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GE/Housatonic River Site, SDMS No. 260369 Field Sampling Plan And

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GE/Housatonic River Site, SDMS No. 260369 Field Sampling Plan And General Electric Company Pittsfield, Massachusetts Field Sampling Plan/ Quality Assurance Project Plan Volume II of III Originally submitted September 2000 Revised March 2007 FSP/QAPP Revision #: 04 Date: March 30, 2007 Volume II - Standard Operating Procedures for Field Based Activities Appendices A Soil Sampling Procedures for Analysis of Volatile Organic Compounds (VOCs) B Soil Sampling Procedures for Analysis of Extractable Petroleum Hydrocarbons (EPH)/Volatile Petroleum Hydrocarbons (VPH) C Soil Boring Installation and Soil Sampling Procedures D Groundwater Purging and Sampling Procedures for Monitoring Wells E Surface Water Sampling Procedures F Sediment Sampling Procedures G Dense Non-Aqueous Phase Liquid (DNAPL)/Light Non-Aqueous Phase Liquid (LNAPL) Sampling Procedures H Biota Sampling Procedures I Soil Gas Sampling Procedures J Air Monitoring Procedures K Radioisotope Analysis of Cesium-137 and Beryllium-7 in Sediments L Handling, Packaging, and Shipping Procedures M Standard Operating Procedures for Shipment of Department of Transportation Hazardous Materials N Photoionization Detector Field Screening Procedures O Temperature, Turbidity, Specific Conductivity, pH, Oxidation/Reduction Potential, and Dissolved Oxygen Field Measurement Procedures P In-Situ Hydraulic Conductivity Test Procedures Q Water Level/Oil Thickness Measurement Procedures R Passive Oil Recovery Procedures S Monitoring Well Installation and Development Procedures T Magnetometer Survey Procedures U Seismic Refraction Survey Procedures V Ground Penetrating Radar (GPR) Procedures W Standard Operating Procedures for Equipment Cleaning X Building Material Sampling Procedures Y Selection of Drilling Method Z Monitoring Well Inventory Procedures AA Groundwater Sampling Procedures Using Passive-Diffusion Bags BB Soil/Water Shake Test Procedures CC Basement Sump Sediment/Water Sampling Procedures DD Manhole/Catch Basin Sediment/Water/NAPL Sampling Procedures EE Electromagnetic Survey Procedures FF Test Pit Excavation Procedures GG Monitoring Well Decommissioning Procedures HH Procedure for Determination of Total Organic Carbon in Solid Samples II Vibracore Sediment Collection Procedures JJ Pore Water Sample Collection Procedures KK Sequential Batch Leach Test Procedures LL Seepage Meter Usage Procedures BLASLAND, BOUCK & LEE, INC. 4/2/2007 engineers, scientists, economists 1 V:\GE_Pittsfield_General\Reports and Presentations\FSP-QAPP 2007\Vol II\164711324VolII&III TOC.doc Appendices Appendix A Soil Sampling Procedures for Analysis of Volatile Organic Compounds (VOCs) VOC Soil Sampling Revision #: 00 Date: September 13, 2000 Appendix A Soil Sampling Procedures for Analysis of Volatile Organic Compounds (VOCs) I. Introduction This standard operating procedure (SOP) describes the field sampling procedures to collect soil samples for the analysis of volatile organic compounds (VOCs). Soil samples will be collected in a manner that will minimize the loss of VOCs through volatilization and biodegradation. This SOP presents the procedures to collect soil and sediment samples for low-level (sample concentrations less than 200 Fg/Kg, wet weight) and high-level (sample concentrations greater than 200 Fg/Kg, wet weight) VOC analyses using field preservation techniques, the procedures to collect soil and sediment samples without field preservation, and the procedures for collection of soil and sediment samples using EnCoreJ, SoilCoreJ, or equivalent samplers. In order to minimize the handling of preservatives (i.e., sodium bisulfate or methanol) in the field, the preferred sample collection method for VOC analysis will employ the EnCoreJ, SoilCoreJ, or equivalent methods. The soil collection procedure to be utilized at each area will be presented in the project-specific work plan. II. Materials The following materials, as required, shall be available during soil sampling: • Health and safety equipment (as required in the Health and Safety Plan); • Photoionization detector (PID); • Modified 10 - 30 mL plastic syringe; 1. Cut off the injection tip, 2. Depending upon the construction of the syringe, cut small air vents into the plunger or remove the rubber tip and retaining post. • Stainless steel spatula; • EnCoreJ Sampler T-Handle; • Resealable-type bags; • Handiwipes or lint-free paper towels; • Field notebook; • Appropriate sample containers depending upon specific methodology (4-oz glass jar with Teflon-lined cap, pre-preserved 40 mL vial with septum seal, EnCoreJ, SoilCoreJ, or equivalent Sampler); and • Appropriate transport containers (coolers) with water ice and appropriate labeling, packing, and shipping materials. III. Field Sampling Option 1 - Collection of Unpreserved Sample Step 1 - Soil samples are collected directly from the split-spoon using a stainless steel decontaminated spatula. Step 2 - Samples are collected in 4-oz (120 mL) wide-mouth glass jars with Teflon-lined screw caps. Step 3 - Wipe the threads of the sample jar with a handiwipe or lint-free paper towel, to ensure an adequate seal. BLASLAND, BOUCK & LEE, INC. 3/30/2007 engineers, scientists, economists A-1 V:\GE_Pittsfield_General\Reports and Presentations\FSP-QAPP 2007\Vol II\164711324AppxA.doc VOC Soil Sampling Revision #: 00 Date: September 13, 2000 Step 4 - Place sample containers in a transportation cooler on ice immediately after collection. Package and label the sample containers following the procedures specified in Appendix L. Option 2A - EnCoreJ Sampler Step 1 - Place EnCoreJ sample container into the EnCoreJ T-handle. Step 2 - Collect soil sample by pressing the EnCoreJ sample container into the soil to be collected. Step 3 - Wipe the outside of the EnCoreJ sample container with a handiwipe or lint-free paper towel to ensure an adequate seal. Step 4 - Using the T-handle, cap and lock the EnCoreJ Sampler for shipment. Step 5 - If low-level VOC analysis is to be performed, repeat Steps 1 through 3 two additional times to collect a total of 3 samples (high-level VOC analysis only requires 1 EnCoreJ Sampler). Step 6 - Collect additional soil in a 4-oz (120 mL) jar for percent moisture determination. Step 7 - Place sample container in a transportation cooler on ice immediately after collection. Package and label the sample container following the procedures in Appendix L. Option 2B - SoilCoreJ Sampler Step 1 - Collect soil sample by pressing the SoilCoreJ sample container into the soil to be collected. A decontaminated stainless steel spatula may be used to assist this procedure. Step 2 - Wipe the outside of the SoilCoreJ sample container with a handiwipe or lint-free paper towel to ensure an adequate seal. Step 3 - Cap the filled end of the SoilCoreJ sample container. Step 4 - Fill the opposite side of the SoilCoreJ sample container by pushing the empty side of the SoilCoreJ into the soil to be collected. A decontaminated stainless steel spatula may be used to assist this procedure. Step 5 - Wipe the outside of the SoilCoreJ sample container with a handiwipe or lint-free paper towel to ensure an adequate seal. Step 6 - Cap the filled end of the SoilCoreJ sample container. Step 7 - Place the locking strap around both endcaps and pull the strap tight to secure endcaps. Check the position of endcaps after tightening to verify that the SoilCoreJ container is properly sealed. Step 8 - Collect additional soil in a 4-oz (120 mL) jar for percent moisture determination. BLASLAND, BOUCK & LEE, INC. 3/30/2007 engineers, scientists, economists A-2 V:\GE_Pittsfield_General\Reports and Presentations\FSP-QAPP 2007\Vol II\164711324AppxA.doc VOC Soil Sampling Revision #: 00 Date: September 13, 2000 Step 9 - Place sample container in a transportation cooler on ice immediately after collection. Package and label the sample container following the procedures in Appendix L. Option 3 - Field Preservation Step 1 - Order the appropriate number of pre-preserved sample containers (sodium bisulfate and/or methanol) from the laboratory. Instruct the laboratory to supply the sample container (with preservative) tare weights with the bottle order. Step 2 - Prior to sample collection, weigh each sample container and compare the weight to the laboratory supplied tare weight to ensure that loss of preservative has not occurred. Do not use sample containers that do not agree within " 0.2 grams of the laboratory tare weight. Step 3 - Remove the plunger from a decontaminated sampler (modified plastic syringe). Step 4 - Immediately after the surface of the soil is exposed to the atmosphere collect approximately 5.0 grams of sample by inserting the sampler into the soil. A decontaminated stainless steel spatula may be used to assist this procedure. Step 5 - Carefully wipe the outside of the sampler with a handiwipe or lint-free towel. Step 6 - Extrude the sample directly into the pre-preserved sample vial supplied by the laboratory. Avoid splashing the preservative solution. Step 7 - Wipe the threads of the sample jar with a handiwipe or lint-free paper towel, to ensure an adequate seal. Step 8 - Weigh the sample container and record the weight on the chain-of-custody form. Add a note on the chain-of-custody form to inform the laboratory to contact the project QA/QC Manager if the laboratory measured sample weight does not agree within " 0.2 grams of the weight recorded on the chain-of- custody form. Step 9 - For each sample location repeat steps 1 through 5 collecting two replicate samples for each method (low-level and/or high-level) in the appropriate sample vials. Step 10- Using a stainless steel decontaminated
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