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Clean from Start to Finish CLEAN COMPOUNDING | PROCESSING Whether for medical, pharma or for engineering applications, demand for high cleanliness compound production is on the rise. Peter Mapleston learns more PHOTO: POLYCOMPOUND PHOTO: Clean from start to finish Mention cleanrooms to most plastics engineers Apex facility at St Albans, in Vermont in the US, Main image: and it is likely they will think of pharmaceutical where the company produces its Medalist medical Swiss toll production, manufacturing of medical and elec- thermoplastic elastomers (the company also has a compounder tronic devices, possibly plastics injection moulding, line dedicated to Medalist compounds in Singa- Polycompound but almost certainly not compounding. It is simply pore). “The adherence to CGMP protocols during reports not a term that is used much in the compounding line clearances ensures each recipe is free from growing business – but perhaps it should be. The reality is foreign materials,” he says (CGMP refers to the demand for its that if a processor working in a field such as Current Good Manufacturing Practice regulations clean com- medical does not start with a clean compound it is enforced by the FDA in the US and which provide for pounding capa- very unlikely they will be able to produce a clean systems that assure proper design, monitoring, and bilities from syringe or similar device. To coin a phrase from the control of manufacturing processes and facilities). customers in computer industry: garbage in, garbage out. “The St Albans facility has a strong commitment the high As it happens, there is plenty of expertise to the needs of our customers and incorporates performance around covering clean compounding. Remember those requirements into their highly controlled power cable that many producers of twin-screw extrusion lines processes. Everything from raw materials through sector for plastics compound production also offer packaging is considered when we produce equipment that is not all that different in concept products for our customers in the regulated for pharmaceutical and food processing. However, applications, including machine lubricants,” a lot of what those equipment builders do in this Ciemniewski says. area is covered by confidentiality agreements, so The Medalist production lines at St Albans and much of what follows in this article is based on in Singapore both carry ISO 13485 certification. input from a number of compound manufacturing This international standard for quality management companies considered to be leaders in the field. in medical manufacturing specifies systems for Eric Ciemniewski is Plant Manager of the Teknor consistent compliance with regulatory and custom- www.compoundingworld.com June 2019 | COMPOUNDING WORLD 61 PROCESSING | CLEAN COMPOUNDING er requirements and includes provisions for risk management, sterile manufacturing, and traceabil- ity. The comprehensive implementation program required for ISO 13485 certification requires focusing of the entire compounding operation on processes and procedures that maximise safety and reliability of the compounds supplied to medical device manufacturers. Clean or white? Lewiston, Maine, US-based Compounding Solutions implemented the use of a white room for all of its medical R&D and production materials back in 2012 (a white room can be considered very much like a cleanroom but without the certifica- tion). “Due to the extremely fine particle sizes of most colorants, the ability to obtain and then maintain the certification is extraordinarily chal- lenging,” the company says. “We conduct our own air quality reviews and have found that we meet Class 100,000 standards.” ICMA delivers In a white paper, the company says that while gloved handling of finished products is a critical element in their customers’ final assembly opera- turnkey pharma tions to help prevent excessive particle counts, many issues may be occurring before a part or solutions product has been received to the plant. In April this year, Italian twin-screw compounding “Depending on how your vendor has built and extruder specialist ICMA San Giorgio delivered operates their facility it may be adding risk to your a complete system to a major European pharma raw materials. Ceiling drop-downs for air, electrical group for direct compounding and extrusion of wires or feed tubes can collect dust and other several types of TPE foils. The system includes contaminates that can easily fall into open hoppers. gravimetric dosing units, a high-efficiency Open water tanks capture the same environmental co-rotating twin screw extruder (ICMA MCM 60) Below: hazards as water baths do,” it says. “Companies and downstream equipment (three-roll calender Applications either have the ability to help with cleanliness and fully automated winding unit). for the Teknor issues or they do not. Most compounders do not ICMA Managing Director Giorgio Colombo Apex ISO run products under anything close to white room says the turn-key project involved complete 13485 conditions.” engineering with several customised features Medalist TPEs The Compounding Solutions white room closely tied to the customer’s requirements, include syringe operates under conditions similar to a clean room including solutions for assuring maximum stoppers using laminar air flow conditions to ensure that no cleanliness of the entire process line dictated by critical pharma applications. The line incorpo- rates several digital solutions and sensor devices applied to key parts such as the calender and thickness control to achieve maximum accuracy during extrusion and the highest standard of safety for the operators. ICMA has also just supplied a multinational pharma group with a turn-key line based on a 25mm compounding unit designed to produce several TPE recipes, Colombo says. “In this case ICMA was able to accommodate a very demand- ing customer with several customised features in line design and services.” PHOTO: TEKNOR APEX ❯ www.icmasg.it 62 COMPOUNDING WORLD | June 2019 www.compoundingworld.com PROCESSING | CLEAN COMPOUNDING PHOTO: PLASTICS COLOR CORPORATION COLOR PLASTICS PHOTO: Above: PCC’s contamination enters the feeders of the com- provided the company with additional warehousing, latest produc- pounding line. The walls and floors are all sealed post blending, packaging and shipping capacity, as tion line in so it is possible to carry out a complete wash from well as housing a new compounding line. Chicago was the ceiling to the floor. The company also took the designed and precaution during construction of the facility to Maintaining integrity installed by bring all electrical and water lines in from the Integrity at all stages of the product development Entek ground up rather than using drop-downs, which process “is absolutely paramount for medical device can collect dust and other contamination. In companies,” says David Witt, a researcher with addition, feeders for various additives are all Chicago, US-based Plastics Color Corporation covered and sealed under nitrogen. (PCC). “Medical device manufacturers have to be The company says special attention is paid in the certain that for each product produced, every plant to water baths, which are areas where component and every process involved adhere to pyrogens collect easily. Thorough cleaning is compliance standards.” carried out after each production run and changing PCC opened a 700m2 “Plant Within a Plant” just the water in the cooling baths and scrubbing the over ten years ago for production of additive and tanks is standard practice. colour masterbatch for medical devices. It says the Compounding Solutions has also recently facility was designed with input from medical announced plans to add a cleanroom, certified to experts who cited reducing contamination risk as a Class 100,000, for medical compounding. It is paramount concern. “We talked to customers in the scheduled to go into operation in January next market and asked what we and they needed to look year. “Clean room compounding is very rare and like in five years,” says Joe Byrne, President of PCC. we continue to look to raise the bar and push “The industry is moving toward quick-turn, boundaries of medical plastic compounding,” said just-in-time processing, as well as toward more a company spokesperson. closed-loop systems for clean compounding,” says The cleanroom investment is part of a 5,500m2 Byrne. “Today, we’re making that all work in one expansion of the Lewiston facility that has already facility. It has been important for customers to see how we handle materials and how the cross-con- tamination risk has been almost eliminated by using such equipment as a sterilised water bath utilising UV filtration and a closed-loop water system.” Adding capacity Foster Corporation, headquartered in Putnam, CT, USA, is another leading supplier of custom compounds for medical applications. It was PHOTO: COMPOUNDING SOLUTIONS COMPOUNDING PHOTO: featured in an earlier Compounding World article on cleanroom compounding back in 2016 but has since added further clean production capacity. “Foster’s has built, and put into service, a new pharmaceutical facility across from our corporate Above: Clean compounding at Compounding Solutions facility. This is a state-of-the-art building with two 64 COMPOUNDING WORLD | June 2019 www.compoundingworld.com PROCESSING | CLEAN COMPOUNDING suppliers regularly); enhanced and tighter material specifications; biocompatibility testing including USP Class VI and/or ISO 10993; no change agreements where suppliers must inform us (so we can inform our
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