89 25.650 43.56 31.36 47.61 39.69 37.21 33.64 25.770 36.00 40.96 43.56 36.00 37.21 50.41 25.890 28.09 34.81 36.00 43.56 43.56 43.56 26.010 37.21 40.96 30.25 54.76 39.69 43.56 26.130 47.61 44.89 34.81 38.44 49.00 38.44 26.250 46.24 33.64 39.69 50.41 37.21 40.96 26.370 44.89 51.84 50.41 59.29 60.84 64.00 26.490 70.56 79.21 96.04 104.04 129.96 151.29 26.610 129.96 127.69 129.96 102.01 77.44 60.84 26.730 65.61 32.49 44.89 43.56 38.44 37.21 26.850 42.25 44.89 40.96 43.56 26.01 38.44 26.970 33.64 40.96 38.44 53.29 43.56 32.49 27.090 44.89 43.56 38.44 30.25 34.81 34.81 27.210 44.89 36.00 44.89 20.25 29.16 47.61 27.330 31.36 38.44 33.64 36.00 40.96 47.61 27.450 34.81 27.04 32.49 40.96 38.44 31.36 27.570 44.89 43.56 31.36 33.64 38.44 38.44 27.690 47.61 34.81 31.36 37.21 47.61 31.36 27.810 37.21 32.49 34.81 34.81 44.89 43.56 27.930 37.21 36.00 43.56 33.64 38.44 39.69 28.050 36.00 39.69 32.49 43.56 30.25 26.01 28.170 36.00 43.56 30.25 43.56 44.89 30.25 28.290 39.69 38.44 34.81 36.00 50.41 39.69 28.410 34.81 42.25 38.44 31.36 46.24 39.69 28.530 40.96 43.56 42.25 53.29 44.89 34.81 28.650 40.96 42.25 47.61 42.25 43.56 30.25 28.770 43.56 38.44 42.25 36.00 43.56 42.25 28.890 43.56 44.89 37.21 40.96 42.25 38.44 29.010 47.61 38.44 43.56 46.24 43.56 38.44 29.130 60.84 47.61 54.76 51.84 46.24 60.84 29.250 47.61 56.25 56.25 40.96 50.41 59.29 29.370 62.41 56.25 59.29 70.56 59.29 56.25 29.490 62.41 51.84 51.84 59.29 50.41 50.41 29.610 56.25 54.76 50.41 51.84 51.84 47.61 29.730 59.29 65.61 62.41 62.41 47.61 72.25 29.850 51.84 60.84 64.00 77.44 81.00 65.61 29.970 70.56 84.64 84.64 79.21 88.36 81.00 30.090 88.36 94.09 118.81 110.25 96.04 116.64 30.210 121.00 123.21 144.00 129.96 144.00 174.24

189

File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 176.89 190.44 204.49 240.25 243.36 285.61 30.450 302.76 313.29 349.69 380.25 445.21 470.89 30.570 506.25 571.21 620.01 795.24 846.81 1024.00 30.690 1169.64 1474.56 1664.64 2079.36 2530.09 3003.04 30.810 3492.81 4173.16 5083.69 5760.81 6384.01 6609.69 30.930 6416.01 6099.61 5580.09 4747.21 4070.44 3294.76 31.050 2724.84 2199.61 1780.84 1436.41 1253.16 942.49 31.170 846.81 712.89 620.01 538.24 457.96 428.49 31.290 388.09 353.44 324.00 292.41 237.16 210.25 31.410 198.81 207.36 174.24 169.00 163.84 158.76 31.530 141.61 144.00 141.61 129.96 112.36 110.25 31.650 108.16 116.64 90.25 100.00 84.64 100.00 31.770 102.01 73.96 96.04 77.44 90.25 82.81 31.890 65.61 82.81 77.44 79.21 67.24 65.61 32.010 64.00 67.24 68.89 59.29 70.56 53.29 32.130 62.41 67.24 62.41 56.25 54.76 53.29 32.250 57.76 50.41 53.29 53.29 50.41 59.29 32.370 56.25 53.29 62.41 67.24 47.61 56.25 32.490 62.41 53.29 44.89 53.29 43.56 53.29 32.610 51.84 50.41 46.24 39.69 53.29 56.25 32.730 62.41 46.24 56.25 60.84 44.89 53.29 32.850 39.69 59.29 57.76 54.76 49.00 46.24 32.970 44.89 59.29 65.61 59.29 56.25 67.24 33.090 60.84 77.44 77.44 67.24 75.69 72.25 33.210 84.64 82.81 108.16 110.25 118.81 116.64 33.330 132.25 171.61 196.00 198.81 204.49 243.36 33.450 292.41 256.00 320.41 324.00 299.29 316.84 33.570 256.00 222.01 207.36 196.00 158.76 141.61 33.690 108.16 100.00 88.36 88.36 65.61 77.44 33.810 70.56 49.00 51.84 64.00 65.61 50.41 33.930 50.41 53.29 56.25 62.41 59.29 39.69 34.050 59.29 37.21 50.41 38.44 33.64 47.61 34.170 34.81 51.84 47.61 46.24 37.21 39.69 34.290 44.89 47.61 42.25 43.56 44.89 44.89 34.410 47.61 32.49 46.24 40.96 43.56 47.61 34.530 38.44 42.25 39.69 50.41 56.25 43.56 34.650 42.25 44.89 59.29 54.76 51.84 44.89 34.770 46.24 54.76 50.41 72.25 54.76 46.24 34.890 51.84 64.00 72.25 65.61 81.00 94.09 35.010 84.64 84.64 106.09 94.09 110.25 136.89 35.130 156.25 166.41 204.49 198.81 231.04 228.01 35.250 265.69 225.00 259.21 259.21 237.16 216.09 35.370 234.09 234.09 198.81 176.89 158.76 106.09 35.490 104.04 108.16 94.09 70.56 75.69 72.25 35.610 72.25 65.61 54.76 67.24 64.00 57.76 35.730 59.29 42.25 62.41 47.61 39.69 54.76 35.850 43.56 53.29 59.29 42.25 40.96 44.89 35.970 47.61 50.41 39.69 49.00 36.00 56.25 36.090 60.84 47.61 37.21 37.21 50.41 50.41 36.210 47.61 38.44 44.89 33.64 39.69 32.49 36.330 47.61 59.29 42.25 64.00 50.41 59.29 36.450 49.00 65.61 59.29 65.61 75.69 73.96

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File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 62.41 82.81 65.61 65.61 82.81 75.69 36.690 70.56 75.69 77.44 72.25 92.16 98.01 36.810 92.16 88.36 121.00 102.01 116.64 127.69 36.930 110.25 129.96 127.69 158.76 141.61 141.61 37.050 153.76 144.00 182.25 207.36 204.49 243.36 37.170 259.21 285.61 327.61 380.25 400.00 445.21 37.290 492.84 515.29 519.84 497.29 488.41 492.84 37.410 441.00 396.01 338.56 313.29 243.36 219.04 37.530 174.24 166.41 146.41 127.69 127.69 123.21 37.650 116.64 92.16 108.16 92.16 88.36 67.24 37.770 82.81 79.21 68.89 82.81 70.56 88.36 37.890 56.25 56.25 57.76 62.41 62.41 59.29 38.010 50.41 46.24 54.76 53.29 50.41 43.56 38.130 53.29 50.41 51.84 49.00 50.41 38.44 38.250 38.44 53.29 34.81 53.29 36.00 42.25 38.370 50.41 50.41 50.41 53.29 49.00 47.61 38.490 57.76 50.41 38.44 50.41 43.56 57.76 38.610 53.29 46.24 44.89 53.29 51.84 46.24 38.730 56.25 43.56 47.61 43.56 50.41 43.56 38.850 50.41 43.56 40.96 42.25 53.29 56.25 38.970 49.00 50.41 40.96 67.24 46.24 57.76 39.090 51.84 62.41 57.76 56.25 65.61 67.24 39.210 59.29 65.61 56.25 46.24 67.24 82.81 39.330 65.61 77.44 90.25 88.36 75.69 81.00 39.450 73.96 102.01 92.16 88.36 100.00 86.49 39.570 86.49 100.00 96.04 123.21 110.25 108.16 39.690 112.36 134.56 121.00 132.25 129.96 141.61 39.810 121.00 146.41 132.25 129.96 129.96 139.24 39.930 144.00 129.96 118.81 136.89 108.16 118.81 40.050 102.01 92.16 96.04 82.81 86.49 84.64 40.170 62.41 62.41 75.69 60.84 64.00 79.21 40.290 62.41 59.29 56.25 79.21 75.69 90.25 40.410 67.24 57.76 70.56 79.21 100.00 123.21 40.530 98.01 73.96 96.04 134.56 129.96 110.25 40.650 125.44 148.84 156.25 179.56 213.16 210.25 40.770 210.25 272.25 316.84 338.56 342.25 404.01 40.890 497.29 529.00 552.25 756.25 882.09 912.04 41.010 1122.25 1190.25 1324.96 1361.61 1521.00 1413.76 41.130 1376.41 1281.64 1281.64 1204.09 1049.76 876.16 41.250 789.61 739.84 595.36 533.61 420.25 372.49 41.370 302.76 324.00 268.96 201.64 216.09 187.69 41.490 182.25 166.41 144.00 141.61 123.21 121.00 41.610 125.44 110.25 98.01 86.49 94.09 90.25 41.730 92.16 90.25 90.25 86.49 62.41 72.25 41.850 62.41 50.41 51.84 64.00 60.84 56.25 41.970 53.29 79.21 57.76 77.44 49.00 62.41 42.090 46.24 49.00 46.24 59.29 53.29 50.41 42.210 56.25 51.84 36.00 50.41 62.41 67.24 42.330 59.29 53.29 70.56 54.76 53.29 70.56 42.450 70.56 57.76 53.29 50.41 59.29 40.96 42.570 50.41 46.24 42.25 46.24 49.00 59.29 42.690 37.21 43.56 46.24 56.25 53.29 51.84

191

File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 62.41 62.41 54.76 53.29 59.29 50.41 42.930 49.00 51.84 53.29 37.21 50.41 54.76 43.050 43.56 62.41 53.29 60.84 50.41 60.84 43.170 60.84 44.89 67.24 60.84 62.41 56.25 43.290 67.24 56.25 56.25 62.41 72.25 72.25 43.410 75.69 62.41 62.41 75.69 92.16 86.49 43.530 100.00 106.09 110.25 110.25 114.49 153.76 43.650 151.29 201.64 187.69 231.04 201.64 240.25 43.770 240.25 225.00 246.49 187.69 231.04 184.96 43.890 184.96 146.41 148.84 123.21 121.00 108.16 44.010 96.04 104.04 100.00 94.09 70.56 86.49 44.130 90.25 77.44 92.16 86.49 92.16 75.69 44.250 86.49 94.09 77.44 90.25 70.56 88.36 44.370 82.81 92.16 88.36 77.44 88.36 108.16 44.490 123.21 96.04 139.24 136.89 146.41 148.84 44.610 169.00 193.21 246.49 243.36 320.41 316.84 44.730 384.16 519.84 533.61 576.00 665.64 686.44 44.850 852.64 906.01 954.81 906.01 924.16 829.44 44.970 686.44 702.25 630.01 561.69 506.25 475.24 45.090 376.36 342.25 299.29 268.96 228.01 216.09 45.210 182.25 158.76 141.61 136.89 132.25 116.64 45.330 125.44 112.36 90.25 81.00 106.09 88.36 45.450 70.56 72.25 81.00 72.25 57.76 79.21 45.570 65.61 77.44 62.41 72.25 40.96 65.61 45.690 70.56 72.25 54.76 53.29 53.29 53.29 45.810 57.76 60.84 51.84 60.84 64.00 50.41 45.930 59.29 49.00 49.00 47.61 56.25 51.84 46.050 43.56 54.76 64.00 43.56 43.56 53.29 46.170 44.89 46.24 43.56 59.29 59.29 43.56 46.290 62.41 62.41 53.29 60.84 56.25 68.89 46.410 47.61 56.25 62.41 65.61 65.61 65.61 46.530 56.25 62.41 59.29 62.41 75.69 67.24 46.650 65.61 73.96 62.41 59.29 67.24 70.56 46.770 47.61 62.41 64.00 53.29 60.84 56.25 46.890 46.24 51.84 53.29 38.44 57.76 47.61 47.010 51.84 39.69 47.61 36.00 34.81 59.29 47.130 53.29 53.29 39.69 47.61 50.41 46.24 47.250 44.89 50.41 44.89 62.41 38.44 59.29 47.370 54.76 50.41 44.89 56.25 43.56 38.44 47.490 50.41 53.29 62.41 47.61 57.76 38.44 47.610 43.56 46.24 38.44 57.76 43.56 49.00 47.730 43.56 39.69 43.56 51.84 40.96 43.56 47.850 40.96 38.44 49.00 47.61 46.24 62.41 47.970 59.29 43.56 53.29 49.00 49.00 56.25 48.090 43.56 38.44 54.76 50.41 39.69 43.56 48.210 40.96 68.89 46.24 59.29 43.56 59.29 48.330 47.61 56.25 54.76 59.29 56.25 59.29 48.450 70.56 59.29 68.89 50.41 51.84 64.00 48.570 67.24 67.24 73.96 54.76 53.29 75.69 48.690 67.24 67.24 90.25 67.24 81.00 75.69 48.810 79.21 92.16 81.00 92.16 94.09 116.64 48.930 102.01 112.36 139.24 123.21 129.96 141.61

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File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 182.25 190.44 184.96 198.81 193.21 234.09 49.170 219.04 246.49 249.64 210.25 240.25 243.36 49.290 240.25 262.44 243.36 201.64 196.00 204.49 49.410 179.56 174.24 174.24 148.84 132.25 156.25 49.530 136.89 129.96 134.56 121.00 129.96 127.69 49.650 125.44 116.64 125.44 125.44 125.44 123.21 49.770 129.96 123.21 110.25 125.44 132.25 136.89 49.890 141.61 136.89 166.41 182.25 176.89 187.69 50.010 196.00 213.16 193.21 228.01 275.56 285.61 50.130 285.61 289.00 324.00 357.21 364.81 388.09 50.250 449.44 479.61 506.25 580.81 610.09 670.81 50.370 718.24 882.09 864.36 961.00 1017.61 1030.41 50.490 1004.89 1049.76 1049.76 1043.29 948.64 942.49 50.610 846.81 930.25 784.00 767.29 778.41 712.89 50.730 660.49 702.25 686.44 665.64 691.69 772.84 50.850 772.84 784.00 906.01 924.16 1036.84 1089.00 50.970 1135.69 1108.89 1169.64 1183.36 1108.89 1190.25 51.090 1102.24 1024.00 992.25 918.09 918.09 846.81 51.210 739.84 691.69 600.25 600.25 515.29 466.56 51.330 436.81 400.00 368.64 338.56 302.76 285.61 51.450 292.41 213.16 222.01 193.21 179.56 158.76 51.570 146.41 169.00 151.29 134.56 123.21 114.49 51.690 125.44 94.09 121.00 98.01 92.16 94.09 51.810 106.09 98.01 84.64 96.04 114.49 92.16 51.930 70.56 64.00 72.25 75.69 77.44 72.25 52.050 51.84 72.25 64.00 68.89 70.56 82.81 52.170 75.69 77.44 68.89 79.21 67.24 81.00 52.290 59.29 75.69 73.96 67.24 72.25 56.25 52.410 79.21 72.25 57.76 51.84 59.29 57.76 52.530 62.41 54.76 62.41 60.84 53.29 43.56 52.650 43.56 49.00 50.41 47.61 47.61 50.41 52.770 57.76 50.41 46.24 43.56 57.76 42.25 52.890 56.25 50.41 56.25 47.61 44.89 36.00 53.010 44.89 50.41 60.84 50.41 40.96 38.44 53.130 56.25 50.41 47.61 39.69 43.56 53.29 53.250 53.29 40.96 46.24 53.29 43.56 40.96 53.370 47.61 42.25 38.44 39.69 44.89 43.56 53.490 43.56 38.44 32.49 49.00 50.41 32.49 53.610 34.81 31.36 42.25 40.96 40.96 47.61 53.730 43.56 40.96 43.56 47.61 43.56 47.61 53.850 42.25 46.24 46.24 31.36 42.25 34.81 53.970 39.69 32.49 38.44 32.49 44.89 32.49 54.090 42.25 50.41 40.96 47.61 42.25 33.64 54.210 42.25 59.29 44.89 43.56 46.24 32.49 54.330 43.56 38.44 39.69 33.64 43.56 43.56 54.450 32.49 40.96 36.00 26.01 49.00 34.81 54.570 42.25 38.44 44.89 44.89 38.44 43.56 54.690 51.84 23.04 30.25 56.25 39.69 50.41 54.810 36.00 64.00 49.00 43.56 47.61 47.61 54.930 43.56 46.24 51.84 32.49 44.89 34.81 55.050 40.96 53.29 31.36 38.44 46.24 28.09 55.170 34.81 34.81 39.69 47.61 38.44 50.41

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File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 32.49 53.29 43.56 31.36 42.25 43.56 55.410 44.89 38.44 38.44 38.44 33.64 39.69 55.530 38.44 43.56 39.69 29.16 37.21 42.25 55.650 33.64 46.24 47.61 34.81 33.64 38.44 55.770 43.56 37.21 42.25 39.69 53.29 46.24 55.890 37.21 47.61 32.49 34.81 39.69 34.81 56.010 38.44 32.49 34.81 43.56 46.24 36.00 56.130 30.25 40.96 27.04 36.00 38.44 42.25 56.250 28.09 49.00 31.36 27.04 32.49 46.24 56.370 32.49 43.56 47.61 36.00 37.21 36.00 56.490 38.44 34.81 29.16 34.81 37.21 34.81 56.610 36.00 43.56 29.16 30.25 33.64 32.49 56.730 32.49 32.49 43.56 43.56 31.36 43.56 56.850 54.76 38.44 32.49 39.69 36.00 38.44 56.970 38.44 37.21 38.44 37.21 33.64 36.00 57.090 42.25 31.36 47.61 36.00 44.89 49.00 57.210 38.44 38.44 43.56 42.25 40.96 43.56 57.330 40.96 44.89 31.36 50.41 43.56 43.56 57.450 39.69 42.25 44.89 40.96 39.69 49.00 57.570 40.96 38.44 34.81 38.44 40.96 40.96 57.690 38.44 39.69 42.25 39.69 38.44 37.21 57.810 38.44 38.44 34.81 42.25 43.56 46.24 57.930 38.44 50.41 33.64 43.56 38.44 31.36 58.050 49.00 38.44 54.76 40.96 54.76 39.69 58.170 47.61 50.41 64.00 56.25 40.96 47.61 58.290 67.24 59.29 51.84 56.25 64.00 75.69 58.410 53.29 59.29 65.61 70.56 92.16 70.56 58.530 100.00 104.04 100.00 114.49 123.21 129.96 58.650 174.24 151.29 176.89 151.29 190.44 198.81 58.770 225.00 216.09 272.25 292.41 249.64 249.64 58.890 282.24 252.81 231.04 234.09 210.25 231.04 59.010 225.00 163.84 179.56 158.76 187.69 136.89 59.130 136.89 125.44 136.89 112.36 121.00 118.81 59.250 129.96 144.00 118.81 116.64 121.00 132.25 59.370 129.96 146.41 134.56 153.76 166.41 184.96 59.490 169.00 187.69 207.36 228.01 243.36 309.76 59.610 265.69 357.21 334.89 384.16 408.04 449.44 59.730 449.44 412.09 453.69 416.16 436.81 436.81 59.850 412.09 396.01 368.64 338.56 331.24 316.84 59.970 275.56 237.16 246.49 231.04 184.96 198.81 60.090 179.56 179.56 169.00 129.96 148.84 141.61 60.210 112.36 110.25 90.25 90.25 81.00 72.25 60.330 75.69 94.09 62.41 77.44 72.25 65.61 60.450 65.61 60.84 67.24 72.25 75.69 62.41 60.570 62.41 49.00 56.25 62.41 50.41 53.29 60.690 62.41 65.61 53.29 53.29 53.29 56.25 60.810 47.61 49.00 64.00 50.41 40.96 50.41 60.930 53.29 51.84 49.00 39.69 53.29 59.29 61.050 49.00 56.25 46.24 43.56 46.24 43.56 61.170 56.25 38.44 50.41 46.24 47.61 40.96 61.290 56.25 28.09 40.96 56.25 50.41 51.84 61.410 43.56 56.25 43.56 29.16 47.61 43.56

194

File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 53.29 39.69 53.29 47.61 54.76 56.25 61.650 51.84 64.00 65.61 67.24 65.61 79.21 61.770 62.41 84.64 77.44 60.84 82.81 94.09 61.890 72.25 72.25 82.81 98.01 96.04 79.21 62.010 82.81 100.00 90.25 81.00 82.81 75.69 62.130 82.81 67.24 53.29 77.44 62.41 62.41 62.250 72.25 54.76 56.25 64.00 67.24 50.41 62.370 49.00 57.76 46.24 75.69 57.76 72.25 62.490 53.29 50.41 57.76 62.41 62.41 65.61 62.610 54.76 65.61 77.44 62.41 65.61 56.25 62.730 73.96 64.00 70.56 62.41 79.21 67.24 62.850 73.96 96.04 92.16 86.49 84.64 94.09 62.970 92.16 114.49 112.36 108.16 127.69 121.00 63.090 146.41 158.76 141.61 166.41 176.89 207.36 63.210 201.64 259.21 259.21 246.49 302.76 327.61 63.330 324.00 380.25 380.25 388.09 353.44 334.89 63.450 353.44 327.61 289.00 292.41 295.84 292.41 63.570 268.96 259.21 243.36 231.04 182.25 196.00 63.690 176.89 158.76 158.76 141.61 114.49 127.69 63.810 114.49 114.49 121.00 112.36 112.36 100.00 63.930 104.04 106.09 88.36 102.01 110.25 100.00 64.050 108.16 100.00 104.04 100.00 118.81 106.09 64.170 114.49 114.49 121.00 141.61 144.00 163.84 64.290 161.29 176.89 163.84 207.36 216.09 190.44 64.410 216.09 219.04 219.04 204.49 240.25 237.16 64.530 231.04 204.49 193.21 176.89 182.25 196.00 64.650 176.89 184.96 174.24 166.41 166.41 151.29 64.770 148.84 161.29 141.61 169.00 158.76 163.84 64.890 166.41 158.76 182.25 176.89 193.21 184.96 65.010 193.21 196.00 222.01 231.04 234.09 228.01 65.130 234.09 207.36 219.04 216.09 161.29 213.16 65.250 193.21 166.41 169.00 163.84 182.25 141.61 65.370 141.61 134.56 176.89 134.56 116.64 116.64 65.490 123.21 116.64 121.00 92.16 110.25 104.04 65.610 96.04 98.01 94.09 118.81 98.01 92.16 65.730 129.96 114.49 110.25 116.64 127.69 151.29 65.850 114.49 153.76 144.00 153.76 151.29 148.84 65.970 190.44 161.29 176.89 163.84 158.76 151.29 66.090 148.84 163.84 148.84 153.76 163.84 139.24 66.210 151.29 127.69 123.21 144.00 123.21 100.00 66.330 106.09 106.09 84.64 96.04 100.00 88.36 66.450 90.25 96.04 90.25 79.21 77.44 84.64 66.570 70.56 62.41 77.44 79.21 84.64 75.69 66.690 77.44 82.81 86.49 94.09 81.00 94.09 66.810 82.81 92.16 77.44 96.04 96.04 132.25 66.930 110.25 125.44 151.29 121.00 144.00 151.29 67.050 144.00 184.96 184.96 204.49 219.04 234.09 67.170 268.96 292.41 302.76 384.16 357.21 376.36 67.290 462.25 388.09 441.00 449.44 400.00 384.16 67.410 372.49 412.09 361.00 353.44 338.56 331.24 67.530 334.89 309.76 302.76 249.64 228.01 204.49 67.650 184.96 184.96 169.00 156.25 146.41 136.89

195

File: JC9.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 125.44 132.25 125.44 106.09 102.01 86.49 67.890 108.16 86.49 100.00 98.01 79.21 98.01 68.010 90.25 79.21 72.25 100.00 94.09 84.64 68.130 79.21 90.25 75.69 92.16 88.36 75.69 68.250 86.49 79.21 67.24 62.41 59.29 68.89 68.370 49.00 56.25 56.25 53.29 68.89 54.76 68.490 56.25 43.56 64.00 56.25 56.25 50.41 68.610 46.24 50.41 47.61 53.29 57.76 46.24 68.730 56.25 32.49 47.61 47.61 40.96 49.00 68.850 49.00 56.25 49.00 53.29 44.89 38.44 68.970 50.41 60.84 39.69 59.29 50.41 49.00 69.090 60.84 49.00 32.49 38.44 49.00 50.41 69.210 57.76 51.84 44.89 47.61 51.84 40.96 69.330 43.56 53.29 49.00 50.41 34.81 40.96 69.450 67.24 49.00 51.84 56.25 49.00 50.41 69.570 53.29 57.76 50.41 70.56 62.41 56.25 69.690 50.41 64.00 56.25 65.61 67.24 75.69 69.810 82.81 70.56 73.96 72.25 82.81 56.25 69.930 72.25 88.36 86.49 94.09 _

196

File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC10 Data measured at: 25-Jan-2011 11:00:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 7396.000 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 100.00 127.69 116.64 98.01 86.49 90.25 2.130 90.25 79.21 88.36 77.44 60.84 67.24 2.250 67.24 79.21 86.49 82.81 65.61 77.44 2.370 56.25 79.21 82.81 70.56 75.69 75.69 2.490 65.61 75.69 67.24 65.61 57.76 77.44 2.610 75.69 50.41 60.84 62.41 56.25 79.21 2.730 70.56 67.24 65.61 56.25 72.25 65.61 2.850 59.29 50.41 50.41 70.56 50.41 67.24 2.970 59.29 70.56 56.25 50.41 49.00 67.24 3.090 49.00 64.00 65.61 54.76 51.84 56.25 3.210 62.41 56.25 54.76 65.61 51.84 67.24 3.330 62.41 72.25 67.24 67.24 50.41 47.61 3.450 59.29 53.29 62.41 57.76 57.76 62.41 3.570 64.00 50.41 53.29 56.25 62.41 49.00 3.690 50.41 50.41 57.76 46.24 50.41 56.25 3.810 49.00 59.29 53.29 62.41 72.25 56.25 3.930 42.25 64.00 50.41 53.29 56.25 59.29 4.050 70.56 60.84 57.76 51.84 46.24 72.25 4.170 53.29 62.41 50.41 54.76 51.84 49.00 4.290 47.61 62.41 65.61 56.25 51.84 65.61 4.410 54.76 54.76 56.25 56.25 57.76 50.41 4.530 50.41 51.84 65.61 53.29 64.00 42.25 4.650 51.84 64.00 64.00 54.76 67.24 51.84 4.770 75.69 50.41 53.29 70.56 56.25 59.29 4.890 64.00 68.89 47.61 56.25 53.29 56.25 5.010 53.29 65.61 65.61 54.76 50.41 73.96 5.130 70.56 65.61 54.76 65.61 51.84 49.00 5.250 65.61 57.76 51.84 70.56 64.00 56.25

197

File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 38.44 59.29 56.25 59.29 60.84 60.84 5.490 56.25 44.89 59.29 62.41 51.84 42.25 5.610 50.41 54.76 51.84 46.24 60.84 59.29 5.730 49.00 53.29 56.25 50.41 49.00 47.61 5.850 47.61 56.25 59.29 70.56 65.61 56.25 5.970 53.29 56.25 53.29 51.84 57.76 43.56 6.090 53.29 59.29 47.61 53.29 50.41 56.25 6.210 56.25 54.76 47.61 46.24 46.24 53.29 6.330 53.29 64.00 43.56 51.84 57.76 79.21 6.450 56.25 65.61 34.81 53.29 56.25 54.76 6.570 53.29 47.61 65.61 43.56 62.41 50.41 6.690 50.41 56.25 42.25 60.84 47.61 54.76 6.810 65.61 56.25 42.25 38.44 47.61 34.81 6.930 56.25 53.29 68.89 50.41 65.61 49.00 7.050 44.89 39.69 50.41 53.29 54.76 50.41 7.170 43.56 59.29 50.41 47.61 47.61 44.89 7.290 53.29 59.29 56.25 62.41 59.29 47.61 7.410 53.29 50.41 42.25 54.76 46.24 53.29 7.530 50.41 49.00 59.29 50.41 60.84 49.00 7.650 59.29 57.76 50.41 50.41 40.96 56.25 7.770 50.41 56.25 49.00 51.84 51.84 49.00 7.890 51.84 56.25 47.61 47.61 59.29 50.41 8.010 56.25 50.41 51.84 50.41 57.76 36.00 8.130 53.29 49.00 59.29 53.29 57.76 39.69 8.250 64.00 59.29 33.64 38.44 46.24 44.89 8.370 56.25 44.89 47.61 42.25 65.61 43.56 8.490 49.00 49.00 53.29 38.44 50.41 49.00 8.610 42.25 38.44 47.61 50.41 43.56 64.00 8.730 47.61 49.00 49.00 47.61 54.76 40.96 8.850 36.00 47.61 47.61 40.96 67.24 53.29 8.970 50.41 54.76 34.81 38.44 60.84 46.24 9.090 46.24 44.89 32.49 53.29 50.41 43.56 9.210 56.25 36.00 49.00 47.61 47.61 43.56 9.330 67.24 50.41 43.56 49.00 31.36 46.24 9.450 38.44 53.29 54.76 50.41 38.44 50.41 9.570 47.61 37.21 50.41 49.00 47.61 47.61 9.690 51.84 43.56 50.41 54.76 42.25 47.61 9.810 49.00 51.84 49.00 57.76 39.69 51.84 9.930 54.76 38.44 49.00 38.44 39.69 46.24 10.050 50.41 49.00 42.25 38.44 39.69 50.41 10.170 53.29 40.96 62.41 47.61 40.96 53.29 10.290 46.24 42.25 42.25 42.25 33.64 56.25 10.410 50.41 49.00 34.81 47.61 40.96 50.41 10.530 38.44 47.61 43.56 51.84 38.44 37.21 10.650 54.76 53.29 44.89 44.89 43.56 40.96 10.770 59.29 36.00 46.24 38.44 50.41 38.44 10.890 56.25 53.29 42.25 50.41 53.29 51.84 11.010 40.96 50.41 38.44 59.29 51.84 68.89 11.130 38.44 37.21 44.89 43.56 34.81 49.00 11.250 32.49 38.44 47.61 43.56 50.41 53.29 11.370 47.61 44.89 53.29 47.61 47.61 43.56 11.490 46.24 47.61 47.61 57.76 43.56 53.29

198

File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 51.84 44.89 51.84 36.00 37.21 53.29 11.730 51.84 43.56 47.61 50.41 34.81 43.56 11.850 50.41 44.89 49.00 44.89 42.25 39.69 11.970 37.21 50.41 53.29 38.44 51.84 36.00 12.090 53.29 49.00 50.41 39.69 43.56 56.25 12.210 50.41 39.69 43.56 47.61 49.00 43.56 12.330 53.29 38.44 42.25 36.00 32.49 47.61 12.450 39.69 43.56 43.56 44.89 32.49 50.41 12.570 38.44 43.56 47.61 32.49 39.69 39.69 12.690 43.56 43.56 42.25 43.56 40.96 53.29 12.810 36.00 26.01 40.96 43.56 32.49 39.69 12.930 43.56 43.56 51.84 36.00 32.49 47.61 13.050 40.96 44.89 42.25 47.61 38.44 34.81 13.170 47.61 46.24 49.00 42.25 38.44 44.89 13.290 38.44 43.56 51.84 53.29 37.21 43.56 13.410 37.21 31.36 40.96 39.69 38.44 42.25 13.530 49.00 50.41 44.89 42.25 39.69 44.89 13.650 49.00 32.49 39.69 44.89 37.21 44.89 13.770 43.56 47.61 47.61 34.81 34.81 43.56 13.890 56.25 36.00 44.89 43.56 43.56 47.61 14.010 47.61 53.29 37.21 42.25 33.64 51.84 14.130 29.16 43.56 43.56 34.81 54.76 38.44 14.250 30.25 42.25 36.00 40.96 37.21 47.61 14.370 32.49 43.56 38.44 40.96 38.44 44.89 14.490 42.25 27.04 38.44 53.29 43.56 38.44 14.610 43.56 47.61 44.89 38.44 50.41 38.44 14.730 47.61 47.61 36.00 38.44 43.56 44.89 14.850 44.89 44.89 44.89 43.56 44.89 44.89 14.970 46.24 32.49 42.25 40.96 44.89 53.29 15.090 33.64 50.41 44.89 47.61 43.56 37.21 15.210 43.56 42.25 46.24 60.84 54.76 47.61 15.330 50.41 47.61 43.56 42.25 49.00 43.56 15.450 34.81 40.96 46.24 47.61 64.00 50.41 15.570 46.24 50.41 46.24 42.25 46.24 42.25 15.690 37.21 46.24 54.76 51.84 47.61 44.89 15.810 62.41 50.41 53.29 50.41 42.25 51.84 15.930 39.69 60.84 43.56 49.00 42.25 56.25 16.050 47.61 57.76 38.44 57.76 50.41 56.25 16.170 47.61 39.69 43.56 53.29 56.25 49.00 16.290 43.56 53.29 51.84 40.96 47.61 50.41 16.410 56.25 43.56 38.44 54.76 54.76 49.00 16.530 43.56 53.29 54.76 50.41 46.24 40.96 16.650 47.61 50.41 44.89 47.61 40.96 56.25 16.770 42.25 57.76 33.64 37.21 40.96 50.41 16.890 43.56 37.21 34.81 32.49 50.41 49.00 17.010 43.56 39.69 44.89 50.41 47.61 42.25 17.130 33.64 44.89 53.29 38.44 39.69 32.49 17.250 44.89 42.25 32.49 53.29 36.00 43.56 17.370 32.49 47.61 38.44 47.61 39.69 43.56 17.490 51.84 42.25 26.01 32.49 43.56 38.44 17.610 34.81 40.96 34.81 53.29 37.21 34.81 17.730 40.96 30.25 34.81 38.44 43.56 53.29

199

File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 36.00 47.61 50.41 24.01 38.44 40.96 17.970 47.61 38.44 38.44 43.56 43.56 42.25 18.090 44.89 25.00 44.89 42.25 36.00 37.21 18.210 43.56 33.64 38.44 40.96 38.44 23.04 18.330 38.44 47.61 43.56 47.61 43.56 29.16 18.450 29.16 34.81 38.44 38.44 36.00 38.44 18.570 43.56 32.49 49.00 44.89 26.01 56.25 18.690 47.61 44.89 54.76 42.25 49.00 39.69 18.810 38.44 34.81 38.44 47.61 43.56 30.25 18.930 29.16 43.56 42.25 46.24 37.21 43.56 19.050 39.69 30.25 42.25 34.81 31.36 43.56 19.170 47.61 50.41 47.61 38.44 39.69 44.89 19.290 38.44 42.25 49.00 39.69 32.49 38.44 19.410 36.00 53.29 34.81 39.69 44.89 39.69 19.530 33.64 28.09 29.16 46.24 44.89 40.96 19.650 42.25 43.56 37.21 49.00 33.64 30.25 19.770 38.44 38.44 43.56 43.56 33.64 32.49 19.890 46.24 40.96 42.25 47.61 37.21 39.69 20.010 43.56 30.25 42.25 28.09 30.25 38.44 20.130 47.61 33.64 33.64 46.24 37.21 33.64 20.250 38.44 38.44 36.00 37.21 43.56 43.56 20.370 47.61 47.61 37.21 47.61 38.44 31.36 20.490 27.04 38.44 37.21 32.49 33.64 42.25 20.610 50.41 40.96 38.44 65.61 43.56 47.61 20.730 49.00 68.89 62.41 67.24 70.56 88.36 20.850 94.09 70.56 56.25 47.61 47.61 47.61 20.970 51.84 53.29 43.56 43.56 38.44 46.24 21.090 37.21 43.56 44.89 42.25 43.56 54.76 21.210 43.56 54.76 38.44 50.41 46.24 50.41 21.330 46.24 43.56 53.29 38.44 31.36 43.56 21.450 38.44 43.56 38.44 38.44 47.61 39.69 21.570 33.64 39.69 50.41 43.56 47.61 38.44 21.690 50.41 39.69 50.41 44.89 50.41 40.96 21.810 47.61 53.29 54.76 59.29 70.56 65.61 21.930 92.16 88.36 104.04 112.36 118.81 112.36 22.050 90.25 84.64 70.56 72.25 50.41 50.41 22.170 59.29 57.76 33.64 47.61 47.61 40.96 22.290 44.89 39.69 33.64 38.44 34.81 32.49 22.410 43.56 37.21 40.96 34.81 30.25 34.81 22.530 43.56 36.00 24.01 42.25 47.61 38.44 22.650 51.84 37.21 44.89 39.69 31.36 38.44 22.770 46.24 30.25 44.89 40.96 32.49 39.69 22.890 39.69 32.49 43.56 31.36 37.21 37.21 23.010 40.96 38.44 40.96 32.49 43.56 32.49 23.130 43.56 38.44 38.44 40.96 39.69 27.04 23.250 40.96 38.44 34.81 43.56 34.81 23.04 23.370 46.24 33.64 30.25 36.00 37.21 38.44 23.490 40.96 39.69 46.24 36.00 44.89 32.49 23.610 44.89 50.41 47.61 46.24 57.76 47.61 23.730 50.41 56.25 65.61 68.89 79.21 77.44 23.850 79.21 112.36 121.00 116.64 116.64 134.56 23.970 190.44 219.04 222.01 259.21 219.04 231.04

200

File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 201.64 151.29 153.76 146.41 102.01 98.01 24.210 64.00 62.41 75.69 65.61 65.61 47.61 24.330 56.25 36.00 46.24 43.56 40.96 34.81 24.450 42.25 49.00 34.81 49.00 46.24 46.24 24.570 26.01 42.25 34.81 38.44 44.89 47.61 24.690 43.56 46.24 47.61 33.64 32.49 38.44 24.810 32.49 40.96 40.96 34.81 40.96 42.25 24.930 42.25 47.61 30.25 37.21 53.29 38.44 25.050 51.84 42.25 30.25 37.21 37.21 38.44 25.170 47.61 42.25 47.61 38.44 36.00 32.49 25.290 49.00 37.21 42.25 38.44 32.49 42.25 25.410 34.81 32.49 34.81 34.81 39.69 26.01 25.530 27.04 33.64 27.04 42.25 49.00 38.44 25.650 47.61 40.96 28.09 38.44 43.56 50.41 25.770 32.49 36.00 50.41 33.64 38.44 31.36 25.890 32.49 42.25 32.49 36.00 34.81 43.56 26.010 51.84 32.49 33.64 42.25 37.21 38.44 26.130 47.61 36.00 57.76 42.25 47.61 44.89 26.250 49.00 40.96 32.49 43.56 46.24 39.69 26.370 28.09 43.56 50.41 56.25 53.29 75.69 26.490 70.56 82.81 100.00 116.64 129.96 153.76 26.610 129.96 132.25 123.21 114.49 88.36 72.25 26.730 65.61 36.00 47.61 29.16 47.61 33.64 26.850 38.44 33.64 40.96 34.81 38.44 37.21 26.970 43.56 32.49 29.16 38.44 38.44 36.00 27.090 27.04 27.04 28.09 46.24 42.25 26.01 27.210 38.44 32.49 37.21 33.64 33.64 25.00 27.330 33.64 32.49 36.00 32.49 33.64 32.49 27.450 49.00 34.81 32.49 43.56 38.44 37.21 27.570 34.81 27.04 36.00 36.00 53.29 39.69 27.690 25.00 30.25 29.16 30.25 33.64 32.49 27.810 37.21 42.25 26.01 34.81 32.49 43.56 27.930 34.81 49.00 28.09 36.00 43.56 25.00 28.050 36.00 26.01 25.00 28.09 39.69 39.69 28.170 43.56 43.56 30.25 38.44 43.56 37.21 28.290 32.49 31.36 47.61 36.00 27.04 32.49 28.410 38.44 39.69 57.76 50.41 46.24 42.25 28.530 54.76 50.41 47.61 33.64 44.89 38.44 28.650 43.56 36.00 49.00 38.44 36.00 36.00 28.770 33.64 44.89 29.16 43.56 33.64 42.25 28.890 39.69 42.25 32.49 47.61 36.00 32.49 29.010 43.56 36.00 40.96 30.25 47.61 33.64 29.130 46.24 37.21 40.96 32.49 40.96 36.00 29.250 39.69 53.29 65.61 53.29 56.25 60.84 29.370 59.29 43.56 59.29 60.84 56.25 47.61 29.490 39.69 65.61 56.25 46.24 56.25 40.96 29.610 43.56 43.56 60.84 50.41 46.24 49.00 29.730 65.61 50.41 54.76 47.61 56.25 53.29 29.850 72.25 60.84 47.61 59.29 49.00 59.29 29.970 67.24 70.56 50.41 77.44 67.24 79.21 30.090 77.44 70.56 67.24 77.44 75.69 81.00 30.210 84.64 102.01 88.36 100.00 125.44 100.00

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File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 141.61 136.89 153.76 169.00 171.61 190.44 30.450 204.49 219.04 272.25 313.29 285.61 361.00 30.570 392.04 416.16 428.49 529.00 595.36 676.00 30.690 918.09 979.69 1260.25 1451.61 1780.84 2332.89 30.810 3036.01 3660.25 4462.24 5372.89 6336.16 7072.81 30.930 7378.81 7396.00 6724.00 5760.81 5012.64 4108.81 31.050 3158.44 2332.89 1806.25 1317.69 1082.41 942.49 31.170 745.29 645.16 515.29 428.49 396.01 324.00 31.290 302.76 299.29 249.64 231.04 219.04 182.25 31.410 182.25 169.00 127.69 134.56 144.00 123.21 31.530 110.25 100.00 106.09 112.36 88.36 104.04 31.650 94.09 98.01 82.81 84.64 75.69 70.56 31.770 90.25 81.00 68.89 68.89 72.25 67.24 31.890 81.00 75.69 60.84 70.56 70.56 82.81 32.010 62.41 56.25 59.29 53.29 43.56 65.61 32.130 57.76 59.29 50.41 46.24 70.56 57.76 32.250 59.29 53.29 64.00 53.29 50.41 50.41 32.370 49.00 53.29 56.25 49.00 42.25 50.41 32.490 49.00 53.29 67.24 39.69 65.61 44.89 32.610 47.61 60.84 49.00 56.25 44.89 53.29 32.730 47.61 47.61 68.89 47.61 54.76 47.61 32.850 64.00 50.41 67.24 56.25 62.41 54.76 32.970 79.21 90.25 67.24 94.09 94.09 67.24 33.090 81.00 75.69 88.36 70.56 82.81 75.69 33.210 67.24 70.56 88.36 98.01 90.25 104.04 33.330 125.44 123.21 129.96 158.76 196.00 225.00 33.450 262.44 275.56 316.84 331.24 353.44 357.21 33.570 289.00 256.00 228.01 207.36 187.69 151.29 33.690 104.04 108.16 94.09 72.25 79.21 73.96 33.810 57.76 72.25 53.29 50.41 57.76 59.29 33.930 56.25 40.96 38.44 50.41 57.76 43.56 34.050 40.96 50.41 51.84 47.61 44.89 38.44 34.170 51.84 47.61 50.41 27.04 44.89 38.44 34.290 34.81 42.25 37.21 47.61 38.44 39.69 34.410 47.61 53.29 39.69 53.29 43.56 50.41 34.530 38.44 43.56 33.64 56.25 42.25 46.24 34.650 47.61 56.25 43.56 49.00 44.89 64.00 34.770 47.61 49.00 57.76 43.56 56.25 54.76 34.890 51.84 53.29 59.29 75.69 56.25 65.61 35.010 77.44 92.16 100.00 94.09 98.01 114.49 35.130 125.44 129.96 158.76 187.69 213.16 240.25 35.250 246.49 262.44 285.61 292.41 282.24 243.36 35.370 228.01 196.00 182.25 148.84 136.89 146.41 35.490 121.00 112.36 79.21 70.56 67.24 59.29 35.610 57.76 65.61 59.29 62.41 50.41 40.96 35.730 57.76 54.76 56.25 62.41 47.61 53.29 35.850 46.24 50.41 50.41 53.29 50.41 42.25 35.970 50.41 60.84 40.96 49.00 54.76 54.76 36.090 38.44 51.84 53.29 43.56 43.56 49.00 36.210 36.00 44.89 39.69 49.00 39.69 38.44 36.330 49.00 50.41 50.41 59.29 50.41 75.69 36.450 70.56 54.76 77.44 70.56 79.21 77.44

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File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 70.56 59.29 57.76 65.61 67.24 70.56 36.690 67.24 70.56 67.24 73.96 84.64 75.69 36.810 75.69 100.00 88.36 90.25 84.64 84.64 36.930 110.25 106.09 129.96 121.00 141.61 148.84 37.050 146.41 136.89 129.96 166.41 171.61 184.96 37.170 184.96 216.09 237.16 265.69 306.25 380.25 37.290 416.16 470.89 515.29 547.56 533.61 453.69 37.410 420.25 334.89 338.56 282.24 240.25 198.81 37.530 174.24 151.29 156.25 125.44 129.96 94.09 37.650 96.04 82.81 77.44 79.21 72.25 65.61 37.770 59.29 65.61 62.41 59.29 46.24 50.41 37.890 43.56 59.29 46.24 42.25 38.44 49.00 38.010 47.61 53.29 39.69 50.41 47.61 46.24 38.130 53.29 62.41 38.44 50.41 40.96 43.56 38.250 32.49 53.29 49.00 53.29 32.49 32.49 38.370 38.44 44.89 32.49 47.61 53.29 44.89 38.490 42.25 49.00 43.56 49.00 44.89 34.81 38.610 43.56 34.81 38.44 37.21 47.61 30.25 38.730 38.44 42.25 36.00 47.61 43.56 31.36 38.850 50.41 42.25 38.44 47.61 39.69 44.89 38.970 51.84 49.00 39.69 34.81 43.56 43.56 39.090 40.96 53.29 40.96 47.61 56.25 43.56 39.210 57.76 67.24 53.29 53.29 50.41 50.41 39.330 72.25 64.00 53.29 67.24 72.25 70.56 39.450 73.96 81.00 62.41 54.76 81.00 72.25 39.570 73.96 70.56 62.41 88.36 92.16 86.49 39.690 92.16 98.01 84.64 94.09 88.36 108.16 39.810 94.09 125.44 112.36 98.01 121.00 108.16 39.930 116.64 127.69 110.25 98.01 108.16 100.00 40.050 100.00 88.36 104.04 88.36 86.49 77.44 40.170 65.61 65.61 62.41 62.41 54.76 67.24 40.290 70.56 57.76 56.25 62.41 56.25 53.29 40.410 65.61 68.89 70.56 79.21 81.00 92.16 40.530 86.49 79.21 86.49 81.00 108.16 118.81 40.650 98.01 108.16 148.84 176.89 163.84 174.24 40.770 174.24 190.44 201.64 237.16 246.49 309.76 40.890 331.24 376.36 475.24 524.41 635.04 784.00 41.010 954.81 1122.25 1253.16 1274.49 1398.76 1444.00 41.130 1466.89 1317.69 1246.09 1102.24 979.69 906.01 41.250 767.29 635.04 590.49 432.64 368.64 342.25 41.370 295.84 272.25 210.25 204.49 184.96 144.00 41.490 136.89 144.00 141.61 92.16 92.16 92.16 41.610 88.36 86.49 82.81 62.41 77.44 67.24 41.730 68.89 81.00 67.24 56.25 53.29 57.76 41.850 56.25 64.00 62.41 49.00 56.25 50.41 41.970 43.56 50.41 44.89 33.64 47.61 50.41 42.090 32.49 42.25 50.41 47.61 47.61 46.24 42.210 42.25 51.84 43.56 32.49 39.69 42.25 42.330 43.56 60.84 72.25 43.56 47.61 59.29 42.450 51.84 50.41 47.61 59.29 56.25 39.69 42.570 34.81 38.44 42.25 34.81 36.00 43.56 42.690 46.24 37.21 47.61 59.29 38.44 43.56

203

File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 38.44 37.21 38.44 38.44 36.00 44.89 42.930 46.24 47.61 49.00 53.29 49.00 53.29 43.050 47.61 44.89 38.44 34.81 43.56 47.61 43.170 59.29 38.44 56.25 47.61 49.00 46.24 43.290 50.41 50.41 57.76 39.69 56.25 54.76 43.410 64.00 82.81 51.84 67.24 72.25 77.44 43.530 81.00 84.64 77.44 104.04 121.00 139.24 43.650 156.25 182.25 156.25 207.36 256.00 262.44 43.770 246.49 278.89 262.44 210.25 228.01 210.25 43.890 216.09 182.25 134.56 123.21 98.01 96.04 44.010 98.01 92.16 77.44 59.29 84.64 67.24 44.130 68.89 68.89 70.56 59.29 56.25 64.00 44.250 54.76 56.25 53.29 59.29 56.25 59.29 44.370 68.89 62.41 59.29 79.21 84.64 77.44 44.490 86.49 70.56 90.25 104.04 121.00 125.44 44.610 136.89 153.76 161.29 184.96 196.00 252.81 44.730 256.00 309.76 380.25 497.29 547.56 665.64 44.850 745.29 784.00 846.81 858.49 894.01 800.89 44.970 734.41 681.21 620.01 580.81 510.76 428.49 45.090 353.44 295.84 240.25 240.25 196.00 163.84 45.210 166.41 129.96 156.25 108.16 106.09 94.09 45.330 92.16 70.56 77.44 84.64 65.61 70.56 45.450 75.69 54.76 70.56 53.29 67.24 59.29 45.570 47.61 46.24 44.89 54.76 56.25 60.84 45.690 47.61 56.25 53.29 38.44 59.29 53.29 45.810 53.29 43.56 47.61 50.41 40.96 43.56 45.930 50.41 39.69 42.25 47.61 53.29 47.61 46.050 39.69 57.76 43.56 47.61 57.76 47.61 46.170 50.41 46.24 53.29 47.61 46.24 59.29 46.290 62.41 56.25 56.25 32.49 38.44 49.00 46.410 44.89 40.96 49.00 50.41 44.89 46.24 46.530 47.61 56.25 38.44 50.41 43.56 60.84 46.650 50.41 59.29 46.24 44.89 53.29 39.69 46.770 46.24 44.89 49.00 32.49 46.24 34.81 46.890 53.29 42.25 43.56 43.56 46.24 38.44 47.010 37.21 44.89 47.61 39.69 53.29 39.69 47.130 47.61 33.64 47.61 31.36 43.56 43.56 47.250 53.29 43.56 56.25 64.00 49.00 59.29 47.370 68.89 84.64 90.25 57.76 53.29 62.41 47.490 54.76 47.61 56.25 59.29 40.96 53.29 47.610 49.00 44.89 46.24 43.56 34.81 42.25 47.730 32.49 46.24 47.61 43.56 47.61 32.49 47.850 47.61 46.24 47.61 32.49 50.41 40.96 47.970 31.36 43.56 43.56 44.89 57.76 40.96 48.090 36.00 54.76 46.24 46.24 42.25 56.25 48.210 50.41 53.29 39.69 47.61 53.29 43.56 48.330 47.61 53.29 46.24 46.24 44.89 62.41 48.450 49.00 59.29 43.56 53.29 51.84 67.24 48.570 46.24 56.25 62.41 38.44 40.96 53.29 48.690 56.25 201.64 47.61 64.00 70.56 77.44 48.810 62.41 59.29 72.25 82.81 56.25 88.36 48.930 81.00 75.69 100.00 114.49 108.16 114.49

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File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 136.89 136.89 171.61 169.00 213.16 198.81 49.170 219.04 249.64 246.49 243.36 278.89 275.56 49.290 285.61 285.61 225.00 231.04 237.16 193.21 49.410 187.69 166.41 153.76 151.29 118.81 114.49 49.530 121.00 104.04 114.49 121.00 98.01 98.01 49.650 100.00 108.16 92.16 106.09 106.09 94.09 49.770 100.00 112.36 88.36 96.04 94.09 127.69 49.890 110.25 132.25 118.81 129.96 110.25 139.24 50.010 169.00 148.84 176.89 196.00 216.09 272.25 50.130 246.49 249.64 272.25 243.36 299.29 295.84 50.250 361.00 388.09 420.25 492.84 542.89 576.00 50.370 660.49 761.76 800.89 1049.76 1135.69 1190.25 50.490 1376.41 1413.76 1398.76 1413.76 1246.09 1169.64 50.610 1102.24 1024.00 998.56 888.04 864.36 712.89 50.730 681.21 635.04 556.96 556.96 552.25 566.44 50.850 625.00 696.96 756.25 789.61 870.25 1036.84 50.970 1069.29 1122.25 1162.81 1218.01 1204.09 1122.25 51.090 1115.56 1043.29 1056.25 888.04 888.04 841.00 51.210 739.84 696.96 620.01 610.09 542.89 470.89 51.330 388.09 345.96 331.24 285.61 299.29 234.09 51.450 231.04 187.69 169.00 169.00 158.76 182.25 51.570 132.25 125.44 139.24 90.25 116.64 96.04 51.690 106.09 92.16 92.16 79.21 70.56 72.25 51.810 67.24 65.61 60.84 73.96 68.89 64.00 51.930 62.41 60.84 62.41 72.25 59.29 56.25 52.050 62.41 59.29 57.76 53.29 65.61 59.29 52.170 67.24 72.25 59.29 65.61 68.89 82.81 52.290 72.25 59.29 64.00 62.41 60.84 73.96 52.410 68.89 70.56 62.41 53.29 57.76 70.56 52.530 67.24 64.00 64.00 53.29 65.61 46.24 52.650 59.29 47.61 57.76 47.61 40.96 42.25 52.770 53.29 40.96 47.61 47.61 47.61 47.61 52.890 49.00 39.69 56.25 50.41 49.00 43.56 53.010 44.89 49.00 43.56 57.76 47.61 59.29 53.130 49.00 44.89 53.29 49.00 50.41 37.21 53.250 33.64 65.61 50.41 39.69 50.41 43.56 53.370 47.61 50.41 38.44 47.61 39.69 42.25 53.490 40.96 43.56 44.89 50.41 43.56 50.41 53.610 43.56 47.61 50.41 43.56 46.24 53.29 53.730 33.64 28.09 46.24 49.00 51.84 50.41 53.850 38.44 34.81 36.00 42.25 34.81 43.56 53.970 43.56 40.96 42.25 36.00 53.29 28.09 54.090 47.61 34.81 49.00 53.29 29.16 47.61 54.210 30.25 46.24 31.36 33.64 49.00 47.61 54.330 42.25 27.04 47.61 44.89 42.25 47.61 54.450 43.56 37.21 38.44 60.84 29.16 39.69 54.570 40.96 43.56 44.89 40.96 34.81 32.49 54.690 39.69 53.29 53.29 37.21 34.81 47.61 54.810 44.89 44.89 47.61 47.61 37.21 42.25 54.930 38.44 38.44 38.44 31.36 33.64 56.25 55.050 43.56 31.36 28.09 37.21 28.09 36.00 55.170 38.44 37.21 32.49 38.44 43.56 37.21

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File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 31.36 38.44 25.00 32.49 49.00 33.64 55.410 40.96 36.00 34.81 26.01 33.64 33.64 55.530 31.36 38.44 38.44 46.24 32.49 31.36 55.650 34.81 29.16 36.00 43.56 31.36 37.21 55.770 29.16 32.49 39.69 36.00 37.21 46.24 55.890 38.44 23.04 39.69 42.25 42.25 37.21 56.010 43.56 29.16 50.41 59.29 43.56 56.25 56.130 54.76 65.61 60.84 62.41 77.44 82.81 56.250 84.64 73.96 56.25 59.29 59.29 57.76 56.370 65.61 59.29 60.84 56.25 38.44 47.61 56.490 38.44 38.44 38.44 25.00 29.16 40.96 56.610 38.44 32.49 38.44 38.44 37.21 32.49 56.730 38.44 51.84 36.00 32.49 43.56 47.61 56.850 33.64 44.89 36.00 32.49 38.44 31.36 56.970 40.96 42.25 23.04 46.24 32.49 36.00 57.090 50.41 31.36 33.64 38.44 39.69 33.64 57.210 38.44 28.09 43.56 39.69 44.89 34.81 57.330 47.61 43.56 40.96 32.49 42.25 51.84 57.450 27.04 33.64 51.84 39.69 47.61 38.44 57.570 47.61 32.49 42.25 28.09 32.49 36.00 57.690 39.69 34.81 30.25 43.56 38.44 31.36 57.810 38.44 34.81 50.41 44.89 42.25 39.69 57.930 28.09 51.84 38.44 49.00 33.64 34.81 58.050 43.56 33.64 39.69 38.44 43.56 38.44 58.170 38.44 51.84 38.44 42.25 47.61 56.25 58.290 47.61 53.29 50.41 59.29 54.76 53.29 58.410 51.84 62.41 64.00 65.61 67.24 77.44 58.530 75.69 72.25 98.01 98.01 86.49 114.49 58.650 106.09 123.21 146.41 163.84 161.29 193.21 58.770 210.25 252.81 282.24 331.24 327.61 327.61 58.890 316.84 282.24 256.00 246.49 231.04 231.04 59.010 198.81 213.16 196.00 169.00 163.84 114.49 59.130 129.96 118.81 110.25 94.09 77.44 116.64 59.250 94.09 88.36 112.36 96.04 100.00 104.04 59.370 104.04 121.00 129.96 129.96 134.56 127.69 59.490 139.24 161.29 158.76 166.41 219.04 207.36 59.610 246.49 313.29 320.41 357.21 376.36 408.04 59.730 492.84 492.84 571.21 576.00 519.84 479.61 59.850 466.56 441.00 457.96 479.61 445.21 388.09 59.970 349.69 313.29 259.21 225.00 198.81 176.89 60.090 158.76 141.61 148.84 112.36 108.16 102.01 60.210 121.00 86.49 82.81 79.21 79.21 67.24 60.330 72.25 70.56 62.41 70.56 51.84 54.76 60.450 53.29 70.56 51.84 50.41 57.76 50.41 60.570 60.84 47.61 36.00 47.61 42.25 59.29 60.690 44.89 43.56 38.44 47.61 59.29 50.41 60.810 42.25 56.25 54.76 38.44 43.56 49.00 60.930 50.41 47.61 43.56 39.69 51.84 57.76 61.050 47.61 50.41 50.41 40.96 42.25 47.61 61.170 46.24 38.44 46.24 39.69 49.00 50.41 61.290 44.89 31.36 53.29 47.61 53.29 39.69 61.410 60.84 42.25 47.61 54.76 54.76 54.76

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File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 50.41 43.56 65.61 57.76 75.69 70.56 61.650 53.29 46.24 59.29 73.96 56.25 73.96 61.770 53.29 75.69 65.61 86.49 62.41 77.44 61.890 70.56 75.69 79.21 84.64 84.64 82.81 62.010 88.36 90.25 84.64 72.25 84.64 65.61 62.130 70.56 65.61 77.44 59.29 49.00 56.25 62.250 47.61 59.29 73.96 47.61 56.25 56.25 62.370 59.29 50.41 62.41 54.76 47.61 54.76 62.490 47.61 50.41 43.56 47.61 49.00 40.96 62.610 59.29 47.61 60.84 49.00 57.76 62.41 62.730 60.84 59.29 47.61 68.89 56.25 64.00 62.850 56.25 68.89 53.29 59.29 82.81 86.49 62.970 90.25 79.21 88.36 73.96 90.25 110.25 63.090 121.00 127.69 144.00 158.76 163.84 158.76 63.210 176.89 193.21 231.04 268.96 327.61 334.89 63.330 342.25 400.00 416.16 396.01 412.09 441.00 63.450 345.96 345.96 349.69 361.00 306.25 306.25 63.570 289.00 259.21 234.09 246.49 201.64 190.44 63.690 144.00 151.29 125.44 134.56 121.00 96.04 63.810 100.00 123.21 90.25 110.25 92.16 106.09 63.930 114.49 92.16 98.01 100.00 82.81 92.16 64.050 88.36 84.64 90.25 86.49 84.64 134.56 64.170 118.81 134.56 121.00 121.00 153.76 144.00 64.290 182.25 148.84 213.16 169.00 213.16 231.04 64.410 240.25 275.56 289.00 299.29 268.96 268.96 64.530 256.00 246.49 231.04 219.04 198.81 204.49 64.650 182.25 176.89 161.29 163.84 139.24 153.76 64.770 129.96 148.84 141.61 132.25 139.24 136.89 64.890 129.96 174.24 151.29 174.24 166.41 201.64 65.010 222.01 225.00 252.81 275.56 237.16 249.64 65.130 249.64 262.44 252.81 231.04 204.49 198.81 65.250 196.00 204.49 198.81 184.96 176.89 158.76 65.370 106.09 148.84 141.61 121.00 104.04 96.04 65.490 104.04 84.64 92.16 98.01 92.16 90.25 65.610 92.16 86.49 92.16 86.49 96.04 79.21 65.730 90.25 90.25 73.96 92.16 98.01 110.25 65.850 96.04 123.21 121.00 144.00 136.89 171.61 65.970 146.41 182.25 163.84 153.76 132.25 148.84 66.090 146.41 151.29 158.76 174.24 118.81 134.56 66.210 118.81 129.96 114.49 106.09 110.25 102.01 66.330 98.01 100.00 96.04 79.21 59.29 70.56 66.450 72.25 72.25 75.69 77.44 73.96 67.24 66.570 59.29 47.61 65.61 65.61 72.25 84.64 66.690 62.41 50.41 67.24 65.61 82.81 70.56 66.810 70.56 77.44 60.84 73.96 65.61 84.64 66.930 96.04 114.49 100.00 106.09 112.36 129.96 67.050 121.00 144.00 144.00 144.00 161.29 196.00 67.170 240.25 246.49 272.25 292.41 357.21 400.00 67.290 420.25 453.69 453.69 475.24 436.81 445.21 67.410 353.44 320.41 376.36 364.81 345.96 331.24 67.530 353.44 292.41 285.61 256.00 234.09 222.01 67.650 184.96 161.29 161.29 161.29 151.29 129.96

207

File: JC10.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 98.01 110.25 96.04 90.25 60.84 81.00 67.890 79.21 84.64 73.96 65.61 81.00 84.64 68.010 79.21 65.61 82.81 90.25 81.00 70.56 68.130 75.69 64.00 82.81 70.56 82.81 67.24 68.250 53.29 79.21 59.29 62.41 67.24 46.24 68.370 53.29 62.41 53.29 56.25 56.25 43.56 68.490 49.00 53.29 47.61 43.56 54.76 51.84 68.610 53.29 34.81 53.29 44.89 53.29 38.44 68.730 34.81 51.84 50.41 42.25 40.96 53.29 68.850 44.89 59.29 42.25 54.76 38.44 43.56 68.970 47.61 33.64 50.41 50.41 49.00 40.96 69.090 51.84 62.41 42.25 43.56 56.25 38.44 69.210 39.69 44.89 43.56 38.44 42.25 46.24 69.330 34.81 47.61 38.44 46.24 50.41 40.96 69.450 47.61 50.41 42.25 42.25 44.89 53.29 69.570 43.56 46.24 50.41 44.89 51.84 43.56 69.690 39.69 47.61 77.44 54.76 70.56 59.29 69.810 51.84 62.41 43.56 65.61 60.84 73.96 69.930 64.00 77.44 77.44 79.21 _

208

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC11 Data measured at: 25-Jan-2011 11:57:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 5314.410 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 62.41 75.69 68.89 57.76 73.96 62.41 2.130 59.29 50.41 62.41 70.56 59.29 53.29 2.250 67.24 56.25 51.84 65.61 70.56 50.41 2.370 49.00 43.56 43.56 53.29 38.44 49.00 2.490 50.41 57.76 54.76 53.29 43.56 49.00 2.610 43.56 38.44 50.41 38.44 56.25 49.00 2.730 53.29 49.00 43.56 46.24 47.61 28.09 2.850 46.24 47.61 56.25 50.41 59.29 46.24 2.970 44.89 51.84 33.64 59.29 46.24 56.25 3.090 38.44 43.56 47.61 50.41 50.41 43.56 3.210 53.29 54.76 44.89 34.81 33.64 56.25 3.330 50.41 43.56 43.56 56.25 42.25 40.96 3.450 50.41 46.24 44.89 50.41 53.29 50.41 3.570 59.29 38.44 56.25 49.00 47.61 44.89 3.690 56.25 44.89 44.89 50.41 39.69 53.29 3.810 43.56 53.29 50.41 59.29 54.76 46.24 3.930 36.00 51.84 46.24 49.00 50.41 47.61 4.050 57.76 47.61 38.44 42.25 38.44 54.76 4.170 56.25 49.00 53.29 38.44 37.21 37.21 4.290 38.44 47.61 47.61 47.61 50.41 46.24 4.410 50.41 43.56 38.44 44.89 38.44 40.96 4.530 50.41 43.56 38.44 46.24 47.61 50.41 4.650 49.00 53.29 47.61 49.00 50.41 47.61 4.770 44.89 38.44 47.61 47.61 40.96 59.29 4.890 53.29 51.84 39.69 56.25 37.21 47.61 5.010 47.61 60.84 44.89 62.41 56.25 57.76 5.130 38.44 43.56 51.84 53.29 47.61 49.00 5.250 44.89 40.96 62.41 49.00 57.76 53.29

209

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 34.81 44.89 43.56 40.96 54.76 47.61 5.490 43.56 47.61 59.29 56.25 56.25 47.61 5.610 53.29 50.41 56.25 51.84 51.84 65.61 5.730 40.96 53.29 46.24 42.25 47.61 59.29 5.850 43.56 50.41 42.25 56.25 49.00 62.41 5.970 62.41 44.89 47.61 50.41 50.41 46.24 6.090 43.56 43.56 51.84 42.25 42.25 51.84 6.210 56.25 43.56 43.56 59.29 53.29 51.84 6.330 50.41 42.25 50.41 47.61 47.61 47.61 6.450 36.00 47.61 53.29 53.29 47.61 39.69 6.570 50.41 47.61 44.89 50.41 38.44 49.00 6.690 51.84 38.44 60.84 36.00 42.25 49.00 6.810 37.21 47.61 53.29 53.29 56.25 43.56 6.930 43.56 46.24 39.69 53.29 36.00 49.00 7.050 44.89 47.61 51.84 36.00 31.36 43.56 7.170 51.84 34.81 53.29 46.24 47.61 46.24 7.290 49.00 54.76 49.00 29.16 47.61 47.61 7.410 37.21 38.44 38.44 47.61 51.84 44.89 7.530 50.41 49.00 51.84 50.41 49.00 50.41 7.650 47.61 40.96 36.00 42.25 42.25 39.69 7.770 56.25 46.24 53.29 49.00 32.49 38.44 7.890 36.00 38.44 54.76 47.61 43.56 40.96 8.010 51.84 53.29 42.25 44.89 49.00 47.61 8.130 47.61 47.61 56.25 42.25 39.69 37.21 8.250 39.69 40.96 49.00 47.61 46.24 43.56 8.370 62.41 51.84 47.61 49.00 49.00 47.61 8.490 37.21 51.84 47.61 43.56 39.69 43.56 8.610 43.56 46.24 43.56 34.81 47.61 38.44 8.730 53.29 40.96 51.84 47.61 53.29 47.61 8.850 56.25 49.00 42.25 42.25 43.56 43.56 8.970 49.00 46.24 38.44 46.24 39.69 56.25 9.090 54.76 62.41 38.44 44.89 47.61 51.84 9.210 50.41 37.21 46.24 47.61 32.49 47.61 9.330 47.61 47.61 43.56 53.29 44.89 46.24 9.450 43.56 40.96 37.21 33.64 43.56 39.69 9.570 27.04 29.16 47.61 40.96 53.29 38.44 9.690 38.44 47.61 38.44 43.56 39.69 38.44 9.810 39.69 47.61 42.25 38.44 28.09 43.56 9.930 37.21 38.44 37.21 49.00 38.44 40.96 10.050 32.49 31.36 44.89 50.41 34.81 43.56 10.170 42.25 60.84 38.44 36.00 51.84 36.00 10.290 43.56 42.25 49.00 36.00 36.00 33.64 10.410 43.56 47.61 44.89 43.56 40.96 38.44 10.530 54.76 38.44 51.84 43.56 43.56 34.81 10.650 25.00 47.61 34.81 39.69 51.84 51.84 10.770 29.16 34.81 42.25 30.25 34.81 47.61 10.890 31.36 47.61 43.56 32.49 49.00 38.44 11.010 50.41 39.69 34.81 32.49 46.24 50.41 11.130 38.44 44.89 40.96 42.25 49.00 38.44 11.250 47.61 37.21 37.21 37.21 40.96 28.09 11.370 32.49 30.25 34.81 25.00 49.00 30.25 11.490 53.29 33.64 32.49 32.49 37.21 44.89

210

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 34.81 51.84 47.61 44.89 43.56 31.36 11.730 39.69 47.61 38.44 47.61 53.29 50.41 11.850 47.61 34.81 29.16 43.56 33.64 28.09 11.970 44.89 47.61 43.56 39.69 46.24 44.89 12.090 43.56 42.25 49.00 36.00 43.56 30.25 12.210 38.44 38.44 53.29 50.41 38.44 36.00 12.330 53.29 38.44 31.36 32.49 43.56 37.21 12.450 39.69 36.00 38.44 40.96 33.64 43.56 12.570 30.25 49.00 39.69 37.21 36.00 36.00 12.690 47.61 43.56 42.25 33.64 39.69 33.64 12.810 36.00 40.96 30.25 34.81 39.69 32.49 12.930 38.44 33.64 46.24 42.25 37.21 43.56 13.050 38.44 50.41 49.00 44.89 43.56 38.44 13.170 43.56 32.49 33.64 37.21 43.56 38.44 13.290 43.56 39.69 33.64 42.25 43.56 47.61 13.410 34.81 38.44 38.44 42.25 30.25 34.81 13.530 34.81 36.00 38.44 31.36 33.64 53.29 13.650 38.44 38.44 29.16 25.00 32.49 57.76 13.770 40.96 30.25 38.44 32.49 31.36 40.96 13.890 40.96 36.00 40.96 39.69 34.81 39.69 14.010 43.56 43.56 40.96 38.44 40.96 39.69 14.130 43.56 28.09 32.49 31.36 36.00 31.36 14.250 46.24 36.00 50.41 42.25 49.00 32.49 14.370 42.25 37.21 28.09 34.81 37.21 33.64 14.490 29.16 47.61 34.81 34.81 47.61 39.69 14.610 37.21 31.36 36.00 38.44 46.24 24.01 14.730 34.81 34.81 33.64 37.21 42.25 32.49 14.850 36.00 38.44 38.44 43.56 34.81 40.96 14.970 43.56 43.56 38.44 40.96 40.96 42.25 15.090 47.61 40.96 43.56 38.44 47.61 46.24 15.210 34.81 43.56 40.96 33.64 43.56 59.29 15.330 40.96 38.44 42.25 47.61 50.41 50.41 15.450 42.25 56.25 43.56 44.89 62.41 56.25 15.570 44.89 47.61 56.25 42.25 53.29 47.61 15.690 56.25 53.29 38.44 68.89 50.41 44.89 15.810 49.00 47.61 60.84 49.00 53.29 39.69 15.930 46.24 56.25 65.61 47.61 53.29 59.29 16.050 49.00 39.69 49.00 39.69 47.61 51.84 16.170 47.61 46.24 38.44 59.29 51.84 46.24 16.290 37.21 57.76 46.24 43.56 49.00 53.29 16.410 47.61 47.61 42.25 56.25 43.56 50.41 16.530 42.25 51.84 47.61 46.24 31.36 38.44 16.650 43.56 39.69 38.44 43.56 47.61 47.61 16.770 36.00 40.96 31.36 38.44 43.56 42.25 16.890 46.24 40.96 31.36 43.56 40.96 38.44 17.010 47.61 34.81 34.81 37.21 38.44 39.69 17.130 38.44 31.36 33.64 53.29 36.00 43.56 17.250 39.69 36.00 49.00 32.49 32.49 32.49 17.370 32.49 37.21 34.81 47.61 38.44 43.56 17.490 33.64 38.44 50.41 49.00 37.21 40.96 17.610 39.69 36.00 34.81 33.64 38.44 47.61 17.730 38.44 43.56 30.25 47.61 43.56 32.49

211

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 30.25 43.56 50.41 32.49 37.21 42.25 17.970 32.49 44.89 36.00 38.44 34.81 42.25 18.090 34.81 36.00 32.49 26.01 33.64 26.01 18.210 44.89 29.16 39.69 32.49 43.56 43.56 18.330 32.49 27.04 36.00 53.29 49.00 32.49 18.450 31.36 36.00 32.49 30.25 38.44 31.36 18.570 33.64 32.49 39.69 40.96 43.56 32.49 18.690 32.49 37.21 42.25 39.69 43.56 38.44 18.810 42.25 43.56 40.96 50.41 38.44 43.56 18.930 32.49 32.49 40.96 50.41 33.64 53.29 19.050 36.00 47.61 53.29 37.21 46.24 34.81 19.170 47.61 51.84 43.56 30.25 42.25 47.61 19.290 54.76 40.96 43.56 54.76 44.89 38.44 19.410 43.56 40.96 38.44 44.89 32.49 38.44 19.530 40.96 47.61 31.36 47.61 39.69 37.21 19.650 50.41 43.56 34.81 40.96 42.25 33.64 19.770 43.56 31.36 37.21 47.61 47.61 24.01 19.890 37.21 37.21 37.21 44.89 38.44 38.44 20.010 49.00 32.49 38.44 32.49 15.21 43.56 20.130 33.64 36.00 33.64 43.56 49.00 31.36 20.250 39.69 30.25 44.89 33.64 32.49 50.41 20.370 40.96 31.36 38.44 38.44 42.25 37.21 20.490 32.49 34.81 32.49 33.64 38.44 44.89 20.610 38.44 31.36 38.44 27.04 33.64 38.44 20.730 47.61 49.00 39.69 42.25 40.96 43.56 20.850 38.44 38.44 42.25 43.56 47.61 67.24 20.970 62.41 70.56 53.29 50.41 50.41 34.81 21.090 33.64 37.21 37.21 38.44 32.49 53.29 21.210 38.44 44.89 43.56 34.81 50.41 42.25 21.330 36.00 36.00 31.36 38.44 43.56 37.21 21.450 37.21 27.04 38.44 39.69 43.56 28.09 21.570 24.01 36.00 22.09 43.56 38.44 46.24 21.690 28.09 33.64 26.01 32.49 40.96 36.00 21.810 42.25 32.49 40.96 42.25 42.25 40.96 21.930 39.69 51.84 47.61 43.56 40.96 53.29 22.050 50.41 56.25 79.21 86.49 127.69 102.01 22.170 104.04 81.00 77.44 72.25 62.41 42.25 22.290 36.00 38.44 43.56 42.25 38.44 38.44 22.410 30.25 31.36 39.69 34.81 36.00 30.25 22.530 40.96 30.25 38.44 33.64 29.16 33.64 22.650 38.44 32.49 36.00 31.36 27.04 43.56 22.770 29.16 44.89 32.49 32.49 34.81 19.36 22.890 34.81 27.04 40.96 39.69 36.00 31.36 23.010 39.69 44.89 34.81 31.36 46.24 32.49 23.130 43.56 42.25 31.36 30.25 29.16 26.01 23.250 46.24 38.44 32.49 37.21 30.25 28.09 23.370 38.44 32.49 26.01 30.25 36.00 30.25 23.490 26.01 32.49 25.00 42.25 32.49 40.96 23.610 34.81 39.69 31.36 29.16 34.81 34.81 23.730 29.16 34.81 27.04 33.64 42.25 34.81 23.850 42.25 38.44 43.56 64.00 44.89 50.41 23.970 59.29 62.41 84.64 88.36 94.09 104.04

212

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 96.04 114.49 118.81 151.29 153.76 174.24 24.210 174.24 132.25 125.44 88.36 72.25 53.29 24.330 50.41 38.44 42.25 32.49 39.69 36.00 24.450 32.49 34.81 30.25 33.64 32.49 34.81 24.570 38.44 27.04 43.56 34.81 30.25 39.69 24.690 33.64 39.69 37.21 38.44 37.21 33.64 24.810 28.09 38.44 30.25 34.81 27.04 33.64 24.930 39.69 32.49 28.09 31.36 32.49 38.44 25.050 27.04 39.69 33.64 43.56 37.21 47.61 25.170 31.36 36.00 34.81 29.16 37.21 43.56 25.290 54.76 29.16 39.69 38.44 37.21 43.56 25.410 37.21 25.00 32.49 39.69 32.49 33.64 25.530 40.96 37.21 37.21 32.49 38.44 32.49 25.650 34.81 27.04 36.00 34.81 38.44 29.16 25.770 43.56 36.00 32.49 38.44 34.81 36.00 25.890 29.16 47.61 34.81 37.21 34.81 33.64 26.010 31.36 29.16 47.61 34.81 29.16 43.56 26.130 47.61 40.96 31.36 33.64 40.96 25.00 26.250 29.16 36.00 29.16 32.49 32.49 38.44 26.370 43.56 27.04 39.69 32.49 47.61 38.44 26.490 33.64 38.44 54.76 43.56 49.00 53.29 26.610 47.61 64.00 77.44 81.00 94.09 110.25 26.730 110.25 136.89 129.96 100.00 81.00 64.00 26.850 70.56 50.41 39.69 42.25 43.56 28.09 26.970 34.81 29.16 33.64 26.01 29.16 32.49 27.090 43.56 32.49 36.00 39.69 40.96 26.01 27.210 36.00 27.04 40.96 32.49 40.96 34.81 27.330 36.00 32.49 34.81 34.81 34.81 34.81 27.450 47.61 34.81 36.00 34.81 26.01 29.16 27.570 30.25 21.16 31.36 38.44 22.09 38.44 27.690 39.69 32.49 34.81 36.00 23.04 33.64 27.810 38.44 23.04 27.04 30.25 22.09 29.16 27.930 38.44 24.01 29.16 26.01 24.01 28.09 28.050 34.81 34.81 36.00 43.56 37.21 32.49 28.170 24.01 39.69 42.25 32.49 30.25 28.09 28.290 29.16 34.81 29.16 28.09 33.64 30.25 28.410 39.69 38.44 42.25 34.81 27.04 30.25 28.530 24.01 28.09 33.64 23.04 27.04 38.44 28.650 21.16 21.16 30.25 38.44 33.64 29.16 28.770 30.25 29.16 34.81 38.44 30.25 37.21 28.890 30.25 37.21 37.21 39.69 34.81 28.09 29.010 37.21 36.00 32.49 34.81 27.04 30.25 29.130 32.49 38.44 47.61 31.36 37.21 46.24 29.250 50.41 34.81 32.49 31.36 50.41 28.09 29.370 37.21 44.89 42.25 62.41 34.81 50.41 29.490 56.25 79.21 70.56 79.21 53.29 62.41 29.610 38.44 43.56 53.29 42.25 34.81 38.44 29.730 46.24 38.44 40.96 42.25 43.56 43.56 29.850 51.84 44.89 36.00 44.89 53.29 46.24 29.970 46.24 40.96 51.84 53.29 53.29 64.00 30.090 62.41 56.25 53.29 49.00 54.76 53.29 30.210 67.24 57.76 59.29 51.84 53.29 56.25

213

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 92.16 84.64 88.36 82.81 86.49 68.89 30.450 88.36 112.36 121.00 106.09 125.44 112.36 30.570 158.76 161.29 174.24 234.09 272.25 306.25 30.690 309.76 361.00 376.36 408.04 510.76 566.44 30.810 681.21 812.25 1049.76 1317.69 1592.01 2061.16 30.930 2641.96 3192.25 3906.25 4610.41 4970.25 5314.41 31.050 5140.89 4858.09 4147.36 3576.04 3014.01 2401.00 31.170 1866.24 1354.24 979.69 784.00 595.36 492.84 31.290 408.04 361.00 282.24 265.69 252.81 222.01 31.410 193.21 151.29 132.25 161.29 132.25 112.36 31.530 102.01 110.25 114.49 92.16 84.64 88.36 31.650 75.69 79.21 84.64 53.29 67.24 70.56 31.770 57.76 50.41 54.76 59.29 53.29 53.29 31.890 67.24 37.21 39.69 59.29 62.41 62.41 32.010 47.61 51.84 54.76 50.41 47.61 51.84 32.130 53.29 65.61 43.56 47.61 42.25 47.61 32.250 38.44 38.44 50.41 54.76 33.64 40.96 32.370 37.21 44.89 33.64 34.81 57.76 34.81 32.490 34.81 36.00 38.44 43.56 43.56 47.61 32.610 39.69 44.89 42.25 28.09 47.61 28.09 32.730 34.81 36.00 56.25 36.00 30.25 49.00 32.850 39.69 37.21 43.56 47.61 42.25 32.49 32.970 44.89 51.84 33.64 39.69 43.56 44.89 33.090 47.61 43.56 46.24 38.44 59.29 59.29 33.210 47.61 56.25 77.44 86.49 72.25 79.21 33.330 77.44 96.04 86.49 114.49 106.09 132.25 33.450 136.89 144.00 182.25 184.96 237.16 268.96 33.570 275.56 313.29 361.00 324.00 327.61 306.25 33.690 256.00 187.69 184.96 141.61 112.36 102.01 33.810 94.09 77.44 77.44 72.25 53.29 47.61 33.930 53.29 44.89 56.25 59.29 30.25 33.64 34.050 42.25 39.69 38.44 32.49 37.21 40.96 34.170 44.89 49.00 43.56 28.09 43.56 42.25 34.290 38.44 32.49 34.81 37.21 39.69 19.36 34.410 26.01 26.01 34.81 28.09 26.01 24.01 34.530 43.56 34.81 27.04 33.64 38.44 38.44 34.650 34.81 27.04 33.64 32.49 34.81 38.44 34.770 36.00 36.00 47.61 43.56 43.56 44.89 34.890 42.25 42.25 38.44 47.61 43.56 47.61 35.010 38.44 54.76 50.41 43.56 44.89 53.29 35.130 54.76 47.61 56.25 56.25 67.24 75.69 35.250 96.04 90.25 141.61 169.00 176.89 196.00 35.370 256.00 295.84 278.89 268.96 262.44 240.25 35.490 207.36 193.21 151.29 121.00 108.16 104.04 35.610 82.81 62.41 67.24 50.41 56.25 60.84 35.730 51.84 54.76 43.56 28.09 43.56 42.25 35.850 50.41 27.04 44.89 39.69 38.44 49.00 35.970 34.81 36.00 38.44 34.81 31.36 46.24 36.090 34.81 36.00 42.25 34.81 49.00 44.89 36.210 42.25 39.69 25.00 42.25 36.00 43.56 36.330 32.49 43.56 37.21 40.96 34.81 39.69 36.450 50.41 49.00 49.00 51.84 51.84 51.84

214

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 56.25 64.00 59.29 84.64 77.44 84.64 36.690 79.21 75.69 82.81 79.21 84.64 84.64 36.810 72.25 77.44 100.00 92.16 65.61 106.09 36.930 110.25 106.09 102.01 108.16 92.16 102.01 37.050 106.09 86.49 110.25 86.49 104.04 94.09 37.170 81.00 125.44 98.01 110.25 116.64 139.24 37.290 158.76 176.89 179.56 228.01 256.00 313.29 37.410 372.49 529.00 501.76 519.84 462.25 436.81 37.530 384.16 349.69 272.25 228.01 176.89 112.36 37.650 88.36 92.16 79.21 67.24 82.81 62.41 37.770 56.25 68.89 68.89 60.84 53.29 62.41 37.890 43.56 64.00 62.41 50.41 53.29 46.24 38.010 38.44 49.00 47.61 67.24 44.89 50.41 38.130 59.29 50.41 44.89 51.84 54.76 59.29 38.250 47.61 50.41 34.81 43.56 49.00 37.21 38.370 40.96 32.49 40.96 53.29 40.96 49.00 38.490 33.64 49.00 32.49 31.36 29.16 42.25 38.610 50.41 40.96 37.21 43.56 49.00 33.64 38.730 31.36 65.61 33.64 47.61 44.89 38.44 38.850 36.00 36.00 38.44 43.56 50.41 53.29 38.970 47.61 54.76 47.61 43.56 30.25 43.56 39.090 47.61 49.00 31.36 50.41 50.41 59.29 39.210 47.61 49.00 56.25 59.29 53.29 51.84 39.330 65.61 64.00 64.00 79.21 67.24 67.24 39.450 77.44 79.21 94.09 144.00 187.69 176.89 39.570 158.76 148.84 141.61 161.29 163.84 153.76 39.690 125.44 129.96 151.29 151.29 136.89 116.64 39.810 141.61 141.61 146.41 146.41 144.00 144.00 39.930 144.00 134.56 139.24 134.56 114.49 121.00 40.050 102.01 104.04 90.25 100.00 86.49 86.49 40.170 59.29 64.00 53.29 40.96 44.89 57.76 40.290 38.44 49.00 56.25 50.41 51.84 50.41 40.410 43.56 38.44 44.89 50.41 46.24 39.69 40.530 50.41 53.29 39.69 43.56 53.29 42.25 40.650 50.41 50.41 53.29 59.29 57.76 46.24 40.770 62.41 59.29 82.81 77.44 81.00 102.01 40.890 98.01 136.89 163.84 222.01 246.49 259.21 41.010 364.81 428.49 547.56 566.44 580.81 640.09 41.130 723.61 835.21 1049.76 1036.84 1253.16 1075.84 41.250 1062.76 888.04 795.24 729.00 696.96 533.61 41.370 400.00 320.41 243.36 210.25 144.00 104.04 41.490 123.21 106.09 104.04 77.44 75.69 79.21 41.610 75.69 60.84 65.61 47.61 44.89 53.29 41.730 53.29 46.24 38.44 46.24 38.44 30.25 41.850 42.25 50.41 51.84 44.89 39.69 43.56 41.970 39.69 59.29 47.61 28.09 36.00 36.00 42.090 44.89 36.00 32.49 42.25 37.21 44.89 42.210 33.64 51.84 39.69 50.41 30.25 37.21 42.330 50.41 42.25 31.36 27.04 34.81 32.49 42.450 43.56 50.41 40.96 39.69 40.96 53.29 42.570 46.24 50.41 47.61 38.44 47.61 37.21 42.690 44.89 34.81 33.64 42.25 39.69 47.61

215

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 38.44 42.25 37.21 36.00 46.24 39.69 42.930 42.25 43.56 31.36 32.49 51.84 38.44 43.050 36.00 34.81 36.00 38.44 40.96 37.21 43.170 43.56 46.24 44.89 42.25 47.61 46.24 43.290 47.61 46.24 43.56 38.44 62.41 43.56 43.410 38.44 42.25 50.41 47.61 38.44 42.25 43.530 40.96 50.41 40.96 56.25 46.24 62.41 43.650 50.41 70.56 75.69 96.04 79.21 102.01 43.770 106.09 136.89 201.64 216.09 272.25 285.61 43.890 268.96 262.44 228.01 219.04 190.44 166.41 44.010 169.00 158.76 88.36 84.64 82.81 67.24 44.130 53.29 43.56 51.84 43.56 65.61 38.44 44.250 43.56 44.89 47.61 56.25 57.76 44.89 44.370 43.56 43.56 43.56 67.24 46.24 43.56 44.490 38.44 60.84 44.89 65.61 46.24 56.25 44.610 57.76 70.56 72.25 62.41 70.56 82.81 44.730 92.16 114.49 114.49 123.21 146.41 174.24 44.850 190.44 299.29 361.00 453.69 538.24 645.16 44.970 756.25 948.64 1089.00 1043.29 942.49 823.69 45.090 665.64 645.16 640.09 533.61 420.25 357.21 45.210 256.00 187.69 151.29 151.29 127.69 110.25 45.330 102.01 102.01 90.25 75.69 82.81 65.61 45.450 65.61 53.29 65.61 51.84 49.00 47.61 45.570 33.64 53.29 31.36 49.00 34.81 43.56 45.690 39.69 39.69 43.56 32.49 39.69 44.89 45.810 39.69 39.69 43.56 40.96 43.56 38.44 45.930 44.89 56.25 40.96 37.21 38.44 38.44 46.050 31.36 46.24 39.69 49.00 31.36 34.81 46.170 44.89 42.25 53.29 46.24 44.89 50.41 46.290 38.44 47.61 47.61 51.84 39.69 46.24 46.410 65.61 67.24 49.00 38.44 62.41 50.41 46.530 54.76 60.84 47.61 65.61 53.29 54.76 46.650 56.25 56.25 59.29 54.76 50.41 56.25 46.770 53.29 53.29 38.44 33.64 54.76 51.84 46.890 46.24 51.84 43.56 37.21 43.56 43.56 47.010 38.44 42.25 37.21 30.25 47.61 26.01 47.130 36.00 39.69 40.96 36.00 36.00 37.21 47.250 36.00 34.81 40.96 31.36 43.56 32.49 47.370 42.25 40.96 37.21 50.41 38.44 53.29 47.490 42.25 43.56 32.49 40.96 56.25 50.41 47.610 40.96 43.56 47.61 50.41 42.25 40.96 47.730 36.00 43.56 40.96 42.25 38.44 38.44 47.850 54.76 47.61 43.56 53.29 43.56 43.56 47.970 34.81 43.56 38.44 43.56 37.21 32.49 48.090 33.64 31.36 44.89 37.21 40.96 47.61 48.210 39.69 39.69 36.00 40.96 38.44 37.21 48.330 39.69 43.56 43.56 47.61 51.84 34.81 48.450 40.96 47.61 46.24 59.29 56.25 46.24 48.570 49.00 50.41 39.69 44.89 50.41 49.00 48.690 43.56 49.00 59.29 40.96 43.56 46.24 48.810 49.00 56.25 43.56 50.41 47.61 49.00 48.930 43.56 59.29 50.41 67.24 68.89 65.61

216

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 64.00 75.69 56.25 70.56 79.21 90.25 49.170 110.25 104.04 102.01 136.89 148.84 184.96 49.290 225.00 184.96 213.16 256.00 228.01 262.44 49.410 228.01 213.16 174.24 163.84 169.00 148.84 49.530 134.56 121.00 108.16 88.36 86.49 104.04 49.650 88.36 75.69 82.81 64.00 62.41 67.24 49.770 65.61 72.25 60.84 77.44 62.41 65.61 49.890 90.25 59.29 60.84 64.00 92.16 90.25 50.010 94.09 98.01 88.36 110.25 110.25 110.25 50.130 108.16 118.81 144.00 158.76 148.84 176.89 50.250 179.56 196.00 225.00 240.25 275.56 289.00 50.370 384.16 416.16 529.00 571.21 676.00 761.76 50.490 882.09 1082.41 1108.89 1246.09 1274.49 1332.25 50.610 1361.61 1339.56 1346.89 1204.09 1142.44 1049.76 50.730 985.96 930.25 795.24 723.61 595.36 605.16 50.850 529.00 470.89 497.29 479.61 515.29 595.36 50.970 660.49 707.56 784.00 954.81 1017.61 1149.21 51.090 1253.16 1376.41 1361.61 1376.41 1310.44 1225.00 51.210 1211.04 1095.61 954.81 912.04 817.96 702.25 51.330 645.16 556.96 462.25 449.44 368.64 309.76 51.450 272.25 225.00 225.00 219.04 169.00 163.84 51.570 136.89 123.21 104.04 108.16 108.16 98.01 51.690 88.36 79.21 68.89 73.96 75.69 68.89 51.810 70.56 64.00 56.25 56.25 62.41 62.41 51.930 53.29 59.29 46.24 62.41 50.41 59.29 52.050 47.61 65.61 57.76 56.25 56.25 43.56 52.170 53.29 38.44 47.61 56.25 43.56 47.61 52.290 60.84 54.76 62.41 53.29 50.41 62.41 52.410 47.61 47.61 67.24 50.41 56.25 56.25 52.530 59.29 59.29 50.41 53.29 44.89 32.49 52.650 44.89 43.56 43.56 34.81 38.44 43.56 52.770 47.61 38.44 50.41 38.44 43.56 43.56 52.890 50.41 43.56 47.61 51.84 43.56 29.16 53.010 38.44 43.56 51.84 38.44 53.29 50.41 53.130 50.41 43.56 47.61 32.49 31.36 37.21 53.250 34.81 49.00 43.56 30.25 49.00 39.69 53.370 40.96 34.81 36.00 33.64 43.56 26.01 53.490 43.56 39.69 42.25 29.16 36.00 34.81 53.610 34.81 38.44 29.16 33.64 34.81 43.56 53.730 42.25 47.61 28.09 42.25 37.21 40.96 53.850 51.84 40.96 39.69 33.64 42.25 39.69 53.970 33.64 38.44 33.64 37.21 44.89 32.49 54.090 37.21 32.49 25.00 31.36 37.21 47.61 54.210 29.16 23.04 38.44 38.44 39.69 42.25 54.330 39.69 33.64 32.49 23.04 38.44 32.49 54.450 39.69 29.16 31.36 32.49 37.21 38.44 54.570 28.09 33.64 34.81 33.64 27.04 37.21 54.690 32.49 26.01 30.25 39.69 31.36 28.09 54.810 47.61 43.56 37.21 32.49 31.36 34.81 54.930 47.61 36.00 32.49 33.64 30.25 28.09 55.050 37.21 30.25 34.81 31.36 27.04 34.81 55.170 31.36 38.44 36.00 25.00 33.64 32.49

217

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 38.44 30.25 36.00 26.01 38.44 31.36 55.410 46.24 31.36 28.09 34.81 38.44 31.36 55.530 23.04 28.09 29.16 37.21 34.81 30.25 55.650 31.36 28.09 21.16 37.21 24.01 24.01 55.770 28.09 32.49 40.96 24.01 43.56 32.49 55.890 26.01 40.96 32.49 32.49 32.49 31.36 56.010 31.36 33.64 34.81 38.44 31.36 30.25 56.130 32.49 17.64 38.44 38.44 32.49 43.56 56.250 39.69 32.49 38.44 43.56 31.36 39.69 56.370 40.96 31.36 34.81 24.01 32.49 28.09 56.490 34.81 38.44 32.49 32.49 33.64 47.61 56.610 33.64 38.44 26.01 36.00 34.81 32.49 56.730 39.69 43.56 34.81 32.49 28.09 34.81 56.850 22.09 32.49 22.09 38.44 32.49 31.36 56.970 34.81 26.01 50.41 34.81 30.25 28.09 57.090 23.04 39.69 38.44 28.09 31.36 28.09 57.210 32.49 37.21 27.04 47.61 40.96 30.25 57.330 34.81 36.00 32.49 36.00 40.96 46.24 57.450 47.61 31.36 43.56 34.81 44.89 46.24 57.570 26.01 40.96 38.44 46.24 30.25 32.49 57.690 29.16 31.36 29.16 36.00 22.09 32.49 57.810 22.09 34.81 44.89 33.64 26.01 46.24 57.930 32.49 38.44 30.25 30.25 28.09 38.44 58.050 25.00 28.09 46.24 32.49 26.01 33.64 58.170 39.69 38.44 29.16 29.16 26.01 30.25 58.290 47.61 26.01 39.69 36.00 33.64 36.00 58.410 40.96 36.00 31.36 32.49 38.44 31.36 58.530 49.00 37.21 34.81 47.61 56.25 51.84 58.650 49.00 60.84 54.76 57.76 72.25 77.44 58.770 90.25 116.64 125.44 153.76 139.24 190.44 58.890 243.36 268.96 278.89 289.00 246.49 252.81 59.010 228.01 228.01 216.09 190.44 193.21 151.29 59.130 163.84 141.61 129.96 116.64 75.69 88.36 59.250 68.89 60.84 65.61 59.29 42.25 50.41 59.370 50.41 56.25 72.25 59.29 62.41 53.29 59.490 50.41 60.84 65.61 79.21 68.89 72.25 59.610 102.01 100.00 114.49 132.25 153.76 136.89 59.730 201.64 265.69 285.61 327.61 400.00 457.96 59.850 492.84 449.44 506.25 445.21 445.21 408.04 59.970 424.36 342.25 302.76 357.21 295.84 256.00 60.090 225.00 179.56 148.84 141.61 116.64 114.49 60.210 112.36 72.25 68.89 75.69 57.76 57.76 60.330 54.76 50.41 31.36 46.24 59.29 38.44 60.450 43.56 47.61 43.56 37.21 53.29 30.25 60.570 54.76 39.69 37.21 33.64 40.96 44.89 60.690 32.49 46.24 40.96 40.96 36.00 42.25 60.810 36.00 43.56 43.56 32.49 32.49 43.56 60.930 38.44 37.21 26.01 46.24 32.49 39.69 61.050 38.44 34.81 42.25 51.84 39.69 38.44 61.170 27.04 42.25 42.25 36.00 40.96 43.56 61.290 38.44 38.44 38.44 31.36 43.56 43.56 61.410 39.69 42.25 33.64 40.96 32.49 38.44

218

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 38.44 31.36 38.44 40.96 42.25 49.00 61.650 43.56 33.64 59.29 38.44 56.25 53.29 61.770 49.00 40.96 47.61 56.25 50.41 57.76 61.890 53.29 67.24 60.84 81.00 88.36 96.04 62.010 114.49 86.49 96.04 121.00 127.69 100.00 62.130 104.04 104.04 96.04 84.64 86.49 77.44 62.250 84.64 86.49 86.49 62.41 59.29 62.41 62.370 65.61 75.69 59.29 47.61 38.44 38.44 62.490 44.89 34.81 53.29 39.69 49.00 47.61 62.610 30.25 38.44 49.00 34.81 51.84 39.69 62.730 40.96 33.64 36.00 46.24 42.25 56.25 62.850 51.84 49.00 47.61 47.61 39.69 42.25 62.970 50.41 67.24 47.61 53.29 70.56 59.29 63.090 70.56 53.29 68.89 82.81 70.56 96.04 63.210 121.00 104.04 134.56 156.25 182.25 174.24 63.330 219.04 231.04 272.25 302.76 306.25 364.81 63.450 380.25 416.16 428.49 345.96 331.24 285.61 63.570 285.61 268.96 249.64 259.21 256.00 246.49 63.690 193.21 136.89 146.41 129.96 112.36 96.04 63.810 90.25 82.81 60.84 73.96 77.44 75.69 63.930 51.84 60.84 64.00 64.00 62.41 72.25 64.050 53.29 60.84 64.00 70.56 73.96 59.29 64.170 72.25 56.25 65.61 75.69 77.44 75.69 64.290 75.69 73.96 102.01 110.25 125.44 156.25 64.410 148.84 193.21 176.89 182.25 207.36 219.04 64.530 222.01 222.01 219.04 225.00 198.81 198.81 64.650 198.81 207.36 182.25 169.00 146.41 144.00 64.770 125.44 132.25 136.89 112.36 104.04 90.25 64.890 114.49 121.00 125.44 141.61 127.69 125.44 65.010 148.84 182.25 219.04 213.16 231.04 292.41 65.130 289.00 278.89 327.61 334.89 331.24 331.24 65.250 327.61 278.89 272.25 285.61 265.69 259.21 65.370 225.00 196.00 225.00 174.24 187.69 136.89 65.490 148.84 136.89 121.00 112.36 102.01 75.69 65.610 75.69 75.69 65.61 75.69 77.44 62.41 65.730 73.96 72.25 77.44 68.89 70.56 75.69 65.850 72.25 88.36 114.49 72.25 110.25 108.16 65.970 136.89 151.29 153.76 156.25 163.84 198.81 66.090 193.21 225.00 216.09 193.21 169.00 184.96 66.210 163.84 171.61 148.84 163.84 153.76 116.64 66.330 102.01 94.09 98.01 94.09 104.04 88.36 66.450 75.69 60.84 70.56 49.00 47.61 46.24 66.570 51.84 43.56 54.76 50.41 59.29 42.25 66.690 59.29 39.69 32.49 65.61 47.61 39.69 66.810 43.56 47.61 57.76 42.25 44.89 49.00 66.930 56.25 50.41 59.29 56.25 46.24 67.24 67.050 62.41 65.61 68.89 84.64 86.49 86.49 67.170 72.25 104.04 104.04 151.29 136.89 171.61 67.290 198.81 246.49 302.76 327.61 364.81 466.56 67.410 445.21 488.41 404.01 357.21 338.56 324.00 67.530 292.41 295.84 278.89 282.24 256.00 278.89 67.650 243.36 193.21 166.41 129.96 144.00 125.44

219

File: JC11.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 129.96 104.04 86.49 84.64 82.81 59.29 67.890 77.44 67.24 67.24 53.29 68.89 62.41 68.010 62.41 56.25 49.00 43.56 65.61 67.24 68.130 40.96 46.24 65.61 59.29 59.29 56.25 68.250 53.29 46.24 59.29 50.41 64.00 68.89 68.370 65.61 59.29 56.25 50.41 50.41 56.25 68.490 47.61 42.25 47.61 65.61 56.25 47.61 68.610 36.00 47.61 47.61 30.25 46.24 30.25 68.730 32.49 38.44 32.49 40.96 40.96 33.64 68.850 42.25 34.81 37.21 43.56 38.44 38.44 68.970 38.44 32.49 43.56 37.21 33.64 39.69 69.090 25.00 38.44 64.00 37.21 43.56 39.69 69.210 34.81 43.56 34.81 38.44 49.00 39.69 69.330 40.96 36.00 40.96 50.41 37.21 32.49 69.450 32.49 42.25 40.96 44.89 47.61 32.49 69.570 37.21 33.64 36.00 42.25 42.25 34.81 69.690 43.56 43.56 43.56 30.25 43.56 39.69 69.810 56.25 38.44 50.41 36.00 33.64 47.61 69.930 62.41 60.84 44.89 44.89 _

220

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC12 Data measured at: 25-Jan-2011 12:55:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 6432.040 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 108.16 110.25 123.21 110.25 129.96 96.04 2.130 110.25 98.01 82.81 90.25 82.81 84.64 2.250 82.81 90.25 79.21 92.16 84.64 96.04 2.370 90.25 57.76 75.69 75.69 79.21 75.69 2.490 67.24 79.21 62.41 65.61 56.25 72.25 2.610 67.24 70.56 67.24 65.61 82.81 77.44 2.730 77.44 70.56 75.69 62.41 64.00 62.41 2.850 70.56 67.24 75.69 68.89 62.41 65.61 2.970 60.84 47.61 72.25 64.00 49.00 59.29 3.090 67.24 73.96 64.00 60.84 59.29 65.61 3.210 68.89 46.24 46.24 56.25 57.76 59.29 3.330 54.76 62.41 49.00 54.76 73.96 54.76 3.450 60.84 54.76 70.56 57.76 65.61 54.76 3.570 53.29 50.41 67.24 70.56 68.89 49.00 3.690 65.61 50.41 59.29 70.56 50.41 49.00 3.810 72.25 57.76 50.41 62.41 53.29 59.29 3.930 49.00 50.41 53.29 47.61 53.29 59.29 4.050 56.25 53.29 53.29 56.25 56.25 53.29 4.170 47.61 42.25 46.24 65.61 51.84 54.76 4.290 43.56 65.61 56.25 62.41 54.76 57.76 4.410 59.29 54.76 53.29 59.29 56.25 47.61 4.530 53.29 47.61 67.24 44.89 43.56 60.84 4.650 65.61 59.29 54.76 39.69 46.24 51.84 4.770 59.29 59.29 46.24 49.00 56.25 56.25 4.890 62.41 53.29 59.29 57.76 54.76 53.29 5.010 56.25 49.00 43.56 51.84 51.84 50.41 5.130 59.29 53.29 51.84 53.29 53.29 49.00 5.250 59.29 54.76 70.56 44.89 53.29 47.61

221

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 56.25 49.00 53.29 56.25 38.44 50.41 5.490 43.56 62.41 62.41 59.29 65.61 46.24 5.610 47.61 60.84 54.76 47.61 59.29 50.41 5.730 57.76 59.29 67.24 60.84 57.76 56.25 5.850 49.00 53.29 59.29 67.24 47.61 60.84 5.970 60.84 44.89 65.61 44.89 56.25 60.84 6.090 56.25 62.41 46.24 56.25 60.84 44.89 6.210 53.29 50.41 67.24 56.25 47.61 47.61 6.330 62.41 53.29 44.89 50.41 50.41 46.24 6.450 57.76 59.29 47.61 47.61 51.84 47.61 6.570 54.76 46.24 43.56 43.56 59.29 53.29 6.690 36.00 53.29 47.61 53.29 57.76 44.89 6.810 49.00 39.69 36.00 40.96 43.56 59.29 6.930 44.89 53.29 50.41 42.25 56.25 50.41 7.050 50.41 43.56 56.25 49.00 40.96 56.25 7.170 40.96 47.61 42.25 50.41 49.00 43.56 7.290 62.41 53.29 47.61 64.00 57.76 38.44 7.410 47.61 59.29 46.24 47.61 44.89 51.84 7.530 56.25 43.56 51.84 40.96 50.41 59.29 7.650 50.41 47.61 53.29 46.24 53.29 38.44 7.770 59.29 47.61 49.00 47.61 51.84 46.24 7.890 54.76 56.25 51.84 43.56 44.89 42.25 8.010 56.25 60.84 36.00 56.25 50.41 46.24 8.130 57.76 62.41 40.96 53.29 54.76 43.56 8.250 53.29 40.96 37.21 53.29 42.25 46.24 8.370 33.64 40.96 47.61 46.24 54.76 53.29 8.490 46.24 43.56 50.41 59.29 54.76 43.56 8.610 43.56 50.41 49.00 42.25 54.76 38.44 8.730 51.84 42.25 39.69 46.24 37.21 51.84 8.850 62.41 36.00 47.61 53.29 43.56 42.25 8.970 53.29 46.24 49.00 47.61 43.56 59.29 9.090 50.41 42.25 53.29 51.84 43.56 46.24 9.210 47.61 49.00 50.41 47.61 50.41 46.24 9.330 40.96 44.89 37.21 47.61 59.29 47.61 9.450 43.56 59.29 46.24 47.61 50.41 38.44 9.570 50.41 39.69 50.41 46.24 50.41 49.00 9.690 32.49 51.84 47.61 46.24 44.89 53.29 9.810 37.21 49.00 44.89 46.24 56.25 42.25 9.930 57.76 46.24 40.96 40.96 44.89 39.69 10.050 54.76 50.41 47.61 44.89 46.24 53.29 10.170 51.84 47.61 47.61 50.41 47.61 47.61 10.290 54.76 36.00 38.44 47.61 38.44 44.89 10.410 43.56 50.41 47.61 37.21 44.89 33.64 10.530 53.29 33.64 59.29 38.44 46.24 50.41 10.650 42.25 40.96 39.69 44.89 47.61 47.61 10.770 49.00 44.89 44.89 38.44 44.89 36.00 10.890 47.61 43.56 50.41 43.56 39.69 47.61 11.010 38.44 32.49 30.25 56.25 50.41 46.24 11.130 54.76 38.44 32.49 47.61 46.24 43.56 11.250 47.61 47.61 43.56 42.25 44.89 47.61 11.370 38.44 42.25 47.61 50.41 43.56 54.76 11.490 39.69 38.44 54.76 43.56 40.96 40.96

222

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 43.56 50.41 39.69 50.41 29.16 50.41 11.730 53.29 42.25 56.25 39.69 56.25 54.76 11.850 44.89 49.00 59.29 47.61 42.25 34.81 11.970 36.00 43.56 38.44 43.56 47.61 43.56 12.090 44.89 43.56 43.56 43.56 46.24 47.61 12.210 39.69 34.81 47.61 43.56 37.21 53.29 12.330 40.96 47.61 47.61 42.25 46.24 34.81 12.450 44.89 38.44 53.29 33.64 53.29 50.41 12.570 43.56 39.69 29.16 43.56 38.44 44.89 12.690 43.56 32.49 44.89 42.25 34.81 43.56 12.810 33.64 32.49 33.64 38.44 43.56 46.24 12.930 40.96 38.44 49.00 38.44 53.29 30.25 13.050 47.61 39.69 50.41 33.64 50.41 33.64 13.170 30.25 42.25 40.96 42.25 46.24 42.25 13.290 43.56 46.24 46.24 39.69 42.25 30.25 13.410 47.61 47.61 50.41 57.76 38.44 38.44 13.530 30.25 37.21 29.16 38.44 32.49 40.96 13.650 38.44 36.00 44.89 38.44 38.44 36.00 13.770 38.44 36.00 37.21 51.84 38.44 46.24 13.890 44.89 40.96 40.96 42.25 37.21 53.29 14.010 32.49 42.25 46.24 32.49 38.44 43.56 14.130 28.09 43.56 29.16 36.00 37.21 49.00 14.250 54.76 36.00 31.36 43.56 36.00 39.69 14.370 40.96 32.49 44.89 39.69 42.25 40.96 14.490 33.64 43.56 40.96 36.00 46.24 50.41 14.610 38.44 38.44 43.56 33.64 36.00 43.56 14.730 36.00 46.24 47.61 36.00 44.89 32.49 14.850 32.49 38.44 50.41 43.56 39.69 51.84 14.970 38.44 49.00 39.69 44.89 43.56 30.25 15.090 38.44 40.96 37.21 39.69 38.44 37.21 15.210 40.96 49.00 43.56 46.24 43.56 38.44 15.330 38.44 56.25 50.41 34.81 46.24 53.29 15.450 53.29 47.61 47.61 49.00 59.29 38.44 15.570 50.41 43.56 51.84 60.84 50.41 53.29 15.690 56.25 53.29 59.29 59.29 53.29 57.76 15.810 57.76 50.41 50.41 50.41 43.56 43.56 15.930 50.41 47.61 51.84 47.61 46.24 73.96 16.050 49.00 43.56 60.84 42.25 53.29 47.61 16.170 47.61 50.41 56.25 56.25 39.69 60.84 16.290 49.00 40.96 51.84 53.29 38.44 57.76 16.410 37.21 47.61 47.61 40.96 56.25 39.69 16.530 31.36 54.76 44.89 47.61 43.56 43.56 16.650 53.29 54.76 50.41 51.84 54.76 36.00 16.770 43.56 82.81 47.61 47.61 49.00 53.29 16.890 40.96 50.41 49.00 43.56 44.89 30.25 17.010 38.44 42.25 37.21 56.25 47.61 38.44 17.130 46.24 40.96 49.00 56.25 40.96 33.64 17.250 32.49 47.61 36.00 34.81 39.69 43.56 17.370 40.96 25.00 34.81 28.09 38.44 42.25 17.490 36.00 36.00 43.56 27.04 33.64 43.56 17.610 42.25 38.44 36.00 38.44 53.29 43.56 17.730 40.96 38.44 33.64 33.64 40.96 38.44

223

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 34.81 37.21 33.64 43.56 38.44 38.44 17.970 44.89 38.44 42.25 44.89 33.64 31.36 18.090 43.56 38.44 47.61 25.00 47.61 25.00 18.210 49.00 40.96 40.96 24.01 43.56 31.36 18.330 36.00 34.81 49.00 37.21 30.25 38.44 18.450 28.09 30.25 37.21 53.29 49.00 32.49 18.570 36.00 46.24 38.44 38.44 46.24 39.69 18.690 37.21 40.96 31.36 30.25 37.21 43.56 18.810 34.81 38.44 50.41 32.49 30.25 25.00 18.930 31.36 38.44 36.00 28.09 50.41 43.56 19.050 38.44 43.56 38.44 53.29 43.56 47.61 19.170 43.56 43.56 50.41 54.76 42.25 43.56 19.290 47.61 34.81 37.21 46.24 50.41 47.61 19.410 50.41 36.00 38.44 33.64 46.24 42.25 19.530 39.69 46.24 39.69 44.89 50.41 43.56 19.650 36.00 42.25 49.00 43.56 43.56 43.56 19.770 34.81 38.44 37.21 44.89 38.44 43.56 19.890 33.64 34.81 30.25 29.16 39.69 40.96 20.010 37.21 47.61 43.56 50.41 43.56 38.44 20.130 32.49 39.69 34.81 24.01 37.21 37.21 20.250 42.25 46.24 43.56 43.56 37.21 38.44 20.370 38.44 40.96 39.69 36.00 47.61 38.44 20.490 38.44 42.25 33.64 42.25 53.29 47.61 20.610 50.41 50.41 42.25 50.41 44.89 43.56 20.730 50.41 54.76 38.44 33.64 68.89 75.69 20.850 47.61 65.61 67.24 54.76 60.84 70.56 20.970 57.76 50.41 44.89 42.25 29.16 47.61 21.090 39.69 42.25 50.41 32.49 42.25 46.24 21.210 42.25 50.41 33.64 27.04 38.44 36.00 21.330 43.56 42.25 47.61 38.44 37.21 38.44 21.450 37.21 38.44 34.81 32.49 37.21 40.96 21.570 40.96 31.36 47.61 44.89 38.44 50.41 21.690 47.61 38.44 53.29 62.41 46.24 47.61 21.810 50.41 43.56 60.84 53.29 67.24 50.41 21.930 59.29 67.24 70.56 104.04 100.00 121.00 22.050 121.00 134.56 96.04 100.00 90.25 84.64 22.170 79.21 59.29 65.61 54.76 50.41 47.61 22.290 42.25 50.41 47.61 38.44 39.69 50.41 22.410 39.69 38.44 43.56 50.41 40.96 43.56 22.530 39.69 43.56 24.01 43.56 33.64 47.61 22.650 38.44 43.56 47.61 46.24 33.64 38.44 22.770 29.16 38.44 34.81 39.69 32.49 43.56 22.890 36.00 51.84 50.41 36.00 34.81 40.96 23.010 31.36 36.00 38.44 47.61 30.25 40.96 23.130 32.49 34.81 38.44 39.69 32.49 36.00 23.250 37.21 46.24 39.69 36.00 46.24 44.89 23.370 38.44 36.00 40.96 43.56 36.00 43.56 23.490 43.56 50.41 43.56 46.24 53.29 31.36 23.610 53.29 43.56 59.29 56.25 51.84 49.00 23.730 54.76 47.61 49.00 47.61 59.29 51.84 23.850 67.24 77.44 82.81 86.49 88.36 106.09 23.970 134.56 144.00 169.00 204.49 213.16 222.01

224

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 213.16 246.49 166.41 201.64 176.89 144.00 24.210 139.24 112.36 96.04 104.04 72.25 70.56 24.330 60.84 53.29 67.24 49.00 50.41 59.29 24.450 56.25 51.84 38.44 38.44 40.96 46.24 24.570 47.61 43.56 59.29 32.49 43.56 40.96 24.690 47.61 37.21 33.64 47.61 43.56 29.16 24.810 25.00 51.84 39.69 32.49 30.25 38.44 24.930 29.16 38.44 42.25 53.29 25.00 42.25 25.050 37.21 33.64 40.96 47.61 36.00 38.44 25.170 31.36 34.81 39.69 40.96 34.81 33.64 25.290 46.24 40.96 27.04 38.44 40.96 47.61 25.410 38.44 37.21 43.56 44.89 38.44 32.49 25.530 39.69 36.00 31.36 38.44 40.96 43.56 25.650 37.21 38.44 54.76 38.44 33.64 46.24 25.770 44.89 36.00 38.44 38.44 38.44 34.81 25.890 32.49 43.56 50.41 33.64 38.44 37.21 26.010 38.44 36.00 38.44 38.44 34.81 47.61 26.130 47.61 38.44 34.81 51.84 32.49 37.21 26.250 38.44 38.44 40.96 40.96 40.96 38.44 26.370 59.29 44.89 37.21 36.00 47.61 32.49 26.490 56.25 39.69 56.25 70.56 65.61 90.25 26.610 108.16 169.00 156.25 182.25 146.41 153.76 26.730 139.24 102.01 73.96 64.00 54.76 49.00 26.850 43.56 37.21 38.44 40.96 50.41 47.61 26.970 32.49 40.96 53.29 42.25 38.44 36.00 27.090 37.21 43.56 36.00 43.56 38.44 32.49 27.210 30.25 39.69 30.25 47.61 31.36 32.49 27.330 29.16 33.64 33.64 32.49 42.25 32.49 27.450 43.56 50.41 39.69 40.96 34.81 43.56 27.570 38.44 39.69 38.44 40.96 27.04 28.09 27.690 36.00 27.04 38.44 27.04 32.49 38.44 27.810 38.44 43.56 32.49 38.44 31.36 49.00 27.930 38.44 39.69 42.25 29.16 31.36 40.96 28.050 34.81 39.69 40.96 39.69 50.41 43.56 28.170 36.00 31.36 49.00 29.16 31.36 30.25 28.290 32.49 29.16 44.89 38.44 34.81 32.49 28.410 30.25 49.00 42.25 47.61 34.81 34.81 28.530 44.89 43.56 37.21 34.81 43.56 44.89 28.650 32.49 38.44 40.96 38.44 23.04 42.25 28.770 50.41 46.24 50.41 44.89 38.44 28.09 28.890 49.00 38.44 47.61 38.44 43.56 43.56 29.010 42.25 40.96 33.64 39.69 49.00 38.44 29.130 47.61 31.36 32.49 47.61 47.61 47.61 29.250 34.81 46.24 53.29 34.81 42.25 59.29 29.370 51.84 53.29 59.29 54.76 67.24 70.56 29.490 73.96 44.89 65.61 64.00 65.61 65.61 29.610 53.29 62.41 67.24 54.76 53.29 49.00 29.730 51.84 50.41 65.61 60.84 67.24 59.29 29.850 57.76 56.25 72.25 57.76 62.41 59.29 29.970 70.56 75.69 65.61 84.64 64.00 84.64 30.090 81.00 92.16 81.00 84.64 96.04 86.49 30.210 108.16 106.09 110.25 112.36 118.81 127.69

225

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 129.96 153.76 146.41 166.41 201.64 182.25 30.450 231.04 249.64 243.36 306.25 316.84 361.00 30.570 345.96 420.25 441.00 488.41 529.00 655.36 30.690 676.00 734.41 924.16 1017.61 1142.44 1428.84 30.810 1624.09 1998.09 2371.69 2905.21 3540.25 4303.36 30.930 4942.09 5715.36 6368.04 6432.04 6177.96 5806.44 31.050 5140.89 4556.25 3906.25 3124.81 2520.04 2070.25 31.170 1772.41 1303.21 1142.44 1030.41 864.36 761.76 31.290 650.25 585.64 515.29 449.44 404.01 380.25 31.410 320.41 272.25 249.64 246.49 216.09 184.96 31.530 187.69 174.24 169.00 151.29 163.84 129.96 31.650 139.24 127.69 118.81 125.44 121.00 114.49 31.770 112.36 86.49 98.01 104.04 104.04 90.25 31.890 98.01 90.25 82.81 67.24 84.64 70.56 32.010 77.44 70.56 84.64 67.24 70.56 70.56 32.130 82.81 73.96 56.25 70.56 65.61 59.29 32.250 50.41 53.29 59.29 62.41 62.41 56.25 32.370 53.29 59.29 47.61 53.29 53.29 62.41 32.490 51.84 51.84 60.84 67.24 42.25 67.24 32.610 60.84 50.41 47.61 56.25 47.61 43.56 32.730 51.84 47.61 38.44 43.56 44.89 62.41 32.850 47.61 40.96 47.61 40.96 56.25 57.76 32.970 57.76 54.76 44.89 50.41 50.41 56.25 33.090 59.29 50.41 50.41 72.25 62.41 73.96 33.210 65.61 84.64 77.44 92.16 86.49 100.00 33.330 98.01 102.01 102.01 158.76 153.76 174.24 33.450 171.61 225.00 240.25 306.25 285.61 327.61 33.570 324.00 324.00 349.69 306.25 278.89 265.69 33.690 210.25 184.96 174.24 148.84 118.81 98.01 33.810 106.09 82.81 88.36 62.41 70.56 70.56 33.930 59.29 47.61 72.25 62.41 44.89 62.41 34.050 64.00 49.00 67.24 56.25 38.44 51.84 34.170 47.61 43.56 56.25 50.41 59.29 36.00 34.290 33.64 47.61 43.56 53.29 30.25 38.44 34.410 57.76 34.81 47.61 47.61 32.49 36.00 34.530 30.25 50.41 47.61 43.56 34.81 49.00 34.650 50.41 44.89 44.89 47.61 53.29 50.41 34.770 46.24 46.24 43.56 60.84 50.41 54.76 34.890 57.76 65.61 65.61 53.29 79.21 67.24 35.010 50.41 70.56 84.64 62.41 84.64 92.16 35.130 86.49 100.00 110.25 123.21 148.84 184.96 35.250 184.96 213.16 207.36 246.49 246.49 289.00 35.370 289.00 285.61 222.01 207.36 216.09 198.81 35.490 174.24 148.84 146.41 127.69 129.96 104.04 35.610 94.09 79.21 77.44 77.44 67.24 56.25 35.730 70.56 79.21 59.29 64.00 59.29 42.25 35.850 65.61 38.44 54.76 60.84 59.29 40.96 35.970 47.61 59.29 56.25 47.61 46.24 39.69 36.090 47.61 39.69 51.84 38.44 38.44 44.89 36.210 51.84 51.84 49.00 44.89 38.44 49.00 36.330 53.29 38.44 33.64 68.89 53.29 50.41 36.450 56.25 47.61 56.25 50.41 67.24 75.69

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File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 65.61 82.81 90.25 73.96 67.24 70.56 36.690 75.69 73.96 98.01 77.44 72.25 64.00 36.810 90.25 104.04 96.04 92.16 104.04 108.16 36.930 127.69 106.09 132.25 118.81 127.69 134.56 37.050 146.41 144.00 136.89 132.25 166.41 153.76 37.170 187.69 151.29 252.81 225.00 259.21 275.56 37.290 316.84 364.81 404.01 457.96 501.76 497.29 37.410 484.00 492.84 484.00 392.04 376.36 376.36 37.530 313.29 259.21 249.64 207.36 179.56 144.00 37.650 158.76 125.44 127.69 100.00 112.36 121.00 37.770 90.25 98.01 104.04 73.96 82.81 88.36 37.890 68.89 60.84 65.61 67.24 67.24 62.41 38.010 73.96 54.76 59.29 65.61 60.84 73.96 38.130 43.56 43.56 59.29 59.29 59.29 62.41 38.250 53.29 65.61 56.25 56.25 60.84 53.29 38.370 53.29 56.25 64.00 59.29 38.44 46.24 38.490 39.69 50.41 32.49 59.29 38.44 50.41 38.610 56.25 51.84 62.41 57.76 54.76 59.29 38.730 46.24 51.84 50.41 53.29 33.64 46.24 38.850 51.84 60.84 56.25 67.24 46.24 36.00 38.970 60.84 60.84 60.84 56.25 59.29 44.89 39.090 54.76 53.29 56.25 53.29 56.25 67.24 39.210 50.41 47.61 59.29 64.00 53.29 59.29 39.330 56.25 77.44 70.56 84.64 65.61 72.25 39.450 86.49 100.00 98.01 100.00 118.81 104.04 39.570 100.00 118.81 121.00 94.09 110.25 146.41 39.690 127.69 125.44 121.00 123.21 127.69 134.56 39.810 144.00 153.76 144.00 148.84 141.61 163.84 39.930 182.25 163.84 166.41 127.69 123.21 136.89 40.050 110.25 123.21 100.00 123.21 110.25 82.81 40.170 98.01 81.00 79.21 90.25 75.69 70.56 40.290 75.69 68.89 67.24 79.21 70.56 82.81 40.410 88.36 70.56 75.69 59.29 73.96 77.44 40.530 77.44 79.21 94.09 92.16 118.81 96.04 40.650 127.69 123.21 110.25 129.96 144.00 148.84 40.770 166.41 171.61 193.21 207.36 275.56 265.69 40.890 313.29 320.41 361.00 392.04 484.00 552.25 41.010 620.01 795.24 789.61 985.96 1036.84 1128.96 41.130 1267.36 1413.76 1332.25 1421.29 1310.44 1296.00 41.250 1162.81 1049.76 954.81 806.56 750.76 696.96 41.370 556.96 519.84 400.00 376.36 338.56 313.29 41.490 246.49 231.04 228.01 174.24 184.96 139.24 41.610 144.00 127.69 125.44 112.36 121.00 116.64 41.730 116.64 77.44 96.04 100.00 65.61 90.25 41.850 88.36 77.44 67.24 81.00 86.49 75.69 41.970 62.41 56.25 81.00 65.61 75.69 62.41 42.090 37.21 75.69 53.29 57.76 60.84 43.56 42.210 54.76 67.24 59.29 50.41 46.24 67.24 42.330 40.96 62.41 49.00 56.25 53.29 67.24 42.450 56.25 51.84 72.25 59.29 54.76 56.25 42.570 49.00 65.61 47.61 51.84 50.41 47.61 42.690 38.44 53.29 44.89 44.89 56.25 54.76

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File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 47.61 56.25 51.84 53.29 43.56 54.76 42.930 50.41 49.00 56.25 50.41 56.25 64.00 43.050 44.89 62.41 65.61 51.84 53.29 64.00 43.170 67.24 57.76 50.41 73.96 53.29 62.41 43.290 65.61 65.61 72.25 65.61 62.41 62.41 43.410 53.29 60.84 77.44 90.25 51.84 84.64 43.530 75.69 102.01 84.64 94.09 110.25 106.09 43.650 121.00 125.44 146.41 169.00 184.96 193.21 43.770 231.04 240.25 246.49 246.49 252.81 246.49 43.890 207.36 198.81 190.44 169.00 187.69 146.41 44.010 114.49 158.76 116.64 118.81 110.25 90.25 44.130 84.64 88.36 98.01 82.81 77.44 82.81 44.250 72.25 73.96 92.16 84.64 72.25 79.21 44.370 86.49 94.09 86.49 98.01 92.16 98.01 44.490 114.49 96.04 112.36 108.16 100.00 116.64 44.610 129.96 153.76 151.29 171.61 166.41 210.25 44.730 228.01 243.36 268.96 338.56 384.16 408.04 44.850 479.61 580.81 665.64 734.41 806.56 812.25 44.970 778.41 846.81 767.29 756.25 718.24 605.16 45.090 600.25 533.61 432.64 345.96 361.00 313.29 45.210 292.41 231.04 231.04 201.64 179.56 182.25 45.330 148.84 136.89 106.09 123.21 123.21 98.01 45.450 92.16 84.64 79.21 75.69 90.25 82.81 45.570 81.00 65.61 64.00 67.24 84.64 57.76 45.690 60.84 72.25 67.24 70.56 57.76 47.61 45.810 51.84 67.24 70.56 68.89 56.25 59.29 45.930 47.61 56.25 56.25 65.61 47.61 56.25 46.050 54.76 57.76 59.29 54.76 50.41 56.25 46.170 37.21 47.61 62.41 51.84 62.41 57.76 46.290 59.29 67.24 56.25 56.25 72.25 53.29 46.410 64.00 59.29 59.29 56.25 79.21 79.21 46.530 90.25 57.76 67.24 67.24 65.61 79.21 46.650 54.76 50.41 62.41 60.84 47.61 62.41 46.770 62.41 75.69 72.25 62.41 56.25 65.61 46.890 65.61 54.76 62.41 51.84 44.89 50.41 47.010 56.25 62.41 46.24 56.25 49.00 59.29 47.130 43.56 39.69 34.81 38.44 49.00 50.41 47.250 57.76 37.21 43.56 43.56 38.44 49.00 47.370 59.29 38.44 46.24 49.00 51.84 50.41 47.490 38.44 50.41 50.41 44.89 38.44 54.76 47.610 57.76 54.76 64.00 56.25 47.61 43.56 47.730 47.61 49.00 47.61 50.41 46.24 59.29 47.850 37.21 39.69 50.41 59.29 44.89 47.61 47.970 59.29 43.56 43.56 39.69 56.25 43.56 48.090 54.76 51.84 62.41 56.25 42.25 47.61 48.210 53.29 56.25 50.41 44.89 46.24 65.61 48.330 40.96 57.76 50.41 62.41 50.41 59.29 48.450 64.00 53.29 51.84 59.29 60.84 67.24 48.570 70.56 68.89 56.25 53.29 68.89 72.25 48.690 70.56 72.25 88.36 68.89 67.24 73.96 48.810 68.89 88.36 75.69 75.69 84.64 88.36 48.930 106.09 98.01 86.49 134.56 114.49 106.09

228

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 121.00 132.25 134.56 144.00 151.29 166.41 49.170 184.96 207.36 216.09 228.01 243.36 252.81 49.290 249.64 272.25 234.09 252.81 225.00 240.25 49.410 225.00 219.04 234.09 198.81 182.25 158.76 49.530 174.24 151.29 146.41 166.41 148.84 151.29 49.650 139.24 118.81 136.89 129.96 132.25 129.96 49.770 121.00 127.69 125.44 112.36 132.25 144.00 49.890 127.69 144.00 158.76 148.84 148.84 166.41 50.010 174.24 144.00 187.69 219.04 210.25 222.01 50.130 243.36 246.49 278.89 302.76 240.25 292.41 50.250 349.69 364.81 364.81 388.09 453.69 449.44 50.370 538.24 571.21 625.00 734.41 772.84 841.00 50.490 924.16 936.36 1004.89 1004.89 1024.00 979.69 50.610 1024.00 1036.84 967.21 1004.89 882.09 858.49 50.730 823.69 784.00 767.29 696.96 756.25 681.21 50.850 712.89 729.00 676.00 750.76 778.41 846.81 50.970 924.16 992.25 1011.24 1082.41 1115.56 1176.49 51.090 1211.04 1122.25 1149.21 1122.25 1115.56 1049.76 51.210 942.49 961.00 912.04 795.24 734.41 645.16 51.330 625.00 595.36 501.76 479.61 424.36 380.25 51.450 388.09 345.96 313.29 272.25 275.56 275.56 51.570 198.81 204.49 201.64 190.44 158.76 148.84 51.690 182.25 153.76 166.41 144.00 123.21 112.36 51.810 121.00 96.04 127.69 110.25 90.25 108.16 51.930 102.01 94.09 82.81 90.25 92.16 90.25 52.050 75.69 84.64 92.16 75.69 75.69 72.25 52.170 84.64 96.04 70.56 92.16 68.89 77.44 52.290 82.81 75.69 75.69 65.61 70.56 70.56 52.410 96.04 65.61 70.56 57.76 56.25 56.25 52.530 59.29 53.29 65.61 53.29 67.24 65.61 52.650 57.76 42.25 57.76 59.29 56.25 60.84 52.770 49.00 53.29 44.89 51.84 44.89 49.00 52.890 50.41 43.56 34.81 44.89 47.61 59.29 53.010 53.29 43.56 53.29 50.41 62.41 39.69 53.130 53.29 51.84 50.41 42.25 56.25 47.61 53.250 56.25 50.41 51.84 43.56 50.41 47.61 53.370 56.25 54.76 40.96 33.64 38.44 33.64 53.490 38.44 50.41 43.56 43.56 38.44 44.89 53.610 38.44 43.56 43.56 43.56 47.61 53.29 53.730 40.96 39.69 38.44 32.49 30.25 38.44 53.850 37.21 46.24 53.29 36.00 36.00 47.61 53.970 42.25 40.96 44.89 39.69 38.44 44.89 54.090 46.24 38.44 37.21 43.56 53.29 38.44 54.210 40.96 49.00 37.21 40.96 40.96 47.61 54.330 38.44 42.25 38.44 51.84 44.89 46.24 54.450 40.96 30.25 40.96 39.69 32.49 38.44 54.570 42.25 38.44 36.00 40.96 53.29 40.96 54.690 42.25 43.56 40.96 39.69 47.61 37.21 54.810 43.56 40.96 54.76 44.89 51.84 38.44 54.930 53.29 44.89 44.89 38.44 43.56 31.36 55.050 32.49 40.96 43.56 51.84 34.81 43.56 55.170 38.44 36.00 40.96 47.61 47.61 59.29

229

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 38.44 46.24 32.49 27.04 40.96 44.89 55.410 43.56 49.00 36.00 33.64 33.64 40.96 55.530 42.25 39.69 33.64 46.24 39.69 38.44 55.650 40.96 31.36 33.64 32.49 38.44 32.49 55.770 34.81 50.41 24.01 27.04 38.44 50.41 55.890 36.00 37.21 59.29 30.25 39.69 43.56 56.010 40.96 43.56 42.25 50.41 34.81 38.44 56.130 47.61 32.49 26.01 43.56 47.61 38.44 56.250 42.25 31.36 38.44 43.56 37.21 40.96 56.370 47.61 42.25 39.69 37.21 43.56 38.44 56.490 39.69 40.96 27.04 42.25 46.24 43.56 56.610 43.56 39.69 51.84 31.36 38.44 34.81 56.730 47.61 43.56 47.61 38.44 38.44 50.41 56.850 53.29 32.49 38.44 38.44 47.61 37.21 56.970 47.61 43.56 38.44 38.44 33.64 47.61 57.090 42.25 37.21 39.69 38.44 39.69 53.29 57.210 27.04 38.44 50.41 38.44 47.61 36.00 57.330 39.69 43.56 42.25 37.21 43.56 38.44 57.450 38.44 46.24 44.89 32.49 49.00 40.96 57.570 36.00 29.16 40.96 43.56 39.69 50.41 57.690 31.36 43.56 44.89 43.56 37.21 39.69 57.810 36.00 39.69 39.69 43.56 53.29 42.25 57.930 47.61 39.69 46.24 38.44 46.24 43.56 58.050 53.29 50.41 47.61 43.56 47.61 53.29 58.170 47.61 50.41 50.41 59.29 56.25 57.76 58.290 62.41 50.41 59.29 70.56 59.29 68.89 58.410 64.00 67.24 68.89 67.24 75.69 70.56 58.530 67.24 84.64 90.25 100.00 86.49 92.16 58.650 100.00 110.25 116.64 121.00 121.00 174.24 58.770 176.89 161.29 196.00 234.09 213.16 272.25 58.890 256.00 282.24 285.61 265.69 228.01 234.09 59.010 225.00 222.01 187.69 193.21 198.81 201.64 59.130 176.89 158.76 153.76 146.41 136.89 127.69 59.250 129.96 123.21 112.36 123.21 114.49 112.36 59.370 121.00 127.69 132.25 129.96 144.00 148.84 59.490 161.29 174.24 169.00 176.89 171.61 201.64 59.610 222.01 265.69 249.64 268.96 302.76 320.41 59.730 338.56 388.09 400.00 396.01 453.69 428.49 59.850 462.25 420.25 420.25 396.01 364.81 357.21 59.970 372.49 316.84 309.76 313.29 256.00 259.21 60.090 201.64 190.44 204.49 193.21 166.41 151.29 60.210 136.89 148.84 114.49 108.16 116.64 110.25 60.330 90.25 96.04 84.64 98.01 102.01 75.69 60.450 98.01 82.81 77.44 70.56 59.29 90.25 60.570 67.24 68.89 67.24 79.21 73.96 47.61 60.690 65.61 46.24 65.61 43.56 50.41 38.44 60.810 70.56 53.29 53.29 62.41 53.29 59.29 60.930 53.29 42.25 59.29 51.84 53.29 32.49 61.050 49.00 49.00 50.41 50.41 43.56 50.41 61.170 47.61 38.44 64.00 56.25 56.25 56.25 61.290 56.25 47.61 60.84 54.76 47.61 56.25 61.410 50.41 47.61 59.29 39.69 56.25 70.56

230

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 40.96 42.25 49.00 47.61 49.00 56.25 61.650 56.25 50.41 65.61 59.29 46.24 70.56 61.770 57.76 56.25 67.24 67.24 64.00 70.56 61.890 67.24 65.61 67.24 79.21 86.49 81.00 62.010 79.21 84.64 100.00 84.64 77.44 75.69 62.130 72.25 77.44 75.69 73.96 84.64 70.56 62.250 62.41 86.49 81.00 56.25 62.41 67.24 62.370 67.24 60.84 60.84 57.76 65.61 67.24 62.490 40.96 46.24 62.41 73.96 64.00 50.41 62.610 59.29 70.56 43.56 53.29 62.41 51.84 62.730 54.76 65.61 68.89 82.81 62.41 65.61 62.850 62.41 70.56 72.25 79.21 72.25 86.49 62.970 77.44 90.25 102.01 88.36 108.16 108.16 63.090 96.04 116.64 121.00 136.89 163.84 141.61 63.210 144.00 169.00 176.89 207.36 237.16 268.96 63.330 299.29 327.61 338.56 372.49 349.69 368.64 63.450 408.04 361.00 368.64 388.09 349.69 327.61 63.570 345.96 324.00 309.76 240.25 275.56 285.61 63.690 243.36 187.69 184.96 182.25 163.84 148.84 63.810 144.00 153.76 148.84 129.96 118.81 121.00 63.930 114.49 106.09 106.09 108.16 100.00 112.36 64.050 114.49 98.01 98.01 96.04 123.21 129.96 64.170 104.04 108.16 112.36 129.96 129.96 121.00 64.290 144.00 144.00 153.76 161.29 169.00 182.25 64.410 190.44 193.21 231.04 213.16 222.01 231.04 64.530 240.25 246.49 249.64 225.00 219.04 196.00 64.650 222.01 184.96 198.81 198.81 190.44 193.21 64.770 190.44 169.00 163.84 158.76 144.00 156.25 64.890 161.29 163.84 171.61 169.00 163.84 174.24 65.010 171.61 169.00 222.01 196.00 213.16 219.04 65.130 252.81 213.16 225.00 234.09 225.00 246.49 65.250 207.36 204.49 216.09 182.25 184.96 166.41 65.370 179.56 158.76 174.24 148.84 134.56 127.69 65.490 134.56 123.21 121.00 118.81 114.49 102.01 65.610 121.00 118.81 118.81 102.01 114.49 104.04 65.730 100.00 104.04 108.16 104.04 94.09 121.00 65.850 125.44 121.00 116.64 102.01 134.56 139.24 65.970 153.76 144.00 151.29 141.61 153.76 144.00 66.090 176.89 141.61 153.76 158.76 153.76 148.84 66.210 134.56 146.41 102.01 118.81 136.89 108.16 66.330 129.96 136.89 112.36 110.25 110.25 108.16 66.450 81.00 92.16 86.49 90.25 84.64 84.64 66.570 86.49 82.81 81.00 72.25 98.01 92.16 66.690 92.16 84.64 75.69 77.44 77.44 94.09 66.810 88.36 98.01 90.25 116.64 102.01 96.04 66.930 102.01 98.01 94.09 116.64 129.96 136.89 67.050 114.49 148.84 153.76 169.00 156.25 176.89 67.170 182.25 216.09 234.09 246.49 285.61 292.41 67.290 282.24 295.84 380.25 408.04 392.04 392.04 67.410 372.49 376.36 353.44 404.01 313.29 334.89 67.530 364.81 316.84 313.29 306.25 299.29 262.44 67.650 278.89 246.49 213.16 204.49 207.36 176.89

231

File: JC12.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 176.89 158.76 153.76 141.61 127.69 100.00 67.890 112.36 132.25 84.64 121.00 98.01 77.44 68.010 79.21 100.00 70.56 86.49 88.36 104.04 68.130 96.04 77.44 94.09 75.69 86.49 79.21 68.250 81.00 79.21 79.21 79.21 84.64 79.21 68.370 59.29 56.25 50.41 75.69 62.41 59.29 68.490 60.84 56.25 50.41 51.84 39.69 56.25 68.610 46.24 47.61 47.61 50.41 54.76 44.89 68.730 51.84 47.61 50.41 56.25 50.41 65.61 68.850 44.89 50.41 46.24 50.41 47.61 54.76 68.970 50.41 38.44 43.56 47.61 53.29 43.56 69.090 49.00 51.84 50.41 44.89 50.41 56.25 69.210 59.29 47.61 56.25 53.29 62.41 64.00 69.330 56.25 57.76 53.29 56.25 54.76 46.24 69.450 47.61 49.00 53.29 54.76 62.41 53.29 69.570 47.61 51.84 59.29 50.41 60.84 57.76 69.690 60.84 50.41 47.61 59.29 65.61 62.41 69.810 72.25 65.61 75.69 57.76 65.61 70.56 69.930 68.89 75.69 72.25 86.49 _

232

File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC13 Data measured at: 25-Jan-2011 13:53:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 10281.96 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 129.96 121.00 116.64 127.69 136.89 100.00 2.130 106.09 100.00 94.09 88.36 110.25 106.09 2.250 102.01 88.36 110.25 94.09 98.01 102.01 2.370 75.69 84.64 94.09 75.69 79.21 77.44 2.490 77.44 77.44 77.44 79.21 79.21 77.44 2.610 70.56 70.56 50.41 81.00 82.81 64.00 2.730 72.25 77.44 65.61 57.76 65.61 59.29 2.850 67.24 65.61 72.25 75.69 65.61 68.89 2.970 59.29 75.69 81.00 57.76 59.29 50.41 3.090 73.96 67.24 62.41 77.44 54.76 64.00 3.210 62.41 43.56 67.24 67.24 60.84 70.56 3.330 56.25 53.29 65.61 57.76 59.29 42.25 3.450 64.00 56.25 59.29 62.41 54.76 53.29 3.570 57.76 60.84 50.41 65.61 50.41 50.41 3.690 43.56 54.76 50.41 49.00 56.25 65.61 3.810 70.56 47.61 53.29 50.41 60.84 57.76 3.930 70.56 46.24 70.56 46.24 56.25 70.56 4.050 56.25 38.44 50.41 59.29 57.76 50.41 4.170 44.89 65.61 60.84 65.61 62.41 56.25 4.290 50.41 60.84 56.25 39.69 57.76 64.00 4.410 82.81 56.25 53.29 65.61 53.29 47.61 4.530 50.41 40.96 56.25 43.56 62.41 60.84 4.650 50.41 57.76 70.56 51.84 56.25 62.41 4.770 68.89 59.29 70.56 62.41 65.61 51.84 4.890 47.61 49.00 60.84 62.41 57.76 51.84 5.010 65.61 59.29 60.84 38.44 51.84 54.76 5.130 67.24 50.41 56.25 56.25 42.25 54.76 5.250 60.84 53.29 56.25 54.76 47.61 56.25

233

File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 56.25 75.69 67.24 47.61 51.84 67.24 5.490 47.61 59.29 56.25 59.29 67.24 53.29 5.610 62.41 53.29 60.84 64.00 68.89 56.25 5.730 53.29 53.29 53.29 50.41 56.25 44.89 5.850 56.25 65.61 65.61 57.76 50.41 54.76 5.970 56.25 50.41 57.76 62.41 50.41 49.00 6.090 53.29 77.44 67.24 57.76 60.84 53.29 6.210 59.29 64.00 46.24 47.61 47.61 46.24 6.330 53.29 51.84 62.41 60.84 57.76 62.41 6.450 51.84 44.89 54.76 43.56 53.29 53.29 6.570 46.24 53.29 50.41 47.61 54.76 53.29 6.690 65.61 53.29 50.41 59.29 49.00 43.56 6.810 65.61 68.89 59.29 56.25 46.24 62.41 6.930 51.84 38.44 47.61 38.44 59.29 51.84 7.050 49.00 47.61 49.00 57.76 43.56 44.89 7.170 59.29 46.24 65.61 53.29 50.41 56.25 7.290 47.61 44.89 49.00 50.41 62.41 57.76 7.410 50.41 47.61 54.76 47.61 44.89 59.29 7.530 44.89 53.29 53.29 57.76 59.29 53.29 7.650 50.41 38.44 57.76 43.56 53.29 54.76 7.770 43.56 43.56 53.29 49.00 43.56 47.61 7.890 54.76 62.41 47.61 47.61 40.96 50.41 8.010 40.96 50.41 42.25 43.56 56.25 51.84 8.130 54.76 49.00 53.29 43.56 46.24 42.25 8.250 38.44 47.61 53.29 59.29 56.25 60.84 8.370 40.96 60.84 47.61 47.61 62.41 53.29 8.490 43.56 51.84 50.41 53.29 53.29 59.29 8.610 44.89 49.00 46.24 50.41 47.61 39.69 8.730 38.44 43.56 56.25 50.41 43.56 40.96 8.850 51.84 47.61 40.96 51.84 50.41 54.76 8.970 51.84 47.61 46.24 59.29 53.29 44.89 9.090 42.25 59.29 37.21 38.44 59.29 46.24 9.210 57.76 53.29 43.56 46.24 42.25 40.96 9.330 62.41 47.61 44.89 47.61 59.29 59.29 9.450 33.64 47.61 50.41 46.24 51.84 42.25 9.570 56.25 36.00 53.29 47.61 49.00 59.29 9.690 37.21 53.29 33.64 46.24 37.21 37.21 9.810 59.29 31.36 53.29 49.00 49.00 53.29 9.930 49.00 53.29 43.56 43.56 40.96 46.24 10.050 43.56 32.49 43.56 50.41 51.84 43.56 10.170 51.84 49.00 38.44 44.89 44.89 43.56 10.290 56.25 47.61 53.29 36.00 57.76 59.29 10.410 51.84 44.89 47.61 47.61 40.96 32.49 10.530 33.64 50.41 43.56 57.76 47.61 47.61 10.650 47.61 44.89 36.00 44.89 47.61 50.41 10.770 44.89 59.29 50.41 40.96 38.44 53.29 10.890 54.76 43.56 51.84 53.29 44.89 50.41 11.010 39.69 42.25 39.69 46.24 33.64 44.89 11.130 40.96 43.56 34.81 34.81 47.61 32.49 11.250 33.64 50.41 40.96 46.24 43.56 50.41 11.370 50.41 54.76 47.61 56.25 50.41 42.25 11.490 38.44 56.25 34.81 38.44 53.29 39.69

234

File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 46.24 39.69 47.61 44.89 62.41 50.41 11.730 49.00 46.24 31.36 50.41 43.56 34.81 11.850 47.61 33.64 43.56 43.56 36.00 53.29 11.970 43.56 47.61 50.41 44.89 46.24 34.81 12.090 50.41 51.84 49.00 44.89 43.56 50.41 12.210 43.56 43.56 32.49 40.96 43.56 30.25 12.330 39.69 37.21 47.61 43.56 43.56 47.61 12.450 33.64 36.00 40.96 37.21 43.56 43.56 12.570 44.89 60.84 59.29 38.44 44.89 37.21 12.690 38.44 53.29 49.00 44.89 44.89 47.61 12.810 40.96 38.44 46.24 43.56 47.61 44.89 12.930 46.24 32.49 43.56 44.89 47.61 49.00 13.050 36.00 59.29 36.00 38.44 42.25 53.29 13.170 44.89 31.36 42.25 36.00 33.64 51.84 13.290 49.00 46.24 43.56 37.21 32.49 37.21 13.410 50.41 37.21 46.24 42.25 43.56 47.61 13.530 40.96 49.00 39.69 50.41 50.41 26.01 13.650 37.21 31.36 47.61 38.44 43.56 40.96 13.770 27.04 53.29 47.61 36.00 49.00 43.56 13.890 43.56 37.21 40.96 40.96 28.09 57.76 14.010 47.61 37.21 43.56 29.16 38.44 31.36 14.130 47.61 43.56 37.21 37.21 43.56 29.16 14.250 47.61 40.96 31.36 47.61 30.25 43.56 14.370 32.49 39.69 40.96 30.25 28.09 42.25 14.490 34.81 43.56 50.41 38.44 46.24 28.09 14.610 42.25 34.81 46.24 43.56 40.96 44.89 14.730 37.21 50.41 47.61 44.89 47.61 47.61 14.850 50.41 38.44 43.56 32.49 39.69 50.41 14.970 50.41 34.81 30.25 37.21 47.61 40.96 15.090 47.61 38.44 46.24 43.56 47.61 54.76 15.210 47.61 39.69 50.41 50.41 47.61 47.61 15.330 39.69 53.29 59.29 59.29 53.29 50.41 15.450 50.41 50.41 47.61 44.89 68.89 65.61 15.570 56.25 57.76 65.61 56.25 54.76 50.41 15.690 59.29 59.29 47.61 53.29 62.41 62.41 15.810 54.76 53.29 62.41 60.84 62.41 53.29 15.930 53.29 47.61 46.24 53.29 51.84 68.89 16.050 68.89 50.41 62.41 62.41 57.76 49.00 16.170 59.29 42.25 50.41 42.25 46.24 54.76 16.290 43.56 46.24 54.76 44.89 43.56 53.29 16.410 51.84 43.56 54.76 44.89 39.69 65.61 16.530 47.61 51.84 62.41 50.41 43.56 40.96 16.650 56.25 50.41 47.61 47.61 38.44 56.25 16.770 53.29 56.25 46.24 42.25 47.61 51.84 16.890 50.41 50.41 50.41 44.89 47.61 43.56 17.010 54.76 37.21 46.24 54.76 46.24 42.25 17.130 38.44 50.41 36.00 37.21 40.96 38.44 17.250 42.25 40.96 40.96 46.24 43.56 29.16 17.370 44.89 40.96 53.29 40.96 43.56 50.41 17.490 32.49 30.25 36.00 38.44 43.56 44.89 17.610 40.96 42.25 39.69 43.56 36.00 53.29 17.730 43.56 40.96 38.44 30.25 36.00 42.25

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 49.00 44.89 32.49 28.09 32.49 39.69 17.970 43.56 27.04 36.00 37.21 49.00 38.44 18.090 38.44 39.69 33.64 47.61 32.49 37.21 18.210 43.56 43.56 38.44 36.00 38.44 47.61 18.330 39.69 32.49 36.00 49.00 43.56 39.69 18.450 43.56 38.44 38.44 40.96 44.89 39.69 18.570 49.00 38.44 40.96 28.09 46.24 42.25 18.690 51.84 38.44 37.21 34.81 38.44 43.56 18.810 43.56 43.56 49.00 39.69 38.44 42.25 18.930 47.61 39.69 50.41 47.61 56.25 40.96 19.050 43.56 38.44 47.61 39.69 44.89 42.25 19.170 54.76 47.61 43.56 38.44 43.56 40.96 19.290 40.96 49.00 42.25 56.25 43.56 36.00 19.410 43.56 46.24 46.24 39.69 54.76 42.25 19.530 42.25 43.56 38.44 42.25 40.96 43.56 19.650 30.25 50.41 38.44 36.00 32.49 42.25 19.770 44.89 43.56 38.44 43.56 38.44 38.44 19.890 56.25 49.00 50.41 60.84 38.44 51.84 20.010 38.44 49.00 43.56 32.49 31.36 38.44 20.130 32.49 42.25 59.29 32.49 56.25 39.69 20.250 34.81 43.56 40.96 43.56 33.64 44.89 20.370 37.21 33.64 34.81 26.01 42.25 30.25 20.490 40.96 39.69 37.21 43.56 50.41 42.25 20.610 46.24 51.84 33.64 42.25 56.25 46.24 20.730 54.76 62.41 67.24 68.89 75.69 82.81 20.850 72.25 50.41 60.84 50.41 39.69 51.84 20.970 54.76 46.24 37.21 42.25 47.61 44.89 21.090 37.21 24.01 49.00 36.00 38.44 43.56 21.210 43.56 43.56 37.21 46.24 36.00 56.25 21.330 59.29 40.96 40.96 49.00 40.96 32.49 21.450 44.89 47.61 40.96 46.24 37.21 46.24 21.570 34.81 34.81 43.56 47.61 47.61 47.61 21.690 40.96 38.44 44.89 53.29 62.41 53.29 21.810 47.61 56.25 77.44 54.76 59.29 94.09 21.930 82.81 96.04 98.01 104.04 144.00 116.64 22.050 94.09 112.36 67.24 67.24 73.96 57.76 22.170 57.76 50.41 44.89 44.89 34.81 50.41 22.290 40.96 47.61 38.44 46.24 47.61 50.41 22.410 46.24 43.56 47.61 44.89 42.25 54.76 22.530 33.64 38.44 42.25 36.00 53.29 37.21 22.650 39.69 38.44 56.25 34.81 28.09 51.84 22.770 43.56 57.76 37.21 42.25 40.96 42.25 22.890 51.84 43.56 38.44 31.36 47.61 39.69 23.010 36.00 43.56 43.56 32.49 37.21 40.96 23.130 46.24 30.25 29.16 33.64 38.44 37.21 23.250 50.41 37.21 53.29 46.24 42.25 36.00 23.370 38.44 29.16 31.36 32.49 38.44 43.56 23.490 40.96 43.56 29.16 40.96 42.25 50.41 23.610 54.76 47.61 60.84 39.69 43.56 53.29 23.730 64.00 50.41 62.41 68.89 62.41 75.69 23.850 82.81 92.16 88.36 129.96 121.00 121.00 23.970 166.41 176.89 216.09 213.16 198.81 196.00

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File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 193.21 169.00 158.76 123.21 104.04 100.00 24.210 79.21 81.00 62.41 65.61 60.84 56.25 24.330 59.29 60.84 53.29 56.25 56.25 43.56 24.450 38.44 44.89 43.56 49.00 47.61 38.44 24.570 32.49 43.56 46.24 40.96 44.89 43.56 24.690 43.56 40.96 42.25 32.49 43.56 38.44 24.810 32.49 39.69 47.61 34.81 29.16 36.00 24.930 43.56 43.56 46.24 38.44 31.36 37.21 25.050 38.44 43.56 25.00 27.04 33.64 47.61 25.170 39.69 40.96 34.81 36.00 36.00 42.25 25.290 44.89 43.56 43.56 32.49 49.00 38.44 25.410 44.89 38.44 38.44 38.44 43.56 32.49 25.530 44.89 43.56 39.69 32.49 44.89 33.64 25.650 30.25 33.64 39.69 43.56 43.56 28.09 25.770 40.96 40.96 37.21 54.76 43.56 42.25 25.890 32.49 49.00 47.61 46.24 38.44 39.69 26.010 39.69 42.25 38.44 40.96 38.44 32.49 26.130 44.89 39.69 33.64 53.29 32.49 42.25 26.250 43.56 44.89 43.56 47.61 38.44 47.61 26.370 60.84 42.25 38.44 49.00 59.29 49.00 26.490 67.24 65.61 82.81 88.36 110.25 132.25 26.610 146.41 136.89 123.21 110.25 108.16 86.49 26.730 79.21 57.76 38.44 56.25 51.84 65.61 26.850 29.16 42.25 28.09 40.96 34.81 37.21 26.970 34.81 40.96 38.44 40.96 39.69 38.44 27.090 44.89 38.44 37.21 29.16 49.00 46.24 27.210 37.21 37.21 40.96 30.25 42.25 38.44 27.330 40.96 34.81 36.00 42.25 30.25 27.04 27.450 33.64 30.25 50.41 34.81 39.69 34.81 27.570 34.81 49.00 38.44 33.64 29.16 37.21 27.690 36.00 43.56 37.21 38.44 34.81 23.04 27.810 42.25 37.21 31.36 39.69 40.96 47.61 27.930 34.81 33.64 42.25 37.21 36.00 43.56 28.050 32.49 37.21 37.21 50.41 38.44 32.49 28.170 39.69 36.00 37.21 31.36 39.69 38.44 28.290 29.16 34.81 30.25 44.89 42.25 43.56 28.410 32.49 32.49 39.69 40.96 43.56 44.89 28.530 40.96 44.89 42.25 34.81 40.96 38.44 28.650 40.96 37.21 43.56 47.61 47.61 42.25 28.770 38.44 44.89 53.29 30.25 47.61 28.09 28.890 43.56 46.24 49.00 38.44 39.69 39.69 29.010 43.56 43.56 40.96 38.44 49.00 56.25 29.130 38.44 59.29 56.25 53.29 47.61 53.29 29.250 47.61 53.29 72.25 59.29 59.29 75.69 29.370 64.00 73.96 59.29 84.64 70.56 72.25 29.490 43.56 67.24 64.00 62.41 47.61 62.41 29.610 56.25 75.69 62.41 47.61 68.89 65.61 29.730 65.61 70.56 75.69 62.41 62.41 75.69 29.850 65.61 67.24 65.61 94.09 56.25 77.44 29.970 86.49 81.00 96.04 104.04 82.81 94.09 30.090 104.04 92.16 108.16 106.09 114.49 102.01 30.210 127.69 127.69 139.24 163.84 151.29 161.29

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 163.84 174.24 207.36 243.36 246.49 262.44 30.450 272.25 353.44 345.96 384.16 408.04 488.41 30.570 533.61 610.09 655.36 772.84 876.16 954.81 30.690 1225.00 1421.29 1713.96 2043.04 2450.25 3102.49 30.810 3868.84 4970.25 6241.00 7551.61 8742.25 10140.49 30.930 10261.69 10281.96 9447.84 8353.96 7191.04 6021.76 31.050 4830.25 3684.49 2819.61 2227.84 1857.61 1459.24 31.170 1288.81 1011.24 882.09 756.25 670.81 571.21 31.290 492.84 488.41 412.09 338.56 324.00 285.61 31.410 275.56 249.64 222.01 207.36 210.25 184.96 31.530 182.25 158.76 144.00 146.41 141.61 144.00 31.650 129.96 148.84 114.49 139.24 121.00 102.01 31.770 94.09 104.04 110.25 98.01 75.69 75.69 31.890 96.04 92.16 77.44 73.96 86.49 88.36 32.010 65.61 81.00 79.21 79.21 65.61 62.41 32.130 67.24 67.24 70.56 90.25 62.41 60.84 32.250 59.29 59.29 65.61 64.00 59.29 53.29 32.370 62.41 47.61 73.96 57.76 62.41 53.29 32.490 53.29 56.25 59.29 59.29 59.29 54.76 32.610 56.25 60.84 50.41 49.00 51.84 51.84 32.730 49.00 49.00 42.25 43.56 56.25 43.56 32.850 50.41 53.29 43.56 50.41 44.89 60.84 32.970 53.29 64.00 39.69 62.41 56.25 65.61 33.090 62.41 57.76 70.56 60.84 59.29 79.21 33.210 84.64 90.25 104.04 92.16 112.36 129.96 33.330 116.64 139.24 144.00 176.89 222.01 231.04 33.450 282.24 331.24 349.69 376.36 372.49 342.25 33.570 334.89 316.84 278.89 262.44 193.21 198.81 33.690 176.89 121.00 96.04 116.64 92.16 84.64 33.810 79.21 65.61 72.25 75.69 82.81 56.25 33.930 77.44 59.29 68.89 50.41 43.56 51.84 34.050 44.89 50.41 53.29 46.24 38.44 50.41 34.170 42.25 56.25 56.25 64.00 37.21 51.84 34.290 44.89 46.24 53.29 53.29 37.21 46.24 34.410 33.64 46.24 38.44 37.21 37.21 47.61 34.530 53.29 49.00 40.96 39.69 47.61 42.25 34.650 37.21 46.24 53.29 53.29 54.76 53.29 34.770 43.56 56.25 42.25 51.84 50.41 65.61 34.890 68.89 62.41 82.81 72.25 64.00 51.84 35.010 77.44 100.00 84.64 106.09 110.25 125.44 35.130 136.89 158.76 166.41 198.81 196.00 234.09 35.250 265.69 313.29 295.84 306.25 272.25 246.49 35.370 249.64 231.04 237.16 207.36 169.00 125.44 35.490 132.25 123.21 102.01 112.36 90.25 64.00 35.610 65.61 67.24 64.00 60.84 50.41 64.00 35.730 54.76 59.29 59.29 62.41 50.41 53.29 35.850 49.00 49.00 42.25 44.89 50.41 59.29 35.970 59.29 49.00 38.44 42.25 51.84 54.76 36.090 43.56 53.29 54.76 32.49 44.89 49.00 36.210 57.76 43.56 32.49 37.21 38.44 33.64 36.330 47.61 46.24 53.29 65.61 43.56 57.76 36.450 62.41 47.61 57.76 72.25 79.21 62.41

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File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 64.00 70.56 73.96 59.29 65.61 73.96 36.690 67.24 60.84 65.61 72.25 79.21 72.25 36.810 77.44 77.44 84.64 96.04 100.00 108.16 36.930 125.44 121.00 121.00 127.69 118.81 129.96 37.050 153.76 171.61 163.84 148.84 151.29 184.96 37.170 210.25 193.21 237.16 278.89 313.29 368.64 37.290 372.49 466.56 475.24 519.84 501.76 466.56 37.410 436.81 408.04 349.69 361.00 278.89 268.96 37.530 210.25 184.96 141.61 148.84 129.96 125.44 37.650 94.09 96.04 94.09 84.64 86.49 88.36 37.770 86.49 72.25 59.29 64.00 67.24 68.89 37.890 43.56 56.25 73.96 49.00 50.41 50.41 38.010 56.25 44.89 40.96 32.49 56.25 51.84 38.130 75.69 50.41 49.00 56.25 50.41 56.25 38.250 42.25 40.96 47.61 51.84 53.29 51.84 38.370 43.56 42.25 53.29 56.25 56.25 47.61 38.490 39.69 50.41 56.25 59.29 42.25 62.41 38.610 46.24 50.41 59.29 50.41 46.24 62.41 38.730 49.00 50.41 53.29 46.24 50.41 53.29 38.850 49.00 34.81 50.41 40.96 38.44 43.56 38.970 56.25 47.61 44.89 44.89 60.84 62.41 39.090 50.41 60.84 60.84 53.29 56.25 53.29 39.210 51.84 49.00 43.56 32.49 44.89 56.25 39.330 54.76 53.29 62.41 72.25 70.56 77.44 39.450 72.25 96.04 56.25 77.44 67.24 84.64 39.570 82.81 75.69 79.21 84.64 96.04 102.01 39.690 102.01 98.01 112.36 96.04 116.64 100.00 39.810 125.44 118.81 136.89 112.36 123.21 114.49 39.930 139.24 112.36 127.69 108.16 153.76 98.01 40.050 118.81 100.00 98.01 96.04 82.81 82.81 40.170 70.56 92.16 67.24 72.25 81.00 67.24 40.290 59.29 70.56 75.69 79.21 56.25 62.41 40.410 64.00 62.41 82.81 79.21 65.61 84.64 40.530 90.25 96.04 96.04 104.04 129.96 134.56 40.650 141.61 125.44 156.25 153.76 169.00 176.89 40.770 193.21 222.01 246.49 252.81 313.29 309.76 40.890 400.00 416.16 510.76 600.25 630.01 817.96 41.010 841.00 1056.25 1075.84 1267.36 1369.00 1383.84 41.130 1369.00 1354.24 1253.16 1102.24 1135.69 1017.61 41.250 852.64 745.29 681.21 561.69 470.89 408.04 41.370 353.44 331.24 306.25 265.69 256.00 216.09 41.490 196.00 158.76 144.00 151.29 136.89 148.84 41.610 110.25 118.81 108.16 108.16 92.16 98.01 41.730 108.16 92.16 79.21 84.64 67.24 84.64 41.850 75.69 60.84 62.41 79.21 53.29 59.29 41.970 60.84 46.24 53.29 62.41 56.25 56.25 42.090 59.29 56.25 50.41 59.29 56.25 62.41 42.210 62.41 53.29 49.00 42.25 44.89 44.89 42.330 54.76 57.76 59.29 64.00 67.24 56.25 42.450 62.41 53.29 51.84 49.00 53.29 59.29 42.570 50.41 60.84 44.89 43.56 36.00 44.89 42.690 53.29 38.44 32.49 37.21 47.61 56.25

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File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 56.25 47.61 38.44 57.76 51.84 47.61 42.930 42.25 53.29 56.25 49.00 56.25 49.00 43.050 62.41 46.24 59.29 56.25 65.61 50.41 43.170 49.00 75.69 59.29 68.89 57.76 68.89 43.290 67.24 70.56 60.84 72.25 81.00 65.61 43.410 60.84 64.00 60.84 72.25 67.24 65.61 43.530 88.36 104.04 92.16 100.00 108.16 141.61 43.650 146.41 144.00 166.41 190.44 210.25 237.16 43.770 231.04 246.49 207.36 213.16 184.96 166.41 43.890 174.24 156.25 158.76 153.76 136.89 98.01 44.010 118.81 92.16 90.25 96.04 96.04 88.36 44.130 68.89 84.64 75.69 70.56 70.56 84.64 44.250 81.00 67.24 62.41 65.61 79.21 81.00 44.370 81.00 92.16 102.01 90.25 90.25 104.04 44.490 110.25 121.00 129.96 114.49 125.44 132.25 44.610 156.25 166.41 187.69 210.25 252.81 275.56 44.730 295.84 376.36 388.09 492.84 497.29 665.64 44.850 784.00 806.56 852.64 906.01 829.44 806.56 44.970 739.84 691.69 665.64 561.69 510.76 462.25 45.090 441.00 376.36 306.25 299.29 262.44 231.04 45.210 187.69 179.56 182.25 163.84 161.29 134.56 45.330 116.64 129.96 102.01 92.16 94.09 106.09 45.450 67.24 82.81 68.89 75.69 79.21 65.61 45.570 65.61 77.44 67.24 67.24 64.00 65.61 45.690 68.89 68.89 73.96 70.56 82.81 59.29 45.810 68.89 72.25 62.41 60.84 40.96 60.84 45.930 56.25 72.25 62.41 53.29 60.84 59.29 46.050 53.29 67.24 65.61 39.69 60.84 59.29 46.170 56.25 53.29 50.41 70.56 64.00 65.61 46.290 56.25 65.61 59.29 59.29 62.41 65.61 46.410 75.69 65.61 53.29 67.24 59.29 62.41 46.530 57.76 53.29 64.00 68.89 60.84 62.41 46.650 64.00 70.56 77.44 70.56 79.21 47.61 46.770 70.56 57.76 70.56 77.44 51.84 51.84 46.890 62.41 54.76 47.61 54.76 56.25 49.00 47.010 56.25 53.29 44.89 31.36 60.84 56.25 47.130 46.24 39.69 44.89 57.76 40.96 39.69 47.250 49.00 43.56 42.25 49.00 46.24 46.24 47.370 42.25 53.29 43.56 50.41 50.41 44.89 47.490 50.41 42.25 44.89 47.61 46.24 50.41 47.610 57.76 53.29 49.00 38.44 43.56 56.25 47.730 40.96 44.89 56.25 53.29 46.24 42.25 47.850 37.21 37.21 47.61 39.69 51.84 50.41 47.970 59.29 44.89 46.24 43.56 50.41 53.29 48.090 53.29 47.61 54.76 44.89 62.41 62.41 48.210 59.29 57.76 56.25 59.29 56.25 47.61 48.330 62.41 59.29 67.24 49.00 51.84 67.24 48.450 54.76 62.41 67.24 38.44 62.41 62.41 48.570 57.76 62.41 67.24 56.25 65.61 72.25 48.690 62.41 53.29 73.96 73.96 75.69 65.61 48.810 70.56 84.64 94.09 75.69 82.81 88.36 48.930 94.09 112.36 118.81 116.64 106.09 144.00

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File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 139.24 148.84 169.00 163.84 171.61 201.64 49.170 190.44 213.16 213.16 237.16 278.89 240.25 49.290 265.69 193.21 207.36 201.64 210.25 210.25 49.410 163.84 171.61 166.41 139.24 151.29 156.25 49.530 134.56 118.81 129.96 112.36 125.44 100.00 49.650 108.16 102.01 116.64 134.56 110.25 106.09 49.770 132.25 132.25 132.25 106.09 134.56 144.00 49.890 129.96 156.25 151.29 153.76 176.89 166.41 50.010 219.04 196.00 249.64 249.64 256.00 246.49 50.130 256.00 299.29 295.84 327.61 364.81 342.25 50.250 416.16 404.01 432.64 510.76 538.24 630.01 50.370 702.25 739.84 829.44 961.00 1017.61 1089.00 50.490 1156.00 1149.21 1169.64 1169.64 1169.64 1056.25 50.610 942.49 973.44 992.25 936.36 858.49 829.44 50.730 767.29 745.29 707.56 712.89 645.16 739.84 50.850 696.96 767.29 829.44 961.00 948.64 1056.25 50.970 1162.81 1260.25 1296.00 1303.21 1267.36 1253.16 51.090 1274.49 1211.04 1135.69 1122.25 1036.84 998.56 51.210 918.09 823.69 729.00 691.69 630.01 600.25 51.330 484.00 475.24 380.25 400.00 357.21 372.49 51.450 324.00 262.44 268.96 225.00 198.81 193.21 51.570 184.96 166.41 174.24 129.96 153.76 139.24 51.690 139.24 121.00 136.89 114.49 118.81 112.36 51.810 96.04 102.01 96.04 114.49 86.49 98.01 51.930 88.36 98.01 86.49 75.69 88.36 81.00 52.050 60.84 72.25 75.69 72.25 77.44 64.00 52.170 65.61 75.69 84.64 84.64 72.25 86.49 52.290 72.25 73.96 60.84 86.49 94.09 75.69 52.410 67.24 90.25 70.56 57.76 77.44 60.84 52.530 67.24 60.84 60.84 70.56 50.41 46.24 52.650 57.76 44.89 38.44 56.25 42.25 60.84 52.770 62.41 43.56 50.41 46.24 39.69 53.29 52.890 49.00 42.25 44.89 57.76 49.00 53.29 53.010 43.56 39.69 43.56 46.24 34.81 44.89 53.130 46.24 50.41 51.84 47.61 40.96 36.00 53.250 46.24 51.84 49.00 32.49 50.41 47.61 53.370 42.25 49.00 31.36 47.61 46.24 43.56 53.490 38.44 49.00 50.41 43.56 42.25 38.44 53.610 50.41 49.00 37.21 30.25 43.56 38.44 53.730 43.56 42.25 51.84 53.29 42.25 36.00 53.850 43.56 50.41 33.64 40.96 34.81 32.49 53.970 38.44 32.49 46.24 33.64 43.56 43.56 54.090 50.41 49.00 36.00 39.69 40.96 36.00 54.210 44.89 38.44 49.00 33.64 34.81 36.00 54.330 32.49 33.64 47.61 38.44 38.44 32.49 54.450 36.00 40.96 33.64 28.09 38.44 36.00 54.570 47.61 30.25 38.44 46.24 38.44 47.61 54.690 40.96 38.44 37.21 43.56 34.81 38.44 54.810 38.44 60.84 44.89 39.69 39.69 40.96 54.930 32.49 42.25 42.25 46.24 53.29 42.25 55.050 44.89 43.56 38.44 47.61 32.49 33.64 55.170 40.96 43.56 38.44 39.69 36.00 38.44

241

File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 30.25 44.89 49.00 49.00 46.24 36.00 55.410 40.96 36.00 33.64 38.44 33.64 37.21 55.530 34.81 42.25 31.36 43.56 40.96 32.49 55.650 46.24 54.76 37.21 30.25 33.64 40.96 55.770 32.49 29.16 40.96 40.96 34.81 36.00 55.890 34.81 32.49 38.44 28.09 38.44 38.44 56.010 42.25 46.24 34.81 43.56 53.29 33.64 56.130 38.44 38.44 38.44 28.09 37.21 46.24 56.250 40.96 39.69 39.69 22.09 34.81 40.96 56.370 42.25 38.44 47.61 39.69 29.16 40.96 56.490 39.69 32.49 29.16 39.69 49.00 44.89 56.610 38.44 38.44 46.24 38.44 40.96 33.64 56.730 34.81 43.56 43.56 43.56 32.49 33.64 56.850 33.64 43.56 34.81 39.69 51.84 30.25 56.970 38.44 30.25 30.25 49.00 44.89 38.44 57.090 43.56 29.16 36.00 32.49 36.00 37.21 57.210 32.49 47.61 43.56 34.81 42.25 46.24 57.330 29.16 43.56 39.69 38.44 38.44 47.61 57.450 40.96 46.24 32.49 39.69 56.25 50.41 57.570 49.00 38.44 39.69 44.89 30.25 31.36 57.690 39.69 36.00 40.96 42.25 47.61 47.61 57.810 53.29 44.89 43.56 42.25 43.56 38.44 57.930 43.56 40.96 51.84 54.76 53.29 43.56 58.050 32.49 53.29 43.56 56.25 39.69 44.89 58.170 53.29 57.76 56.25 56.25 60.84 47.61 58.290 54.76 50.41 57.76 62.41 51.84 57.76 58.410 59.29 77.44 57.76 70.56 79.21 75.69 58.530 70.56 72.25 96.04 102.01 104.04 116.64 58.650 104.04 136.89 116.64 148.84 171.61 179.56 58.770 166.41 207.36 225.00 275.56 252.81 256.00 58.890 210.25 204.49 213.16 169.00 204.49 176.89 59.010 204.49 179.56 174.24 174.24 151.29 121.00 59.130 144.00 132.25 118.81 127.69 110.25 114.49 59.250 129.96 114.49 112.36 102.01 123.21 100.00 59.370 136.89 129.96 153.76 129.96 153.76 139.24 59.490 176.89 169.00 158.76 207.36 198.81 228.01 59.610 228.01 259.21 282.24 327.61 349.69 384.16 59.730 462.25 428.49 492.84 449.44 432.64 412.09 59.850 408.04 380.25 396.01 368.64 345.96 364.81 59.970 331.24 289.00 259.21 234.09 246.49 216.09 60.090 166.41 182.25 146.41 153.76 129.96 112.36 60.210 114.49 98.01 114.49 104.04 79.21 102.01 60.330 86.49 75.69 86.49 77.44 75.69 82.81 60.450 57.76 62.41 72.25 50.41 60.84 65.61 60.570 67.24 65.61 54.76 70.56 53.29 65.61 60.690 46.24 57.76 53.29 50.41 57.76 49.00 60.810 57.76 59.29 53.29 40.96 47.61 46.24 60.930 59.29 42.25 60.84 56.25 50.41 53.29 61.050 42.25 47.61 36.00 50.41 47.61 40.96 61.170 37.21 43.56 40.96 40.96 62.41 54.76 61.290 50.41 51.84 47.61 42.25 53.29 53.29 61.410 64.00 60.84 50.41 43.56 54.76 62.41

242

File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 32.49 50.41 50.41 59.29 47.61 54.76 61.650 73.96 62.41 75.69 59.29 67.24 59.29 61.770 50.41 57.76 73.96 82.81 67.24 75.69 61.890 67.24 82.81 84.64 90.25 70.56 86.49 62.010 96.04 90.25 82.81 70.56 73.96 98.01 62.130 100.00 86.49 65.61 68.89 70.56 72.25 62.250 72.25 60.84 70.56 51.84 50.41 47.61 62.370 50.41 50.41 50.41 42.25 67.24 56.25 62.490 54.76 53.29 56.25 56.25 59.29 56.25 62.610 54.76 49.00 59.29 53.29 47.61 59.29 62.730 59.29 65.61 75.69 56.25 77.44 60.84 62.850 73.96 72.25 72.25 90.25 75.69 96.04 62.970 102.01 88.36 96.04 106.09 94.09 118.81 63.090 125.44 153.76 146.41 144.00 158.76 198.81 63.210 210.25 210.25 262.44 256.00 295.84 302.76 63.330 338.56 357.21 388.09 364.81 361.00 361.00 63.450 392.04 368.64 338.56 349.69 313.29 313.29 63.570 302.76 275.56 243.36 219.04 207.36 169.00 63.690 182.25 176.89 156.25 176.89 132.25 127.69 63.810 127.69 108.16 116.64 121.00 116.64 94.09 63.930 112.36 88.36 110.25 112.36 104.04 108.16 64.050 90.25 88.36 86.49 112.36 121.00 112.36 64.170 129.96 129.96 136.89 127.69 134.56 163.84 64.290 146.41 182.25 216.09 213.16 252.81 292.41 64.410 353.44 353.44 357.21 361.00 331.24 324.00 64.530 338.56 309.76 289.00 313.29 324.00 275.56 64.650 278.89 252.81 282.24 213.16 243.36 182.25 64.770 193.21 174.24 182.25 163.84 163.84 182.25 64.890 182.25 187.69 174.24 169.00 176.89 210.25 65.010 207.36 249.64 231.04 249.64 213.16 228.01 65.130 259.21 243.36 219.04 249.64 246.49 219.04 65.250 249.64 213.16 210.25 184.96 182.25 187.69 65.370 174.24 158.76 158.76 132.25 121.00 132.25 65.490 114.49 121.00 121.00 104.04 108.16 98.01 65.610 90.25 127.69 102.01 100.00 104.04 108.16 65.730 106.09 90.25 129.96 102.01 114.49 118.81 65.850 129.96 134.56 139.24 141.61 146.41 153.76 65.970 141.61 153.76 166.41 158.76 169.00 148.84 66.090 139.24 141.61 136.89 153.76 153.76 123.21 66.210 139.24 148.84 144.00 110.25 110.25 100.00 66.330 79.21 90.25 112.36 108.16 92.16 98.01 66.450 81.00 92.16 94.09 90.25 92.16 79.21 66.570 68.89 70.56 86.49 81.00 75.69 70.56 66.690 84.64 73.96 92.16 88.36 94.09 84.64 66.810 68.89 75.69 90.25 94.09 84.64 100.00 66.930 112.36 118.81 108.16 110.25 153.76 136.89 67.050 156.25 158.76 182.25 158.76 201.64 207.36 67.170 234.09 252.81 234.09 295.84 299.29 331.24 67.290 334.89 408.04 384.16 441.00 392.04 388.09 67.410 368.64 338.56 342.25 320.41 331.24 316.84 67.530 285.61 272.25 256.00 275.56 237.16 193.21 67.650 193.21 190.44 169.00 151.29 179.56 132.25

243

File: JC13.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 132.25 125.44 134.56 116.64 112.36 106.09 67.890 100.00 92.16 98.01 82.81 92.16 96.04 68.010 75.69 73.96 82.81 96.04 100.00 79.21 68.130 72.25 72.25 77.44 79.21 68.89 62.41 68.250 70.56 67.24 65.61 68.89 65.61 53.29 68.370 68.89 64.00 53.29 53.29 62.41 62.41 68.490 53.29 56.25 49.00 50.41 47.61 65.61 68.610 47.61 59.29 42.25 47.61 46.24 46.24 68.730 40.96 47.61 43.56 32.49 50.41 46.24 68.850 54.76 46.24 56.25 50.41 36.00 53.29 68.970 53.29 43.56 51.84 50.41 53.29 38.44 69.090 38.44 47.61 47.61 53.29 50.41 62.41 69.210 50.41 59.29 53.29 51.84 54.76 50.41 69.330 56.25 53.29 62.41 46.24 47.61 47.61 69.450 50.41 57.76 70.56 50.41 62.41 70.56 69.570 50.41 77.44 72.25 65.61 53.29 62.41 69.690 51.84 68.89 60.84 72.25 67.24 67.24 69.810 60.84 79.21 62.41 82.81 92.16 72.25 69.930 86.49 84.64 92.16 81.00 _

244

File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC14 Data measured at: 25-Jan-2011 14:51:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 5806.440 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 104.04 96.04 98.01 82.81 86.49 96.04 2.130 106.09 84.64 94.09 90.25 81.00 92.16 2.250 81.00 79.21 75.69 79.21 77.44 62.41 2.370 73.96 67.24 77.44 72.25 64.00 62.41 2.490 67.24 77.44 65.61 47.61 65.61 72.25 2.610 53.29 59.29 60.84 68.89 75.69 56.25 2.730 73.96 72.25 75.69 70.56 56.25 59.29 2.850 56.25 56.25 70.56 56.25 59.29 75.69 2.970 47.61 59.29 62.41 56.25 77.44 62.41 3.090 65.61 62.41 65.61 57.76 54.76 67.24 3.210 56.25 56.25 75.69 65.61 50.41 43.56 3.330 57.76 62.41 65.61 47.61 59.29 64.00 3.450 59.29 47.61 53.29 62.41 43.56 59.29 3.570 56.25 67.24 82.81 59.29 53.29 59.29 3.690 57.76 70.56 59.29 50.41 56.25 60.84 3.810 70.56 57.76 65.61 59.29 60.84 67.24 3.930 49.00 44.89 59.29 56.25 68.89 62.41 4.050 62.41 53.29 56.25 65.61 59.29 54.76 4.170 49.00 53.29 50.41 53.29 50.41 50.41 4.290 38.44 51.84 57.76 56.25 50.41 53.29 4.410 53.29 56.25 56.25 56.25 56.25 56.25 4.530 50.41 67.24 54.76 60.84 51.84 62.41 4.650 59.29 62.41 50.41 57.76 57.76 62.41 4.770 51.84 65.61 65.61 49.00 59.29 57.76 4.890 65.61 44.89 59.29 44.89 67.24 56.25 5.010 46.24 53.29 70.56 60.84 53.29 47.61 5.130 72.25 64.00 59.29 65.61 57.76 62.41 5.250 56.25 53.29 50.41 47.61 46.24 77.44

245

File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 49.00 53.29 49.00 36.00 57.76 54.76 5.490 68.89 50.41 53.29 59.29 44.89 54.76 5.610 44.89 59.29 53.29 50.41 59.29 43.56 5.730 54.76 38.44 51.84 53.29 43.56 42.25 5.850 50.41 59.29 70.56 40.96 50.41 50.41 5.970 59.29 56.25 49.00 49.00 59.29 62.41 6.090 44.89 62.41 47.61 65.61 59.29 46.24 6.210 40.96 47.61 56.25 54.76 60.84 47.61 6.330 60.84 59.29 54.76 62.41 50.41 53.29 6.450 50.41 50.41 50.41 62.41 53.29 53.29 6.570 64.00 62.41 39.69 68.89 53.29 39.69 6.690 50.41 53.29 56.25 53.29 47.61 44.89 6.810 51.84 49.00 60.84 56.25 57.76 56.25 6.930 49.00 43.56 59.29 53.29 51.84 42.25 7.050 59.29 53.29 59.29 56.25 50.41 53.29 7.170 56.25 47.61 34.81 59.29 47.61 36.00 7.290 59.29 54.76 51.84 53.29 60.84 59.29 7.410 43.56 62.41 53.29 67.24 51.84 53.29 7.530 40.96 50.41 49.00 36.00 59.29 37.21 7.650 59.29 51.84 51.84 53.29 53.29 43.56 7.770 59.29 62.41 43.56 32.49 43.56 57.76 7.890 56.25 51.84 56.25 59.29 54.76 65.61 8.010 47.61 53.29 54.76 47.61 56.25 50.41 8.130 51.84 46.24 34.81 38.44 46.24 50.41 8.250 50.41 38.44 47.61 54.76 42.25 57.76 8.370 56.25 38.44 50.41 47.61 49.00 56.25 8.490 59.29 53.29 56.25 59.29 50.41 40.96 8.610 50.41 49.00 51.84 40.96 57.76 43.56 8.730 50.41 65.61 44.89 47.61 40.96 54.76 8.850 59.29 50.41 53.29 51.84 46.24 39.69 8.970 46.24 54.76 54.76 44.89 44.89 62.41 9.090 47.61 53.29 47.61 47.61 53.29 50.41 9.210 44.89 51.84 47.61 49.00 50.41 44.89 9.330 47.61 40.96 54.76 49.00 42.25 56.25 9.450 53.29 46.24 59.29 57.76 40.96 46.24 9.570 50.41 47.61 44.89 43.56 54.76 56.25 9.690 46.24 57.76 42.25 39.69 50.41 43.56 9.810 42.25 50.41 43.56 47.61 47.61 47.61 9.930 46.24 38.44 59.29 37.21 44.89 64.00 10.050 40.96 57.76 56.25 54.76 53.29 36.00 10.170 40.96 44.89 47.61 47.61 46.24 44.89 10.290 40.96 53.29 42.25 43.56 32.49 44.89 10.410 47.61 42.25 49.00 64.00 42.25 51.84 10.530 47.61 53.29 43.56 53.29 57.76 57.76 10.650 47.61 49.00 43.56 49.00 50.41 33.64 10.770 32.49 43.56 40.96 40.96 47.61 43.56 10.890 42.25 47.61 40.96 46.24 53.29 32.49 11.010 51.84 47.61 38.44 50.41 46.24 40.96 11.130 56.25 51.84 40.96 47.61 38.44 44.89 11.250 36.00 38.44 50.41 51.84 47.61 40.96 11.370 56.25 47.61 40.96 47.61 40.96 42.25 11.490 44.89 43.56 43.56 50.41 51.84 43.56

246

File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 39.69 49.00 43.56 53.29 40.96 43.56 11.730 38.44 50.41 33.64 49.00 46.24 62.41 11.850 38.44 43.56 53.29 50.41 50.41 47.61 11.970 50.41 46.24 38.44 49.00 50.41 39.69 12.090 37.21 44.89 50.41 43.56 43.56 56.25 12.210 49.00 42.25 46.24 36.00 53.29 42.25 12.330 42.25 42.25 46.24 39.69 50.41 39.69 12.450 51.84 36.00 49.00 49.00 54.76 53.29 12.570 38.44 50.41 34.81 32.49 40.96 54.76 12.690 47.61 44.89 37.21 47.61 57.76 50.41 12.810 44.89 39.69 51.84 50.41 38.44 46.24 12.930 54.76 38.44 39.69 39.69 49.00 44.89 13.050 27.04 53.29 56.25 43.56 40.96 44.89 13.170 49.00 50.41 49.00 43.56 44.89 43.56 13.290 56.25 42.25 38.44 36.00 32.49 38.44 13.410 36.00 53.29 44.89 37.21 49.00 28.09 13.530 44.89 34.81 53.29 47.61 40.96 37.21 13.650 40.96 37.21 38.44 47.61 40.96 33.64 13.770 43.56 38.44 38.44 33.64 32.49 43.56 13.890 43.56 37.21 40.96 47.61 37.21 38.44 14.010 39.69 34.81 47.61 46.24 50.41 49.00 14.130 43.56 29.16 43.56 40.96 38.44 43.56 14.250 42.25 36.00 28.09 37.21 51.84 42.25 14.370 42.25 40.96 42.25 36.00 47.61 51.84 14.490 50.41 50.41 42.25 38.44 33.64 38.44 14.610 49.00 38.44 47.61 43.56 50.41 49.00 14.730 50.41 33.64 43.56 44.89 53.29 46.24 14.850 44.89 32.49 50.41 37.21 43.56 34.81 14.970 32.49 42.25 46.24 29.16 33.64 57.76 15.090 59.29 47.61 59.29 36.00 43.56 47.61 15.210 56.25 47.61 59.29 53.29 42.25 49.00 15.330 54.76 42.25 47.61 43.56 42.25 47.61 15.450 54.76 59.29 57.76 43.56 56.25 56.25 15.570 42.25 47.61 53.29 72.25 39.69 56.25 15.690 50.41 59.29 56.25 59.29 59.29 47.61 15.810 43.56 43.56 36.00 47.61 43.56 47.61 15.930 42.25 67.24 59.29 38.44 43.56 62.41 16.050 50.41 56.25 53.29 38.44 37.21 50.41 16.170 39.69 38.44 60.84 47.61 46.24 44.89 16.290 44.89 46.24 46.24 43.56 47.61 34.81 16.410 50.41 43.56 47.61 57.76 47.61 56.25 16.530 54.76 42.25 47.61 60.84 47.61 51.84 16.650 40.96 49.00 39.69 46.24 42.25 46.24 16.770 29.16 38.44 62.41 51.84 44.89 46.24 16.890 65.61 59.29 46.24 39.69 43.56 42.25 17.010 44.89 57.76 38.44 49.00 46.24 53.29 17.130 54.76 46.24 44.89 47.61 40.96 57.76 17.250 56.25 38.44 40.96 47.61 53.29 37.21 17.370 47.61 29.16 44.89 50.41 51.84 43.56 17.490 47.61 43.56 36.00 38.44 39.69 28.09 17.610 47.61 46.24 32.49 36.00 40.96 42.25 17.730 53.29 43.56 43.56 47.61 42.25 38.44

247

File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 43.56 56.25 38.44 51.84 43.56 38.44 17.970 53.29 47.61 40.96 34.81 47.61 38.44 18.090 44.89 47.61 43.56 37.21 31.36 38.44 18.210 38.44 33.64 39.69 51.84 36.00 47.61 18.330 44.89 46.24 47.61 54.76 53.29 39.69 18.450 47.61 38.44 43.56 39.69 43.56 56.25 18.570 39.69 42.25 33.64 44.89 50.41 50.41 18.690 51.84 57.76 31.36 53.29 49.00 42.25 18.810 47.61 43.56 49.00 47.61 44.89 44.89 18.930 40.96 33.64 43.56 43.56 46.24 47.61 19.050 54.76 44.89 43.56 39.69 46.24 47.61 19.170 49.00 36.00 43.56 47.61 42.25 54.76 19.290 34.81 51.84 31.36 49.00 39.69 33.64 19.410 47.61 40.96 43.56 59.29 38.44 38.44 19.530 40.96 47.61 43.56 39.69 50.41 50.41 19.650 46.24 40.96 46.24 46.24 53.29 34.81 19.770 39.69 43.56 44.89 57.76 42.25 28.09 19.890 44.89 44.89 33.64 50.41 42.25 37.21 20.010 39.69 43.56 29.16 39.69 37.21 56.25 20.130 32.49 53.29 46.24 36.00 46.24 32.49 20.250 37.21 39.69 43.56 31.36 43.56 64.00 20.370 53.29 43.56 31.36 33.64 50.41 43.56 20.490 44.89 43.56 44.89 47.61 46.24 44.89 20.610 56.25 51.84 42.25 54.76 38.44 50.41 20.730 84.64 136.89 144.00 136.89 134.56 106.09 20.850 92.16 86.49 59.29 56.25 44.89 42.25 20.970 44.89 47.61 51.84 47.61 49.00 32.49 21.090 59.29 39.69 43.56 44.89 37.21 50.41 21.210 44.89 36.00 46.24 39.69 36.00 38.44 21.330 37.21 50.41 53.29 47.61 39.69 46.24 21.450 47.61 44.89 38.44 50.41 39.69 53.29 21.570 40.96 53.29 43.56 43.56 32.49 44.89 21.690 40.96 38.44 40.96 43.56 53.29 49.00 21.810 42.25 50.41 47.61 53.29 53.29 60.84 21.930 62.41 82.81 82.81 110.25 88.36 108.16 22.050 106.09 90.25 79.21 65.61 65.61 56.25 22.170 53.29 51.84 42.25 40.96 59.29 43.56 22.290 43.56 40.96 43.56 43.56 39.69 50.41 22.410 34.81 39.69 50.41 42.25 43.56 34.81 22.530 36.00 32.49 43.56 38.44 47.61 40.96 22.650 49.00 43.56 37.21 32.49 39.69 44.89 22.770 38.44 34.81 28.09 46.24 46.24 46.24 22.890 34.81 32.49 40.96 36.00 42.25 49.00 23.010 40.96 53.29 39.69 47.61 32.49 38.44 23.130 44.89 47.61 53.29 38.44 42.25 33.64 23.250 43.56 38.44 50.41 44.89 32.49 39.69 23.370 38.44 38.44 56.25 42.25 34.81 37.21 23.490 32.49 46.24 34.81 40.96 43.56 47.61 23.610 32.49 39.69 38.44 32.49 47.61 47.61 23.730 59.29 53.29 39.69 60.84 49.00 62.41 23.850 67.24 77.44 90.25 94.09 102.01 102.01 23.970 127.69 153.76 193.21 182.25 198.81 210.25

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 193.21 193.21 146.41 96.04 88.36 92.16 24.210 72.25 53.29 56.25 49.00 70.56 42.25 24.330 54.76 49.00 57.76 43.56 39.69 39.69 24.450 43.56 28.09 39.69 37.21 39.69 56.25 24.570 53.29 36.00 53.29 43.56 47.61 29.16 24.690 40.96 47.61 42.25 34.81 43.56 37.21 24.810 40.96 34.81 39.69 50.41 47.61 36.00 24.930 50.41 47.61 47.61 44.89 43.56 38.44 25.050 40.96 42.25 43.56 36.00 44.89 37.21 25.170 29.16 39.69 46.24 46.24 40.96 54.76 25.290 38.44 43.56 31.36 38.44 38.44 36.00 25.410 39.69 39.69 37.21 39.69 44.89 46.24 25.530 39.69 29.16 46.24 44.89 33.64 47.61 25.650 37.21 37.21 38.44 53.29 47.61 53.29 25.770 37.21 42.25 32.49 53.29 34.81 54.76 25.890 42.25 38.44 39.69 47.61 38.44 62.41 26.010 36.00 43.56 42.25 47.61 39.69 40.96 26.130 32.49 36.00 42.25 51.84 47.61 47.61 26.250 47.61 43.56 46.24 42.25 42.25 40.96 26.370 40.96 50.41 49.00 62.41 39.69 56.25 26.490 47.61 65.61 90.25 72.25 79.21 90.25 26.610 112.36 110.25 114.49 106.09 106.09 62.41 26.730 56.25 62.41 46.24 44.89 47.61 47.61 26.850 32.49 36.00 42.25 40.96 28.09 43.56 26.970 32.49 50.41 38.44 47.61 42.25 39.69 27.090 39.69 46.24 47.61 37.21 33.64 30.25 27.210 40.96 39.69 38.44 37.21 43.56 34.81 27.330 38.44 33.64 46.24 46.24 51.84 38.44 27.450 40.96 36.00 29.16 43.56 29.16 37.21 27.570 46.24 37.21 47.61 37.21 38.44 34.81 27.690 40.96 37.21 34.81 34.81 36.00 31.36 27.810 40.96 31.36 43.56 39.69 46.24 53.29 27.930 47.61 32.49 32.49 39.69 37.21 38.44 28.050 38.44 37.21 29.16 40.96 32.49 37.21 28.170 31.36 44.89 32.49 39.69 43.56 38.44 28.290 49.00 42.25 36.00 53.29 46.24 47.61 28.410 42.25 36.00 46.24 42.25 37.21 39.69 28.530 39.69 46.24 36.00 43.56 34.81 42.25 28.650 44.89 46.24 40.96 42.25 39.69 56.25 28.770 40.96 53.29 37.21 32.49 43.56 50.41 28.890 39.69 43.56 39.69 33.64 53.29 43.56 29.010 50.41 38.44 43.56 57.76 44.89 40.96 29.130 50.41 50.41 34.81 47.61 46.24 51.84 29.250 50.41 56.25 64.00 57.76 56.25 79.21 29.370 82.81 73.96 90.25 104.04 84.64 100.00 29.490 106.09 102.01 84.64 72.25 70.56 65.61 29.610 59.29 51.84 56.25 65.61 43.56 65.61 29.730 54.76 65.61 64.00 57.76 44.89 56.25 29.850 49.00 59.29 62.41 65.61 53.29 70.56 29.970 50.41 53.29 60.84 59.29 70.56 54.76 30.090 67.24 72.25 72.25 70.56 82.81 73.96 30.210 73.96 82.81 90.25 92.16 77.44 104.04

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File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 106.09 102.01 106.09 121.00 125.44 134.56 30.450 158.76 171.61 193.21 204.49 222.01 237.16 30.570 268.96 262.44 299.29 338.56 432.64 462.25 30.690 529.00 655.36 812.25 888.04 1169.64 1436.41 30.810 1672.81 2070.25 2766.76 3352.41 3893.76 4569.76 30.930 5285.29 5806.44 5700.25 5155.24 4502.41 3794.56 31.050 3147.21 2470.09 1866.24 1451.61 1075.84 841.00 31.170 686.44 620.01 484.00 420.25 372.49 345.96 31.290 292.41 289.00 225.00 210.25 196.00 174.24 31.410 146.41 146.41 141.61 102.01 129.96 114.49 31.530 96.04 96.04 104.04 92.16 116.64 108.16 31.650 96.04 92.16 75.69 82.81 72.25 62.41 31.770 67.24 67.24 77.44 77.44 67.24 62.41 31.890 79.21 75.69 62.41 72.25 56.25 68.89 32.010 70.56 70.56 59.29 62.41 65.61 68.89 32.130 60.84 53.29 43.56 50.41 50.41 38.44 32.250 57.76 62.41 54.76 60.84 62.41 73.96 32.370 53.29 43.56 50.41 65.61 49.00 39.69 32.490 47.61 56.25 50.41 51.84 54.76 51.84 32.610 56.25 60.84 56.25 51.84 47.61 65.61 32.730 42.25 31.36 40.96 47.61 47.61 47.61 32.850 44.89 38.44 43.56 49.00 42.25 67.24 32.970 46.24 44.89 53.29 32.49 54.76 62.41 33.090 72.25 57.76 59.29 75.69 67.24 38.44 33.210 65.61 65.61 67.24 86.49 84.64 86.49 33.330 70.56 92.16 118.81 146.41 174.24 210.25 33.450 219.04 262.44 275.56 299.29 345.96 324.00 33.570 334.89 256.00 265.69 193.21 196.00 158.76 33.690 134.56 129.96 90.25 104.04 82.81 70.56 33.810 70.56 79.21 60.84 59.29 51.84 54.76 33.930 49.00 53.29 47.61 47.61 56.25 42.25 34.050 39.69 44.89 49.00 60.84 43.56 51.84 34.170 43.56 43.56 46.24 43.56 44.89 47.61 34.290 50.41 40.96 44.89 59.29 32.49 47.61 34.410 43.56 50.41 44.89 40.96 47.61 47.61 34.530 54.76 46.24 43.56 36.00 46.24 36.00 34.650 60.84 40.96 56.25 54.76 39.69 47.61 34.770 39.69 57.76 43.56 53.29 53.29 68.89 34.890 56.25 46.24 53.29 59.29 56.25 60.84 35.010 68.89 75.69 72.25 90.25 81.00 106.09 35.130 114.49 125.44 129.96 176.89 184.96 169.00 35.250 210.25 240.25 262.44 243.36 252.81 285.61 35.370 275.56 231.04 213.16 179.56 156.25 136.89 35.490 134.56 104.04 88.36 92.16 94.09 77.44 35.610 56.25 73.96 70.56 65.61 53.29 56.25 35.730 60.84 56.25 54.76 65.61 62.41 62.41 35.850 64.00 56.25 59.29 54.76 47.61 60.84 35.970 47.61 62.41 50.41 50.41 50.41 43.56 36.090 47.61 65.61 40.96 51.84 50.41 44.89 36.210 49.00 50.41 39.69 62.41 56.25 46.24 36.330 46.24 43.56 54.76 56.25 51.84 44.89 36.450 56.25 59.29 51.84 56.25 68.89 59.29

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File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 47.61 60.84 68.89 62.41 82.81 67.24 36.690 65.61 73.96 67.24 82.81 67.24 77.44 36.810 84.64 79.21 104.04 96.04 90.25 106.09 36.930 112.36 96.04 98.01 123.21 125.44 136.89 37.050 139.24 116.64 141.61 148.84 151.29 148.84 37.170 174.24 169.00 222.01 213.16 246.49 285.61 37.290 306.25 372.49 372.49 445.21 420.25 441.00 37.410 392.04 349.69 306.25 268.96 275.56 225.00 37.530 182.25 146.41 136.89 121.00 100.00 88.36 37.650 100.00 79.21 79.21 88.36 68.89 62.41 37.770 59.29 60.84 62.41 56.25 57.76 54.76 37.890 47.61 39.69 56.25 57.76 62.41 50.41 38.010 62.41 53.29 67.24 53.29 62.41 51.84 38.130 43.56 43.56 54.76 46.24 67.24 53.29 38.250 46.24 65.61 42.25 53.29 49.00 43.56 38.370 47.61 46.24 47.61 51.84 47.61 51.84 38.490 49.00 53.29 51.84 50.41 37.21 53.29 38.610 36.00 59.29 65.61 38.44 37.21 38.44 38.730 46.24 40.96 42.25 59.29 44.89 50.41 38.850 42.25 49.00 49.00 56.25 50.41 64.00 38.970 42.25 62.41 42.25 53.29 54.76 53.29 39.090 62.41 38.44 49.00 47.61 53.29 42.25 39.210 56.25 42.25 51.84 70.56 62.41 72.25 39.330 82.81 81.00 88.36 84.64 86.49 92.16 39.450 116.64 110.25 98.01 90.25 86.49 108.16 39.570 104.04 108.16 106.09 90.25 104.04 102.01 39.690 108.16 102.01 96.04 110.25 112.36 151.29 39.810 132.25 139.24 129.96 132.25 146.41 136.89 39.930 132.25 151.29 136.89 123.21 129.96 125.44 40.050 110.25 118.81 100.00 108.16 88.36 96.04 40.170 92.16 62.41 68.89 64.00 64.00 65.61 40.290 59.29 50.41 64.00 64.00 50.41 44.89 40.410 62.41 50.41 62.41 70.56 65.61 79.21 40.530 62.41 70.56 82.81 81.00 94.09 86.49 40.650 106.09 84.64 96.04 98.01 106.09 108.16 40.770 129.96 129.96 176.89 163.84 210.25 237.16 40.890 228.01 292.41 349.69 416.16 479.61 538.24 41.010 665.64 750.76 912.04 1030.41 1128.96 1211.04 41.130 1218.01 1197.16 1246.09 1043.29 930.25 864.36 41.250 767.29 686.44 585.64 492.84 384.16 316.84 41.370 278.89 252.81 193.21 184.96 156.25 148.84 41.490 108.16 139.24 114.49 98.01 94.09 94.09 41.610 70.56 86.49 79.21 72.25 65.61 59.29 41.730 72.25 79.21 49.00 65.61 50.41 57.76 41.850 65.61 64.00 65.61 59.29 53.29 51.84 41.970 43.56 38.44 47.61 43.56 44.89 50.41 42.090 50.41 42.25 44.89 49.00 33.64 43.56 42.210 53.29 50.41 38.44 36.00 43.56 50.41 42.330 54.76 46.24 46.24 51.84 47.61 62.41 42.450 37.21 38.44 46.24 47.61 43.56 50.41 42.570 47.61 50.41 37.21 43.56 38.44 38.44 42.690 43.56 38.44 39.69 39.69 47.61 32.49

251

File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 40.96 42.25 42.25 57.76 43.56 47.61 42.930 49.00 42.25 50.41 39.69 51.84 39.69 43.050 53.29 53.29 49.00 51.84 53.29 50.41 43.170 56.25 64.00 57.76 56.25 47.61 57.76 43.290 53.29 43.56 40.96 53.29 70.56 57.76 43.410 62.41 60.84 64.00 47.61 62.41 65.61 43.530 79.21 68.89 79.21 88.36 94.09 118.81 43.650 129.96 129.96 153.76 161.29 201.64 210.25 43.770 219.04 222.01 243.36 196.00 166.41 198.81 43.890 161.29 148.84 151.29 123.21 94.09 100.00 44.010 82.81 68.89 59.29 75.69 65.61 67.24 44.130 67.24 67.24 72.25 57.76 72.25 75.69 44.250 49.00 43.56 64.00 53.29 67.24 49.00 44.370 81.00 59.29 73.96 72.25 65.61 88.36 44.490 72.25 77.44 77.44 104.04 82.81 94.09 44.610 114.49 98.01 132.25 132.25 156.25 171.61 44.730 190.44 256.00 334.89 345.96 436.81 538.24 44.850 547.56 686.44 750.76 817.96 835.21 784.00 44.970 723.61 630.01 625.00 571.21 519.84 436.81 45.090 372.49 282.24 259.21 222.01 190.44 151.29 45.210 169.00 144.00 110.25 118.81 102.01 102.01 45.330 86.49 65.61 68.89 77.44 72.25 73.96 45.450 70.56 77.44 67.24 62.41 60.84 59.29 45.570 62.41 43.56 62.41 46.24 43.56 56.25 45.690 50.41 39.69 56.25 51.84 64.00 57.76 45.810 43.56 64.00 62.41 43.56 54.76 47.61 45.930 56.25 59.29 46.24 39.69 53.29 44.89 46.050 50.41 43.56 47.61 37.21 40.96 43.56 46.170 44.89 36.00 42.25 38.44 53.29 37.21 46.290 50.41 54.76 50.41 40.96 40.96 51.84 46.410 50.41 56.25 49.00 59.29 46.24 38.44 46.530 43.56 47.61 57.76 50.41 54.76 59.29 46.650 49.00 47.61 50.41 50.41 50.41 51.84 46.770 53.29 50.41 53.29 53.29 44.89 50.41 46.890 50.41 43.56 51.84 47.61 43.56 50.41 47.010 56.25 44.89 37.21 47.61 57.76 68.89 47.130 62.41 43.56 42.25 65.61 50.41 33.64 47.250 65.61 50.41 46.24 57.76 43.56 50.41 47.370 40.96 53.29 53.29 51.84 46.24 57.76 47.490 46.24 64.00 67.24 62.41 49.00 56.25 47.610 56.25 43.56 57.76 75.69 50.41 43.56 47.730 53.29 65.61 43.56 36.00 39.69 53.29 47.850 50.41 39.69 39.69 43.56 47.61 47.61 47.970 49.00 39.69 47.61 51.84 46.24 59.29 48.090 37.21 44.89 53.29 34.81 47.61 54.76 48.210 56.25 50.41 56.25 50.41 49.00 67.24 48.330 38.44 62.41 47.61 51.84 56.25 49.00 48.450 57.76 53.29 56.25 67.24 67.24 70.56 48.570 60.84 65.61 67.24 53.29 90.25 59.29 48.690 59.29 57.76 59.29 57.76 70.56 50.41 48.810 56.25 70.56 68.89 72.25 72.25 86.49 48.930 84.64 73.96 77.44 84.64 92.16 88.36

252

File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 98.01 139.24 127.69 151.29 169.00 176.89 49.170 198.81 210.25 222.01 243.36 243.36 225.00 49.290 225.00 222.01 213.16 196.00 222.01 198.81 49.410 179.56 141.61 129.96 136.89 102.01 114.49 49.530 106.09 96.04 92.16 88.36 102.01 102.01 49.650 94.09 79.21 96.04 77.44 90.25 79.21 49.770 82.81 79.21 88.36 84.64 77.44 104.04 49.890 104.04 94.09 108.16 100.00 112.36 129.96 50.010 129.96 139.24 158.76 144.00 134.56 171.61 50.130 161.29 176.89 190.44 225.00 225.00 275.56 50.250 272.25 299.29 327.61 349.69 416.16 428.49 50.370 506.25 529.00 640.09 718.24 795.24 858.49 50.490 973.44 998.56 1062.76 961.00 967.21 846.81 50.610 876.16 784.00 778.41 676.00 650.25 650.25 50.730 600.25 547.56 501.76 547.56 524.41 484.00 50.850 519.84 566.44 645.16 645.16 729.00 864.36 50.970 924.16 1056.25 1017.61 1036.84 1122.25 1128.96 51.090 1062.76 1004.89 961.00 924.16 852.64 806.56 51.210 767.29 718.24 605.16 542.89 524.41 436.81 51.330 416.16 353.44 327.61 259.21 289.00 256.00 51.450 210.25 166.41 166.41 158.76 171.61 144.00 51.570 127.69 127.69 114.49 92.16 108.16 98.01 51.690 88.36 88.36 90.25 77.44 86.49 67.24 51.810 90.25 98.01 81.00 59.29 75.69 70.56 51.930 75.69 60.84 67.24 67.24 67.24 65.61 52.050 54.76 75.69 57.76 56.25 59.29 47.61 52.170 50.41 62.41 72.25 67.24 65.61 70.56 52.290 60.84 54.76 81.00 53.29 65.61 47.61 52.410 59.29 75.69 65.61 65.61 50.41 57.76 52.530 47.61 59.29 57.76 47.61 56.25 56.25 52.650 53.29 38.44 38.44 51.84 53.29 50.41 52.770 47.61 50.41 49.00 34.81 62.41 49.00 52.890 50.41 47.61 49.00 59.29 46.24 32.49 53.010 44.89 42.25 50.41 46.24 36.00 47.61 53.130 42.25 65.61 50.41 51.84 43.56 44.89 53.250 47.61 43.56 42.25 43.56 37.21 57.76 53.370 43.56 38.44 47.61 57.76 56.25 43.56 53.490 38.44 49.00 47.61 49.00 50.41 39.69 53.610 43.56 42.25 46.24 53.29 56.25 36.00 53.730 43.56 44.89 50.41 38.44 40.96 53.29 53.850 43.56 54.76 43.56 38.44 36.00 42.25 53.970 47.61 49.00 53.29 33.64 49.00 34.81 54.090 39.69 33.64 39.69 39.69 30.25 40.96 54.210 40.96 33.64 39.69 37.21 38.44 43.56 54.330 38.44 40.96 43.56 38.44 46.24 42.25 54.450 37.21 40.96 43.56 42.25 37.21 42.25 54.570 34.81 43.56 39.69 42.25 32.49 37.21 54.690 38.44 40.96 39.69 51.84 32.49 43.56 54.810 47.61 39.69 44.89 38.44 33.64 44.89 54.930 39.69 46.24 32.49 36.00 44.89 57.76 55.050 44.89 44.89 44.89 36.00 43.56 34.81 55.170 47.61 50.41 38.44 40.96 37.21 36.00

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File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 36.00 50.41 40.96 33.64 37.21 33.64 55.410 44.89 50.41 40.96 50.41 50.41 43.56 55.530 30.25 43.56 37.21 32.49 46.24 33.64 55.650 42.25 31.36 42.25 36.00 36.00 32.49 55.770 39.69 53.29 38.44 51.84 34.81 30.25 55.890 43.56 43.56 40.96 38.44 31.36 43.56 56.010 39.69 47.61 37.21 39.69 43.56 40.96 56.130 38.44 32.49 37.21 32.49 46.24 36.00 56.250 28.09 46.24 38.44 47.61 38.44 43.56 56.370 44.89 47.61 37.21 50.41 43.56 50.41 56.490 43.56 53.29 34.81 43.56 38.44 47.61 56.610 39.69 47.61 46.24 44.89 38.44 49.00 56.730 43.56 32.49 37.21 46.24 42.25 47.61 56.850 47.61 42.25 42.25 44.89 50.41 38.44 56.970 54.76 34.81 34.81 36.00 31.36 38.44 57.090 38.44 32.49 47.61 40.96 49.00 44.89 57.210 53.29 38.44 50.41 33.64 42.25 44.89 57.330 42.25 49.00 53.29 70.56 54.76 57.76 57.450 43.56 47.61 50.41 38.44 43.56 53.29 57.570 38.44 56.25 47.61 43.56 50.41 40.96 57.690 49.00 56.25 42.25 43.56 56.25 46.24 57.810 62.41 39.69 38.44 57.76 37.21 56.25 57.930 40.96 49.00 53.29 47.61 40.96 53.29 58.050 46.24 43.56 43.56 51.84 50.41 53.29 58.170 53.29 42.25 39.69 54.76 53.29 43.56 58.290 60.84 53.29 60.84 47.61 60.84 62.41 58.410 56.25 47.61 70.56 67.24 64.00 75.69 58.530 68.89 82.81 92.16 75.69 100.00 98.01 58.650 90.25 112.36 144.00 134.56 153.76 176.89 58.770 182.25 213.16 201.64 210.25 237.16 252.81 58.890 234.09 231.04 222.01 222.01 198.81 176.89 59.010 166.41 148.84 190.44 163.84 136.89 127.69 59.130 125.44 121.00 96.04 104.04 110.25 90.25 59.250 86.49 100.00 88.36 84.64 88.36 98.01 59.370 90.25 102.01 81.00 104.04 108.16 110.25 59.490 121.00 134.56 163.84 158.76 161.29 198.81 59.610 216.09 216.09 285.61 259.21 331.24 309.76 59.730 357.21 412.09 424.36 457.96 396.01 424.36 59.850 404.01 380.25 408.04 338.56 302.76 306.25 59.970 292.41 252.81 252.81 198.81 174.24 174.24 60.090 163.84 151.29 144.00 106.09 116.64 92.16 60.210 88.36 82.81 90.25 81.00 94.09 90.25 60.330 73.96 62.41 62.41 70.56 54.76 59.29 60.450 72.25 59.29 67.24 72.25 49.00 56.25 60.570 62.41 67.24 53.29 56.25 79.21 57.76 60.690 54.76 53.29 77.44 56.25 62.41 47.61 60.810 51.84 47.61 53.29 60.84 64.00 49.00 60.930 50.41 53.29 59.29 60.84 53.29 43.56 61.050 50.41 53.29 43.56 59.29 53.29 62.41 61.170 53.29 59.29 53.29 44.89 56.25 53.29 61.290 50.41 64.00 47.61 62.41 56.25 44.89 61.410 44.89 64.00 43.56 57.76 47.61 46.24

254

File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 40.96 47.61 49.00 62.41 47.61 44.89 61.650 64.00 54.76 56.25 56.25 77.44 62.41 61.770 60.84 59.29 65.61 77.44 72.25 59.29 61.890 68.89 82.81 94.09 88.36 94.09 86.49 62.010 108.16 82.81 94.09 90.25 88.36 75.69 62.130 77.44 88.36 68.89 84.64 62.41 64.00 62.250 56.25 49.00 50.41 47.61 60.84 67.24 62.370 67.24 53.29 62.41 50.41 53.29 50.41 62.490 65.61 56.25 56.25 67.24 56.25 47.61 62.610 67.24 56.25 56.25 62.41 59.29 57.76 62.730 72.25 57.76 59.29 50.41 65.61 73.96 62.850 65.61 67.24 73.96 73.96 67.24 72.25 62.970 92.16 86.49 98.01 79.21 102.01 104.04 63.090 94.09 127.69 123.21 104.04 136.89 136.89 63.210 151.29 176.89 187.69 222.01 231.04 265.69 63.330 342.25 316.84 349.69 345.96 357.21 392.04 63.450 353.44 295.84 320.41 272.25 285.61 282.24 63.570 259.21 225.00 237.16 243.36 207.36 163.84 63.690 139.24 110.25 116.64 104.04 112.36 108.16 63.810 88.36 96.04 92.16 77.44 106.09 98.01 63.930 81.00 79.21 108.16 75.69 100.00 100.00 64.050 77.44 82.81 88.36 70.56 68.89 75.69 64.170 86.49 84.64 94.09 102.01 108.16 136.89 64.290 123.21 125.44 129.96 144.00 174.24 207.36 64.410 190.44 196.00 246.49 184.96 259.21 210.25 64.530 225.00 187.69 193.21 193.21 187.69 166.41 64.650 201.64 166.41 153.76 166.41 153.76 144.00 64.770 134.56 104.04 148.84 123.21 125.44 144.00 64.890 144.00 148.84 158.76 146.41 166.41 182.25 65.010 182.25 193.21 231.04 231.04 240.25 228.01 65.130 231.04 222.01 222.01 213.16 201.64 198.81 65.250 196.00 179.56 174.24 158.76 148.84 134.56 65.370 127.69 127.69 121.00 112.36 98.01 110.25 65.490 112.36 72.25 72.25 106.09 90.25 88.36 65.610 94.09 96.04 77.44 73.96 81.00 98.01 65.730 94.09 98.01 86.49 106.09 96.04 100.00 65.850 86.49 114.49 127.69 129.96 132.25 151.29 65.970 163.84 146.41 153.76 169.00 161.29 176.89 66.090 174.24 156.25 136.89 134.56 171.61 141.61 66.210 158.76 125.44 114.49 112.36 106.09 92.16 66.330 94.09 100.00 94.09 77.44 84.64 68.89 66.450 82.81 75.69 67.24 64.00 67.24 72.25 66.570 70.56 60.84 65.61 65.61 64.00 79.21 66.690 56.25 67.24 68.89 59.29 56.25 70.56 66.810 77.44 59.29 73.96 75.69 65.61 88.36 66.930 96.04 104.04 98.01 98.01 110.25 100.00 67.050 98.01 127.69 127.69 144.00 148.84 169.00 67.170 169.00 198.81 222.01 246.49 272.25 299.29 67.290 309.76 353.44 392.04 400.00 424.36 384.16 67.410 376.36 334.89 309.76 302.76 320.41 289.00 67.530 275.56 299.29 249.64 237.16 243.36 222.01 67.650 198.81 174.24 163.84 148.84 116.64 102.01

255

File: JC14.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 98.01 90.25 108.16 102.01 92.16 92.16 67.890 77.44 86.49 77.44 84.64 77.44 73.96 68.010 75.69 67.24 81.00 81.00 51.84 67.24 68.130 57.76 67.24 60.84 67.24 68.89 67.24 68.250 62.41 72.25 65.61 54.76 75.69 60.84 68.370 59.29 62.41 47.61 46.24 56.25 53.29 68.490 50.41 50.41 56.25 51.84 56.25 39.69 68.610 53.29 40.96 54.76 56.25 57.76 42.25 68.730 42.25 50.41 53.29 50.41 37.21 50.41 68.850 59.29 50.41 57.76 44.89 56.25 50.41 68.970 36.00 49.00 56.25 65.61 47.61 56.25 69.090 53.29 62.41 56.25 44.89 36.00 43.56 69.210 43.56 47.61 43.56 39.69 46.24 43.56 69.330 51.84 47.61 56.25 53.29 43.56 39.69 69.450 54.76 53.29 59.29 40.96 50.41 53.29 69.570 53.29 50.41 56.25 70.56 56.25 50.41 69.690 51.84 77.44 49.00 67.24 67.24 62.41 69.810 68.89 68.89 56.25 65.61 92.16 75.69 69.930 82.81 90.25 77.44 81.00 _

256

File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC15 Data measured at: 25-Jan-2011 15:48:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 5776.000 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 104.04 116.64 104.04 100.00 110.25 108.16 2.130 90.25 79.21 84.64 98.01 92.16 84.64 2.250 88.36 81.00 67.24 94.09 86.49 79.21 2.370 86.49 92.16 77.44 70.56 86.49 90.25 2.490 72.25 82.81 67.24 56.25 67.24 75.69 2.610 67.24 60.84 60.84 77.44 73.96 77.44 2.730 62.41 67.24 75.69 60.84 75.69 67.24 2.850 75.69 62.41 62.41 65.61 54.76 73.96 2.970 70.56 70.56 59.29 53.29 59.29 67.24 3.090 54.76 77.44 59.29 60.84 56.25 65.61 3.210 62.41 53.29 75.69 54.76 68.89 65.61 3.330 67.24 57.76 62.41 56.25 59.29 67.24 3.450 53.29 62.41 51.84 54.76 51.84 67.24 3.570 47.61 53.29 72.25 53.29 60.84 67.24 3.690 50.41 68.89 65.61 57.76 38.44 62.41 3.810 56.25 59.29 53.29 50.41 79.21 59.29 3.930 59.29 62.41 39.69 47.61 53.29 54.76 4.050 50.41 53.29 60.84 59.29 49.00 62.41 4.170 49.00 53.29 50.41 47.61 43.56 51.84 4.290 50.41 50.41 50.41 49.00 60.84 54.76 4.410 53.29 60.84 53.29 62.41 50.41 51.84 4.530 43.56 56.25 72.25 49.00 56.25 56.25 4.650 43.56 56.25 62.41 40.96 47.61 59.29 4.770 53.29 50.41 72.25 62.41 51.84 65.61 4.890 56.25 56.25 56.25 53.29 49.00 42.25 5.010 59.29 59.29 68.89 46.24 65.61 47.61 5.130 65.61 54.76 59.29 59.29 57.76 56.25 5.250 51.84 47.61 59.29 46.24 51.84 57.76

257

File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 57.76 62.41 62.41 60.84 51.84 50.41 5.490 62.41 50.41 49.00 59.29 47.61 56.25 5.610 56.25 62.41 42.25 67.24 56.25 77.44 5.730 51.84 39.69 50.41 56.25 56.25 50.41 5.850 67.24 54.76 49.00 67.24 42.25 51.84 5.970 62.41 56.25 49.00 43.56 65.61 43.56 6.090 56.25 47.61 59.29 62.41 51.84 50.41 6.210 53.29 54.76 53.29 56.25 51.84 44.89 6.330 53.29 51.84 46.24 59.29 70.56 47.61 6.450 51.84 59.29 50.41 50.41 67.24 40.96 6.570 56.25 46.24 46.24 59.29 47.61 43.56 6.690 54.76 44.89 37.21 64.00 43.56 42.25 6.810 50.41 57.76 44.89 60.84 56.25 47.61 6.930 43.56 49.00 47.61 54.76 46.24 44.89 7.050 56.25 56.25 49.00 57.76 43.56 43.56 7.170 44.89 53.29 53.29 47.61 42.25 51.84 7.290 46.24 57.76 42.25 57.76 64.00 44.89 7.410 53.29 59.29 50.41 56.25 53.29 38.44 7.530 47.61 51.84 59.29 50.41 53.29 50.41 7.650 47.61 50.41 53.29 40.96 53.29 51.84 7.770 49.00 44.89 40.96 47.61 51.84 64.00 7.890 43.56 50.41 43.56 56.25 59.29 50.41 8.010 53.29 46.24 53.29 60.84 46.24 53.29 8.130 49.00 47.61 57.76 56.25 34.81 50.41 8.250 38.44 59.29 43.56 60.84 53.29 53.29 8.370 39.69 53.29 50.41 60.84 46.24 64.00 8.490 32.49 53.29 43.56 53.29 46.24 60.84 8.610 42.25 53.29 38.44 53.29 49.00 44.89 8.730 37.21 50.41 46.24 39.69 57.76 53.29 8.850 57.76 40.96 47.61 36.00 56.25 38.44 8.970 47.61 38.44 59.29 43.56 62.41 47.61 9.090 46.24 39.69 40.96 40.96 47.61 53.29 9.210 53.29 56.25 34.81 37.21 46.24 54.76 9.330 39.69 47.61 47.61 47.61 51.84 53.29 9.450 42.25 29.16 43.56 49.00 49.00 59.29 9.570 38.44 51.84 37.21 59.29 50.41 43.56 9.690 47.61 44.89 50.41 50.41 53.29 40.96 9.810 44.89 51.84 47.61 50.41 46.24 37.21 9.930 43.56 44.89 60.84 34.81 49.00 49.00 10.050 53.29 53.29 34.81 34.81 50.41 44.89 10.170 50.41 44.89 37.21 47.61 46.24 56.25 10.290 46.24 44.89 50.41 43.56 47.61 49.00 10.410 44.89 42.25 43.56 44.89 42.25 30.25 10.530 43.56 56.25 46.24 47.61 43.56 38.44 10.650 57.76 43.56 43.56 56.25 46.24 40.96 10.770 33.64 49.00 50.41 38.44 43.56 43.56 10.890 40.96 37.21 38.44 43.56 42.25 56.25 11.010 43.56 32.49 36.00 44.89 47.61 47.61 11.130 39.69 43.56 43.56 38.44 31.36 44.89 11.250 37.21 53.29 38.44 62.41 39.69 47.61 11.370 34.81 46.24 53.29 38.44 59.29 42.25 11.490 44.89 40.96 47.61 32.49 47.61 38.44

258

File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 34.81 44.89 43.56 47.61 38.44 49.00 11.730 51.84 62.41 57.76 47.61 47.61 47.61 11.850 44.89 51.84 51.84 38.44 40.96 42.25 11.970 39.69 42.25 50.41 53.29 47.61 56.25 12.090 38.44 47.61 40.96 38.44 47.61 53.29 12.210 38.44 44.89 50.41 43.56 46.24 37.21 12.330 47.61 40.96 47.61 50.41 50.41 34.81 12.450 43.56 39.69 53.29 50.41 51.84 44.89 12.570 43.56 33.64 46.24 34.81 33.64 32.49 12.690 49.00 32.49 44.89 43.56 31.36 46.24 12.810 34.81 43.56 37.21 40.96 49.00 43.56 12.930 42.25 46.24 50.41 38.44 39.69 44.89 13.050 32.49 43.56 40.96 42.25 56.25 47.61 13.170 42.25 38.44 44.89 38.44 29.16 37.21 13.290 38.44 32.49 29.16 38.44 43.56 33.64 13.410 49.00 28.09 40.96 36.00 36.00 38.44 13.530 46.24 43.56 38.44 32.49 43.56 43.56 13.650 38.44 32.49 47.61 46.24 39.69 46.24 13.770 33.64 50.41 49.00 53.29 46.24 30.25 13.890 49.00 40.96 56.25 36.00 38.44 30.25 14.010 47.61 42.25 32.49 39.69 40.96 40.96 14.130 42.25 38.44 53.29 39.69 32.49 33.64 14.250 29.16 51.84 51.84 53.29 56.25 46.24 14.370 32.49 44.89 50.41 39.69 42.25 33.64 14.490 30.25 39.69 50.41 24.01 37.21 32.49 14.610 32.49 39.69 32.49 43.56 33.64 49.00 14.730 39.69 54.76 31.36 44.89 43.56 31.36 14.850 43.56 43.56 47.61 40.96 53.29 47.61 14.970 43.56 40.96 42.25 40.96 50.41 46.24 15.090 40.96 36.00 59.29 47.61 42.25 33.64 15.210 28.09 42.25 51.84 43.56 47.61 47.61 15.330 51.84 32.49 36.00 44.89 56.25 43.56 15.450 53.29 38.44 53.29 44.89 38.44 50.41 15.570 38.44 50.41 47.61 53.29 65.61 51.84 15.690 51.84 68.89 53.29 53.29 62.41 44.89 15.810 62.41 50.41 56.25 51.84 56.25 53.29 15.930 38.44 43.56 53.29 39.69 59.29 54.76 16.050 49.00 47.61 51.84 38.44 47.61 49.00 16.170 53.29 37.21 43.56 47.61 38.44 49.00 16.290 44.89 53.29 47.61 40.96 42.25 32.49 16.410 53.29 47.61 53.29 56.25 44.89 47.61 16.530 54.76 47.61 50.41 49.00 49.00 42.25 16.650 47.61 40.96 43.56 47.61 40.96 36.00 16.770 37.21 33.64 46.24 39.69 40.96 42.25 16.890 37.21 43.56 40.96 50.41 42.25 49.00 17.010 34.81 50.41 38.44 50.41 47.61 47.61 17.130 46.24 32.49 38.44 49.00 33.64 40.96 17.250 38.44 42.25 33.64 38.44 38.44 37.21 17.370 53.29 38.44 36.00 43.56 40.96 34.81 17.490 26.01 38.44 36.00 46.24 37.21 40.96 17.610 39.69 46.24 43.56 34.81 47.61 36.00 17.730 42.25 31.36 40.96 47.61 43.56 36.00

259

File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 40.96 38.44 47.61 38.44 37.21 38.44 17.970 38.44 37.21 46.24 43.56 34.81 32.49 18.090 36.00 32.49 56.25 31.36 43.56 42.25 18.210 33.64 42.25 36.00 43.56 37.21 30.25 18.330 28.09 37.21 38.44 38.44 46.24 47.61 18.450 43.56 40.96 38.44 39.69 37.21 32.49 18.570 38.44 56.25 33.64 50.41 38.44 43.56 18.690 56.25 46.24 40.96 39.69 43.56 40.96 18.810 51.84 34.81 44.89 34.81 34.81 32.49 18.930 39.69 40.96 50.41 40.96 47.61 47.61 19.050 44.89 47.61 42.25 46.24 43.56 30.25 19.170 34.81 43.56 43.56 38.44 53.29 33.64 19.290 53.29 32.49 38.44 38.44 38.44 39.69 19.410 47.61 38.44 31.36 37.21 65.61 38.44 19.530 43.56 27.04 42.25 56.25 40.96 42.25 19.650 31.36 47.61 42.25 39.69 38.44 51.84 19.770 27.04 50.41 37.21 30.25 43.56 43.56 19.890 40.96 34.81 32.49 38.44 40.96 43.56 20.010 44.89 47.61 50.41 47.61 42.25 43.56 20.130 38.44 43.56 39.69 32.49 49.00 36.00 20.250 43.56 38.44 32.49 47.61 32.49 46.24 20.370 40.96 37.21 29.16 47.61 47.61 43.56 20.490 32.49 44.89 40.96 50.41 47.61 47.61 20.610 44.89 38.44 46.24 42.25 54.76 43.56 20.730 34.81 50.41 54.76 46.24 47.61 47.61 20.850 57.76 67.24 72.25 62.41 65.61 56.25 20.970 56.25 47.61 34.81 36.00 43.56 43.56 21.090 46.24 53.29 46.24 44.89 40.96 37.21 21.210 38.44 37.21 43.56 32.49 32.49 39.69 21.330 32.49 43.56 39.69 39.69 40.96 47.61 21.450 39.69 43.56 47.61 36.00 50.41 29.16 21.570 43.56 53.29 40.96 43.56 47.61 50.41 21.690 34.81 46.24 50.41 38.44 40.96 47.61 21.810 42.25 57.76 36.00 57.76 53.29 54.76 21.930 64.00 75.69 96.04 121.00 121.00 125.44 22.050 132.25 94.09 96.04 84.64 81.00 79.21 22.170 59.29 64.00 49.00 59.29 53.29 46.24 22.290 51.84 53.29 42.25 39.69 32.49 56.25 22.410 38.44 40.96 44.89 28.09 49.00 53.29 22.530 30.25 37.21 51.84 31.36 40.96 49.00 22.650 32.49 47.61 37.21 47.61 39.69 38.44 22.770 47.61 53.29 38.44 32.49 50.41 59.29 22.890 53.29 38.44 49.00 56.25 39.69 39.69 23.010 40.96 47.61 36.00 34.81 38.44 47.61 23.130 39.69 25.00 47.61 39.69 38.44 44.89 23.250 40.96 44.89 34.81 38.44 37.21 32.49 23.370 38.44 32.49 40.96 46.24 43.56 33.64 23.490 38.44 39.69 38.44 39.69 51.84 49.00 23.610 43.56 40.96 49.00 50.41 56.25 43.56 23.730 60.84 59.29 49.00 65.61 75.69 68.89 23.850 88.36 77.44 86.49 106.09 118.81 125.44 23.970 114.49 169.00 146.41 207.36 213.16 196.00

260

File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 201.64 207.36 198.81 174.24 161.29 136.89 24.210 96.04 94.09 84.64 62.41 65.61 53.29 24.330 62.41 56.25 33.64 56.25 57.76 44.89 24.450 40.96 39.69 51.84 30.25 38.44 38.44 24.570 37.21 47.61 40.96 43.56 39.69 37.21 24.690 43.56 40.96 38.44 47.61 33.64 38.44 24.810 40.96 38.44 37.21 38.44 47.61 32.49 24.930 54.76 27.04 36.00 36.00 32.49 30.25 25.050 30.25 38.44 42.25 32.49 43.56 39.69 25.170 40.96 43.56 30.25 26.01 43.56 38.44 25.290 27.04 37.21 37.21 42.25 40.96 60.84 25.410 44.89 38.44 38.44 38.44 42.25 32.49 25.530 32.49 31.36 36.00 29.16 37.21 36.00 25.650 43.56 33.64 33.64 32.49 44.89 31.36 25.770 42.25 47.61 39.69 39.69 38.44 27.04 25.890 51.84 23.04 49.00 43.56 39.69 38.44 26.010 33.64 34.81 38.44 39.69 37.21 24.01 26.130 38.44 38.44 50.41 36.00 43.56 32.49 26.250 40.96 40.96 54.76 34.81 49.00 47.61 26.370 43.56 38.44 46.24 50.41 43.56 51.84 26.490 50.41 42.25 77.44 70.56 88.36 112.36 26.610 139.24 184.96 222.01 249.64 225.00 187.69 26.730 158.76 110.25 81.00 72.25 62.41 42.25 26.850 43.56 50.41 43.56 44.89 38.44 38.44 26.970 43.56 33.64 50.41 38.44 46.24 40.96 27.090 42.25 40.96 34.81 46.24 44.89 33.64 27.210 32.49 34.81 27.04 38.44 34.81 34.81 27.330 38.44 33.64 30.25 43.56 38.44 33.64 27.450 37.21 53.29 38.44 38.44 36.00 38.44 27.570 36.00 38.44 43.56 40.96 30.25 33.64 27.690 44.89 27.04 37.21 30.25 31.36 32.49 27.810 37.21 29.16 39.69 38.44 36.00 28.09 27.930 37.21 46.24 22.09 28.09 29.16 38.44 28.050 33.64 30.25 40.96 42.25 32.49 38.44 28.170 38.44 34.81 21.16 32.49 24.01 42.25 28.290 38.44 47.61 40.96 43.56 38.44 39.69 28.410 32.49 40.96 39.69 29.16 40.96 38.44 28.530 40.96 38.44 38.44 42.25 44.89 43.56 28.650 38.44 42.25 40.96 34.81 34.81 38.44 28.770 33.64 42.25 32.49 51.84 34.81 53.29 28.890 57.76 44.89 42.25 37.21 40.96 62.41 29.010 42.25 49.00 32.49 43.56 49.00 37.21 29.130 50.41 44.89 42.25 56.25 51.84 42.25 29.250 62.41 50.41 40.96 51.84 44.89 57.76 29.370 70.56 75.69 50.41 57.76 59.29 65.61 29.490 59.29 62.41 53.29 65.61 62.41 50.41 29.610 79.21 50.41 57.76 53.29 60.84 65.61 29.730 59.29 46.24 57.76 53.29 46.24 51.84 29.850 62.41 59.29 72.25 79.21 73.96 82.81 29.970 59.29 72.25 73.96 79.21 94.09 73.96 30.090 77.44 92.16 100.00 96.04 94.09 96.04 30.210 96.04 110.25 118.81 129.96 134.56 148.84

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 156.25 132.25 193.21 196.00 201.64 219.04 30.450 228.01 268.96 299.29 299.29 320.41 349.69 30.570 424.36 445.21 515.29 533.61 640.09 650.25 30.690 739.84 948.64 1082.41 1267.36 1451.61 1722.25 30.810 1953.64 2381.44 2894.44 3433.96 3943.84 4692.25 30.930 5112.25 5505.64 5776.00 5520.49 5112.25 4719.69 31.050 3943.84 3457.44 2992.09 2304.00 1857.61 1497.69 31.170 1232.01 1075.84 924.16 806.56 670.81 635.04 31.290 547.56 457.96 420.25 353.44 338.56 327.61 31.410 289.00 265.69 240.25 222.01 222.01 193.21 31.530 153.76 176.89 129.96 127.69 132.25 129.96 31.650 129.96 129.96 100.00 110.25 102.01 114.49 31.770 81.00 82.81 106.09 79.21 90.25 84.64 31.890 84.64 82.81 70.56 88.36 77.44 67.24 32.010 56.25 72.25 67.24 73.96 75.69 53.29 32.130 70.56 40.96 62.41 65.61 68.89 56.25 32.250 59.29 59.29 46.24 56.25 62.41 56.25 32.370 56.25 59.29 44.89 53.29 57.76 53.29 32.490 50.41 51.84 64.00 39.69 47.61 37.21 32.610 62.41 62.41 49.00 53.29 50.41 43.56 32.730 53.29 56.25 47.61 53.29 50.41 50.41 32.850 46.24 50.41 42.25 47.61 42.25 49.00 32.970 42.25 56.25 75.69 62.41 65.61 67.24 33.090 53.29 56.25 60.84 62.41 56.25 72.25 33.210 82.81 77.44 72.25 84.64 100.00 82.81 33.330 108.16 123.21 132.25 153.76 158.76 182.25 33.450 222.01 216.09 275.56 292.41 268.96 306.25 33.570 306.25 313.29 292.41 234.09 216.09 198.81 33.690 171.61 148.84 129.96 121.00 102.01 90.25 33.810 77.44 70.56 70.56 81.00 67.24 77.44 33.930 70.56 53.29 56.25 53.29 50.41 43.56 34.050 44.89 50.41 43.56 46.24 50.41 43.56 34.170 47.61 50.41 43.56 38.44 42.25 59.29 34.290 39.69 43.56 37.21 38.44 51.84 44.89 34.410 43.56 46.24 46.24 44.89 43.56 54.76 34.530 40.96 36.00 43.56 42.25 38.44 30.25 34.650 44.89 47.61 44.89 42.25 51.84 50.41 34.770 43.56 56.25 38.44 54.76 60.84 59.29 34.890 70.56 65.61 72.25 56.25 72.25 70.56 35.010 77.44 57.76 81.00 90.25 102.01 90.25 35.130 118.81 127.69 132.25 132.25 163.84 198.81 35.250 198.81 237.16 231.04 249.64 243.36 265.69 35.370 256.00 237.16 201.64 210.25 182.25 176.89 35.490 127.69 125.44 94.09 108.16 92.16 92.16 35.610 84.64 67.24 75.69 65.61 62.41 68.89 35.730 62.41 59.29 51.84 53.29 56.25 44.89 35.850 49.00 43.56 54.76 46.24 59.29 47.61 35.970 38.44 54.76 42.25 56.25 44.89 44.89 36.090 37.21 50.41 43.56 46.24 44.89 46.24 36.210 59.29 50.41 50.41 32.49 42.25 44.89 36.330 53.29 59.29 28.09 53.29 47.61 32.49 36.450 54.76 42.25 49.00 53.29 60.84 53.29

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File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 57.76 47.61 57.76 67.24 59.29 75.69 36.690 64.00 64.00 70.56 65.61 77.44 90.25 36.810 84.64 82.81 82.81 88.36 98.01 102.01 36.930 94.09 121.00 98.01 108.16 134.56 139.24 37.050 112.36 139.24 136.89 141.61 163.84 151.29 37.170 171.61 196.00 204.49 243.36 252.81 309.76 37.290 327.61 372.49 424.36 392.04 479.61 466.56 37.410 453.69 392.04 392.04 361.00 349.69 309.76 37.530 262.44 243.36 196.00 190.44 163.84 146.41 37.650 129.96 123.21 96.04 88.36 104.04 114.49 37.770 94.09 84.64 75.69 82.81 59.29 75.69 37.890 72.25 75.69 54.76 70.56 60.84 47.61 38.010 65.61 57.76 50.41 67.24 50.41 47.61 38.130 47.61 54.76 64.00 47.61 50.41 33.64 38.250 53.29 51.84 50.41 49.00 56.25 50.41 38.370 47.61 34.81 42.25 43.56 56.25 40.96 38.490 40.96 38.44 39.69 38.44 49.00 34.81 38.610 53.29 50.41 46.24 36.00 38.44 42.25 38.730 53.29 46.24 43.56 43.56 62.41 39.69 38.850 50.41 42.25 39.69 47.61 37.21 51.84 38.970 57.76 47.61 57.76 59.29 38.44 43.56 39.090 37.21 51.84 54.76 47.61 39.69 51.84 39.210 50.41 51.84 59.29 51.84 49.00 50.41 39.330 51.84 50.41 56.25 54.76 50.41 57.76 39.450 81.00 62.41 70.56 72.25 75.69 67.24 39.570 64.00 75.69 67.24 53.29 88.36 77.44 39.690 77.44 88.36 90.25 98.01 98.01 116.64 39.810 110.25 112.36 102.01 98.01 100.00 127.69 39.930 118.81 123.21 108.16 114.49 123.21 108.16 40.050 108.16 110.25 104.04 94.09 79.21 77.44 40.170 77.44 82.81 82.81 65.61 67.24 65.61 40.290 68.89 62.41 84.64 79.21 75.69 82.81 40.410 72.25 86.49 82.81 92.16 94.09 86.49 40.530 88.36 86.49 114.49 106.09 116.64 118.81 40.650 125.44 123.21 148.84 166.41 161.29 176.89 40.770 198.81 234.09 249.64 243.36 302.76 331.24 40.890 338.56 408.04 475.24 510.76 561.69 660.49 41.010 778.41 835.21 985.96 1095.61 1162.81 1339.56 41.130 1332.25 1303.21 1332.25 1361.61 1267.36 1190.25 41.250 1089.00 961.00 846.81 817.96 585.64 610.09 41.370 488.41 380.25 338.56 331.24 331.24 237.16 41.490 252.81 176.89 219.04 196.00 179.56 169.00 41.610 134.56 144.00 139.24 141.61 108.16 112.36 41.730 110.25 100.00 62.41 79.21 86.49 73.96 41.850 77.44 84.64 77.44 50.41 62.41 56.25 41.970 70.56 70.56 68.89 53.29 62.41 79.21 42.090 70.56 49.00 50.41 54.76 65.61 59.29 42.210 50.41 65.61 38.44 60.84 42.25 53.29 42.330 59.29 49.00 53.29 70.56 70.56 62.41 42.450 49.00 50.41 56.25 56.25 57.76 56.25 42.570 50.41 40.96 53.29 47.61 47.61 37.21 42.690 38.44 42.25 57.76 46.24 47.61 38.44

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File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 50.41 43.56 53.29 59.29 59.29 53.29 42.930 59.29 44.89 59.29 59.29 44.89 51.84 43.050 57.76 56.25 59.29 70.56 42.25 65.61 43.170 67.24 70.56 62.41 54.76 56.25 67.24 43.290 53.29 57.76 65.61 64.00 72.25 75.69 43.410 70.56 77.44 72.25 70.56 82.81 77.44 43.530 72.25 86.49 92.16 114.49 132.25 144.00 43.650 144.00 125.44 171.61 163.84 201.64 237.16 43.770 256.00 246.49 219.04 216.09 216.09 198.81 43.890 222.01 171.61 153.76 174.24 151.29 144.00 44.010 132.25 108.16 102.01 106.09 94.09 84.64 44.130 86.49 94.09 88.36 75.69 100.00 116.64 44.250 86.49 77.44 94.09 75.69 90.25 86.49 44.370 81.00 88.36 102.01 84.64 98.01 102.01 44.490 112.36 116.64 100.00 127.69 129.96 153.76 44.610 176.89 139.24 171.61 207.36 243.36 256.00 44.730 272.25 268.96 342.25 361.00 453.69 506.25 44.850 542.89 665.64 745.29 745.29 812.25 829.44 44.970 795.24 718.24 691.69 686.44 650.25 561.69 45.090 484.00 466.56 392.04 338.56 316.84 265.69 45.210 231.04 196.00 196.00 182.25 176.89 161.29 45.330 156.25 116.64 116.64 136.89 110.25 102.01 45.450 82.81 92.16 90.25 90.25 88.36 75.69 45.570 82.81 67.24 56.25 70.56 65.61 70.56 45.690 60.84 59.29 62.41 43.56 60.84 70.56 45.810 72.25 62.41 49.00 72.25 53.29 67.24 45.930 59.29 70.56 50.41 60.84 56.25 44.89 46.050 65.61 82.81 56.25 44.89 65.61 62.41 46.170 57.76 57.76 60.84 70.56 67.24 72.25 46.290 59.29 67.24 65.61 67.24 62.41 67.24 46.410 62.41 70.56 64.00 57.76 75.69 56.25 46.530 73.96 82.81 75.69 88.36 75.69 72.25 46.650 62.41 67.24 72.25 60.84 60.84 70.56 46.770 64.00 62.41 65.61 59.29 51.84 68.89 46.890 54.76 53.29 42.25 56.25 43.56 42.25 47.010 53.29 60.84 54.76 53.29 54.76 49.00 47.130 31.36 47.61 47.61 49.00 43.56 53.29 47.250 44.89 42.25 47.61 42.25 40.96 51.84 47.370 51.84 47.61 46.24 56.25 47.61 51.84 47.490 46.24 67.24 50.41 50.41 42.25 56.25 47.610 62.41 42.25 50.41 38.44 56.25 38.44 47.730 53.29 47.61 47.61 37.21 38.44 51.84 47.850 44.89 60.84 50.41 53.29 51.84 50.41 47.970 40.96 53.29 50.41 42.25 46.24 46.24 48.090 50.41 46.24 53.29 56.25 50.41 56.25 48.210 65.61 56.25 50.41 60.84 47.61 46.24 48.330 57.76 62.41 60.84 54.76 56.25 68.89 48.450 62.41 70.56 62.41 65.61 59.29 50.41 48.570 44.89 62.41 77.44 68.89 59.29 67.24 48.690 68.89 79.21 67.24 70.56 62.41 60.84 48.810 82.81 86.49 86.49 98.01 90.25 108.16 48.930 106.09 106.09 104.04 118.81 121.00 132.25

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Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 108.16 151.29 134.56 169.00 139.24 174.24 49.170 193.21 196.00 234.09 237.16 252.81 231.04 49.290 278.89 246.49 265.69 219.04 240.25 216.09 49.410 216.09 174.24 182.25 201.64 182.25 158.76 49.530 158.76 153.76 132.25 144.00 108.16 125.44 49.650 132.25 116.64 121.00 123.21 127.69 129.96 49.770 125.44 141.61 123.21 144.00 136.89 136.89 49.890 161.29 156.25 161.29 139.24 153.76 176.89 50.010 184.96 198.81 231.04 219.04 198.81 228.01 50.130 259.21 299.29 292.41 299.29 313.29 295.84 50.250 342.25 466.56 412.09 484.00 515.29 497.29 50.370 600.25 620.01 707.56 745.29 829.44 936.36 50.490 948.64 1049.76 1011.24 1056.25 1056.25 973.44 50.610 979.69 985.96 912.04 870.25 912.04 823.69 50.730 756.25 739.84 729.00 707.56 761.76 707.56 50.850 718.24 756.25 750.76 846.81 846.81 961.00 50.970 876.16 1030.41 1011.24 1095.61 1024.00 1102.24 51.090 1082.41 1115.56 1049.76 1017.61 961.00 906.01 51.210 876.16 870.25 772.84 739.84 655.36 625.00 51.330 519.84 524.41 457.96 445.21 384.16 353.44 51.450 299.29 295.84 289.00 275.56 256.00 249.64 51.570 193.21 190.44 190.44 136.89 161.29 158.76 51.690 151.29 125.44 148.84 123.21 110.25 121.00 51.810 112.36 94.09 104.04 116.64 94.09 90.25 51.930 81.00 86.49 79.21 84.64 92.16 82.81 52.050 86.49 90.25 72.25 72.25 59.29 75.69 52.170 86.49 68.89 65.61 65.61 86.49 65.61 52.290 77.44 47.61 77.44 70.56 65.61 77.44 52.410 75.69 56.25 62.41 64.00 64.00 62.41 52.530 47.61 79.21 60.84 56.25 50.41 46.24 52.650 60.84 50.41 54.76 53.29 59.29 49.00 52.770 43.56 59.29 54.76 50.41 46.24 56.25 52.890 50.41 37.21 32.49 43.56 46.24 56.25 53.010 57.76 47.61 37.21 47.61 59.29 46.24 53.130 49.00 49.00 50.41 56.25 57.76 44.89 53.250 53.29 47.61 44.89 40.96 42.25 40.96 53.370 40.96 53.29 39.69 56.25 32.49 50.41 53.490 50.41 50.41 44.89 47.61 33.64 43.56 53.610 47.61 39.69 32.49 38.44 46.24 44.89 53.730 31.36 50.41 59.29 40.96 43.56 43.56 53.850 50.41 43.56 38.44 38.44 38.44 31.36 53.970 46.24 43.56 39.69 53.29 47.61 32.49 54.090 34.81 38.44 44.89 46.24 43.56 24.01 54.210 38.44 39.69 32.49 38.44 32.49 47.61 54.330 50.41 44.89 43.56 40.96 38.44 29.16 54.450 32.49 38.44 51.84 40.96 46.24 40.96 54.570 39.69 44.89 42.25 44.89 33.64 46.24 54.690 27.04 40.96 30.25 47.61 40.96 29.16 54.810 56.25 46.24 56.25 53.29 56.25 47.61 54.930 53.29 44.89 38.44 57.76 44.89 40.96 55.050 43.56 50.41 27.04 38.44 39.69 38.44 55.170 50.41 46.24 42.25 32.49 50.41 44.89

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File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 51.84 33.64 39.69 38.44 34.81 43.56 55.410 38.44 37.21 32.49 31.36 36.00 36.00 55.530 43.56 42.25 43.56 36.00 29.16 39.69 55.650 33.64 34.81 33.64 34.81 38.44 50.41 55.770 32.49 34.81 40.96 42.25 50.41 31.36 55.890 42.25 38.44 40.96 30.25 39.69 37.21 56.010 31.36 37.21 43.56 47.61 38.44 39.69 56.130 47.61 37.21 38.44 32.49 34.81 50.41 56.250 40.96 32.49 37.21 42.25 42.25 29.16 56.370 43.56 46.24 32.49 29.16 31.36 39.69 56.490 39.69 40.96 38.44 37.21 40.96 33.64 56.610 38.44 43.56 37.21 34.81 43.56 25.00 56.730 44.89 28.09 37.21 42.25 43.56 43.56 56.850 38.44 38.44 40.96 38.44 40.96 47.61 56.970 37.21 39.69 32.49 38.44 39.69 40.96 57.090 38.44 33.64 43.56 33.64 32.49 43.56 57.210 32.49 32.49 39.69 50.41 30.25 43.56 57.330 37.21 39.69 43.56 47.61 37.21 39.69 57.450 46.24 31.36 43.56 38.44 40.96 32.49 57.570 43.56 43.56 32.49 33.64 34.81 43.56 57.690 47.61 46.24 53.29 39.69 42.25 46.24 57.810 56.25 32.49 34.81 42.25 46.24 47.61 57.930 47.61 42.25 53.29 51.84 57.76 47.61 58.050 46.24 43.56 47.61 49.00 54.76 53.29 58.170 40.96 50.41 72.25 50.41 54.76 56.25 58.290 60.84 54.76 65.61 64.00 64.00 57.76 58.410 62.41 68.89 73.96 68.89 67.24 73.96 58.530 70.56 90.25 90.25 92.16 102.01 125.44 58.650 121.00 118.81 136.89 136.89 161.29 141.61 58.770 187.69 190.44 213.16 201.64 231.04 265.69 58.890 237.16 219.04 243.36 228.01 210.25 225.00 59.010 222.01 201.64 193.21 198.81 169.00 166.41 59.130 174.24 153.76 146.41 125.44 132.25 141.61 59.250 136.89 136.89 118.81 134.56 148.84 114.49 59.370 146.41 139.24 125.44 139.24 161.29 169.00 59.490 174.24 158.76 184.96 198.81 213.16 207.36 59.610 252.81 265.69 265.69 306.25 299.29 316.84 59.730 384.16 420.25 428.49 412.09 408.04 432.64 59.850 420.25 428.49 372.49 364.81 357.21 368.64 59.970 364.81 306.25 331.24 289.00 262.44 243.36 60.090 198.81 193.21 176.89 190.44 144.00 125.44 60.210 153.76 153.76 144.00 106.09 108.16 94.09 60.330 106.09 94.09 79.21 90.25 90.25 77.44 60.450 79.21 98.01 64.00 65.61 65.61 68.89 60.570 67.24 62.41 54.76 59.29 65.61 79.21 60.690 54.76 51.84 46.24 60.84 57.76 51.84 60.810 50.41 51.84 42.25 51.84 50.41 57.76 60.930 50.41 68.89 50.41 53.29 44.89 50.41 61.050 43.56 36.00 51.84 50.41 51.84 53.29 61.170 53.29 67.24 46.24 46.24 53.29 51.84 61.290 54.76 56.25 59.29 47.61 64.00 59.29 61.410 49.00 50.41 43.56 51.84 53.29 47.61

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File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 59.29 44.89 67.24 51.84 38.44 59.29 61.650 56.25 47.61 68.89 62.41 59.29 60.84 61.770 67.24 67.24 65.61 82.81 62.41 67.24 61.890 72.25 67.24 84.64 65.61 75.69 67.24 62.010 84.64 114.49 100.00 82.81 79.21 81.00 62.130 88.36 70.56 60.84 82.81 70.56 64.00 62.250 70.56 73.96 70.56 59.29 64.00 53.29 62.370 64.00 65.61 53.29 79.21 50.41 64.00 62.490 53.29 53.29 56.25 50.41 59.29 54.76 62.610 62.41 56.25 68.89 51.84 50.41 65.61 62.730 65.61 67.24 70.56 84.64 75.69 75.69 62.850 67.24 86.49 96.04 79.21 90.25 112.36 62.970 92.16 96.04 100.00 100.00 110.25 125.44 63.090 127.69 110.25 125.44 132.25 156.25 169.00 63.210 171.61 225.00 216.09 237.16 231.04 256.00 63.330 252.81 302.76 313.29 361.00 320.41 331.24 63.450 331.24 331.24 338.56 299.29 306.25 292.41 63.570 265.69 278.89 225.00 240.25 265.69 213.16 63.690 182.25 198.81 163.84 156.25 158.76 132.25 63.810 116.64 144.00 127.69 118.81 127.69 127.69 63.930 94.09 118.81 106.09 118.81 114.49 110.25 64.050 112.36 125.44 100.00 94.09 125.44 121.00 64.170 116.64 116.64 127.69 118.81 110.25 139.24 64.290 158.76 161.29 146.41 148.84 174.24 166.41 64.410 201.64 210.25 225.00 193.21 213.16 210.25 64.530 222.01 219.04 198.81 198.81 196.00 179.56 64.650 201.64 184.96 176.89 153.76 148.84 153.76 64.770 136.89 151.29 176.89 158.76 146.41 156.25 64.890 136.89 161.29 171.61 153.76 182.25 158.76 65.010 193.21 207.36 198.81 184.96 216.09 213.16 65.130 219.04 231.04 207.36 210.25 182.25 231.04 65.250 222.01 184.96 201.64 187.69 171.61 158.76 65.370 182.25 161.29 139.24 144.00 141.61 123.21 65.490 112.36 116.64 121.00 121.00 125.44 110.25 65.610 96.04 100.00 114.49 118.81 121.00 88.36 65.730 110.25 121.00 86.49 116.64 102.01 116.64 65.850 123.21 118.81 106.09 139.24 136.89 161.29 65.970 151.29 166.41 151.29 163.84 169.00 179.56 66.090 136.89 144.00 163.84 136.89 132.25 136.89 66.210 125.44 136.89 139.24 125.44 123.21 118.81 66.330 114.49 125.44 100.00 92.16 98.01 96.04 66.450 92.16 92.16 118.81 82.81 84.64 84.64 66.570 112.36 77.44 96.04 79.21 82.81 75.69 66.690 90.25 79.21 100.00 88.36 79.21 77.44 66.810 88.36 77.44 90.25 108.16 94.09 102.01 66.930 127.69 114.49 116.64 114.49 161.29 127.69 67.050 156.25 169.00 176.89 166.41 174.24 210.25 67.170 187.69 187.69 243.36 272.25 295.84 309.76 67.290 349.69 349.69 396.01 357.21 380.25 368.64 67.410 380.25 368.64 368.64 334.89 364.81 282.24 67.530 345.96 313.29 306.25 289.00 265.69 275.56 67.650 265.69 234.09 196.00 228.01 179.56 161.29

267

File: JC15.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 146.41 163.84 148.84 134.56 127.69 136.89 67.890 116.64 116.64 108.16 82.81 98.01 104.04 68.010 90.25 94.09 92.16 118.81 82.81 77.44 68.130 77.44 73.96 88.36 92.16 86.49 100.00 68.250 84.64 75.69 82.81 75.69 86.49 62.41 68.370 60.84 72.25 56.25 62.41 54.76 64.00 68.490 62.41 47.61 56.25 57.76 47.61 44.89 68.610 60.84 56.25 59.29 50.41 50.41 47.61 68.730 50.41 47.61 70.56 65.61 50.41 47.61 68.850 46.24 47.61 54.76 39.69 38.44 59.29 68.970 50.41 50.41 39.69 51.84 46.24 50.41 69.090 57.76 49.00 54.76 53.29 56.25 57.76 69.210 43.56 53.29 43.56 50.41 50.41 40.96 69.330 42.25 60.84 49.00 42.25 62.41 46.24 69.450 43.56 47.61 72.25 50.41 53.29 62.41 69.570 38.44 50.41 75.69 53.29 59.29 65.61 69.690 62.41 73.96 73.96 68.89 72.25 70.56 69.810 62.41 67.24 70.56 86.49 84.64 86.49 69.930 79.21 77.44 81.00 68.89 _

268

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Sample identification: JC16 Data measured at: 25-Jan-2011 16:46:00

Start angle [ø2é]: 2.010 End angle [ø2é]: 69.990 Step size [ø2é]: 0.020 Maximum intensity: 8010.250 Time per step [s]: 1.000 Type of scan: CONTINUOUS

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

2.010 158.76 148.84 132.25 129.96 132.25 114.49 2.130 125.44 132.25 132.25 136.89 121.00 108.16 2.250 116.64 110.25 100.00 106.09 121.00 102.01 2.370 96.04 94.09 86.49 81.00 88.36 92.16 2.490 84.64 104.04 108.16 77.44 84.64 94.09 2.610 92.16 64.00 75.69 90.25 100.00 60.84 2.730 72.25 81.00 73.96 72.25 94.09 72.25 2.850 84.64 77.44 70.56 68.89 67.24 64.00 2.970 86.49 59.29 65.61 75.69 86.49 92.16 3.090 73.96 84.64 82.81 68.89 65.61 77.44 3.210 64.00 77.44 64.00 54.76 68.89 60.84 3.330 67.24 73.96 53.29 54.76 56.25 56.25 3.450 64.00 72.25 65.61 59.29 56.25 57.76 3.570 84.64 56.25 57.76 53.29 54.76 57.76 3.690 54.76 65.61 73.96 60.84 56.25 65.61 3.810 53.29 51.84 65.61 51.84 54.76 57.76 3.930 65.61 59.29 72.25 72.25 57.76 53.29 4.050 56.25 73.96 56.25 62.41 59.29 62.41 4.170 59.29 56.25 60.84 59.29 59.29 51.84 4.290 54.76 62.41 62.41 57.76 56.25 60.84 4.410 47.61 57.76 56.25 65.61 62.41 67.24 4.530 57.76 54.76 56.25 65.61 57.76 53.29 4.650 59.29 64.00 62.41 56.25 60.84 49.00 4.770 75.69 70.56 49.00 53.29 62.41 56.25 4.890 44.89 65.61 56.25 65.61 59.29 67.24 5.010 68.89 62.41 54.76 62.41 60.84 62.41 5.130 65.61 70.56 47.61 64.00 59.29 56.25 5.250 59.29 62.41 60.84 46.24 57.76 59.29

269

File: JC16.RD 3-Feb-2011 9:12 ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

5.370 79.21 65.61 50.41 47.61 60.84 73.96 5.490 62.41 59.29 67.24 47.61 67.24 50.41 5.610 42.25 60.84 65.61 42.25 50.41 46.24 5.730 56.25 53.29 54.76 49.00 70.56 43.56 5.850 67.24 53.29 65.61 62.41 62.41 53.29 5.970 56.25 57.76 65.61 59.29 57.76 64.00 6.090 53.29 53.29 50.41 67.24 53.29 57.76 6.210 54.76 50.41 59.29 53.29 57.76 51.84 6.330 42.25 59.29 57.76 62.41 46.24 50.41 6.450 54.76 38.44 56.25 46.24 51.84 47.61 6.570 57.76 65.61 47.61 47.61 50.41 53.29 6.690 43.56 53.29 56.25 47.61 39.69 70.56 6.810 50.41 50.41 53.29 44.89 56.25 59.29 6.930 59.29 59.29 50.41 46.24 47.61 46.24 7.050 53.29 43.56 59.29 56.25 54.76 49.00 7.170 36.00 53.29 54.76 59.29 51.84 40.96 7.290 70.56 54.76 59.29 47.61 57.76 54.76 7.410 43.56 62.41 56.25 38.44 51.84 46.24 7.530 49.00 54.76 57.76 49.00 53.29 54.76 7.650 53.29 50.41 49.00 72.25 51.84 56.25 7.770 50.41 47.61 70.56 46.24 62.41 56.25 7.890 50.41 70.56 56.25 47.61 57.76 47.61 8.010 56.25 47.61 59.29 57.76 53.29 60.84 8.130 56.25 50.41 49.00 50.41 57.76 46.24 8.250 39.69 53.29 50.41 37.21 60.84 43.56 8.370 47.61 51.84 38.44 46.24 46.24 49.00 8.490 53.29 50.41 53.29 53.29 54.76 50.41 8.610 53.29 42.25 56.25 51.84 36.00 53.29 8.730 43.56 44.89 60.84 40.96 43.56 43.56 8.850 43.56 43.56 57.76 51.84 40.96 62.41 8.970 39.69 59.29 56.25 50.41 54.76 44.89 9.090 51.84 50.41 57.76 39.69 50.41 47.61 9.210 53.29 44.89 36.00 46.24 38.44 38.44 9.330 46.24 38.44 56.25 44.89 47.61 59.29 9.450 38.44 42.25 38.44 38.44 46.24 47.61 9.570 53.29 49.00 49.00 50.41 43.56 44.89 9.690 68.89 62.41 46.24 47.61 42.25 38.44 9.810 57.76 42.25 47.61 42.25 38.44 40.96 9.930 50.41 43.56 59.29 38.44 47.61 47.61 10.050 47.61 42.25 56.25 42.25 54.76 50.41 10.170 49.00 59.29 53.29 43.56 39.69 43.56 10.290 51.84 43.56 44.89 47.61 56.25 47.61 10.410 43.56 42.25 54.76 38.44 49.00 44.89 10.530 54.76 54.76 38.44 38.44 38.44 56.25 10.650 51.84 59.29 53.29 43.56 49.00 43.56 10.770 43.56 53.29 53.29 39.69 38.44 50.41 10.890 51.84 51.84 50.41 42.25 47.61 49.00 11.010 34.81 36.00 47.61 43.56 47.61 43.56 11.130 43.56 37.21 50.41 46.24 53.29 37.21 11.250 54.76 43.56 53.29 39.69 42.25 50.41 11.370 43.56 38.44 44.89 38.44 42.25 54.76 11.490 43.56 34.81 54.76 38.44 53.29 47.61

270

File: JC16.RD 3-Feb-2011 9:12 ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

11.610 50.41 40.96 53.29 37.21 43.56 47.61 11.730 43.56 49.00 44.89 39.69 38.44 57.76 11.850 50.41 40.96 43.56 38.44 50.41 47.61 11.970 47.61 32.49 44.89 43.56 36.00 50.41 12.090 49.00 44.89 38.44 42.25 56.25 39.69 12.210 38.44 34.81 39.69 34.81 42.25 40.96 12.330 53.29 32.49 39.69 42.25 44.89 37.21 12.450 43.56 37.21 43.56 47.61 47.61 44.89 12.570 50.41 38.44 50.41 47.61 44.89 43.56 12.690 39.69 34.81 40.96 38.44 56.25 38.44 12.810 44.89 46.24 43.56 44.89 34.81 39.69 12.930 40.96 36.00 54.76 44.89 34.81 49.00 13.050 42.25 34.81 53.29 34.81 42.25 43.56 13.170 44.89 38.44 53.29 38.44 32.49 43.56 13.290 39.69 44.89 43.56 42.25 36.00 50.41 13.410 38.44 53.29 51.84 50.41 38.44 28.09 13.530 53.29 38.44 42.25 50.41 46.24 27.04 13.650 47.61 47.61 39.69 34.81 47.61 44.89 13.770 33.64 51.84 33.64 42.25 50.41 28.09 13.890 49.00 38.44 43.56 32.49 32.49 46.24 14.010 39.69 49.00 34.81 37.21 54.76 38.44 14.130 37.21 42.25 42.25 50.41 39.69 30.25 14.250 38.44 32.49 38.44 40.96 44.89 43.56 14.370 47.61 40.96 34.81 50.41 46.24 42.25 14.490 34.81 37.21 38.44 37.21 36.00 33.64 14.610 28.09 38.44 43.56 43.56 40.96 39.69 14.730 39.69 32.49 44.89 47.61 32.49 38.44 14.850 39.69 37.21 34.81 54.76 40.96 43.56 14.970 39.69 43.56 44.89 39.69 49.00 43.56 15.090 46.24 50.41 50.41 53.29 44.89 40.96 15.210 44.89 42.25 50.41 56.25 51.84 42.25 15.330 33.64 46.24 44.89 51.84 62.41 47.61 15.450 46.24 53.29 43.56 59.29 49.00 51.84 15.570 59.29 60.84 49.00 51.84 49.00 50.41 15.690 56.25 54.76 53.29 54.76 44.89 57.76 15.810 59.29 59.29 59.29 50.41 44.89 56.25 15.930 47.61 43.56 53.29 60.84 59.29 65.61 16.050 50.41 50.41 50.41 56.25 57.76 44.89 16.170 56.25 49.00 47.61 50.41 53.29 51.84 16.290 47.61 50.41 56.25 50.41 49.00 50.41 16.410 56.25 39.69 33.64 50.41 51.84 40.96 16.530 40.96 38.44 32.49 57.76 59.29 49.00 16.650 43.56 43.56 38.44 47.61 38.44 47.61 16.770 50.41 60.84 49.00 38.44 42.25 49.00 16.890 47.61 54.76 42.25 56.25 43.56 43.56 17.010 32.49 62.41 37.21 47.61 59.29 43.56 17.130 36.00 37.21 43.56 32.49 37.21 43.56 17.250 34.81 40.96 36.00 47.61 47.61 34.81 17.370 57.76 47.61 53.29 39.69 50.41 37.21 17.490 51.84 38.44 37.21 57.76 38.44 38.44 17.610 47.61 44.89 39.69 33.64 43.56 34.81 17.730 31.36 43.56 32.49 43.56 40.96 32.49

271

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

17.850 46.24 50.41 33.64 28.09 43.56 44.89 17.970 27.04 43.56 40.96 28.09 38.44 39.69 18.090 40.96 44.89 44.89 42.25 40.96 39.69 18.210 32.49 43.56 43.56 39.69 32.49 40.96 18.330 25.00 27.04 43.56 37.21 38.44 44.89 18.450 47.61 51.84 44.89 36.00 38.44 53.29 18.570 38.44 50.41 32.49 40.96 56.25 50.41 18.690 40.96 33.64 38.44 39.69 56.25 38.44 18.810 47.61 37.21 40.96 39.69 39.69 50.41 18.930 43.56 39.69 31.36 33.64 54.76 39.69 19.050 43.56 50.41 38.44 30.25 32.49 47.61 19.170 43.56 38.44 28.09 34.81 33.64 33.64 19.290 33.64 37.21 47.61 39.69 42.25 43.56 19.410 32.49 43.56 44.89 38.44 47.61 51.84 19.530 43.56 56.25 43.56 36.00 28.09 38.44 19.650 50.41 43.56 32.49 43.56 49.00 43.56 19.770 51.84 53.29 37.21 46.24 47.61 50.41 19.890 44.89 32.49 29.16 51.84 42.25 47.61 20.010 51.84 43.56 43.56 43.56 33.64 49.00 20.130 47.61 44.89 37.21 43.56 43.56 33.64 20.250 47.61 43.56 43.56 31.36 44.89 31.36 20.370 53.29 50.41 34.81 38.44 36.00 44.89 20.490 34.81 39.69 38.44 44.89 43.56 50.41 20.610 42.25 39.69 39.69 42.25 44.89 47.61 20.730 56.25 51.84 62.41 73.96 73.96 68.89 20.850 72.25 88.36 47.61 62.41 59.29 59.29 20.970 46.24 49.00 36.00 51.84 44.89 46.24 21.090 37.21 43.56 53.29 47.61 53.29 43.56 21.210 44.89 47.61 51.84 38.44 43.56 42.25 21.330 47.61 38.44 39.69 47.61 47.61 43.56 21.450 56.25 49.00 38.44 50.41 53.29 44.89 21.570 32.49 38.44 49.00 51.84 43.56 38.44 21.690 47.61 40.96 44.89 56.25 43.56 47.61 21.810 53.29 67.24 50.41 68.89 68.89 75.69 21.930 72.25 86.49 96.04 123.21 118.81 112.36 22.050 100.00 108.16 84.64 77.44 59.29 56.25 22.170 56.25 44.89 59.29 56.25 47.61 51.84 22.290 50.41 38.44 47.61 51.84 38.44 40.96 22.410 38.44 31.36 50.41 40.96 47.61 46.24 22.530 44.89 50.41 38.44 40.96 33.64 32.49 22.650 40.96 38.44 37.21 42.25 40.96 50.41 22.770 38.44 37.21 44.89 47.61 34.81 29.16 22.890 43.56 46.24 42.25 43.56 37.21 37.21 23.010 37.21 38.44 43.56 47.61 34.81 38.44 23.130 42.25 32.49 37.21 33.64 47.61 33.64 23.250 37.21 50.41 38.44 34.81 32.49 40.96 23.370 38.44 42.25 40.96 42.25 29.16 36.00 23.490 47.61 43.56 33.64 43.56 43.56 46.24 23.610 38.44 53.29 57.76 59.29 40.96 72.25 23.730 47.61 49.00 62.41 75.69 72.25 84.64 23.850 98.01 94.09 127.69 110.25 146.41 158.76 23.970 182.25 184.96 207.36 204.49 198.81 204.49

272

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

24.090 182.25 184.96 144.00 136.89 114.49 96.04 24.210 94.09 88.36 70.56 90.25 77.44 60.84 24.330 57.76 65.61 39.69 56.25 36.00 47.61 24.450 46.24 50.41 42.25 39.69 59.29 29.16 24.570 56.25 47.61 40.96 51.84 34.81 34.81 24.690 47.61 42.25 37.21 43.56 38.44 34.81 24.810 37.21 47.61 37.21 29.16 43.56 34.81 24.930 47.61 49.00 42.25 38.44 40.96 32.49 25.050 36.00 31.36 34.81 39.69 32.49 32.49 25.170 46.24 47.61 33.64 34.81 28.09 46.24 25.290 38.44 47.61 37.21 44.89 32.49 38.44 25.410 40.96 33.64 43.56 36.00 33.64 33.64 25.530 36.00 34.81 44.89 33.64 47.61 32.49 25.650 43.56 40.96 32.49 32.49 46.24 50.41 25.770 42.25 47.61 31.36 42.25 50.41 47.61 25.890 40.96 34.81 44.89 38.44 31.36 39.69 26.010 27.04 51.84 40.96 42.25 47.61 38.44 26.130 39.69 50.41 38.44 43.56 30.25 36.00 26.250 36.00 38.44 40.96 34.81 36.00 38.44 26.370 38.44 38.44 44.89 59.29 43.56 50.41 26.490 65.61 75.69 82.81 90.25 132.25 127.69 26.610 148.84 187.69 169.00 169.00 108.16 114.49 26.730 84.64 56.25 54.76 38.44 50.41 34.81 26.850 43.56 34.81 33.64 38.44 40.96 53.29 26.970 49.00 57.76 38.44 36.00 38.44 37.21 27.090 38.44 38.44 37.21 31.36 34.81 37.21 27.210 37.21 32.49 46.24 38.44 33.64 38.44 27.330 34.81 32.49 33.64 40.96 32.49 42.25 27.450 43.56 38.44 39.69 42.25 33.64 33.64 27.570 46.24 43.56 44.89 38.44 38.44 43.56 27.690 36.00 32.49 33.64 43.56 47.61 38.44 27.810 34.81 33.64 24.01 53.29 37.21 38.44 27.930 38.44 38.44 31.36 47.61 43.56 39.69 28.050 28.09 50.41 32.49 38.44 28.09 47.61 28.170 32.49 32.49 40.96 47.61 40.96 47.61 28.290 43.56 46.24 38.44 38.44 43.56 37.21 28.410 44.89 43.56 36.00 43.56 32.49 38.44 28.530 46.24 33.64 39.69 43.56 28.09 36.00 28.650 38.44 40.96 32.49 47.61 54.76 43.56 28.770 46.24 37.21 33.64 38.44 39.69 44.89 28.890 53.29 40.96 42.25 34.81 43.56 43.56 29.010 51.84 53.29 49.00 47.61 50.41 49.00 29.130 53.29 44.89 39.69 42.25 44.89 51.84 29.250 47.61 62.41 60.84 53.29 65.61 60.84 29.370 70.56 79.21 92.16 88.36 84.64 79.21 29.490 77.44 77.44 72.25 67.24 65.61 68.89 29.610 59.29 46.24 72.25 62.41 67.24 72.25 29.730 82.81 51.84 54.76 70.56 81.00 67.24 29.850 81.00 70.56 84.64 77.44 88.36 68.89 29.970 90.25 100.00 92.16 88.36 90.25 92.16 30.090 82.81 112.36 123.21 121.00 104.04 106.09 30.210 118.81 148.84 156.25 158.76 144.00 184.96

273

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

30.330 182.25 231.04 213.16 198.81 256.00 272.25 30.450 299.29 299.29 327.61 400.00 420.25 484.00 30.570 510.76 600.25 655.36 789.61 864.36 1011.24 30.690 1169.64 1267.36 1600.00 1909.69 2275.29 2693.61 30.810 3249.00 4019.56 4774.81 5852.25 6955.56 7586.41 30.930 8010.25 7832.25 7106.49 6496.36 5715.36 4844.16 31.050 4032.25 3226.24 2570.49 2125.21 1656.49 1428.84 31.170 1204.09 1030.41 876.16 734.41 645.16 645.16 31.290 479.61 428.49 416.16 384.16 320.41 278.89 31.410 289.00 275.56 237.16 201.64 196.00 193.21 31.530 158.76 158.76 158.76 139.24 127.69 148.84 31.650 132.25 110.25 121.00 127.69 123.21 100.00 31.770 114.49 102.01 114.49 106.09 94.09 121.00 31.890 94.09 77.44 73.96 77.44 75.69 72.25 32.010 77.44 79.21 72.25 64.00 70.56 82.81 32.130 67.24 47.61 72.25 72.25 59.29 59.29 32.250 62.41 59.29 53.29 59.29 57.76 53.29 32.370 56.25 57.76 51.84 62.41 67.24 59.29 32.490 59.29 59.29 53.29 49.00 59.29 54.76 32.610 65.61 54.76 47.61 65.61 56.25 60.84 32.730 46.24 46.24 56.25 56.25 57.76 54.76 32.850 56.25 57.76 47.61 50.41 51.84 60.84 32.970 57.76 56.25 65.61 62.41 60.84 68.89 33.090 77.44 59.29 73.96 86.49 70.56 86.49 33.210 67.24 75.69 75.69 102.01 112.36 132.25 33.330 144.00 156.25 153.76 156.25 207.36 222.01 33.450 249.64 275.56 282.24 306.25 338.56 306.25 33.570 313.29 259.21 231.04 216.09 171.61 169.00 33.690 136.89 134.56 121.00 96.04 88.36 88.36 33.810 68.89 70.56 54.76 70.56 59.29 73.96 33.930 43.56 60.84 50.41 51.84 50.41 46.24 34.050 60.84 50.41 34.81 47.61 46.24 50.41 34.170 44.89 49.00 42.25 40.96 42.25 49.00 34.290 50.41 40.96 47.61 40.96 38.44 43.56 34.410 57.76 43.56 33.64 43.56 62.41 47.61 34.530 53.29 47.61 47.61 33.64 33.64 39.69 34.650 56.25 46.24 44.89 54.76 57.76 56.25 34.770 38.44 50.41 46.24 32.49 53.29 62.41 34.890 62.41 70.56 51.84 59.29 70.56 72.25 35.010 90.25 90.25 94.09 90.25 121.00 116.64 35.130 125.44 141.61 184.96 184.96 198.81 213.16 35.250 228.01 256.00 275.56 272.25 240.25 262.44 35.370 234.09 246.49 198.81 158.76 146.41 153.76 35.490 123.21 141.61 106.09 100.00 102.01 75.69 35.610 88.36 72.25 86.49 82.81 67.24 38.44 35.730 57.76 77.44 53.29 50.41 44.89 40.96 35.850 51.84 43.56 50.41 49.00 46.24 47.61 35.970 54.76 54.76 54.76 59.29 49.00 51.84 36.090 56.25 39.69 42.25 49.00 62.41 42.25 36.210 40.96 50.41 53.29 40.96 44.89 44.89 36.330 49.00 47.61 51.84 51.84 57.76 39.69 36.450 50.41 59.29 62.41 60.84 60.84 79.21

274

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

36.570 70.56 68.89 68.89 62.41 64.00 72.25 36.690 77.44 67.24 79.21 98.01 98.01 86.49 36.810 98.01 104.04 98.01 114.49 102.01 121.00 36.930 134.56 121.00 116.64 136.89 132.25 134.56 37.050 176.89 196.00 184.96 182.25 182.25 193.21 37.170 201.64 256.00 256.00 306.25 320.41 368.64 37.290 408.04 436.81 497.29 492.84 445.21 449.44 37.410 376.36 408.04 361.00 282.24 268.96 256.00 37.530 222.01 201.64 148.84 174.24 141.61 132.25 37.650 114.49 118.81 98.01 106.09 90.25 98.01 37.770 94.09 81.00 79.21 92.16 67.24 56.25 37.890 72.25 68.89 50.41 75.69 65.61 64.00 38.010 56.25 60.84 57.76 47.61 44.89 50.41 38.130 62.41 46.24 42.25 56.25 65.61 47.61 38.250 50.41 53.29 53.29 53.29 59.29 50.41 38.370 46.24 54.76 46.24 56.25 54.76 53.29 38.490 53.29 43.56 46.24 57.76 51.84 60.84 38.610 57.76 47.61 50.41 47.61 46.24 50.41 38.730 50.41 43.56 62.41 50.41 38.44 43.56 38.850 60.84 42.25 57.76 40.96 56.25 43.56 38.970 47.61 51.84 49.00 50.41 43.56 47.61 39.090 47.61 50.41 42.25 54.76 60.84 50.41 39.210 44.89 65.61 67.24 67.24 62.41 86.49 39.330 73.96 72.25 60.84 72.25 72.25 98.01 39.450 96.04 96.04 92.16 82.81 98.01 92.16 39.570 132.25 114.49 116.64 114.49 108.16 134.56 39.690 139.24 139.24 129.96 146.41 129.96 153.76 39.810 129.96 136.89 169.00 148.84 123.21 146.41 39.930 161.29 141.61 146.41 127.69 136.89 114.49 40.050 112.36 94.09 102.01 96.04 123.21 92.16 40.170 67.24 84.64 84.64 77.44 57.76 68.89 40.290 70.56 59.29 75.69 70.56 72.25 82.81 40.410 77.44 75.69 77.44 86.49 84.64 90.25 40.530 108.16 102.01 104.04 110.25 118.81 118.81 40.650 153.76 156.25 163.84 169.00 174.24 213.16 40.770 222.01 234.09 246.49 306.25 306.25 392.04 40.890 412.09 441.00 576.00 640.09 718.24 835.21 41.010 948.64 1036.84 1156.00 1274.49 1310.44 1354.24 41.130 1361.61 1346.89 1267.36 1149.21 1056.25 1017.61 41.250 800.89 767.29 718.24 605.16 529.00 457.96 41.370 400.00 361.00 299.29 272.25 231.04 246.49 41.490 207.36 184.96 156.25 163.84 158.76 148.84 41.610 110.25 121.00 118.81 96.04 82.81 104.04 41.730 79.21 92.16 72.25 72.25 59.29 72.25 41.850 82.81 82.81 56.25 79.21 70.56 75.69 41.970 62.41 72.25 62.41 77.44 62.41 56.25 42.090 62.41 49.00 50.41 62.41 62.41 62.41 42.210 53.29 56.25 53.29 54.76 57.76 57.76 42.330 65.61 56.25 46.24 56.25 62.41 62.41 42.450 65.61 65.61 65.61 53.29 33.64 47.61 42.570 56.25 50.41 50.41 43.56 38.44 46.24 42.690 54.76 37.21 38.44 56.25 42.25 47.61

275

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

42.810 53.29 68.89 47.61 47.61 56.25 47.61 42.930 51.84 40.96 47.61 51.84 65.61 59.29 43.050 64.00 65.61 54.76 64.00 62.41 77.44 43.170 67.24 64.00 56.25 64.00 60.84 70.56 43.290 72.25 62.41 67.24 65.61 70.56 70.56 43.410 79.21 82.81 73.96 75.69 75.69 100.00 43.530 81.00 86.49 102.01 139.24 100.00 125.44 43.650 144.00 161.29 193.21 169.00 190.44 207.36 43.770 243.36 240.25 213.16 246.49 213.16 198.81 43.890 174.24 169.00 158.76 151.29 139.24 112.36 44.010 106.09 132.25 110.25 81.00 86.49 90.25 44.130 77.44 112.36 94.09 96.04 82.81 75.69 44.250 77.44 81.00 90.25 84.64 90.25 100.00 44.370 88.36 94.09 88.36 75.69 90.25 102.01 44.490 106.09 127.69 118.81 134.56 144.00 161.29 44.610 153.76 187.69 174.24 234.09 262.44 302.76 44.730 306.25 353.44 412.09 501.76 556.96 635.04 44.850 718.24 823.69 924.16 912.04 841.00 864.36 44.970 739.84 729.00 681.21 660.49 585.64 497.29 45.090 466.56 368.64 313.29 285.61 268.96 249.64 45.210 216.09 204.49 171.61 158.76 141.61 144.00 45.330 125.44 116.64 106.09 108.16 88.36 94.09 45.450 77.44 81.00 67.24 75.69 88.36 62.41 45.570 67.24 65.61 70.56 67.24 73.96 62.41 45.690 67.24 59.29 53.29 77.44 77.44 67.24 45.810 59.29 64.00 53.29 59.29 54.76 53.29 45.930 49.00 59.29 59.29 54.76 50.41 77.44 46.050 56.25 47.61 62.41 56.25 47.61 50.41 46.170 50.41 53.29 50.41 49.00 57.76 59.29 46.290 56.25 70.56 77.44 72.25 70.56 59.29 46.410 77.44 54.76 53.29 62.41 60.84 60.84 46.530 67.24 79.21 65.61 65.61 70.56 65.61 46.650 60.84 57.76 82.81 72.25 64.00 82.81 46.770 54.76 90.25 68.89 67.24 67.24 60.84 46.890 49.00 65.61 57.76 70.56 44.89 56.25 47.010 47.61 53.29 46.24 59.29 47.61 50.41 47.130 49.00 39.69 49.00 47.61 53.29 51.84 47.250 47.61 49.00 50.41 56.25 46.24 47.61 47.370 47.61 47.61 53.29 59.29 36.00 59.29 47.490 59.29 59.29 53.29 56.25 56.25 59.29 47.610 53.29 59.29 57.76 54.76 62.41 43.56 47.730 50.41 60.84 62.41 38.44 53.29 47.61 47.850 67.24 59.29 47.61 56.25 47.61 54.76 47.970 46.24 46.24 47.61 53.29 56.25 50.41 48.090 70.56 50.41 56.25 47.61 54.76 54.76 48.210 60.84 54.76 62.41 50.41 57.76 62.41 48.330 59.29 56.25 72.25 62.41 50.41 59.29 48.450 59.29 65.61 65.61 70.56 75.69 62.41 48.570 75.69 62.41 77.44 67.24 77.44 86.49 48.690 70.56 75.69 82.81 72.25 79.21 86.49 48.810 70.56 77.44 86.49 102.01 90.25 110.25 48.930 112.36 96.04 116.64 129.96 121.00 156.25

276

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

49.050 144.00 156.25 163.84 171.61 156.25 176.89 49.170 196.00 228.01 234.09 222.01 222.01 222.01 49.290 243.36 184.96 222.01 207.36 243.36 207.36 49.410 216.09 153.76 176.89 182.25 174.24 136.89 49.530 158.76 132.25 139.24 141.61 112.36 158.76 49.650 125.44 129.96 132.25 114.49 127.69 136.89 49.770 118.81 136.89 134.56 139.24 139.24 148.84 49.890 148.84 169.00 153.76 171.61 187.69 184.96 50.010 207.36 204.49 207.36 237.16 252.81 289.00 50.130 292.41 316.84 357.21 334.89 376.36 392.04 50.250 416.16 453.69 501.76 506.25 610.09 635.04 50.370 712.89 800.89 894.01 900.00 1004.89 1024.00 50.490 1049.76 1095.61 1049.76 1056.25 1082.41 1004.89 50.610 985.96 930.25 852.64 812.25 812.25 739.84 50.730 784.00 756.25 756.25 734.41 772.84 712.89 50.850 756.25 888.04 906.01 924.16 948.64 1030.41 50.970 1062.76 1082.41 1142.44 1156.00 1102.24 1056.25 51.090 1128.96 1049.76 1049.76 1024.00 954.81 870.25 51.210 789.61 767.29 729.00 650.25 605.16 547.56 51.330 547.56 466.56 432.64 400.00 384.16 327.61 51.450 334.89 262.44 268.96 222.01 219.04 196.00 51.570 193.21 182.25 179.56 151.29 158.76 139.24 51.690 144.00 129.96 139.24 136.89 127.69 108.16 51.810 100.00 106.09 108.16 88.36 92.16 104.04 51.930 81.00 84.64 68.89 86.49 77.44 84.64 52.050 77.44 82.81 68.89 82.81 79.21 84.64 52.170 72.25 75.69 77.44 81.00 59.29 70.56 52.290 65.61 65.61 77.44 90.25 73.96 60.84 52.410 56.25 72.25 62.41 77.44 65.61 59.29 52.530 50.41 39.69 56.25 67.24 56.25 67.24 52.650 53.29 47.61 54.76 62.41 67.24 50.41 52.770 56.25 39.69 53.29 44.89 60.84 46.24 52.890 40.96 37.21 40.96 43.56 40.96 39.69 53.010 54.76 40.96 50.41 54.76 49.00 46.24 53.130 50.41 56.25 56.25 47.61 49.00 40.96 53.250 57.76 47.61 47.61 47.61 53.29 44.89 53.370 50.41 46.24 46.24 53.29 53.29 46.24 53.490 38.44 37.21 38.44 40.96 28.09 36.00 53.610 50.41 56.25 43.56 39.69 50.41 38.44 53.730 43.56 54.76 38.44 36.00 40.96 38.44 53.850 53.29 47.61 46.24 56.25 33.64 57.76 53.970 43.56 38.44 39.69 42.25 36.00 31.36 54.090 47.61 36.00 50.41 36.00 47.61 32.49 54.210 47.61 37.21 38.44 31.36 50.41 32.49 54.330 38.44 28.09 40.96 33.64 39.69 32.49 54.450 36.00 37.21 33.64 34.81 29.16 31.36 54.570 38.44 42.25 39.69 39.69 36.00 39.69 54.690 43.56 50.41 43.56 38.44 32.49 47.61 54.810 32.49 50.41 49.00 49.00 47.61 42.25 54.930 33.64 43.56 44.89 47.61 36.00 46.24 55.050 47.61 53.29 46.24 36.00 46.24 38.44 55.170 36.00 40.96 31.36 36.00 33.64 40.96

277

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

55.290 34.81 53.29 34.81 50.41 50.41 44.89 55.410 36.00 42.25 39.69 33.64 33.64 37.21 55.530 40.96 47.61 33.64 28.09 43.56 40.96 55.650 27.04 46.24 46.24 39.69 33.64 43.56 55.770 38.44 24.01 36.00 38.44 33.64 49.00 55.890 40.96 33.64 38.44 34.81 38.44 38.44 56.010 33.64 37.21 39.69 26.01 44.89 37.21 56.130 43.56 39.69 43.56 47.61 44.89 50.41 56.250 38.44 36.00 34.81 32.49 43.56 43.56 56.370 31.36 47.61 47.61 43.56 38.44 39.69 56.490 29.16 42.25 24.01 44.89 36.00 33.64 56.610 30.25 53.29 31.36 27.04 32.49 28.09 56.730 44.89 50.41 38.44 42.25 44.89 26.01 56.850 38.44 40.96 50.41 36.00 46.24 38.44 56.970 163.84 33.64 50.41 31.36 38.44 36.00 57.090 40.96 39.69 53.29 42.25 39.69 43.56 57.210 34.81 44.89 39.69 44.89 49.00 39.69 57.330 40.96 43.56 50.41 32.49 38.44 47.61 57.450 50.41 47.61 46.24 47.61 44.89 36.00 57.570 36.00 43.56 29.16 44.89 31.36 34.81 57.690 56.25 39.69 44.89 39.69 53.29 40.96 57.810 33.64 46.24 53.29 44.89 39.69 50.41 57.930 37.21 36.00 44.89 32.49 47.61 54.76 58.050 50.41 38.44 53.29 53.29 60.84 39.69 58.170 50.41 60.84 57.76 42.25 50.41 53.29 58.290 51.84 51.84 53.29 67.24 62.41 54.76 58.410 75.69 53.29 64.00 72.25 90.25 79.21 58.530 90.25 100.00 92.16 86.49 100.00 112.36 58.650 114.49 123.21 134.56 151.29 193.21 193.21 58.770 193.21 225.00 252.81 222.01 231.04 204.49 58.890 216.09 207.36 213.16 198.81 207.36 184.96 59.010 184.96 193.21 184.96 176.89 161.29 144.00 59.130 134.56 129.96 127.69 114.49 114.49 125.44 59.250 129.96 125.44 102.01 136.89 127.69 134.56 59.370 148.84 141.61 123.21 141.61 153.76 190.44 59.490 198.81 187.69 222.01 207.36 216.09 243.36 59.610 285.61 327.61 295.84 331.24 372.49 368.64 59.730 400.00 424.36 441.00 445.21 396.01 416.16 59.850 361.00 376.36 400.00 364.81 345.96 306.25 59.970 289.00 313.29 246.49 262.44 207.36 216.09 60.090 198.81 174.24 174.24 148.84 134.56 127.69 60.210 134.56 116.64 112.36 129.96 104.04 125.44 60.330 96.04 102.01 88.36 75.69 73.96 79.21 60.450 75.69 72.25 81.00 62.41 70.56 70.56 60.570 65.61 47.61 57.76 56.25 56.25 54.76 60.690 70.56 53.29 47.61 62.41 56.25 43.56 60.810 54.76 50.41 39.69 54.76 43.56 51.84 60.930 56.25 38.44 50.41 49.00 53.29 59.29 61.050 50.41 47.61 50.41 44.89 56.25 65.61 61.170 50.41 60.84 43.56 33.64 47.61 51.84 61.290 50.41 43.56 46.24 57.76 65.61 56.25 61.410 59.29 44.89 47.61 46.24 43.56 47.61

278

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

61.530 51.84 54.76 49.00 51.84 56.25 67.24 61.650 57.76 62.41 47.61 59.29 62.41 53.29 61.770 67.24 72.25 65.61 64.00 67.24 84.64 61.890 68.89 88.36 84.64 88.36 82.81 90.25 62.010 75.69 84.64 77.44 96.04 72.25 82.81 62.130 70.56 62.41 72.25 84.64 73.96 67.24 62.250 64.00 64.00 50.41 68.89 77.44 72.25 62.370 54.76 70.56 50.41 59.29 51.84 57.76 62.490 57.76 53.29 70.56 53.29 47.61 54.76 62.610 59.29 56.25 60.84 67.24 77.44 64.00 62.730 65.61 70.56 72.25 67.24 84.64 81.00 62.850 75.69 79.21 77.44 90.25 94.09 102.01 62.970 88.36 114.49 108.16 134.56 116.64 125.44 63.090 125.44 151.29 132.25 174.24 171.61 198.81 63.210 182.25 193.21 240.25 259.21 272.25 313.29 63.330 327.61 384.16 349.69 376.36 357.21 331.24 63.450 324.00 334.89 302.76 331.24 275.56 289.00 63.570 275.56 262.44 225.00 228.01 201.64 201.64 63.690 213.16 163.84 141.61 174.24 132.25 148.84 63.810 121.00 121.00 139.24 108.16 116.64 114.49 63.930 108.16 102.01 125.44 112.36 108.16 121.00 64.050 106.09 114.49 114.49 125.44 129.96 116.64 64.170 116.64 121.00 156.25 146.41 141.61 169.00 64.290 174.24 196.00 198.81 207.36 228.01 249.64 64.410 265.69 299.29 299.29 320.41 256.00 285.61 64.530 246.49 240.25 259.21 240.25 231.04 234.09 64.650 243.36 246.49 228.01 207.36 174.24 184.96 64.770 174.24 163.84 187.69 174.24 176.89 184.96 64.890 187.69 169.00 182.25 182.25 179.56 198.81 65.010 204.49 219.04 207.36 234.09 246.49 216.09 65.130 234.09 225.00 219.04 182.25 176.89 225.00 65.250 201.64 182.25 207.36 210.25 213.16 158.76 65.370 158.76 148.84 114.49 151.29 129.96 108.16 65.490 102.01 114.49 116.64 121.00 125.44 110.25 65.610 94.09 112.36 102.01 112.36 98.01 104.04 65.730 123.21 114.49 104.04 134.56 112.36 104.04 65.850 129.96 136.89 132.25 136.89 156.25 134.56 65.970 161.29 127.69 158.76 146.41 158.76 161.29 66.090 174.24 153.76 148.84 141.61 153.76 141.61 66.210 129.96 144.00 127.69 146.41 114.49 102.01 66.330 108.16 104.04 100.00 96.04 102.01 68.89 66.450 92.16 98.01 64.00 70.56 88.36 77.44 66.570 67.24 65.61 62.41 73.96 60.84 57.76 66.690 53.29 50.41 49.00 49.00 49.00 44.89 66.810 59.29 65.61 51.84 39.69 38.44 42.25 66.930 38.44 43.56 38.44 36.00 39.69 44.89 67.050 37.21 37.21 43.56 37.21 49.00 39.69 67.170 34.81 42.25 59.29 51.84 62.41 68.89 67.290 67.24 50.41 73.96 60.84 70.56 64.00 67.410 43.56 40.96 37.21 43.56 34.81 50.41 67.530 39.69 33.64 43.56 19.36 36.00 26.01 67.650 29.16 12.96 33.64 29.16 16.81 25.00

279

File: JC16.RD ======Philips Analytical X-Ray B.V. PC-APD, Diffraction software

Angle Intensity Intensity Intensity Intensity Intensity Intensity [ø2é] [counts] [counts] [counts] [counts] [counts] [counts]

67.770 20.25 17.64 21.16 13.69 12.96 6.76 67.890 16.00 12.25 15.21 15.21 10.24 16.00 68.010 12.96 4.84 7.84 13.69 17.64 5.76 68.130 9.00 12.25 16.81 6.76 10.89 17.64 68.250 16.81 10.89 5.76 10.89 10.89 10.24 68.370 7.84 6.76 9.00 4.84 4.00 5.76 68.490 10.24 9.00 9.00 10.24 4.84 7.84 68.610 10.89 9.00 5.76 6.76 6.76 2.89 68.730 6.76 7.84 10.24 4.84 0.00 2.89 68.850 17.64 6.76 10.24 13.69 1.96 6.76 68.970 13.69 12.25 5.76 4.84 4.84 6.76 69.090 9.00 1.96 6.76 7.84 5.76 9.00 69.210 4.84 7.84 4.84 12.25 10.24 10.24 69.330 9.00 12.25 9.00 4.84 5.76 5.76 69.450 10.24 5.76 7.84 4.00 4.84 9.00 69.570 6.76 7.84 7.84 7.84 13.69 5.76 69.690 10.24 10.89 12.96 9.00 9.00 10.24 69.810 10.24 17.64 10.24 12.96 16.81 12.25 69.930 13.69 10.89 13.69 12.25 _

280

Appendix C XRD Diffractograms

281

282

283

284

285

286

287

288

289