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01 Contents Food Sheet No CONTENTS 01 CONTENTS FOOD SHEET NO. TITLE PAGE SHEET NO. TITLE PAGE F001 Separation of Water-soluble Vitamins - 1 05 F069 Separation of Acesulfame K 25 F002 Separation of Water-soluble Vitamins - 2 05 F080 Separation of Aspartame and Acesulfame K in breath mint 25 F067 Separation of Vitamins 06 F049 Separation of Saccharin & Sorbic Acid 25 F005 Separation of Fat-soluble Vitamins 06 F076 Separation of Cyclamic acid 25 F070 Separation of Vitamin C 07 F051 Separation of Pyrazines 26 F003 Separation of Vitamin D2, D3 07 F089 Separation of Ubiquinone 9,10 26 F057 Separation of Tocopherols 07 F090 Separation of DL-Thioctic acid 26 F058 Separation of Vitamin C and E 08 F091 Separation of Benzoyl Peroxide in Flour 26 F097 Separation of Vitamin B12 in Health food 08 F053 Separation of Caffeine and Catechins 27 F071 Separation of Carotenoids 08 F054 Separation of Commercial Tea Drink 27 F004 Separation of β-Carotene in Broccoli 09 F055 Separation of Catechins 28 F059 Separation of β-Carotene 09 F056 Separation of Catechins, Caffeine, Chlorophyll a 28 F007 Separation of Synthetic Antibiotics (Quinolone Derivatives)-1 09 F063 Separation of Allyl isothiocyanate 29 F008 Separation of Synthetic Antibiotics (Quinolone Derivatives)-2 10 F064 Separation of Quassins 29 F009 Separation of Synthetic Antibiotics (Sulfa drugs) 10 F065 Separation of Capsaicins 29 F010 Separation of Synthetic Antibiotics (Furan Derivatives) 11 F082 Separation of Curcumin 29 F011 Separation of Synthetic Antibiotics (Protozoicides) 11 F083 Separation of Curcumin in a commercial drink by LC/MS 30 F012 Separation of Synthetic Antibiotics (Protozoicide & Quinolone) 11 F078 Separation of Rutin and Quercetin 30 F013 Separation of 18 Synthetic Antibiotics 12 F099 Separation of Apigenin 30 F026 Separation of Carbadox 13 F100 Separation of 5,6-Benzoflavone 30 F027 Separation of a Metabolite of Carbadox 13 F101 Separation of 7,8-Benzoflavone 31 F028 Separation of Sulfadimidine 13 F102 Separation of Biochanin A 31 F006 Separation of Tetracycline Antibiotics 13 F103 Separation of Chrysin 31 F014 Separation of Drugs for Animals -1 14 F104 Separation of Diosmin 31 F015 Separation of Drugs for Animals -2 14 F105 Separation of Flavonol 32 F019 Analysis of Oxytetracyclne in Pork 14 F106 Separation of Hesperetin 32 F016 Analysis of α-Trenbolone in Pork 15 F107 Separation of Hesperidin 32 F017 Analysis of β-Trenbolone in Pork 15 F108 Separation of Isoquercitrin 32 F021 Analysis of Zeranol in Pork 15 F109 Separation of Kaempferol 33 F018 Analysis of lvermectin in Pork 15 F110 Separation of Luteolin 33 F020 Analysis of Closantel in Pork 16 F111 Separation of Naringenin 33 F022 Analysis of Flubendazole in Pork 16 F112 Separation of Naringin 33 F029 Separation of Thiabendazole 16 F113 Separation of Rhoifolin 34 F030 Separation of a Metabolite of Thiabendazole 16 F114 Separation of 4,2',4'-Trihydroxychalcone 34 F023 Separation of Albendazole 17 F066 Separation of Oligosaccharide 34 F024 Separation of a Metabolite of Albendazole 17 F068 Separation of Carbohydrates 34 F025 Separation of Isomethamidium 17 F032 Separation of di-Carbonic Acids - 1 35 F031 Separation of Avoparcins 17 F092 Separation of di-Carbonic Acids - 2 35 F044 Separation of Preservatives - 1 18 F035 Separation of Organic Acids - 1 35 F047 Separation of Preservatives - 2 18 F093 Separation of Organic Acids – 2 35 F075 Separation of Preservatives - 3 18 F036 Separation of Organrc Acids - 3 36 F043 Separation of Preservatives - 4 18 F094 Separation of Organic Acids - 4 36 F074 Separation of Preservatives - 5 19 F098 Separation of Organic Acids - 5 36 F077 Separation of Preservatives - 6 19 F062 Separation of Formic acid and Tartaric acid 36 F061 Separation of Preservatives and Saccharin 20 F033 Separation of Oxalic Acid and Nitric Acid in Spinach 37 F042 Separation of Antioxidants - 1 20 F034 Separation of Aromatic Acids -1 37 F073 Separation of Antioxidants - 2 20 F096 Separation of Aromatic Acids -2 37 F048 Separation of Ascorbic Acid & Erythorbic Acid 21 F095 Separation of Aromatic Acids -3 37 F045 Separation of anti-Fungal Preservatives - 1 21 F084 Separation of Malachite green and Leucomalachite green 38 F046 Separation of anti-Fungal Preservatives - 2 21 F085 Separation of Malachite green and Leucomalachite green by 38 F037 Separation of Food Dyes - 1 21 LC/MS F038 Separation of Food Dyes - 2 22 F086 Separation of Sudan 38 F039 Separation of Food Dyes - 3 22 F087 Separation of Sudan by LC/MS 39 F040 Separation of Food Dyes - 4 23 F052 Separation of Aflatoxin G1, G2, B1, B2 39 F041 Separation of Food Dyes - 5 23 F081 Separation of Fumonisins 40 F072 Separation of Food Dyes - 6 24 F088 Separation of Melamine 40 F060 Separation of Anthocyanins 24 F079 Separation of Putrefactive amines 40 F050 Separation of Aspartame in a Beverage 24 CONTENTS 01 CONTENTS ENVIRONMENT SHEET NO. TITLE PAGE E001 Separation of N-Methylcarbamate derivatives- 1 43 E002 Separatiori of N-Methylcarbamate derivatives- 2 43 E003 Separatron of Oxine-Copper and Asulam 44 E004 Separation of Oxine-Copper and Thiram 44 E005 Separation of Simazine, Thiram and Thiobencarb 44 E006 Separation of Thiram, Iprodione and Bensulide 44 E007 Separation of Thiram 45 E008 Separation of Thiophanate-methyl and its metabolite 45 E009 Separation of Fenitrothion and its metabolite 45 E011 Separation of Agricultural Chemicals (Germicides) 45 E012 Separation of Agricultural Chemicals (Pesticides) 46 E013 Separation of Agricultural Chemicals (Herbicides)- 1 46 E014 Separation of Agricultural Chemicals (Herbicides)- 2 46 E015 Separation of 5 Agricultural Chemicals - 1 46 E016 Separation of 5 Agricultural Chemicals - 2 47 E028 Separation of 5 Agricultural Chemicals - 3 47 E029 Separation of 5 Agricultural Chemicals - 4 47 E034 Separation of 5 Agricultural Chemicals - 5 47 E017 Separation of 6 Agricultural Chemicals 48 E018 Separation of 9 Agricultural Chemicals - 1 48 E030 Separation of 12 Agricultural Chemicals 48 E035 Separation of 9 Agricultural Chemicals - 2 49 E036 Separation of 3 Agricultural Chemicals 49 E045 Separation of Pesticides standard solution 24【A golf course 50 pesticide】 E019 Separation of Intermediates of Agricultural Chemicals 50 (halogenized Benzoic acids) E027 Separation of Carbofuran 50 E032 Separation of Acephate 51 E033 Separation of Imazalil in Concentrated Lemonade Juice 51 E040 Separation of Pesticides standard solution 28 51 E041 Separation of 3 Agricultural Chemicals 51 E042 Separation of Carbaryl 52 E043 Separation of Diquat 52 E044 Separation of Iminoctadine triacetate 52 E039 Separation of LAS 52 E010 Separation of 15 Synthetic Antibiotics 53 E020 Separation of Benzo[a]pyrene 53 E023 Separation of Microsystins 53 E046 Separation of Patulin 54 E024 Separation of Bisphenol A -1 54 E025 Separation of Bisphenol A -2 54 E026 Separation of Trace Level Bisphenol A 54 E031 Separation of 4-Vinylguaiacol 55 E021 Separation of DNPH-Aldehydes-1 55 E022 Separation of DNPH-Aldehydes-2 55 E037 Separation of DNPH-Aldehydes-3 56 E038 Separation of DNPH-Aldehydes-4 56 Concerning Mightysil RP-18 GP series All columns with the "GP" title include the batch certificate. The guaranteed content is as follows. 1. The physical properties of the packing materials, and carbon content after bonding 2. Analytical results and Test-chromatograms of a separation with our own standard of test-mixtures Difference in entitling "GP"or not is only including a batch certificate or not. In addition, they are made with the same packing material. 02 CONTENTS FOOD 03 04 FOOD F001 Separation of Water-soluble Vitamins - 1 Column Mightysil RP-18 150-4.6mmØ 5μm Eluent Acetonitrile/ 20mM Phosphoric acid including 25mM of Sodium hexanesulfonate = 10/ 90 Flow Rate 1.0mL/min. Detection UV210nm 0.16AUFS Temperature 40°C Sample Vol. 5μL Samples 1. Nicotinic acid 50μg/mL 2. Nicotinamide 50μg/mL 3. Riboflavin phosphate sodium salt 50μg/mL 4. Pyridoxine hydrochloride (Vitamin B6) 200μg/mL 5. Riboflavin (Vitamin 2B ) 150μg/mL 6. Folic acid (Vitamin B9) 50mg/mL 7. Thiamin hydrochloride(Vitamin B1) 150μg/mL F002 Separation of Water-soluble Vitamins - 2 Column Mightysil RP-18 150-4.6mmØ 5μm Eluent Acetonitrile/ 20mM Phosphoric acid including 25mM of Sodium hexanesulfonate = 10/ 90 Flow Rate 1.0mL/min. Detection UV210nm 0.08AUFS Temperature 40°C Sample Vol. 5μL Samples 1. Pantothenic acid calcium salt 160μg/mL 2. Nicotinamide 20μg/mL 3. Pyridoxine hydrochloride (Vitamin B6) 40μg/mL 4. Riboflavin(Vitamin 2B ) 80μg/mL FOOD 05 F067 Separation of Vitamins Column Mightysil RP-18GP Aqua 250-4.6mmØ 5μm Eluent 0.1% Phosphoric acid containing 10mM Sodium hexanesulfonate/ Acetonitrile = 90/10 Flow Rate 1.0mL/min. Detection UV210nm Temperature 35°C Sample Vol. 5μL Samples 1. Nicotinic acid 0.05mg/mL 2. Pantothenic acid Calcium salt 0.3 mg/mL 3. Nicotinamide 0.05mg/mL 4. Riboflavin phosphate Sodium salt 0.2 mg/mL 5. Pyridoxine hydrochloride(VitaminB6) 0.05mg/mL 6. Riboflavin (VitaminB2) 0.15mg/mL 7. Folic acid (VitaminB9) 0.05mg/mL 8. Thiamine hydrochloride 0.15mg/mL F005 Separation of Fat-soluble Vitamins Column Mightysil RP-18 150-4.6mmØ 5μm Eluent Acetonitrile/ Methanol = 60/40 Flow Rate 1.0mL/min. Detection UV280nm 0.16AUFS Temperature 40ºC Sample Vol. 5μL Samples 1. Menadione (Vitamin K3) 0.25mg/mL 2. Retinol acetate (Vitamin A acetate) 0.09mg/mL 3. Ergocalciferol (Vitamin D2) 0.10mg/mL 4. Cholecalciferol (Vitamin D3) 0.10mg/mL 5. Tocopherol (Vitamin E) 0.75mg/mL 6. Tocopherol acetate (Vitamin E acetate) 1.00mg/mL 7. Phylloquinone (Vitamin K1) 0.50mg/mL 06 FOOD F070 F003 Separation of Vitamin C Separation of Vitamin D2, D3 Column Mightysil RP-18 250-4.6mmØ 5μm Column Mightysil RP-18GP Aqua 150-4.6mmØ 5μm Eluent Acetonitrile/ Water = 95/ 5 Eluent 1% Methaphosphoric acid Flow Rate 1.0mL/min. Flow Rate 1.0mL/min. Detection UV210nm 0.08AUFS Detection UV242nm Temperature Room Temperature Temperature Ambient Sample Vol.
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