Review of Pyrethroid, Fipronil and Toxicity Monitoring Data from California Urban Watersheds

Prepared for the California Stormwater Quality Association (CASQA)

Prepared by: Armand Ruby Armand Ruby Consulting

July 10, 2013

Preface and Acknowledgements

This investigation and the production of this report were funded by the California Stormwater Quality Association (CASQA) and the County of Sacramento. The work effort was coordinated through and performed with the assistance of the CASQA Pesticides Subcommittee, particularly subcommittee Co-Chairs Dave Tamayo and Jamison Crosby, as well as Kelly Moran of TDC Environmental, who provided the majority of the new data sources and carefully reviewed the draft documents.

This investigation includes literature and data sources (including unpublished data) available from public agencies and other reputable sources with documented quality control, as well as from sources published in the scientific literature. The responsibility for the accuracy and veracity of the various study results rests with the original authors. This compilation is as complete as was feasible as of early 2013, but almost certainly does not include every relevant study.

This report was prepared by: Armand Ruby Armand Ruby Consulting 303 Potrero St., #43-204 Santa Cruz, CA 95060 831-477-1214

Page ii Executive Summary

In recent years, numerous studies have documented the presence of pyrethroid pesticides and fipronil, as well as pesticide-caused toxicity, in both surface waters and sediments in California’s urban waterways. This report compiles and summarizes chemistry data from monitoring performed in urban areas of California for pyrethroid and fipronil pesticides, as well as related toxicity testing results, covering the ten year period from 2003-2012. Over 9200 pyrethroid sample analysis results and over 3200 fipronil results are evaluated and summarized.

Over the past ten years, pyrethroid pesticides have become the predominant group of chemicals deployed for insect control in urban areas in California (TDC Environmental, 2010b), and are the primary cause of toxicity in urban water bodies in the state (Anderson et al., 2011). The pyrethroids are synthetic versions of the naturally-occurring pyrethrins, but are more toxic and longer-lasting when released into the environment.

As state and federal regulatory actions have begun to address the widespread impacts of urban pyrethroid uses, alternative insecticides, particularly fipronil, are also of increasing concern (TDC Environmental, 2007). Fipronil has four relatively stable degradates that may contribute to aquatic toxicity. For that reason, this report also summarizes the results of recent monitoring for fipronil and its degradates.

Key Findings – Pyrethroids Bifenthrin, considered to be the leading cause of pyrethroid-related toxicity in urban areas (c.f., Weston et al., 2005; Amweg et al., 2006; Holmes et al., 2008, TDC Environmental, 2006), was detected most frequently of all the pesticides evaluated, in both water and sediment. Bifenthrin was detected in 69% in sediment samples and 64% in water samples.

Detection rates were generally higher for pyrethroids in sediment than in water. Permethrin was the most extreme case of this difference, detected in 50% of sediment samples but only 16% of water samples. Overall, pyrethroids were detected at a rate of 31% in sediments and 24% in water samples.

Pyrethroids were commonly found at concentrations exceeding levels known to cause toxicity to sensitive aquatic organisms in water. The average reported concentrations of bifenthrin, cyfluthrin, cyhalothrin, cypermethrin and permethrin in water samples range from approximately one to more than three orders of magnitude above the non-regulatory chronic criteria values published by UC Davis. Maximum reported concentrations of these five pyrethroids range from two to more than four orders of magnitude higher than the UC Davis acute criteria values.

For the seven pyrethroids for which sediment toxicity (LC50) values are available, the average concentrations reported in this summary would be substantially greater than the published LC50s, following organic carbon normalization. This means that, under average conditions in urban waterways in California, these pesticides are typically present in sediments at levels toxic to sensitive aquatic macroinvertebrates such as Hyalella azteca.

Page iii These comparisons may understate the actual potential for pyrethroids to cause toxicity to sensitive aquatic organisms, because they do not account for concurrent exposures to multiple pyrethroids. Multiple pyrethroids typically were found in each sample in the summarized chemistry studies, in both water and sediments. Because pyrethroid toxicity is generally understood to be additive (c.f., Trimble et al., 2009), the actual in-situ toxicity estimated from chemistry results should account for the mixtures of pyrethroids found.

Key Findings – Fipronil and Degradates Fipronil was detected in 39% of water samples tested from studies evaluated for this summary, and 19% of sediment samples. This contrasts with the pattern for most pyrethroids, for which there were typically higher percent detections in sediment. Presumably this reflects fipronil’s lower KOW, and/or fipronil’s relatively higher solubility in water.

The fipronil degradates as a group were detected analytically in 24% of the water samples tested from studies evaluated for this study, and in 35% of sediment samples. This pattern is similar to that of the pyrethroids.

Published aquatic toxicity values for fipronil are in the sub-ppb (µg/L) range (c.f., Gunasekara and Troung, 2007 and Mize et al., 2008). Maximum observed levels of fipronil and its degradates in water samples were higher than these LC50 values.

Key Findings – Toxicity Toxic effects are documented in both water and sediment in urban waterways throughout California. Effects of pyrethroids on aquatic organisms are widespread throughout the aquatic environment, as documented in studies involving water column toxicity testing, sediment toxicity testing, and tissue analysis. Of the 25 toxicity studies that were summarized, all reported some level of toxicity for one or more organisms tested.

Research has for some time now indicated widespread sediment toxicity in urban areas of California (c.f., Amweg et al., 2005, Amweg et al., 2006, Anderson et al., 2011, Holmes et al., 2008, Weston et al. 2005), with pyrethroids often identified as the apparent cause of the toxicity.

Recent research also highlights the toxic effects of pyrethroids in water column samples. For example, Weston and Lydy (2012) found toxicity in a majority of urban creek and river samples tested during 2009-10 rain events. Toxicity Identification Evaluations (TIEs) and water chemistry testing identified pyrethroids as the principal cause of the water column toxicity.

Geographical Summary Evidence of the presence and effects of pyrethroids and fipronil, and associated toxic effects in urban watercourses, is widely distributed geographically throughout urbanized areas of the state of California. This review identified such data from the north coast, Lake Tahoe region, San Francisco Bay Area, Central Valley, Central Coast, and both coastal and inland areas of southern California. Pyrethroid-related toxicity has been documented in nearly every major urban watershed in the state and in eight of the nine California Water Board regions.

Page iv TABLE OF CONTENTS

Preface and Acknowledgements ii Executive Summary iii Background and Introduction 1 Scope of Review and Approach 5 Findings 6 Recommendations 19 Conclusions 19 References 20

Appendix A: “Study Summaries by Author” Table Appendix B: “Results Summaries by Geography” Table Appendix C: “Chemistry Results Summary” Table Appendix D: “Toxicity Results Summary” Table

Page v Background and Introduction

Legal uses of some registered pesticides have been found to result in adverse impacts to water quality and aquatic life in receiving waters within urban areas (see summary and references in TDC Environmental, 2010a). Over the past ten years, pyrethroid pesticides have become the predominant group of chemicals deployed for insect control in urban areas in California (TDC Environmental, 2010b). During this period, observations of pyrethroids and pyrethroid-caused toxicity in urban runoff and receiving waters have multiplied, increasingly resulting in listings of urban waterways on the Clean Water Act Section 303(d) List of Impaired Waters for California (the “303(d) List”; State Water Resources Control Board, 2011).

Urban pyrethroid use increased dramatically beginning in the early 2000’s, when most urban uses of the organophosphate pesticides diazinon and chlorpyrifos were curtailed by the United States Environmental Protection Agency (USEPA). In response, other pesticides, principally pyrethroids, were substituted as the active ingredients most commonly used for urban pest management. The pyrethroids are synthetic versions of the naturally-occurring pyrethrins, but are more toxic and longer-lasting when released into the environment. In recent years, numerous studies have documented the presence of pyrethroid pesticides and pesticide-caused toxicity in both surface waters and sediments in California’s urban waterways. This report compiles and summarizes those findings.

Within urban areas, pesticides are often applied directly and intentionally to impervious surfaces, and applications to impervious surfaces are considered to be the controlling factor in urban runoff contributions to receiving water toxicity (Moran and TenBrook, 2011). The relatively low aqueous solubility and high octanol-water partition coefficient (KOW) of most pyrethroids indicate that these chemicals are likely to partition to suspended particulates in runoff and accumulate in the sediments of receiving waters. Studies in California waterways have shown that sediments contaminated with pyrethroid pesticides are frequently toxic to sediment-dwelling organisms (c.f., Weston et al., 2005; Amweg et al., 2006; Holmes et al., 2008). However, as documented in this report, pyrethroid pesticides are commonly found in both the waters and sediments of urban watercourses throughout California.

With nearly 700 pyrethroid products available to professional pest control operators and consumers in California, it is common for multiple pyrethroids to be present in the water and sediments of urban receiving waters, as shown by numerous studies summarized in this report. Studies involving urban monitoring data have demonstrated that mixtures of pyrethroids are contributing to pyrethroid-related toxicity in both water and sediments in urban creeks, and pyrethroid toxicity is generally considered to be additive in such mixtures (c.f., Trimble et al. 2009, Anderson et al., 2011).

As state and federal regulatory actions have begun to address the widespread impacts of urban pyrethroid uses, replacement insecticides, particularly fipronil, are also of increasing concern (TDC Environmental, 2007). For that reason, this report also summarizes the results of recent monitoring data for fipronil and its degradates.

Page 1 Table 1 provides a summary of available water column toxicity information pertaining to pyrethroid pesticides, with references. What is most notable about the information presented in Table 1 is that the pyrethroids are generally toxic to the most sensitive aquatic arthropods at extremely low levels – generally at concentrations in the single-digit (or lower) nanograms per liter (ng/L) (parts per trillion) range. As shown in Table 1, toxicity studies typically identify the LC50, the concentration that is lethal on average to 50% of the test organisms, and/or the EC50, the concentration at which a sub-lethal effect is observed on average to 50% of the test organisms. The Toxicity Values shown in Table 1 illustrate the greater sensitivity of Hyalella azteca to pyrethroids compared to Ceriodaphnia dubia, the test species most commonly used to identify water toxicity due to organophosphate pesticides.

USEPA has not developed recommended water quality criteria for the protection of aquatic life for pyrethroids (or for many other current-use pesticides), as it has for other common water pollutants. Therefore Table 1 summarizes other, non-regulatory information that can be used as comparison values to evaluate the data compiled for this report. The available comparison values include water quality criteria values developed by UC Davis, as described below, as well as USEPA Aquatic Life Benchmark values.

To address recent pyrethroid-related additions to the 303(d) List within the Sacramento and San Joaquin River watersheds, the Central Valley Regional Water Quality Control Board (RWQCB) is developing a Basin Plan amendment to establish water quality objectives and Total Maximum Daily Loads (TMDLs) for waterbodies that are listed for pyrethroids on the 303(d) list, and a program of implementation for the control of pyrethroid pesticide discharges. This effort is part of a broader program to establish water quality objectives and a program of implementation for the control of pesticides that are impacting or could potentially impact aquatic life uses in surface waters in the Sacramento and San Joaquin River watersheds of the Central Valley, including the Delta. To support the development of pesticide water quality objectives and TMDLs, the Central Valley RWQCB contracted with the Environmental Toxicology Department of the University of California, Davis (UC Davis) to develop and evaluate a methodology for development of aquatic life criteria. Under this contract, to date UC Davis has developed acute and chronic criteria values for five pyrethroid pesticides, as shown in Table 1. The Central Valley RWQCB is still in the process of determining whether or how to make use of the UC Davis criteria values in the development of pyrethroid TMDLs for Central Valley watersheds. The context for the development of these criteria is explained in the “Sacramento and San Joaquin River Watersheds Pesticide Basin Plan Amendment Fact Sheet” (Central Valley RWQCB, 2006).

Table 2 provides the available water column toxicity information for fipronil and its principal degradate compounds, as well as the corresponding USEPA Aquatic Life Benchmarks.

There are limited sediment toxicity values available for pyrethroids and fipronil/degradates, and no corresponding comparison values for sediment (UC Davis criteria or USEPA aquatic life benchmarks). The available published sediment toxicity LC50 values are included for pyrethroids in Table 5 and for fipronil/degradates in Table 7.

Page 2 Table 1. Pyrethroids Water Column Toxicity and Comparison Values (ng/L) Species Bifenthrin Cyfluthrin Cypermethrin Deltamethrin Esfenvalerate Lambda- Permethrin Tralomethrin Cyhalothrin Fresh Water Toxicity Values Hyalella azteca 7.5 2.4 2.5 8 21.1 96-hr LC50 (lethal) Hyalella azteca 3.3 1.9 1.7 2.3 96-hr EC50 (sub-lethal effects) Ceriodaphnia dubia 70 140 300 550 48-hr LC50 (96-h) (lethal) Salt Water Toxicity Values Americamysis bahia 4 2.4 5 1.7 38 20 (Mysidopsis bahia) 96-hr EC50 (sub-lethal effects) Comparison Values U.C. Davis acute 4 0.3 1 1 10 criterion value (1-hr) U.C. Davis chronic 0.6 0.05 0.2 0.5 2 criterion value (96-hr) Lowest USEPA 1.3 7 69 4.1 17 2 1.4 4.4 Pesticide Aquatic life benchmark Notes for Table 1: Compiled by TDC Environmental, 11/30/11; data not verified for this report. Note: No USEPA water quality criteria exist for any pyrethroid. No data are available for sensitive aquatic species for these pyrethroids (therefore excluded from table): Allethrins, tau-fluvalinate, tetramethrin. Pyrethroids excluded because they are not used in urban areas: fenvalerate, fenpropathrin. Pyrethroid toxicity is usually additive. Toxicity usually correlates with the sum of toxic units (sum of pyrethroid concentrations divided by their toxicity values). Sources for Toxicity Values: Werner and Moran, 2008; Weston and Jackson, 2009; Mokry and Hoagland, 1990; Maund et al., 1998; Anderson et al., 2006. UC Davis criteria development reports (Brander et al., 2010; Fojut et al., 2010; Fojut and Tjeerdema, 2010; Fojut et al., 2011a; Fojut et al., 2011b) are available on the Central Valley Regional Water Quality Control Board website: http://tinyurl.com/2etvvg3 U.S. EPA Aquatic Life Benchmarks website: http://www.epa.gov/oppefed1/ecorisk_ders/aquatic_life_benchmark.htm

Page 3 Table 2. Fipronil and Degradates Water Column Toxicity and Comparison Values (ng/L) Fipronil Fipronil Fipronil Fipronil Species Fipronil Desulfinyl Sulfone Sulfide Desulfinyl Amide d Fresh Water Toxicity Values Lepomis 25,000 - macrochirus 25,000 a 20,000 a 83,000 a 96-hr LC50 Chironomus tentans 410 c 720 c 2,130 c 200,000 c 96-hr LC50 Salt Water Toxicity Values Americamysis bahia 140 a 1,500 b 96-hr LC50 Comparison Values

Lowest U.S. EPA Aquatic Life 11 37 110 590

Benchmark

Notes for Table 1: Compiled by TDC Environmental; data not verified for this report. Sources for Table 2: a = Gunasekara and Troung, 2007 (DPR) b = Konwick et al., 2005 c = U.S. EPA, 2011. Registration Review – Preliminary Problem Formulation for Ecological Risk and Environmental Fate, Endangered Species, and Drinking Water Assessments for Fipronil. d = no comparison value data available for this compound U.S. EPA Aquatic Life Benchmarks website: http://www.epa.gov/oppefed1/ecorisk_ders/aquatic_life_benchmark.htm

Page 4 Scope of Review and Approach

This report summarizes available chemistry data for pyrethroid pesticides and for fipronil and its degradates, as well as related results of toxicity testing, from monitoring performed in urban areas of California. The current report updates and expands upon the initial Pyrethroids Data Compilation produced for CASQA in 2008 (Ruby, 2008). Data from predominantly agricultural areas were excluded from the summaries. Otherwise, no attempt was made to distinguish the specific land use composition of contributing watersheds for the various study results. In some cases, the monitoring was performed in waterways that include contributions from a variety of land use types, but in all cases the monitored watershed includes an urban component.

Primary information sources include published scientific literature, as well as unpublished data produced under the direction of public agencies. All primary information sources are clearly referenced, including web links where available.

This report provides summaries of the various study results as provided by the study authors. Where the underlying data or statistical summaries of the data were available, this report also separately summarizes the chemistry and toxicity testing data. Distinctions are made for data produced from water vs. sediment matrices, and from urban runoff discharges vs. receiving waters (i.e., named water bodies that receive urban runoff discharges). The investigation was limited to surface waters; results of groundwater monitoring are not included.

The Chemistry Results Summary and Toxicity Results Summary tables contain data only for more recent studies, generally those published during 2008-2012, covering data generated since ca. 2005. This compilation is as complete as was feasible as of mid-calendar year 2012, but may not include every relevant study. Ongoing and planned monitoring undoubtedly will continue to reveal additional evidence of the presence of pyrethroids and other pesticides - and related effects - in California’s urban watersheds. This work should be updated periodically to incorporate additional material as it becomes available. This will be particularly important as other insecticides, beyond fipronil, become more commonly used. The underlying spreadsheets upon which this report’s tables are based are readily expandable, and can be updated over time.

Notes regarding nomenclature and approach used in this study: x Chemical names, rather than brand names, are used to designate the pesticides. x Like pyrethrins, pyrethroids have multiple chiral isomers. Most commercial products are comprised of mixtures of these isomers (e.g., permethrin is generally available as a mixture of cis-permethrin and trans-permethrin). Only a few pyrethroids appear as single isomers in commercial products (e.g., esfenvalerate, beta-cyfluthrin). Although it is known that chirality can affect toxicity (Gerlach, 2012), not enough information is available to adequately assess this factor in the context of the current report, in part because most laboratories do not report results on an isomer-specific basis. For purposes of this summary, where isomer-specific data are available, these have been totaled by chemical (e.g., “permethrin” includes the sum of available data for cis-permethrin and trans-permethrin).

Page 5 x The summary tables generally exclude studies that relied on chemical analysis methods that are incapable of detecting pyrethroids at the ng/L (water) or ng/g (sediment) concentration levels, as non-detect results at higher analytical detection levels do not indicate whether potentially harmful concentrations of pyrethroids are actually present.

Findings

There is an expanding diversity of research focusing on the presence and effects of pesticides in the environment within California. Earlier (pre-2000) research on pesticides effects focused principally on agricultural areas, but that has changed in recent years. Many studies are now available documenting the presence and effects of pyrethroids and other pesticides in urban areas. Over 100 studies were evaluated for this project. After eliminating reports presenting repeat data, purely methods research projects, and studies involving predominantly agricultural watersheds, summaries are provided for over 80 studies. Many more projects and studies are currently being undertaken or planned. Over 9200 pyrethroid sample analysis results and over 3200 results for fipronil and degradates were evaluated and summarized for this report.

Summary of Findings – Pyrethroid Pesticides Pyrethroids are frequently detected at quantifiable levels in both water and sediment in urban waterways throughout California. For environmental contaminants such as pesticides, the rate of analytical (laboratory) detection is an important metric, as it indicates how frequently the pesticide is observed at a quantifiable level in environmental samples. Due to the very low concentrations at which many of these pesticides can cause toxicity, the rate of detection is a useful indicator of the extent to which these chemicals are migrating from the site of application to the aquatic environment. The rates of analytical detection from the summarized chemistry results are presented in Table 3 for the most commonly-detected pyrethroids. This table generally summarizes chemistry data for the more recent studies evaluated (those published since 2005). Because detection rates are only relevant for studies that employ environmentally relevant detection limits, this summary focuses on studies that reported chemical analysis methods capable of detecting pyrethroids at the ng/L (water) or ng/g (sediment) concentration levels. Results are shown separately for water and sediment samples.

Bifenthrin, considered to be the leading cause of pyrethroid-related toxicity in urban areas (c.f., Weston et al., 2005; Amweg et al., 2006; Holmes et al., 2008, TDC Environmental, 2006), was detected most frequently of all the pesticides evaluated, in both water and sediment. For samples tested in studies evaluated for this summary, the rate of analytical detection for bifenthrin was 69% in sediment samples and 64% in water samples, as indicated in Table 3.

Detection rates were generally higher for pyrethroids in sediment than in water. Permethrin was the most extreme case of this difference, detected in 50% of sediment samples but only 16% of water samples. Overall, pyrethroids were detected at a rate of 31% in sediments and 24% in water samples.

Page 6 Table 3. Analytical Detection Rates – Pyrethroids

# % WATER SAMPLES: Samples Detected Allethrin 235 0.4% Bifenthrin 748 64% Cyfluthrin 847 28% Cyhalothrin 663 22% Cypermethrin 503 31% Deltamethrin/Tralomethrin 533 5% Esfenvalerate/Fenvalerate 704 19% Fenpropathrin 306 21% Fluvalinate 224 3% Permethrin 1,146 16% Phenothrin 5 0% Prallethrin 219 2% Resmethrin 175 0% Tetramethrin 16 6% All Pyrethroids 6,511 24%

# % SEDIMENT SAMPLES: Samples Detected Allethrin 64 0% Bifenthrin 359 69% Cyfluthrin 324 33% Cyhalothrin 334 30% Cypermethrin 284 29% Deltamethrin/Tralomethrin 252 22% Esfenvalerate/Fenvalerate 314 12% Fenpropathrin 147 16% Fluvalinate 59 3% Permethrin 367 50% Phenothrin 8 13% Prallethrin 46 0% Resmethrin 117 3% Tetramethrin 23 0% All Pyrethroids 2,704 31%

Notes for Table 3: Table summarizes data for more recent studies evaluated (generally published since 2005). This summary generally includes only data from studies that relied on chemical analysis methods capable of detecting pyrethroids at the ng/L (water) or ng/g (sediment) concentration levels. Fenpropathrin (trade name, Danitol) has no registered urban uses; the levels of detection may reflect results from mixed-use watersheds and/or drift from agricultural areas to urban watersheds.

Page 7 Pyrethroid Concentrations – Water Pyrethroids were commonly found at concentrations exceeding levels known to cause toxicity to aquatic organisms in water. The average and maximum concentrations from the summarized water chemistry results are presented in Table 4 for the pyrethroids, along with the relevant acute and chronic aquatic toxicity comparison values from Table 1. This table generally summarizes chemistry data for the more recent studies evaluated (those published since 2005).

For all five pyrethroids for which there are UC Davis chronic toxicity criteria comparison values in Table 1, the average observed environmental concentration is higher than the chronic toxicity comparison value. The average reported concentrations of bifenthrin, cyfluthrin, cyhalothrin, cypermethrin and permethrin in water samples range from approximately one to more than three orders of magnitude above the chronic criteria values published by UC Davis (from Table 1).

Maximum reported concentrations of these five pyrethroids are in the range of two to more than four orders of magnitude higher than the UC Davis acute criteria values (from Table 1). The most prominent examples from Table 4 include: x The maximum reported concentration of bifenthrin in water was 398 ng/L, compared to the UC Davis acute criterion value of 4 ng/L; x The maximum reported concentration of cypermethrin in water was 519 ng/L, compared to the UC Davis acute criterion value of 1 ng/L; x The maximum reported concentration of permethrin in water was 12,652 ng/L, compared to the UC Davis acute criterion value of 10 ng/L.

Pyrethroid Concentrations – Sediment The average and maximum concentrations from the summarized sediment chemistry results are presented in Table 5 for the pyrethroids. Published LC50 values exist for Hyalella azteca exposure in sediments for several pyrethroids (Amweg, et al., 2005; Maund et al., 2002). However, because organic carbon helps mitigate pyrethroid toxicity to invertebrates in sediments, these LC50 values are expressed as µg/g organic carbon. Conversion of the statewide sediment data to the organic carbon-normalized format was beyond the scope of this report (and not all sources provide organic carbon data). Nonetheless, for the seven pyrethroids for which sediment LC50 values are available, it is apparent that the average concentrations reported in Table 5 would be substantially greater than the published LC50s following organic carbon normalization, assuming a typical organic carbon level of 1-3 percent for California sediments (c.f., Amweg et al., 2005). This means that, under average conditions in urban waterways in California, these pesticides are typically present at levels toxic to sensitive macroinvertebrates such as Hyalella azteca in sediments. As shown in Table 5, the level of exceedance of the average reported concentration over the LC50 value is particularly significant for bifenthrin.

Multiple Pyrethroids Commonly Detected Multiple pyrethroids typically were found in each sample in the summarized chemistry studies, in both water and sediment samples. Because pyrethroid toxicity is generally considered to be additive (c.f., Trimble et al., 2009), the actual in-situ toxicity estimated from chemistry results must account for the mixtures of pyrethroids and other pesticides found.

Page 8 Table 4. Average and Maximum Reported Pyrethroid Concentrations (Water) Compared to U.C. Davis Criteria Values

Ratio of Ratio of UC Davis Average UC Davis Maximum Chronic Conc.: Acute Conc.: Average Maximum Criterion Chronic Criterion Acute Conc. Conc. Value Criterion Value Criterion WATER SAMPLES: (ppt) (ppt) (ppt) Value (ppt) Value Allethrin 0.203 9.50 Bifenthrin 26 398 0.6 43 4 100 Cyfluthrin 14.9 423 0.05 298 0.3 1409 Cyhalothrin 4.80 243 0.5 10 1 243 Cypermethrin 13.3 519 0.2 66 1 519 Deltamethrin/Tralomethrin 1.40 252 Esfenvalerate/Fenvalerate 1.43 36.8 Fenpropathrin 4.80 459.9 Fluvalinate 0.566 154.8 Permethrin 51.2 12652 2 26 10 1265 Phenothrin ND ND Prallethrin 2.13 287 Resmethrin ND ND Tetramethrin 0.219 2.80

Notes for Table 4: Table summarizes data for more recent studies evaluated (generally published since 2005). “Average” concentrations = mean values of mean concentrations reported from summarized studies. “ppt” = parts per trillion “ND” means all data were reported as non-detect. Water column toxicity criteria comparison values shown are the UC Davis chronic and acute criteria; see Table 1 for references. Fenpropathrin has no registered urban uses; the reported concentrations may reflect results from mixed-use watersheds and/or drift from agricultural areas to urban watersheds.

Page 9 Table 5. Average and Maximum Reported Sediment Concentrations – Pyrethroids

Published LC50 Values Average Max. (µg/g Conc. Conc. organic SEDIMENT SAMPLES: (ppb) (ppb) carbon) Allethrin ND ND Bifenthrin 45.8 744 0.52 Cyfluthrin 17.4 187 1.08 Cyhalothrin 4.64 31.9 0.45 Cypermethrin 10.1 987.5 Deltamethrin/Tralomethrin 5.11 78.0 0.79 Esfenvalerate/Fenvalerate 1.47 20.3 1.54 Fenpropathrin 0.393 8.8 Fluvalinate 0.080 3.60 Permethrin 27.8 539 10.83 Phenothrin 0.661 0.750 Prallethrin ND ND Resmethrin 2.03 24.0 Tetramethrin ND ND

Notes for Table 5: Table summarizes data for more recent studies evaluated (generally published since 2005). “Average” concentrations = mean values of mean concentrations reported from summarized studies. “ND” means all data were reported as non-detect. “ppb” = parts per billion Published LC50 Values (Amweg et al., 2005; Maund et al., 2002) are reported as organic carbon- normalized values (µg/g organic carbon), calculated by dividing the measured pyrethroid concentration by the measured percent organic carbon in the sediment sample. The organic carbon- normalized LC50 values therefore cannot be directly compared to the average or maximum observed concentrations for pyrethroids in sediments. The organic carbon-normalized average and maximum pyrethroid concentrations would be higher than those shown by a factor of roughly 33-100, assuming typical sediment organic carbon concentrations of 1-3%. Fenpropathrin has no registered urban uses; the reported concentrations may reflect results from mixed-use watersheds and/or drift from agricultural areas to urban watersheds.

Page 10 Summary of Findings – Fipronil and Degradates The non-pyrethroid pesticide, fipronil, is a leading replacement for pyrethroid pesticides in urban areas (TDC Environmental, 2007). Fipronil has multiple degradates, some of which are more environmentally stable than fipronil itself, and some of which have equal or greater aquatic toxicity than the parent compound. Fipronil and its degradates also are frequently detected in both water and sediment in urban watercourses. Data were identified for Fipronil Amide, Fipronil Desulfinyl, Fipronil Desulfinyl Amide, Fipronil Sulfide, and Fipronil Sulfone. The rates of analytical detection from the summarized chemistry results are presented in Table 6 for fipronil and its degradates. Results are shown for both water and sediment samples.

Fipronil was detected in 39% of water samples tested from studies evaluated for this summary, and 19% of sediment samples. This is in contrast to the pattern for most pyrethroids, for which there were typically higher percent detections in sediment. Presumably this reflects fipronil’s lower KOW, and/or fipronil’s relatively higher solubility in water.

The fipronil degradates as a group were detected analytically in 24% of the water samples tested from studies evaluated for this study, and 35% of sediment samples. This pattern is similar to that of the pyrethroids.

Table 6. Analytical Detection Rates – Fipronil and Degradates

# % WATER SAMPLES: Samples Detected Fipronil 871 39% Fipronil degradates 2,271 24%

# % SEDIMENT SAMPLES: Samples Detected Fipronil 16 19% Fipronil degradates 48 35%

Notes for Table 6: Table summarizes data for more recent studies evaluated (generally published since 2005). “Fipronil degradates” included are: Fipronil Amide, Fipronil Desulfinyl, Fipronil Desulfinyl Amide, Fipronil Sulfide, and Fipronil Sulfone.

The average and maximum concentrations from the summarized chemistry results are presented in Table 7 for fipronil and the group of fipronil degradates. As shown in Table 2, some published aquatic toxicity values and all of the published USEPA benchmarks for fipronil and its principal degradates are in the sub-ppb (µg/L) range. Average fipronil concentrations in water samples were higher than the USEPA Aquatic Life Benchmark for fipronil, while average concentrations of the fipronil degradates were in the range of the associated USEPA benchmarks, as shown in Table 7. The maximum reported concentrations for fipronil and its degradates in water samples were well above the USEPA benchmarks. Similarly, the maximum reported concentrations of fipronil and its degradates in sediment samples were well above published LC50 values.

Page 11 Table 7. Average and Maximum Reported Concentrations in Water and Sediment – Fipronil and Degradates US EPA Aquatic Average Max. Life Conc. Conc. Benchmark WATER SAMPLES: (ppt) (ppt) (ppt) Fipronil 89.7 10004 11 Fipronil degradates 71.2 1961 37-590

Published LC50 Values Average Max. (µg/g SEDIMENT Conc. Conc. organic SAMPLES: (ppb) (ppb) carbon) Fipronil 0.078 0.30 0.13 Fipronil degradates 0.297 2.60 0.12-0.16

Notes for Table 7: Table summarizes data for more recent studies evaluated (generally published since 2005). Water sample results are reported as ppt (parts per trillion), while sediment results are reported as ppb (parts per billion). “Average” concentrations = mean values of mean concentrations reported from summarized studies. “Fipronil degradates” included are: Fipronil Amide, Fipronil Desulfinyl, Fipronil Desulfinyl Amide, Fipronil Sulfide, and Fipronil Sulfone. Published sediment LC50 Values (Maul et al., 2008) are reported as organic carbon-normalized values (µg/g organic carbon), calculated by dividing the measured pyrethroid concentration by the measured percent organic carbon in the sediment sample. The organic carbon-normalized LC50 values therefore cannot be directly compared to the average or maximum observed concentrations for pyrethroids in sediments. The organic carbon-normalized average and maximum fipronil concentrations would be higher than those shown by a factor of roughly 33-100, assuming typical sediment organic carbon concentrations of 1-3%.

Summary of Findings – Toxicity Toxic effects are documented in both water and sediment in urban waterways throughout California. Effects of pyrethroids on aquatic organisms are widespread throughout the aquatic environment, as documented in studies involving water column toxicity testing, sediment toxicity testing, and tissue analysis. Of the 25 toxicity studies that were summarized, all reported some level of toxicity for one or more organisms tested.

There has been a notable shift in aquatic (water column) toxicity in urban areas since the phase- out of urban uses of diazinon and chlorpyrifos in the early 2000s. Prior to that time, samples of urban runoff and urban creeks were frequently found to be toxic to Ceriodaphnia, with the organophosphate pesticides diazinon and chlorpyrifos commonly identified as the likely causes (c.f., San Francisco Bay Regional Quality Control Board, 2005; Anderson et al., 2011). Since the federally mandated restrictions in diazinon and chlorpyrifos took effect, there have been few

Page 12 reports of toxicity to Ceriodaphnia, from samples collected in urban (non-agricultural) waters, and few reports of toxicity due to the organophosphate pesticides.

The common amphipod, Hyalella azteca, is more sensitive to pyrethroid pesticides than other common test species (Amweg et al., 2005; Anderson et al., 2011). Data reviewed for this report show that urban waters in recent years frequently have exhibited toxicity to Hyalella azteca, with pyrethroids as the likely cause, based on TIEs and correlations with pyrethroid chemical concentration data (see also a summary in Anderson et al., 2011).

Early research into the toxic effects of pyrethroids as replacement pesticides for the organophosphate pesticides indicated widespread sediment toxicity in urban areas of California (c.f., Amweg et al., 2005, Amweg et al. 2006, Holmes et al., 2008, Weston et al. 2005). In these studies, pyrethroids were identified as the apparent cause of the sediment toxicity.

While the toxic effects of pyrethroids in sediments have now been thoroughly documented, recent research also highlights the toxic effects of pyrethroids in water column samples. For example, Weston and Lydy (2012) found that water samples from five of seven creeks tested during a 2009 rain event were toxic to Hyalella, with acute toxicity (mortality or paralysis) rates in the toxic samples ranging from 74% to 96%. Over half (52%) of water samples from two stations in the lower American River collected during storm events in 2009-2010 were acutely toxic to Hyalella. TIEs and water chemistry testing were used to identify pyrethroids as the cause of most of the observed water column toxicity.

The results of a number of the toxicity studies that are summarized in this report were further evaluated in a 2011 SWAMP report entitled, Toxicity in California Waters (Anderson et al, 2011). The reader is referred to that report for additional information on state-sponsored toxicity studies conducted during the period 2001-2010. The period of the SWAMP review spans the transition from the phase-out of orthophosphate pesticides to the rise in prominence of pyrethroids as replacement pesticides. The study includes discussions of comparisons of toxicity test results among urban, agricultural, and open space locations, as well as the findings from toxicity identification studies (TIEs) linking specific pesticides to toxicity.

Geographical Summary Lists of the water bodies for which data were summarized are shown in Table 8a (Northern and Central California) and Table 8b (Southern California), and then alphabetically by water body name within each of those two regions.

Evidence of the presence and effects of pyrethroids and fipronil, and associated toxic effects in urban watercourses, is widely distributed geographically throughout the state of California. The review identified data from the North Coast, Lake Tahoe region, San Francisco Bay Area, Central Valley, Central Coast, and both coastal and inland areas of Southern California. Pyrethroid-related toxicity has been documented in nearly every major urban watershed in the state and eight of the nine California Water Board regions.

Page 13 Table 8a. Northern/Central California Monitoring Locations with Reported Chemistry/Toxicity Results

Water Board Monitoring Location(s) Geographic Area Region Alamo Creek Solano County 5 Alder Creek Sacramento County 5 Alisal Creek Monterey County 3 American Canyon Creek Napa County 2 American River Sacramento County 5 Arcade Creek Sacramento County 5 Blue Rock Springs Solano County 2 Bodega Bay Sonoma County 1 Carpinteria Salt Marsh Santa Barbara County 3 Castro Valley Creek Alameda County 2 Chicken Ranch Slough Sacramento County 5 Corte Madera Creek Marin County 2 Coyote Creek (fresh) Santa Clara County 2 Coyote Creek (tidal) Santa Clara County 2 Curry Creek Sarasota County 5 Dry Creek Roseville 5 Ducker Creek Sonoma County 1 Elder Creek Sacramento County 5 Elk Grove storm drains Sacramento County 5 Gabilan Creek Monterey County 3 Glen Echo Creek Alameda County 2 Grayson Creek Contra Costa County 2 Hinebaugh Creek Sonoma County 1 Hospital Creek San Joaquin County. 5 Ingram Creek San Joaquin County. 5 Jane's Creek Meadows Humboldt County 1 Kaseberg Creek Roseville 5 Kirker Creek Contra Costa County 2 Koopman Canyon Creek Alameda County 2 Laguna Creek Sacramento County 5 Lauterwasser Creek Contra Costa County 2 Lion Creek City of Oakland 2 Mammoth Creek Tahoe/Lahontan Area 6 Marsh Creek Contra Costa County 5 Martin Canyon Creek Alameda County 2 Merced River Merced County 5 Napa River (fresh) Napa County 2

Page 14 Napa River (tidal) Napa County 2 Natividad Creek Monterey County 3 Natomas drain Sacramento County 5 Petaluma River (fresh) Sonoma County 2 Petaluma River (tidal) Marin County 2 Pine Creek Contra Costa County 2 Pleasant Grove Creek Placer County 5 Quimby Creek Santa Clara County 2 Rheem Creek Contra Costa County 2 Roseville storm drains Placer County 5 Sacramento River Sacramento County 5 Sacramento-San Joaquin Delta Sacramento County 5 Salinas urban creeks Salinas 3 San Francisquito Creek San Mateo/Santa Clara Counties 2 San Joaquin River San Joaquin R. Valley 5 San Joaquin River tributaries San Joaquin R. Valley 5 San Leandro Creek Alameda County 2 San Lorenzo Creek San Leandro 2 San Mateo Creek San Mateo County 2 San Pablo Creek Contra Costa County 2 South Branch Roseville 5 Stanislaus Creek Stanislaus County 5 Stege Marsh Contra Costa County 2 Stevens Creek Santa Clara County 2 Stockton Creek Sacramento County 5 Strong Ranch Slough Sacramento County 5 Suburban watershed Bodega Bay 1 Suisun Slough Tributary Solano County 2 Sump 111 Sacramento County 5 Tahoe Keys Tahoe/Lahontan Area 6 Truckee River Swale Tahoe/Lahontan Area 6 Tuolumne Creek Stanislaus County 5 Ulatis Creek Solano County 5 Willow Creek Sacramento County 5

Page 15 Table 8b. Southern California Monitoring Locations with Reported Chemistry/Toxicity Results

Water Board Monitoring Location(s) Geographic Area Region Agua Hedionda Creek San Diego County 9 Arroyo Seco Channel Los Angeles County 4 Ballona Creek Los Angeles County 4 Ballona Creek Estuary Los Angeles County 4 Bouquet Canyon Creek Los Angeles County 4 Calleguas Creek Ventura County 4 Cole Creek Riverside County 8 Chollas Creek San Diego County 9 Chollas Creek - North Fork San Diego County 9 Chollas Creek - South Fork San Diego County 9 Conejo Creek Calleguas Creek Watershed 4 Cottonwood Creek San Diego County 9 Huntington Harbor tributaries Huntington Harbor/Orange County 8 Los Angeles River Los Angeles County 4 Lindo Lake San Diego County 9 Long Canyon Channel Riverside County 8 Los Peñasquitos Creek San Diego County 9 Mugu Lagoon Ventura County 4 Murrieta Creek Riverside County 9 N. Fork Arroyo Conejo Calleguas Creek Watershed 4 New River at Boundary Calexico 9 Newport Harbor Orange County 8 Newport Harbor tributaries Orange County 8 Peters Canyon Wash Orange County 8 Revolon Slough Calleguas Creek Watershed 4 Redhawk Channel Riverside County 8 Salt Creek watershed Orange County 8 San Diego River San Diego County 9 San Diego Harbor San Diego County 9 San Dieguito River San Diego County 9 San Juan Creek Orange County 9 San Luis Rey River San Diego County 9 Santa Gertrudis Channel Riverside County 8 San Marcos Creek San Diego County 9 Santa Clara River watershed Ventura County 4 Santa Margarita River Riverside County 9 Santa Margarita R. tributaries Riverside County 9

Page 16 Sweetwater River San Diego County 9 Switzer Creek City of San Diego 9 Tecolote Creek City of San Diego 9 Temecula Creek Riverside County 9 Tijuana River San Diego County 9 Upper Newport Bay Newport Bay 8 Warm Springs Channel Riverside County 8 Wood Creek watershed Orange County 8

Page 17 Detailed Results Details of the summarized studies are presented in the tables included in the appendices, as described below. These appendix tables are based on spreadsheets in which information can be easily sorted and from which selected information can be extracted, and there are a number of clickable web links to studies.

The appendices to this memorandum include the following tables: Appendix A: The “Study Summaries by Author” table, organized alphabetically by abbreviated citation in (author, date) format. This table contains detailed information on the source documents, including web links where available (in some cases these links lead to just an abstract or perhaps ordering information). The "Citation – Abbrev." field can be used as a cross-reference for the various studies across the different tables. Appendix B: The “Results Summaries by Geography” table contains at-a-glance summaries of the methods and key results of the compiled studies. The Results Summaries entries are organized geographically (Northern/Central California vs. Southern California and then by local area, nominally ordered from north to south within each of those two regions). Appendix C: The “Chemistry Results Summary” table contains detailed results of water and sediment chemistry tests compiled where available from the more recent studies (generally those published 2005-2012) summarized in the preceding tables. The Chemistry Results Summary table summarizes results for more than 12,400 pesticide analyses (including pyrethroid pesticides plus fipronil and its degradates). Appendix D: The “Toxicity Results Summary” table contains detailed results of water and sediment toxicity tests compiled where available from the more recent studies (generally those published 2005-2012) summarized in the preceding tables.

Note that the Study Summaries by Author (Appendix A) and Results Summaries by Geography (Appendix B) tables contain all studies investigated and found to be pertinent, including the studies evaluated for the previous (2008) Pyrethroids Data Compilation. The Chemistry Results Summary (Appendix C) and Toxicity Results Summary (Appendix D) tables contain data only for more recent studies evaluated for the current report, generally those published since 2005.

Page 18 Recommendations

Improvements in Laboratory Analytical Methods Are Needed Some studies involving chemical analysis of pyrethroids in water and sediment are performed with analytical detection limits that are not sufficiently low to detect these pesticides at environmentally relevant concentrations. This has the effect of understating the extent of the problem, as some samples reported as “non-detect” may in fact contain pyrethroids at potentially harmful concentrations. Personnel responsible for pesticides analysis should ensure that the analytical work can be done so as to detect the target pesticides at environmentally relevant concentrations (i.e., near the “comparison values” shown in Tables 1 and 2). Some commercial laboratories are currently capable of providing appropriate analytical detection limits on a routine basis. However, a systematic means is called for by which analytical protocols are established at the federal level, with analytical detection limits sufficient to detect pesticides at environmentally-relevant concentrations in both waters and sediments.

Cumulative Impacts of Pesticide Mixtures Should Be Addressed A clear need exists for quantitative assessment of cumulative impacts of pesticide mixtures, as this appears to be a significant factor contributing to the observed toxicity in urban creeks.

Conclusions

Monitoring data compiled for this report indicate significant levels of pyrethroid pesticides found in water and sediment samples from surface waters in California’s urban areas. Average reported concentrations of several commonly-used pyrethroids in urban water samples are typically well above published comparison values, including UC Davis chronic toxicity criteria levels and USEPA Aquatic Life Benchmarks. Under average conditions in the sediments of urban waterways in California, pyrethroids also are typically present at levels known to be toxic to sensitive organisms. Bifenthrin, thought to be a principal cause of toxicity in urban waterways, is found in 64% of water samples and 67% of sediment samples in urban areas of California. Detections of pyrethroid pesticides in both water and sediment are widely distributed geographically throughout the state. In most samples, multiple pyrethroids are detected.

Fipronil, a common pyrethroid replacement pesticide, is also found in substantial numbers of water and sediment samples, along with its most common degradate compounds. Average fipronil concentrations in water samples are higher than the USEPA Aquatic Life Benchmark for fipronil, while average concentrations of the fipronil degradates are in the range of the associated USEPA benchmarks. The maximum reported concentrations for fipronil and its degradates in water samples are well above the USEPA benchmarks. Similarly, the maximum reported concentrations of fipronil and its degradates in sediment samples are well above published toxicity (LC50) values.

Toxicity in urban waterways throughout California is also well-documented in the compiled results, with many studies indicating pyrethroids as the likely cause of the observed toxicity. Because pyrethroid toxicity is generally considered to be additive, the level of toxicity estimated from chemistry results must account for the mixtures of pyrethroids and other pesticides found, including fipronil.

Page 19 References

Amweg, E. L., D. P. Weston, and N. Ureda (2005). “Use and Toxicity of Pyrethroid Pesticides in the Central Valley, California, USA.” Environ. Tox. Chem., 24 (4) 966-972; erratum: 24(5)

Amweg, E. L., D. P. Weston, J. You, M. J. Lydy. (2006). "Pyrethroid Insecticides and Sediment Toxicity in Urban Creeks from California and Tennessee." Environ. Sci. Technol. 40(5) 1700- 1706.

Anderson, B. S.; Phillips, B. M.; Hunt, J. W.; Connor, V.; Richard, N.; Tjeerdema, R. S. (2006). Identifying primary stressors impacting macroinvertebrates in the Salinas River (California, USA): Relative effects of pesticides and suspended particles. Environ. Pollut. 141, 402–408.

Anderson B., Hunt, J., Markiewicz, D., and Larsen, K. (2011). Toxicity in California Waters. Surface Water Ambient Monitoring Program. California State Water Resources Control Board. Sacramento, CA." Oct. 2011

Brander, S.M.; Fojut, T.L.; Palumbo, A.J. and Tjeerdema, R.S. (2010). “Water Quality Criteria Report for Bifenthrin.” Department of Environmental Toxicology, University of California, Davis, prepared for: California Environmental Protection Agency, Central Valley Regional Water Quality Control Board. March. Available at: http://www.swrcb.ca.gov/rwqcb5/water_issues/tmdl/central_valley_projects/central_valley_pesti cides/criteria_method/bifenthrin/final_bifenthrin_criteria_rpt.pdf

Central Valley RWQCB. (2006). Sacramento and San Joaquin River Watersheds Pesticide Basin Plan Amendment Fact Sheet. California Regional Water Quality Control Board, Central Valley Region. October. Available at: http://www.swrcb.ca.gov/rwqcb5/water_issues/tmdl/central_valley_projects/central_valley_pesti cides/att2_fact.pdf

Fojut, T.L.; Chang, S. and Tjeerdema, R.S. (2010). “Water Quality Criteria Report for Cyfluthrin.” Department of Environmental Toxicology, University of California, Davis, prepared for the California Environmental Protection Agency, Central Valley Regional Water Quality Control Board. March. Available at: http://www.swrcb.ca.gov/rwqcb5/water_issues/tmdl/central_valley_projects/central_valley_pesti cides/criteria_method/cyfluthrin/final_cyfluthrin_criteria_rpt.pdf

Fojut, T.L. and Tjeerdema, R.S. (2010). “Water Quality Criteria Report for Lambda- Cyhalothrin.” Department of Environmental Toxicology, University of California, Davis, prepared for: California Environmental Protection Agency, Central Valley Regional Water Quality Control Board. March. Available at: http://www.swrcb.ca.gov/rwqcb5/water_issues/tmdl/central_valley_projects/central_valley_pesti cides/criteria_method/lambda_cyhalothrin/final_lambda_cyhalothrin_criteria_rpt.pdf

Fojut, T.L.; Mulligan, R. and Tjeerdema, R.S. (2011a). “Water Quality Criteria Report for Cypermethrin.” Department of Environmental Toxicology, University of California, Davis, prepared for: California Environmental Protection Agency, Central Valley Regional Water Quality Control Board. September. Available at:

Page 20 http://www.swrcb.ca.gov/rwqcb5/water_issues/tmdl/central_valley_projects/central_valley_pesti cides/criteria_method/cypermethrin/cypermethrin_final_criteria.pdf

Fojut, T.L.; Rering, C. and Tjeerdema, R.S. (2011b). “Water Quality Criteria Report for Permethrin.” Department of Environmental Toxicology, University of California, Davis, prepared for: California Environmental Protection Agency, Central Valley Regional Water Quality Control Board. September. Available at: http://www.swrcb.ca.gov/rwqcb5/water_issues/tmdl/central_valley_projects/central_valley_pesti cides/criteria_method/permethrin/permethrin_final_criteria.pdf

Gerlach, R.W. (2012). Chiral Chemistry and Toxicity Assessments for Pyrethroid Pesticides, in Parameters for Pesticide QSAR and PBPK/PD Models for Human Risk Assessment, Chapter 2, pp 19–29, ACS Symposium Series, Vol. 1099

Gunasekara, A. S. and T. Troung (2007). “Environmental Fate of Fipronil.” Environmental Monitoring Branch, Department of Pesticide Regulation, California Environmental Protection Agency, Sacramento, CA. Revised March 5, 2007

Holmes, R. W., B. S. Anderson, et al. (2008). "Statewide investigation of the role of pyrethroid pesticides in sediment toxicity in California's urban waterways." Environmental Science and Technology 42(18): 7003-9.

Konwick, B.J., A.T. Fisk, et al. (2005). "Acute Enantioselective Toxicity of Fipronil and Its Desulfinyl Photoproduct to Ceriodaphnia Dubia." Environmental Toxicology and Chemistry 24(9): 2350-2355; supplemented by addendum with corrected citations for aquatic toxicity data Environ. Toxicol. Chem. 25(4): 1184.

Maul, J.D., A.A. Brennan, A.D. Harwood, and M.J. Lydy. (2008). Effect of sediment-associated pyrethroids, fipronil, and metabolites on Chironomus tentans growth rate, body mass, condition index, immobilization, and survival. Environ. Toxicol. Chem. 27 (12): 2582–2590.

Maund, S. J., Hamer, M. J., Warinton, J. S. and Kedwards, T. J. (1998). Aquatic ecotoxicology of the pyrethroid insecticide lambda-cyhalothrin: considerations for higher-tier aquatic risk assessment. Pestic. Sci., 54: 408–417. doi: 10.1002/(SICI)1096-9063(199812)54:4<408::AID- PS843>3.0.CO;2-T

Maund, S. J.; Hamer, M. J.; Lane, M. C. G.; Farrelly, E.; Rapley, J. H.; Goggin, U. M.; Gentle, W. E. (2002). Partitioning, bioavailability, and toxicity of the pyrethroid insecticide cypermethrin in sediments. Environ. Toxicol. Chem. 21: 9-15.

Mize, S.V.; S.D. Porter, and D.K. Demcheck (2008). "Influence of fipronil compounds and rice- cultivation land-use intensity on macroinvertebrate communities in streams of southwestern Louisiana, USA". USGS Staff -- Published Research. Paper 435.

Mokry, L. E. and Hoagland, K. D. (1990). Acute toxicities of five synthetic pyrethroid insecticides to Daphnia magna and Ceriodaphnia dubia. Environmental Toxicology and Chemistry, 9: 1045–1051. doi: 10.1002/etc.5620090811

Moran, K.D., and P.L. TenBrook (2011). “Sources of Pyrethroid Insecticides in California’s Urban Watersheds: A Conceptual Model.” In Pesticide Mitigation Strategies for Surface Water

Page 21 Quality; Goh, K.S., J. Gan, and B. Bret, Eds. ACS Symposium Series; American Chemical Society: Washington, DC.

Ruby, A. (2008). “Pyrethroids Monitoring Data Compilation”. Memorandum prepared for the California Stormwater Quality Association (CASQA) by Armand Ruby Consulting. July 8.

San Francisco Bay Regional Quality Control Board (2005). Diazinon and Pesticide-Related Toxicity in Bay Area Urban Creeks Water Quality Attainment Strategy and Total Maximum Daily Load (TMDL), Proposed Basin Plan Amendment and Staff Report. California Regional Water Quality Control Board, San Francisco Bay Region. November 9, 2005. Available at: http://www.waterboards.ca.gov/sanfranciscobay/water_issues/programs/TMDLs/urbancrksdiazinon/b_final_staff_report.pdf

State Water Resources Control Board (2011). Impaired Water Bodies web site; see: http://www.swrcb.ca.gov/water_issues/programs/tmdl/integrated2010.shtml

TDC Environmental (2006). Pesticides in Urban Surface Water: Annual Research and Monitoring Update 2006. Prepared for the San Francisco Estuary Project. April.

TDC Environmental (2007). Urban Use of the Insecticide Fipronil--Water Quality Implications, Memorandum to the Urban Pesticide Committee from Kelly D. Moran, June 18, 2007.

TDC Environmental (2010a). Pesticides in Urban Runoff, Wastewater, and Surface Water: Annual Review of New Scientific Findings 2010. Prepared for the San Francisco Estuary Partnership. March.

TDC Environmental (2010b). Pesticides in Urban Runoff, Wastewater, and Surface Water: Annual Urban Pesticide Use Data Report 2010. Prepared for the San Francisco Estuary Partnership. June.

Trimble, A. J., D. P. Weston, J. B. Belden, M. J. Lydy. (2009). "Identification and Evaluation of Pyrethroid Insecticide Mixtures in Urban Sediments." Environmental Toxicology and Chemistry 28(8): 1687-1695.

UC Davis criteria development reports (Brander et al., 2010; Fojut et al., 2010; Fojut and Tjeerdema, 2010; Fojut et al., 2011a; Fojut et al., 2011b) are available on the Central Valley Regional Water Quality Control Board website: http://tinyurl.com/2etvvg3

U.S. EPA Aquatic Life Benchmarks website: http://www.epa.gov/oppefed1/ecorisk_ders/aquatic_life_benchmark.htm

Werner, I. and K. Moran. (2008). Effects of Pyrethroid Insecticides on Aquatic Organisms. In Synthetic Pyrethroids, Am. Chem. Soc.: Washington, DC, 2008; pp 310-334.

Weston, D. P., R. W. Holmes, J. You, M. J. Lydy. (2005). “Aquatic Toxicity Due to Residential Use of Pyrethroid Insecticides,” Environ. Sci. Technol. 39(24): 9778-9784.

Weston, D.P. and C.J. Jackson. (2009). Use of Engineered Enzymes to Identify Organophosphate and Pyrethroid-Related Toxicity in Toxicity Identification Evaluations Environ. Sci. Technol. 2009, 43, 5514–5520

Page 22

Appendix A:“Study Summaries by Author” Table

Citation - Abbrev. Author(s)/Date Agency Report/Study Title Journal/Publication Reference Web Link Water/ Sediment Chemical Constituents

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Appendix B: “Results Summaries by Geography” Table

Geographic Area Monitoring Location(s) Water Citation - Abbrev. Study Date(s) Principal Testing Approach Test Results Summary Board Region

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Appendix C: “Chemistry Results Summary” Table

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Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 0DUWLQ.RRSPDQ&DQ\RQ (QVPLQJHUDQG.HOOH\D  6)% &UHHN0&&  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 0DUWLQ.RRSPDQ&DQ\RQ (QVPLQJHUDQG.HOOH\D  6)% &UHHN0&&  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 3OHDVDQW*URYH&UHHN (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR 3*&  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     3OHDVDQW*URYH&UHHN 3*&  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 3OHDVDQW*URYH&UHHN 3*&  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     3OHDVDQW*URYH&UHHN 3*&  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 3OHDVDQW*URYH&UHHN 3*&  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 3OHDVDQW*URYH&UHHN 3*&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 3OHDVDQW*URYH&UHHN 3*&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 3OHDVDQW*URYH&UHHN (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR 3*&  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     3OHDVDQW*URYH&UHHN 3*&  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 3OHDVDQW*URYH&UHHN 3*&  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 3OHDVDQW*URYH&UHHN 3*&  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 3OHDVDQW*URYH&UHHN 3*&  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     3OHDVDQW*URYH&UHHN 3*&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 3OHDVDQW*URYH&UHHN 3*&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 3OHDVDQW*URYH&UHHN (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR 3*&  %LIHQWKULQ 'U\ 6HGLPHQW 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3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     6DOW&UHHN6&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     6DOW&UHHN6&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 6DOW&UHHN6&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  6DQ'LHJR 6DQ'LHJR5LYHU6'5  %LIHQWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\     $OWKRXJKWKHORZHVWGHWHFWLRQYDOXHLVORZHUWKDQKDOIWKH5/ LWZDVQRWODEHOHGDVDQ     6DQ'LHJR5LYHU6'5  &\IOXWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  &\SHUPHWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  'HOWDPHWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  3HUPHWKULQFLV 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  5HVPHWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 6DQ'LHJR5LYHU6'5  )HQSURSDWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  6DQ'LHJR 6DQ'LHJR5LYHU6'5  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     $OWKRXJKWKHORZHVWGHWHFWLRQYDOXHLVORZHUWKDQKDOIWKH5/ LWZDVQRWODEHOHGDVDQ     6DQ'LHJR5LYHU6'5  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     6DQ'LHJR5LYHU6'5  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     6DQ'LHJR5LYHU6'5  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     6DQ'LHJR5LYHU6'5  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 6DQ'LHJR5LYHU6'5  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  6DQ'LHJR 6DQ'LHJR5LYHU6'5  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DQ'LHJR5LYHU6'5  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DQ'LHJR5LYHU6'5  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  6DQ'LHJR 6DQ'LHJR5LYHU6'5  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DQ'LHJR5LYHU6'5  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DQ'LHJR5LYHU6'5  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DQ'LHJR5LYHU6'5  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DQ'LHJR5LYHU6'5  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DQ'LHJR5LYHU6'5  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  6DQ'LHJR 6DQ'LHJR5LYHU6'5  %LIHQWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\     6DQ'LHJR5LYHU6'5  &\IOXWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 6DQ'LHJR5LYHU6'5  &\SHUPHWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 6DQ'LHJR5LYHU6'5  'HOWDPHWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 6DQ'LHJR5LYHU6'5  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  3HUPHWKULQFLV 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —JNJ 6DQ'LHJR5LYHU6'5  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  5HVPHWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 6DQ'LHJR5LYHU6'5  )HQSURSDWKULQ 'U\ 6HGLPHQW 5HFHLYLQJ     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  2UDQJH&RXQW\ :RRG&DQ\RQ:&  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ :RRG&DQ\RQ:&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  2UDQJH&RXQW\ :RRG&DQ\RQ:&  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ :RRG&DQ\RQ:&  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ :RRG&DQ\RQ:&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  2UDQJH&RXQW\ :RRG&DQ\RQ:&  %LIHQWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  &\IOXWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  &\SHUPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  'HOWDPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes :RRG&DQ\RQ:&  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  /DPEGDF\KDORWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  3HUPHWKULQFLV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  3HUPHWKULQWUDQV 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  5HVPHWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ :RRG&DQ\RQ:&  )HQSURSDWKULQ 'U\ 6HGLPHQW 'LVFKDUJH     —JNJ 'U\ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 3OHDVDQW*URYH&UHHN (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR 3*&  'HVXOILQ\OILSURQLO 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLODPLGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOILGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —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—J/ 3OHDVDQW*URYH&UHHN 3*&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  %LIHQWKULQ :HW :DWHU 'LVFKDUJH     QJ/     3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ :HW :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\SHUPHWKULQ :HW :DWHU 'LVFKDUJH     QJ/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV :HW :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV :HW :DWHU 'LVFKDUJH     QJ/ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 3OHDVDQW*URYH&UHHN (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR 3*&  'HVXOILQ\OILSURQLO 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLODPLGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOILGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —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—J/ 3OHDVDQW*URYH&UHHN 3*&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  %LIHQWKULQ :HW :DWHU 'LVFKDUJH     QJ/     2QHVDPSOHYDOXHPLVVLQJ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ :HW :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\SHUPHWKULQ :HW :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV :HW :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV :HW :DWHU 'LVFKDUJH     QJ/ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 3OHDVDQW*URYH&UHHN (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR 3*&  'HVXOILQ\OILSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLODPLGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOILGH 'U\ :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —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—J/ 3OHDVDQW*URYH&UHHN 3*&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —J/ 3OHDVDQW*URYH&UHHN 3*&  %LIHQWKULQ :HW :DWHU 'LVFKDUJH     QJ/     2QHVDPSOHYDOXHPLVVLQJ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ :HW :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\SHUPHWKULQ :HW :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV :HW :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV :HW :DWHU 'LVFKDUJH     QJ/ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 3OHDVDQW*URYH&UHHN (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR 3*&  'HVXOILQ\OILSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     2QHVDPSOHYDOXHPLVVLQJDQG1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLODPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOILGH 'U\ :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     2QHVDPSOHYDOXHPLVVLQJDQG1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 3OHDVDQW*URYH&UHHN 3*&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\SHUPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 3OHDVDQW*URYH&UHHN (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR 3*&  'HVXOILQ\OILSURQLO :HW :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  'HVXOILQ\O)3DPLGH :HW :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO :HW :DWHU 5HFHLYLQJ     —J/ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 3OHDVDQW*URYH&UHHN 3*&  )LSURQLODPLGH :HW :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOILGH :HW :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH :HW :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  %LIHQWKULQ :HW :DWHU 5HFHLYLQJ     QJ/     2QHVDPSOHYDOXHPLVVLQJ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ :HW :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\SHUPHWKULQ :HW :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV :HW :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV :HW :DWHU 5HFHLYLQJ     QJ/ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR *UD\VRQ&UHHN*5<  'HVXOILQ\OILSURQLO :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ *UD\VRQ&UHHN*5<  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —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—J/ *UD\VRQ&UHHN*5<  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ *UD\VRQ&UHHN*5<  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —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—J/ *UD\VRQ&UHHN*5<  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  %LIHQWKULQ :HW :DWHU 'LVFKDUJH     QJ/     1'VXEVWLWXWHGDVWKH5/ QJ/ *UD\VRQ&UHHN*5<  &\IOXWKULQ :HW :DWHU 'LVFKDUJH     QJ/     2QHVDPSOHYDOXHPLVVLQJ *UD\VRQ&UHHN*5<  &\SHUPHWKULQ :HW :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  3HUPHWKULQFLV :HW :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  3HUPHWKULQWUDQV :HW :DWHU 'LVFKDUJH     QJ/ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD 0DUWLQ.RRSPDQ&DQ\RQ (QVPLQJHUDQG.HOOH\D  6DFUDPHQWR &UHHN0&&  'HVXOILQ\OILSURQLO :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —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—J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —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—J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —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—J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  'HVXOILQ\O)3DPLGH :HW :DWHU 5HFHLYLQJ     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLO :HW :DWHU 5HFHLYLQJ     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLODPLGH :HW :DWHU 5HFHLYLQJ     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLOVXOILGH :HW :DWHU 5HFHLYLQJ     —J/ 0DUWLQ.RRSPDQ&DQ\RQ &UHHN0&&  )LSURQLOVXOIRQH :HW :DWHU 5HFHLYLQJ     —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—J/     :RRG&DQ\RQ$9  'HVXOILQ\O)3DPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ$9  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     :RRG&DQ\RQ$9  )LSURQLODPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ$9  )LSURQLOVXOILGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ$9  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ :RRG&DQ\RQ$9  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&DQ\RQ$9  )HQYDOHUDWHHVIHQYDOHUDWH 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&DQ\RQ$9  /DPEGDF\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&DQ\RQ$9  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&DQ\RQ$9  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  2UDQJH&RXQW\ :RRG&DQ\RQ$9  'HVXOILQ\OILSURQLO :HW :DWHU 5HFHLYLQJ     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ$9  'HVXOILQ\O)3DPLGH :HW :DWHU 5HFHLYLQJ     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ$9  )LSURQLO :HW :DWHU 5HFHLYLQJ     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ$9  )LSURQLODPLGH :HW :DWHU 5HFHLYLQJ     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ$9  )LSURQLOVXOILGH :HW :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ$9  )LSURQLOVXOIRQH :HW :DWHU 5HFHLYLQJ     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes :RRG&DQ\RQ$9  %LIHQWKULQ :HW :DWHU 5HFHLYLQJ     QJ/ 6DPSOHYDOXHPLVVLQJ :RRG&DQ\RQ$9  )HQYDOHUDWHHVIHQYDOHUDWH :HW :DWHU 5HFHLYLQJ     QJ/ 6DPSOHYDOXHPLVVLQJ :RRG&DQ\RQ$9  /DPEGDF\KDORWKULQ :HW :DWHU 5HFHLYLQJ     QJ/ 6DPSOHYDOXHPLVVLQJ :RRG&DQ\RQ$9  3HUPHWKULQFLV :HW :DWHU 5HFHLYLQJ     QJ/ 6DPSOHYDOXHPLVVLQJ :RRG&DQ\RQ$9  3HUPHWKULQWUDQV :HW :DWHU 5HFHLYLQJ     QJ/ 6DPSOHYDOXHPLVVLQJ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  2UDQJH&RXQW\ 6DOW&UHHN6&  'HVXOILQ\OILSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 6DOW&UHHN6&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 6DOW&UHHN6&  )LSURQLODPLGH 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 6DOW&UHHN6&  )LSURQLOVXOILGH 'U\ :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —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—J/ 6DOW&UHHN6&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DOW&UHHN6&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DOW&UHHN6&  %LIHQWKULQ :HW :DWHU 'LVFKDUJH     QJ/ 6DPSOHYDOXHPLVVLQJ 6DOW&UHHN6&  )HQYDOHUDWHHVIHQYDOHUDWH :HW :DWHU 'LVFKDUJH     QJ/ 6DPSOHYDOXHPLVVLQJ 6DOW&UHHN6&  /DPEGDF\KDORWKULQ :HW :DWHU 'LVFKDUJH     QJ/ 6DPSOHYDOXHPLVVLQJ 6DOW&UHHN6&  3HUPHWKULQFLV :HW :DWHU 'LVFKDUJH     QJ/ 6DPSOHYDOXHPLVVLQJ 6DOW&UHHN6&  3HUPHWKULQWUDQV :HW :DWHU 'LVFKDUJH     QJ/ 6DPSOHYDOXHPLVVLQJ 0RQLWRULQJ8UEDQ3HVWLFLGH5XQRIILQ&DOLIRUQLD (QVPLQJHUDQG.HOOH\D  2UDQJH&RXQW\ 6DOW&UHHN6&  'HVXOILQ\OILSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 6DOW&UHHN6&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 6DOW&UHHN6&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 6DOW&UHHN6&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —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—J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DOW&UHHN6&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DOW&UHHN6&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 6DOW&UHHN6&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —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—J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 6DOW&UHHN6&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ 6DOW&UHHN6&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ 6DOW&UHHN6&  )LSURQLODPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ 6DOW&UHHN6&  )LSURQLOVXOILGH 'U\ :DWHU 5HFHLYLQJ     —J/ 6DOW&UHHN6&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —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—J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DOW&UHHN6&  'HVXOILQ\O)3DPLGH :HW :DWHU 5HFHLYLQJ     —J/ 6DOW&UHHN6&  )LSURQLO :HW :DWHU 5HFHLYLQJ     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DOW&UHHN6&  )LSURQLODPLGH :HW :DWHU 5HFHLYLQJ     —J/ 6DOW&UHHN6&  )LSURQLOVXOILGH :HW :DWHU 5HFHLYLQJ     —J/ 6DOW&UHHN6&  )LSURQLOVXOIRQH :HW :DWHU 5HFHLYLQJ     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes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—J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ :RRG&DQ\RQ:&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ :RRG&DQ\RQ:&  )LSURQLODPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLOVXOILGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —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—J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ :RRG&DQ\RQ:&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ :RRG&DQ\RQ:&  )LSURQLODPLGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLOVXOILGH 'U\ :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —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—J/ :RRG&DQ\RQ:&  'HVXOILQ\O)3DPLGH :HW :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLO :HW :DWHU 5HFHLYLQJ     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  )LSURQLODPLGH :HW :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLOVXOILGH :HW :DWHU 5HFHLYLQJ     —J/ :RRG&DQ\RQ:&  )LSURQLOVXOIRQH :HW :DWHU 5HFHLYLQJ     —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—J/     :RRG&DQ\RQ:&  'HVXOILQ\O)3DPLGH 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ :RRG&DQ\RQ:&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     :RRG&DQ\RQ:&  )LSURQLODPLGH 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ :RRG&DQ\RQ:&  )LSURQLOVXOILGH 'U\ :DWHU 'LVFKDUJH     —J/     1'VXEVWLWXWHGDVWKHUHSRUWLQJOLPLW —J/ :RRG&DQ\RQ:&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —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—J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ :RRG&DQ\RQ:&  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG :RRG&DQ\RQ:&  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ :RRG&DQ\RQ:&  )LSURQLOVXOIRQH :HW :DWHU 'LVFKDUJH     —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—J/ 6DQ'LHJR5LYHU6'5  'HVXOILQ\O)3DPLGH :HW :DWHU 'LVFKDUJH     —J/ 6DQ'LHJR5LYHU6'5  )LSURQLO :HW :DWHU 'LVFKDUJH     —J/    2QO\RQHVDPSOHQRPHGLDQFDOFXODWHG 6DQ'LHJR5LYHU6'5  )LSURQLODPLGH :HW :DWHU 'LVFKDUJH     —J/ 6DQ'LHJR5LYHU6'5  )LSURQLOVXOILGH :HW :DWHU 'LVFKDUJH     —J/ 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Unit Citation - Abbrev. 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 QJ/ 6DOW&UHHN6&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 2UDQJH&RXQW\/DJXQD1LJXHO 6DOW&UHHN6&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 6DOW&UHHN6&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 6DOW&UHHN6&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 6DOW&UHHN6&  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 6DOW&UHHN6&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 6DOW&UHHN6&  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 6DOW&UHHN6&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 6DOW&UHHN6&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 2UDQJH&RXQW\$OLVR9LHMR :RRG&UHHN:&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ :RRG&UHHN:&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ :RRG&UHHN:&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ :RRG&UHHN:&  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ :RRG&UHHN:&  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ :RRG&UHHN:&  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ :RRG&UHHN:&  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ :RRG&UHHN:&  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 2UDQJH&RXQW\$OLVR9LHMR :RRG&UHHN:&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ :RRG&UHHN:&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ :RRG&UHHN:&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ :RRG&UHHN:&  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 2UDQJH&RXQW\$OLVR9LHMR :RRG&UHHN:&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ :RRG&UHHN:&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ :RRG&UHHN:&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —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± (QVPLQJHUHWDO 2UDQJH&RXQW\$OLVR9LHMR :RRG&UHHN:&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     :RRG&UHHN:&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ :RRG&UHHN:&  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ :RRG&UHHN:&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DFUDPHQWR 6$& $OGHU&UHHN)2/  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ $OGHU&UHHN)2/  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ $OGHU&UHHN)2/  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ $OGHU&UHHN)2/  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $OGHU&UHHN)2/  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $OGHU&UHHN)2/  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $OGHU&UHHN)2/  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ $OGHU&UHHN)2/  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DFUDPHQWR 6$& )ROVRP $OGHU&UHHN)2/  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ $OGHU&UHHN)2/  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/ $OGHU&UHHN)2/  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/ $OGHU&UHHN)2/  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $OGHU&UHHN)2/  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $OGHU&UHHN)2/  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $OGHU&UHHN)2/  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ $OGHU&UHHN)2/  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DFUDPHQWR 6$& )ROVRP $OGHU&UHHN)2/  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ $OGHU&UHHN)2/  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/ $OGHU&UHHN)2/  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/ $OGHU&UHHN)2/  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ $OGHU&UHHN)2/  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ $OGHU&UHHN)2/  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ $OGHU&UHHN)2/  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ $OGHU&UHHN)2/  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH .%&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     3OHDVDQW*URYH&UHHN .%&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN .%&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN .%&  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN .%&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 3OHDVDQW*URYH&UHHN .%&  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN .%&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN .%&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH 3*&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —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± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH 3*&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 3OHDVDQW*URYH&UHHN 3*&  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH 3*&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 3OHDVDQW*URYH&UHHN 3*&  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH 3*&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH 3*&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 3OHDVDQW*URYH&UHHN 3*&  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH 3*&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —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± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH 3*&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ 3OHDVDQW*URYH&UHHN 3*&  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± 3OHDVDQW*URYH&UHHN (QVPLQJHUHWDO 6DFUDPHQWR 6$& 5RVHYLOOH 3*&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     3OHDVDQW*URYH&UHHN 3*&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/ 3OHDVDQW*URYH&UHHN 3*&  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ Wet/Dry Water/ Discharge/ # # % Sed. Unit Citation - Abbrev. Report/study Title Region Site(s) Timeframe Pesticide (Analyte) Weather Sediment Receiving Water # Sites Samples Detected Detected Units Weight Mean Median Min Max Notes 3OHDVDQW*URYH&UHHN 3*&  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3OHDVDQW*URYH&UHHN 3*&  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DQ)UDQFLVFR%D\ 6)% *UD\VRQ&UHHN*5<  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ *UD\VRQ&UHHN*5<  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/ *UD\VRQ&UHHN*5<  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DQ)UDQFLVFR%D\ 6)% *UD\VRQ&UHHN*5<  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ *UD\VRQ&UHHN*5<  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ *UD\VRQ&UHHN*5<  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ *UD\VRQ&UHHN*5<  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DQ)UDQFLVFR%D\ 6)% *UD\VRQ&UHHN*5<  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ *UD\VRQ&UHHN*5<  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/ *UD\VRQ&UHHN*5<  )LSURQLOVXOIRQH 'U\ :DWHU 5HFHLYLQJ     —J/ *UD\VRQ&UHHN*5<  'HOWDPHWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ *UD\VRQ&UHHN*5<  &\IOXWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ *UD\VRQ&UHHN*5<  /&\KDORWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/ *UD\VRQ&UHHN*5<  3HUPHWKULQFLV 'U\ :DWHU 5HFHLYLQJ     QJ/ *UD\VRQ&UHHN*5<  3HUPHWKULQWUDQV 'U\ :DWHU 5HFHLYLQJ     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DQ)UDQFLVFR%D\ 6)% $ODPR&UHHN0&&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ $ODPR&UHHN0&&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ $ODPR&UHHN0&&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/ $ODPR&UHHN0&&  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DQ)UDQFLVFR%D\ 6)% $ODPR&UHHN0&&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ $ODPR&UHHN0&&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/ $ODPR&UHHN0&&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/ $ODPR&UHHN0&&  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DQ)UDQFLVFR%D\ 6)% $ODPR&UHHN0&&  %LIHQWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ $ODPR&UHHN0&&  )LSURQLO 'U\ :DWHU 'LVFKDUJH     —J/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ —J/ $ODPR&UHHN0&&  )LSURQLOVXOIRQH 'U\ :DWHU 'LVFKDUJH     —J/ $ODPR&UHHN0&&  'HOWDPHWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  &\IOXWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  /&\KDORWKULQ 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  3HUPHWKULQFLV 'U\ :DWHU 'LVFKDUJH     QJ/ $ODPR&UHHN0&&  3HUPHWKULQWUDQV 'U\ :DWHU 'LVFKDUJH     QJ/ 3HVWLFLGHRFFXUUHQFHDQGDTXDWLFEHQFKPDUN H[FHHGDQFHVLQXUEDQVXUIDFHZDWHUVDQGVHGLPHQWVLQ WKUHHXUEDQDUHDVRI&DOLIRUQLD86$± (QVPLQJHUHWDO 6DQ)UDQFLVFR%D\ 6)% $ODPR&UHHN0&&  %LIHQWKULQ 'U\ :DWHU 5HFHLYLQJ     QJ/     1RQGHWHFWVVXEVWLWXWHGDVWKHUHSRUWLQJOLPLW 5/ QJ/ $ODPR&UHHN0&&  )LSURQLO 'U\ :DWHU 5HFHLYLQJ     —J/     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Unit Citation - Abbrev. 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Appendix D: “Toxicity Results Summary” Table

Number of % Non- Average Study Wet/Dry Discharge/Receiving Number Number of Number of Non-toxic % Toxic toxic % Acute or Citation - Abbrev. Report/study Title Region Site(s) Timeframe Weather Water/Sediment Water Organism tested of Sites Samples Tested Toxic Samples Samples Samples Samples Survival Chronic test Notes

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