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Nemc 20042004 TheThe 20th20th AnnualAnnual NationalNational EnvironmentalEnvironmental MonitoringMonitoring ConferenceConference NEMCNEMC 20042004 Monday, July 19th — Friday, July 23rd Proceedings Conference: Monday, July 19th – Wednesday, July 21st Short Courses: Thursday, July 22nd – Friday, July 23rd Wyndham Washington Hotel 1400 M Street, NW Washington, DC ILI QUALITY TRAINING FOR THE LABORATORY COMMUNITY NEMC is managed by the Independent Laboratory Institute (ILI), in association with the American Council of Independent Laboratories (ACIL) and Instant References Sources, Inc. under a cooperative agreement with the U.S. Environmental Protection Agency. ILI is the educational foundation affiliated with the American Council of Independent Laboratories. NEMC 2004 Organizing Committee Symposium Co-Chairs: David Friedman, US EPA, Office of Research and Development, Washington, DC Larry Keith, Instant Reference Sources, Inc., Monroe, GA Jan Young, US EPA, Office of Solid Waste, Washington, DC Program Committee Aruna Arakali, River Protection Project-Waste Treatment Plant, Richland, WA Lara Autry, US EPA, Office of Research and Development, RTP, NC Joan Walsh Cassedy, Independent Laboratories Institute, Washington, DC Deana Crumbling, US EPA, Technology Innovation Office, Washington, DC Jack Farrell, Analytical Excellence, Inc., Altamonte Springs, FL Daro Ferrara, Westinghouse Savannah River Company, Aiken, SC Maria Gomez-Taylor, US EPA, Office of Water, Washington, DC Skip Kingston, Duquesne University, Pittsburgh, PA Douglas Lipka, U.S. EPA Region 6 Laboratory, Houston, TX David E. Mills, NM Department of Health , Albuquerque, NM Elizabeth A. Mishalanie, EPA/OECA/OCEFT/NEIC, Denver, Colorado Anita Mishra, AOAC International, Gaithersburg, MD Marlene Moore, Advanced Systems, Inc., Baltimore, MD Anand R. Mudambi, US EPA, Analytical Operations/Data Quality Center, Washington, DC Tony Pagliaro, Bearing Point, McLean, VA Jerry Parr, Catalyst LLC, Weatherford, TX Oksana Pozda, US EPA, Office of Pollution Prevention and Toxics, Washington, DC Lynn Riddick, CSC/DynCorp, Alexandria, Virginia Grace M. Robiou, US EPA / Water Security Division, Washington, DC Debbie Schatzlein, Niton LLC, Billerica MA Deb Szaro, US EPA, Raritan Depot, Edison, NJ Charles Sellers, USEPA Headquarters, Washington, DC Joe Solsky, US Army Corps of Engineers, Omaha, NE Shannon Sturgeon, US EPA, Office of Solid Waste, Washington, DC Gary Ward, Columbia Analytical Services, Kelso, WA Llew Williams, Llew Williams Consulting, Naples, FL Shen-yi Yang, US EPA, Office of Solid Waste, Washington, DC th NEMC 2004 – 20 Annual National Environmental Monitoring Conference Table of Contents Welcome 3 Overview 4 Logistics 5 Hotel Information 7 Conference at a Glance 8 Technical Sessions (Titles linked to PowerPoint/Slides) Opening Plenary 10 Poster Session 10 Organic Methods – I 11 Inorganic Methods – I 11 Ensuring the Integrity of Laboratory Data 12 Characterization of Mixed Wastes at DOE Sites 12 Organic Methods – II 13 Inorganic Methods – II 13 Assessing Performance of New Methods 14 Innovative Approaches to Environmental Monitoring 14 Sampling and Analysis for Homeland Security – I 15 Laboratory Accreditation – I 15 Advances in Electronic Data Deliverables – I 16 Advances in Implementing the Triad Approach and Documenting 16 Measurement Uncertainty Sampling and Analysis for Homeland Security – II 17 Laboratory Accreditation – II 17 Advances in Electronic Data Deliverables – II 18 Roundtable: Changing Federal Requirements to Manage Environmental 18 Data Quality Short Courses 18 Papers (Titles linked to papers) Poster Session 19 Organic Methods – I 20 Inorganic Methods – I 20 1 th NEMC 2004 – 20 Annual National Environmental Monitoring Conference Ensuring the Integrity of Laboratory Data 21 Characterization of Mixed Wastes at DOE Sites 21 Organic Methods – II 22 Inorganic Methods – II 22 Assessing Performance of New Methods 23 Innovative Approaches to Environmental Monitoring 23 Sampling and Analysis for Homeland Security – I 24 Laboratory Accreditation – I 24 Advances in Electronic Data Deliverables – I 24 Advances in Implementing the Triad Approach and Documenting 25 Measurement Uncertainty Sampling and Analysis for Homeland Security – II 25 Laboratory Accreditation – II 26 Advances in Electronic Data Deliverables – II 26 Roundtable: Changing Federal Requirements to Manage Environmental 27 Data Quality Author Index 369 Notes 375 2 th NEMC 2004 – 20 Annual National Environmental Monitoring Conference Welcome Welcome to the 20th Annual National Environmental Monitoring Conference – NEMC 2004. The conference is managed by the Independent Laboratories Institute (ILI) in association with the American Council of Independent Laboratories (ACIL) and Instant Reference Sources, Inc. under a cooperative agreement with the U.S. Environmental Protection Agency (U.S. EPA). The symposium series was established as a means of fostering a partnership among the regulated community, its supporting laboratories and consultants and state and federal regulators. Key to implementing these goals are the technical sessions, composed of both oral and poster presentations, the table top exposition and a varied offering of short courses. The conference has continued to grow and diversify in spite of difficult economic and geopolitical times. This year again we have over 100 technical presentations in four concurrent oral presentation sessions, a poster session and a plenary session. This ties last year's record for this venerable conference, long-known as the Waste Testing and Quality Assurance Symposium (WTQA). In this year’s program, you will find papers that cover all aspects of environmental monitoring in all media (i.e., water, air, soil and wastes). Participants include experts from private industry, public agencies engaged in environmental monitoring (e.g., U.S. EPA, DOE, DoD and States) and academia. In addition to the long-standing sessions on organic methods and inorganic methods, we have added several new topics this year. For example, environmental monitoring as it relates to homeland security, laboratory accreditation, ensuring the integrity of laboratory data, analysis of DOE mixed wastes, assessing the performance of new methods and innovative approaches to environmental monitoring. Leveraging on popular topics from last year we have sessions on advances in implementation of the Triad approach and measurement uncertainty and also advances in electronic data deliverables. Finally, a round-table discussion on changing federal requirements to manage environmental data will present the newest information on this subject. Complementing the technical sessions are plenary session presentations from leaders in government and industry, a large table-top exposition and three short courses. Join us in a relaxed atmosphere at the complimentary Opening Reception on Monday evening. This reception is sponsored in part by the generous contributions of Annual Reviews, Dionex Corporation, Environmental Research Programs, Environmental Resources Associates, Environmental Standards, Inc. and Severn Trent Laboratories. Enjoy the conference, learn about changing technology, make new contacts, visit with old friends and let us know how we can help you. 3 th NEMC 2004 – 20 Annual National Environmental Monitoring Conference Overview General Schedule All sessions will take place at the Wyndham Washington Hotel, located at 1400 M Street, NW Washington, DC (Phone: 202-429-1700). Technical presentations and other sessions will run concurrently to allow participants the opportunity to attend those sessions most relevant to them. • Opening Plenary Session The opening plenary session will be held Monday, July 19th from 2:00–4:30 pm in the Monticello East and Monticello West rooms. • Oral Sessions Concurrent oral sessions will be held in four adjacent rooms on the Lobby Level from 8:15 am to 5:15 pm on July 20–21, 2004. Morning and afternoon sessions have three initial 30-minute presentations (which include time for questions), a 45 minute refreshment break and three final 30-minute presentations. Concurrent times for each presentation facilitate moving among various presentations if desired. • Poster Sessions All posters will be on display Tuesday, July 20th in the Vista B and C Ballrooms along with the Table Top Exhibition. Authors will be available to discuss their work from 9:45–10:30 am and from 3:00–3:45 pm each day. These times correspond to the breaks in the oral presentations. Poster boards 4' X 8' (with pins supplied) will be arranged for easy viewing and discussions with authors. • Short Courses Short courses will be offered Thursday and Friday, July 22 and 23, the days after the conference and each has an additional registration fee. Two full-day courses and one two-day course are offered. • Table Top Exhibition The Table Top Exhibition is in the Vista B and C Ballrooms along with the poster sessions. The exhibition is a feature of the Opening Reception on Monday evening from 5:00–6:30 pm and continues Tuesday and Wednesday, July 20-21 in conjunction with the poster presentations (on July 20) and the morning and afternoon refreshment breaks. • Opening Reception The opening reception will be held Monday, July 19th from 5:00–6:30 pm in the Vista B and C Ballrooms. Complimentary hors d'oeuvres and soft drinks will be served and a cash bar will also be available. The Table Top Exhibition is also a featured attraction of this reception. Please extend your thanks to representatives from Annual Reviews, Dionex Corporation,
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