Michigan Register Issue No. 22 – 2017 (Published December 15, 2017) GRAPHIC IMAGES IN THE

MICHIGAN REGISTER

COVER DRAWING

Michigan State Capitol:

This image, with flags flying to indicate that both chambers of the legislature are in session, may have originated as an etching based on a drawing or a photograph. The artist is unknown. The drawing predates the placement of the statue of Austin T. Blair on the capitol grounds in 1898.

(Michigan State Archives)

PAGE GRAPHICS

Capitol Dome:

The architectural rendering of the Michigan State Capitol’s dome is the work of Elijah E. Myers, the building’s renowned architect. Myers inked the rendering on linen in late 1871 or early 1872. Myers’ fine draftsmanship, the hallmark of his work, is clearly evident.

Because of their size, few architectural renderings of the 19th century have survived. Michigan is fortunate that many of Myers’ designs for the Capitol were found in the building’s attic in the 1950’s. As part of the state’s 1987 sesquicentennial celebration, they were conserved and deposited in the Michigan State Archives.

(Michigan State Archives)

East Elevation of the Michigan State Capitol:

When Myers’ drawings were discovered in the 1950’s, this view of the Capitol – the one most familiar to Michigan citizens – was missing. During the building’s recent restoration (1989-1992), this drawing was commissioned to recreate the architect’s original rendering of the east (front) elevation.

(Michigan Capitol Committee)

Michigan Register

Published pursuant to § 24.208 of The Michigan Compiled Laws

Issue No. 22— 2017 (This issue, published December 15, 2017, contains documents filed from November 15, 2017 to December 1, 2017)

Compiled and Published by the Office of Regulatory Reinvention

© 2017 by Office of Regulatory Reinvention, State of Michigan All rights reserved. Printed in the of America

Michigan Register (ISSN 0892-3124). Published twice per month, with a cumulative index, by the Office of Regulatory Reinvention, pursuant to §24.208 of the Michigan Compiled Laws. Subscription $400.00 per year, postpaid to points in the U.S. First class postage paid at Lansing, Michigan. Direct all mail concerning subscriptions to Office of Regulatory Reinvention, Romney Building – Eight Floor, 111 S. Capitol, Lansing, MI 48909

Jeff Bankowski, Executive Director, Office of Performance and Transformation; Deidre O’Berry, Administrative Rules Specialist for Operations and Publications.

Rick Snyder, Governor

Brian Calley, Lieutenant Governor

PREFACE

PUBLICATION AND CONTENTS OF THE MICHIGAN REGISTER

The Office of Regulatory Reform publishes the Michigan Register.

While several statutory provisions address the publication and contents of the Michigan Register, two are of particular importance.

24.208 Michigan register; publication; cumulative index; contents; public subscription; fee; synopsis of proposed rule or guideline; transmitting copies to office of regulatory reform. Sec. 8.

(1) The office of regulatory reform shall publish the Michigan register at least once each month. The Michigan register shall contain all of the following:

(a) Executive orders and executive reorganization orders.

(b) On a cumulative basis, the numbers and subject matter of the enrolled senate and house bills signed into law by the governor during the calendar year and the corresponding public act numbers.

(c) On a cumulative basis, the numbers and subject matter of the enrolled senate and house bills vetoed by the governor during the calendar year.

(d) Proposed administrative rules.

(e) Notices of public hearings on proposed administrative rules.

(f) Administrative rules filed with the secretary of state.

(g) Emergency rules filed with the secretary of state.

(h) Notice of proposed and adopted agency guidelines.

(i) Other official information considered necessary or appropriate by the office of regulatory reform.

(j) Attorney general opinions.

(k) All of the items listed in section 7(m) after final approval by the certificate of need commission under section 22215 of the public health code, 1978 PA 368, MCL 333.22215.

(2) The office of regulatory reform shall publish a cumulative index for the Michigan register.

(3) The Michigan register shall be available for public subscription at a fee reasonably calculated to cover publication and distribution costs.

(4) If publication of an agency's proposed rule or guideline or an item described in subsection (1)(k) would be unreasonably expensive or lengthy, the office of regulatory reform may publish a brief synopsis of the proposed rule or guideline or item described in subsection (1)(k), including information on how to obtain a complete copy of the proposed rule or guideline or item described in subsection (1)(k) from the agency at no cost.

(5) An agency shall electronically transmit a copy of the proposed rules and notice of public hearing to the office of regulatory reform for publication in the Michigan register. 4.1203 Michigan register fund; creation; administration; expenditures; disposition of money received from sale of Michigan register and amounts paid by state agencies; use of fund; price of Michigan register; availability of text on internet; copyright or other proprietary interest; fee prohibited; definition. Sec. 203.

(1) The Michigan register fund is created in the state treasury and shall be administered by the office of regulatory reform. The fund shall be expended only as provided in this section.

(2) The money received from the sale of the Michigan register, along with those amounts paid by state agencies pursuant to section 57 of the administrative procedures act of 1969, 1969 PA 306, MCL 24.257, shall be deposited with the state treasurer and credited to the Michigan register fund.

(3) The Michigan register fund shall be used to pay the costs of preparing, printing, and distributing the Michigan register.

(4) The department of management and budget shall sell copies of the Michigan register at a price determined by the office of regulatory reform not to exceed the cost of preparation, printing, and distribution.

(5) Notwithstanding section 204, beginning January 1, 2001, the office of regulatory reform shall make the text of the Michigan register available to the public on the internet.

(6) The information described in subsection (5) that is maintained by the office of regulatory reform shall be made available in the shortest feasible time after the information is available. The information described in subsection (5) that is not maintained by the office of regulatory reform shall be made available in the shortest feasible time after it is made available to the office of regulatory reform.

(7) Subsection (5) does not alter or relinquish any copyright or other proprietary interest or entitlement of this state relating to any of the information made available under subsection (5).

(8) The office of regulatory reform shall not charge a fee for providing the Michigan register on the internet as provided in subsection (5).

(9) As used in this section, “Michigan register” means that term as defined in section 5 of the administrative procedures act of 1969, 1969 PA 306, MCL 24.205.

CITATION TO THE MICHIGAN REGISTER The Michigan Register is cited by year and issue number. For example, 2001 MR 1 refers to the year of issue (2001) and the issue number (1).

CLOSING DATES AND PUBLICATION SCHEDULE The deadlines for submitting documents to the Office of Regulatory Reinvention for publication in the Michigan Register are the first and fifteenth days of each calendar month, unless the submission day falls on a Saturday, Sunday, or legal holiday, in which event the deadline is extended to include the next day which is not a Saturday, Sunday, or legal holiday. Documents filed or received after 5:00 p.m. on the closing date of a filing period will appear in the succeeding issue of the Michigan Register.

The Office of Regulatory Reinvention is not responsible for the editing and proofreading of documents submitted for publication.

Documents submitted for publication should be delivered or mailed in an electronic format to the following address: MICHIGAN REGISTER, Office of Regulatory Reinvention, Ottawa Building – Second Floor, 611 W. Ottawa Street, Lansing, MI 48909.

RELATIONSHIP TO THE MICHIGAN ADMINISTRATIVE CODE The Michigan Administrative Code (1979 edition), which contains all permanent administrative rules in effect as of December 1979, was, during the period 1980-83, updated each calendar quarter with the publication of a paperback supplement. An annual supplement contained those permanent rules, which had appeared in the 4 quarterly supplements covering that year.

Quarterly supplements to the Code were discontinued in January 1984, and replaced by the monthly publication of permanent rules and emergency rules in the Michigan Register. Annual supplements have included the full text of those permanent rules that appear in the twelve monthly issues of the Register during a given calendar year. Emergency rules published in an issue of the Register are noted in the annual supplement to the Code.

SUBSCRIPTIONS AND DISTRIBUTION The Michigan Register, a publication of the State of Michigan, is available for public subscription at a cost of $400.00 per year. Submit subscription requests to: Office of Regulatory Reinvention, Romney Building –Eight Floor, 111 S. Capitol Avenue, Lansing, MI 48909. Checks Payable: State of Michigan. Any questions should be directed to the Office of Regulatory Reinvention (517) 335-8658.

INTERNET ACCESS The Michigan Register can be viewed free of charge on the Internet web site of the Office of Regulatory Reinvention: www.michigan.gov/orr.

Issue 2000-3 and all subsequent editions of the Michigan Register can be viewed on the Office of Regulatory Reinvention Internet web site. The electronic version of the Register can be navigated using the blue highlighted links found in the Contents section. Clicking on a highlighted title will take the reader to related text, clicking on a highlighted header above the text will return the reader to the Contents section.

Jeff Bankowski, Executive Director, Office of Performance and Transformation 2017 PUBLICATION SCHEDULE

Closing Date for Issue Filing or Submission Publication No. Of Documents (5 p.m.) Date

1 January 15, 2017 February 1, 2017 2 February 1, 2017 February 15, 2017 3 February 15, 2017 March 1, 2017 4 March 1, 2017 March 15, 2017 5 March 15, 2017 April 1, 2017 6 April 1, 2017 April 15, 2017 7 April 15, 2017 May 1, 2017 8 May 1, 2017 May 15, 2017 9 May 15, 2017 June 1, 2017 10 June 1, 2017 June 15, 2017 11 June 15, 2017 July 1, 2017 12 July 1, 2017 July 15, 2017 13 July 15, 2017 August 1, 2017 14 August 1, 2017 August 15, 2017 15 August 15, 2017 September 1, 2017 16 September 1, 2017 September 15, 2017 17 September 15, 2017 October 1, 2017 18 October 1, 2017 October 15, 2017 19 October 15, 2017 November 1, 2017 20 November 1, 2017 November 15, 2017 21 November 15, 2017 December 1, 2017 22 December 1, 2017 December 15, 2017 23 December 15, 2017 January 1, 2018 24 January 1, 2018 January 15, 2018

CONTENTS

ADMINISTRATIVE RULES FILED WITH SECRETARY OF STATE

Department of Licensing and Regulatory Affairs Director’s Office (2014-037) Billing Practices Applicable to Non-Residential Electric and Gas Customers ...... 2-4

Department of Licensing and Regulatory Affairs Director’s Office (2014-038) Consumer Standards and Billing Practices for Electric And Gas Residential Service ..... 5-40

Department of Licensing and Regulatory Affairs Director’s Office (2017-007) Electrical Supply and Communication Lines and Associated Equipment ...... 41-41

PROPOSED ADMINISTRATIVE RULES, NOTICES OF PUBLIC HEARINGS

Department of Natural Resources Parks and Recreation Division (2014-155) Pure Michigan Trail, Water Trail, and Trail Town Designation ...... 43-46 Public Hearing Notice ...... 47-47

Department of Environmental Quality Director’s Office (2015-094) Environmental Contamination Response Activity ...... 48-386 Public Hearing Notice ...... 387-387

Department of Licensing and Regulatory Affairs Director’s Office (2017-059) Part 63. Pulp, Paper, and Paperboard Mills ...... 388-401

Department of Licensing and Regulatory Affairs Director’s Office (2017-061) Part 94 Textiles ...... 402-403

CERTIFICATION OF NEED REVIEW STANDARDS

Department of Health and Human Services Certificate of Need Review Standards Synopsis for Publication in the Michigan Register for Surgical Services ...... 405-405

EMERGENCY RULES

Department of Licensing and Regulatory Affairs Director’s Office (2017-029) Extension of Emergency Rule Standing Order for Dispensing Opioid Antagonist ...... 407-409

Department of Licensing and Regulatory Affairs Director’s Office (2017-090) Medical Marihuana Facilities Licensing Act ...... 410-435

EXECUTIVE ORDERS AND EXECUTIVE REORGANIZATION ORDERS

Executive Order No. 2017 - 10 Department of Health and Human Services; Creation of the Public Health Advisory Council ... 437-441

Executive Order No. 2017 - 11 Cleanup of Obsolete and Outdated Boards, Commissions and Councils ...... 442-445

MICHIGAN ADMINISTRATIVE CODE TABLE

Table (2017 Session) ...... 447-451

CUMULATIVE INDEX

Cumulative Index (2017) ...... 452-456

BILLS SIGNED INTO LAW OR VETOED

Appendix Table 1 (2017 Session) (Legislative Service Bureau Pages (1-20) ...... 457-457 2017 MR 22 – December 15, 2017

ADMINISTRATIVE RULES FILED WITH THE SECRETARY OF STATE

MCL 24.208 states in part:

“Sec. 8. (1) The Office of Regulatory Reinvention shall publish the Michigan register at least once each month. The Michigan register shall contain all of the following:

* * *

(f) Administrative rules filed with the secretary of state.”

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ADMINISTRATIVE RULES

DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

PUBLIC SERVICE COMMISSION

BILLING PRACTICES APPLICABLE TO NON-RESIDENTIAL ELECTRIC AND GAS CUSTOMERS

Filed with the Secretary of State on December 4, 2017 These rules take effect 7 days after filing with the Secretary of State.

(By authority conferred on the public service commission by section 7 of 1909 PA 106, section 2 of 1909 PA 300, section 5 of 1919 PA 419, sections 4 and 6 of 1939 PA 3, sections 3, 9, and 231 of 1965 PA 380, MCL 460.557(6), MCL 460.55, MCL 460.4, MCL 460.6, MCL 462.2(12), MCL 16.103, MCL 16.109, and MCL 16.331.)

R 460.1601, R 460.1602, R 460.1603, R 460.1604, R 460.1605, R 460.1606, R 460.1607, R 460.1608, R 460.1609, R 460.1610, R 460.1611, R 460.1612, R 460.1613, R 460.1614, R 460.1615, R 460.1616, R 460.1617, R 460.1618, R 460.1619, R 460.1620, R 460.1621, R 460.1622, R 460.1623, R 460.1624, R 460.1625, R 460.1626, R 460.1628, R 460.1629, R 460.1630, R 460.1631, R 460.1632, R 460.1633, R 460.1634, R 460.1635, R 460.1636, R 460.1637, R 460.1638, R 460.1639, R 460.1640 of the Michigan Administrative Code are rescinded.

PART 1. GENERAL PROVISIONS

R 460.1601 Rescinded.

R 460.1602 Rescinded.

R 460.1603 Rescinded.

R 460.1604 Rescinded.

R 460.1605 Rescinded.

PART 2. APPLICATION FOR SERVICE

R 460.1606 Rescinded.

PART 3. GENERAL CUSTOMER DEPOSIT CONDITIONS

R 460.1607 Rescinded.

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PART 4. METER READING, ESTIMATED BILLS, BILLING ADJUSTMENTS, VOLUNTARY TERMINATION, AND METER RELOCATION

R 460.1608 Rescinded.

R 460.1609 Rescinded.

R 460.1610 Rescinded.

R 460.1611 Rescinded.

PART 5. BILLING AND PAYMENTS

R 460.1612 Rescinded.

R 460.1613 Rescinded.

R 460.1614 Rescinded.

R 460.1615 Rescinded.

R 460.1616 Rescinded.

R 460.1617 Rescinded.

PART 6. CUSTOMER RELATIONS AND UTILITY PROCEDURES

R 460.1618 Rescinded.

R 460.1619 Rescinded.

R 460.1620 Rescinded.

R 460.1621 Rescinded.

R 460.1622 Rescinded.

R 460.1623 Rescinded.

PART 7. SHUTOFFS AND RESTORATION

R 460.1624 Rescinded.

R 460.1625 Rescinded.

R 460.1626 Rescinded.

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PART 8. DISPUTED CLAIMS, HEARINGS AND SETTLEMENT AGREEMENTS

R 460.1628 Rescinded.

R 460.1629 Rescinded.

R 460.1630 Rescinded.

R 460.1631 Rescinded.

R 460.1632 Rescinded.

R 460.1633 Rescinded.

R 460.1634 Rescinded.

R 460.1635 Rescinded.

R 460.1636 Rescinded.

R 460.1637 Rescinded.

R 460.1638 Rescinded.

R 460.1639 Rescinded.

R 460.1640 Rescinded.

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ADMINISTRATIVE RULES

DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

PUBLIC SERVICE COMMISSION

CONSUMER STANDARDS AND BILLING PRACTICES

FOR ELECTRIC AND NATURAL GAS SERVICE

Filed with the Secretary of State on December 4, 2017 These rules take effect 7 days after filing with the Secretary of State.

(By authority conferred on the public service commission by section 7 of 1909 PA 106, section 2 of 1909 PA 300, section 5 of 1919 PA 419, sections 4 and 6 of 1939 PA 3, and sections 3, 9, and 231 of 1965 PA 380, MCL 460.557, MCL 460.55, MCL 460.4, MCL 460.6, MCL 462.2(12), MCL 16.103, MCL 16.109, MCL 16.331, and Executive Reorganization Order Nos. 1996-2, 2003-1, 2008-4, and 2011-4, MCL 445.2001, MCL 445.2011, MCL 445.2025, and MCL 445.2030.)

R 460.101, R 460.102, R 460.106, R 460.107, R 460.108, R 460.109, R 460.110, R 460.111, R 460.112, R 460.113, R 460.114, R 460.115, R 460.116, R 460.117, R 460.118, R 460.119, R 460.120, R 460.121, R 460.122, R 460.123, R 460.124, R 460.125, R 460.126, R 460.127, R 460.128, R 460.129, R 460.130, R 460.131, R 460.132, R 460.133, R 460.134, R 460.136, R 460.137, R 460.138, R 460.139, R 460.140, R 460.141, R 460.142, R 460.143, R 460.144, R 460.145, R 460.146, R 460.147, R 460.148, R 460.149, R 460.150, R 460.151, R 460.152, R 460.153, R 460.154, R 460.155, R 460.156, R 460.157, R 460.158, R 460.159, R 460.160, R 460.161, R 460.162, R 460.163, R 460.164, R 460.165, R 460.166, R 460.167, R 460.168, and R 460.169 of the Michigan Administrative Code are amended, R 460.110 and R 460.135 are rescinded, and R 460.101a, R 460.102a, R 460.102b, R 460.111a, R 460.126a, R 460.126b and R 460.130a are added as follows:

R 460.101 Applicability; purpose. Rule 1. (1) These rules apply to utility service that is provided by electric and natural gas utilities that are subject to the jurisdiction of the public service commission. (2) These rules are intended to promote safe and adequate service to the public and to provide standards for uniform and reasonable practices by electric and natural gas utilities in dealing with residential and nonresidential customers. (3) These rules do not relieve a utility from any of its duties under the laws of this state.

R 460.101a Scope of rules. Rule 1a. (1) Nothing contained in these rules covering consumer standards and billing practices shall be implemented in a manner that circumvents or is inconsistent with utility rules, orders, or tariffs approved by the commission to ensure the safe and reliable delivery of energy service. (2) After notice and an opportunity to be heard, utilities determined by the commission to be in violation of these rules shall be subject to all damages and fines contained within the statutes under which these rules are promulgated.

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(3) Upon written request of a person, utility, or on its own motion, the commission may temporarily waive any requirements of these rules when it determines the waiver will further the effective and efficient administration of these rules and is in the public interest.

R 460.102 Definitions; A to F. Rule 2. As used in these rules: (a) "Actual meter reading" means a natural gas or electric meter reading that is based on the customer's actual energy use during the period reported and that complies with any of the following: (i) Performed by a utility representative. (ii) Performed by the customer and communicated to the company by mail, telephone, fax, on a secure company website, or other reasonable means. (iii) Transmitted to the utility from the meter through a secure communication channel, or by an automated or remote meter reading device. (b) "Aggregate data" means any customer account information from which all identifying information has been removed so that the individual data or information of a customer cannot be associated with that customer without extraordinary effort. (c) "Applicant" means an emancipated minor, a person 18 years of age or older, or a business entity requesting utility electric or natural gas service in the name of that person or entity. (d) "Billing error" means an undercharge or overcharge that is caused by any of the following: (i) An incorrect actual meter reading by a company representative. (ii) An incorrect remote meter reading. (iii) An incorrect meter constant or pressure factor. (iv) An incorrect calculation of the applicable rate. (v) A meter switched by the utility or a utility representative. (vi) An incorrect application of the rate schedule. (vii) Failure to provide a monthly bill to the customer at the end of a billing cycle except as provided in these rules or other relevant tariffs. (viii) Another similar act or omission by the utility in determining the amount of a customer's bill. An undercharge or overcharge that is caused by a non-registering meter, a meter error, or the use of an estimated meter reading or a customer reading is not a billing error. (e) "Billing month" means a natural gas or electric consumption period of not less than 26 days or more than 35 days. (f) "Billing specialist" means a representative of a utility who investigates and resolves meter reading discrepancies or errors. (g) "Commission" means the Michigan public service commission. (h) "Complaint determination" means the written decision of a hearing officer after a customer hearing. (i) "Critical care customer" means any customer who requires, or has a household member who requires, home medical equipment or a life support system, and who, on an annual basis, provides a commission-approved medical certification form from a physician or medical facility to the utility identifying the medical equipment or life support system and certifying that an interruption of service would be immediately life-threatening. (j) "Customer" means an account holder who purchases electric or natural gas service from a utility. An individual who is a customer must be at least 18 years of age or an emancipated minor. (k) "Customer hearing" means a hearing on a disputed matter before a hearing officer that a utility offers to a customer under the provisions of R 460.155. (l) "Cycle billing" means a system that renders bills for utility service to various customers on different days of a calendar month.

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(m) "Delinquent account" means an account with charges for utility service that remains unpaid 5 days or more after the due date. (n) "Eligible low-income customer" means a utility customer whose household income does not exceed 150% of the federal poverty guidelines as published by the United States department of health and human services or who receives any of the following: (i) Supplemental security income or low-income assistance through the department of human services or successor agency. (ii) Food stamps. (iii) Medicaid. (o) "Eligible military customer" means a utility customer, spouse of a customer, or customer whose spouse is in the military who meets all of the following: (i) Is on full-time active duty. (ii) Is deployed overseas in response to a declared war or undeclared hostilities or is deployed within the United States in response to a declared national or state emergency and the household income is reduced as a result. (iii) Notifies the utility of his or her eligibility. (iv) Provides verification of eligibility if requested by the utility. (p) "Eligible senior citizen customer" means a utility customer who meets both of the following criteria: (i) Is 65 years of age or older. (ii) Advises the utility of his or her eligibility. (q) "Energy assistance program" means a program that provides financial assistance or assistance in improving residential energy efficiency and energy conservation. (r) "Energy usage" means the consumption of electricity or natural gas. (s) "Estimated bill" means a bill for service at the premises that is not based on an actual meter reading for the period being billed but that is based on calculations of how much natural gas or electricity a customer likely used during the billing period. (t) "Formal hearing" means a dispute resolution process administered by an administrative law judge pursuant to these rules, applicable tariffs, and the rules of practice and procedure before the commission, R 792.10101 to R 792.11903. (u) "Formal hearing request" means a document describing how a regulated utility has violated these rules, a commission order, or a tariff that is presented in writing to the executive secretary of the commission to initiate an administrative process pursuant to the rules of practice and procedure before the commission.

R 460.102a Definitions; G to P. Rule 2a. As used in these rules: (a) "Gas cost recovery" means the adjustment in rates to recognize the cost of purchased natural gas. (b) "Hearing officer" means a notary public who is qualified to administer oaths to conduct customer hearings against the utility company and who is on a list filed with the commission. (c) "Heating season" means the period between November 1 and March 31. (d) "In dispute" means that a matter is the subject of an unresolved disagreement, claim, or complaint against a utility by a customer, or the customer's authorized agent. (e) "Informal complaint" means a matter that requires follow-up action or investigation by the utility or the commission to resolve the matter without a customer hearing or formal hearing.

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(f) "Inquiry" means a question regarding a utility matter that is asked by the customer and answered by the utility or the commission. (g) "Large nonresidential customer" means a nonresidential customer with usage of 300 Mcf or more of natural gas per year or 30,000 kWh or more of electric usage per year, including schools and centrally metered apartment buildings. (h) "Late payment charge" means a finance, service, carrying, or penalty charge that is assessed by a utility because a bill or portion of a bill is delinquent. (i) "Medical emergency" means an existing medical condition of the customer or a member of the customer's household, as defined and certified by a physician or public health official on a commission-approved medical certification form, that will be aggravated by the lack of utility service. (j) "Meter" means a utility-owned device that measures the quantity of natural gas used by a customer, including a device that measures the heat content of natural gas or a utility-owned device that measures and registers the amount of electrical power used. (k) "Meter error" means a failure to accurately measure and record all of the natural gas or electrical quantities used that are required by the applicable rate or rates. (l) "New customer" means a customer who has not received the utility's service within the previous 6 years. (m) "Occupant" means an individual or entity, other than the customer of record, occupying a premises. An occupant who is an individual must be at least 18 years of age or an emancipated minor. (n) "Peak season" means the period during which a utility experiences its maximum demand for electric or natural gas service. (o) "Positive identification information" means a consistently used appropriate identification such as, but not limited to, any of the following: (i) A driver's license, identification card issued by a state, U.S. military card, U.S. military dependent's identification card, Native American tribal document, passport, or other government-issued identification containing a photograph. (ii) Articles of incorporation, tax identification documents, business license, certificate of authority, or similar documents proving identity of a business. (p) "Power supply cost recovery" means the adjustment in rates to recognize the cost of purchased power and fuel for electric generation. (q) "Prepaid service" means a commission-authorized plan that entitles a utility to receive payments for service to a customer’s premises in advance of the customer’s actual usage of the service. (r) "Previous customer" means a customer who has received the utility's service within the previous 6 years but is not currently receiving service. (s) "Primary purpose" means the collection, use, or disclosure of information that a utility collects or a customer supplies when an authorized business need exists or as an emergency response requires in order to do any of the following: (i) Provide, bill, or collect for regulated electric or natural gas service. (ii) Provide for system, grid, or operational needs. (iii) Provide services as state or federal law requires or as the utility’s approved tariff specifically authorizes. (iv) Plan, implement, or evaluate programs, products, or services related to energy assistance, demand response, energy management, or energy efficiency.

R 460.102b Definitions; Q to Z. Rule 2b. As used in these rules:

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(a) "Regulation officer" means a member of the commission staff who resolves complaints pursuant to these rules. (b) "Remote shutoff and restoration capability" means the ability to terminate or restore service to a premises from another location. (c) "Residential service or use" means the provision or use of electricity or natural gas for residential purposes. (d) "Satisfactory payment history" means that a customer's account was not delinquent more than 1 time in the past 12 months. (e) "Seasonally billed customer" means a customer who is billed on a seasonal basis pursuant to a utility tariff that is approved by the commission. (f) "Secondary purpose" means any purpose that is not a primary purpose. (g) "Settlement agreement" means a documented agreement that is entered into by a customer and a utility and that resolves any matter in dispute. (h) "Shutoff of service" means a discontinuance of utility service that is not requested by a customer. (i) "Small nonresidential customer" means a nonresidential customer with usage of less than 300 Mcf of natural gas per year or less than 30,000 kWh of electric usage per year, including schools and centrally metered apartment buildings. (j) "Termination of service" means a discontinuance of utility service that is requested by a customer or when there is no customer of record. (k) "Third party" means a person or entity that has no contractual relationship with the utility to perform services or act on behalf of the utility or customer. (l) "Unauthorized use of utility service" or “unauthorized use” means theft, fraud, interference, or diversion of service, including but not limited to, meter tampering which is any act that affects the proper registration of service through a meter; by-passing which is unmetered service that flows through a device connected between a service line and customer-owned facilities; and, service restoration by anyone other than the utility or its representative. (m) "Utility" means a firm, corporation, cooperative, association, or other legal entity that is subject to the jurisdiction of the commission and that provides electric or gas service.

PART 2. APPLICATION FOR SERVICE

R 460.106 Service requests Rule 6. (1) Applicants for service may become customers by requesting service in person at the utility company office, in writing, by telephone, fax, or internet, or other means of communication. Using any of these methods, an applicant shall do all of the following: (a) Provide positive identification information as defined in R 460.102a. (b) Upon request, show ownership or a lease for the property where service will be rendered if applying to be a nonresidential customer. (c) Pay a deposit, if required by these rules. (2) The utility may also require payment of a delinquent account as a condition of providing or continuing service if the following conditions apply: (a) The delinquent account is in the customer's or applicant's name. (b) The delinquent account is not in dispute, owed to the utility, and accrued within the last 6 years. The utility shall provide the applicant with information on the process to refute or contest the delinquent account.

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R 460.107 Residential service account requirements. Rule 7. (1) A utility, applicant, or customer may request the addition of more than 1 adult on the residential service account by meeting both of the following requirements: (a) The utility obtains documented approval from both the applicant and additional adult. (b) The additional adult provides positive identification information. (2) If the applicant is renting the premises for which residential service is requested, a utility may require proof that the applicant is a tenant. Written or oral confirmation by the manager, landlord, or owner of the property, or a verified signed copy of the rental agreement is sufficient proof. A utility may verify a lease by requesting a lease agreement containing notarized signatures of the landlord and tenant or by obtaining contact information for the landlord. (3) A utility may require proof of ownership if an applicant is requesting residential service for a premises he or she has purchased. (4) An occupant shall establish an account with a utility within 30 business days of taking occupancy or ownership, whichever comes first, except where residential service is included in a lease. (5) If a customer ceases to live in a residence while another occupant continues to live in the residence, both of the following requirements shall be met: (a) The customer shall notify the utility pursuant to R 460.127 that he or she is discontinuing service. (b) An occupant desiring to continue utility service at that address shall establish an account in his or her name within 30 days of the customer's notification of termination of service, or, if the customer fails to notify the utility, within 30 days of the date the customer ceases to reside at the address. A utility may hold an occupant who fails to establish an account under this subdivision responsible for the use of the utility service after the customer has ceased to reside at the residence. The utility shall not back bill the occupant for a period longer than 24 months from the date the customer terminated service, or, if the customer has failed to notify the utility of the termination of service, from the date that the utility first discovered the customer's change in residency.

PART 3. DEPOSITS AND GUARANTEE TERMS AND CONDITIONS

R 460.108 Prohibited practices. Rule 8. A utility shall not require a deposit or other guarantee as a condition of new or continued utility service based upon any of the following: (a) Consumer credit score, if the customer or applicant has prior utility service credit history with any electric or gas utility during the previous 6 years. (b) Income. (c) Home ownership. (d) Residence location. (e) Race. (f) Color. (g) Creed. (h) Sex. (i) Age. (j) National origin. (k) Marital status. (l) Familial status. (m) Disability. (n) Any other criteria not authorized by these rules.

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R 460.109 Deposit for residential customer. Rule 9. (1) A utility may require a deposit as a condition of providing, restoring, or continuing residential service to an applicant or customer if any of the following provisions apply: (a) At the time of the request for service, the applicant or customer has an unpaid balance for electric or natural gas service that accrued within the last 6 years and that remains unpaid and is not in dispute. (b) The applicant or customer misrepresents his or her identity or credit standing. (c) The applicant or customer fails to provide positive identification information upon request at the time of applying for new service. (d) The applicant or customer requests service for a location at which he or she does not reside. (e) The applicant or customer engaged in unauthorized use of utility service within the last 6 years, if the finding of unauthorized use of utility service was made after notice and an opportunity for a hearing and is not in dispute. (f) The utility has had 1 or more checks issued from the customer's account returned from a financial institution for insufficient funds or no account or has had 1 or more payments from the customer's debit or credit card or other form of payment denied within the last 12 months, excluding financial institution error. (g) The customer or applicant has sought relief under federal bankruptcy laws within the last 6 years. (h) Within the past 3 years, the customer or applicant lived in a residence with a person under all of the following circumstances: (i) The person accrued a delinquent account for electric or natural gas service to the shared residence during the time the customer or applicant lived there. (ii) The delinquent account remains unpaid and is not in dispute. (iii) The person with the delinquent account now resides with the applicant. (2) Notwithstanding any of the provisions of subrule (1) of this rule, a utility shall not require a deposit as a condition of providing service or continuing service to a current residential customer if any of the following provisions apply: (a) The department of health and human services or its successor agency is currently making or has committed to making a payment or payments to the utility on behalf of the applicant. (b) The applicant or customer secures a guarantor who is a customer in good standing with the utility. (c) The applicant is 65 years of age or older and has a satisfactory payment history for the past 3 years with any natural gas or electric utility.

R 460.110 Rescinded.

R 460.111 General deposit conditions for residential customers. Rule 11. (1) All of the following apply to payment of deposits for residential service: (a) For a primary residence, a deposit that is required under these rules due to a prior outstanding account that is not in dispute or a shutoff for nonpayment shall not be more than twice the average monthly bill for the premises or, if the current customer's consumption history for the premises is unavailable, twice the utility's system average monthly bill for residential service. (b) For seasonal properties, a deposit that is required under these rules due to a prior outstanding account that is not in dispute or a shutoff for nonpayment shall not be more than twice the average monthly bill for peak season usage. (c) A utility shall offer an eligible low-income customer the option of paying a deposit required under these rules in 2 monthly installments. (2) Whenever a utility requests a deposit because of an unpaid account for residential service incurred in another household member's name for a time when the customer and the other person shared

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a residence, as described in R 460.109(1)(h), the utility shall provide the customer with notice of the reason for the request, the commission rule that allows the utility to make the request, and the process for refuting the action. (3) A deposit that is required during the heating season due to a shutoff of service for nonpayment within the past 12 months, shall not exceed the utility system average monthly natural gas bill for natural gas residential service or the utility system average monthly electric bill for electric residential service. If the customer receives natural gas and electric residential service from a combination utility, the deposit shall not exceed the total of the utility's combined system average monthly natural gas and electric bills. (4) A deposit that is required as a condition of providing, restoring, or continuing residential service due to unauthorized use of utility service shall not be more than either of the following: (a) Four times the average peak season monthly bill for the premises if the customer's consumption history for the premises is available. (b) Four times the utility's system average peak season monthly bill for residential service if the customer's consumption history for the premises is unavailable. (5) The utility may also require payment of the delinquent account and approved charges as a condition of providing, restoring, or continuing residential service if the account is in the customer's, or applicant's name, is delinquent, owed to the utility, and accrued within the last 6 years. (6) Unless the applicant misrepresents his or her identity or credit standing or fails to provide positive identification information, if requested, at the time of applying for residential service, the utility shall not assess a deposit if the customer has been receiving service for 30 days or more. (7) Except in the case of unauthorized use of utility service, if the utility shuts off residential service for nonpayment, the utility shall not require a deposit as a condition of restoring service unless the utility offered the customer, prior to shutoff for nonpayment, the opportunity to enter into a payment plan as provided in Part 10 of these rules, R 460.154 to R 460.159. (8) A utility shall pay interest at the rate of 5% per annum on all deposits. A utility shall credit interest semiannually to the residential service account of the customer or pay it upon the return of the deposit, whichever occurs first. (9) The customer's credit shall be established and the utility shall return the deposit and accrued interest upon satisfactory payment by the customer of all proper charges for residential service for a period of 12 consecutive months. A utility may retain the deposit assessed because of unauthorized use of utility service for a period of 36 months and shall refund the deposit upon satisfactory payment of the final 12 months' charges. (10) For purposes of this rule, payment is satisfactory if it is made before the issuance of a notice of shutoff of service for nonpayment that is not in dispute or within 5 days after the issuance of the next succeeding monthly bill, whichever is sooner. (11) For customers terminating residential service, if the utility has not already returned the deposit, the utility shall credit the deposit, with accrued interest, to the final bill. For customers continuing to receive service, a utility may apply the deposit against an existing arrearage that is not in dispute. The utility shall promptly return the balance to the customer. (12) A utility shall maintain a detailed record of all deposits received for residential service. The record shall show all of the following information: (a) The name and address of the depositor and either the applicant or customer. (b) The location served by the utility at the time of making the deposit and each successive location while the deposit is retained. (c) The amount and date of the deposit. (d) The dates the utility paid interest and the amounts. (e) Each transaction concerning the deposit.

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(f) The terms and conditions governing the return of the deposit. (13) A utility shall provide the applicant or customer with a receipt for the deposit and instructions regarding how a person who is entitled to the return of his or her deposit may obtain the deposit. (14) A utility shall make reasonable efforts to locate applicants or customers with unclaimed deposits or credits. (15) A utility shall apply deposit standards uniformly to all applicants and customers. A utility shall provide to any person who objects to paying a deposit information on the process to contest the deposit requirement.

R 460.111a General deposit conditions for nonresidential customers. Rule 11a. (1) A utility may require a deposit from a customer or applicant as a condition of receiving or continuing nonresidential service if 1 of the following conditions applies: (a) The customer or applicant has an unfavorable credit rating with a credit reporting agency. (b) The customer or applicant has an unpaid delinquent bill for natural gas or electric service. (c) The customer or applicant has engaged in unauthorized use of utility service within the last 6 years. (d) Two or more shutoff notices have been issued within the most recent 12-month period. (e) Service has been discontinued for nonpayment. (f) An unsatisfactory record of bill payment within the first 6 months after service commenced exists. (2) If a deposit for nonresidential service is required, all of the following limitations apply: (a) A deposit for small nonresidential customers shall not be more than 15% of the customer's annual electric or natural gas bill. (b) Large nonresidential customers may be required to pay a deposit equal to 25% of the customer's annual electric or natural gas bill. (c) If a customer or applicant has engaged in unauthorized use of utility service, the deposit shall not be more than 4 times the average peak season monthly bill, or 4 times the utility's system average peak season monthly bill for the same class of service if the customer's consumption history for the service is unavailable. (3) During the heating season, a small nonresidential customer shall not pay a deposit unless that customer has been shut off for nonpayment during the prior 12 months. A customer deposit under this subrule may not exceed the customer's average monthly bill. (4) A utility may retain a deposit for nonresidential service until the customer accrues a record of 12 continuous months of bill payment on or before the due date. (5) A utility shall pay interest at the rate of 5% per annum on all deposits for nonresidential service. A utility shall credit interest semiannually to the customer's service account or pay it upon the return of the deposit, whichever occurs first. (6) If nonresidential service is terminated, the utility may apply the deposit, plus accrued interest, to the customer's unpaid balance. If the deposit plus the accrued interest is more than the unpaid balance, then the utility shall return the excess to the customer. (7) A utility shall maintain a detailed record of all deposits received for nonresidential service. The record shall show all of the following information: (a) The name and address of the depositor and applicant or customer. (b) The location served by the utility at the time of making the deposit and each successive location while the deposit is retained. (c) The amount and date of the deposit. (d) The dates the utility paid interest and the amounts. (e) Each transaction concerning the deposit. (f) The terms and conditions governing the return of the deposit.

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(8) A utility shall provide the nonresidential customer or applicant with a receipt for the deposit and instructions regarding how a customer who is entitled to the return of the deposit may obtain it. (9) The utility shall make reasonable efforts to locate customers due unclaimed deposits and credits for nonresidential service. (10) Each utility shall, within 60 days of the effective date of this rule, transmit a notice explaining the conditions under which a deposit for nonresidential service may be required to all existing customers. This notice shall also be provided to new customers within 30 days after service has commenced or, at the utility's option, with the first bill rendered. (11) The utility may, at its option, accept an irrevocable financial institution letter of credit, a surety bond, or other corporate guarantee instead of a deposit for nonresidential service.

R 460.112 Guarantee terms and conditions for residential customers. Rule 12. (1) A guarantee for residential service that is accepted in accordance with these rules shall be in writing and shall be in effect for not more than 36 months. The written guarantee shall state all of the terms of the guarantee and the maximum amount guaranteed. The utility shall not hold the guarantor liable for a greater amount, unless agreed to in a separate written guarantee. (2) Notwithstanding the stated term of the guarantee, if longer than 12 months, the customer's credit shall be established and the utility shall release the guarantor upon satisfactory payment by the customer of all proper charges for residential service for a period of 12 consecutive months, unless the guarantee was required due to unauthorized use of utility service. (3) A utility may require a guarantee for residential service because of unauthorized use of utility service for 36 months. (4) For purposes of this rule, payment is satisfactory if it is made before the issuance of a notice of shutoff of service for nonpayment that is not in dispute or within 5 days after the issuance of the next succeeding monthly bill, whichever is sooner. (5) A utility may withhold the release of a guarantor pending the resolution of a shutoff for nonpayment that is in dispute in accordance with these rules.

PART 4. METER READING PROCEDURES, METER ACCURACY, METER ERRORS AND METER RELOCATION

R 460.113 Actual and estimated meter reading. Rule 13. (1) Except as specified in these rules, a utility shall provide all customers with an actual meter reading each billing month. (2) A utility shall outline in its tariff a process that addresses missing or invalid usage data affecting the amount billed to a customer and that ensures the amount billed during the billing period is appropriate. (3) A utility may estimate a meter reading under any of the following circumstances: (a) An actual meter reading cannot be obtained by any reasonable or applicable method described in R 460.102. (b) An automated or remote meter reading device is not functioning and customer usage data cannot be retrieved. (c) A utility meter reader does not have access to the meter. (d) There is a condition at the meter location that puts the meter reader's safety at risk. (e) The utility bills the customer seasonally in accordance with its commission-approved tariffs.

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(4) If a utility estimates a meter reading pursuant to subrule (3)(c) or (3)(d) of this rule, the utility shall notify the customer of all of the following information: (i) The reason for the estimated reading. (ii) Safe access must be provided. (iii) A customer has the option of reading the meter and submitting the actual meter reading to the utility pursuant to these rules. (iv) A utility may install a remote meter, actual meter reading device, or other similar device that provides the utility with an actual meter reading. (5) If a meter reading equipment failure occurs, the utility shall make all reasonable efforts to replace or repair equipment so that not more than 2 estimated bills are issued. (6) A utility shall not use estimated meter reads to deny residential customers the benefit of a lower- tiered rate, if available. (7) If a utility cannot obtain an actual meter reading, then the utility shall maintain records of the efforts made to obtain such a reading and its reasons for failing to obtain it. (8) A utility may estimate customer bills only upon a finding by the commission that a utility's estimated bill procedures assure reasonable billing accuracy. A bill that is rendered on an estimated basis shall be clearly and conspicuously identified as such. A utility shall submit any substantive changes to its billing estimation procedures to the commission for approval. (9) An estimated bill that is generated because the actual meter reading is outside the range for the premises usage shall not be issued in consecutive months. If the utility is actively engaged in resolving the problem, an additional 30 days is permitted to correct the problem and obtain an actual meter reading. (10) If a utility shuts off service due to nonpayment, the utility shall complete a final reading, or, if unable to obtain an actual meter reading after reasonable attempts, the utility may estimate the bill. (11) If a utility estimates a customer's bill for 2 or more consecutive months and an actual meter reading is then obtained, the utility shall offer the residential and small nonresidential customer the opportunity to pay the bill over the same number of months as consecutively estimated bills. This subrule does not apply if the utility cannot obtain access to the meter and the customer fails to provide an actual meter reading if requested by the utility.

R 460.114 Customer meter reading. Rule 14. A utility shall provide residential and small nonresidential customers with the opportunity to read and report energy usage provided that the customer accurately reports energy usage on a regular basis. A utility shall provide postage-paid, pre-addressed postcards for this purpose upon request, or the utility may permit customers to report meter readings on a secure company website, by telephone, or other reasonable means. At least once every 12 months, a utility shall obtain an actual meter reading of energy usage to verify the accuracy of readings reported in this manner. Notwithstanding the provisions of this rule, a utility company representative may read meters on a regular basis.

R 460.115 Meter accuracy and errors. Rule 15. (1) Meters with actual meter readings that are rejected by the utility billing system for 2 consecutive months because they are outside the expected range of the customer's usage for the premises shall be reviewed by a billing specialist, investigated, and, if necessary, the utility shall repair or replace the meter. (2) A utility shall calculate the period and amount of inaccuracy of electric meters pursuant to R 460.3616 and R 460.3309. A utility shall calculate the period and amount of inaccuracy of gas meters pursuant to R 460.2361 and R 460.2362.

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(3) If a utility finds that an electric or gas meter has an average meter accuracy less than 98% or more than 102%, an adjustment for bills for the inaccuracy may be made in the case of under registration and shall be made in the case of over registration. (4) Notwithstanding the provisions of any other rule, except in the case of unauthorized use of utility service, back billing of customers or refunds to customers for meter errors is limited to the 12-month period immediately preceding discovery of the error. The customer shall be given a reasonable time in which to pay the amount of the back billing, after consideration of the amount of the back bill and the duration of the inaccuracy, and service shall not be shut off during this time for nonpayment of the amount of the back billing if the customer is complying with the repayment agreement. (5) If the amount due the utility is more than $5.00, the utility may bill the customer for the amount due. The utility shall offer the customer reasonable payment arrangements for the amount due. The bill for the undercharge shall not include interest. (6) If the amount of the refund due an existing or previous customer as the result of meter over registration is less than $5.00, a refund is not required to be made. Paid overcharges shall be credited to the existing customer or paid to a previous customer with 5% interest, commencing on the 60th day following payment.

R 460.116 Meter relocation. Rule 16. (1) A utility may assess a meter relocation charge in any of the following situations: (a) The utility shut off service by disconnection at the street or pole because the utility could not obtain access to the meter or utility facilities. (b) The customer, its authorized agent, or another responsible adult refused to permit the utility access to the meter on 2 separate occasions, or on a single occasion if harm is threatened, and the utility can produce documentation of requests for access and/or requests for the customer to perform a meter reading that were refused. (c) The utility shut off service due to unauthorized use of utility service or the customer acknowledges personal responsibility and the utility bills the customer for unauthorized use of utility service. (d) The customer requests that the utility relocate the meter or other utility facilities. (2) If the utility moves the meter for reasons other than the reasons listed under subrule (1) of this rule, and the customer wants the meter placed in a different location than that selected by the utility, then the customer shall pay any additional costs.

PART 5. BILLING AND PAYMENT STANDARDS

R 460.117 Bill information. Rule 17. (1) Except for prepaid service, the utility shall bill each customer promptly after reading the meter. The bill shall state clearly all of the following information: (a) The beginning and ending actual meter readings and dates for the billing period. (b) The units of energy consumed during the billing period and the units of energy consumed during the comparable period the prior year. Upon customer request, the utility shall provide weather-adjusted consumption data to the customer or to a third party designated by the customer. (c) A designation of the rate. (d) The due date. (e) Any previous balance. (f) The amount due for energy usage. (g) The amount due for other authorized charges.

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(h) The amount of tax. (i) The total amount due. (j) The applicable rate schedules, the explanation of rate schedules, and the explanation of how to verify the accuracy of the bill will be provided by the company upon request. (k) That the customer should contact the company regarding an inquiry or complaint about the bill before the due date. (l) The address and telephone number of the utility at which the customer may initiate any inquiry or complaint regarding the bill or the service provided by the utility. (m) That the utility is regulated by the commission. (n) For nonresidential customers, the bills shall contain all of the following: (i) The date by which the customer must pay the bill to benefit from any discount or to avoid any penalty. (ii) Any conversions from meter reading units to billing units, any calculations to determine billing units from recording or other devices, or any other factors, such as power supply cost recovery adjustments, used in determining the bill. A statement may appear on the bill advising the customer that the information can be obtained by contacting the utility. Any multiplier used to determine billing units shall be shown when used. (iii) If the billing period differs from the meter reading cycle and the reading data is calculated from actual metered data, then the actual meter reading shall be shown on the bill. (2) A commission-regulated utility proposing a new bill format shall submit its proposed bill format to the commission staff prior to introduction to its customers.

R 460.118 Electronic billing requirements. Rule 18. Any utility wishing to issue billing statements electronically shall comply with all of the following requirements: (a) A customer shall not be required to use electronic billing. (b) No enrollment or usage fees shall be assessed to a customer who chooses to receive bills or customer information electronically. (c) The electronic billing statement shall include, at minimum, all information listed in R 460.117. (d) The company shall maintain a secure and encrypted site to be accessed by the customer after completing a secure registration process. (e) The utility may require that the customer use a password or security question to access the electronic billing system. The company shall not require the customer to use his or her social security number to enroll in or access the billing system. (f) Any fees to accept electronic payments shall be clearly displayed in the payment window. (g) Any payment made electronically shall be treated as a payment to the company business office. (h) Use of the electronic system shall not restrict the customer in using other payment methods. All other payment methods shall continue to be available to the customer.

R 460.119 Separate bill; consolidation and balance transfers for residential and small nonresidential customers. Rule 19. (1) A utility shall transmit a separate bill pursuant to R 460.117 for service to residential and small nonresidential customers provided at each service location. (2) A utility may consolidate 2 or more active accounts with the documented authorization of the residential or small nonresidential customer. (3) Notwithstanding the provisions of subrule (1) of this rule, if there is a shutoff or termination of service at a separate metering point, residence, or other location pursuant to these rules, then a utility

17 2017 MR 22 – December 15, 2017 may transfer an unpaid balance to any other account of the customer if either of the following requirements are met: (a) Unpaid balances from residential accounts are only transferred to another residential service account of that customer. (b) Unpaid balances from any nonresidential account are only transferred to another nonresidential account of that customer. (4) The utility shall have positive identification information that shows that the residential or small nonresidential customer is the same at both residences or locations and shall present that information to the customer upon request. (5) When a utility transfers an unpaid balance, the utility shall provide the residential or small nonresidential customer with a written notice of the balance transfer, the balance transfer address, the amount of the transfer, the commission rule that allows the transfer, and the process for refuting the action.

R 460.120 Billing frequency; method of delivery. Rule 20. (1) A utility shall send a bill each billing month to its customers pursuant to the approved rate schedules unless the utility and the customer agree to another billing interval or the commission approves an alternative billing frequency method. A utility shall send a bill to customers by mail unless the utility and the customer agree to another method of delivery. (2) A utility that is authorized to bill customers seasonally or use a customer-read system shall send a bill pursuant to the tariffs approved by the commission. (3) A bill shall be mailed, transmitted, or delivered to the customer not less than 21 days before the due date. Failure to receive a bill properly mailed, transmitted, or delivered by the utility does not extend the due date. (4) A customer may designate a third party to receive bills, shutoff notices, or other communications from the utility on the customer's behalf if the customer submits a document signed by the customer and the designated third party to the utility. The receipt of bills by a third party does not make that party responsible for the bills unless the third-party recipient is a guarantor under R 460.112. (5) Customers who use electronic billing and payment shall have the same rights and responsibilities as customers who use paper bills and payment by United States mail.

R 460.121 Equal monthly billing. Rule 21. Upon a residential customer’s request, a utility shall bill a residential customer with a satisfactory payment history under an equal monthly billing program, if the commission finds that the billing program assures reasonable billing accuracy. If a residential customer has a credit balance of more than $10.00 at the end of the program year, upon the request of the customer, the utility shall either return the credit balance or credit it to the next month's bill. If the balance is less than $10.00, the utility shall credit the amount to the residential customer's account.

R 460.122 Cycle billing. Rule 22. A utility may use cycle billing if a customer receives a bill on or about the same day of each billing month. If a utility changes meter reading routes or schedules by more than 7 days, it shall provide notice to affected customers at least 10 days before making the change.

R 460.123 Payment of bill. Rule 23. (1) A utility shall permit each customer a period of not less than 21 days from the date the bill was sent to pay in full, unless the customer and the utility agree on a different due date. A utility

18 2017 MR 22 – December 15, 2017 shall not withdraw funds from a customer’s account before the due date in cases where a customer uses an automatic bill payment plan unless the customer agrees to a different period. (2) Except as otherwise provided in subrule (3) of this rule, a utility shall not attempt to recover from a customer any outstanding bills or other charges due upon the account of any other person, unless that customer has entered into a lawful guarantee under R 460.112, or another lawful agreement to pay those bills and charges. (3) To avoid shut off of residential service pursuant to R 460.137(2)(b), when an occupant has lived with a residential customer within the last 3 years, currently resides with the customer, and the customer has a delinquent account that remains unpaid, is not in dispute, and accrued during shared residency, both are equally responsible for the unpaid bill. The utility shall advise the customer and occupant of the process by which the customer may refute this claim unless that customer has entered into a guarantee under R 460.112, or another agreement to pay those bills and charges. (4) The customer has the right to pay any delinquent account at any time prior to the shut off of service date to preserve uninterrupted service. After proper notice of shut off under R 460.139 and R 460.140 has been provided, it shall be the customer's responsibility to contact the utility and arrange payment before disconnection. (5) The utility may authorize an agent to accept payments on behalf of the utility. The authorized agent shall accept payment and provide payment verification, without request, that may be used by the customer to verify payment with the utility. The payment verification shall clearly state all of the following: (a) That the payment may not be credited to the customer's account for up to 2 business days. (b) Any charges or fees for use of the authorized agent services. (c) That to avoid shutoff, the customer must contact the utility with verification of payment made to an authorized agent. (6) The authorized agent shall remit payments to the utility every other business day, at a minimum, and the company shall credit those payments to customer accounts within 1 business day of receiving them from the payment agent. Authorized agent locations shall be clearly marked as "Authorized Agent for [Company]." The utility shall provide information on bills every 6 months that warns customers not to use unauthorized payment centers. (7) Except in situations of unauthorized use of utility service, a combination utility company, when requested, shall permit eligible low-income customers to do any of the following: (a) Designate how partial payments shall be applied to their account. (b) Choose to retain either the electric service or natural gas service if faced with a shutoff, provided that the customer allows the utility to have access to the non-chosen service for shutoff. (c) Protect the retained service from shut off during the heating season, provided that payments for current usage are made on the retained service and the customer is in good standing with the utility on any payment plan for which the customer qualifies. (8) Whenever an eligible low-income customer of a combination utility company receives a disconnect notice, the notice shall clearly show the customer has both of the following options: (a) An extended payment plan for both gas and electric service. (b) An extended payment plan to retain either gas or electric service as chosen by the customer.

R 460.124 Payment period. Rule 24. (1) The date a bill is sent is the date the utility transmits the billing information to the customer. If the last day for payment falls on a day when the mail is not delivered, or other day when the utility offices that accept customer payments are not open to the general public, the payment date shall

19 2017 MR 22 – December 15, 2017 be extended through the next business day. Customer remittances postmarked on the due date shall be considered to have been timely paid. If the postmark is illegible, the date of mailing shall be designated as 2 days before receipt by the utility. (2) If a customer fails to make full payment by the due date, the utility may implement its collection practices, including the use of automated telephone calls which remind the customer or a third party that the bill is past due. Neither the utility nor its agents shall make more than 1 call per day to a specific customer or third party in which contact is made with the customer or third party.

R 460.125 Late payment charges. Rule 25. (1) Except as otherwise provided by statute, a utility shall bill each residential customer for the amount of natural gas or electricity consumed and any other approved charges pursuant to the rates and tariffs approved by the commission. (2) A utility may assess residential customers a late payment charge that is not more than 2%, not compounded, of the portion of the bill, net of taxes, that is delinquent. A utility shall not assess a late- payment charge against a residential customer whose payments are made by the department of health and human services or who is participating in a shutoff protection program described in Part 9 of these rules, R 460.145 to R 460.153. (3) A utility may not charge residential customers a late payment fee for failure to pay an estimated bill by the due date unless the customer is subsequently delinquent on a bill using an actual meter reading. This rule shall not apply if the bill is estimated because the utility was unable to gain access to the meter, the utility's lack of access is documented, and the customer refused to provide an actual meter reading. (4) For nonresidential customers, unless the utility’s tariff states otherwise, a late payment charge of not more than 2%, not compounded, may be applied to the unpaid balance outstanding, net of taxes, if the bill is not paid in full on or before the date on which the bill is due.

R 460.126 Billing for unregulated non-energy services. Rule 26. A utility may include charges for unregulated non-energy services, such as appliance repair or appliance protection programs, together with charges for natural gas and electric service on the same monthly bill if the charges for the unregulated non-energy services are designated clearly and separately from the charges for the natural gas or electric service and it is noted that it is an unregulated service. Failure to pay for unregulated non-energy service charges may result in the termination of that service but not the shut off of the natural gas or electric service. If partial payment is made, the utility shall first credit payment to the balance outstanding for natural gas or electric service pursuant to the provisions of R 460.123(7) and R 460.123(8) where applicable.

R 460.126a Billing error. Rule 26a. (1) If a utility overcharges a customer due to a billing error, then the utility shall refund or credit the amount of the paid overcharge to the customer. Paid overcharges shall be credited to a customer with 5% APR interest, commencing on the sixtieth day following payment. A utility is not required to adjust, refund, or credit an overcharge plus 5% APR interest for more than the 3 years immediately preceding discovery of the billing error, unless the customer is able to establish an earlier date for commencement of the error. (2) Upon customer request, paid overcharges for billing errors greater than $10.00 shall be refunded within 30 days of the request. (3) If a utility undercharges a customer, in cases that do not involve unauthorized use of utility service, the utility may back bill the customer for the amount of the undercharge during the 12-month period

20 2017 MR 22 – December 15, 2017 immediately preceding discovery of the error, and the utility shall offer the customer reasonable payment arrangements for the amount of the back bill, which shall allow the customer to make installment payments over a period at least as long as the period of the undercharge. The utility shall take into account the customer’s financial circumstances when setting payment amounts.

R 460.126b Responsibility for unauthorized use of utility service. Rule 26b. (1) In cases that involve unauthorized use of utility service, the utility may back bill the customer for the service used. The back bill for service used may include 5% interest. (2) The utility may charge fees for unauthorized use of utility service in accordance with commission- approved tariffs. (3) If a utility shuts off service for unauthorized use of utility service, the utility may bill a customer for all of the following: (a) The cost of investigating the unauthorized use. (b) The cost of relocating the meter. (c) The cost of any damages that have been caused to utility-owned equipment.

PART 6. VOLUNTARY TERMINATION OF SERVICE

R 460.127 Voluntary termination. Rule 27. (1) Subject to the provisions of these rules, a utility customer or authorized representative shall do all of the following: (a) Notify the utility in person, or by telephone, in writing, by fax or on the internet at least 10 business days prior to requested service termination. (b) Allow safe access to the utility, if necessary, to perform a final meter read. (c) Provide an address for final billing at the time of request for a final read. (d) Notify the utility if an existing occupant continues to occupy the premises. (2) The utility shall do both of the following: (a) Provide a final actual meter reading within 10 business days of the request for termination or estimate the final reading and offer the customer the option to provide an actual meter reading. If the meter is not read within the 10-day time frame the utility shall document the reason for no actual meter reading. An actual meter reading shall be obtained by the next normal actual meter reading cycle. (b) Schedule the customer's final reading within a 4-hour time frame if the utility cannot access the meter. (3) A property owner shall provide notice to the utility within 30 days after abandoning or surrendering a property to avoid liability for any unauthorized use of utility service as provided in MCL 460.9d(6).

PART 7. ENERGY ASSISTANCE AND SHUTOFF PROTECTION PROGRAMS FOR RESIDENTIAL CUSTOMERS

R 460.128 Listing of energy assistance programs for residential customers. Rule 28. The commission shall annually provide a listing of all federal and state energy assistance programs and the eligibility requirements of each program to all utilities.

R 460.129 Notice of energy assistance programs for residential customers. Rule 29. (1) A utility shall annually inform each residential customer of all of the following information:

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(a) The federal and state energy assistance programs that are available and the eligibility requirements of the programs, as provided to the utility by the commission. (b) The medical emergency provisions of R 460.130. (c) The critical care customer provisions of R 460.130a. (d) The shutoff protection programs described in R 460.131 and R 460.132. (e) The military shutoff protections of R 460.133. (2) The utility shall provide to residential customers the information required by subrule (1) of this rule. The information in subrule (1) of this rule may be explained on the customer's bill, provided as a bill insert, or provided by other means of transmittal. This information shall also be posted on the company's website. If the utility does not print an explanation on the customer's bill, then the utility shall, on the customer's bill, direct the customer to the bill insert or other transmittal. (3) If additional information regarding energy assistance programs becomes available after the utility's initial notice to residential customers, the commission shall provide that information to all utilities. Within 60 days of receiving the information, the utility shall provide the new eligibility requirements or benefits levels for energy assistance programs to all of its residential customers and the new benefit levels to all customers currently enrolled in the programs. (4) When a residential customer receives a past-due notice from the utility, the utility shall provide the customer access to information about energy assistance programs referenced in subrules (1) and (3) of this rule, which shall, at minimum, include a telephone number of a utility representative who is able to provide this information.

R 460.130 Medical emergency. Rule 30. (1) A utility shall restore service or postpone shut off of service for not more than 21 days if the customer or a member of the customer's household has a medical emergency. The customer shall provide the utility with a commission-approved medical certification form that identifies all of the following: (a) The medical condition. (b) Any medical equipment needed for the medical emergency. (c) The specific time period during which the shut off of service will aggravate the medical emergency. (2) A utility shall not require payment of an after-hours reconnect fee or a deposit as a condition of restoring service for a 21-day medical emergency hold under this rule. (3) Upon request, a utility shall provide and make available on its website a commission-approved medical certification form for use in obtaining a medical emergency hold under this rule. (4) The utility shall provide the customer with a grace period of 3 business days during which the utility shall postpone the shutoff of utility service to allow the customer time to obtain a completed commission-approved medical certification form. (5) The utility shall extend the restoration or postponement for additional periods of not more than 21 days, not to exceed a total postponement of shut off of service of 63 days in any 12-month period per household member, only if the customer provides additional certification that the customer or a member of the customer's household has a medical emergency. (6) A utility shall not be required to grant shutoff extensions totaling more than 126 days per household in any 12-month period. (7) Nothing in this rule relieves the customer of his or her obligation to pay for utility service. (8) Nothing in this rule shall prohibit a utility that observes an unsafe connection at a customer's location caused by unauthorized use of electric or natural gas service, from implementing measures to cure or address the unsafe connection pursuant to section 9d(1) of 1939 PA 3, MCL 460.9d(1).

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R 460.130a Critical care customer shut off protection Rule 30a. (1) A utility shall restore or refrain from shutting off utility service to a critical care customer due to an inability to pay a utility bill where an interruption of service would be immediately life threatening. (2) On an annual basis, a critical care customer shall provide the utility with an updated commission- approved medical certification form certifying his or her continued status as a critical care customer. If the customer’s status as a critical care customer ends, a customer or occupant of the household shall notify the utility of the change in status. (3) A utility shall provide a critical care customer with a grace period of 3 business days during which it shall postpone the shutoff of utility service to the critical care customer to allow the customer time to obtain a completed commission-approved medical certification form. (4) Upon request, a utility shall provide and make available on its website a commission-approved medical certification form for use in obtaining a physician’s or medical facility’s certification demonstrating the customer’s status as a critical care customer. Upon receipt of the medical certification form, the utility shall notify the customer that it has received the form. (5) A utility shall maintain a special file on critical care customers and an appropriate identification of such customers for the purpose of ensuring that utility service is provided for as long as the customer remains a critical care customer and the customer’s inability to pay continues. (6) When a utility has notice of a critical care customer for whom a planned service interruption would be immediately life threatening, the utility shall notify the customer of the planned service interruption and shall not shut off service using remote shutoff capability without first initiating person-to-person contact with the customer. (7) Nothing in this rule relieves the customer of his or her obligation to pay for utility service. A utility may require that the customer enter into a reasonable payment plan. (8) Nothing in this rule shall prohibit a utility that observes an unsafe connection at a customer's location caused by unauthorized use of electric or natural gas service, from implementing measures to cure or address the unsafe connection pursuant to section 9d(1) of 1939 PA 3, MCL 460.9d(1).

R 460.131 Winter protection plan for eligible low-income customers. Rule 31. (1) Except where unauthorized use of utility service has occurred, a utility shall not shut off service to an eligible low-income customer during the heating season for nonpayment of a delinquent account if the customer pays to the utility a monthly amount equal to 7% of the estimated annual bill for the eligible customer and the eligible customer demonstrates, within 14 days of requesting shutoff protection, that he or she has made application for state or federal heating assistance. If an arrearage exists at the time an eligible low-income customer applies for protection from shut off of service during the heating season, the utility shall permit the customer to pay the arrearage in equal monthly installments between the date of application and the start of the subsequent heating season. (2) A utility may shut off service to an eligible low-income customer who does not pay the monthly amounts referred to in subrule (1) of this rule after giving notice in the manner required by these rules. (3) If an eligible low-income customer fails to comply with the terms and conditions of this rule, a utility may shut off service after giving the customer notice, by personal service or first-class mail, which contains all of the following information: (a) The eligible low-income customer has defaulted on the winter protection plan. (b) The nature of the default.

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(c) That unless the customer makes the payments that are past due under this rule within 10 days of the date of mailing, the utility may shut off service. (d) The date on or after which the utility may shut off service, unless the customer takes appropriate action. (e) That the customer has the right to file a complaint disputing the claim of the utility before the date of the proposed shut off of service by calling the company. (f) That the customer has the right to request a hearing before a hearing officer if the complaint cannot be otherwise resolved and that the customer must pay to the utility that portion of the bill that is not in dispute within 7 business days of the date that the customer requests a hearing. (g) That the customer has the right to represent himself or herself, be represented by counsel, or be assisted by other persons of his or her choice in the complaint process. (h) That the utility will not shut off service pending the resolution of a complaint that is filed with the utility or the commission pursuant to these rules. (i) The telephone number and address of the utility where the customer may make inquiry, enter into a payment plan or settlement agreement, or file a complaint. (j) That the customer should contact a social services agency immediately if the customer believes he or she might be eligible for emergency economic assistance. (k) That the utility will postpone shut off of service if a medical emergency exists at the customer's residence and the customer provides the documentation as specified in R 460.147. (l) That the utility may require a deposit and restoration charge if the utility shuts off service for nonpayment of winter protection monthly amounts. (m) That the utility will not shut off service if the customer or the spouse of the customer is on active military duty. (4) At the conclusion of the heating season, the utility shall reconcile the accounts of eligible low- income customers and permit customers to pay any amounts owing in equal monthly installments between April 1 and October 31. A utility may shut off service to eligible customers who fail to make installment payments on a timely basis in the manner required by these rules. (5) Except where unauthorized use of utility service has occurred at a customer's premises within the past 2 years and the bill remains unpaid, during the heating season a utility shall not require an eligible low-income customer, whose utility service has been shut off, to pay a fee for restoring service or a security deposit pursuant to R 460.109 or R 460.111, before applying for protection under this rule. (6) Except where unauthorized use of utility service has occurred within the past 2 years at the premises where the customer has resided and the bill remains unpaid or safety is a concern, a utility may not require an amount greater than 1/12 of an arrearage owed to restore service or initiate participation in the winter protection plan. (7) Winter protection provisions of these rules do not apply to customers who have been shut off or who have a pending shut off for unauthorized use of utility service within the past 2 years at the customer's current premises until all charges are paid pursuant to these rules or satisfactory payment arrangements are made with the utility. (8) Upon request, the utility shall provide customers who enroll in the winter protection program with documentation that they are participating in the program. (9) Bills issued to customers participating in the winter protection program shall clearly identify the minimum amount that the customer must pay to prevent shut off of service. Utilities may bill at higher amounts to recover past due amounts and the utility may encourage customers to pay amounts in excess of the minimum provided that the minimum payment is clearly designated on the bill. (10) Subject to prior commission approval, a utility may offer an optional shutoff protection program to its customers, provided that the optional shutoff protection program offers eligibility and shutoff

24 2017 MR 22 – December 15, 2017 protection that meets or exceeds the eligibility criteria and customer protections contained in subrule (1) of this rule.

R 460.132 Winter protection plan for eligible senior citizen customers. Rule 32. (1) A utility shall not shut off service to an eligible senior citizen customer during the heating season. (2) At the customer's request, a utility shall restore service to an eligible senior citizen customer's documented personal residence during the heating season without payment of the amount due, deposits, reconnection fees, or other charges. (3) At the conclusion of the heating season, the utility shall reconcile the accounts of eligible senior citizen customers and permit them to pay any amounts owing in equal monthly installments between April 1 and October 31. (4) Nothing in this rule relieves the customer of his or her obligation to pay for utility service. (5) Nothing in this rule shall prohibit a utility that observes an unsafe connection at a customer's location caused by unauthorized use of electric or natural gas service, from implementing measures to cure or address the unsafe connection pursuant to section 9d(1) of 1939 PA 3, MCL 460.9d(1).

R 460.133 Eligible military customer. Rule 33. (1) The utility shall not shut off service to an eligible military customer for a period of 90 days. The utility shall continue to provide shutoff protection for at least 1 additional 90-day period as long as the customer meets all of the conditions for an eligible military customer and requests the utility to do so. After the close of the last 90-day period, the utility shall require the customer to pay any past due amounts in equal monthly payments over a period of up to 12 months. (2) The utility shall provide the eligible military customer with information on payment assistance programs. (3) Nothing in this rule shall prohibit a utility that observes an unsafe connection at a customer's location caused by unauthorized use of electric or natural gas service, from implementing measures to cure or address the unsafe connection pursuant to section 9d(1) of 1939 PA 3, MCL 460.9d(1).

R 460.134 Extreme weather condition policy. Rule 34. (1) Within 6 months of the effective date of this rule, a utility shall adopt and submit an extreme weather condition policy to the commission for approval that provides, at a minimum, both of the following: (a) The criteria or factors a utility follows in suspending disconnection of service to residential customers during extreme hot and cold weather. (b) Any preferential treatment given to certain classes of residential customers. (2) In the event of any subsequent changes to the extreme weather condition policy, a utility shall submit those changes to the commission for its review and approval.

R 460.135 Rescinded.

PART 8. PROCEDURES FOR SHUTOFF AND RESTORATION OF SERVICE

R 460.136 Emergency shutoff. Rule 36. Notwithstanding any other provision of these rules, a utility may shut off service temporarily for reasons of health or safety or in a state or national emergency. When a utility shuts off service for reasons of health or safety, the utility shall leave a notice at the premises in accordance with the provisions of R 460.140(1)(a),(b), and (j).

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R 460.137 Shutoff or denial of service permitted. Rule 37. (1) Subject to the requirements of these rules, a utility may shut off or deny service to a customer for any of the following reasons: (a) The customer has not paid a delinquent account that accrued within the last 6 years. (b) The customer has failed to provide a deposit or guarantee permitted by these rules. (c) The customer has engaged in unauthorized use of utility service or unauthorized use of equipment furnished and owned by the utility occurs, including obtaining the use of equipment by submitting an application containing false information. (d) The customer has refused to arrange access at reasonable times for the purpose of inspection, meter reading, maintenance, or replacement of equipment that is installed upon the premises, or for the removal of a meter. (e) An occupant who has used electricity or natural gas has failed to establish service in conformance with these rules. (f) The customer has failed to comply with the terms and conditions of a payment plan or settlement agreement. (g) For violation of, or noncompliance with, the utility's rules on file with, and approved, by the commission. (2) Residential customers may also be shut off or denied service for either or both of the following reasons: (a) The customer misrepresented his or her identity for the purpose of obtaining utility service or put service in another person's name without permission of the other person. (b) An individual living in the customer's residence meets both of the following: (i) Has a delinquent account for service with the utility within the past 3 years that remains unpaid and is not in dispute. (ii) The individual lived in the customer's residence when all or part of the debt was incurred. The utility may transfer a prorated amount of the debt to the customer's account, based upon the length of time that the individual resided at the customer's residence. This paragraph does not apply if the individual was a minor while living in the customer's residence. (3) Nonresidential customers may also be shut off or denied service for either of the following reasons: (a) Failure of the customer to fulfill his or her contractual obligations for service or facilities that are subject to regulation by the commission. (b) Nonpayment of unpaid balances on any other nonresidential account incurred by the customer under a different account name by the customer’s predecessor in interest, or by any other entity, the debt of which the customer is legally obligated to assume.

R 460.138 Shut off prohibited. Rule 38. (1) A utility shall not shut off service for any of the following reasons: (a) The customer has not paid for items, such as merchandise, appliances, or services that are not approved by the commission as an integral part of the utility service that is provided by the utility. (b) During the heating season, the customer is an eligible senior citizen. (c) The customer has not paid for concurrent service received at a separate metering point, residence, or location. (d) The customer has not paid for a different type or class of service received at the same or a different location. The placing of more than 1 meter at the same location for the purpose of billing the usage of specific residential energy-using devices under optional rate schedules or provisions is not a different type or class of service for the purposes of this rule.

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(e) The customer has not paid for service used by another person, such as a tenant. A utility may shutoff service in any of the following circumstances where proper notice has been given: (i) If the customer supplies a written, notarized statement that the premises are unoccupied. (ii) If the premises are occupied and the occupant agrees, in writing, to the shut off of service. (iii) If it is not feasible to provide service to the occupant as a customer without a major revision of existing distribution facilities. Where it is feasible to provide service, the utility shall offer the occupant the opportunity to subscribe for service in his or her own name. If the occupant refuses, the utility may shut off service pursuant to these rules. (f) A person qualifies as an eligible military customer. (g) For nonresidential customers, failure to pay the bill of another customer as guarantor. (h) The customer has an informal complaint, customer hearing, or formal hearing pending with the utility or the commission, except pursuant to the terms of an interim determination, pursuant to R 460.155, R 460.163, and R 460.168.

R 460.139 Notice of shut off. Rule 39. (1) Not less than 10 days before the proposed shut off of service, pursuant to the provisions of R 460.140, R 460.142 and R 460.143, a utility shall send a notice to the customer by first-class mail, or personal service. (2) The utility shall send the 10-day notice to the account name and address and to the address where service is provided if the service address is different and the notice can be delivered at that address. A utility shall maintain a record of the date the notice was sent. (3) A utility shall permit a customer to designate a consenting individual or agency to receive a copy of a notice of shut off. (4) Not less than 30 days before the proposed shut off of service to a single-metered dwelling that is used as a residence for 3 or more separate households, a utility shall transmit a notice to each dwelling unit that indicates that the customer of record, the landlord, has failed to pay an outstanding bill and is subject to shutoff of service on or after a specified date. (5) Not less than 10 days before the proposed shut off of service to a nonresidential facility that is occupied by more than 5 business entities that are not responsible for payment of the bill, a utility shall make a reasonable attempt to notify each occupant that service may be subject to shut off after a specified date. (6) For an involuntary shut off, at least 1 day before shut off of service, the utility shall make not less than 2 attempts to contact the customer by telephone, if a telephone number is available to the utility, to advise the customer of the shutoff and what steps the customer must take to avoid shutoff. If the utility uses an automated notification system, the utility shall document the process for ensuring that at least 2 attempts are made to notify the customer of the pending shutoff. If the telephone number is not available, the customer has no telephone, or the utility chooses not to make telephone contacts, the utility shall either leave a notice at the premises advising the customer that service will be shut off on or after the next business day or send notice by first-class mail postmarked at least 5 business days before shutoff of service is scheduled. The utility shall document all attempts to contact the customer. The 10- day notice sent under subrule (1) or (5) of this rule shall be considered as 1 attempt.

R 460.140 Form of notice. Rule 40. (1) A notice of shut off of service shall contain all of the following information: (a) The name and address of the customer, and the address at which service is provided, if different. (b) A clear and concise statement of the reason for the proposed shut off of service. (c) The date on or after which the utility may shut off service, unless the customer takes appropriate action.

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(d) That the residential and small nonresidential customer may have the right to enter into a payment plan with the utility for an amount owed to the utility that is not in dispute and that the customer is presently unable to pay in full. (e) That the residential and small nonresidential customer may have the right to enter into a settlement agreement with the utility if the claim is for an amount that is in dispute. (f) That the customer has the right to file a complaint disputing the claim of the utility before the proposed date of the shut off of service. (g) That the customer has the right to request a hearing before a hearing officer if the customer disputes the reasonableness of the payment plan or settlement agreement offered by the utility or if the complaint cannot be otherwise resolved and that the customer must pay to the utility that portion of the bill that is not in dispute within 10 business days of the date that the customer requests a hearing. (h) That the customer has the right to represent himself or herself, to be represented by counsel, or to be assisted by other persons of his or her choice in the complaint process. (i) That the utility will not shut off service pending the resolution of a complaint that is filed with the utility or the commission pursuant to these rules. (j) The telephone number and address of the utility where the customer may make inquiry, enter into a payment plan or settlement agreement, or file a complaint. (k) That the utility may require a deposit and restoration charge if the utility shuts off service for nonpayment of a delinquent account or for unauthorized use of utility service. (2) For residential customers a notice of shut off of service shall also contain all of the following information: (a) A combination utility shall include all of the following information on disconnection notices for eligible low-income customers whose natural gas and electric services are combined: (i) The amounts for both natural gas and electric service, listed separately. (ii) That the customer has the option of choosing 1 of his or her services to retain with the appropriate payment. (iii) That the customer may have the option to enter into a payment plan for both natural gas and electric service, or to retain either natural gas or electric service as chosen by the customer. (b) That the customer should contact a social services agency immediately if the customer believes he or she might be eligible for an energy assistance program or other emergency economic assistance and should inform the utility of any efforts being made to obtain payment assistance. (c) That customers who believe they may be eligible for assistance from an energy assistance program should determine if assistance is available before enrolling in a payment plan because many agencies may not provide assistance if shut off is avoided by signing a settlement agreement. (d) That during the heating season the utility will postpone shut off of service if a customer is an eligible low-income customer that enters into a winter protection payment plan with the utility and the customer provides documentation that the customer is actively seeking emergency assistance from an energy assistance program. (e) The energy assistance telephone line number at the department of health and human services or an operating 2-1-1 system telephone number. (f) That the utility will postpone the shut off of service if a certified medical emergency exists at the customer's residence and the customer informs and provides documentation to the utility of that medical emergency. (g) That the customer should contact the utility for information about a shutoff protection program.

R 460.141 Time of shut off. Rule 41. (1) Subject to the requirements of these rules, a utility may shut off service to a customer on the date specified in the notice of shut off or at a reasonable time following that date. If a utility does not

28 2017 MR 22 – December 15, 2017 shut off service and mails a subsequent notice, then the utility shall not shut off service before the date specified in the subsequent notice. Shut off shall occur only between the hours of 8:00 a.m. and 4:00 p.m. (2) A utility shall not shut off service on a day, or a day immediately preceding a day, when the services of the utility are not available to the general public for the purpose of restoring service and shall not shut off service on a Friday during the heating season to a customer who has defaulted on a shutoff protection program under these rules.

R 460.142 Manner of shutoff. Rule 42. (1) Immediately preceding the shut off of service, an employee of the utility who is designated to perform that function may identify himself or herself to the customer or another responsible person at the premises and may announce the purpose of his or her presence. (2) The employee shall have in his or her possession a copy of the delinquent account of the customer and request any available verification that the outstanding claims have been satisfied or are currently in dispute. Unless the customer presents evidence that reasonably indicates that the claim has been satisfied or is currently in dispute, the employee may shut off service. (3) The employee may be authorized to accept payment and shall not shut off service if the customer offers payment in full, together with a commission-approved collection charge for sending the employee to the premises, if provided in the utility's schedule of rates and tariffs. (4) The customer may pay in any reasonable manner, including by personal check, credit card, or debit card. Payment by personal check, credit or debit card is not reasonable if the customer has paid with a personal check, credit card, or debit card within the last 12 months and at least 1 check has been returned for insufficient funds or no account, or at least 1 credit card or debit card payment has been denied excluding financial institution error. (5) After notice has been provided pursuant to R 460.139, and if the customer does not respond, the employee may shut off service. (6) When the utility employee shuts off service, the employee shall leave a notice in a conspicuous place upon the premises. For all forms printed after the effective date of these rules, the notice shall state that service has been shut off, the address and telephone number of the utility where the customer may arrange to have service restored, and that any efforts by the customer to restore his or her own service are unlawful and dangerous.

R 460.143 Manner of shut off for service provided with remote shut off and restoration capability. Rule 43. (1) For an involuntary shut off of service using meters with remote shut off and restoration capability, at least 1 day before shut off of service, the utility shall make at least 2 attempts to contact the customer by 1 of the methods listed in R 460.139(6). The notice shall conspicuously state that the disconnection of service will be done remotely and that a utility representative will not return to the premises before disconnection. (2) The utility shall document all attempts to contact the customer. (3) If the utility contacts the customer or other responsible adult in the customer's household or premises by telephone on the day service is to be shut off, the utility shall inform the customer or other responsible person that shutoff of service is imminent and the steps necessary to avoid shut off. Unless the customer presents evidence that reasonably demonstrates that the claim is satisfied or is in dispute, or the customer makes payment, the utility may shut off service. (4) If the utility complies with the notice requirements of this rule, no further customer contact is required on the day service is to be shut off and the utility may shut off service.

R 460.144 Restoration of service.

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Rule 44. (1) After a utility has shut off service, it shall restore service promptly upon the customer's request when the cause has been cured or credit arrangements satisfactory to the utility have been made. (2) When a utility is required to restore service at the customer's meter manually, the utility shall make every effort to restore service on the day the customer requests restoration. Except for reasons beyond its control, including excavation or reconnection at a pole, the utility shall restore service not later than the first working day after the customer's request. (3) For utilities using meter technology with remote shutoff and restoration capability, service shall be restored on the day the customer requests restoration, except in the case of documented equipment failure. (4) The utility may assess the customer a charge, including reasonable costs, for restoring service and relocating the customer's meter as specified in the utility's approved schedule of rates and tariffs. (5) In cases of unauthorized use, a utility may reestablish electric or natural gas service if the legal owner cannot provide documentation establishing the identity of the tenant responsible for the prior unauthorized use, proves that he or she is the legal owner of the property, and agrees to payment of the additional fees for reestablishing electric or natural gas service at the location as provided in section 9d(4) of 1939 PA 3, MCL 460.9d(4). (6) Nothing in these rules shall prohibit the prosecution of an individual or customer for unauthorized use, sale, or transfer of service as permitted by law.

PART 9. CUSTOMER RELATIONS AND UTILITY PROCEDURES

R 460.145 Applicability. Rule 45. The rules in this part apply to all customer inquiries, service requests, and complaints that are made to a utility regarding utility service and charges.

R 460.146 Payment plan procedures for residential and small nonresidential customers. Rule 46. (1) A utility shall establish a policy to allow a residential or small nonresidential customer the opportunity to enter into a minimum of 2 documented payment plans for an amount owed to the utility that is not in dispute, if a customer claims an inability to pay in full. (2) In negotiating a payment plan due to the customer's inability to pay an outstanding bill in full, the utility shall not require the residential or small nonresidential customer to pay more than a reasonable amount of the outstanding bill upon entering into the plan, and not more than reasonable installments until the remaining balance is paid. For purposes of determining reasonableness, the parties shall consider all of the following factors: (a) The size of the delinquent account. (b) The customer's ability to pay. (c) The time that the debt has been outstanding. (d) The reasons that the customer has not paid the bill. (e) The customer's payment history. (f) Any other relevant factors concerning the circumstances of the customer. (3) A utility is not required to enter into more than 2 payment plans with a residential or small nonresidential customer who defaulted on the terms and conditions of such payment plan within the last 12 months.

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(4) A utility shall document that a residential customer has been notified by telephone, other electronic media, or letter of all of the following: (a) If a customer is seeking payment assistance from a social service agency, agreeing to this payment plan may prevent the customer from getting emergency assistance. (b) That the customer needs to notify the utility if the customer is working with an agency. (c) That a customer should not agree to the payment plan if he or she is not satisfied with it. (d) If the customer has an unexpected loss or reduction of income after the payment plan is implemented, he or she may request a review and modification of the plan.

R 460.147 Personnel procedures. Rule 47. A utility shall establish personnel procedures that, at a minimum, ensure all of the following: (a) That qualified personnel are available and prepared at all times during normal business hours to receive and respond to all customer inquiries, service requests, and complaints. A utility shall make the necessary arrangements to ensure that customers who are unable to communicate in the English language receive prompt and effective assistance. (b) That qualified personnel who are responsible for, and authorized to enter into, payment plans or settlement agreements on behalf of the utility are available at all times during normal business hours to respond to customer inquiries and complaints. (c) That qualified personnel are available at all times to receive and respond to customer contacts regarding any shut off of service and emergency conditions that occur within the utility's service area. (d) That the names, business addresses, and telephone numbers of personnel who are designated and authorized to receive and respond to the requests and directives of the commission regarding customer inquiries, service requests, and complaints during business hours are current and on file with the commission. The utility shall also provide a contact for emergency situations that may arise after business hours. (e) That upon request, the utility representative reading the meter shall provide the customer or other household member with appropriate picture identification confirming the representative's employment with the company. (f) That employees are informed of their responsibility to protect customers' information and data.

R 460.148 Publication of procedures for residential and small nonresidential customers. Rule 48. (1) A utility shall prepare a publication that summarizes, in easily understood terms, the rights and responsibilities of its residential and small nonresidential customers pursuant to these rules and other applicable provisions of statutes, rules, and tariffs. (2) A utility shall display the publication prominently at all utility office locations open to the general public and make it available to residential and small nonresidential customers. A utility shall also make the information available on its website. A utility shall transmit the publication to each new residential and small nonresidential customer via the customer's preferred method upon the commencement of service and shall provide it at all times upon request. When substantial revisions to or new information required by the provisions of subrule (3) of this rule occur, the utility shall provide the changes to all current residential and small nonresidential customers by a bill insert, revised publication, or a periodical that is sent to all current residential and small nonresidential customers of the utility and to the commission. The form of this transmittal shall be at the discretion of the utility. (3) The publication shall contain all of the following information: (a) Billing procedures and estimation standards. (b) Methods for customers to verify billing accuracy and procedures to correct or change the customer's personal information associated with their account.

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(c) Instructions on accessing customer data electronically and the information or data available through such access. (d) An explanation of the power supply cost recovery or gas cost recovery procedures. (e) Customer payment standards and procedures. (f) Security deposit and guarantee standards. (g) Shutoff and restoration of service procedures. (h) Inquiry, service, and complaint procedures. (i) Procedures for terminating service. (j) Instructions on accessing the utility's data privacy tariff. (4) Each publication shall indicate conspicuously that the publication is provided pursuant to the rules of the commission.

R 460.149 Access to rules and rates. Rule 49. (1) A utility, except for a rural electric cooperative, shall provide to each customer, within 60 days of commencing service, within 60 days after issuance of a new rate case order, and at least once each year, all of the following information with a copy to the commission: (a) A clear and concise explanation of all rates for which the customer may be eligible. (b) A notice that complete rate schedules are available upon request. (c) A notice of the availability of company assistance in determining the most appropriate rate if the customer is eligible to receive service under more than 1 rate. (2) A rural electric cooperative shall provide to each customer, at least annually, all of the following information: (a) A notice that complete rate schedules are available upon request. (b) A notice that a clear and concise explanation of all rates for which the customer may be eligible is available upon request. (c) A notice of the availability of company assistance in determining the most appropriate rate if the customer is eligible to receive service under more than 1 rate. (3) A utility, except for a rural electric cooperative, shall provide to each customer, within 60 days after the utility has filed a general rate case application with the commission, all of the following information: (a) A notice that the utility has requested that the commission change its rates. (b) A notice that copies of the utility's application are available for inspection at all offices of the utility and on the utility’s website. (c) A notice that an explanation of the proposed changes to the utility's rates is available from the utility upon request. (4) A rural electric cooperative shall provide to each customer, within a reasonable time after it has filed a general rate case application or a times interest earned ratio ratemaking application, all of the following information: (a) A notice that the cooperative has requested that the commission change its rates. (b) A notice that copies of the cooperative's application are available for inspection at all offices of the cooperative. (c) A notice that an explanation of the proposed changes to the cooperative's rates is available from the cooperative upon request. (5) A utility, including a rural electric cooperative, shall provide the notice required by this rule either through a publication that is transmitted to each of its customers by a bill insert, or whatever transmission method is used to provide the customer's bill and on its website.

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(6) Upon request, a utility shall assist the customer in selecting the most economical rate schedule based on information supplied by the customer; however, selection of the appropriate rate is the responsibility of the customer. Once the selection is made, the customer shall stay on that rate not less than 12 months unless the customer notifies the utility of permanent changes in the conditions of service that warrant a different rate schedule. (7) A utility shall keep on file, at all offices of the utility, and shall provide public access to, all of the following documents: (a) A copy of these rules. (b) A copy of all other rules of the utility filed with the commission regarding customer service. (c) Schedules of all residential rates and charges. (d) Proposed rate schedules. (e) Clear and concise explanations of both existing and proposed rate schedules. (f) An explanation of its power supply cost recovery or gas cost recovery process. (8) A utility shall post suitable signs in conspicuous locations at all bill payment offices that are operated by the utility or authorized agents calling attention to the fact that the rules, regulations, rate schedules, proposed rate schedules, explanations of rate schedules, and explanations of proposed rate schedules are on file and available for inspection. Upon request, a utility shall provide a copy of these rules, explanations, or schedules to a customer without charge.

R 460.150 Complaint procedures. Rule 50. (1) A utility shall establish complaint procedures, promptly and thoroughly investigate customer complaints, and, when possible, resolve all customer inquiries, service requests, and complaints and report the resolution of commission-referred complaints to the commission staff. (2) The utility shall keep records of customer complaints that will enable the utility to review and analyze its procedures and actions. The records shall be available to the commission. (3) After referral of a customer's complaint from the commission, a utility shall make reasonable attempts to contact the customer within 2 business days and shall develop and report to the commission within 10 days after referral its plan for resolution of the complaint. (4) A utility shall provide to customers who are not satisfied with the utility's resolution of a complaint or inquiry the toll-free telephone number and internet address of the commission. (5) A utility shall obtain commission approval of any substantive changes in its procedures.

R 460.151 Reporting requirements. Rule 51. A utility shall file with the commission quarterly reports that disclose all of the following: (a) The payment performance of its customers in relation to established due and payable periods. (b) The number and general description of all complaints registered with the utility. (c) The number of shut off notices issued by the utility and the reasons for the notices. (d) The number of hearings held by the utility, the types of disputes involved, and the number of complaint determinations issued. (e) The number of written settlement agreements entered into by the utility. (f) The number of shut offs of service and the number of reconnections. (g) Any other customer service quality information requested by the commission staff.

R 460.152 Inspection. Rule 52. A utility shall permit authorized staff of the commission to inspect all of the utility's operations that relate to customer service.

R 460.153 Customer access to consumption data and confidentiality.

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Rule 53. (1) A utility shall provide to each customer, upon request, a clear and concise statement of the customer's actual energy usage, or weather adjusted consumption data for each billing period during the last 12 months, or both. A utility shall notify its customers at least once each year by whatever method is used to transmit the customers' bills, that a customer may request energy usage, or weather- adjusted consumption data, or both. (2) Each electric and natural gas utility shall file with the commission, for the commission’s approval, a customer data privacy tariff that contains a customer data privacy policy. The privacy policy shall do all of the following: (a) Encompass all customer information or data collected or maintained by the utility. (b) Clearly define customer information or data that the utility collects or maintains. (c) Protect all customer information or data collected for the utility from unauthorized use or disclosure by the utility, its affiliates, or contractors. (d) Ensure that, for secondary purposes, customer usage data, personally identifiable information, and certain other customer information are only disclosed to third parties with the customer's written consent. (e) Specify that customer information may be disclosed without consent in response to a warrant or court order, as required for collection activities, or as necessary for primary purposes. (f) Permit a customer to share his or her information with a third party that is not affiliated with the utility. The utility may elect to insert language in the privacy policy stating that the utility is not responsible, in this circumstance, for a third party's unauthorized disclosure or use of this information. (g) Provide clear instructions regarding the method by which a customer and a third party, authorized by the customer, may obtain customer usage data in a timely manner and a readily accessible format from the utility. (h) Indicate that the policy does not apply to aggregate data, containing general characteristics of a customer group, which is used for analysis, reporting, or program design purposes. (3) The privacy policy shall be posted on the utility's website.

PART 10. DISPUTES, HEARINGS AND SETTLEMENTS

R 460.154 Disputed matters. Rule 54. (1) If a customer advises a utility, or if the utility is notified by a regulation officer on behalf of a customer, before the date of the proposed shut off of service, that all or part of a bill is in dispute, then the utility shall do all of the following: (a) Immediately record the date, time, and place the customer made the complaint and transmit verification to the customer. (b) Investigate the dispute promptly and completely. (c) Advise the customer of the results of the investigation. (d) Attempt to resolve the dispute informally in a manner that is satisfactory to both parties. (e) Provide the opportunity for the customer to settle the disputed claim or to satisfy any liability that is not in dispute. (2) A customer may advise a utility that a matter is in dispute in any reasonable manner, such as by written notice, in person, by a telephone call directed to the utility, or through a regulation officer. (3) A utility, in attempting to resolve the dispute, may employ telephone communication, personal meetings, on-site visits, or any other method that is reasonably conducive to obtaining a settlement. (4) If the utility has resolved the matter in dispute but the customer remains dissatisfied, the utility shall inform the residential or small nonresidential customer of the right to request a customer hearing and the procedure for requesting the hearing. The utility shall also inform the customer that they contact

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the commission to file a complaint. Unless the customer takes action by either requesting a customer hearing or taking its dispute to the commission, the matter in dispute shall be considered closed.

R 460.155 Customer hearing and hearing officers for residential and small nonresidential customers. Rule 55. (1) If the parties are unable to resolve the dispute, the utility shall offer the customer the opportunity for a customer hearing before a hearing officer selected from a list of hearing officers filed with the commission. (2) If the customer requests a customer hearing with the utility or with the commission regulation officer, the utility shall place a hold on any action to shut off or suspend service until 1 of the following occurs: (a) The customer fails to complete his or her responsibilities required for a customer hearing. (b) The customer withdraws the request. (c) The utility and the customer settle the dispute. (d) The customer hearing officer issues a decision finding that shut off or suspension of service is appropriate. (3) The utility shall accept notification from a regulation officer of a customer's request for a customer hearing. (4) If the parties are unable to resolve the dispute, the utility shall offer the customer the opportunity for an informal hearing before a hearing officer selected from a list of hearing officers filed with the commission. (5) If the customer chooses to have a customer hearing, the customer shall do both of the following: (a) Notify the utility within 5 business days of the utility’s offer for a hearing. (b) Pay the amount not in dispute, or if the utility and customer cannot agree, pay 50% of the disputed amount not to exceed $100.00. (6) If the customer notifies the utility of the intent to pursue an informal hearing, then the utility shall do all of the following: (a) Complete the necessary investigation. (b) Schedule the hearing within 10 business days of the customer's request for a hearing. (c) Hold the hearing within 45 business days of the customer's request for a hearing. (7) If the customer fails to pay the part of the bill that is determined under subrule (5)(b) of this rule within 15 business days of the date that the utility sends the hearing notice, the utility may exercise its right to shut off service pursuant to these rules. (8) A utility shall select hearing officers who meet all of the following requirements: (a) They are on the list of hearing officers on file with the commission. (b) They are notaries public who are qualified to administer oaths. (c) They are not a past or present employee of the utility, and they are not engaged in or have not been engaged in any other activities that would cause bias or lack of objectivity. (d) They comply with part 10 of these rules, R 460.154 to R 460.159. (9) In January of each year, utilities shall provide to the commission's executive secretary the name or names of selected hearing officers and update those lists as necessary. Upon notice to the commission, a hearing officer, other than those on the list, may be used subject to the requirements specified in subrule (8) of this rule. Upon request, utilities shall provide the resume of a hearing officer to the commission or any party participating in a customer hearing. (10) If the dispute is ultimately resolved, in whole or in part, in favor of the customer, the utility shall return promptly any excess amount paid by the customer, with interest at the rate specified pursuant to R 460.111(8).

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R 460.156 Notice of hearing. Rule 56. (1) On the day a utility schedules the hearing, the utility shall send or personally serve the customer with written notice of the time, date, and place of the hearing. (2) The notice shall describe the hearing procedures as specified in R 460.157. (3) The notice shall specify the amount of required payment and the due date, which shall be 10 business days from the date the notice was sent to the customer.

R 460.157 Customer hearing procedures. Rule 57. (1) A utility shall establish hearing procedures that ensure the impartiality and integrity of the hearing process and that provide the customer and the utility with all of the following rights: (a) The right to represent themselves, to be represented by counsel, or to be assisted by persons of their choice. (b) The right to examine, not less than 2 business days before the scheduled hearing, a list of all witnesses who will testify and all documents, records, files, account data, and similar material that may be relevant to the issues to be raised at the hearing. (c) The right to present evidence, testimony, and oral and written arguments. (d) The right to question witnesses who will be appearing on behalf of the other party. (2) A hearing shall be held during normal business hours, except as otherwise agreed to by all parties. A utility shall take reasonable steps to ensure that a customer who is unable to attend the hearing due to physical incapacity is not denied the right to a hearing. Failure of the customer, or the utility, to attend the hearing without a good reason, or without having requested an adjournment, constitutes a waiver of the right of that party to the hearing. (3) For the convenience of the parties, a hearing officer may conduct the hearing by telephone or other electronic media. In this case, all parties shall provide any documents to be introduced at the hearing to the other parties and the hearing officer at least 2 business days in advance of the hearing date. (4) The utility has the burden of proof by a preponderance of the evidence. (5) All witnesses who appear for either party shall testify under oath. (6) A hearing shall be informal and the proceedings do not have to be recorded or transcribed. All relevant evidence shall be received and the formal rules of evidence shall not apply. (7) For each hearing, the hearing officer shall compile a hearing record that includes all of the following: (a) A concise statement, in writing, of the position of the utility. (b) A concise statement, in writing, of the position of the customer. If the customer has not put his or her position in writing, then the hearing process shall provide a method for accomplishing this writing with the opportunity for proper acknowledgment by the customer. (c) Copies of all evidence submitted by the parties. (8) At the conclusion of the hearing, the hearing officer may orally state his or her findings and the decision; or, may adjourn the hearing and inform the parties that the decision will be transmitted to them within 10 business days. At the request of the customer, the hearing officer shall adjourn the hearing and transmit the decision to the parties within 10 business days of the conclusion of the hearing. In either case, the hearing officer shall issue a complaint determination in a form that is approved by the commission. The complaint determination shall contain both of the following: (a) A concise summary of the evidence and arguments presented by the parties. (b) The decision, and the reasons for the decision, based solely on the evidence received. (9) At the conclusion of the hearing and again upon issuance of the complaint determination, the hearing officer shall advise the customer and the utility of all of the following:

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(a) That each party has a right to appeal the decision to the commission staff, by mail, telephone, internet, fax, or in person, within 15 business days of issuance of the complaint determination. (b) That, if appealed, the decision of the hearing officer, including a finding that service may be shut off, cannot be implemented until the commission staff completes a review. (c) The address and telephone number where the customer or the utility may make an informal appeal to the commission staff. (10) Before issuance of a complaint determination, the hearing officer may propose a settlement to the parties. If both parties accept the settlement, it shall be put in writing and both parties shall sign the settlement agreement. (11) Within 10 business days of the conclusion of the hearing, the hearing officer shall serve the parties with all of the following: (a) A copy of the complaint determination. (b) Appeal information as provided in subrule (9) of this rule. (c) If applicable, a copy of the signed settlement agreement as provided in subrule (10) of this rule. (12) The complaint determination and a copy of the signed settlement agreement, if any, shall be made part of the hearing record. The hearing officer shall certify the hearing record. (13) The complaint determination is binding upon the parties, unless appealed, as provided in R 460.160 to R 460.169. (14) A utility's hearing procedures shall be subject to investigation and review by the commission.

R 460.158 Settlement agreement procedures for residential and small nonresidential customers. Rule 58. (1) If the utility and the residential or small nonresidential customer arrive at a mutually satisfactory settlement of a matter in dispute, then the utility may offer the residential or small nonresidential customer the opportunity to enter into a settlement agreement, and the customer shall provide written documentation of approval. (2) The utility shall confirm the terms of the settlement agreement with the residential or small nonresidential customer and shall provide documentation of the settlement to the customer or the customer's authorized representative. The utility shall retain documentation of the original settlement agreement for the term of the settlement agreement or 2 years, whichever is longer. In case of a dispute over the terms of a settlement agreement, the utility shall have the burden of proving that the residential or small nonresidential customer understood and accepted the terms of the settlement agreement. (3) Services shall not be shut off if the residential or small nonresidential customer follows the terms of the settlement agreement. (4) A settlement agreement that is offered by a utility shall state, immediately preceding the space provided for the residential or small nonresidential customer's signature and in bold print that is not less than 2 sizes larger than any other print that is used on the form: "IF YOU ARE NOT SATISFIED WITH THIS AGREEMENT, DO NOT SIGN. YOU MAY FILE A CUSTOMER COMPLAINT AND HAVE A HEARING BEFORE A HEARING OFFICER BEFORE YOUR SERVICE MAY BE SHUT OFF. IF YOU SIGN THIS AGREEMENT, YOU GIVE UP YOUR RIGHT TO A CUSTOMER HEARING BEFORE A HEARING OFFICER ON ANY MATTER INVOLVED IN THIS DISPUTE, EXCEPT THE UTILITY'S FAILURE OR REFUSAL TO FOLLOW THE TERMS OF THIS AGREEMENT."

R 460.159 Default of settlement agreement procedures for residential and small nonresidential customers. Rule 59. (1) If a residential or small nonresidential customer fails to comply with the terms and conditions of a settlement agreement, the utility may shut off service after notifying the customer in writing, by personal service, or first-class mail of the following information:

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(a) That the residential or small nonresidential customer is in default of the settlement agreement. (b) The nature of the default. (c) That unless the residential or small nonresidential customer pays in full the amount due within 10 business days of the date of mailing, the utility may shut off service. (d) The date the utility may shut off service. (e) That the residential or small nonresidential customer has a right to do either of the following: (i) Request a hearing before a hearing officer selected from a list on file with the commission, but only if the customer alleges that the utility has failed or refused to follow the terms of the settlement agreement. (ii) File a formal hearing request pursuant to the commission's rules of practice and procedure in R 792.10101 to R 792.11903. (f) The address and telephone number where the residential or small nonresidential customer may file the request for a hearing with the utility or the commission. (2) If the residential or small nonresidential customer and the utility reach a settlement agreement following a notice of shutoff, the failure of the residential or small nonresidential customer to abide by the terms of the settlement agreement during the first 60 days of the agreement constitutes a waiver of the notice required by subrule (1) of this rule. The utility may shut off service after notice as described in R 460.137.

PART 11. APPEAL PROCEDURES

R 460.160 Customer hearing appeal. Rule 60. Within 15 business days after a hearing officer issues a written complaint determination, either party may make an informal appeal to the commission staff.

R 460.161 Filing procedures. Rule 61. (1) A party may make a customer hearing appeal which does not have to be in writing but may be initiated by telephone, internet, mail, fax, or in person at the offices of the commission. (2) The appealing party shall provide all of the following information: (a) Name and address of the customer. (b) Name of the utility involved. (c) The nature of the original complaint in a clear and concise manner. (d) The hearing officer's decision. (e) The relief requested.

R 460.162 Customer hearing appeal procedures. Rule 62. (1) The commission staff shall assign the customer hearing appeal to a regulation officer who shall do all of the following: (a) Advise the appealing party by telephone or in writing of the procedures of the commission. (b) Advise the other party that a customer hearing appeal has been filed. (c) Issue interim determinations as necessary and as provided in R 460.163. (d) Review or investigate the appeal. (e) Issue a customer hearing appeal decision. (2) Upon notification by the commission staff that a customer hearing appeal has been made, the utility shall promptly file with the commission staff, the certified hearing record. The parties shall be bound by the evidence presented at the hearing and contained in the hearing record. In arriving at the

38 2017 MR 22 – December 15, 2017 customer hearing appeal decision, the regulation officer shall not be required to receive or consider any additional evidence or information. (3) In all customer hearing appeals, the utility has the burden of proof by a preponderance of the evidence.

R 460.163 Interim determination. Rule 63. (1) After receiving the hearing record and pending the final resolution of a customer hearing appeal, the regulation officer may issue an interim determination with appropriate terms and conditions. In the case of an appeal regarding a bill or deposit, the regulation officer may require a customer to pay the undisputed portion of a claim in order to continue the prohibition against the shut off of service. The regulation officer may consider the amounts that reasonably appear to reflect the cost of utility service in determining the undisputed portion of a claim. (2) If a customer fails to abide by the terms and conditions of an interim determination within 10 days of the date of personal service or mailing of the interim determination by first-class mail, then the utility may shut off service as provided in R 460.137.

R 460.164 Appeal review. Rule 64. The regulation officer shall thoroughly review the customer hearing appeal and, when necessary, conduct further investigation. A party may offer new evidence if the regulation officer determines that it is relevant. When further investigation is necessary, the regulation officer may request additional evidence or, at his or her own initiative, may hold a customer hearing appeal conference with the parties or their representatives at a time and place designated by the officer. If either party fails to appear at the conference without a good reason or without having requested an adjournment, the right of the absent party to appear at the conference shall be waived. At the customer hearing appeal conference, the parties may do any of the following: (a) Represent themselves, be represented by counsel, or be assisted by other persons of their choice. (b) Offer oral and documentary evidence, which may be considered at the discretion of the regulation officer. (c) Refute, in a reasonable manner, the evidence of the other party. (d) Submit an oral or written statement of position.

R 460.165 Customer hearing appeal decision. Rule 65. The regulation officer shall, within 30 days after the utility files the certified record, issue a written customer hearing appeal decision affirming, modifying, or reversing the customer hearing determination. In reversing or modifying the customer hearing determination, the decision shall set forth the terms and conditions for continued service, shut off, or a proposed settlement agreement as required by the facts and circumstances. The decision shall state the relevant findings of fact, the reasons for the decision, and remedies for failure to comply with the customer hearing appeal decision. A copy of the customer hearing appeal decision shall be served personally, or by first-class mail, on the parties.

R 460.166 Failure to comply with customer hearing appeal decision. Rule 66. Failure of either party to comply with the decision within 10 days after the date that decision was served by mail shall permit implementation of the action or remedy provided by the decision.

R 460.167 Same dispute. Rule 67. The commission staff may dismiss a subsequent informal appeal that involves the same question or issue based upon the same facts without following every procedure set forth in these rules.

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R 460.168 Formal appeal. Rule 68. Either party may appeal before the commission the decision of the regulation officer by filing a formal hearing request pursuant to the rules of practice and procedure before the commission in R 792.10101 to R 792.11903. If a formal hearing request is filed, the terms of the customer hearing appeal decision shall be held in abeyance unless otherwise ordered by the commission or the presiding officer who is assigned to the formal complaint.

R 460.169 Other remedies. Rule 69. Nothing in these rules shall be construed to prevent a party at any time from pursuing appropriate legal and equitable remedies.

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ADMINISTRATIVE RULES

DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

PUBLIC SERVICE COMMISSION

ELECTRICAL SUPPLY AND COMMUNICATION LINES AND ASSOCIATED EQUIPMENT

Filed with the Secretary of State on December 4, 2017

These rules become effective immediately upon filing with the Secretary of State unless adopted under section 33, 44, or 45a(6) of 1969 PA 306. Rules adopted under these sections become effective 7 days after filing with the Secretary of State.

(By authority conferred on the public service commission by section 7 of 1909 PA 106, sections 4 and 6 of 1939 PA 3, and section 5 of 1939 PA 419, MCL 460.557, 460.4, 460.6, and 460.55)

R 460.813 Standards of good practice; adoption by reference. Rule 3. Parts 1, 2, and 3 and sections 1, 2, 3, and 9 of the national electrical safety code, 2017 edition (ANSI-C2-2017), are adopted by reference in these rules as standards of accepted good practice. Parts 1, 2, and 3 and sections 1, 2, 3, and 9 of the national electrical safety code, 2017 edition (ANSI-C2- 2017), are available from the Institute of Electrical and Electronics Engineers (IEEE) via the internet at the following web site: http://www.techstreet.com/standards/ieee-c2-2017?product_id=1914980 at a cost of $190.00 for a pdf download, $210.00 for a print copy, or $285.00 for both as of the time of adoption of this rule, plus any applicable handling charge. Copies of the code may also be obtained from the Michigan Public Service Commission, 7109 W. Saginaw, P.O. Box 30221, Lansing, MI 48909 at the same cost charged by the IEEE as of the adoption of this rule, plus $20 for shipping and handling.

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PROPOSED ADMINISTRATIVE RULES, NOTICES OF PUBLIC HEARINGS

MCL 24.242(3) states in part:

“… the agency shall submit a copy of the notice of public hearing to the Office of Regulatory Reform for publication in the Michigan register. An agency's notice shall be published in the Michigan register before the public hearing and the agency shall file a copy of the notice of public hearing with the Office of Regulatory Reform.”

MCL 24.208 states in part:

“Sec. 8. (1) The Office of Regulatory Reform shall publish the Michigan register at least once each month. The Michigan register shall contain all of the following:

* * *

(d) Proposed administrative rules.

(e) Notices of public hearings on proposed administrative rules.”

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PROPOSED ADMINISTRATIVE RULES

DEPARTMENT OF NATURAL RESOURCES PARKS AND RECREATION DIVISION PURE MICHIGAN TRAIL, WATER TRAIL, AND TRAIL TOWN DESIGNATION Filed with the Secretary of State on

These rules become effective immediately upon filing with the Secretary of State unless adopted under section 33, 44, 45a(6), or 48 of 1969 PA 306. Rules adopted under these sections become effective 7 days after filing with the Secretary of State. (By authority conferred on the director of the department of natural resources by section 72112 of 2014 PA 210, MCL 324.72112) R 324.1401, R 324.1402, R 324.1403, R 324.1404, R 324.1405, R 324.1406, R 324.1407 of the Michigan Administrative Code are added, as follows:

R 324.1401 Definitions. Rule 1. (1) As used in these rules: (a) “Access site” means public or private land where it is legal for the public to access, launch, and land a boat into and from its adjoining waters. An access site has at least some legal parking along a public roadway. Access sites may be rest areas and may include amenities. (b) “Act” means Part 721 of 1994 PA 451, MCL 324.72101 to 324.72118. (c) “Easily accessible” means within 2 miles of the trail unless otherwise designated in these rules. (d) “Formally adopted” means adopted by resolution of the governing body overseeing the trail or the city, village, or township seeking a Pure Michigan designation. (e) “Lodging” means a place to sleep, including but not limited to, a designated campsite, hut, shelter, or other licensed overnight accommodation. (f) “Rest areas” means places where it is permissible to leave the water and may have amenities such as restrooms, trash receptacles, and picnic tables. Rest areas may be access points. (g) “Staging area” means public or private land where it is legal for the public to assemble and access a right-of-way adapted to foot, horseback, motorized, or other nonmotorized travel and provides some legal parking along a public roadway. (h) “Trailhead” means public or private land where it is legal for the public to access a right-of- way adapted to foot, horseback, motorized, or other nonmotorized travel and provides some legal parking along a public roadway. (2) A term defined in Act has the same meaning when used in these rules.

R 324.1402 Nomination process. Rule 2. (1) To nominate a trail, water trail, or trail town for a Pure Michigan designation, an individual, local unit of government, authority, or non-profit shall complete an electronic form available on the department’s website and include all of the following: (a) A description of how the nominated trail, water trail, or trail town meets the requirements identified in section 72103 or 72104 of the Act and these rules. (b) A description of the natural resources, cultural resources, historic resources, attractions to non-resident users, or any other factors that make the trail, water trail, or trail town an iconic example of its type.

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(c) A description of whether the trail, water trail, or trail town meets standards determined and approved by the department. (d) For a trail town nomination, evidence of sufficient funds to erect and maintain an official Pure Michigan Trail Town sign and logo. (e) If the nominated trail has not been completed, evidence of sufficient funds and governmental support to complete the trail within 1 year after receiving a Pure Michigan Trail designation. (2) The department shall review the nomination. If the nomination meets the criteria identified in section 72103 or 72104 of the Act and these rules, the department shall forward the nomination to the Michigan Economic Development Corporation for a Pure Michigan license. (3) Upon receipt of a Pure Michigan license, the department shall proceed with the process as provided in the Act.

R 324.1403 Requirements for designation; trail; water trail. Rule 3. (1) The department shall consider a trail or water trail for a Pure Michigan designation if the trail or water trail meets the requirements established in section 72103 of the Act, and the following requirements: (a) The trail or water trail is open for use by the public and publicly available access sites, staging areas, trailheads, and rest areas are appropriately spaced for the type of trail. (b) The trail or water trail is identified on a website with a map that can be printed and is appropriately signed to make the user aware of all of the following: (i) The location and length of the trail or water trail. (ii) Hazards and level of difficulty of the trail or water trail. (iii) Amenities related to the trail or water trail, including easily accessible access sites, staging areas, trailheads, rest areas, lodging, eating facilities, and other recreational opportunities. (c) The trail or water trail is appropriately signed, including pictures as appropriate, to do all of the following: (i) Make users aware of their location on the trail or water trail. (ii) Make users aware of easily accessible access sites, staging areas, trailheads, rest areas, trail amenities, lodging facilities, and eating facilities as well as hazards, towns, and emergency contacts. (iii) Encourage safety and respect for the environment. (d) Unless the trail or water trail is primarily a looped trail or water trail or otherwise intended for the user to return to his or her vehicle in 1 day or less, lodging facilities appropriate to the type of trail or water trail users are available for at least the following: (i) Every 12 miles for trails primarily used by walkers. (ii) Every 12 miles for trails located upon water. (iii) Every 15 miles for trails primarily used by cross country skiers. (iv) Every 40 miles for trails primarily used by bikers. (v) Every 40 miles for trails primarily used by equestrians. (vi) Every 100 miles for trails primarily used by snowmobile or ORV riders. (e) The trail or water trail is designed so that increased use of the trail or water trail will not degrade the local experience, cultural resources, or the environment. Applicants shall identify the designs applied to ensure sustainability of the trail or water trail. (f) At a minimum, for a water trail, the water body shall meet water quality use designations for Partial Body Contact standards, as established by Michigan department of environmental quality, in addition to the requirements established by section 72103(3)(c) of the Act. (g) The trail or water trail has a formally adopted plan that does the following:

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(i) Identifies the existing and planned amenities associated with the trail or water trail and how those amenities will be maintained and enhanced. (ii) Establishes a schedule for the maintenance of the trail or water trail that identifies funding sources and the party or parties responsible for maintaining the trail or water trail and discouraging vandalism. (iii) Includes programming and educational activity associated with the trail or water trail that allow or increase enjoyment of the trail or water trail, understanding of the natural, cultural, and historic resources related to the trail or water trail, boating skills, outdoor ethics and, for a water trail, efforts to improve the quality of the waterway and its water. (iv) Identifies a mechanism to evaluate the economic impact of the trail or water trail at least every 5 years that includes an understanding of users and where they live, impact on area businesses, and money spent in conjunction with trail or water trail use. (v) Includes a marketing plan for the trail or water trail. (h) The trail or water trail has a resolution of support of the designation of the trail or water trail as a Pure Michigan Trail or Water Trail by the local unit of government, authority, or non- profit that is primarily responsible for the trail or water trail. (i) The trail or water trail is supported, managed, and maintained by 1 or more organizations. If the trail or water trail is supported, managed, and maintained by more than 1 organization, the organizations shall enter into a written agreement with each other. The organizations shall be broadly representative of the community, including recreation, education, conservation, heritage, business, public safety, health, and government organizations and shall obtain permission from all persons or entities that have an ownership interest over any portion of the trail or water trail. (j) The trail or water trail is part of the statewide trail network. (2) The department may consult with the Michigan economic development corporation when considering a trail or water trail nomination for a Pure Michigan designation.

R 324.1404 Requirements for designation; trail town. Rule 4. To be considered for a Pure Michigan Trail Town designation, a city, village, or township shall meet the requirements established in section 72104 of the Act and the following requirements: (a) The city, village, or township has a formally adopted plan for marketing the trail or water trail and evidence of implementation of that plan. The plan may be part of a trail or water trail marketing effort that includes this state, other trail towns, or other trail marketing efforts. (b) The city, village, or township has a plan to evaluate the economic impact of a Pure Michigan Trail Town designation every 5 years.

R 324.1405 Application review; notification; designation. Rule 5. The department shall review applications for a Pure Michigan designation for consistency with the requirements established in the Act and these rules, and notify the petitioner whether the director approved the Pure Michigan designation. The department shall keep a list of the active Pure Michigan Trails, Water Trails, and Trail Towns on its website.

R 324.1406 Generally accepted trail standards. Rule 6. The generally accepted trail standards shall be determined and approved by the department.

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R 324.1407 Expiration, re-designation, and revocation. Rule. 7. (1) A Pure Michigan Trail, Water Trail, or Trail Town designation shall expire every 5 years. (2) Unless re-designated, all trademarked Pure Michigan materials shall be removed by the governing body overseeing the trail, water trail, or the city, village, or township within 60 days of expiration of the Pure Michigan designation. (3) A nominee may seek re-designation upon a form available on the department’s website. (4) Before approving a nominee’s re-designation, the department shall inspect the trail, water trail, or trail town and evaluate the success of the trail, water trail, or trail town and related marketing plans by reviewing the economic impact report. (5) If, after inspection and evaluation, the department determines that the trail, water trail, or trail town warrants re-designation based on continued compliance with these rules, the department shall recommend to the Michigan economic development corporation the licensing of the trail, water trail, or trail town with the Pure Michigan brand. (6) A Pure Michigan Trail, Water Trail, or Trail Town designation may be revoked by the director under the Act.

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NOTICE OF PUBLIC HEARING

NOTICE OF PUBLIC HEARING The Michigan Department of Natural Resources will hold public hearings to receive comments on proposed amendments to administrative rules, Pure Michigan Trail, Water Trail, and Trail Town Designation, promulgated under authority of section 72112 of 2014 PA 210, MCL 324.72112. Information about the proposed rules will be provided and a public hearing will be held at the following date, time, and location: Wednesday, December 20, 2017, 5:30 pm Demmer Shooting Sports and Education Center 4830 East Jolly Road Lansing, Michigan 48910

A copy of the proposed rules (ORR 2014-155 NR) is available on the Michigan Office of Regulatory Reinvention’s web site at http://www.michigan.gov/orr and by contacting Regulatory Affairs Officer, Legislative and Legal Affairs Office, Michigan Department of Natural Resources, P.O. Box 30028, Lansing, MI 48909, Telephone: 517-284-6029, FAX: 517-335-4242, or [email protected].

Notice of public hearing is given in accordance with Section 41 and 42 of Michigan’s Administrative Procedures Act, 1969 PA 306, [MCL 24.241 and 24.242]. These rules will become effective immediately upon filing with the Secretary of State.

All interested persons are invited to attend and present their views. Statements should be submitted in writing for the hearing record. For those unable to attend, written statements may also be submitted to: Regulatory Affairs Officer, Legislative and Legal Affairs Office, Michigan Department of Natural Resources, P.O. Box 30028, Lansing, MI 48909, or [email protected]. All statements must be received by 5:00 p.m., on January 10, 2018. Persons with disabilities requesting accommodations for effective participation in the meeting should call 517-284-6118, or email to [email protected], 7 days before the meeting date to request mobility, visual, hearing, or other assistance.

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PROPOSED ADMINISTRATIVE RULES

DEPARTMENT OF ENVIRONMENTAL QUALITY

REMEDIATION AND REDEVELOPMENT DIVISION

ENVIRONMENTAL CONTAMINATION RESPONSE ACTIVITY

Filed with the Secretary of State on

These rules will become effective 180 days after filing with the Secretary of State unless adopted under Section 33, 44, or 45a(6) of 1969 PA 306. Rules adopted under these subsections become effective 7 days after filing with the Secretary of State.

(By authority conferred on the director of the Department of Environmental Quality by sections 20104(1) and 20120a(1817) of 1994 PA 451, MCL 324.20104(1) and 324.20120a(1817).

R 299.1, R 299.2, R 299.3, R 299.4, R 299.6, R 299.8, R 299.9, R 299.10, R 299.18, R 299.20, R 299.22, R 299.26, R 299.30, R 299.34, R 299.36, R 299.38, R 299.46, R 299.49, and R 299.50 of the Michigan Administrative Code are amended, and R 299.7, R 299.16, and R 299.27 are added to the Code, and R 299.14, R 299.24, R 299.40, R 299.44, and R 299.48 of the Code are rescinded, as follows:

CLEANUP CRITERIA REQUIREMENTS FOR RESPONSE ACTIVITY

R 299.1 Definitions; A to I. Rule 1. As used in this partthese rules: (a) “Act” means the natural resources and environmental protection act, 1994 PA 451, MCL 324.101 to 324.90106, known as the Natural Resources and Environmental Protection Act. (b) “Acute toxicity” means the ability of a hazardous substance to cause a debilitating or injurious effect in an organism as a result of a single or short-term exposure. (c) “Additivity” means the combined effect of 2 or more hazardous substances estimated directly from the summing of effects, responses, or scaled exposure levels. (d) “Ambient air” means the atmosphere outside of buildings. (d) “Applicable criterion” means a cleanup criterion for a relevant pathway. A criterion is not an applicable criterion if the exposure pathway is not a relevant pathway at the facility or if the exposure it addresses is reliably restricted by a restrictive covenant or institutional control or other mechanism allowed for under part 201 of the act and these rules. (e) “Aquifer” means a geological formation, group of formations, or part of a formation capable of yielding a significant amount of groundwater to wells or springs. (f) “Best available information” means, when used in relation to a risk assessment or the development of cleanup criteria, the most scientifically credible and relevant data available about for a particular hazardous substance, exposure assumptions, or the methodology for characterizing dose-response or risk. Such information may include, but is not limited to, any of the following:

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(i) The peer reviewed scientific literature. (ii) Information sources recognized by the risk assessment community, such as the integrated risk information system databaseRisk assessment guidance and databases maintained by the United States eEnvironmental pProtection aAgency. or other scientifically reliable databases. (iii) Other peer reviewed risk assessment guidance, databases, and other information sources recognized by the risk assessment community as scientifically reliable. (iiiiv) Other scientific studies that are acceptable to the department. (g) “Cancer slope factor” means a plausible upper-bound estimate of the probability of a response per unit dose of a hazardous substance over a lifetime. The cancer slope factor is used to estimate an upper bound probability of an individual developing cancer as a result of a lifetime exposure to a particular level of a potential carcinogen. an upper bound, approximating a 95% confidence limit, on the increased cancer risk from a lifetime exposure to a hazardous substance. (h) “Carcinogen” means a hazardous substance which, based on the weight of evidence, causes an increased incidence of benign or malignant neoplasms in animals or humans or that substantially decreases the time in which neoplasms develop in animals or humans. (i) “Chronic toxicity” means the ability of a hazardous substance to cause an injurious or debilitatingadverse effect in an organism that results from repeated exposure to the hazardous substance for a time period representing a substantial portion of the natural life expectancy of the organism. that occurs as a result of repeated or long-term (chronic) exposure. (j) “Csat” means the concentration of a single hazardous substance in soil at which the solubility limits of the soil pore water, the vapor phase limits of the soil pore air, and the absorptive limits of the soil particles have been reached. As used in these rules, Csat is a theoretical threshold above which a free-phase liquid (non-aqueous phase liquid)NAPL hazardous substance may exist. (k) “Direct contact” means exposure to hazardous substances through ingestion or dermal contact. (l) “Facility-specific” means department-approved generic input values that when representative of conditions at the facility may be used as input for the calculated health-based values. The generic input values include the following: (i) Environmental conditions that allow the resulting criterion to represent unrestricted generic residential categorical criteria that do not depend upon any land use or resource use restriction to ensure protection pursuant to section 20120a(1)(a) of the act. (ii) Land use or building conditions that when used pursuant to R 299.27 allow the resulting volatilization to indoor air criteria to represent restricted categorical criteria pursuant to section 20120a(1)(b) to (d) of the act. (lm) “Generic residential” means the cleanup criteria established by the department under section 20120a(1)(a) of the act and these rules. (mn) “Groundwater” means water below the land surface in a zone of saturation. (no) “Increased cancer risk of 1 in 100,000” means the 95% upper bound on the calculated risk of 1 additional cancer above the background cancer rate per 100,000 individuals continuously exposed to a carcinogen at a given average daily dose for a 70-year lifetime. (op) “Inhalation unit risk factor” means the additional lifetime cancer risk occurring in a population in which all individuals are exposed continuously for life to a concentration of 1 microgram per cubic meter of the hazardous substance in the air they breathe. The inhalation unit risk factor shall be calculated under the provisions of part 55 of the act and the rules promulgated under that part. (p) “Initial threshold screening level” means a concentration in air of a toxic air contaminant which is used to evaluate noncarcinogenic health effects and is calculated under part 55 of the act and the rules promulgated under that part. (q) “Institutional control” means a measure which is approved by the department, which takes a form other than a restrictive covenant, and which limits or prohibits certain activities that may interfere with the integrity or effectiveness of a remedial action or result in exposure to hazardous substances at a

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facility, or which provides notice about the presence of a hazardous substance at a facility in concentrations that exceed only an aesthetic-based cleanup criterion. (rq) “Ionizing organic hazardous substance” means an organic hazardous substance that has functional chemical groups that become ions when exposed to varying pH conditions.

R 299.2 Definitions; L to V. Rule 2. As used in this partthese rules: (a) “Land or resource use restrictions” means the provisions of any of the following measures that are used to limit reduce or restrict exposure to hazardous substances, to eliminate an exposure pathway, to assure the effectiveness and integrity of containment or exposure barriers, to otherwise assure the effectiveness and integrity of response actions at a property prohibit activities that may interfere with the integrity or effectiveness of a response activity, or to limit or prohibit activities that may result in exposure to hazardous substances at a facility, or to provide notice about the presence of a hazardous substance at a facilityproperty in concentrations that exceed only an aesthetic- based cleanup criterion: (i) A restrictive covenant. (ii) A notice of approved environmental remediation. A conservation easement. (iii) A court order or judicially approved settlement. (iv) An institutional control, which may be a local ordinance or any form of preapproved institutional control, such as a notice of aesthetic impact.state law and regulation that limits or prohibits the use of contaminated groundwater, prohibits the raising of livestock, prohibits development in certain locations, or restricts property to certain uses, such as a zoning ordinance. (v) An alternate instrument approved by the department, which may be a license and license agreement, contract with local, state, or federal unit of government, health code or regulation, or government permitting requirement. (vi) Any form of land or resource use restriction preapproved by the department, such as a notice of aesthetic impact. (b) “Leachate” means liquid, including any suspended components in the liquid, that has percolated through or drained from a hazardous substance or soil contaminated with a hazardous substance. (c) “Linearized multistage model” means a dose-response model which assumes that there are a number of distinct biological stages or changes that must occur for a normal cell to be transformed into a tumor and which assumes the dose-response relationship to be linear at low doses.modification of the multistage dose-response model, used for estimating carcinogenic risk, that incorporates a linear upper bound on extra risk for exposures below the experimental range. (d) “Notice of aesthetic impact” means a document that describes conditions at a facility that result from the presence of hazardous substances at concentrations which exceed only cleanup criteria that are based on aesthetic impacts. (e) “Reference concentration” or “RfC” means an estimate of the continuous inhalation exposure to the human population, including sensitive subgroups and lifestages, that is likely to be without appreciable risk of adverse effect during a lifetime. The reference concentration is expressed in units of micrograms of hazardous substance per cubic meter of air. (ef) “Reference dose” or “RfD” means an conservative estimate of the daily intake oral exposure to of the human population, including sensitive subgroups and lifestages, that is likely to be without appreciable risk of deleterious adverse effect during a lifetime. The reference dose is expressed in units of milligrams hazardous substance per kilogram of body weight per day.

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(fg) “Relative source contribution factor” or “RSC” means that portion of a person’s total daily intake of a noncarcinogenic hazardous substance that comes from the medium being addressed by the cleanup criterion the portion of the total daily exposure to a noncarcinogenic hazardous substance that is attributed or allocated to the environmental medium being addressed by the cleanup criterion. (gh) “Relevant pathway” means an exposure pathway that is reasonable and relevant because there is a reasonable potential for exposure to a hazardous substance to occur to a human or nonhuman receptor. The components of an exposure pathway are a source or release of a hazardous substance, an exposure point, and, if the exposure point is not the source or point of release, a transport medium. The existence of a municipal water supply, exposure barrier, or other similar feature does not automatically make an exposure pathway irrelevant. (hi) “Risk assessment” means the analytical process used to determine estimate the risk to the public health, safety, or welfare or to the environment associated with a release or threat of release of a hazardous substance at a facility. (i) "Secondary maximum contaminant level" means the United States environmental protection agency's secondary maximum contaminant level for protection of the public welfare for substances that may adversely affect the taste, odor, color, appearance, or any aesthetic quality of drinking water, as set forth in 40 C.F.R. part 143 (revised as of July 1, 2012), which is adopted by reference in these rules and which is available for inspection at the Lansing office of the department, 525 West Allegan Street, Lansing, Michigan. Copies of the provisions may be purchased, at a cost as of the time of adoption of these rules of $55.00, from the Superintendent of Documents, Government Printing Office, Washington, DC 20401 (Stock Number 869-044-00152-7), or from the Department of Environmental Quality, Remediation and Redevelopment Division, 525 West Allegan Street, Lansing, Michigan 48933, at cost. (j) “Toxicological interaction” means simultaneous exposure to 2 or more hazardous substances whichthat will produce a toxicological response that is greater or less than their individual responsesadditivity. (k) “Volatile” means a hazardous substance that exhibits either of the following: (i) Vapor pressure greater than 1 millimeter of mercury. (ii) A Henry’s law constant equal to or greater than 0.00001 atmosphere-cubic meter per mole at standard temperature and pressure. (kl) “Weight of evidence” a term of art used in risk assessment, means an evaluation of the relevant scientific data conducted to determine the likelihood that a hazardous substance is a human carcinogen or causes noncancer adverse health effects, or both. The evaluation may include, but is not limited to, any of the following information in addition to toxicological bioassays: (i) Structure-activity relationships. (ii) cChemical-physical properties. (iii) Short-term test findings. (iv) Results of appropriate physiological, biological, and toxicological observations. (v) Comparative metabolism and pharmacokinetic studies. (l) “Volatile” means any compound that exhibits a Henry’s law constant equal to or greater than 0.00001 atmosphere-cubic meter per mole at standard temperature and pressure. (m) A term defined in the act has the same meaning when used in these rules.

R 299.3 Response activitiesy; protection of public health, safety, welfare, and environment required; rules applicable to interim response actionsactivity designed to meet cleanup criteria; degree of cleanup; modification of cleanup category; aquifers; unacceptability of response activity plan.

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Rule 3. (1) All response activitiesy shall be protective of the public health, safety, and welfare and the environment. Applicable generic cleanup criteria established by the department pursuant tounder section 20120a(1) and site-specific cleanup criteria approved by the department under section 20120a(2) and 20120b of the act and these rules reflect the department’s judgment, at the time the criteria are established or approved by the department, about the numerical criteria required to meet this protectiveness requirement, subject to the provisions of R 299.4(3), R 299.28 and R 299.34(2). The inclusion of a hazardous substance in the list with a “not available” in place of a value or a criterion means an evaluation was conducted and data were not available for the value or criterion to be developed. (2) All of the following are hazardous substances for which response activity is required: (a) Those hazardous substances determined to have been released at the facility. (b) A hazardous substance that is known to be a metabolite or breakdown product of a hazardous substance released at a facility. (c) A hazardous substance that has resulted from a reaction or any other physical or chemical change associated with the release. (23) These rules in this part apply to interim response activitiesy. that are designed to meet cleanup criteria. References in this part to response activity also include those interim response activities. (3) The category of land use-based remedial action under section 20120a(1) of the act or the site- specific cleanup criteria identified under sections 20120a(2) and 20120b of the act may be modified by the person proposing to conduct the response activity that will result in modification during implementation or after completion of a remedial action, if appropriate to the facility and if that modification is accomplished in a manner that is consistent with the act and these rules. (4) If a revised land use-based remedial action includes characteristics that are required to be approved by the department, then the person implementing the change shall seek department approval as required by part 201 of the act and these rules. (5) The horizontal and vertical extent of hazardous substance concentrations in an aquifer above the higher of either the concentration allowed by section 20120a(1)(a) or (10) of the act, as applicable, shall not increase after the initiation of remedial actions to address an aquifer, except as approved by the directordepartment as provided in section 20118(54) and (65) of the act. (6) All remedial actions that address the remediation of an aquifer shall provide for removal of the hazardous substance or substances from the aquifer, either through active remediation or as a result of naturally occurring biological or chemical processes which can be documented to occur at the facility, except as provided in section 20118(54) and (65) of the act.

R 299.4 General requirements for application of generic cleanup criteria. Rule 4. (1) All cleanup criteria used in response activity undertaken under part 201 of the act and these rules shall be based on best available information and weight of evidence. (2) The generic cleanup criteria developed by the department using the algorithms presented in these rules are derived primarily from data that reflect chronic toxicity endpoints. If a hazardous substance has a more sensitive toxic effect than those associated with the chronic toxicity data used to calculate a generic criterion, then the department shall develop a generic criterion shall be developed to address the most sensitive effect. The generic cleanup criteria established by the department shall be accepted as protective of the most sensitive toxic effect in a given exposure pathway for the hazardous substance in question. (3) If the department has not calculated a criterion for a hazardous substance for a given exposure pathway, then the person proposing or implementing the response activity shall supply the necessary

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data for the department to calculate a criterion or establish a criterion under subrule (4) of this rule, unless the department determines that a numerical criterion is not required to assure that a given response activity will be protective.When a hazardous substance, in addition to the chronic exposure accounted for with a generic criterion, has the potential to cause adverse human health effects for short-term exposures, the department may develop interim response screening levels for the purpose of evaluating the risk. (4) The department may establish Aa generic or site-specific cleanup criterion may be established by the department based on best professional judgment instead of a calculation based on minimum toxicity data for a specific hazardous substance when the minimum toxicity data are not available for that hazardous substance, but data of sufficient quality are available to show that the hazardous substance in question can be adequately assessed by comparison to the toxicity of another hazardous substance for which sufficient data are available. The department may establish Aa criterion may be established by the department in this manner when the hazardous substances are expected by the department to have similar fate and toxicity. (5) For the application of cleanup criteria, environmental data shall reliably represent conditions of the environmental media. Environmental data shall include quality assurance and quality control processes that ensures data is representative and of sufficient quality. (6) If a generic soil cleanup criterion developed under R 299.20 to R 299.27 is greater than the Csat concentration for that hazardous substance as shown in the generic soil cleanup criteria tables of R 299.46, then the generic soil criterion may not apply in all cases. If the release is a mixture of hazardous substances, then comparison to Csat is not appropriate. All of the following apply: (a) A person proposing or implementing response activity shall evaluate whether additional response activity is required to control NAPL or to protect against risks associated with NAPL that are not accounted for in development of the generic soil criteria. (b) A site-specific risk evaluation may be conducted for each relevant exposure pathway when NAPL is present. (c) Corrective action for a petroleum release regulated under part 213 of this act shall evaluate NAPL under part 213 of this act. (7) If the concentration of a hazardous substance in groundwater is greater than the flammability and explosivity screening levels shown in the generic groundwater cleanup criteria table in R 299.46, then the person proposing or implementing response activity shall document whether additional response activity is required to protect against an acute flammability and explosivity hazard. (8) The department may identify specific isomers of hazardous substances that must be added together and the sum compared to an identified chemical compound-specific or class-specific cleanup criterion for a given environmental medium. If analytical data detects a single isomer, additional analytical evaluation for the total of the isomers is necessary for comparison to the identified criterion. (9) Hazardous substances that exhibit the characteristics as defined under part 111 of the act by R 299.9212 of ignitability, reactivity, corrosivity, or toxicity are footnoted in the criteria tables in R 299.46. (10) If a person submits a no further action report under part 201 of the act or a closure report under part 213 of the act during the timeframe of 6 months before the promulgation of these rules up to the effective date of these rules, the review of the report shall be based on the criteria in effect at the time of the submittal unless the director makes a determination that a new or changed criterion renders the remedial or corrective actions completed no longer protective of the public health, safety, or welfare, or the environment. The decision of the director is reviewable as

53 2017 MR 22 – December 15, 2017 allowed by law. This provision does not affect an owner’s or operator’s obligations under section 20107a or 21304c of the act.

R 299.6 Establishment of Ggeneric cleanup criteria; toxicological and chemical-physical properties; use of generic cleanup criteria as risk-based screening levels; procedure for developing additional generic criteria. Rule 6. (1) Except as provided in subrules (9), (10) and (11) of this rule, generic groundwater cleanup criteria for the residential and nonresidential categories shall be the values shown in table 1 of R 299.44. If a generic groundwater cleanup criterion is higher than the flammability and explosivity screening level shown in table 1 of R 299.44, then the person proposing or implementing response activity shall document whether additional response activity is required to protect against the acute hazard. Generic groundwater and soil cleanup criteria for the residential and nonresidential categories are established pursuant to this rule and are shown in the generic cleanup criteria tables in R 299.46. Volatilization to indoor air groundwater, soil, and vapor Tier 1 screening levels are established pursuant to this rule and are shown in the generic cleanup criteria tables in R 299.46. (2) Except as provided in subrules (9), (10), and (11) of this rule, generic soil cleanup criteria for the residential category shall be the values shown in table 2 of R 299.46. If soil concentrations are greater than Csat, then the person proposing or implementing response activity shall evaluate whether additional response activity is required to control free-phase liquids or to protect against risks associated with free- phase liquids that are not accounted for in development of the generic criteria. Except as provided in the footnotes of the generic cleanup criteria tables in R 299.49, groundwater, soil, and volatilization to indoor air health-based values for the residential and nonresidential categories are derived from the equations in R 299.10 and R 299.20 to R 299.27. The minimum value calculated for carcinogenic, noncarcinogenic, mutagenic, or developmental effects establishes the calculated health-based value. (3) Except as provided in subrules (9), (10), and (11) of this rule, generic soil cleanup criteria for the nonresidential category shall be the values shown in table 3 of R 299.48. Except as provided in the footnotes of the generic cleanup criteria tables in R 299.49, the toxicological, chemical-specific, and chemical-physical input values used by the department to establish generic cleanup criteria with the equations and generic input values provided in R 299.10 and R 299.20 to R 299.27 are shown in the tables of R 299.50. (4) The generic cleanup criteria shown in R 299.44, R 299.46, and R 299.48 and identified under subrule (12) of this rule may be used and known as risk-based screening levels for corrective actions required under part 213 of the act. When the calculated health-based value derived from R 299.10 for a hazardous substance differs from the state drinking water standard, the criterion is the state drinking water standard pursuant to section 20120a(5) of the act. Criteria to which this subrule applies are designated with a footnote in the generic groundwater cleanup criteria table in R 299.46. (5) Generic cleanup criteria under R 299.44, R 299.46, and R 299.48 are based on the target detection limit or background concentration in the following cases: (a) If a calculated cleanup criterion is less than the target detection limit for that hazardous substance in a given medium, then the target detection limit is the cleanup criterion. Criteria to which this subdivision applies are designated with a footnote in the criteria tables. (b) A background concentration may be substituted for a generic cleanup criterion when the background concentration is higher than a criterion shown in R 299.44, R 299.46, or R 299.48.If a hazardous substance imparts adverse aesthetic characteristics to groundwater at a concentration

54 2017 MR 22 – December 15, 2017

less than the state drinking water standard from subrule (4) of this rule , then the aesthetic-based criterion derived under R 299.9 is the drinking water criterion in the table of the generic groundwater cleanup criteria table in R 299.46 and designated with a footnote. (6) If a hazardous substance imparts adverse aesthetic characteristics to groundwater at a concentration less than the health-based criterion for that hazardous substance, then the aesthetic-based criterion derived under R 299.9 is shown as the drinking water criterion in the table of generic cleanup criteria in R 299.44 and designated with a footnote. Except as provided in subrule (4) of this rule, if the calculated health-based value is greater than the solubility limit of the hazardous substance in water at 25 degrees Celsius, then the solubility limit is the generic groundwater cleanup criterion. Criteria to which this subrule applies are designated with a footnote in the generic groundwater cleanup criteria table in R 299.46. (7) Except as provided in section 20120a(9) of the act, R 299.49(1)(l), and R 299.49(1)(o), the toxicological, and physical-chemical, input values used by the department to derive generic cleanup criteria with the equations and default assumptions provided in R 299.10, R 299.14, R 299.20, R 299.22, R 299.24, and R 299.26 are shown in tables 4 of R 299.50. The maximum ceiling concentration for soil health-based criteria is 10% by dry weight, or 1.0E+8 parts per billion. Except for ambient air soil criteria derived from R 299.26, criteria to which this subrule applies are designated with a footnote in the generic soil cleanup criteria tables in R 299.46. Ambient air soil criteria as shown in the soil criteria tables represent a ½ acre source size and may require source size modification before application of this subrule. If soil criteria established under this subrule exceed the chemical-specific Csat, then additional response activity may be necessary under R 299.4(6). (8) Toxicological, and chemical-physical data in tables 4 of R 299.50, if available, shall be used in conjunction with the equations and default assumptions that appear in these rules for the development of generic cleanup criteria under subrules (9) or (10) of this rule, except as provided in section 20120a(9) of the act, R 299.49(1)(l), and R 299.49(1)(o). The target detection limit or the background concentration of a hazardous substance becomes the generic cleanup criteria in the following cases: (a) If a calculated health-based value is less than the target detection limit for that hazardous substance in a given medium, then the target detection limit is the cleanup criterion. (b) A background concentration may be substituted for a generic cleanup criterion when the background concentration is higher than a criterion shown in the tables in R 299.46. (9) For a substance that is not listed in the cleanup criteria tables in R 299.44, R 299.46, or R 299.48, the department may determine if the substance is a hazardous substance using best available information about the toxicological and physical-chemical properties of that substance and use that information to develop a generic or site-specific cleanup criterion.When the department has determined cleanup criteria are necessary under R 299.28, that criterion is shown in the criteria tables in R 299.46 and designated with a footnote. (10) For a substance that is listed in the cleanup criteria tables in R 299.44, R 299.46, or R 299.48, if the department obtains sufficient information to support calculation of a cleanup criterion which is designated in the cleanup criteria tables or tables 4 of R 299.50 with a footnote “ID” or “NA,” the department shall use best available information to calculate a cleanup criterion for the hazardous substance.Groundwater-surface water interface generic cleanup criteria is the minimum of the water quality standards for surface water developed for toxic substances or otherwise applicable water quality standards for surface water, developed pursuant to part 31 of the act. (11) If a new state drinking water standard is established or a state drinking water standard is changed after the effective date of this rule, the drinking water standard in effect under section 5 of 1976 PA 399, MCL 325.1005, shall become the generic residential cleanup criterion under R 299.44, as provided in

55 2017 MR 22 – December 15, 2017 section 20120a(5) of the act.The generic cleanup criteria shown in R 299.46 and identified under subrule (18) of this rule are the risk-based screening levels for corrective actions required under part 213 of the act. (12) If a generic cleanup criterion is developed under subrules (9) or (10) of this rule, or modified under subrules (11) of this rule, the department shall make the new toxicological and physical-chemical data and criterion available by announcing it on the department’s internet web site, and by publishing notice of the change in the department calendar, or by such other means that effectively notifies interested persons. The new criterion shall take effect when published and announced by the department as required in this rule. The new data and resulting cleanup criterion shall remain effective and be used as required under these rules until the department promulgates revised data and criteria pursuant to administrative procedures act, 1969 PA 306, MCL 24.201 to 24.328

R 299.7 Generic soil type and soil temperature value, facility-specific soil type and soil temperature value, site-specific soil type and soil temperature values. Rule 7. (1) The generic soil type input values used to develop Csat, soil-water partitioning values for groundwater protection criteria, soil volatilization to ambient air health-based values, and volatilization to indoor air screening levels are based on the soil-type sand as classified by the Natural Resources Conservation Services of the United States Department of Agriculture. (2) Soil information specific to a facility may allow revisions to the generic soil type values identified in R 299.18 and R 299.22 to R 299.27. When facility-specific soil information is used to revise the generic soil type and soil temperature values under these rules, the resulting generic criterion allows the facility to satisfy the categorical criteria in section 20120a(1)(a) to (d) of the act. (3) The department-approved generic input values by soil type are identified in table 1 of this rule. Facility-specific soil type shall be based on representative characterization. Documentation of all facility-specific input values shall be provided in the response activity plan, no further action report, or other response activity documentation. Facility-specific values are allowed as follows: (i) When soil has been classified with department-approved field methods sufficient to characterize a United States Department of Agriculture soil type as sand, sandy loam, loamy sand, or loam per figure 1 of this rule, the facility-specific soil input values shall be as identified in table 1 of this rule for those soil types. (ii) When soil information has been classified with department-approved methods sufficient to determine the use of a specific United States Department of Agriculture soil type other than those identified in subdivision (i) of this subrule, the input values shall be based on the generic input values in table 1 of this rule for the soil type identified. (iii) When heterogeneous soils are present, if a person does not rely on the generic soil type sand, a sensitivity analysis of the soil types and associated input values shall be performed. The soil type selected shall be the soil type that generates the most restrictive criterion. Department approved models or methods may be used to evaluate heterogeneous or multilayer soil present at a property for the volatilization to indoor air pathway pursuant to R 299.27(11). (iv) When non-native material consistent with materials defined as beneficial use by-products in part 115 of the act is present, the generic input values for sand in table 1 of this rule may be used. A site-specific evaluation shall be conducted for other non-native materials. Non-native material for this purpose means the material cannot be classified as 1 of the 12 soil types in the United States Department of Agriculture classification system.

56 2017 MR 22 – December 15, 2017

(v) When bedrock is within 1 meter of the structure’s foundation, a site-specific evaluation shall be conducted. (vi) All applicable generic input values for the soil type on table 1 shall be substituted to revise the criteria for any relevant soil exposure pathway. (4) The generic soil temperature value is 10 degrees Celsius or 283.15 Kelvin. When using facility-specific soil type assumptions, the generic soil temperature assumption shall be adjusted to the department-approved county-specific soil temperature values identified in table 2 of this rule. (5) Site-specific soil type and soil temperature values may be used to generate a site-specific criterion under sections 20120a(2) and 20120b of the act. Site-specific values shall be based upon representative characterization. All applicable soil type input values shall be determined and used to develop the criterion. A revision to generic residential criterion using only site-specific soil input values may allow department approval for unrestricted residential use. A location where concentrations of the hazardous substance do not exceed department approved site-specific cleanup criterion for unrestricted residential use would not be defined as a facility by part 201 of the act. (6) Figure 1 of this rule is as follows:

FIGURE 1.

(7) Tables 1 to 2 of this rule read as follows:

57 2017 MR 22 – December 15, 2017 TABLE 1. Generic Input Values for United States Department of Agriculture (USDA) Soil Conservation Service Soil Textural Classifications

Saturated Residual Soil Water- Saturated Soil Total Soil Air- A,B Dry Bulk Soil Texture A,B Water Water Filled van Genuchten parameters Mean Particle A,E Hydraulic Soil Texture Porosity A,C A,B A Filled A,E Density A Abbreviation Content Content Porosity A,D Diameter Conductivity (USDA) n Porosity ρb (USDA) 3 3 θs θr θw 3 3 (cm) 3 Ks (cm /cm ) θa (cm /cm ) (g/cm ) (cm3/cm3) (cm3/cm3) (cm3/cm3) (cm/h) α1 (1/cm) N M

Clay C 0.459 0.459 0.098 0.215 0.244 0.01496 1.253 0.2019 0.0092 1.43 0.61

Clay loam CL 0.442 0.442 0.079 0.168 0.274 0.01581 1.416 0.2938 0.016 1.48 0.34

Loam L 0.399 0.399 0.061 0.148 0.251 0.01112 1.472 0.3207 0.02 1.59 0.5

Loamy sand LS 0.39 0.39 0.049 0.076 0.314 0.03475 1.746 0.4273 0.04 1.62 4.38

Silt SI 0.489 0.489 0.05 0.167 0.322 0.00658 1.679 0.4044 0.0046 1.35 1.82

Silty loam SIL 0.439 0.439 0.065 0.18 0.259 0.00506 1.663 0.3987 0.011 1.49 0.76

Silty clay SIC 0.481 0.481 0.111 0.216 0.265 0.01622 1.321 0.243 0.0039 1.38 0.4

Silty clay loam SICL 0.482 0.482 0.09 0.198 0.284 0.00839 1.521 0.3425 0.0056 1.63 0.46

Sand S 0.375 0.375 0.053 0.054 0.321 0.03524 3.177 0.6852 0.044 1.66 26.78

Sandy clay SC 0.385 0.385 0.117 0.197 0.188 0.03342 1.208 0.1722 0.025 1.63 0.47

Sandy clay loam SCL 0.384 0.384 0.063 0.146 0.238 0.02109 1.33 0.2481 0.029 1.63 0.55

Sandy loam SL 0.387 0.387 0.039 0.103 0.284 0.02667 1.449 0.3099 0.03 1.62 1.6

A - From User’s Guide for Evaluating Subsurface Vapor Intrusion into Buildings. United States Environmental Protection Agency, Office of Emergency and Remedial Response. February 22, 2004. B - Hers, I. June 3, 2002 Technical Memorandum to Debbie Newberry, United States Environmental Protection Agency, Office of Solid Waste. Input Parameters for Office of Solid Waste and Emergency Response Wide Guidance for Vapor Intrusion Pathway.

C - Saturated water content is assumed to be equal to the water soil total porosity because the saturated water between drainage and wetting conditions varies but is always less than the fully saturated water content which is equal to the soil total porosity.

D - The air-filled porosity is calculated as the total porosity minus soil water-filled porosity.

E - Nielson, K. K., and V. C. Rogers. 1990. Radon transport properties of soil classes for estimating indoor radon entry. In: F. T. Cross (ed), Proceedings of the 29th Hanford Symposium of Health and the Environment. Indoor Radon and Lung Cancer: Reality or Myth? Part 1. Battelle Press, Richland, Washington.

58

TABLE 2. Facility-specific Soil Temperatures by County (degrees Celsius) COUNTY TEMP COUNTY TEMP COUNTY TEMP COUNTY TEMP Alcona 9 Dickinson 9 Lake 11.5 Oceana 12 Alger 8.5 Eaton 12 Lapeer 11 Ogemaw 9.5 Allegan 11.5 Emmet 9.5 Leelanau 11 Ontonagon 8 Alpena 9 Genesee 10.5 Lenawee 11.5 Osceola 11 Antrim 10 Gladwin 10 Livingston 11 Oscoda 9.5 Arenac 9.5 Gogebic 8 Luce 8.5 Otsego 9.5 Baraga 8.5 Grand Traverse 11 Mackinac 8.5 Ottawa 11 Barry 12 Gratiot 11 Macomb 11 Presque Isle 9 Bay 10 Hillsdale 12.5 Manistee 11.5 Roscommon 10 Benzie 11 Houghton 8 Marquette 8.5 Saginaw 10.5 Berrien 13 Huron 11 Mason 12 Sanilac 11 Branch 12.5 Ingham 11.5 Mecosta 11 Schoolcraft 8.5 Calhoun 13 Ionia 11 Menominee 9.5 Shiawassee 11 Cass 12.5 Iosco 9.5 Midland 10.5 St. Clair 11 Charlevoix 9.5 Iron 8.5 Missaukee 10 St. Joseph 12 Cheboygan 9 Isabella 10.5 Monroe 11 Tuscola 10 Chippewa 8.5 Jackson 12.5 Montcalm 11 Van Buren 12 Clare 10.5 Kalamazoo 12 Montmorency 9 Washtenaw 11.5 Clinton 11 Kalkaska 10 Muskegon 12 Wayne 11 Crawford 9.5 Kent 11 Newaygo 12 Wexford 11 Delta 9 Keweenaw 8 Oakland 11

R 299.8 Groundwater cleanup criteria generally. Rule 8. (1) Except as provided in subrule (2) of this rule, tThe generic groundwater cleanup criteria applicable at a given facility shall beis the most restrictive of the criteria developed under R 299.9, R 299 10, or R 299.14, established under R 299.6 considering those relevant pathways that are reasonable and relevant toat the facility and the category of cleanup criteria being proposed or implemented. (2) If a generic groundwater cleanup criterion developed under R299.9, R299.10, or R299.14 is greater than the solubility limit of that hazardous substance in water at 25o Celsius, then the solubility limit shall be the generic criteria for that pathway. For the purposes of groundwater cleanup criteria developed under R 299.9 and R 299.10, the point of exposure is presumed to be any point in an affected aquifer.

R 299.9 Calculation of generic cleanup criteria for groundwater in an aquifer based on adverse aesthetic impacts. Rule 9. (1) If a hazardous substance, singly or in combination with other hazardous substances present at the facility, imparts adverse aesthetic characteristics to groundwater in an aquifer, then the cleanup criterion shall beis the national secondary maximum contaminant leveldrinking water regulation, or, if there is no national secondary

59 2017 MR 22 – December 15, 2017

maximum contaminant leveldrinking water regulation, then the concentration that is documented as the taste or odor threshold concentration or the concentration below which appearance or other aesthetic characteristics are not adversely affected. The criteria of this subrule shall apply only when the level required by this subrule is less than the level required by section 20120a(4) of the act. A taste or odor threshold concentration or a concentration adversely affecting appearance shall be determined according pursuant to methods approved by the United States eEnvironmental pProtection aAgency. (2) For the purposes of this rule, the point of exposure shall be presumed to be any point in the affected aquifer.

R 299.10 Generic cleanup drinking water criteria based on ingestion of for groundwater in an aquifer based on ingestion of groundwater for drinking water. Rule 10. (1) Exposure to groundwater by ingestion shall beis considered a relevant pathway for groundwater that satisfies either of the following conditions: (a) The groundwater is in an aquifer. (b) The groundwater is not in an aquifer, but can reasonably be expected to transport a hazardous substance into an aquifer in a concentration that exceeds the generic residential criteria developed under subrule (2) of this rule. (2) The generic drinking water criteria developed pursuant to R 299.9 and R 299.10 are not applicable if ingestion of the groundwater is, or as part of the response activity will be, reliably restricted by a restrictive covenant, a notice of approved environmental remediation, or an institutional control that is allowed for under these rules land or resource use restriction as required by the act and approved by the department, if approval is required. (3) Cleanup criteria for groundwater based on ingestion of groundwater forThe health- based drinking water value shall be calculated accordingpursuant to the following algorithmsequations, except as provided for in R 299.34, and in the footnotes of the generic cleanup criteria tables in R 299.49. Criteria calculated under this subrule shall be the generic cleanup criterion, unless a state drinking water standard is available or, if a criterion protective of adverse aesthetic characteristics is more restrictive, as provided for in section 20120a(5) of the act. (4) The residential drinking water value shall be the minimum of the drinking water health-based values calculated pursuant to equations 1 to 5 of this rule. The nonresidential drinking water value shall be the minimum of the health-based drinking water values calculated pursuant to equations 8 to 10 of this rule. (5) Toxicological, chemical-specific, and chemical-physical generic input values are provided in R 299.50. (6) The generic drinking water equations are as follows:

RESIDENTIAL: 1. EQUATION FOR CARCINOGENIC EFFECTS:

TR ATca CF DWVca  SFEFres IFdw

60 2017 MR 22 – December 15, 2017 where, DWVc (Drinking water value) = chemical-specific, µg/L or ppb a TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days CF (Conversion factor) = 1,000 µg/mg SF (Oral cancer slope factor) = chemical-specific, (mg/kg-day)-1 EFres (Exposure frequency) = 350 days/year IFdw (Age-adjusted drinking water = 1.1 L-year/kg-day ingestion factor)

2. EQUATION FOR CARCINOGENS WITH MUTAGENIC EFFECTS:

TR ATca CF DWVmut  SFEFres IFdw,mut where, DWVm (Drinking water value) = chemical-specific, µg/L or ppb ut TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days CF (Conversion factor) = 1,000 µg/mg SF (Oral cancer slope factor) = chemical-specific, (mg/kg-day)-1 EFres (Exposure frequency) = 350 days/year IFdw,mut (Age-adjusted drinking water = 3.6 L-year/kg-day ingestion factor)

3. EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ ATres RfDRSCw CF DWVnc  EFres IFdw where, DWVn (Drinking water value) = chemical-specific, µg/L or ppb c THQ (Target hazard quotient) = 1 ATres (Averaging time) = 11,680 days RfD (Oral reference dose) = chemical-specific, mg/kg-day RSCw (Relative source contribution) = chemical-specific or 0.2 CF (Conversion factor) = 1,000 µg/mg EFres (Exposure frequency) = 350 days/year IFdw (Age-adjusted drinking water = 1.1 L-year/kg-day ingestion factor)

4. EQUATION FOR DEVELOPMENTAL EFFECTS - CHILD:

61 2017 MR 22 – December 15, 2017

THQ ATchild RfDdev BWchild RSCw  CF DWVdev  EDchild EFres IRdw,child where, DWVdev (Drinking water value) = chemical-specific, µg/L or ppb THQ (Target hazard quotient) = 1 ATchild (Averaging time) = 2,190 days RfDdev (Oral reference dose) = chemical-specific, mg/kg-day BWchild (Body weight) = 15 kg RSCw (Relative source contribution) = 0.2 or chemical-specific CF (Conversion factor) = 1,000 µg/mg EDchild (Exposure duration) = 6 years EFres (Exposure frequency) = 350 days/year IRdw, child (Drinking water ingestion rate) = 0.78 L/day

5. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT RESIDENT:

THQ ATpreg RfDdev BWpreg RSCw  CF DWVdev  EDpreg EFres IRdw,preg where, DWVdev (Drinking water value) = chemical-specific, µg/L or ppb THQ (Target hazard quotient) = 1 ATpreg,FT (Averaging time, full-term = 280 days or chemical-specific pregnancy) ATpreg,SE (Averaging time, single event = 1 day or chemical-specific exposure during pregnancy) RfDdev (Oral reference dose) = chemical-specific, mg/kg-day BWpreg (Body weight, pregnant = 75 kg resident) RSCw (Relative source contribution) = 0.2 or chemical-specific CF (Conversion factor) = 1,000 µg/mg EDpreg,FT (Exposure duration, full-term = 0.767 year or chemical-specific pregnancy) EDpreg,SE (Exposure duration, single event = 1 day or chemical-specific exposure during pregnancy) EFpreg,FT (Exposure frequency, full-term = 268.5 days/year or chemical- pregnancy) specific EFpreg,SE (Exposure frequency, single = 1 day/day or chemical-specific event exposure during pregnancy) IRdw, preg (Drinking water ingestion rate, = 1.8 L/day pregnant resident)

The age-adjusted drinking water ingestion factors shall be calculated pursuant to equations 6 and 7 of this rule.

62 2017 MR 22 – December 15, 2017

6. IFdw for carcinogens (Equation 1) and noncarcinogens (Equation 3):

IR ED  IR ED  IF   dw,age 16 age 16   dw,adult adult  dw      BWage 16   BWadult  where, IFdw (Age-adjusted drinking water = 1.1 L-year/kg-day ingestion factor) IRdw,age <1-6 (Drinking water ingestion = 0.78 L/day rate, child) EDage <1-6 (Exposure duration, child) = 6 years BWage <1-6 (Body weight, child) = 15 kg

IRdw,adult (Drinking water ingestion = 2.5 L/day rate, adult) EDadult (Exposure duration, adult) = 26 years BWadult (Body weight, adult) = 80 kg

7. IFdw,mut for carcinogens with mutagenic effects (Equation 2): I R ED ADAF I R ED ADAF I F  2  2  2   2 6  2 6  2 6  dw, mut    B W      BW     2   2 6       

I R ED ADAF I R ED ADAF  6 16  6 16  6 16   16  16  16    BW     32 B W32 32   6 16   16      32  where, IFdw,mut (Age-adjusted drinking water = 3.6 L-year/kg-day ingestion factor) IRdw,age <2 (Drinking water ingestion = 0.82 L/day rate, age <2 years) EDage <2 (Exposure duration) = 2 years BWage <2 (Body weight, age <2 years) = 9.6 kg ADAF<2 (Age-dependent adjustment = 10, unitless factor for cancer potency, age <2 years) IRdw,age 2-6 (Drinking water ingestion = 0.76 L/day rate, age 2-6 years) EDage 2-6 (Exposure duration, age 2-6 = 4 years years) BWage 2-6 (Body weight, age 2-6 years) = 17 kg ADAF2-6 (Age-dependent adjustment = 3, unitless factor for cancer potency, age 2-6 years) IRdw,age 6-16 (Drinking water ingestion = 1.3 L/day rate, age 6-16 years) EDage 6-16 (Exposure duration, age 6-16 = 10 years years)

63 2017 MR 22 – December 15, 2017

BWage 6-16 (Body weight, age 6-16 years) = 44 kg ADAF6-16 (Age-dependent adjustment = 3, unitless factor for cancer potency, age 6-16 years) IR16-32 (Drinking water ingestion = 2.3 L/day rate, age 16-32 years) ED16-32 (Exposure duration, age 16-32 = 16 years years) BW16-32 (Body weight, age 16-32 = 77 kg years) ADAF16-32 (Age-dependent adjustment = 1, unitless factor for cancer potency, age 16-32 years)

NONRESIDENTIAL: 8. EQUATION FOR CARCINOGENIC EFFECTS:

TR ATca BWadult  CF DWVca  SFEDnr EFnr IRdw,nr

where, DWVca (Drinking water value) = chemical-specific, µg/L or ppb TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days BWadult (Body weight, adult) = 80 kg CF (Conversion factor) = 1,000 µg/mg SF (Oral cancer slope factor) = chemical-specific (mg/kg-day)-1 EDnr (Exposure duration) = 20 years EFnr (Exposure frequency) = 238 days/year IRdw,nr (Drinking water ingestion rate) = 1.3 L/day

9. EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ ATnr RfDBWadult RSCw CF DWVnc  EDnr EFnr IRdw,nr where, DWVnc (Drinking water value) = chemical-specific, µg/L or ppb THQ (Target hazard quotient) = 1 ATnr (Averaging time) = 7,300 days RfD (Oral reference dose) = chemical-specific, mg/kg-day BWadult (Body weight, adult) = 80 kg RSCw (Relative source contribution) = 0.2 or chemical-specific CF (Conversion factor) = 1,000 µg/mg EDnr (Exposure duration) = 20 years EFnr (Exposure frequency) = 238 days/year

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IRdw, nr (Drinking water ingestion rate) = 1.3 L/day

10. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT WORKER:

THQ ATdev RfDBWdev RSCw  CF DWVdev  EDdev EFdev IRdw,dev where, DWVde (Drinking water value) = chemical-specific, µg/L or ppb v THQ (Target hazard quotient) = 1 ATdev,F (Averaging time, pregnant worker, = 280 days or chemical-specific T full-term pregnancy) ATdev,S (Averaging time, pregnant worker, = 1 day or chemical-specific E single event exposure during pregnancy) RfD (Oral reference dose) = chemical-specific, mg/kg-day BWdev (Body weight, pregnant worker) = 75 kg RSCw (Relative source contribution) = 0.2 or chemical-specific CF (Conversion factor) = 1,000 µg/mg EDdev,F (Exposure duration, pregnant = 0.767 year or chemical-specific T worker, full-term pregnancy) EDdev,S (Exposure duration, pregnant = 1 day or chemical-specific E worker, single event exposure during pregnancy) EFdev,F (Exposure frequency, pregnant = 183 days/year or chemical- T worker, full-term) specific EFdev,S (Exposure frequency, pregnant = 1 day/day or chemical-specific E worker, single event exposure during pregnancy) IRdw, (Drinking water ingestion rate) = 0.9 L/day dev

EQUATION FOR CARCINOGENIC EFFECTS:

TR  BW  AT  CF DWC  SF  EF  ED  IR dw where, DWC (Drinking water criterion) = chemical-specific (ug/L or ppb) TR (Target risk level) = 10-5 BW (Body weight) = 70 kg AT (Averaging time in days) = 25,550 days (70 years x 365 days/year) CF (Conversion factor) = 1000 ug/mg SF (Oral cancer slope factor) = chemical-specific (mg/kg-day)-1 EF (Exposure frequency) = 350 days/year (residential)

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=245 days/year (nonresidential) ED (Exposure duration) = 30 years (residential) =21 years (nonresidential)

IRdw (Drinking water ingestion rate) = 2 liters/day (residential) =1 liter/day (nonresidential)

EQUATION FOR NONCARCINOGENS:

THQ  RfD  BW  AT  RSC  CF DWC  EF  ED  IR dw where, DWC (Drinking water criterion) = chemical-specific (ug/L or ppb) THQ (Target hazard quotient) = 1 RfD (Oral reference dose) = chemical-specific (mg/kg-day) BW (Body weight) = 70 kg = 10,950 days (30 years x 365 AT (Averaging time) days/year - residential) 7,665 days (21 years x 365 days/year - nonresidential) RSC (Relative source contribution) = chemical-specific or 0.2 if chemical-specific data are not available CF (Conversion factor) = 1000 ug/mg EF (Exposure frequency) = 350 days/year (residential) 245 days/year (nonresidential) ED (Exposure duration) = 30 years (residential) 21 years (nonresidential) IRdw (Drinking water ingestion rate) = 2 liters/day (residential) 1 liter/day (nonresidential)

(4) For the purposes of this rule, the point of exposure shall be presumed to be any point in the affected aquifer.

R 299.14 Rescinded. Generic cleanup criteria for groundwater based on hazardous substance vapors emanating from groundwater to indoor air. Rule 14. (1) Inhalation of hazardous substance vapors volatilizing from groundwater to indoor air shall be considered a reasonable and relevant exposure pathway for hazardous substances in groundwater that have a Henry’s law constant greater than or equal to 0.00001 atm-m3/mole. (2) Except as provided in subrule (1) of this rule, if any of the following conditions exist, the generic criteria developed pursuant to this rule shall not apply and a site- specific evaluation of indoor inhalation risks shall be conducted: (a) There is a structure present or planned to be constructed at the facility which does not have a concrete block or poured concrete floor and walls. (b) The highest water table elevation of a contaminated saturated zone at the facility, considering seasonal variation, is within 3 meters of the ground surface.

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(c) There is a sump present that is not completely isolated from the surrounding soil by its materials of construction, or there is other direct entry of contaminated groundwater into the basement. (3) Groundwater cleanup criteria based on inhalation of hazardous substance vapors volatilizing from groundwater to indoor air shall be called groundwater volatilization indoor air inhalation criteria (“GVIIC”). The GVIIC is determined by the following series of calculations, except as provided in R 299.34(3):

EQUATION FOR CARCINOGENIC EFFECTS:

TR  AT x AIR GVIIC  IURFEFED CRbuilding where, GVIIC (Groundwater volatilization indoor = chemical-specific, ug/L air inhalation criteria) TR (Target risk level) = 10-5 AT (Averaging time) = 25,550 days (70 x 365) AIR (Adjusted inhalation rate) = 1 (residential) = 2 (nonresidential) IURF (Inhalation unit risk factor) = chemical-specific, (ug/m3)-1 EF (Exposure frequency) = 350 days/year (residential) = 245 days/year (nonresidential) ED (Exposure duration) = 30 years (residential) = 21 years (nonresidential) CRbuilding (Ratio of indoor air concentration to = chemical-specific, groundwater concentration) (ug/m3)/(ug/L)

EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ  AT GVIIC  1 ITSL EF ED  CRbuilding where, GVIIC (Groundwater volatilization indoor = chemical-specific, ug/L air inhalation criteria) THQ (Target hazard quotient) = 1 AT (Averaging time) = 10,950 days (residential) = 7,665 days (nonresidential) EF (Exposure frequency) = 350 days/year (residential) = 245 days/year (nonresidential) ED (Exposure duration) = 30 years (residential) = 21 years (nonresidential) ITSL (Initial threshold screening level) = chemical-specific, ug/m3 CRbuilding (Ratio of indoor air concentration to = chemical-specific, groundwater concentration) (ug/m3)/(ug/L)

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The ratio of the indoor air concentration to the groundwater concentration is calculated as: gw CRbuildingCRsource where, CRbuilding (Ratio of indoor air concentration to = chemical-specific, groundwater concentration) (ug/m3)/(ug/L)  (Attenuation coefficient) = chemical-specific, unitless gw CR source (Ratio of soil vapor concentration to = chemical-specific, groundwater/source concentration) (ug/m3)/(ug/L)

The soil vapor-phase concentration generated from a hazardous substance in groundwater is assumed to be in equilibrium with the aqueous phase concentration (Cw) of that substance as related by the dimensionless Henry’s law constant (H’) such that:

gw 3 3 CR source  H' x TAF  C w 10 L/m where, gw CRsource (Ratio of soil vapor concentration to = chemical-specific, groundwater/source concentration) (ug/m3)/(ug/L) H’ (Dimensionless Henry’s law constant, = chemical-specific, unitless where H’ = HLC x 41) HLC (Henry’s law constant at 25 degrees = chemical-specific, Celsius) (atm-m3/mol) TAF (Temperature adjustment factor) = 0.5, unitless Cw (Uniform unit groundwater = 1 ug/L concentration)

The intrusion rate of hazardous substance vapors into buildings is predicted using an analytical solution which couples both diffusive and convective transport of vapors emanating from groundwater into enclosed spaces. An attenuation coefficient () is calculated that is expressed as the ratio of building indoor air concentration to the vapor- phase concentration at the source. Values of  are calculated assuming infinite source conditions. For infinite source conditions  is written as follows:  eff   D A b   Q soilL crack   T   exp     crack  Qbuilding L T  D A crack           eff   eff   D A b D A b     Q soilL crack   T   T   Q soilL crack   exp    exp   1   crack  Q L  Q L   crack    D A crack  building T soil T   D A crack         where,

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 (Attenuation coefficient) = unitless eff (Total effective diffusion coefficient) = chemical-specific, cm2/s D T Dcrack (Effective diffusion coefficient 2 crack eff = cm /s, (D = Dv , see through crack) eff equation for Dv below) 2 Ab (Area of enclosed space below grade) = 1.96E+6 cm (residential) = 3.83E+6 cm2 (nonresidential) 3 Qbuilding (Building ventilation rate) = 1.51E+5 cm /s (residential) = 5.04E+5 cm3/s (nonresidential) Lcrack (Building foundation thickness) = 15 cm LT (Source-building separation distance) = 115 cm (residential) = 300 cm (nonresidential) 3 Qsoil (Volumetric flow rate of soil vapor = 0.81 cm /s (residential) into the building) = 2.10 cm3/s (nonresidential) 2 Acrack (Total area of cracks below grade) = 196 cm (residential) = 383 cm2 (nonresidential) exp(p) (The base of the natural logarithm = ep raised to power p)

To characterize contaminant diffusion from groundwater into buildings a total effective eff diffusion coefficient (DT ) is calculated to account for both liquid phase diffusion of the eff contaminant through the capillary fringe, (D cf ) , and vapor phase diffusion through the eff vadose zone, (Dv ). The calculation is as follows:

eff L T DT  eff eff hv  Lcrack Dv  hcf Dcf where,

eff (Total effective diffusion coefficient) = chemical-specific, cm2/s DT LT (Source-building separation distance) = 115 cm (residential) = 300 cm (nonresidential) hv (Thickness of vadose zone below = 75 cm (residential) enclosed space floor) = 260 cm (nonresidential) Lcrack (Building foundation thickness) = 15 cm eff (Effective diffusion coefficient through = chemical-specific, cm2/s Dv vadose zone) hcf (Thickness of capillary fringe) = 25 cm eff 2 D cf (Effective diffusion coefficient through = chemical-specific, cm /s capillary fringe)

eff The effective diffusion coefficient calculation for the vadose zone (Dv ) is written as:

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eff 3.33 2  Dw 3.33 2  Dv  Da a n   w n  H'TAF  where, eff (Effective diffusion coefficient through = chemical-specific, cm2/s Dv vadose zone) 2 Da (Diffusivity in air) = chemical-specific, cm /s 3 3 a (Soil air-filled porosity) = 0.13 cm /cm N (Total soil porosity) = 0.43 cm3/cm3 2 Dw (Diffusivity in water) = chemical-specific, cm /s H’ (Dimensionless Henry’s law constant, = chemical-specific, unitless where H’ = HLC x 41) HLC (Henry’s law constant = chemical-specific, (atm-m3/mol) TAF (Temperature adjustment factor) = 0.5 3 3 w (Soil water-filled porosity) = 0.3 cm /cm

eff The effective diffusion coefficient calculation for the capillary fringe (D cf ) is written as:

eff 3.33 2  Dw 3.33 2  Dcf  Da θa,cf n   θw,cf n  H'TAF  where,

eff 2 D cf (Effective diffusion coefficient through = chemical-specific, cm /s capillary fringe) 2 Da (Diffusivity in air) = chemical-specific, cm /s 3 3 a,cf (Soil air-filled porosity in capillary = 0.078 cm /cm fringe) 2 Dw (Diffusivity in water) = chemical-specific, cm /s H’ (Dimensionless Henry’s law constant, = chemical-specific, unitless where H’ = HLC x 41) HLC (Henry’s law constant) = chemical-specific, (atm-m3/mol) TAF (Temperature adjustment factor) = 0.5 3 3 w,cf (Soil water-filled porosity in capillary = 0.352 cm /cm fringe) N (Total soil porosity) = 0.43 cm3/cm3

(4) Facility-specific measurements of the following parameters may be substituted individually for the generic assumptions and still allow the facility to satisfy the generic categorical criteria under section 20120a(1)(a) to (e) of the act: (a) Dry soil bulk density. (b) Fraction of organic carbon in soil. (c) Soil vapor permeability. (d) Temperature adjustment factor for Henry’s law constant.

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(e) Source-building foundation separation distance. (f) Vertical thickness of capillary fringe. Facility-specific measurements shall be based on representative characterization. Documentation of all facility specific values shall be provided in the response activity plan, no further action report, or other response activity documentation. (5) The department may approve methods to demonstrate compliance with criteria for the exposure pathway if those methods are more representative of in-situ conditions at the facility. Methods acceptable to the department may include, but are not limited to, use of representative soil gas concentrations.

R 299.16 Generic flammability and explosivity screening level for hazardous substances in groundwater. Rule 16. (1) Except as provided in the footnotes of the generic cleanup criteria tables in R 299.49, the flammability and explosivity screening level (FESL) shall be calculated using chemical-specific and chemical-physical generic input values provided in R 299.50 pursuant to the following equation:

EQUATION FOR FESL:

LEL 0.2MW PCF FESL  1 HLC TAFCF2 where, FESL (Flammability/explosivity = chemical-specific, µg/L screening level) LEL (Lower explosive limit) = chemical-specific, % MW (Molecular weight) = chemical-specific, g/mol P (Atmospheric pressure) = 1 atm (Conversion factor for % to = CF 106 µg/g 1 µg/L) HLC (Henry’s law constant) = chemical-specific atm- m3/mol TAF (Temperature adjustment factor) = 0.5, unitless 3 3 CF2 (Conversion factor for volume) = 10 L/m

(2) The FESL is not a cleanup criterion for unrestricted residential use as used in determining whether a location is a facility as defined under part 201 of the act or property as defined under part 213 of the act.

R 299.18 Cleanup criteria for soil generally. Rule 18. (1) The generic cleanup criteria for soil at a facility shall be the most restrictive of the applicable criteria developed under R 299.20 to R 299.28established pursuant to R 299.6, considering those relevant pathways that are reasonable and relevant at the facility and the category of cleanup criteria being proposed or implemented. (2) If a generic soil cleanup criterion developed under R 299.20 to R 299.26 is greater than the Csat concentration for that hazardous substance, then the generic criteria may not

71 2017 MR 22 – December 15, 2017

apply. A site specific risk evaluation may be conducted for each relevant exposure pathway where free-phase liquids or non-aqueous phase liquids (NAPL) are present.The Csat shall be calculated for a single hazardous substance using the chemical-specific and chemical-physical generic input values provided in R 299.50 pursuant to the following equation:

S Csat  Kd ρb  θw  H'TAFθa  ρb where, Csat (Soil saturation concentration) = chemical-specific, µg/kg S (Solubility in water) = chemical-specific, µg/L 3 Kd (Soil-water partition coefficient for = chemical-specific, cm /g or organic compounds: Kd =Koc x foc) L/kg 3 Koc (Soil organic carbon partition = chemical-specific, cm /g coefficient) foc (Organic carbon content of soil) = 0.002 g/g 3 b (Dry soil bulk density) = 1.66 g/cm w (Soil water-filled porosity) = 0.054 Lwater/Lsoil a (Soil air-filled porosity) = 0.375Lair/Lsoil H (Dimensionless Henry’s law constant) = chemical-specific, unitless TAF (Temperature adjustment factor) = 0.5, unitless

Department-approved facility-specific inputs to the Csat equation are allowed pursuant to R 299.7. (3) The department may develop values to represent saturated total petroleum hydrocarbon conditions at facilities where petroleum releases have occurred. (4) The generic soil criteria are applicable at all soil depths. (5) The department may develop and publish statewide default soil background levels for hazardous substances that occur naturally in soil.

R 299.20 Generic cleanup criteria for soil based on direct contact. Rule 20. (1) Direct contact with soil is considered a relevant pathway for all facilities. (2) The health-based direct contact value shall be calculated pursuant to the equations in this rule, except as provided for in R 299.34, and in the footnotes of the generic cleanup criteria tables in R 299.49. (3) Toxicological, chemical-specific, and chemical-physical generic input values are provided in R 299.50. Both of the following apply: (a) Chemical-specific absorption data shall be used in this rule if determined by the department to be the best available information. (b) If chemical-specific absorption data are not available, then the following generic absorption efficiencies shall be used: (i) Ingestion adsorption efficiency (AEi) shall be 50% for organic hazardous substances that exhibit a log octanol water partitioning coefficient greater than 5

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and a molecular weight greater than 200 grams per mole or that are not ionizing organic compounds, and 100% for all other organic hazardous substances. (ii) AEi shall be 50% for inorganic hazardous substances. (iii) Dermal absorption efficiency (AEd) shall be assumed to be 10% for organic hazardous substances. (iv) AEd shall be assumed to be 1% for inorganic hazardous substances. (v) Gastrointestinal absorption efficiency (ABSgi) shall be assumed to be 100% for all hazardous substances. (4) The residential soil direct contact value is the minimum of the health-based values calculated pursuant to equations 1 to 5 of this rule. The nonresidential soil direct contact value is the minimum of the health-based values calculated pursuant to equations 11 to 13 of this rule. (5) The generic soil direct contact equations are as follows:

RESIDENTIAL: 1. EQUATION FOR CARCINOGENIC EFFECTS:

TR  ATca  CF DCVca  SF EF IF  AE  SF EF DF AE o i,res s i d d,res d

where, DCVca (Direct contact value) = chemical-specific, µg/kg TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days CF (Conversion factor) = 1E+9 µg/kg SFo (Oral cancer slope factor) = chemical-specific, (mg/kg-day)-1 EFi,res (Ingestion exposure frequency) = 350 days/year IFs (Age-adjusted soil ingestion factor) = 100.5 mg-year/kg-day AEi (Ingestion absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule SFd (Dermal cancer slope factor) = chemical-specific, (mg/kg-day)-1 EFd,res (Dermal exposure frequency) = 275 days/year DF (Age-adjusted soil dermal factor) = 424.5 mg-year/kg-day AEd (Dermal absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule

2. EQUATION FOR CARCINOGEN WITH MUTAGENIC EFFECTS:

TR  ATca  CF DCVmut  SFo  EFi,res IFs,mut  AEi  SFd  EFd,res  DFmut  AEd where,

DCVmut (Direct contact value) = chemical-specific, µg/kg or ppb

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TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days CF (Conversion factor) = 1E+9 µg/kg SFo (Oral cancer slope factor) = chemical-specific, (mg/kg-day)-1 EFi,res (Ingestion exposure frequency) = 350 days/year IFs,mut (Age-adjusted soil ingestion factor) = 578.4 mg-year/kg-day AEi (Ingestion absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule SFd (Dermal cancer slope factor) = chemical-specific, (mg/kg-day)-1 EFd,res (Dermal exposure frequency) = 275 days/year DFmut (Age-adjusted soil dermal factor) = 2,060 mg-year/kg-day AEd (Dermal absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule

3. EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ  AT RSC  CF DCV  res s nc 1 1 ( EFi,res IFs  AEi )  ( EFd,res DF  AEd ) RfD o RfD d where, DCVnc (Direct contact value) = chemical-specific, µg/kg or ppb THQ (Target hazard quotient) = 1 ATres (Averaging time) = 11,680 days RSCs (Relative source contribution for = 1 or chemical-specific soil) CF (Conversion factor) = 1E+9 µg/kg RfDo (Oral reference dose) = chemical-specific, mg/kg-day EFi,res (Ingestion exposure frequency) = 350 days/year IFs (Age-adjusted soil ingestion factor) = 100.5 mg-year/kg-day AEi (Ingestion absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule RfDd (Dermal reference dose) = chemical-specific, mg/kg-day EFd,res (Dermal exposure frequency) = 275 days/year DF (Age-adjusted soil dermal factor) = 424.5 mg-year/kg-day AEd (Dermal absorption efficiency) = chemical-specific or as specified in subrule (3)(b)

4. EQUATION FOR DEVELOPMENTAL EFFECTS - CHILD:

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THQ  AT BW RSC  CF DCV  child child s dev 1 1 EDchild  [( EFi,res IRs,child  AEi )  ( EFd,res  SA child EV  AFchild  AEd )] RfDo,dev RfDd,dev where, DCVdev (Direct contact value) = chemical-specific, µg/kg or ppb THQ (Target hazard quotient) = 1 ATchild (Averaging time) = 2,190 days BWchild (Body Weight) = 15 kg RSCs (Relative source contribution for = 1 or chemical-specific soil) CF (Conversion factor) = 1E+9 µg/kg EDchild (Exposure duration) = 6 years RfDo,dev (Oral reference dose) = chemical-specific, mg/kg-day EFi,res (Ingestion exposure frequency) = 350 days/year IRs,child (Soil ingestion rate) = 179 mg/day AEi (Ingestion absorption efficiency) = chemical-specific or as specified in subrule(3)(b) of this rule RfDd,dev (Dermal reference dose) = chemical-specific, mg/kg-day EFd,res (Dermal exposure frequency) = 275 days/year 2 SAchild (Skin surface area) = 2,400 cm EV (Event frequency) = 1 event/day 2 AFchild (Soil adherence factor) = 0.3 mg/cm -event AEd (Dermal absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule

5. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT RESIDENT:

THQ  AT  BW  RSC  CF DCV  preg preg s dev 1 1 EDpreg  [(  EFi,preg IRs,preg  AEi )  (  EFd,preg  SApreg  EV  AFpreg  AEd )] RfDo,dev RfDd,dev where, DCVdev (Direct contact value) = chemical-specific, µg/kg or ppb) THQ (Target hazard quotient) = 1 ATpreg,FT (Averaging time, full-term = 280 days or chemical-specific pregnancy) ATpreg,SE (Averaging time, single event = 1 day or chemical-specific exposure during pregnancy) BWpreg (Body weight, pregnant resident) = 75 kg RSCs (Relative source contribution for = 1 or chemical-specific soil)

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CF (Conversion factor) = 1E+9 µg/kg EDpreg,FT (Exposure duration, full-term = 0.767 year or chemical-specific pregnancy) EDpreg,SE (Exposure duration, single event = 1 day or chemical-specific exposure during pregnancy) RfDo,dev (Oral reference dose) = chemical-specific, mg/kg-day EFi,preg,FT (Ingestion exposure frequency, full- = 268.5 days/year or chemical- term pregnancy) specific EFi,preg,SE (Ingestion exposure frequency, = 1 day/day or chemical-specific single event exposure during pregnancy) IRs,preg (Soil ingestion rate) = 89 mg/day AEi (Ingestion absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule RfDd,dev (Dermal reference dose) = chemical-specific, mg/kg-day EFd,preg,F (Dermal exposure frequency, full- = 268.5 days/year or chemical- T term pregnancy) specific EFd,preg,S (Dermal exposure frequency, single = 1 day/day or chemical-specific E event exposure during pregnancy) 2 SApreg (Skin surface area, pregnant = 5,500 cm resident) EV (Event frequency) = 1 event/day 2 AFpreg (Soil adherence factor) = 0.07 mg/cm -event AEd (Dermal absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule

The dermal slope factors and dermal reference dose shall be extrapolated from the oral toxicity values pursuant to the following equations, except when dermal toxicity endpoints are available.

6. Dermal slope factor and dermal reference dose: SF SF o d  ABS gi

RfDd  RfDo  ABSgi where, -1 SFd (Dermal cancer slope factor) = chemical-specific, (mg/kg-day) -1 SFo (Oral cancer slope factor) = chemical-specific, (mg/kg-day) ABSgi (Gastrointestinal absorption = 1 or chemical-specific factor) RfDd (Dermal reference dose) = chemical-specific, mg/kg-day RfDo (Oral reference dose) = chemical-specific, mg/kg-day

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The age-adjusted soil ingestion factors (IFs) shall be calculated pursuant to equations 7 and 8 of this rule.

7. IFs for carcinogens (Equation 1) and noncarcinogens (Equation 3):

IR ED  IR ED  IF   s, 16 16  s,adult adult  s      BW16   BWadult  where, IFs (Age-adjusted soil ingestion = 100.5 mg-year/kg-day factor) IRs,age <1-6 (Soil ingestion rate) = 179 mg/day EDage <1-6 (Exposure duration) = 6 years BWage <1-6 (Body weight) = 15 kg IRs,adult (Soil ingestion rate) = 89 mg/day EDadult (Exposure duration) = 26 years BWadult (Body weight) = 80 kg

8. IFs for carcinogens with mutagenic effects (Equation 2):

IR ED  ADAF  IR ED  ADAF   s, 2 2 2   s, 26 26 26  IFs,mut         BW2   BW26 

I R ED ADAF I R ED ADAF  s, 6 16  6 16  6 16   s, 16 32  16  16    B W      B W32 32   6 16   16      32  where, IFs,mut (Soil ingestion factor for = 578.4 mg-year/kg-day mutagens) IRs, <2 (Soil ingestion rate, age <2 = 179 mg/day years) ED <2 (Exposure duration, age <2 = 2 years years) BW <2 (Body weight, age <2 years) = 9.6 kg ADAF <2 (Age-dependent adjustment = 10, unitless factor for cancer potency, age <2 years) IRs, 2-6 (Soil ingestion rate, age 2-6 = 179 mg/day years) ED2-6 (Exposure duration, age 2-6 = 4 years years) BW 2-6 (Body weight, age 2-6 years) = 17 kg ADAF2-6 (Age-dependent adjustment = 3, unitless factor for cancer potency, age 2-6 years) IRs, 6-16 (Soil ingestion rate, age 6-16 = 89 mg/day years)

77 2017 MR 22 – December 15, 2017

ED 6-16 (Exposure duration, age 6-16 = 10 years years) BW6-16 (Body weight, age 6-16 years) = 44 kg ADAF6-16 (Age-dependent adjustment = 3, unitless factor for cancer potency, age 6-16 years) IRs,16-32 (Soil ingestion rate, age 16-32 = 89 mg/day years) ED16-32 (Exposure duration, age 16-32 = 16 years years) BW16-32 (Body weight, age 16-32 = 77 kg years) ADAF16-32 (Age-dependent adjustment = 1, unitless factor for cancer potency, age 16-32 years)

The age-adjusted soil dermal factors shall be calculated pursuant to equations 9 and 10 of this rule.

Age-adjusted soil dermal factor (DF): 9. DF for carcinogens (Equation 1) and noncarcinogens (Equation 3):

 SA EV AF ED   SA EV AF ED  DF   16 16 16  adult adult adult       BW 16   BWadult  where, DF (Age-adjusted soil dermal = 424.5 mg-year/kg-day factor) 2 SA <1-6 (Skin surface area) = 2,400 cm EV (Event frequency) = 1 event/day 2 AF <1-6 (Soil adherence factor) = 0.3 mg/cm -event ED <1-6 (Exposure duration) = 6 years BW <1-6 (Body weight) = 15 kg 2 SAadult (Skin surface area) = 6,000 cm 2 AFadult (Soil adherence factor) = 0.07 mg/cm -event EDadult (Exposure duration) = 26 years BWadult (Body weight) = 80 kg

10. DF for carcinogens with mutagenic effects (Equation 2):

 SA EV AF ED  ADAF   SA EV AF ED  ADAF   2 2 2 2   2-6 26 2-6 26  DFmut         BW2   BW2-6 

 SA616 EV  AF616 ED616  ADAF616   SA16-32 EV  AF16-32 ED16-32  ADAF16-32        BW616   BW16-32 

78 2017 MR 22 – December 15, 2017 where, DFmut (Soil dermal factor for = 2,060 mg-year/kg-day mutagens) 2 SA <2 (Skin surface area, age <2 = 2,000 cm years) EV (Event frequency) = 1 event/day 2 AF <2 (Skin adherence factor, age = 0.3 mg/cm -event <2 years) ED <2 (Exposure duration, age <2 = 2 years years) BW <2 (Body weight, age <2 years) = 9.6 kg ADAF<2 (Age-dependent adjustment = 10, unitless factor for cancer potency, age <2 years) 2 SA, 2-6 (Skin surface area, age 2-6 = 2,600 cm years) 2 AF 2-6 (Skin adherence factor, age 2- = 0.3 mg/cm -event 6 years) ED 2-6 (Exposure duration, age 2-6 = 4 years years) BW 2-6 (Body weight, age 2-6 years) = 17 kg ADAF2-6 (Age-dependent adjustment = 3, unitless factor for cancer potency, age 2-6 years) 2 SA 6-16 (Skin surface area, age 6-16 = 3,700 cm years) 2 AF 6-16 (Skin adherence factor, age 6- = 0.07 mg/cm -event 16 years) ED 6-16 (Exposure duration, age 6-16 = 10 years years) BW 6-16 (Body weight, age 6-16 years) = 44 kg ADAF6-16 (Age-dependent adjustment = 3, unitless factor for cancer potency, age 6-16 years) 2 SA16-32 (Skin surface area, age 16-32 = 5,700 cm years) 2 AF16-32 (Skin adherence factor, age = 0.07 mg/cm -event 16-32 years) ED16-32 (Exposure duration, age 16-32 = 16 years years) BW16-32 (Body weight, age 16-32 = 77 kg years) ADAF16-32 (Age-dependent adjustment = 1, unitless factor for cancer potency, age 16-32 years)

NONRESIDENTIAL:

79 2017 MR 22 – December 15, 2017

11. EQUATION FOR CARCINOGENIC EFFECTS:

TR ATca BWadult CF DCVca,nr  EDnr SFo EFi,nr IRs,nr  AEi  SFd EFd,nr SAnr EV  AFnr  AEd where, DCVca,n (Direct contact value) = chemical-specific, µg/kg or r ppb TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days BWadult (Body weight, adult) = 80 kg CF (Conversion factor) = 1E+9 µg/kg EDnr (Exposure duration) = 20 years SFo (Oral cancer slope factor) = chemical-specific, (mg/kg- day)-1 EFi,nr (Ingestion exposure frequency) = 238 days/year IRs,nr (Soil ingestion rate) = 89 mg/day AEi (Ingestion absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule SFd (Derived dermal cancer slope = chemical-specific, (mg/kg- factor) day)-1 EFd,nr (Dermal exposure frequency) = 188 days/year 2 SAnr (Skin surface area, adult) = 3,500 cm EV (Event frequency) = 1 event/day 2 AFnr (Soil adherence factor) = 0.2 mg/cm -event AEd (Dermal absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule

12. EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ  ATnr  BWadult RSCs  CF DCVnc   1   1     nr  EDnr   EFi,nr IRs,nr  AEi    EFd,nr  SA EV  AFnr  AEd   RfDo   RfDd  where, DCVnc (Direct contact value) = chemical-specific, µg/kg or ppb THQ (Target hazard quotient) = 1 ATnr (Averaging time) = 7,300 days BWadult (Body weight) = 80 kg RSCs (Relative source contribution) = 1 or chemical-specific CF (Conversion factor) = 1E+9 µg/kg EDnr (Exposure duration) = 20 years RfDo (Oral reference dose) = chemical-specific, mg/kg-day EFi,nr (Ingestion exposure frequency) = 238 days/year IRs,nr (Soil ingestion rate) = 89 mg/day

80 2017 MR 22 – December 15, 2017

AEi (Ingestion absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule RfDd (Derived dermal reference dose) = chemical-specific, mg/kg-day EFd,nr (Dermal exposure frequency) = 188 days/year 2 SAnr (Skin surface area, adult) = 3,500 cm EV (Event frequency) = 1 event/day 2 AFnr (Soil adherence factor, worker) = 0.2 mg/cm -event AEd (Dermal absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule

13. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT WORKER:

THQ  ATdev BWdev RSCs  CF DCVnc   1   1  ED   EF IR  AE    EF  SA EV  AF  AE  dev  RfD i,dev s,dev i   RfD d,dev dev dev d   o,dev   d,dev  where, DCVdev (Direct contact value) = chemical-specific, µg/kg or ppb THQ (Target hazard quotient) = 1 ATdev,FT (Averaging time, pregnant = 280 days or chemical-specific worker, full-term pregnancy) ATdev,SE (Averaging time, pregnant = 1 day or chemical-specific worker, single event exposure during pregnancy) BWdev (Body weight, pregnant worker) = 75 kg RSCs (Relative source contribution) = 1 or chemical-specific CF (Conversion factor) = 1E+9 µg/kg EDdev,FT (Exposure duration, pregnant = 0.767 year or chemical- worker, full-term pregnancy) specific EDdev,SE (Exposure duration, pregnant = 1 day or chemical-specific worker, single event exposure during pregnancy) RfDo, dev (Oral reference dose) = chemical-specific, mg/kg-day EFi,dev,F (Ingestion exposure frequency, = 183 days/year or chemical- T pregnant worker, full-term specific pregnancy) EFi,dev,S (Ingestion exposure frequency, = 1 day/day or chemical- E pregnant worker, single event specific exposure during pregnancy) IRs,dev (Soil ingestion rate, pregnant = 89 mg/day worker) AEi (Ingestion absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of

81 2017 MR 22 – December 15, 2017

this rule RfDd, dev (Dermal reference dose) = chemical-specific, mg/kg-day EFd,dev,F (Ingestion exposure frequency, = 183 days/year or chemical- T pregnant worker, full-term specific pregnancy) EFd,dev,S (Dermal exposure frequency, = 1 day/day E pregnant worker) 2 SAdev (Skin surface area, pregnant = 3,100 cm worker) EV (Event frequency) = 1 event/day 2 AFdev (Soil adherence factor, pregnant = 0.2 mg/cm -event worker) AEd (Dermal absorption efficiency) = chemical-specific or as specified in subrule (3)(b) of this rule (1) Cleanup criteria for soil based on direct contact shall be calculated for the generic residential category according to the following algorithms, except as provided in R 299.34(3):

EQUATION FOR CARCINOGENS:

TR  AT  CF DCC  SF  [(EFi IF  AE i )  (EFd  DF  AE d )] where,

DCC (Direct contact criterion) = chemical-specific, ug/kg or ppb TR (Target risk level) = 10-5 AT (Averaging time) = 25,550 days (70 years x 365 days/year) CF (Conversion factor) = 1E+9 ug/kg SF (Oral cancer slope factor) = chemical-specific (mg/kg-day)- 1 EFi (Ingestion exposure frequency) = 350 days/year IF (Age-adjusted soil ingestion factor) = 114 mg-year/kg-day* AEi (Ingestion absorption efficiency) = chemical-specific or default specified at R 299.20(3) EFd (Dermal exposure frequency) = 245 days/year DF (Age-adjusted soil dermal factor) = 353 mg-year/kg-day** AEd (Dermal absorption efficiency) = chemical-specific or default specified at R 299.20(3)

EQUATIONS FOR NONCARCINOGENS:

THQ  RfD  AT  CF  RSC DCC  [(EFi IF  AE i )  (EFd  DF  AE d )]

82 2017 MR 22 – December 15, 2017 where,

DCC (Direct contact criterion) = chemical-specific (ug/kg or ppb) THQ (Target hazard quotient) = 1 RfD (Oral reference dose) = chemical-specific mg/kg-/day AT (Averaging time) = 10,950 days (30 years x 365 days/year) CF (Conversion factor) = 1E+9 ug/kg RSC (Relative source contribution) = 1 EFi (Ingestion exposure frequency) = 350 days/year IF (Age-adjusted soil ingestion factor) = 114 mg-year/kg-day* AEi (Ingestion absorption efficiency) = chemical-specific or default specified at R 299.20(3) EFd (Dermal exposure frequency) = 245 days/year DF (Age-adjusted soil dermal factor) = 353 mg-year/kg-day** AEd (Dermal absorption efficiency) = chemical-specific or default specified at R 299.20(3) and,

IR ED  IR ED  *IF   age 16 age 16   adult adult       BWage 16   BWadult  where,

IRsoil/age 1-6 (Soil ingestion rate) = 200 mg/day EDage 1-6 (Exposure duration) = 6 years BWage 1-6 (Body weight) = 15 kg IRadult (Soil ingestion rate) = 100 mg/day EDadult (Exposure duration) = 24 years BWadult (Body weight) = 70 kg and,  SA EV AF ED   SA EV AF ED  DF   age 16 age 16 age 16  adult adult adult  **      BWage 16   BWadult  where,

2 SAage 1-6 (Skin surface area) = 2,670 cm /dayevent EV (Event frequency) = 1 event/day 2 AFage 1-6 (Soil adherence factor) = 0.2 mg/cm EDage 1-6 (Exposure duration) = 6 years BWage 1-6 (Body weight) = 15 kg 2 SAadult (Skin surface area) = 5,800 cm /dayevent

83 2017 MR 22 – December 15, 2017

2 AFadult (Soil adherence factor) = 0.07 mg/cm EDadult (Exposure duration) = 24 years BWadult (Body weight) = 70 kg

(2) Cleanup criteria for soil based on direct contact shall be calculated for the generic nonresidential category according to the following algorithms, except as provided in R 299.34(3):

EQUATION FOR CARCINOGENS:

TRBW ATCF DCC SFED[(EFi IRs  AEi )  (EFd SAEV AF AEd )] where,

DCC (Direct contact criterion) = chemical-specific, ug/kg or ppb TR (Target risk level) = 10-5 BW (Body weight) = 70 kg AT (Averaging time) = 25,550 days (70 years x 365 days/year) CF (Conversion factor) = 1E+9 ug/kg SF (Oral cancer slope factor) = chemical-specific (mg/kg-day)- 1 ED (Exposure duration) = 21 years EFi (Ingestion exposure frequency) = 245 days/year IRs (Soil ingestion rate) = 100 mg/day (residential)

AEi (Ingestion absorption efficiency) = chemical-specific or default specified at R 299.20(3) EFd (Dermal exposure frequency) = 160 days/year SA (Skin surface area) = 3,300 cm2/day event EV (Event frequency) = 1 event/day AF (Soil adherence factor) = 0.2 mg/cm2 (nonresidential) AEd (Dermal absorption efficiency) = chemical-specific or default specified at R 299.20(3)

EQUATION FOR NONCARCINOGENS:

THQ  RfD  BW  AT  CF  RSC DCC  ED  [(EFi IR s  AE i )  (EFd  SA  EV  AF  AE d )]

where,

DCC (Direct contact criterion) = chemical-specific, ug/kg or ppb THQ (Target hazard quotient) = 1 RfD (Oral reference dose) = chemical-specific, mg/kg-/day

84 2017 MR 22 – December 15, 2017

BW (Body weight) = 70 kg AT (Averaging time) = 7,665 days (21 years x 365 days/year) CF (Conversion factor) = 1E+9 ug/kg RSC (Relative source contribution) = 1 ED (Exposure duration) = 21 years EFi (Ingestion exposure frequency) = 245 days/year IRs (Soil ingestion rate) = 100 mg/day AEi (Ingestion absorption efficiency) = chemical-specific or default specified at R 299.20(3) EFd (Dermal exposure frequency) = 160 days/year SA (Skin surface area) = 3,300 cm2/day event EV (Event frequency) = 1 event/day AF (Soil adherence factor) = 0.2 mg/cm2 (nonresidential) AEd (Dermal absorption efficiency) = chemical-specific or default specified at R 299.20(3)

(3) Absorption efficiencies used to calculate generic direct contact criteria are as follows: (a) Chemical-specific data may be submitted to the department to support development of a new generic criterion under R 299.6(9) or (10) and shall be used in this rule if determined by the department to be the best available information. (b) If chemical-specific data are not available, then the following default absorption efficiencies shall be used: (i) AEi shall be 50% for organic hazardous substances which exhibit a log octanol water partitioning coefficient greater than 5 and a molecular weight greater than 200 grams per mole or which are not ionizing organic compounds, and 100% for all other organic hazardous substances. (ii) AEi shall be 50% for inorganic hazardous substances. (iii) AEd shall be assumed to be 10% for organic hazardous substances. (iv) AEd shall be assumed to be 1% for inorganic hazardous substances. (4) To demonstrate compliance with generic direct contact criteria, the criteria shall be applied without regard to the depth of contaminated soil.

R 299.22 Generic cleanup criteria for soil based on leaching of hazardous substances into groundwater. Rule 22. (1) To assure that soils do not pose a threat of aquifer contamination, the concentration of the hazardous substance in soil shall be below that which produces a concentration in leachate that is equal to the least restrictive of the applicable groundwater criteria specified in subdivisions (a) to (c) of this subrule, or below a criterion based on the soil-water partitioning characteristics of a hazardous substance as provided in subrule (4) of this rule, whichever is higher. The selection of the following least restrictive value, and comparison to the soil-water partitioning value, shall be done separately for each pathway that is relevant at the facility: (a) The groundwater criteria developed under R 299.8 to 299.14. (b) The leachate concentration generated by background soil.

85 2017 MR 22 – December 15, 2017

(c) The groundwater concentration allowed by target detection limit, if it is higher than a risk-based criterion that would otherwise be the most restrictive. meet either of the following: (a) The total soil concentration groundwater protection criteria as described in subrule (2) of this rule. (b) The groundwater criteria in soil leachate as described in subrule (2) of this rule. (2) Leachate testing is not required to demonstrate compliance with subrule (1) of this rule if the total concentration of a hazardous substance in soil does not exceed 20 times the lowest groundwater cleanup criterion that is applicable at the facility or does not exceed the soil-water partitioning value established under subrule (4) of this rule, whichever is higher.The soil concentration protective of groundwater is the higher of the values derived as follows: (a) Soil-water partition value, if sufficient information is available to derive the value for the hazardous substance. (b) The groundwater criterion multiplied by 20. (3) When sufficient information is available, the soil-water partition value shall be calculated using the toxicological, chemical-specific, and chemical-physical generic input values provided in R 299.50 pursuant to equations 1 and 2 of this rule:

1. EQUATION FOR SOIL-WATER PARTITION VALUE (SWPV):

  θ  H  TAF θ   w a  SWPV  Cw  Kd      ρb  where, SWPV (Soil-water partition value) = chemical-specific, µg/kg or ppb Cw (Target soil leachate = chemical-specific, µg/L or ppb concentration; applicable groundwater criterion x 16) 3 Kd (Soil-water partition coefficient; = chemical-specific, cm /g or L/kg Kd for organics: Kd = Koc × foc) 3 Koc (Soil organic carbon partition = chemical-specific, cm /g coefficient) foc (Fraction of organic carbon = 0.002 g/g content of soil)  (Total soil porosity) = 0.375 Lpore/Lsoil w (Soil water-filled porosity) = 0.054 Lwater/Lsoil a (Soil air-filled porosity) = 0.321 Lair/ Lsoil H' (Dimensionless Henry’s law = chemical-specific, unitless constant) Note: for calculation of the SWPV for inorganic hazardous substances, H' equals zero. TAF (Temperature adjustment = 0.5, unitless factor) 3 ρb (Dry soil bulk density) = 1.66 g/cm

86 2017 MR 22 – December 15, 2017

Department-approved facility-specific inputs are allowed pursuant to R 299.7.

2. EQUATION FOR DIMENSIONLESS HENRY’S LAW CONSTANT (H'):

HLCCF H'  R  T where, H (Dimensionless Henry’s law constant) = chemical-specific, unitless HL (Henry’s law constant at 25º C) = chemical-specific, atm- C m3/mol R (Ideal gas constant) = 8.206E-2 atm-L/mol-K T (Temperature at 25C) = 298.15 K CF (Conversion factor) = 1,000 L/m3

(4) Soil leach testing is not required to demonstrate compliance with subrule (1) of this rule if the total concentration of a hazardous substance in soil does not exceed the soil criterion developed under subrule (2) of this rule. (35) Soil leachate shall meet the lowest applicable groundwater criterion. Soil leachate concentrations shall be determined by a method that best represents in-situ conditions. For the purposes of this rule, the following test methods are acceptable: (a) The United States eEnvironmental pProtection aAgency's toxicity characteristic leaching procedure, method 1311,(TCLP) (revised as of July 1992) or the synthetic precipitation leachate procedure, method 1312, (SPLP) (revised as of September 1994) as set forth in SW-846, Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, (revised to include Update IVII, June 13, 1997)dated August 2015, published by the United States Environmental Protection Agency, which are adopted by reference in these rules and which are available for inspection at the Lansing office of the dDepartment of Environmental Quality, 525 West Allegan Street, Lansing, Michigan. Copies of the provisions may be purchased at a cost as of the time of adoption of these rules of $239.00 from the National Technical Information Service, United States Department of Commerce, Alexandria5285 Port Royal Road, Springfield, Virginia 2216122312 product code PB2002105723 (publication number PB97-156111GEI), or from the Department of Environmental Quality, Remediation and Redevelopment Division, 525 West Allegan, Lansing, Michigan 48909, at cost. (b) Other methods accepted by the department to more accurately simulate conditions at the site than the test methods specified in subdivision (a) of this subrule. (4) The department may, if adequate data are available, establish acceptable soil concentrations based on soil-water partitioning characteristics of a hazardous substance.

R 299.24 Rescinded. Generic cleanup criteria for soil based on indoor inhalation of hazardous substance vapors volatilized from soil. Rule 24. (1) Indoor inhalation of hazardous substance vapors volatilizing to indoor air from soil shall be considered a reasonable and relevant exposure pathway only for hazardous substances that have a Henry’s law constant greater than or equal to 0.00001 atm-m3/mole.

87 2017 MR 22 – December 15, 2017

(2) Except as provided in subrule (1) of this rule, if any of the following conditions exist, the generic criteria developed pursuant to this rule shall not apply and a site- specific evaluation of indoor inhalation risks shall be conducted: (a) There is a structure present or planned to be constructed at the facility which does not have a concrete block or poured concrete floor and walls. (b) There is a sump present that is not completely isolated from the surrounding soil by its materials of construction. (3) Soil cleanup criteria based on indoor inhalation of volatile emissions from hazardous substances in soil shall be called soil volatilization indoor air inhalation criteria (“SVIIC”). The SVIIC is determined by the following series of calculations, except as provided in R 299.34(3):

EQUATION FOR CARCINOGENIC EFFECTS:

TR AT X AIR SVIIC  IURFEFEDCRbuilding where,

SVIIC (Soil volatilization indoor air = chemical-specific, ug/kg inhalation criterion) TR (Target risk level) = 10-5 AT (Averaging time) = 25,550 days (70 years x 365 days/year) AIR (Adjusted inhalation rate) = 1 (residential) = 2 (nonresidential) IURF (Inhalation unit risk factor) = chemical-specific, (ug/m3)-1 EF (Exposure frequency) = 350 days/year (residential) = 245 days/year (nonresidential) ED (Exposure duration) = 30 years (residential) = 21 years (nonresidential) CRbuilding (Ratio of indoor air concentration = chemical-specific, to soil concentration) (ug/m3)/(ug/kg)

EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ  AT SVIIC  1 ITSL  EF ED  CRbuilding where,

SVIIC (Soil volatilization indoor air = chemical-specific, ug/kg inhalation criterion) THQ (Target hazard quotient) = 1 AT (Averaging time) = 10,950 days (residential) = 7,665 days (nonresidential)

88 2017 MR 22 – December 15, 2017

EF (Exposure frequency) = 350 days/year (residential) = 245 days/year (nonresidential) ED (Exposure duration) = 30 years (residential) = 21 years (nonresidential) ITSL (Initial threshold screening level) = chemical-specific, ug/m3 CRbuilding (Ratio of indoor air concentration = chemical-specific, to soil concentration) (ug/m3)/(ug/kg)

The contaminant vapor concentration in the building indoor air is written as:

soil CRbuildingCRsource

where,

CRbuilding (Ratio of indoor air concentration to = chemical-specific, soil concentration) (ug/m3)/(ug/kg)  (Attenuation coefficient) = chemical-specific, Unitless soil CR source (Ratio of soil vapor concentration to = chemical-specific, soil/source concentration) (ug/m3)/(ug/kg)

The vapor-phase contaminant concentration at the source for soil is written as:

3 6 3 3 soil H'TAFCs b 10 kg g10 cm m CRsource  w  k d b  H'TAF a 

where,

soil CRsource (Ratio of soil vapor concentration to = chemical-specific, 3 soil/source concentration) (ug/m )/(ug/kg) H’ (Dimensionless Henry’s law constant, = chemical-specific, unitless where H’ = HLC x 41) HLC (Henry’s law constant at 25 degrees = chemical-specific, Celsius) (atm-m3/mol) TAF (Temperature adjustment factor) = 0.5, unitless

C s (Uniform concentration in soil) = 1 ug/kg 3 b (Dry soil bulk density) = 1.5 g/cm (Soil water-filled porosity) = 0.3 cm3/cm3 w 3 k d (Soil-water partition coefficient) = chemical-specific, cm /g (equivalent to L/kg) 3 For organic compounds = Koc (cm /g) x foc (g/g) For inorganic compounds = chemical-specific, cm3/g 3 K oc (Soil organic carbon partition = chemical-specific, cm /g coefficient)

89 2017 MR 22 – December 15, 2017

(Fraction of organic carbon content of = 0.002 g/g (0.2%) foc soil) 3 3 a (Soil air-filled porosity) = 0.13 cm /cm

The intrusion rate of hazardous substance vapors into buildings is predicted using an analytical solution which couples both diffusive and convective transport of vapors emanating from subsurface soil into enclosed spaces. An attenuation coefficient () is calculated that is expressed as the ratio of building indoor air concentration to the vapor- phase concentration at the source. Values of  are calculated assuming infinite source conditions. For infinite source conditions  is written as follows:  eff   D A b   Q soilL crack   v   exp     crack  QbuildingL T  D A crack           eff   eff   D A b D A b     Q soilL crack   v   v   Q soilL crack   exp    exp   1   crack  Q L  Q L   crack    D A crack  building T soil T   D A crack         where,

 (Attenuation coefficient) = unitless eff (Effective diffusion coefficient = chemical-specific, cm2/s Dv through vadose zone) Dcrack (Effective diffusion coefficient 2 crack eff = cm /s, (D = Dv , see through crack) eff equation for Dv below) 2 Ab (Area of enclosed space below grade) = 1.96E+6 cm (residential) = 3.83E+6 cm2 (nonresidential) 3 Qbuilding (Building ventilation rate) = 1.51E+5 cm /s (residential) = 5.04E+5 cm3/s (nonresidential) Lcrack (Building foundation thickness) = 15 cm LT (Source-building separation distance) = 15 cm (All land use categories) 3 Qsoil (Volumetric flow rate of soil vapor = 0.81 cm /s (residential) into the building) = 2.10 cm3/s (nonresidential) 2 Acrack (Total area of cracks below grade) = 196 cm (residential) = 383 cm2 (nonresidential) exp(p) (The base of the natural logarithm = ep raised to power p)

eff The effective diffusion coefficient calculation for the vadose zone ( D v ) is written as:

eff 3.33 2  Dw 3.33 2  Dv  Da a n   w n  H'TAF  where,

90 2017 MR 22 – December 15, 2017

eff (Effective diffusion coefficient through = chemical-specific, cm2/s Dv vadose zone) 2 Da (Diffusivity in air) = chemical-specific, cm /s 3 3 a (Soil air-filled porosity) = 0.13 cm /cm n (Total soil porosity) = 0.43 cm3/cm3 2 Dw (Diffusivity in water) = chemical-specific, cm /s H’ (Dimensionless Henry’s law constant, = chemical-specific, unitless where H’ = HLC x 41) HLC (Henry’s law constant = chemical-specific, (atm-m3/mol) 3 3 w (Soil water-filled porosity) = 0.3 cm /cm

(4) Facility-specific measurements of the following parameters may be substituted individually for the generic assumptions and still allow the facility to satisfy the categorical criteria in section 20120a(1)(a) to (e) of the act: (a) Dry soil bulk density. (b) Fraction of organic carbon in soil. (c) Soil vapor permeability. (d) Temperature adjustment factor for Henry’s law constant. Facility-specific measurements shall be based on representative characterization. Documentation of all facility specific values shall be provided in the response activity plan or no further action report. (5) The department may approve methods to demonstrate compliance with criteria for this exposure pathway if those methods are more representative of in-situ conditions at the facility. Methods acceptable to the department may include, but are not limited to, evaluation of representative soil gas concentrations.

R 299.26 Generic cleanup criteria for soil based on inhalation of hazardous substances in ambient air. Rule 26. (1) Inhalation of hazardous substance emissions in ambient air from soil shall beis considered a reasonable and relevant pathway for all facilities. (2) Generic cleanup criteria for soil based on inhalation of volatile hazardous substance emission to ambient air shall beis called volatile soil inhalation criteria (VSIC). Generic cleanup criteria for soil based on inhalation of particulate hazardous substance emission to ambient air shall be called particulate soil inhalation criteria (PSIC). The generic residential VSIC and PSIC are calculated as follows, except as provided in R 299.34(3): All of the following apply: (a) The VSIC is calculated for infinite and finite sources. (b) If the vertical extent of the hazardous substance source has not been characterized, then the infinite source criterion shall be used. (c) If the vertical extent of the hazardous substance source has been adequately characterized throughout the facility, then the criterion based on the finite 2 meter or the 5 meter source thickness may be used. The finite source thickness assumes no cover layer of clean soil.

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(3) Generic cleanup criteria for soil based on inhalation of particulate hazardous substance emission to ambient air is called particulate soil inhalation criteria (PSIC). (4) Toxicological, chemical-specific, and chemical-physical generic input values are provided in R 299.50 and soil type-specific inputs pursuant to R 299.7. (5) The health-based soil inhalation values are calculated pursuant to the equations of this rule, except as provided in R 299.34, and in the footnotes of the generic cleanup criteria tables in R 299.49. (6) The residential volatile soil inhalation values are the minimum of the health- based values calculated pursuant to equations 1 to 5 of this rule. The generic nonresidential volatile soil inhalation value shall be the minimum of the health- based values pursuant to equations 6 to 8 of this rule. (7) The residential particulate soil inhalation values are the minimum of the health-based values calculated pursuant to equations 11 to 15 of this rule. The generic nonresidential particulate soil inhalation value are the minimum of the health-based values pursuant to equations 16 to 18 of this rule. (8) The health-based soil inhalation values for volatiles and particulates are calculated using a dispersion factor (Q/C) value for a source area contamination size of ½ acre. The VSIC and PSIC presented in the generic soil cleanup criteria tables in R 299.46 shall be adjusted for other contamination source area sizes appropriate for the site to derive the generic VSIC and PSIC for the property by multiplying the ½ acre VSIC and PSIC by the modifiers given in the following table. (9) Where the actual source area size falls between the sizes given in this subrule, the ½ acre generic VSIC and PSIC shall be multiplied by the modifier for the next larger source size.

Table of Dispersion Factor (Q/C) Values Contamination Source Modifier for Dispersion Factor (Q/C) Area Size deriving final (g/m2-s per kg/m3) (ft2 or acres) VSIC/PSIC 100 ft2 295.82 6.97 400 ft2 129.34 3.05 1000 ft2 91.05 2.14 2000 ft2 73.72 1.74 ½ acre 42.45 1.00 1 acre 37.24 0.88 2 acres 32.81 0.77 5 acres 28.02 0.66 10 acres 25.02 0.59 20 acres 22.27 0.52 30 acres 20.89 0.49 50 acres 19.24 0.45 75 acres 18.06 0.43 100 acres 17.21 0.41 150 acres 16.17 0.38 200 acres 15.43 0.36 300 acres 14.50 0.34 400 acres 13.88 0.33 500 acres 13.38 0.32 1000 acres 12.02 0.28 1500 acres 11.25 0.26

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(10) The equations for the generic nonresidential soil inhalation health-based values do not explicitly include an exposure time. Continuous 24-hour per day exposure may not be representative of worker exposures in commercial or industrial settings. Both of the following apply: (a) Except as identified in subdivision (b) of this subrule, the generic nonresidential VSIC and PSIC derived from the health-based value equations of this rule may be adjusted to represent a 12-hour work day by multiplying the source size modified health-based criterion from the criteria tables by 2, except criteria with an exposure time designated as less than 12 hours shall not be adjusted. An exposure time adjusted VSIC or PSIC shall not exceed the maximum ceiling concentration or be lower than the target detection limit. A 12-hour exposure time adjusted VSIC or PSIC remains a generic nonresidential criterion. Other adjustments for exposure time may be proposed as site-specific criteria based on a nonresidential land use that by its nature would only allow activities for a limited exposure time. The activities allowed by the land use must be easily identifiable, enforceable, and included in the land or resource use restriction for the property. (b) Exposure time shall not be adjusted for nonresidential VSIC and PSIC developed from acceptable air concentrations based upon short-term inhalation reference values for exposures of less than 12 hours designated in R 299.49(1) (DD) to (FF).

(11) The generic volatile soil inhalation values and particulate soil inhalation values equations are as follows:

RESIDENTIAL: 1. EQUATION FOR CARCINOGENIC EFFECTS:

TR AT VSIV  ca ca  1    IURFEDres EFres    VFres  where, VSIVca (Volatile soil inhalation value = chemical and source size-specific, for infinite or finite source) µg/kg or ppb TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific (µg/m3)-1 EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year VFres (Volatilization factor for = chemical and source size-specific, infinite or finite source) m3/kg

2. EQUATION FOR CARCINOGENS WITH MUTAGENIC EFFECTS:

93 2017 MR 22 – December 15, 2017

TR ATca VSIVmut   1    IURFEFres  ED2  ADAF2  ED26  ADAF26  ED616  ADAF616  ED1632  ADAF1632     VFres  where, VSIVmut (Volatile soil inhalation value for = chemical and source size- infinite or finite source) specific, µg/kg or ppb TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific, (µg/m3)-1 EFres (Exposure frequency) = 350 days/year ED <2 (Exposure duration, age <2) = 2 years ADAF<2 (Age-dependent adjustment factor = 10, unitless for cancer potency) ED 2-6 (Exposure duration, age 2-6 years) = 4 years ADAF2-6 (Age-dependent adjustment factor = 3, unitless for cancer potency, age 2-6 years) ED 6-16 (Exposure duration, age 6-16 years) = 10 years ADAF6-16 (Age-dependent adjustment factor = 3, unitless for cancer potency, age 6-16 years) ED 16-32 (Exposure duration, age 16-32 = 16 years years) ADAF16-32 (Age-dependent adjustment factor = 1, unitless for cancer potency, age 16-32 years) VFres (Volatilization factor for infinite or = chemical and source size-specific, finite source) m3/kg

3. EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ AT RfCRSC VSIV  res nc  1    EDres EFres     VFres  where, VSIVnc (Volatile soil inhalation value = chemical and source size-specific, for infinite or finite source) µg/kg or ppb THQ (Target hazard quotient) = 1 ATres (Averaging time) = 11,680 days RfC (Reference concentration) = chemical-specific, µg/m3 RSC (Relative source contribution) = 1 or chemical-specific EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year VFres (Volatilization factor for = chemical and source size-specific, infinite or finite source) m3/kg

4. EQUATION FOR DEVELOPMENTAL EFFECTS - CHILD:

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THQ AT RfC RSC VSIV  child dev dev  1    EDchild EFres     VFres  where, VSIVde (Volatile soil inhalation value = chemical and source size-specific, v for infinite or finite source) µg/kg or ppb THQ (Target hazard quotient) = 1 ATchild (Averaging time) = 2,190 days 3 RfCdev (Reference concentration) = chemical-specific, µg/m RSC (Relative source = 1 or chemical-specific contribution) EDchild (Exposure duration) = 6 years EFres (Exposure frequency) = 350 days/year VFres (Volatilization factor for = chemical and source size-specific, infinite or finite source) m3/kg

5. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT RESIDENT:

THQ  AT  RfC  RSC VSIV  preg dev dev  1    EDpreg  EFpreg     VFres  where, VSIVdev (Volatile soil inhalation = chemical and source size-specific, value for infinite or finite µg/kg or ppb source) THQ (Target hazard quotient) = 1 ATpreg,F (Averaging time, full-term = 280 days or chemical-specific T pregnancy) ATpreg,S (Averaging time, single = 1 day or chemical-specific E event exposure during pregnancy) 3 RfCdev (Reference concentration) = chemical-specific, µg/m RSC (Relative source = 1 or chemical-specific contribution) EDpreg,F (Exposure duration, full- = 0.767 year or chemical-specific T term pregnancy) EDpreg,S (Exposure duration, single = 1 day or chemical-specific E event exposure during pregnancy) EFpreg,FT (Exposure frequency, full- = 268.5 days/year or chemical-specific term pregnancy) EFpreg,SE (Exposure frequency, single = 1 day/day or chemical-specific event exposure during pregnancy)

95 2017 MR 22 – December 15, 2017

VFres (Volatilization factor for = chemical and source size-specific, infinite or finite source) m3/kg

NONRESIDENTIAL: 6. EQUATION FOR CARCINOGENIC EFFECTS:

TR AT VSIV  ca ca  1    IURFEDnr EFnr    VFnr  where, VSIVca (Volatile soil inhalation value = chemical and source size-specific, for infinite or finite source) µg/kg or ppb TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific (µg/m3)-1 EDnr (Exposure duration) = 20 years EFnr (Exposure frequency) = 238 days/year VFnr (Volatilization factor for = chemical and source size-specific, infinite or finite source) m3/kg

7. EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ  AT  RfC  RSC VSIV  nr nc  1  EDnr  EFnr     VF nr  where, VSIVn (Volatile soil inhalation value = chemical- and source size-specific, c for infinite or finite source) µg/kg or ppb THQ (Target hazard quotient) = 1 ATnr (Averaging time) = 7,300 days RfC (Reference concentration) = chemical-specific, µg/m3 RSC (Relative source contribution) = chemical-specific or 1 EDnr (Exposure duration) = 20 years EFnr (Exposure frequency) = 238 days/year VFnr (Volatilization factor for = chemical- and source size-specific, infinite or finite source) m3/kg

8. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT WORKER:

THQ  ATdev  RfC dev  RSC VSIV dev  ED dev  EFdev  (1 VFdev ) where, VSIVde (Volatile soil inhalation value = chemical and source size-specific, v for infinite or finite source) µg/kg or ppb

96 2017 MR 22 – December 15, 2017

THQ (Target hazard quotient) = 1 ATdev,F (Averaging time, pregnant = 280 days or chemical-specific T worker, full-term pregnancy) ATdev,S (Averaging time, pregnant = 1 day or chemical-specific E worker, single exposure event during pregnancy) 3 RfCdev (Reference concentration) = chemical-specific, µg/m RSC (Relative source contribution) = 1 or chemical-specific EDdev,F (Exposure duration, pregnant = 0.767 year or chemical-specific T worker, full-term pregnancy) EDdev,S (Exposure duration, single = 1 day or chemical-specific E exposure event during pregnancy) EFdev,F (Exposure frequency, pregnant = 183 days/year or chemical-specific T worker, full-term pregnancy) EFdev,S (Exposure frequency, pregnant = 1 day/day or chemical-specific E worker, single exposure event during pregnancy) VFdev (Volatilization factor for = chemical and source size-specific, infinite or finite source, m3/kg pregnant worker)

The soil to air volatilization factors (VF) shall be calculated for infinite and finite sources pursuant to equations 9 and 10 of this rule, respectively.

The average flux for the finite sources may be derived using the United States Environmental Protection Agency Exposure Model for Soil-Organic Fate and Transport (EMSOFT) model or a modeling method approved by the department.

Soil to air volatilization factor (VF): 9. VF for infinite source equations:  1  VF  (Q/C)   (a) inf  ave   Js, inf 

ave 1/2 4 2 2 (b) Js,inf  ρb (4D A /πt)  10 cm /m

3.33 3.33 2 [(a Da (H  TAF)  w Dw )/n ] (c) DA  bK d  w  a (H  TAF) where, VFin (Volatilization factor for infinite = chemical and source size- 3 f source) specific, m /kg Q/C (Dispersion factor for 1/2 acre) = 42.45 g/m2-sec per kg/m3 ave (Normalized average flux for infinite = chemical-specific, g/m2-sec J s,inf source in soil) 3 b (Dry soil bulk density) = 1.66 g/cm

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2 DA (Apparent diffusivity) = chemical-specific, cm /sec π (Pi) = 3.14159, unitless t (Exposure time: 32 years x 3.1536E+7 sec/year = 1.01E+09 sec (residential) 20 years x 3.1536E+7 sec/year) = 6.31E+08 sec (nonresidential)  (Total soil porosity) = 0.375 Lpore/Lsoil w (Soil water-filled porosity) = 0.054 Lwater/Lsoil a (Soil air-filled porosity) = 0.321 Lair/Lsoil 2 Da (Diffusivity in air) = chemical-specific, cm /sec 2 Dw (Diffusivity in water) = chemical-specific, cm /sec H (Dimensionless Henry’s law constant) = chemical-specific, unitless TAF (Temperature adjustment factor) = 0.5, unitless 3 Kd (Soil-water partition coefficient) = chemical-specific, cm /g 3 For organic compounds = Koc (cm /g) x foc (g/g) For inorganic compounds = chemical-specific, cm3/g 3 Koc (Soil organic carbon partition = chemical-specific, cm /g coefficient) foc (Organic carbon content of soil) = 0.002 g/g

10. VF for finite source (2 or 5 meter depth) equation:  1  VF  (Q/C)  fin  ave   Js,fin  where, VFfi (Volatilization factor for finite = chemical and source size- 3 n source) specific, m /kg Q/C (Dispersion factor for 1/2 acre) = 42.45 g/m2-sec per kg/m3 ave (Normalized average flux for 2- or = chemical-specific, g/m2-sec J s,fin 5-meter finite source derived using EMSOFT flux (Js) and the ave equation: Js,fin = Js × (b/C0)) 2 Js (Instantaneous flux from soil at = chemical-specific, g/m -second time t derived using EMSOFT) 3 C0 Uniform contaminant = 1.66E-06 g/cm concentration at t = 0) 3 b (Dry soil bulk density) = 1.66 g/cm

RESIDENTIAL: 11. EQUATION FOR CARCINOGENIC EFFECTS:

TR  AT PSIV  ca ca  1    IURF EDres EFres     PEFres  where, PSIVca (Particulate soil inhalation = chemical and source size-specific,

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value) µg/kg or ppb -5 TR (Target risk level) = 10 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific, (µg/m3)-1 EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year 3 PEFres (Particulate emission factor) = source size-specific, m /kg

12. EQUATION FOR CARCINOGENS WITH MUTAGENIC EFFECTS:

TR  ATca PSIVmut   1    IURF EFres  ED2  ADAF2  ED26  ADAF26  ED616  ADAF616  ED1632  ADAF1632    PEFres  where, PSIVmut (Particulate soil inhalation value) = chemical and source size-specific, µg/kg or ppb TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific, (µg/m3)-1 EFres (Exposure frequency) = 350 days/year ED <2 (Exposure duration, age <2 years) = 2 years ADAF<2 (Age-dependent adjustment factor = 10, unitless for cancer potency, age <2 years) ED 2-6 (Exposure duration, age 2-6 years) = 4 years ADAF2-6 (Age-dependent adjustment factor = 3, unitless for cancer potency, age 2-6 years) ED 6-16 (Exposure duration, age 6-16 years) = 10 years ADAF6- (Age-dependent adjustment factor = 3, unitless 16 for cancer potency, age 6-16 years) ED 16-32 (Exposure duration, age 16-32 = 16 years years) ADAF16- (Age-dependent adjustment factor = 1, unitless 32 for cancer potency, age 16-32 years) 3 PEFres (Particulate emission factor) = source size-specific, m /kg

13. EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ  AT RfCRSC PSIV  res nc  1    EDres EFres    PEFres  where, PSIVnc (Particulate soil inhalation = chemical and source size-specific, value) µg/kg or ppb THQ (Target hazard quotient) = 1 ATres (Averaging time) = 11,680 days RfC (Reference concentration) = chemical-specific, µg/m3

99 2017 MR 22 – December 15, 2017

RSC (Relative source contribution) = chemical-specific or 1 EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year 3 PEFres (Particulate emission factor) = source size-specific, m /kg

14. EQUATION FOR DEVELOPMENTAL EFFECTS - CHILD:

THQ AT RfC RSC PSIV  child dev dev  1  ED EF    child res PEF   dev  where, PSIVde (Particulate soil inhalation = chemical and source size-specific, v value) µg/kg or ppb THQ (Target hazard quotient) = 1 ATchild (Averaging time) = 2,190 days 3 RfCdev (Reference concentration) = chemical-specific, µg/m RSC (Relative source contribution) = 1 or chemical-specific EDchild (Exposure duration) = 6 years EFres (Exposure frequency) = 350 days/year 3 PEFdev (Particulate emission factor) = source size-specific, m /kg

15. EQUATION FOR DEVELOPMENTAL EFFECTS - PREGNANT RESIDENT

THQ  AT RfC RSC PSIV  preg dev dev  1    EDpreg EFpreg     PEFdev  where, PSIVdev (Particulate soil inhalation = chemical and source size-specific, value) µg/kg or ppb THQ (Target hazard quotient) = 1 ATpreg,F (Averaging time, full-term = 280 days or chemical-specific T pregnancy) ATpreg,F (Averaging time, single event = 1 day or chemical-specific T exposure during pregnancy) 3 RfCdev (Reference concentration) = chemical-specific, µg/m RSC (Relative source contribution) = 1 or chemical-specific EDpreg,F (Exposure duration, full-term = 0.767 year or chemical-specific T pregnancy) EDpreg,S (Exposure duration, single = 1 day or chemical-specific E event exposure during pregnancy) EFpreg,FT (Exposure frequency, full- = 268.5 days/year or chemical specific term pregnancy) EFpreg,SE (Exposure frequency, single = 1 day/day or chemical specific event exposure during pregnancy)

100 2017 MR 22 – December 15, 2017

3 PEFdev (Particulate emission factor) = source size-specific, m /kg

NONRESIDENTIAL: 16. EQUATION FOR CARCINOGENic EFFECTS: TR  AT PSIV  ca ca  1    IURF EFnr EDnr     PEFnr  where, PSIVc (Particulate soil inhalation value) = chemical and source size- a specific, µg/kg TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific, (µg/m3)-1 EFnr (Exposure frequency) = 238 days/year EDnr (Exposure duration) = 20 years 3 PEFnr (Particulate emission factor) = source size-specific, m /kg

17. EQUATIONS FOR NONCARCINOGENIC EFFECTS:

THQ  AT  RfC  RSC PSIV  nr nc  1  ED  EF    nr nr  PEF   nr  where, PSIVnc (Particulate soil inhalation value) = chemical and source size- specific, µg/kg or ppb THQ (Target hazard quotient) = 1 ATnr (Averaging time) = 7,300 days RfC (Reference concentration) = chemical-specific, µg/m3 RSC (Relative source contribution) = 1 or chemical-specific EDnr (Exposure duration) = 20 years EFnr (Exposure frequency) = 238 days/year 3 PEFnr (Particulate emission factor) = source size-specific, m /kg

18. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT WORKER:

THQ AT RfC RSC PSIV  dev dev dev  1  ED EF    dev dev PEF   dev  where, PSIVdev (Particulate soil inhalation = chemical and source size-specific, value) µg/kg or ppb THQ (Target hazard quotient) = 1 ATdev,FT (Averaging time, pregnant = 280 days or chemical specific worker, full-term pregnancy)

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ATdev,SE (Averaging time, pregnant = 1 day or chemical specific worker, single event exposure during pregnancy) 3 RfCdev (Reference concentration) = chemical-specific, µg/m RSC (Relative source contribution) = 1 or chemical-specific EDdev,FT (Exposure duration, pregnant = 0.767 year or chemical-specific worker, full-term pregnancy) EDdev,SE (Exposure duration, pregnant = 1 day or chemical-specific worker, single event exposure during pregnancy) EFdev,FT (Exposure frequency, pregnant = 183 days/year or chemical-specific worker, full-term pregnancy) EFdev,SE (Exposure frequency, pregnant = 1 day/day or chemical-specific worker, single event exposure during pregnancy) 3 PEFdev (Particulate emission factor, = source size-specific, m /kg pregnant worker)

The particulate emission factors (PEF) shall be calculated for paved roads or driveways pursuant to equation 19 of this rule.

RESIDENTIAL AND NONRESIDENTIAL: 19. EQUATION FOR PEF:

1 PEF  Q/C  Ew where, PEF (Particulate emission factor) = 5.014E+7 for residential or nonresidential ½ acre source size, or source size-specific, m3/kg Q/C (Dispersion factor for 1/2 acre) = 42.45, g/m2-sec per kg/m3 Ew (Emission due to wind erosion) = 8.466E-07 g/m2 per sec (residential) = 8.466E-07 g/m2 per sec (nonresidential)

The emissions due to wind erosion (Ew) shall be calculated pursuant to equation 20 of this rule:

If a site has unpaved roads or driveways, the generic PEF developed under equation 19 is not applicable and site-specific criteria must be calculated based on a site-specific PEF using the following equation.

Site-specific PEF: 1 PEF  Q/C  Ew  Ev

102 2017 MR 22 – December 15, 2017 where, PEF (Particulate emission factor) = m3/kg Q/C (Dispersion factor for site source = g/m2-sec per kg/m3 size) Ew (Emission due to wind erosion) = g/m2 per sec Ev (Emission due to vehicle traffic on = g/m2 per sec unpaved road for site source size)

RESIDENTIAL AND NONRESIDENTIAL: 20. EQUATIONS FOR EMISSION DUE TO WIND EROSION (Ew):

3 0 036 2 1  U  . g/m hr   V   mz  Fx  U  (a) Ew  3 600  adj  , sec/hr where, Ew (Emission due to wind erosion) = 8.466E-07 g/m2 per sec (residential) = 8.466E-07 g/m2 per sec (nonresidential) V (Vegetative cover) = 0.5, unitless (residential) = 0.5, unitless (nonresidential) (Michigan annual wind speed = 6.56 m/sec U mz adjusted to 7.0 meters) Utadj (Equivalent threshold friction = 11.319 m/sec (residential) value of wind speed at 7.0 m) = 11.319 m/sec (nonresidential) F(x) (Function of x based on Cowherd, = 0.87, unitless (residential) 1985) = 0.87, unitless (nonresidential)

0.15  z  (b) Umz  Um     h  where, (Michigan annual wind speed = 6.56 m/sec U mz adjusted to 7.0 meters) (Michigan annual wind speed at = 6.92 m/sec U m measurement height h) h (Michigan wind speed = 10 m measurement height) z (Height above test surface) = 7 m

 Ut   z  (c)   Ut adj     ln   Cf  0.4   z0  where, Utadj (Equivalent threshold friction = 11.319 m/sec (residential)

103 2017 MR 22 – December 15, 2017

value of wind speed at 7.0 m) = 11.319 m/sec (nonresidential) Ut (Threshold friction value of wind = 0.5 m/sec (residential) speed for a residential soil aggregate size of 0.5 mm For a nonresidential soil aggregate = 0.5 m/sec (nonresidential) size of 0.5 mm Cf (Correction factor for non- = 1.25, unitless or default erodible elements) z (Height above test surface) = 7 m z0 (Roughness height) = 0.005 m

 Ut adj  (d) x  0.886     Umz  where, x Cowherd derived x = 1.529, unitless (residential) = 1.529, unitless (nonresidential) Utadj (Equivalent threshold friction value of wind speed at 7.0 m) = 11.3 m/sec (residential) = 11.3 m/sec (nonresidential) (Michigan annual wind speed U mz adjusted to 7.0 meters) = 6.56 m/sec (residential) = 6.56 m/sec (nonresidential)

(12) Facility-specific values of the following input values may be substituted for the generic input values pursuant to R 299.7: (a) Dry soil bulk density (b). (b) Soil water-filled porosity (w). (c) Soil air-filled porosity (a). (13) Site-specific values of the following input values may be substituted for the generic residential criterion input values for department approval as unrestricted residential use: (a) Fraction of organic carbon in soil (foc). (b) Dispersion factor (Q/C). (c) Wind speed (Ew).

EQUATIONS FOR CARCINOGENS:

TR  AT VSIC  IURF EF  ED  (1 VF) where, VSIC (Volatile soil inhalation = chemical-specific, ug/kg or ppb criterion) TR (Target risk level) = 10-5

104 2017 MR 22 – December 15, 2017

AT (Averaging time) = 25,550 days (70 years x 365 days/year) IURF (Inhalation unit risk factor) = chemical-specific (ug/m3)-1 EF (Exposure frequency) = 350 days/year ED (Exposure duration) = 30 years VF (Volatilization factor) = chemical-specific, m3/kg

and, TR  AT PSIC  IURF EF ED (1 PEF) where, PSIC (Particulate soil inhalation = chemical-specific, ug/kg or ppb criterion) TR (Target risk level) = 10-5 AT (Averaging time) = 25,550 days (70 years x 365 days/year) IURF (Inhalation unit risk factor) = chemical-specific (ug/m3)-1 EF (Exposure frequency) = 350 days/year ED (Exposure duration) = 30 years PEF (Particulate emission factor) = chemical-specific, m3/kg

EQUATIONS FOR NONCARCINOGENS:

THQ  AT VSIC  EF  ED  (1 ITSL 1 VF) where, VSIC (Volatile soil inhalation = chemical-specific, ug/kg or ppb criterion) THQ (Target hazard quotient) = 1 AT (Averaging time) = 10,950 days (30 years x 365 days/year) EF (Exposure frequency) = 350 days/year ED (Exposure duration) = 30 years ITSL (Initial threshold screening = chemical-specific, ug/m3 level) VF (Volatilization factor) = chemical-specific, m3/kg

and, THQ  AT PSIC  EF  ED  (1 ITSL  1 PEF) where, PSIC (Particulate soil inhalation = chemical-specific, ug/kg or ppb criterion)

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THQ (Target hazard quotient) = 1 AT (Averaging time) = 10,950 days (30 years x 365 days/year) EF (Exposure frequency) = 350 days/year ED (Exposure duration) = 30 years ITSL (Initial threshold screening = chemical-specific, ug/m3 level) PEF (Particulate emission factor) = chemical-specific, m3/kg

(3) The soil to air volatilization factor (VF) relates the concentration of a contaminant in the soil to the concentration of volatilized contaminant in the ambient air. If the vertical extent of the contaminant source has not been characterized, then the VF shall be calculated based on the infinite equation presented in subdivision (a) of this subrule. If the vertical extent of the contaminant source has been adequately characterized throughout the facility, then the VF shall be calculated either by the finite source equation presented in subdivision (b) of this subrule or the mass balance equation presented in subdivision (c) of this subrule, whichever yields the highest VSIC.

ave (a) VF  (Q/C)  (1/Js ) ave Js , using the infinite source model shall be calculated as follows:

ave 1/2 4 2 2 Js  b (4D A /t)  10 cm /m and DA shall be calculated as:

3.33 3.33 2 [(a Da (H  TAF)  w Dw )/n ] DA  bK d  w  a (H  TAF) where, VF (Volatilization factor) = chemical-specific, m3/kg ave 2 Js (Normalized average flux from soil) = chemical-specific, g/m - second 2 DA (Apparent diffusivity) = chemical-specific, cm /second Q/C (Dispersion factor for 1/2 acre) = 82.33, g/m2-second per kg/m3 T (Exposure time) = seconds (ED x 3.1536E+7 seconds/yr) a (Soil air-filled porosity) = 0.28 Lair/Lsoil N (Total soil porosity) = 0.43 Lpore/Lsoil w (Soil water-filled porosity) = 0.15 Lwater/Lsoil 3 b (Dry soil bulk density) = 1.5 g/cm 2 Da (Diffusivity in air) = chemical-specific, cm /second 2 Dw (Diffusivity in water) = chemical-specific, cm /second H (Dimensionless Henry’s law constant, = chemical-specific, unitless where H = HLC x 41)

106 2017 MR 22 – December 15, 2017

HLC (Henry’s law constant at 250 C) = chemical-specific, atm- m3/mol TAF (Temperature adjustment factor) = 0.5

3 Kd (Soil-water partition coefficient) = chemical-specific, cm /g 3 For organic compounds = Koc (cm /g) x foc (g/g) For inorganic compounds = chemical-specific, cm3/g 3 Koc (Soil organic carbon partition = chemical-specific, cm /g coefficient) foc (Organic carbon content of soil) = 0.006 g/g (0.6%)

(b) The simplified finite source model equation for VF shall be calculated as follows:

ave VF  (Q/C)  (C 0  b )  (1 J s ) and, 1/2 2 Js CoDA t 1expds 4DAt

where, VF (Volatilization factor) = chemical-specific, m3/kg Q/C (Dispersion factor for 1/2 acre) = 82.33, g/m2-second per kg/m3 3 C0 (Uniform contaminant = 1.5 E-6 g/cm concentration at t=0) 3 b (Dry soil bulk density) = 1.5 g/cm ave 2 Js (Normalized average flux from = chemical-specific, g/m - soil) second 2 Js (Instantaneous flux from soil at = chemical-specific, g/m - time t) second DA (Apparent diffusivity - see equation = chemical-specific, above) cm2/second T (Time) = seconds ds (Thickness of source) = site-specific, meters exp(p) (The base of the natural logarithm = ep raised to power (p))

(c) Mass balance VF shall be calculated as follows:

AT (3.1510-7 seconds/year) VF  Q/C  6 b  ds 10 g/Mg where, VF (Volatilization factor) = chemical-specific, m3/kg Q/C (Dispersion factor for 1/2 acre) = 82.33, g/m2-second per kg/m3

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AT (Exposure period) = scenario-specific, years 3 b (Dry soil bulk density) = 1.5 mg/m ds (Average source depth) = site-specific, meters

(4) The particulate emission factor shall be calculated as follows:

PEF Q/C 1 (Ew (1 V))  Ev

where,

PEF (Particulate emission factor) = chemical-specific, m3/kg Q/C (Dispersion factor for 1/2 acre) = 82.33, g/m2-second per kg/m3 Ew (Emission due to wind) = g/m2 per second Ev (Emission due to vehicle traffic) = g/m2 per second V (Vegetative cover) = 0.5 (50%), unitless

(5) VSIC and PSIC for nonresidential facilities shall be calculated as follows, except as provided in R 299.34(3):

EQUATIONS FOR CARCINOGENS:

TR  AT  AIR VSIC  IURF  EF  ED  (1/VF)

where,

VSIC (Volatile soil inhalation criterion) = chemical-specific, ug/kg or ppb TR (Target risk level) = 10-5 AT (Averaging time) = 25,550 days (70 years x 365 days/year) AIR (Adjusted inhalation rate) = (20 m3/day)/(10 m3/day) IURF (Inhalation unit risk factor) = chemical-specific (ug/m3)-1 EF (Exposure frequency) = 245 days/year ED (Exposure duration) = 21 years VF (Volatilization factor) = chemical-specific, m3/kg

and, TR  AT  AIR PSIC  IURF  EF  ED  (1/PEF)

where,

PSIC (Particulate soil inhalation criterion) = chemical-specific, ug/kg or ppb

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TR (Target risk level) = 10-5 AT (Averaging time) = 25,550 days (70 years x 365 days/year) AIR (Adjusted inhalation rate) = (20 m3/day)/(10 m3/day) IURF (Inhalation unit risk factor) = chemical-specific (ug/m3)-1 EF (Exposure frequency) = 245 days/year ED (Exposure duration) = 21 years PEF (Particulate emission factor) = chemical-specific, m3/kg

EQUATIONS FOR NONCARCINOGENS:

THQ  AT VSIC  EF ED  (1/ITSL 1/VF) where,

VSIC (Volatile soil inhalation criterion) = chemical-specific, ug/kg or ppb THQ (Target hazard quotient) = 1 AT (Averaging time) = 7,665 days (21 years x 365 days/year) EF (Exposure frequency) = 245 days/year ED (Exposure duration) = 21 years ITSL (Initial threshold screening level) = chemical-specific, ug/m3 VF (Volatilization factor) = chemical-specific, m3/kg

and,

THQ  AT PSIC  EF ED  (1/ITSL 1/PEF)

where,

PSIC (Particulate soil inhalation criterion) = chemical-specific, ug/kg or ppb THQ (Target hazard quotient) = 1 AT (Averaging time) = 7,665 days (21 years x 365 days/year) EF (Exposure frequency) = 245 days/year ED (Exposure duration) = 21 years ITSL (Initial threshold screening level) = chemical-specific, ug/m3 PEF (Particulate emission factor) = chemical-specific, m3/kg

(6) The generic SIC are calculated for a source area size of 1/2 acre. The generic SIC shall be adjusted for other source area sizes by multiplying the generic SIC by the modifiers given in the following table. Where the actual source area size falls between

109 2017 MR 22 – December 15, 2017 the sizes given in this subrule, generic SIC shall be multiplied by the modifier for the next largest source size.

Modifiers Source Size Q/C (ft2 or acres) (g/m2-s per kg/m3) Modifier 400 ft2 261.26 3.17 1000 ft2 180.76 2.2 2000 ft2 144.91 1.76 ¼ acre 94.56 1.15 ½ acre 82.33 1 1 acre 71.74 0.87 2 acres 63.51 0.77 5 acres 54.62 0.66 10 acres 49.13 0.6 32 acres 41.55 0.5 100 acres 35.66 0.43

(7) Facility-specific measurements of the following parameters may be substituted for the generic assumptions and still allow the facility to satisfy the categorical criteria in section 20120a(1)(a) to (e) of the act: (a) Dry soil bulk density (b). (b) Soil water-filled porosity (w). (c) Soil air-filled porosity (a). (d) Fraction of organic carbon in soil (foc). (e) Emission due to wind (Ew). (f) Dispersion factor (Q/C).

Facility-specific measurements shall be based on representative characterization. Documentation of all facility-specific values shall be provided in the response activity plan, no further action report, or other response activity documentation. (8) A person who is implementing response activity may demonstrate compliance with the generic criteria developed under this rule through the collection and analysis of ambient air samples within the facility boundaries, if the hazardous substance concentration in surficial soil is representative of facility conditions.

R 299.27 Volatilization to indoor air screening levels and criteria Rule 27. (1). As used in this rule: (a) “Air exchange rate” means the rate of air flow into and out of a building that may include air flow through a window, doorway, intake, mechanical ventilation, and exhaust, or other adventitious opening. (b) “Acceptable air concentration” or “AAC” means the concentration of a hazardous substance in indoor air that represents an acceptable inhalation exposure risk to human health.

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(c) “Capillary zone” means the zone immediately above the water table within which the groundwater is drawn by capillary forces and the fluid is under tension. (d) “Conceptual site model” or “CSM” means a written or illustrative representation, or both, of the surface and subsurface conditions. The CSM includes the physical, chemical, and biological processes that control the transport, migration, and potential impacts of contamination to a human receptor. (e) “Lateral inclusion zone” means the horizontal distance beyond a vapor source that may make a property or structure vulnerable to the migration of vapors. It is identified as the following: (i) Thirty feet from the extent of a vapor source solely comprised of petroleum. (ii) One hundred feet from the extent of all other vapor sources. (iii) When the concentration of a hazardous substance in any media exceeds the unrestricted generic residential criterion within these distances the vapor source shall be further evaluated. (f) “Petroleum vertical separation distance” means the vertical distance from a petroleum vapor source to an existing or potential building foundation. (g) “Uninhabitable residential basement” means a basement where all the following conditions exist: (i) As measured from floor to ceiling, the height of the basement is less than 2.032 meters or 80 inches in every part. (ii) There is no existing, or the potential for the installation of, a bathroom, water fixture, or laundry area. (iii) The basement does not contain an emergency egress or rescue opening. (iv) No evidence of human habitation. (h) “Vapor” or “Soil gas” means gas found in the air space between soil particles. (i) “Vapor cloud” means a hazardous substance in the vapor phase with no colocated contamination in the soil or groundwater. (j) “Vapor intrusion” means a process by which a hazardous substance from a vapor source has migrated or has the potential to migrate through the subsurface or preferential pathways, or both, into an existing or potential structure. (k) “Vapor source” means a hazardous substance in an environmental medium that may form vapors that have the potential to migrate. (l) “Vertical separation distance” means the vertical distance between the vapor source and an existing or potential structure. The vertical separation distance for groundwater shall consider seasonal variations of the first encountered contaminated groundwater elevation and is the lesser of the following: (i) The distance between the top of the capillary zone of the first encountered contaminated groundwater and the bottom of the structure. (ii) The distance between the first encountered contaminated groundwater and the bottom of the foundation and subsurface utilities that may be present beneath the structure. (m) “Volatilization to indoor air Tier 1 screening level” or “VI Tier 1 screening level” means the initial screening levels used to identify the presence of a hazardous substance as a vapor source. (n) “Volatilization to indoor air Tier 2 generic criterion” or “VI Tier 2 generic criterion” means the VI Tier 1 screening level that incorporates facility-specific

111 2017 MR 22 – December 15, 2017 geological and hydrogeological site conditions that establish the generic cleanup criteria for unrestricted residential use. (o) “Volatilization to indoor air Tier 3A generic criterion” or “VI Tier 3A generic criterion” means the VI Tier 2 generic criterion that also incorporates the use of facility-specific land use or building information, or both, that require a land or resource use restriction. (p) “Volatilization to indoor air Tier 3B site-specific criterion” or “VI Tier 3B site- specific criterion” means a criterion developed using an alternate method or model approved by the department. (2) The generic cleanup criteria based on inhalation of hazardous substance vapors volatilizing from a vapor source to indoor air is called volatilization to indoor air criteria (“VIAC”) and the pathway is referred to as the volatilization to indoor air pathway (“VIAP”). All of the following apply: (a) Indoor inhalation of hazardous substance vapors volatilizing to indoor air from a vapor source is considered a relevant pathway for volatile hazardous substances. (b) The VIAP is relevant for properties within the lateral inclusion zone. (c) The process to assess the VIAP is the VI Tier process shown in figure 1 of this rule. The process is presented as a sequential step-by-step approach; parties may skip tiers as appropriate to the conditions at a facility or the circumstances of an investigation. (d) The VIAP shall be evaluated using soil, groundwater, and vapor samples to satisfy the screening levels or criteria for each media pursuant to the VI Tier process and is based upon the following: (i) The CSM is based on representative characterization of the surface and subsurface conditions to evaluate the VIAP. (ii) The location of the media sample is aligned with the location of the vapor source within the lateral inclusion zone and is appropriate for evaluating the VIAP. (iii) A vapor source may be present and represent a risk to human health when the concentration of a hazardous substance in soil or groundwater does not exceed the criteria that are based on the target detection limit. (iv) A vapor sample may be used as the best available information to represent in- situ conditions at the facility for evaluating a vapor source and the ability to migrate when comparing samples that are colocated or are similarly located. (3) The development of the screening level or generic VIAC for shallow groundwater where the vertical separation distance is less than or equal to 0 centimeters uses the assumptions in table 1 of this rule and assumes all of the following: (a) Any structure present or planned to be constructed at the facility has a concrete block or poured concrete walls and concrete floor. If the present or planned structure is not constructed with a block or poured concrete walls and concrete floor, the screening level or generic VIAC developed pursuant to this rule does not apply and a site-specific evaluation shall be conducted. (b) The direct diffusion of a volatile hazardous substance from the water into the indoor air is established based on the equations identified in R 299.27(13)(a) to (b). All of the following apply: (i) A volatile hazardous substance designated as single event in R 299.49(1)(DD) or for short-term exposure in R 299.49(1)(EE) and (FF) shall be based upon a single

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event where the first encountered groundwater enters the structure and the direct diffusion of a volatile hazardous substance from the water into the indoor air is established based on the equations identified in R 299.27(13)(b). (ii) A volatile hazardous substance not designated as a single event in R 299.49(1)(DD) or for short-term exposure in R 299.49(1)(EE) and (FF) is based on the sum of the following: (A) Direct diffusion of a volatile hazardous substance into indoor air from groundwater occurs from the weighted contribution from the surface area of a sump and the extent of cracks in the building foundation footprint. This area is represented by 1 square meter. The direct diffusion is established by using the equations identified in R 299.27(13)(b). (B) Diffusion of a volatile hazardous substance from the groundwater through the concrete into indoor air occurs from the weighted contribution across the remaining area of the floor of the structure using an attenuation factor of 0.03 and the equations identified in R 299.27(13)(a). (iii) The direct diffusion into indoor air from an area greater than 1 square meter requires a site-specific evaluation. (4) The development of the screening level or generic VIAC for groundwater where the vertical separation distance is greater than 0 centimeters uses the assumptions in table 1 of this rule and assumes all of the following: (a) Any structure present or planned to be constructed at the facility has a concrete block or poured concrete walls and concrete floor. The base of the floor considering the thickness of the concrete is not more than 2 meters below ground surface. If the present or planned structure is not constructed with a block or poured concrete walls and concrete floor, or the base of the floor is more than 2 meters below ground surface, the screening level or generic VIAC developed pursuant to this rule does not apply and a site-specific evaluation shall be conducted. (b) The diffusion of a volatile hazardous substance from groundwater into the indoor air is established based on the equations identified in R 299.27(13)(a). (5) The development of the screening level or generic VIAC for vapor uses the assumptions in table 1 of this rule and assumes all of the following: (a) A vapor sample that is representative of a vapor source can be used to evaluate the VIAP. If a vapor sample can not be collected due to site-specific conditions, a site-specific evaluation shall be completed to evaluate alternate means to demonstrate compliance. (b) A vapor source that is less than 1 meter from an existing or potential structure uses an attenuation factor of 0.03. (c) When the vertical separation is greater than 1 meter, the VIAP may be evaluated using the equations of subrule (13)(d) of this rule based on all of the following: (i) A vapor source does not exist between the compliance point and an existing or potential structure. (ii) The distance to a vapor source used in the equations of subrule (13)(d) is the distance from an existing or a potential structure to the compliance point. (6) The development of the screening level or generic VIAC for soil uses the assumptions in table 1 of this rule, the equations of subrule (13)(c) of this rule, and

113 2017 MR 22 – December 15, 2017 is based on the soil type being homogeneous and isotropic. When heterogeneous soils are present the VIAC may be developed pursuant to R 299.7(3)(iii). (7) When a hazardous substance does not have sufficient chemical-physical generic input values available in the tables of R 299.50 to allow the development of a screening level or generic criterion using the equations of this rule, the screening level or generic VIAC may be developed using the following: (a) If the department cannot develop a screening level or generic criterion where the vertical separation distance is greater than 0 centimeters using the equations identified in R 299.27(13)(a), the screening level or generic criterion where the vertical separation distance is less than or equal to 0 centimeters shall be developed using the equations identified in R 299.27(13)(b) and the assumptions in table 1 of this rule. Alternatively, a person may evaluate the VIAP using VI Tier 3B site- specific criteria. (b) If the department cannot develop a screening level or generic criterion for vapor using the equations of this rule, and the hazardous substance has sufficient input values to develop an AAC, an attenuation factor of 0.03 shall be used. Alternatively, a person may evaluate the VIAP using VI Tier 3B site-specific criteria. (8) The VIAP is evaluated using VI Tier 1 screening levels. VI Tier 1 screening levels identify concentrations that may represent a vapor source or a vapor cloud without any geological or hydrogeological information specific to a facility. All of the following apply: (a) The VI Tier 1 screening levels are applicable at all depths and are based on generic input values that represent the following: (i) Shallow groundwater where the vertical separation distance is less than or equal to 0 centimeters in accordance with subrule (3) of this rule. (ii) Vapor pursuant to subrule (5)(a) to (b) of this rule. (iii) A soil type of sand pursuant to R 299.7 and the generic input values in table 1 of this rule. (b) A person may use the screening level as the criterion to evaluate the VIAP when no further facility data is available. (c) If concentrations in environmental media exceed VI Tier 1 screening levels then the person proposing or implementing response activity shall evaluate whether additional response activity is required to assess the vapor source for the VIAP pursuant to this rule. (9) If the concentration of a hazardous substance in environmental media exceeds VI Tier 1 screening level, the VIAP may be evaluated using VI Tier 2 generic unrestricted residential criteria. The VI Tier 2 generic unrestricted residential criteria identify a vapor source. The generic unrestricted residential VIAC are based on the following: (a) Department-approved soil and soil temperature facility-specific input values are allowed pursuant to R 299.7. When no soil information has been obtained during an investigation the facility-specific input values are those listed for sand in table 1 of R 299.7. (b) When the depth to groundwater is 3 meters or less below the ground surface, the development of the generic VIAC for shallow groundwater is pursuant to subrule (3) of this rule.

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(c) When the depth to groundwater is greater than 3 meters below the ground surface the development of the generic VIAC is pursuant to subrule (4) of this rule. (d) The generic VIAC for vapor is pursuant to subrule (5) of this rule. (e) Department-approved input values provided in table 1 of this rule identify additional generic input values to develop the VI Tier 2 generic criteria. (f) The calculated value for a hazardous substance based upon shallow groundwater is considered protective when it is greater than the calculated value for groundwater with a vertical separation distance greater than 0 centimeters. (10) If the concentration of a hazardous substance in environmental media exceeds VI Tier 1 screening levels, VI Tier 2 generic unrestricted residential criteria, or both, the VIAP may be evaluated using VI Tier 3A generic criteria. VI Tier 3A generic criteria represent restricted categorical criteria and are based on the following: (a) The generic VIAC for soil is pursuant to subrule (9)(a) of this rule. (b) The generic VIAC for shallow groundwater is pursuant to subrule (3) of this rule. (c) The generic VIAC for groundwater where the vertical separation distance is greater than 0 centimeters is pursuant to subrule (4) of this rule. (d) The generic VIAC for vapor is pursuant to subrule (5) of this rule (e) The environmental input values specific to the facility from subrule (9) of this rule. (b) Department-approved facility-specific input values for land use and building information as identified in table 1 of this rule. (11) The VIAP may be evaluated with VI Tier 3B site-specific criterion pursuant to sections 20120a(2) and 20120b of the act, using any of the following: (a) The equations in subrules (13) and (14) of this rule and associated input values, with data collected from the facility that is demonstrated to be representative of site-specific conditions and has undergone a sensitivity and validation analysis that will determine and evaluate all of the following: (i) The parameters that require additional information to reduce output uncertainty. (ii) The inputs that contribute most to output variability. (iii) The parameters that are most highly correlated with the output. (iv) The change in the output that results from changing a given input parameter. (v) The expected reliability of the identified parameters. (b) The actual building parameters including air exchange rate, enclosed-space floor thickness, enclosed-space floor length, enclosed-space floor width, and enclosed-space height, with an analysis that includes all of the following: (i) An evaluation of the smaller areas contained within the structure. (ii) An evaluation of how the footings, walls, and air exchange patterns impact the data. (iii) An evaluation of whether the inputs used are representative of the actual site conditions. (c) Different models or methods may be reviewed and approved by the department to determine that the model or method is appropriate to evaluate the VIAP based on an analysis as identified in subdivisions (a) and (b) of this subrule. VIAP models or methods are available to evaluate the following conditions:

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(i) Heterogeneous or multilayer soil present at a property. (ii) A vapor source that consists solely of dissolved phase petroleum. (iii) A NAPL vapor source. (iv) A finite vapor source in unsaturated soil for circumstances where the vertical and horizontal extent of a vapor source throughout the facility has been defined based upon all applicable VI Tier 2 generic criteria. (12) A VI Tier 3B evaluation of a release that is solely petroleum products may utilize a petroleum vertical separation distance that is based upon all of the following: (a) The petroleum vertical separation distance represents the minimum distance between a petroleum vapor source and a building foundation that is needed to effectively biodegrade hydrocarbons below a level of concern for a current or potential future structure. (b) The release being evaluated contains no non-petroleum volatile compounds and represents solely a petroleum release. (c) All soil contamination associated with a release from a petroleum product is considered to be petroleum non-aqueous phase liquid unless by using department approved methods, a demonstration can be made that a non-aqueous phase liquid is not present. (d) Meeting a petroleum vertical separation distance does not remove the need for land or resource use restrictions to prevent future exposure unless a demonstration can be made that the site would remain protective without a land or resource restriction. (e) The petroleum vertical separation distance shall consider seasonal variations, if appropriate, and shall be the greater of the following: (i) Fifteen feet vertically from a petroleum non-aqueous phase liquid source regardless of the NAPL state. (ii) Five feet vertically from a dissolved-phase petroleum source. (13) The volatilization to indoor air values are determined by the following series of equations, except as provided in R 299.34, and in the footnotes of the generic cleanup criteria tables in R 299.49. The toxicological, chemical-specific, and chemical-physical generic input values are provided in R 299.50, except as provided in R 299.34, and in the footnotes of the generic cleanup criteria tables in R 299.49. The soil type-specific values and other inputs for a VI Tier 2 and VI Tier 3A generic criteria are identified in table 1 of this rule and table 1 and 2 of R 299.7. (a) The volatilization to indoor air value based on diffusion from the groundwater is determined by the following equations:

1. EQUATION FOR CALCULATION OF THE GROUNDWATER HEALTH- BASED CONCENTRATION:

AAC VI  1000 GW  , L  3 H'TS       m  where, VIGW (Volatilization to indoor air = chemical-specific, g/L

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concentration for groundwater) AAC (Acceptable air concentration) = chemical-specific, g/m3-v α (Steady-state attenuation = unitless (Equation 6 and table 1 coefficient) of this rule) H′TS (Henry’s law constant at the = chemical-specific, dimensionless system (groundwater) (Equation 4) temperature)

2. THE RELATIONSHIP OF THE ATTENUATION COEFFICIENT TO THE STEADY-STATE VAPOR PHASE CONCENTRATION OF THE HAZARDOUS SUBSTANCE IN THE BUILDING:

C building  α  C source where, Cbuilding (Vapor concentration in = chemical-specific (subrule (11) building using the AAC) of this rule), g/m3-v Csource (Vapor concentration at the = g/m3-v (Equation 3) vapor source) α (Steady-state attenuation = unitless (Equation 6 and table 1 coefficient) of this rule)

3. THE RELATIONSHIP OF THE GROUNDWATER VAPOR SOURCE CONCENTRATION TO THE GROUNDWATER CONCENTRATION:

Csource  H'TS Cw where, Csource (Vapor concentration at the = g/m3-v vapor source) H′TS (Henry’s law constant at the = chemical-specific, dimensionless system (groundwater) (Equation 4) temperature) Cw (Groundwater concentration = g/m3-w using 1 g/L × 1,000 L/m3 conversion)

4. EQUATION FOR THE DIMENSIONLESS FORM OF THE HENRY’S LAW CONSTANT AT THE SYSTEM TEMPERATURE:

1 1  HV,TS   exp    HLC  Rc  TS TR  H'TS  R  TS where, H′TS (Henry’s law constant at the = chemical-specific, dimensionless system temperature) Hv, TS (Enthalpy of vaporization at the = chemical-specific, cal/mol

117 2017 MR 22 – December 15, 2017

system temperature) (Equation 5) TS (System temperature) = 283.15 K or facility-specific TR (Henry’s law constant reference = 298.15 K temperature) HLC (Henry’s law constant at the = chemical-specific, atm-m3/mol reference temperature) RC (Gas constant) = 1.9872 cal/mol-K R (Gas constant) = 8.206E-05 atm-m3/mol-K

5. EQUATION FOR ENTHALPY OF VAPORIZATION:

Y    1 TS TC  ΔHv,TS  ΔHv,b      1 TBP TC  where, Hv,TS (Enthalpy of vaporization at the = chemical-specific, cal/mol system temperature) Hv,b (Enthalpy of vaporization at the = chemical-specific, cal/mol normal boiling point) TS (System temperature) = 283.15 K or facility-specific TC (Critical Temperature) = chemical-specific, K TBP (Standard boiling point) = chemical-specific, K Y (Constant) = unitless

Y (constant) is established as a function of the ratio TBP/TC such that: if TBP/TC < 0.57, Y is 0.30; if TBP/TC is between 0.57 and 0.71, Y is established as 0.74(TBP/TC) - 0.116; and if TBP/TC > 0.71, Y is 0.41.

6. EQUATION FOR AN INFINITE VAPOR SOURCE ASSUMING STEADY STATE MASS TRANSFER:

 Deff  A   Q L   T B   exp soil crack       Qbuilding LT  Dcrack  Acrack        Q L   Deff  A   Deff  A    Q L  1 exp  soil crack    T B    T B  exp soil crack    D  A   Q L   Q L  D  A    crack crack   building T   soil T    crack crack  

where,  (Steady-state attenuation = unitless coefficient) eff 2 DT (Total overall effective diffusion =cm/sec (Equation 7) coefficient) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)]) 3 Qbuilding (Building ventilation rate) = cm /sec (Equation 14)

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LT (Vapor source-building = cm (table 1 of this rule) separation) 3 Qsoil (Volumetric flow rate of soil gas =cm/sec (Equation 15) into the enclosed space) Lcrack (Enclosed space foundation or = cm (table 1 of this rule) slab thickness) 2 Acrack (Area of total cracks: Acrack = =cm(LB & WB in table 1 of this 2w(LB + WB)) rule) 2 Dcrack (Effective diffusion coefficient =cm/sec (assumed equivalent to eff through the cracks) Dv , Equation 8)

Equation 6 contains the exponent of the following dimensionless group:

 Qsoil Lcrack     Dcrack  Acrack  where, 3 Qsoil (Volumetric flow rate of soil gas =cm/sec (Equation 15) entering the enclosed space of a building) Lcrack (Enclosed space foundation or = cm (table 1 of this rule) slab thickness) 2 Dcrack (Effective diffusion coefficient =cm/sec (assumed equivalent to eff through the cracks) Dv , Equation 8) 2 Acrack (Area of total cracks: Acrack = =cm (LB & WB in table 1 of this 2w(LB + WB)) rule)

This dimensionless group represents the equivalent Peclet number for transport through the building foundation. As the dimensionless group approaches infinity and if the exponent of the equation identified above is too great to be calculated then the attenuation factor is established as:

eff  DT  Lcrack    Dcrack  Acrack    eff 1  DT  AB      Qsoil  LT  where, α (Steady-state attenuation = unitless coefficient) eff (Total overall effective diffusion = chemical-specific, cm2/sec (as DT coefficient) established in Equation 7) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 of below grade: AB = [(LB × WB) + this rule) 2(LF x LB) + 2(LF x WB)]) 3 Qbuilding (Building ventilation rate) = cm /sec (Equation 14)

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3 Qsoil (Volumetric flow rate of soil gas =cm/sec (Equation 15) into the enclosed space) LT (Vapor source-building = cm (table 1 of this rule) separation)

7. EQUATION FOR THE OVERALL EFFECTIVE DIFFUSION COEFFICIENT OF THE SOIL SYSTEM:

eff LT DT  L  L  L   L   WT cz F    cz   eff   eff   DV  Dcz  where, eff (Total overall effective diffusion = chemical-specific, cm2/sec D T coefficient) eff (Effective diffusion coefficient = chemical-specific, cm2/sec D V across vadose zone) (Equation 8)

eff 2 D cz (Effective diffusion coefficient = chemical-specific, cm /sec across capillary zone) (Equation 9) LT (Vapor source-building = cm (table 1 of this rule) separation) LWT (Depth below grade to water = cm (table 1 of this rule) table) LCZ (thickness of capillary zone) = cm (Equation 13) LF (Depth below grade of enclosed = cm (table 1 of this rule) space)

8. EQUATION FOR THE EFFECTIVE DIFFUSION COEFFICIENT WITHIN THE VADOSE ZONE:

3 33 2 3 33 2 eff . . D V  D a  a n  D w H'TS  w n  where, eff (Effective diffusion coefficient = chemical-specific, cm2/sec D V across vadose zone) 2 Da (Diffusivity in air) = chemical-specific, cm /sec 3 3 a (Soil air-filled porosity) = 0.321 cm /cm or soil type- specific n (Soil total porosity) = 0.375 cm3/cm3 or soil type- specific 2 Dw (Diffusivity in water) = chemical-specific, cm /sec 3 3 w (Soil water-filled porosity) = 0.054 cm /cm or soil type- specific H′TS (Henry’s law constant at the = chemical-specific, dimensionless system temperature) (Equation 4)

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9. EQUATION FOR THE EFFECTIVE DIFFUSION COEFFICIENT ACROSS THE CAPILLARY ZONE:

3 33 2 3 33 2 eff . . D cz  Da  a,cz ncz  D w H'TS w,cz ncz  where, eff (Effective diffusion coefficient = chemical-specific, cm2/sec Dcz across the capillary zone) 2 Da (Diffusivity in air) = chemical-specific, cm /sec 3 3 a,cz (Soil air-filled porosity in the =cm/cm capillary zone: a,cz = n - w,cz) 3 3 ncz (Soil total porosity in the = 0.375 cm /cm or soil type- capillary zone) specific 2 Dw (Diffusivity in water) = chemical-specific, cm /sec H′TS (Henry’s law constant at the = chemical-specific, dimensionless system temperature) (Equation 4) 3 3 w,cz (Soil water-filled porosity in the =cm/cm (Equation 10) capillary zone)

For calculating soil type-specific ncz, use the information associated with the soil total porosity (n) in table 1 of R 299.7.

10. EQUATION FOR WATER-FILLED POROSITY IN THE CAPILLARY ZONE:

θs  θr θw,cz  θr  N M 1 α1 h where, 3 3 w,cz (Water-filled porosity in the =cm/cm capillary zone) 3 3 r (Residual soil water content) = 0.053 cm /cm or soil type- specific 3 3 s (Saturated soil water content) = 0.375 cm /cm or soil type- specific -1 1 (Point of inflection in the water = 0.03524 cm or soil type-specific retention curve where dθw/dh is maximal) h (Air-entry pressure head: h= =cm 1/α1 and assumed to be positive) N (van Genuchten curve shape = 3.177, dimensionless or soil parameter) type-specific M (1-(1/N)) = 0.6852 dimensionless or soil type-specific

11. EQUATION FOR THE MEAN RISE OF THE CAPILLARY ZONE:

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2   2 cos L  cz  g R w where, Lcz (Thickness (mean rise) of =cm capillary zone) 2 α2 (Surface tension of water) = 73 g/sec  (Angle of the water meniscus = degrees (assumed to be zero) with respect to the capillary tube) 3 w (Density of water) = 0.999 g/cm g (Acceleration due to gravity) = 980.665 cm/sec2 R (Mean interparticle pore radius) = cm (Equation 12)

12. EQUATION FOR THE MEAN INTERPARTICLE PORE RADIUS:

R  0.2 D

where, R (Mean interparticle pore radius) = cm D (Mean particle diameter) = 0.044 cm or soil type-specific

13. EQUATIONS 11 AND 12 ARE REDUCED TO: 0 15 . L  cz R where, Lcz (Mean rise of capillary zone) = cm R (Mean interparticle pore radius) = cm (Equation 12)

14. EQUATION FOR THE BUILDING VENTILATION RATE:

 1hr 

Qbuilding  (LB WB HB ER)  3,600sec where, 3 Qbuilding (Building ventilation rate) = cm /sec LB (Length of building) = cm (table 1 of this rule) WB (Width of building) = cm (table 1 of this rule) HB (Height of building) = cm (table 1 of this rule) ER (Air exchange rate) = hr-1 (table 1 of this rule)

15. EQUATION FOR THE VOLUMETRIC FLOW RATE OF SOIL GAS ENTERING THE BUILDING:

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2    P kv  Xcrack Qsoil   ln 2Zcrack rcrack where, 3 Qsoil (Volumetric flow rate of soil gas =cm/sec entering the enclosed space of a building) π (Constant) = 3.14159 P (Pressure differential between = 40 g/cm-sec2 (table 1 of this rule) the soil surface and the enclosed space) 2 kv (Soil vapor permeability: kv = ki =cm (Equations 16 and 17) × krg) Xcrack (Floor-wall seam perimeter: = cm (LB & WB in table 1 of this Xcrack = 2(LB + WB)) rule) μ (Viscosity of air: μ = = g/cm-sec 0.00018*((TS)/298.15)^0.5) Zcrack (Portion of the structure below = cm (table 1 of this rule) grade in which vapors will pass) rcrack (Equivalent crack radius) = cm (Equation 19)

16. EQUATION FOR THE SOIL INTRINSIC PERMEABILITY:

   1hr    Ks  w    3,600sec  ki  w g where, 2 ki (Soil intrinsic permeability) = cm Ks (Soil saturated hydraulic = 26.78 cm/hr or soil type-specific conductivity) w (Dynamic viscosity of water) = 0.01307 g/cm-sec @ 10 3 w (Density of water) = 0.999 g/cm g (Acceleration due to gravity) = 980.665 cm/sec2

17. EQUATION FOR RELATIVE AIR PERMEABILITY:

2 1 1 G 1 2 1 k   S    S G  rg te  te  where, krg (Relative air permeability) = unitless (0 ≤ krg ≤ 1) Ste (Effective total fluid saturation) = unitless (Equation 18) G (van Genuchten shape = 0.6852 unitless or soil type- parameter) specific

18. EQUATION FOR EFFECTIVE TOTAL FLUID SATURATION:

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θ w  θ r S te  n - θ r where, Ste (Effective total fluid saturation) = unitless 3 3 w (Vadose zone soil water-filled = 0.054 cm /cm or soil type- porosity) specific 3 3 r (Residual soil-water content) = 0.053 cm /cm or soil type- specific n (Soil total porosity) = 0.375 cm3/cm3 or soil type- specific

19. EQUATION FOR THE EQUIVALENT RADIUS OF THE FLOOR-WALL SEAM CRACK:

rcrack    AB X crack where, rcrack (Equivalent crack radius) = cm 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)]) η (Crack to enclosed floor area = unitless (0 ≤ η ≤ 1) (Equation ratio: Acrack/AB) 20) Xcrack (Floor-wall seam perimeter: = cm (LB & WB in table 1 of this Xcrack = 2(LB + WB)) rule)

20. EQUATION FOR THE RATIO OF THE CRACK AREA TO ENCLOSED FLOOR AREA IS ESTABLISHED AS: 2 w  L  W   B B AB where, η (Crack to enclosed floor area = unitless ratio: Acrack/AB) w (Floor-wall seam crack width) = cm (table 1 of this rule) WB (Enclosed space floor width) = cm (table 1 of this rule) LB (Enclosed space floor length) = cm (table 1 of this rule) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)])

(b) The direct diffusion of a volatile hazardous substance into indoor air from groundwater is determined by the following equations:

1. EQUATION FOR CALCULATION OF THE GROUNDWATER HEALTH- BASED CONCENTRATION:

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AAC VISG  VFSG where, VISG (Volatilization to indoor air = chemical-specific, g/L concentration for shallow groundwater) AAC (Acceptable air concentration) = chemical-specific, g/m3-v

3 VFSG (Volatilization factor) = chemical-specific, L/m (Equation 2)

2. EQUATION FOR THE VOLATILIZATION FACTOR:

L 103 m3 VFSG   1   fRVB      H'  KoverallASG  where, 3 VFSG (Volatilization factor) = chemical-specific, L/ m H’ (Dimensionless Henry’s law = chemical-specific, dimensionless constant, where H’ = HLC x 41) −1 fR (Frequency of renovation of air) = ER converted to sec 3 VB (Room volume VB = HB × LB × =m(HB, LB & WB in table 1 of WB ) this rule) Koverall (Overall mass-transfer = m/sec (Equation 3) coefficient) 2 ASG (Surface area of contaminated = m (table 1 of this rule) water within the structure)

3. EQUATION FOR THE MASS TRANSFER COEFFICIENT:

1 KOverall   1   1       KL  KG x H' where, KOverall (Overall mass transfer = chemical-specific, m/sec coefficient) KL (Mass transfer coefficient for = chemical-specific, m/sec water) (Equation 4) KG (Mass transfer coefficient for = chemical-specific, m/sec air) (Equation 5) H’ (Dimensionless Henry’s law = chemical-specific, dimensionless constant, where H’ = HLC x 41)

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4. EQUATION FOR THE MASS TRANSFER COEFFICIENT FOR WATER:

0.67 6  DW  KL  6.5 x 10 1.488 x 109  where, KL (Mass transfer coefficient for = chemical-specific, m/sec water) DW (Diffusivity in water) = chemical-specific, converted from cm2/sec to m2/sec

5. EQUATION FOR THE MASS TRANSFER COEFFICIENT FOR AIR:

0.67  Da  KG  KG,H20 2.6 x 105  where, KG (Mass transfer coefficient for = chemical-specific, m/sec air) −3 KG,H20 (Evaporation rate in air) = 3 × 10 m/sec Da (Diffusivity in air) = chemical-specific, converted from cm2/sec to m2/sec

(c) The volatilization to indoor air value for soil are determined by the following equations:

1. EQUATION FOR CALCULATION OF A RISK BASED MEDIA CONCENTRATION FOR SOIL:

AAC  θw  Kd ρb  H'TS  θa VI  1000 3 soil  , cm kg  3  H'TS    ρb     m g  where, VIsoil (Volatilization to indoor air = g/kg concentration for soil) AAC (Acceptable air concentration) = chemical-specific, µg/m3-v H′TS (Henry’s law constant at the = chemical-specific, dimensionless system (soil) temperature) (Equation 4) 3 3 a (Soil air-filled porosity) = 0.321 cm /cm or soil type- specific 3 b (Soil dry bulk density) = 1.66 g/cm or soil type-specific α (Steady-state attenuation = unitless (Equation 6 and table 1 coefficient) of this rule) 3 3 w (Soil water-filled porosity) = 0.054 cm /cm or soil type- specific

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3 Kd (Soil-water partition coefficient =Koc chemical-specific, cm /g for organics compounds: foc 0.002 unitless Kd = Koc × foc)

2. EQUATION FOR THE DIMENSIONLESS FORM OF THE HENRY’S LAW CONSTANT AT THE SYSTEM TEMPERATURE:

1 1  Hv,TS   exp     HLC  Rc  TS TR  H'TS  RTs where, H′TS (Henry’s law constant at the = chemical-specific, dimensionless system temperature) Hv, TS (Enthalpy of vaporization at the = chemical-specific, cal/mol system temperature) (Equation 5) TS (System temperature) = 283.15 K or facility-specific TR (Henry’s law constant reference = 298.15 K temperature) HLC (Henry’s law constant at the = chemical-specific, atm-m3/mol reference temperature) RC (Gas constant) = 1.9872 cal/mol-K R (Gas constant) = 8.206E-05 atm-m3/mol-K

3. EQUATION FOR ENTHALPY OF VAPORIZATION:

1 Y     TS TC  Hv,TS  Hv,b   1      TBP TC  where, Hv,TS (Enthalpy of vaporization at the = chemical-specific, cal/mol system temperature) Hv,b (Enthalpy of vaporization at the = chemical-specific, cal/mol normal boiling point) TS (System temperature) = 283.15 K or facility-specific TC (Critical Temperature) = chemical-specific, K TBP (Standard boiling point) = chemical-specific, K Y (Constant) = unitless

Y (constant) is established as a function of the ratio TBP/TC such that: if TBP/TC < 0.57, Y is 0.30; if TBP/TC is between 0.57 and 0.71, Y is established as 0.74(TBP/TC) - 0.116; and if TBP/TC > 0.71, Y is 0.41.

4. EQUATION FOR AN INFINITE VAPOR SOURCE ASSUMING STEADY STATE MASS TRANSFER THE ATTENUATION COEFFICIENT:

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 Deff  A   Q L   v B   exp soil crack       Qbuilding LT  Dcrack  Acrack        Q L   Deff  A   Deff  A   Q L  1 exp  soil crack    v B    v B exp soil crack    D  A   Q L   Q L  D  A    crack crack   building T   soil T   crack crack   where,  (Steady-state attenuation = unitless coefficient) eff (Effective diffusion coefficient =cm2/sec (Equation 7) Dv across vadose zone) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)]) 3 Qbuilding (Building ventilation rate) = cm /sec (Equation 8) LT (Vapor source-building = cm (table 1 of this rule) separation) 3 Qsoil (Volumetric flow rate of soil gas =cm/sec (Equation 9) into the enclosed space) Lcrack (Enclosed space foundation or = cm (table 1 of this rule) slab thickness) 2 Acrack (Area of total cracks: Acrack = =cm(LB & WB-table 1 of this 2w(LB + WB)) rule) 2 Dcrack (Effective diffusion coefficient =cm/sec (assumed equivalent to eff through the cracks) Dv of Equation 7)

Equation 6 contains the exponent of the following dimensionless group:

 Qsoil  Lcrack     Dcrack  A crack  where, 3 Qsoil (Volumetric flow rate of soil gas =cm/sec (Equation 9) entering the enclosed space of a building) Lcrack (Enclosed space foundation or = cm (table 1 of this rule) slab thickness) 2 Dcrack (Effective diffusion coefficient =cm/sec (assumed equivalent to eff through the cracks) Dv of Equation 7) 2 Acrack (Area of total cracks: Acrack = =cm (LB & WB in table 1 of this 2w(LB + WB)) rule)

This dimensionless group represents the equivalent Peclet number for transport through the Building Foundation. As the dimensionless group approaches infinity and if the exponent of the equation identified above is too great to be calculated then the attenuation factor is established as:

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eff  Dv  Lcrack     Dcrack  A crack    eff 1  Dv  AB      Qsoil  L T  where, α (Steady-state attenuation = unitless coefficient) eff (Effective diffusion coefficient =cm2/sec (Equation 7) D v across vadose zone) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)]) 3 Qbuilding (Building ventilation rate) = cm /sec (Equation 8) 3 Qsoil (Volumetric flow rate of soil gas =cm/sec (Equation 9) into the enclosed space) LT (Vapor source-building = cm (table 1 of this rule) separation)

5. EQUATION FOR THE EFFECTIVE DIFFUSION COEFFICIENT WITHIN THE UNSATURATED ZONE:

eff 3.33 2 3.33 2 D v  D a  θ a n  D w H' TS θ w n  where, eff (Effective diffusion coefficient = chemical-specific, cm2/sec Dv across vadose zone) 2 Da (Diffusivity in air) = chemical-specific, cm /sec 3 3 a (Soil air-filled porosity) = 0.321 cm /cm or soil type- specific n (Soil total porosity) = 0.375 cm3/cm3 or soil type- specific 2 Dw (Diffusivity in water) = chemical-specific, cm /sec 3 3 w (Soil water-filled porosity) = 0.054 cm /cm or soil type- specific H′TS (Henry’s law constant at the = dimensionless (Equation 4) system temperature)

6. EQUATION FOR THE BUILDING VENTILATION RATE:

 1hr 

Qbuilding  (LB WB HB ER)  3,600sec where, 3 Qbuilding (Building ventilation rate) = cm /sec LB (Length of building) = cm (table 1 of this rule)

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WB (Width of building) = cm (table 1 of this rule) HB (Height of building) = cm (table 1 of this rule) ER (Air exchange rate) = hr-1 (table 1 of this rule)

7. EQUATION FOR THE VOLUMETRIC FLOW RATE OF SOIL GAS ENTERING THE BUILDING:

2  π  ΔP k v  X crack Qsoil  μ ln 2Zcrack rcrack where, 3 Qsoil (Volumetric flow rate of soil gas =cm/sec entering the enclosed space of a building) π (Constant) = 3.14159 P (Pressure differential between = 40 g/(cm-sec2) (table 1 of this the soil surface and the enclosed rule) space) 2 kv (Soil vapor permeability: kv = ki =cm (Equations 10 and 11) × krg) Xcrack (Floor-wall seam perimeter: = cm (LB & WB in table 1 of this Xcrack = 2(LB + WB)) rule) μ (Viscosity of air: μ = = g/(cm-sec) 0.00018*((TS)/298.15)^0.5) Zcrack (Portion of the structure below = cm (table 1 of this rule) grade in which vapors will pass) rcrack (Equivalent crack radius) = cm (Equation 13)

8. EQUATION FOR THE SOIL INTRINSIC PERMEABILITY:

   1hr    K s   w  3,600 sec  k    i   g w where, 2 ki (Soil intrinsic permeability) = cm Ks (Soil saturated hydraulic = 26.78 cm/hr or soil type-specific conductivity) w (Dynamic viscosity of water) = 0.01307 g/cm·sec @ 10 3 w (Density of water) = 0.999 g/cm g (Acceleration due to gravity) = 980.665 cm/sec2

9. EQUATION FOR RELATIVE AIR PERMEABILITY:

2 1 1 G 1 2 1 k   S    S G  rg te  te  where,

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krg (Relative air permeability) = unitless (0 ≤ krg ≤ 1) Ste (Effective total fluid saturation) = unitless (Equation 12) G (van Genuchten shape = 0.6852 unitless or soil type- parameter) specific

10. EQUATION FOR EFFECTIVE TOTAL FLUID SATURATION:

w  r Ste  n - θr where, Ste (Effective total fluid saturation) = unitless 3 3 w (Soil water-filled porosity) = 0.054 cm /cm or soil type- specific 3 3 r (Residual soil-water content) = 0.053 cm /cm or soil type- specific n (Soil total porosity) = 0.375 cm3/cm3 or soil type- specific

The effective air permeability (kv) is the product of the intrinsic permeability (ki) and the relative air permeability (krg) at the soil water-filled porosity θw.

11. EQUATION FOR THE EQUIVALENT RADIUS OF THE FLOOR-WALL SEAM CRACK:

rcrack    AB X crack where, rcrack (Equivalent crack radius) = cm 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)]) η (Acrack/AB) = unitless (0 ≤ η ≤ 1) (Equation 14) Xcrack (Floor-wall seam perimeter: = cm (LB & WB in table 1 of this Xcrack = 2(LB + WB)) rule)

12. EQUATION FOR THE RATIO OF THE CRACK AREA TO ENCLOSED FLOOR AREA IS ESTABLISHED AS: 2 w  L  W   B B AB where, η (Crack to enclosed floor area = unitless ratio) w (Floor-wall seam crack width) = cm (table 1 of this rule) WB (Enclosed space floor width) = cm (table 1 of this rule)

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LB (Enclosed space floor length) = cm (table 1 of this rule) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)])

(d) The volatilization to indoor air values for vapor are determined by the following equations:

1. EQUATION FOR CALCULATION OF A RISK BASED MEDIA CONCENTRATION FOR VAPOR:

AAC VI  sg  where, VIsg (Volatilization to indoor air = g/m3 concentration for vapor) AAC (Acceptable air concentration) = chemical-specific, µg/m3-v α (Steady-state attenuation = unitless (Equation 2 or table 1 of coefficient) this rule)

For developing VI Tier 2 and VI Tier 3A criteria for a vapor source within 1 meter of a structure use a steady-state attenuation coefficient of 0.03. For developing VI Tier 3A criteria for a vapor source greater than 1 meter from a structure, use the calculated steady-state attenuation coefficient in Equation 2 of this subrule with a vapor source-building separation of 1 meter.

2. EQUATION FOR THE ATTENUATION COEFFICIENT OF AN INFINITE VAPOR SOURCE ASSUMING STEADY STATE MASS TRANSFER:

 Deff  A   Q L   v B   exp soil crack   Q L  D  A   building T   crack crack    whe   Q L   Deff  A   Deff  A   Q L  1 exp  soil crack    v B    v B exp soil crack    D  A   Q L   Q L  D  A    crack crack   building T   soil T   crack crack   re,  (Steady-state attenuation = unitless coefficient) eff (Effective diffusion coefficient =cm2/sec (Equation 3) Dv across vadose zone) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)]) 3 Qbuilding (Building ventilation rate) = cm /sec (Equation 6) LT (Vapor source-building = cm (table 1 of this rule)

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separation) 3 Qsoil (Volumetric flow rate of soil gas =cm/sec (Equation 7) into the enclosed space) Lcrack (Enclosed space foundation or = cm (table 1 of this rule) slab thickness) 2 Acrack (Area of total cracks: Acrack = =cm(LB & WB-table 1 of this 2w(LB + WB)) rule) 2 Dcrack (Effective diffusion coefficient =cm/sec (assumed equivalent to eff through the cracks) Dv of Equation 3)

Equation 2 contains the exponent of the following dimensionless group:

 Qsoil Lcrack     Dcrack  Acrack  where, 3 Qsoil (Volumetric flow rate of soil gas =cm/sec (Equation 7) entering the enclosed space of a building) Lcrack (Enclosed space foundation or = cm (table 1 of this rule) slab thickness) 2 Dcrack (Effective diffusion coefficient =cm/sec (assumed equivalent to eff through the cracks) Dv of Equation 3) 2 Acrack (Area of total cracks: Acrack = =cm (LB & WB in table 1 of this 2w(LB + WB)) rule)

This dimensionless group represents the equivalent Peclet number for transport through the building foundation. As the dimensionless group approaches infinity and if the exponent of the equation identified above is too great to be calculated then the attenuation factor is established as:

 Deff L   v crack   D  A     crack crack  eff 1  Dv AB      Qsoil LT  where, α (Steady-state attenuation = unitless coefficient) Deff (Effective diffusion coefficient =cm2/sec (Equation 3) v across vadose zone) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)]) 3 Qbuilding (Building ventilation rate) = cm /sec (Equation 6) 3 Qsoil (Volumetric flow rate of soil gas = cm /sec (Equation 7)

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into the enclosed space) LT (Vapor source-building = cm (table 1 of this rule) separation)

3. EQUATION FOR THE EFFECTIVE DIFFUSION COEFFICIENT WITHIN THE UNSATURATED ZONE:

3 33 2 3 33 2 eff . . D v  Da  a n  D w H'TS w n  where, eff (Effective diffusion coefficient = chemical-specific, cm2/sec Dv across vadose zone) 2 Da (Diffusivity in air) = chemical-specific, cm /sec 3 3 a (Soil air-filled porosity) = 0.321 cm /cm or soil type- specific n (Soil total porosity) = 0.375 cm3/cm3 or soil type- specific 2 Dw (Diffusivity in water) = chemical-specific, cm /sec 3 3 w (Soil water-filled porosity) = 0.054 cm /cm or soil type- specific H′TS (Henry’s law constant at the = dimensionless (Equation 4) system temperature)

4. EQUATION FOR THE DIMENSIONLESS FORM OF THE HENRY’S LAW CONSTANT AT THE SYSTEM TEMPERATURE:

1 1  Hv,TS   exp     HLC  Rc  TS TR  H'TS  R  Ts where, H′TS (Henry’s law constant at the = chemical-specific, dimensionless system temperature) Hv, TS (Enthalpy of vaporization at the = chemical-specific, cal/mol system temperature) (Equation 5) TS (System temperature) = 283.15 K or facility-specific TR (Henry’s law constant reference = 298.15 K temperature) HLC (Henry’s law constant at the = chemical-specific, atm-m3/mol reference temperature) RC (Gas constant) = 1.9872 cal/mol-K R (Gas constant) = 8.206E-05 atm-m3/mol-K

5. EQUATION FOR ENTHALPY OF VAPORIZATION:

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1 Y     TS TC  Hv,TS  Hv,b   1      TBP TC  where, Hv,TS (Enthalpy of vaporization at the = chemical-specific, cal/mol system temperature) Hv,b (Enthalpy of vaporization at the = chemical-specific, cal/mol normal boiling point) TS (System temperature) = 283.15 K or facility-specific TC (Critical Temperature) = chemical-specific, K TBP (Standard boiling point) = chemical-specific, K Y (Constant) = unitless

Y (constant) is established as a function of the ratio TBP/TC such that: if TBP/TC < 0.57, Y is 0.30; if TBP/TC is between 0.57 and 0.71, Y is established as 0.74(TBP/TC) - 0.116; and if TBP/TC > 0.71, Y is 0.41.

6. EQUATION FOR THE BUILDING VENTILATION RATE:

 1hr 

Qbuilding  (LB  WB HB ER)   3,600sec where, 3 Qbuilding (Building ventilation rate) = cm /sec LB (Length of building) = cm (table 1 of this rule) WB (Width of building) = cm (table 1 of this rule) HB (Height of building) = cm (table 1 of this rule) ER (Air exchange rate) = hr-1 (table 1 of this rule)

7. EQUATION FOR THE VOLUMETRIC FLOW RATE OF SOIL GAS ENTERING THE BUILDING: 2    P kv  Xcrack Qsoil  2  lnZcrack rcrack where, 3 Qsoil (Volumetric flow rate of soil gas =cm/sec entering the enclosed space of a building) π (Constant) = 3.14159 P (Pressure differential between = 40 g/(cm-sec2) (table 1 of this the soil surface and the enclosed rule) space) 2 kv (Soil vapor permeability: kv = ki =cm (Equations 8 and 9) × krg) Xcrack (Floor-wall seam perimeter: = cm (LB & WB in table 1 of this Xcrack = 2(LB + WB)) rule)

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μ (Viscosity of air: μ = = g/(cm-sec) 0.00018*((TS)/298.15)^0.5) Zcrack (Portion of the structure below = cm (table 1 of this rule) grade in which vapors will pass) rcrack (Equivalent crack radius) = cm (Equation 11)

8. EQUATION FOR THE SOIL INTRINSIC PERMEABILITY:

   1hr    Ks   w  3,600 sec  k    i   g w where, 2 ki (Soil intrinsic permeability) = cm Ks (Soil saturated hydraulic = 26.78 cm/hr or soil type-specific conductivity) w (Dynamic viscosity of water) = 0.01307 g/cm·sec @ 10 3 w (Density of water) = 0.999 g/cm g (Acceleration due to gravity) = 980.665 cm/sec2

9. EQUATION FOR RELATIVE AIR PERMEABILITY:

2 1 1 G 1 2 1 k   S    S G  rg te  te  where, krg (Relative air permeability) = unitless (0 ≤ krg ≤ 1) Ste (Effective total fluid saturation) = unitless (Equation 10) G (van Genuchten shape = 0.6852 unitless or soil type- parameter) specific

10. EQUATION FOR EFFECTIVE TOTAL FLUID SATURATION:

θw  θr Ste  n - θr where, Ste (Effective total fluid saturation) = unitless 3 3 w (Vadose zone soil water-filled = 0.054 cm /cm or soil type- porosity) specific 3 3 r (Residual soil-water content) = 0.053 cm /cm or soil type- specific n (Soil total porosity) = 0.375 cm3/cm3 or soil type- specific

11. EQUATION FOR THE EQUIVALENT RADIUS OF THE FLOOR-WALL SEAM CRACK:

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rcrack   AB Xcrack where, rcrack (Equivalent crack radius) = cm 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)]) η (Acrack/AB) = unitless (0 ≤ η ≤ 1) (Equation 11) Xcrack (Floor-wall seam perimeter: = cm (LB & WB in table 1 of this Xcrack = 2(LB + WB)) rule)

12. EQUATION FOR THE RATIO OF THE CRACK AREA TO ENCLOSED FLOOR AREA IS ESTABLISHED AS: 2 w L  W   B B AB where, η (Crack to enclosed floor area = unitless ratio) w (Floor-wall seam crack width) = cm (table 1 of this rule) WB (Enclosed space floor width) = cm (table 1 of this rule) LB (Enclosed space floor length) = cm (table 1 of this rule) 2 AB (Area of the enclosed space =cm (LB, WB, and LF in table 1 below grade: AB = [(LB × WB) + of this rule) 2(LF x LB) + 2(LF x WB)])

(14) The residential AAC is the minimum of the health risk-based acceptable air values (AAV) calculated according to equations 1 to 5 of this subrule, except as provided in R 299.49(1)(EE) and (FF). The nonresidential AAC is the minimum of the health risk-based AAV calculated according to equations 6 to 8 of this subrule, except as provided in R 299.49(1)(EE) and (FF).

RESIDENTIAL: 1. EQUATION FOR CARCINOGENIC EFFECTS:

TR ATca AAVca  IURFEDres EFres where, 3 AAVca (Acceptable air value) = chemical-specific, µg/m TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific, (µg/m3)-1 EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year

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2. EQUATION FOR CARCINOGENS WITH MUTAGENIC EFFECTS:

TR ATca AAVmut  IURFEFres ED2  ADAF2  ED26  ADAF26  ED616  ADAF616  ED1632  ADAF1632  where, 3 AAVmut (Acceptable air value) = chemical-specific, µg/m TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific, (µg/m3)-1 EFres (Exposure frequency) = 350 days/year ED age <2 (Exposure duration, age <2 years) = 2 years ADAF<2 (Age-dependent adjustment factor = 10 for cancer potency, age <2 years) EDage 2-6 (Exposure duration, age 2-6 years) = 4 years ADAF2-6 (Age-dependent adjustment factor = 3 for cancer potency, age 2-6 years) EDage 6-16 (Exposure duration, age 6-16 years) = 10 years ADAF6-16 (Age-dependent adjustment factor = 3 for cancer potency, age 6-16 years) EDage 16-32 (Exposure duration, age 16-32 = 16 years years) ADAF16-32 (Age-dependent adjustment factor = 1 for cancer potency, age 16-32 years)

3. EQUATION FOR NONCARCINOGENIC EFFECTS:

THQ AT RfCRSC AAV  res nc ED EF res res where, 3 AAVnc (Acceptable air value) = chemical-specific, µg/m THQ (Target hazard quotient) = 1 ATres (Averaging time) = 11,680 days RfC (Reference concentration) = chemical-specific, µg/m3 RSC (Relative source contribution) = 1 or chemical-specific EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year

4. EQUATION FOR DEVELOPMENTAL EFFECTS - CHILD:

THQ  AT  RfC  RSC AAV  child dev dev ED  EF child child where, 3 AAVdev (Acceptable air value) = chemical-specific, µg/m THQ (Target hazard quotient) = 1 ATchild (Averaging time) = 2,190 days

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3 RfCdev (Reference concentration, = chemical-specific, µg/m developmental) RSC (Relative source contribution) = 1 or chemical-specific EDchild (Exposure duration) = 6 years EFchild (Exposure frequency) = 350 days/year

5. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT RESIDENT:

THQ  ATpreg  RfC dev  RSC AAVdev  ED preg  EFpreg where, 3 AAVdev (Acceptable air value) = chemical-specific, µg/m THQ (Target hazard quotient) = 1 ATpreg,FT (Averaging time, full-term = 280 days or chemical- pregnancy) specific ATpreg,SE (Averaging time, single event = 1 day or chemical- exposure during pregnancy) specific 3 RfCdev (Reference concentration, = chemical-specific, µg/m developmental) RSC (Relative source contribution) = chemical-specific or 1 EDpreg,FT (Exposure duration, full-term = 0.767 year or chemical- pregnancy) specific EDpreg,SE (Exposure duration, single event = 1 day or chemical- exposure during pregnancy) specific EFpreg,FT (Exposure frequency, full-term = 268.5 days/year or pregnancy) chemical-specific EFpreg,SE (Exposure frequency, single event = 1 day/day or chemical- exposure during pregnancy ) specific

NONRESIDENTIAL: 6. EQUATION FOR CARCINOGENIC EFFECTS:

TR  ATca AAVca  IURFEDnr EFnr where, 3 AAVca (Acceptable air value) = chemical-specific, µg/m TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = chemical-specific, (µg/m3)-1 EDnr (Exposure duration) = 20 years EFnr (Exposure frequency) = 238 days/year

7. EQUATION FOR NONCARCINOGENIC EFFECTS:

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THQ ATnr RfCRSC AAVnc  EFnr EDnr where, 3 AAVnc (Acceptable air value) = chemical-specific, µg/m THQ (Target hazard quotient) = 1 ATnr (Averaging time) = 7,300 days RfC (Reference concentration) = chemical-specific, µg/m3 RSC (Relative source contribution) = 1 or chemical-specific EFnr (Exposure frequency) = 238 days/year EDnr (Exposure duration) = 20 years

8. EQUATION FOR DEVELOPMENTAL EFFECTS – PREGNANT WORKER:

THQ  AT  RfC  RSC AAV  dev dev dev ED  EF dev dev where, 3 AAVdev (Acceptable air value) = chemical-specific, µg/m THQ (Target hazard quotient) = 1 ATdev,FT (Averaging time, pregnant worker, = 280 days or chemical- full-term pregnancy) specific ATdev,SE (Averaging time, pregnant worker, = 1 day or chemical- single event exposure during specific pregnancy) 3 RfCdev (Reference concentration) = chemical-specific, µg/m RSC (Relative source contribution) = chemical-specific or 1 EDdev,FT (Exposure duration, pregnant worker, = 0.767 year or chemical- full-term pregnancy) specific EDdev,SE (Exposure duration, pregnant worker, = 1 day or chemical- single event exposure during specific pregnancy) EFdev,FT (Exposure frequency, pregnant = 183 days/year or worker, full-term pregnancy) chemical-specific EFdev,SE (Exposure frequency, pregnant = 1 day/day or chemical- worker, single event exposure during specific pregnancy)

(15) Figure 1 of this rule reads as follows:

140 99

FIGURE 1: VI Tier Process

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(16) Table 1 of this rule reads as follows:

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TABLE 1 Generic Input Values VI Tier 1 VI Tier 2 VI Tier 3A Variable Screening Levels Generic criteria Generic criteria Limited Residential & -- Exposure scenario category Unrestricted Residential Unrestricted Residential Limited Nonresidential For sand: 10oC or 283.15K or county System or soil temperature specific temperature if < TS 10oC or 283.15K VI Tier 2 values (Table 2 of R 299.7) 10oC For all other soil types: County-specific value Soil: Soil and Vapor: 1 cm or 0.01 m 1 cm or 0.01 m Vapor : Shallow Groundwater: 1 cm or 0.01 m when the Soil and Vapor: VI Tier 1 value vapor source is ≤ to 1 m 1 cm or 0.01 m Groundwater: vertically from the structure Distance to a vapor source Shallow Groundwater: When actual depth to 100 cm or 1 m when the LT (subrule (3) of this rule) Use equations in subrule groundwater > depth of vapor source is > 1 m (13)(a) and (13)(b) of this building considering vertically from the structure rule capillary zone, depth of Shallow Groundwater: footings, and subsurface VI Tier 1 value utilities, LT = LWT – (LF + Groundwater: LFF) VI Tier 2 value

Depth of footings and LFF utilities below enclosed 100 cm; 1 m VI Tier 1 value VI Tier 1 value space Residential: Basement: 15 cm or 0.15 m Basement (uninhabitable): 200 cm or 2 m Slab-on-grade: Portion of the structure Basement: 15 cm or 0.15 m Zcrack below grade in which VI Tier 1 value 15 cm or 0.15 m Nonresidential: vapors will pass Basement: 15 cm or 0.15 m Basement (unoccupied): 200 cm or 2 m Slab-on-grade: 15 cm or 0.15 m Residential or Nonresidential: Depth below grade of 200 cm or 2 m LF, VI Tier 1 value Basement: 200 cm or 2 m enclosed space Slab-on-grade: 15 cm or 0.15 m Actual depth to Actual depth to groundwater groundwater > depth of > depth of building building considering considering capillary zone, capillary zone, depth of depth of footings, and footings, and subsurface subsurface utilities. Depth to groundwater Shallow Groundwater: 3 utilities. Shallow Shallow Groundwater: LWT m or 300 cm Groundwater: Pursuant Pursuant to subrule (3) of to subrule (3) of this rule. this rule. Groundwater: Groundwater: Pursuant to subrule (4) of Pursuant to subrule (4) of this rule. this rule.: Basement:

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VI Tier 1 VI Tier 2 VI Tier 3A Variable Screening Levels Generic criteria Generic criteria Limited Residential & -- Exposure scenario category Unrestricted Residential Unrestricted Residential Limited Nonresidential

LWT – (LF + LFF) > 0 and LWT – (LF + LFF) > 0 and LWT – (LF + LCZ) > 0 LWT – (LF + LCZ) > 0 Slab-on-grade: LWT – (LFF + LCZ) > 0

Subrule (13)(a) Equation Subrule (13)(a) Equation Subrule (13)(a) Equation 13 LCZ Thickness of capillary zone 13 of this rule 13 of this rule of this rule

Residential or Enclosed space floor Lcrack 15 cm or 0.15 m VI Tier 1 value Nonresidential: thickness 15 cm or; 0.15 m Residential: 1,000 cm or 10 m Nonresidential use of a LB Enclosed space floor length 1,000 cm or 10 m VI Tier 1 value former residential structure: 1,000 cm or 10 m All other nonresidential: 2,000 cm or 20 m Residential: 1,000 cm or 10 m Nonresidential use of a WB Enclosed space floor width 1,000 cm or 10 m VI Tier 1 value former residential structure: 1,000 cm or 10 m All other nonresidential: 2,000 cm or; 20 m Residential: Basement: 244 cm or 2.44 m Basement (uninhabitable): 366 cm or 3.66 m Slab-on-grade: 244 cm or 2.44 m Enclosed space height HB 244 cm or 2.44 m VI Tier 1 value Nonresidential: (mixing height) Basement: 244 cm or 2.44 m Basement (unoccupied): 366 cm or 3.66 m Slab-on-grade: 244 cm or 2.44 m

Floor-wall seam crack w 0.1 cm or 0.001 m VI Tier 1 value VI Tier 1 value width Residential: House: 0.25 hr-1 High-rise Apartment: 0.61 hr-1 Nonresidential: ER Air Exchange Rate 0.25 hr-1 VI Tier 1 value Nonresidential use of a former residential structure: 0.5 hr-1 An individual nonresidential structure or portion < 50,000 ft2:

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VI Tier 1 VI Tier 2 VI Tier 3A Variable Screening Levels Generic criteria Generic criteria Limited Residential & -- Exposure scenario category Unrestricted Residential Unrestricted Residential Limited Nonresidential 1.0 hr-1 An individual nonresidential structure or portion ≥ 50,000 ft2: 1.5 hr-1 Other site-specific values: Pursuant to subrule (11) of this rule. Soil-bldg. differential P pressure, Residential or 40 g/cm-s2 VI Tier 1 value VI Tier 1 value Nonresidential

Soil organic carbon weight foc 0.002 VI Tier 1 value VI Tier 1 value fraction

Volatilization factor for Calculated from subrule VFsg VI Tier 1 value VI Tier 1 value shallow groundwater (13)(b) of this rule.

Soil: Calculated pursuant Soil: Calculated pursuant to to subrule (6) of this rule. subrule (6) of this rule. Vapor: Vapor: Vapor source <1 m: 0.03 Soil: Calculated Vapor source <1 m: 0.03 Vapor source and pursuant to subrule (6) Vapor source and sampling sampling location is >1 m: of this rule. location is >1 m: May be May be calculated Vapor: 0.03 calculated pursuant to  Attenuation coefficient pursuant to subrule (5) of Shallow Groundwater: subrule (5) of this rule. this rule. 0.03 pursuant to subrule Shallow Groundwater: 0.03 Shallow Groundwater: (3) of this rule. pursuant to subrule (3) of this 0.03 pursuant to subrule rule. (3) of this rule. Groundwater: Groundwater: Calculated Calculated pursuant to pursuant to subrule (4) of subrule (4) of this rule. this rule. Surface area of contaminated water within the structure, for a hazardous substance identified with a risk from LB x WB = 1E+06 cm2, or a short term exposure or 100 m2 for a hazardous substance that does not have sufficient chemical- physical inputs. VI Tier 1 value that may be -- VI Tier 1 value adjusted for the nonresidential assumptions Area of direct diffusion from sump and cracks: 10,000 cm2, or 1 m2 The weighted contribution

to indoor air from shallow Area of diffusion groundwater. through the concrete: 9.5E+05 cm2, or 99 m2

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VI Tier 1 VI Tier 2 VI Tier 3A Variable Screening Levels Generic criteria Generic criteria Limited Residential & -- Exposure scenario category Unrestricted Residential Unrestricted Residential Limited Nonresidential Residential: House, High-rise Apartment Nonresidential: Residential house with a Former residential structure -- Building Type basement VI Tier 1 value now nonresidential use, Nonresidential structure or portion < 50,000 ft2, Nonresidential structure or portion ≥ 50,000 ft2 Residential: Basement Basement (uninhabitable) Basement Slab-on-grade -- Foundation Type VI Tier 1 value Nonresidential: Basement Basement (unoccupied) Slab-on-grade No info available: Sand Approved Field methods: Sand, sandy loam, loamy Soil type input values sand, or loam -- Sand VI Tier 2 values (Table 1 of R 299.7) Other Approved methods: United States Department of Agriculture 12 classifications

Calculated based on Calculated based on soil -- Basis of Capillary Zone VI Tier 2 values sand type

-- Soil source type Infinite VI Tier 1 value VI Tier 1 value

(17) The equations for the generic VI Tier 3A nonresidential volatilization to indoor air health- based values do not explicitly include an exposure time. Continuous 24-hour per day exposure may not be representative of worker exposures in commercial or industrial settings. Both of the following apply: (a) Except as identified below the generic nonresidential groundwater, soil or vapor VI Tier 3A criteria based upon the health-based value derived from the equations of this rule may be adjusted to represent a 12-hour work day by multiplying the VI Tier 3A criterion by 2. An exposure time adjusted soil value shall not exceed the maximum ceiling concentration or be lower than the target detection limit. An exposure time adjusted groundwater value shall not exceed the solubility limit or be lower than the target detection limit. A 12-hour exposure time adjusted value remains a generic nonresidential criterion. Other adjustments for exposure time may be proposed as site-specific criteria based on a nonresidential land use that by its nature would only allow activities for a limited exposure time. The activities allowed by the land use must be easily identifiable, enforceable, and included in the land or resource use restriction for the property. This provision does not affect a person’s ability to demonstrate compliance using section 20120a(18) of the act. (b) Exposure time shall not be adjusted for the VI Tier 3A criteria developed from acceptable air concentrations based upon short-term inhalation reference values for exposures of less than 12 hours designated in R 299.49(1)(DD) to (FF).

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R 299.28 Cleanup criteria for contaminated environmental media based on other injury which requires consideration. Rule 28. (1) To assure that hazardous substances in contaminated environmental media do not pose unacceptable risks not accounted for by other rules in this part, the concentration of a hazardous substance in a given environmental medium shall meet cleanup criteria based on sound scientific principles and determined by the department to be necessary to protect the public health, safety, and welfare and the environment from any of the following: (a) Food chain contamination. (b) Damage to soil or biota in the soil that impairs the use of such soil for agricultural purposes. (c) Phytotoxicity. (d) Physical hazards. (e) Nonsystemic or acute toxicity. (f) Injury that may result from the direct transport or runoff of hazardous substances in soil into surface water. (g) Injury to the groundwater resource which may impair its use for other purposes that are determined by the department to be reasonable and relevant considerations at a facility. (h) Other injury that requires consideration. (2) The basis for and information used by the department to develop cleanup criteria under this rule shall be made available to the public upon request.

R 299.30 Surface water and surface water sediments; cleanup criteria. Rule 30. (1) Any response activity plan that addresses surface water or sediments that are associated with surface waters of the state as defined by part 31 of the act shall include site-specific cleanup criteria approved by the department pursuant to sections 20120a(2) and 20120b of the act. Criteria shall be established by the department on the basis of sound scientific principles and evaluation of bulk sediment chemistry, sediment toxicity, and benthic community populations and be approved by the department. Criteria shall be established considering the need to eliminate or mitigate the following use impairments, as appropriate to the facility in question: (a) Restrictions on fish or wildlife consumption. (b) Tainting of fish and wildlife flavor. (c) Degraded fish or wildlife populations. (d) Fish tumors or other deformities. (e) Bird or animal deformities or reproductive problems. (f) Degradation of benthos. (g) Restrictions on dredging activities. (h) Eutrophication or undesirable algae. (i) Restrictions on drinking water consumption or taste or odor problems. (j) Beach closings. (k) Degradation of aesthetics. (l) Added costs to agriculture, industry, or a local unit of government. (m) Degradation of phytoplankton or zooplankton populations. (n) Loss of fish and wildlife habitat. (o) Unacceptable risk through human contact as a result of absorption of hazardous substances through the skin or by incidental ingestion of sediments.

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(p) Other unacceptable risks to human receptors exposed to hazardous substances. in sediments. (2) The basis for, and information used by the department to develop, cleanup criteria and relied upon by the department to approve the criteria under this rule, shall be made available to the public upon request.

R 299.34 Risk assessment and development of cleanup criteria for certain substances; special considerations. Rule 34. (1) All polychlorinated and polybrominated dibenzodioxins and dibenzofurans shall be considered as 1 hazardous substance, expressed as an equivalent concentration of 2,3,7,8- tetrachlorodibenzo-p-dioxin, based upon the relative potency and concentration of the congeners present at the facility. (21) If 2 or more hazardous substances are present and known to result in toxicological interaction, then the interactive effects, including additivity, shall be considered in establishing levels that are protective of the public health, safety, and welfare and the environment. Both of the following apply: (a) All polychlorinated dibenzodioxins and dibenzofurans and dioxin-like polychlorinated biphenyls shall be evaluated as a single hazardous substance and environmental concentrations expressed as an equivalent concentration of 2,3,7,8-tetrachlorodibenzo-p-dioxin based upon the relative potency and concentration of the dioxin-like chemicals present at the facility. All classes of hazardous substances that have documented dioxin-like activity and have toxicity equivalent factors or other relative potency factors recognized by the United States Environmental Protection Agency shall be evaluated as a single hazardous substance and environmental concentrations calculated on the basis of the relative potencies and chemical-specific concentrations present at the facility. The adjusted environmental concentrations shall be summed and the resulting total equivalent concentration compared to the criterion for 2,3,7,8- tetrachlorodibenzo-p-dioxin. (b) Carcinogenic polynuclear aromatic hydrocarbons shall be evaluated as a single hazardous substance and environmental concentrations expressed as an equivalent concentration of benzo(a)pyrene based upon the relative potency and concentration of the carcinogenic polynuclear aromatic hydrocarbons present at the facility. All carcinogenic polynuclear aromatic hydrocarbons that have documented carcinogenic activity that is additive to that of benzo(z)pyrene and have relative potency factors recognized by the United States Environmental Protection Agency shall be evaluated as a single hazardous substance and environmental concentrations calculated on the basis of the relative potencies and chemical-specific concentrations present at the facility. The adjusted environmental concentrations shall be summed and the resulting total equivalent concentration compared to the criteria for benzo(a)pyrene. (32) The department may calculate generic cleanup criteria for certain hazardous substances using exposure assumptions other than those shown in the algorithmsequations in these rules if either of the following conditions is satisfied: (a) A hazardous substance causes an adverse effect in a sensitive lifestage or subpopulation that is not adequately protected by a generic criterion or represented by any of the generic exposure assumptions. Adverse effects to be addressed by this subrule include, but are not limited to, developmental or reproductive effects. (b) The toxicokinetics of a hazardous substance are not best represented by the average daily dose, when accounting for the most sensitive effect.

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(3) When determining compliance with generic cleanup criteria calculated under subrule (2) of this rule, the environmental data shall represent the exposure assumptions used to develop the criteria. (4) When polychlorinated biphenyls are present, refer to the federal Toxic Substances Control Act (TSCA), 40 C.F.R. 761 to determine the applicability of the TSCA cleanup standards.

R 299.36 Calculation of criteria based onDetermination of noncarcinogenic endpoints; minimum toxicity datavalues. Rule 36. (1) The minimum data required to calculate a cleanup criterionhealth-based value for a noncarcinogenhazardous substance when the route of exposure is ingestion or dermal absorption shall be the reference dose or an equivalent noncarcinogenic toxicity value that is determined on the basis of the best available information and considering the weight of evidence. (2) The minimum data required to calculate a cleanup criterion for a noncarcinogen when the route of exposure is inhalation shall be the minimum data required for calculation of an initial threshold screening level developed under part 55 of the act, and rules promulgated under part 55The data required to calculate a health-based value that is based on or incorporates the inhalation route of exposure shall be the reference concentration or an equivalent inhalation noncarcinogenic toxicity value that is determined on the basis of the best available information and considering the weight of evidence.

R 299.38 Determination of cancer slope factors for use in calculation of criteria based on carcinogenic endpointstoxicity values. Rule 38. (1) The department shall rely on the cancer risk for oral or inhalation exposure conducted by the United States Environmental Protection Agency and published in the integrated risk information system as a basis for calculation of criteria for those hazardous substances that cause cancer unless the department determines that other sources represent best available scientific information. (2) If the department develops a carcinogenic toxicity value or a site-specific carcinogenic toxicity value is proposed, the following apply: (a) A non-threshold mechanism of carcinogenesis shall beis assumed unless biological data adequately demonstrate the existence of a threshold on a hazardous substance chemical-specific basis. (2b) All appropriate human epidemiologic cancer data, animal cancer bioassay data, and all other pertinent data shall be considered and a cancer slope factor carcinogenic toxicity value developed if the weight of evidence for carcinogenicity is sufficient. The carcinogenic toxicity value shall be developed consistent with the cancer risk assessment guidelines developed by the United States Environmental Protection Agency. Preferred data are those from studies which use the same route of exposure addressed by the criteria. However, in the absence of such data, route-to-route extrapolations may be conducted where appropriate, considering whether the critical effect is systemic and thus possible for each different route of exposure. The risk-associated dose shall be set at a level corresponding to an increased cancer risk of 1 in 100,000. If acceptable human epidemiologic data are available for a hazardous substance, then those data shall be used to derive the risk-associated dose. If acceptable human epidemiologic data are not available, then the risk-associated dose shall be derived from available animal bioassay data. Data from a species that is considered most biologically relevant to humans, that is, responds most like humans, is preferred where all other considerations regarding quality of data are equal. In the absence of data to distinguish the most relevant species, data from the

149 2017 MR 22 – December 15, 2017 most sensitive species tested, that is the species showing a carcinogenic effect at the lowest administered dose, shall generally be used. (c) The cancer risks associated with early life exposures shall be addressed using the United States Environmental Protection Agency guidance for assessing susceptibility from early-life exposure to carcinogens with a mutagenic mode of action. When chemical-specific data are available for a sensitive lifestage, the data may be used to develop chemical-specific age-dependent adjustment factors. When chemical-specific data are not available, generic age-dependent adjustment factors shall be used. (3d) If animal bioassay data are used and a non-threshold mechanism of carcinogenicity is assumed, then the data shall be fitted to a linearized multistage model, for example, a Global ‘86 or equivalent computer model. Global ‘86 is the linearized multistage model that was derived by Howe, Crump, and Van Landingham (1986), which was prepared for the United States environmental protection agency under subcontract 2-251u-2745 to Research Triangle Institute, contract 68-01-6826, and which the United States environmental protection agency uses to determine cancer potencies. The upper-bound 95% confidence limit on risk, or the lower 95% confidence limit on dose, at the 1 in 100,000 risk level shall be used to calculate a risk-associated dose for individual hazardous substances. Other models, including modifications or variations of the linearized multistage model that are more appropriate to the available data, may be used where scientifically justified. (4e) If the duration of the study is significantly less than the natural lifespan of the test animal, then the slope factor may be adjusted on a case-by-case basis to compensate for latent tumors that were not expressed. The lifespan of a rat is assumed to be 104 weeks and the lifespan of a mouse is assumed to be 90 weeks. If the test animal is a rat and the study duration is less than 90 weeks, or if the test animal is a mouse and the study duration is less than 78 weeks, then the slope factor shall be multiplied by the following factor: the expected lifespan (L) divided by the study duration (Le) raised to the third power, 3 [(L/Le) ]. (5f) A species scaling factor shall be used to account for differences between test species and humans. It shall be assumed that scaling daily administered doses by body mass raised to the 3/4 power achieves equivalence in lifetime carcinogenic risk in different mammalian species. To derive a human slope factor from animal data, the default procedure shall be to multiply the animal slope factor by the ratio of human to animal body weights raised to the 1/4 power. However, if adequate pharmacokinetic and metabolism studies are available, then these data may be factored into the adjustment for species differences on a case-by-case basis. (6g) Additional adjustments shall be made to the data as appropriate. For some cancer data sets, it may be appropriate to combine incidences of multiple tumor types or combine benign and malignant tumors of the same histogenic origin. All doses shall be adjusted to give an average daily dose over the study duration. Adjustments shall be made to the tumor incidence for early mortality. Animals dying before the appearance of the first tumor within their dose group shall be removed from the data set. Before quantification of the dose response, a goodness-of-fit evaluation of the data shall be conducted. (7h) If human epidemiologic data, animal bioassay data, or other biological data indicate that a chemical causes cancer via a threshold mechanism, then the risk-associated dose may, on a case-by-case basis, be calculated using a method that assumes a threshold mechanism is operative. (8) Inhalation unit risk factors shall be calculated in the same manner as cancer risk screening levels for inhalation risk under part 55 of the act.

R 299.40 Availability of information used by department to establish cleanup criteria; public review and comment on revised criteria.

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Rule 40. (1) The department shall make available to the public the detailed basis for calculation of any cleanup criterion established under these rules, including the referencessource citations for original studies, papers, or other sources of information that were used or consideredrelied upon to calculate the criterion. Requests for information under this rule shall specify the hazardous substance and exposure pathways for which information is desired. (2) Any proposed change to a criterion shall be published by the department and subject to review and comment as part of the rule-making process.

R 299.44 Rescinded.Generic groundwater cleanup criteria. Rule 44. The generic groundwater cleanup criteria for all categories shall be as shown in table 1.

151 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Groundwa Residential Nonresidentia Residenti Nonresid ter Groundwater l Groundwater Flammabilit Chemical al ential Surface Volatilization Volatilization y and Abstract Drinking Drinking Water to Indoor Air to Indoor Air Water Explosivity Hazardous Service Water Water Interface Inhalation Inhalation Solubi Screening Substance Number Criteria Criteria Criteria Criteria Criteria lity Level Acenaphthene 83329 1,300 3,800 38 4,200 (S) 4,200 (S) 4,240 ID Acenaphthylene 208968 52 150 ID 3,900 (S) 3,900 (S) 3,930 ID 1.00E Acetaldehyde (I) 75070 950 2,700 130 1.1E+6 2.3E+6 +9 8.9E+6 Acetate 71501 4,200 12,000 (G) ID ID ID ID 6.00E Acetic acid 64197 4,200 12,000 (G) NLV NLV +9 1.0E+9 (D) 1.00E Acetone (I) 67641 730 2,100 1,700 1.0E+9 (D,S) 1.0E+9 (D,S) +9 1.5E+7 2.00E Acetonitrile 75058 140 400 NA 2.4E+7 4.5E+7 +8 2.1E+7 6.10E Acetophenone 98862 1,500 4,400 ID 6.1E+6 (S) 6.1E+6 (S) +6 ID 2.10E Acrolein (I) 107028 120 330 NA 2,100 4,200 +8 6.7E+6 2.20E Acrylamide 79061 0.5 (A) 0.5 (A) 10 (X) NLV NLV +9 NA 1.00E Acrylic acid 79107 3,900 11,000 NA 1.2E+7 2.8E+7 +9 1.0E+9 (D) 2.0 (M); 7.50E Acrylonitrile (I) 107131 2.6 11 1.2 34,000 1.9E+5 +7 6.4E+6 Alachlor 15972608 2.0 (A) 2.0 (A) 11 (X) NLV NLV 1.83E ID

152 2017 MR 22 – December 15, 2017 Groundwa Residential Nonresidentia Residenti Nonresid ter Groundwater l Groundwater Flammabilit Chemical al ential Surface Volatilization Volatilization y and Abstract Drinking Drinking Water to Indoor Air to Indoor Air Water Explosivity Hazardous Service Water Water Interface Inhalation Inhalation Solubi Screening Substance Number Criteria Criteria Criteria Criteria Criteria lity Level +5 6.00E Aldicarb 116063 3.0 (A) 3.0 (A) NA NLV NLV +6 ID 7.80E Aldicarb sulfone 1646884 2.0 (A) 2.0 (A) NA NLV NLV +6 ID 2.80E Aldicarb sulfoxide 1646873 4.0 (A) 4.0 (A) NA NLV NLV +7 ID 0.01 (M); Aldrin 309002 0.098 0.4 8.7E-6 180 (S) 180 (S) 180 ID Aluminum (B) 7429905 50 (V) 50 (V) NA NLV NLV NA ID 10,000 10,000 5.30E Ammonia 7664417 (N) (N) (CC) 3.2E+6 7.1E+6 +8 ID t-Amyl methyl ether 2.64E (TAME) 994058 190 (E) 190 (E) NA 2.6E+5 5.7E+5 +6 NA 3.60E Aniline 62533 53 220 4 NLV NLV +7 NA Anthracene 120127 43 (S) 43 (S) ID 43 (S) 43 (S) 43.4 ID Antimony 7440360 6.0 (A) 6.0 (A) 130 (X) NLV NLV NA ID Arsenic 7440382 10 (A) 10 (A) 10 NLV NLV NA ID 7.0E 7.0E Asbestos (BB) 1332214 MFL (A) MFL (A) NA NLV NLV NA NA Atrazine 1912249 3.0 (A) 3.0 (A) 7.3 NLV NLV 70,000 ID Azobenzene 103333 23 94 ID 6,400 (S) 6,400 (S) 6,400 ID Barium (B) 7440393 2,000 (A) 2,000 (A) (G) NLV NLV NA ID

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based

153 2017 MR 22 – December 15, 2017 criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Flammability Chemical Residential Surface Volatilization Volatilization and Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air Explosivity Service Water Drinking Interface Inhalation Inhalation Water Screening Hazardous Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Level Benzene (I) 71432 5.0 (A) 5.0 (A) 200 (X) 5,600 35,000 1.75E+6 68,000 0.3 (M); 0.3 (M); Benzidine 92875 0.0037 0.3 (M); 0.015 0.073 NLV NLV 5.20E+5 ID Benzo(a)anthracene (Q) 56553 2.1 8.5 ID NLV NLV 9.4 ID Benzo(b)fluoranthene (Q) 205992 1.5 (S,AA) 1.5 (S,AA) ID ID ID 1.5 ID Benzo(k)fluoranthene 1.0 (M); 1.0 (M); 0.8 (Q) 207089 0.8 (S) (S) NA NLV NLV 0.8 ID 1.0 (M); 1.0 (M); 0.26 Benzo(g,h,i)perylene 191242 0.26 (S) (S) ID NLV NLV 0.26 ID Benzo(a)pyrene (Q) 50328 5.0 (A) 5.0 (A) ID NLV NLV 1.62 ID Benzoic acid 65850 32,000 92,000 NA NLV NLV 3.50E+6 ID Benzyl alcohol 100516 10,000 29,000 NA NLV NLV 4.40E+7 ID Benzyl chloride 100447 7.7 32 NA 12,000 77,000 4.90E+5 NA Beryllium 7440417 4.0 (A) 4.0 (A) (G) NLV NLV NA ID bis(2- Chloroethoxy)ethane 112265 ID ID ID NLV NLV 1.89E+7 ID bis(2-Chloroethyl)ether 1.0 (M); (I) 111444 2 8.3 0.79 38,000 2.1E+5 1.72E+7 1.7E+7 (S) bis(2- Ethylhexyl)phthalate 117817 6.0 (A) 6.0 (A) 25 NLV NLV 340 NA Boron (B) 7440428 500 (F) 500 (F) 7,200 (X) NLV NLV NA ID Bromate 15541454 10 (A) 10 (A) 40 (X) NLV NLV 38,000 ID Bromobenzene (I) 108861 18 50 NA 1.8E+5 3.9E+5 4.13E+5 ID Bromodichloromethane 75274 80 (A,W) 80 (A,W) ID 4,800 37,000 6.74E+6 ID Bromoform 75252 80 (A,W) 80 (A,W) ID 4.7E+5 3.1E+6 (S) 3.10E+6 ID

154 2017 MR 22 – December 15, 2017 Bromomethane 74839 10 29 35 4,000 9,000 1.45E+7 ID n-Butanol (I) 71363 950 2,700 9,800 (X) NLV NLV 7.40E+7 4.7E+7 2-Butanone (MEK) (I) 78933 13,000 38,000 2,200 2.4E+8 (S) 2.4E+8 (S) 2.40E+8 ID n-Butyl acetate 123864 550 1,600 NA 6.7E+6 (S) 6.7E+6 (S) 6.70E+6 2.5E+6 t-Butyl alcohol 75650 3,900 11,000 NA 1.0E+9 (D,S) 1.0E+9 (D,S) 1.00E+9 6.1E+7 Butyl benzyl phthalate 85687 1,200 2,700 (S) 67 (X) NLV NLV 2,690 ID n-Butylbenzene 104518 80 230 ID ID ID NA ID sec-Butylbenzene 135988 80 230 ID ID ID NA ID t-Butylbenzene (I) 98066 80 230 ID ID ID NA ID

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TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Flammability Chemical Residential Surface Volatilization Volatilization and Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air Explosivity Hazardous Service Water Drinking Interface Inhalation Inhalation Water Screening Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Level Cadmium (B) 7440439 5.0 (A) 5.0 (A) (G,X) NLV NLV NA ID Camphene (I) 79925 ID ID NA 440 1,000 33,400 ID Caprolactam 105602 5,800 17,000 NA NLV NLV 5.25E+9 NA Carbaryl 63252 700 2,000 NA ID ID 1.26E+5 ID Carbazole 86748 85 350 10 (M); 4.0 NLV NLV 7,480 ID Carbofuran 1563662 40 (A) 40 (A) NA NLV NLV 7.00E+5 ID Carbon disulfide (I,R) 75150 800 2,300 ID 2.5E+5 5.5E+5 1.19E+6 13,000 Carbon tetrachloride 56235 5.0 (A) 5.0 (A) 45 (X) 370 2,400 7.93E+5 ID 2.0 (M); Chlordane (J) 57749 2.0 (A) 2.0 (A) 0.00025 56 (S) 56 (S) 56 ID Chloride 16887006 2.5E+5 (E) 2.5E+5 (E) (FF) NLV NLV NA ID Chlorobenzene (I) 108907 100 (A) 100 (A) 25 2.1E+5 4.7E+5 (S) 4.72E+5 1.6E+5 p-Chlorobenzene sulfonic acid 98668 7,300 21,000 ID ID ID NA ID 1-Chloro-1,1- difluoroethane 75683 15,000 44,000 NA 3.9E+6 (S) 3.9E+6 (S) 3.90E+6 NA Chloroethane 75003 430 1,700 1,100 (X) 5.7E+6 (S) 5.7E+6 (S) 5.74E+6 1.1E+5 2-Chloroethyl vinyl 110758 ID ID NA ID ID 1.50E+7 ID

156 2017 MR 22 – December 15, 2017 ether Chloroform 67663 80 (A,W) 80 (A,W) 350 28,000 1.8E+5 7.92E+6 ID Chloromethane (I) 74873 260 1,100 ID 8,600 45,000 6.34E+6 36,000 4-Chloro-3- methylphenol 59507 150 420 7.4 NLV NLV 3.90E+6 ID beta- Chloronaphthalene 91587 1,800 5,200 NA ID ID 6,740 ID 2-Chlorophenol 95578 45 130 18 4.9E+5 1.1E+6 2.20E+7 ID o-Chlorotoluene (I) 95498 150 420 ID 2.2E+5 3.7E+5 (S) 3.73E+5 ID 2.0 (M); Chlorpyrifos 2921882 22 63 0.002 2.9 6.6 1,120 ID Chromium (III) (B,H) 16065831 100 (A) 100 (A) (G,X) NLV NLV NA ID Chromium (VI) 18540299 100 (A) 100 (A) 11 NLV NLV NA ID Chrysene (Q) 218019 1.6 (S) 1.6 (S) ID ID ID 1.6 ID Cobalt 7440484 40 100 100 NLV NLV NA ID Copper (B) 7440508 1,000 (E) 1,000 (E) (G) NLV NLV NA ID Cyanazine 21725462 2.3 9.4 56 (X) NLV NLV 1.70E+5 ID

157 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Flammability Chemical Residential Surface Volatilization Volatilization and Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air Explosivity Service Water Drinking Interface Inhalation Inhalation Water Screening Hazardous Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Level Cyanide (P,R) 57125 200 (A) 200 (A) 5.2 NLV NLV NA ID Cyclohexanone 108941 33,000 94,000 NA 1,500 3,300 2.30E+7 NA Dacthal 1861321 73 210 NA NLV NLV 500 ID Dalapon 75990 200 (A) 200 (A) NA NLV NLV 5.02E+8 ID 4-4'-DDD 72548 9.1 37 NA NLV NLV 90 ID 4-4'-DDE 72559 4.3 15 NA NLV NLV 120 ID 0.02 (M); 4-4'-DDT 50293 3.6 10 1.1E-5 NLV NLV 25 NA Decabromodiphenyl ether 1163195 30 (S) 30 (S) NA 30 (S) 30 (S) 30 ID Di-n-butyl phthalate 84742 880 2,500 9.7 NLV NLV 11,200 NA Di(2-ethylhexyl) adipate 103231 400 (A) 400 (A) ID NLV NLV 471 ID Di-n-octyl phthalate 117840 130 380 ID NLV NLV 3,000 ID Diacetone alcohol (I) 123422 ID ID NA NLV NLV 1.00E+9 1.0E+9 (S) 1.0 (M); Diazinon 333415 1.3 3.8 0.004 NLV NLV 68,800 NA Dibenzo(a,h)anthracene 2.0 (M); (Q) 53703 0.21 2.0 (M); 0.85 ID NLV NLV 2.49 ID Dibenzofuran 132649 ID ID 4 10,000 (S) 10,000 (S) 10,000 ID Dibromochloromethane 124481 80 (A,W) 80 (A,W) ID 14,000 1.1E+5 2.60E+6 ID Dibromochloropropane 96128 0.2 (A) 0.2 (A) ID 220 1,200 (S) 1,230 NA Dibromomethane 74953 80 230 NA ID ID 1.10E+7 ID

158 2017 MR 22 – December 15, 2017 Dicamba 1918009 220 630 NA NLV NLV 4.50E+6 ID 1,2-Dichlorobenzene 95501 600 (A) 600 (A) 13 1.6E+5 (S) 1.6E+5 (S) 1.56E+5 NA 1,3-Dichlorobenzene 541731 6.6 19 28 18,000 41,000 1.11E+5 ID 1,4-Dichlorobenzene 106467 75 (A) 75 (A) 17 16,000 74,000 (S) 73,800 NA 3,3'-Dichlorobenzidine 91941 1.1 4.3 0.3 (M); 0.2 NLV NLV 3,110 ID Dichlorodifluoromethane 75718 1,700 4,800 ID 2.2E+5 3.0E+5 (S) 3.00E+5 ID 1,1-Dichloroethane 75343 880 2,500 740 1.0E+6 2.3E+6 5.06E+6 3.8E+5 1,2-Dichloroethane (I) 107062 5.0 (A) 5.0 (A) 360 (X) 9,600 59,000 8.52E+6 2.5E+6 1,1-Dichloroethylene (I) 75354 7.0 (A) 7.0 (A) 130 200 1,300 2.25E+6 97,000 cis-1,2-Dichloroethylene 156592 70 (A) 70 (A) 620 93,000 2.1E+5 3.50E+6 5.3E+5

159 2017 MR 22 – December 15, 2017

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Chemical Residential Surface Volatilization Volatilization Flammability Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air and Explosivity Service Water Drinking Interface Inhalation Inhalation Water Screening Hazardous Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Level trans-1,2- Dichloroethylene 156605 100 (A) 100 (A) 1,500 (X) 85,000 2.0E+5 6.30E+6 2.3E+5 2,6-Dichloro-4- nitroaniline 99309 2,200 6,300 NA NLV NLV 7,000 ID 2,4-Dichlorophenol 120832 73 210 11 NLV NLV 4.50E+6 ID 2,4- Dichlorophenoxyacetic acid 94757 70 (A) 70 (A) 220 NLV NLV 6.80E+5 ID 1,2-Dichloropropane (I) 78875 5.0 (A) 5.0 (A) 230 (X) 16,000 36,000 2.80E+6 5.5E+5 1,3-Dichloropropene 542756 8.5 35 9.0 (X) 3,900 26,000 2.80E+6 1.3E+5 Dichlorovos 62737 1.6 6.7 NA NLV NLV 1.60E+7 NA Dicyclohexyl phthalate 84617 ID ID NA ID ID 4,000 ID 0.02 (M); Dieldrin 60571 0.11 0.43 6.5E-6 200 (S) 200 (S) 195 ID Diethyl ether 60297 10 (E) 10 (E) ID 6.1E+7 (S) 6.1E+7 (S) 6.10E+7 6.5E+5 Diethyl phthalate 84662 5,500 16,000 110 NLV NLV 1.08E+6 NA Diethylene glycol monobutyl ether 112345 88 250 NA NLV NLV 1.00E+9 ID Diisopropyl ether 108203 30 86 ID 8,000 (S) 8,000 (S) 8,041 8,000 (S)

160 2017 MR 22 – December 15, 2017 Diisopropylamine (I) 108189 5.6 16 NA 2.1E+7 3.7E+7 (S) 3.69E+7 4.6E+6 Dimethyl phthalate 131113 73,000 2.10E+05 NA NLV NLV 4.19E+6 NA N,N- Dimethylacetamide 127195 180 520 4,100 (X) NLV NLV 1.00E+9 NA N,N-Dimethylaniline 121697 16 46 NA 2.4E+5 1.3E+6 (S) 1.27E+6 NA Dimethylformamide (I) 68122 700 2,000 NA NLV NLV 1.00E+9 ID 2,4-Dimethylphenol 105679 370 1,000 380 NLV NLV 7.87E+6 ID 2,6-Dimethylphenol 576261 4.4 13 NA NLV NLV 6.14E+6 ID 3,4-Dimethylphenol 95658 10 29 25 NLV NLV 4.93E+6 ID Dimethylsulfoxide 67685 2.2E+5 6.3E+5 1.9E+5 NLV NLV 1.66E+8 ID 2,4-Dinitrotoluene 121142 7.7 32 NA NLV NLV 2.70E+5 ID 1.0 (M); Dinoseb 88857 7.0 (A) 7.0 (A) 0.48 NLV NLV 52,000 ID 1,4-Dioxane (I) 123911 7.2 (II) 350 2,800 (X) NLV NLV 9.00E+8 1.4E+8 Diquat 85007 20 (A) 20 (A) 20 (M); 6.0 NLV NLV 7.00E+5 ID Dissolved oxygen (DO) NA ID ID (EE) ID ID NA NA Diuron 330541 31 90 NA NLV NLV 37,300 ID

161 2017 MR 22 – December 15, 2017

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Chemical Residential Surface Volatilization Volatilization Flammability Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air and Explosivity Service Water Drinking Interface Inhalation Inhalation Water Screening Hazardous Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Level 0.03 (M); Endosulfan (J) 115297 44 130 0.029 ID ID 510 ID Endothall 145733 100 (A) 100 (A) NA NLV NLV 1.00E+8 ID Endrin 72208 2.0 (A) 2.0 (A) ID NLV NLV 250 ID 5.0 (M); 5.0 (M); 2.0 Epichlorohydrin (I) 106898 2.0 (A) (A) NA 3.2E+5 6.3E+5 6.60E+7 4.7E+7 Ethanol (I) 64175 1.9E+6 3.8E+6 ID NLV NLV 1.00E+9 9.7E+7 Ethyl acetate (I) 141786 6,600 19,000 NA 6.4E+7 (S) 6.4E+7 (S) 6.40E+7 4.2E+6 Ethyl-tert-butyl ether (ETBE) 637923 49 (E) 49 (E) ID 2.9E+6 5.6E+6 (S) 5.63E+6 ID Ethylbenzene (I) 100414 74 (E) 74 (E) 18 1.1E+5 1.7E+5 (S) 1.69E+5 43,000 Ethylene dibromide 106934 0.05 (A) 0.05 (A) 5.7 (X) 2,400 15,000 4.20E+6 ID Ethylene glycol 107211 15,000 42,000 1.9E+5 (X) NLV NLV 1.00E+9 NA Ethylene glycol monobutyl ether 111762 3,700 10,000 NA 2.9E+6 6.5E+6 2.24E+8 NA Fluoranthene 206440 210 (S) 210 (S) 1.6 210 (S) 210 (S) 206 ID Fluorene 86737 880 2,000 (S) 12 2,000 (S) 2,000 (S) 1,980 ID Fluorine (soluble fluoride) (B) 7782414 2,000 (E) 2,000 (E) ID NLV NLV NA ID Formaldehyde 50000 1,300 3,800 120 63,000 3.6E+5 5.50E+8 ID

162 2017 MR 22 – December 15, 2017 Formic acid (I,U) 64186 10,000 29,000 ID 7.7E+6 1.5E+7 1.00E+9 1.0E+9 (D) 1-Formylpiperidine 2591868 80 230 NA ID ID NA ID Gentian violet 548629 15 63 NA NLV NLV 1.00E+6 ID Glyphosate 1071836 700 (A) 700 (A) NA NLV NLV 1.16E+7 ID 0.01 (M); Heptachlor 76448 0.4 (A) 0.4 (A) 0.0018 180 (S) 180 (S) 180 ID Heptachlor epoxide 1024573 0.2 (A) 0.2 (A) ID NLV NLV 200 ID n-Heptane 142825 2,700 (S) 2,700 (S) NA 2,700 (S) 2,700 (S) 2,690 200 0.17 (S); Hexabromobenzene 87821 20 0.17 (S); 58 ID ID ID 0.17 ID 0.2 (M); Hexachlorobenzene (C-66) 118741 1.0 (A) 1.0 (A) 0.0003 440 3,000 6,200 ID Hexachlorobutadiene (C- 46) 87683 15 42 0.053 1,600 3,200 (S) 3,230 ID alpha- Hexachlorocyclohexane 319846 0.43 1.7 ID 2,000 (S) 2,000 (S) 2,000 ID beta- Hexachlorocyclohexane 319857 0.88 3.6 ID NLV NLV 240 ID Hexachlorocyclopentadiene (C-56) 77474 50 (A) 50 (A) ID 130 420 1,800 ID

163 2017 MR 22 – December 15, 2017

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Chemical Residential Surface Volatilization Volatilization Flammability Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air and Explosivity Hazardous Service Water Drinking Interface Inhalation Inhalation Water Screening Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Level Hexachloroethane 67721 7.3 21 6.7 (X) 27,000 50,000 (S) 50,000 ID n-Hexane 110543 3,000 8,600 NA 12,000 (S) 12,000 (S) 12,000 12,000 (S) 2-Hexanone 591786 1,000 2,900 ID 4.2E+6 8.7E+6 1.60E+7 NA Indeno(1,2,3- 2.0 (M); 2.0 (M); 0.022 cd)pyrene (Q) 193395 0.022 (S) (S) ID NLV NLV 0.022 ID Iron (B) 7439896 300 (E) 300 (E) NA NLV NLV NA ID Isobutyl alcohol (I) 78831 2,300 6,700 NA 7.6E+7 (S) 7.6E+7 (S) 7.60E+7 ID Isophorone 78591 770 3,100 1,300 (X) NLV NLV 1.20E+7 ID Isopropyl alcohol (I) 67630 470 1,300 57,000 (X) NLV NLV 1.00E+9 6.0E+7 Isopropyl benzene 98828 800 2,300 28 56,000 (S) 56,000 (S) 56,000 29,000 Lead (B) 7439921 4.0 (L) 4.0 (L) (G,X) NLV NLV NA ID 0.03 (M); Lindane 58899 0.2 (A) 0.2 (A) 0.026 ID ID 6,800 ID Lithium (B) 7439932 170 350 440 NLV NLV NA ID Magnesium (B) 7439954 4.0E+5 1.1E+6 NA NLV NLV NA ID Manganese (B) 7439965 50 (E) 50 (E) (G,X) NLV NLV NA ID Mercury (Total) (B,Z) Varies 2.0 (A) 2.0 (A) 0.0013 56 (S) 56 (S) 56 ID Methane 74828 ID ID NA (K) (K) NA (AA)

164 2017 MR 22 – December 15, 2017 Methanol 67561 3,700 10,000 5.9E+5 (X) 2.9E+7 (S) 2.9E+7 (S) 2.90E+7 4.5E+6 Methoxychlor 72435 40 (A) 40 (A) NA ID ID 45 ID 2-Methoxyethanol (I) 109864 7.3 21 NA NLV NLV 1.00E+9 ID 2-Methyl-4- chlorophenoxyacetic acid 94746 7.3 21 NA NLV NLV 9.24E+5 ID 2-Methyl-4,6- 20 (M); dinitrophenol 534521 2.6 20 (M); 7.3 NA NLV NLV 2.00E+5 ID N-Methyl- morpholine (I) 109024 20 56 NA NLV NLV 1.00E+9 ID Methyl parathion 298000 1.8 5.2 NA NLV NLV 50,000 ID 4-Methyl-2- pentanone (MIBK) (I) 108101 1,800 5,200 ID 2.0E+7 (S) 2.0E+7 (S) 2.00E+7 ID Methyl-tert-butyl ether (MTBE) 1634044 40 (E) 40 (E) 7,100 (X) 4.7E+7 (S) 4.7E+7 (S) 4.68E+7 ID Methylcyclopentane (I) 96377 ID ID NA 22,000 49,000 73,890 ID 4,4'-Methylene-bis- 2- chloroaniline 101144 1.1 4.5 NA NLV NLV 14,000 ID Methylene chloride 75092 5.0 (A) 5.0 (A) 1,500 (X) 2.2E+5 1.4E+6 1.70E+7 ID

165 2017 MR 22 – December 15, 2017

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Chemical Residential Surface Volatilization Volatilization Flammability Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air and Explosivity Service Water Drinking Interface Inhalation Inhalation Water Screening Hazardous Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Level 2-Methylnaphthalene 91576 260 750 19 25,000 (S) 25,000 (S) 24,600 ID Methylphenols (J) 1319773 370 1,000 30 (M); 25 NLV NLV 2.80E+7 NA Metolachlor 51218452 240 990 15 NLV NLV 5.30E+5 ID Metribuzin 21087649 180 520 NA ID ID 1.20E+6 ID 0.02 (M); 0.02 (M); 0.02 (M); Mirex 2385855 6.8E-6 (S) 6.8E-6 (S) 6.8E-6 (S) ID ID 6.80E-6 NA Molybdenum (B) 7439987 73 210 3,200 (X) NLV NLV NA ID Naphthalene 91203 520 1,500 11 31,000 (S) 31,000 (S) 31,000 NA Nickel (B) 7440020 100 (A) 100 (A) (G) NLV NLV NA ID 10,000 Nitrate (B,N) 14797558 (A,N) 10,000 (A,N) ID NLV NLV NA ID 1,000 Nitrite (B,N) 14797650 (A,N) 1,000 (A,N) NA NLV NLV NA ID Nitrobenzene (I) 98953 3.4 9.6 180 (X) 2.8E+5 5.5E+5 2.09E+6 NA 2-Nitrophenol 88755 20 58 ID NLV NLV 2.50E+6 ID n-Nitroso-di-n- 5.0 (M); propylamine 621647 0.19 5.0 (M); 0.77 NA NLV NLV 9.89E+6 ID N- Nitrosodiphenylamine 86306 270 1,100 NA NLV NLV 35,100 ID Oxamyl 23135220 200 (A) 200 (A) NA NLV NLV 2.80E+8 ID

166 2017 MR 22 – December 15, 2017 Oxo-hexyl acetate 88230357 73 210 NA ID ID NA ID Pendimethalin 40487421 280 (S) 280 (S) NA NLV NLV 275 ID 5.0 (M); Pentachlorobenzene 608935 6.1 17 0.019 ID ID 650 ID Pentachloronitrobenzene 82688 32 (S) 32 (S) NA 32 (S) 32 (S) 32 ID Pentachlorophenol 87865 1.0 (A) 1.0 (A) (G,X) NLV NLV 1.85E+6 ID Pentane 109660 ID ID NA 38,000 (S) 38,000 (S) 38,200 340 2-Pentene (I) 109682 ID ID NA ID ID 2.03E+5 ID 6.5 to 8.5 pH NA (E) 6.5 to 8.5 (E) 6.5 to 9.0 ID ID NA NA Phenanthrene 85018 52 150 2.0 (M); 1.4 1,000 (S) 1,000 (S) 1,000 ID Phenol 108952 4,400 13,000 450 NLV NLV 8.28E+7 NA Phenytoin 57410 17 68 89 (X) NLV NLV 32,000 ID Phosphorus (Total) 7723140 63,000 2.40E+05 (EE) NLV NLV NA ID Phthalic acid 88993 14,000 40,000 NA NLV NLV 1.42E+7 ID

167 2017 MR 22 – December 15, 2017

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Chemical Residential Surface Volatilization Volatilization Flammability Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air and Explosivity Hazardous Service Water Drinking Interface Inhalation Inhalation Water Screening Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Level Phthalic anhydride 85449 15,000 44,000 NA NLV NLV 6.20E+6 NA Picloram 1918021 500 (A) 500 (A) 46 NLV NLV 4.30E+5 ID Piperidine 110894 3.2 9.2 NA NLV NLV 1.00E+9 ID Polybrominated biphenyls (J) 67774327 0.03 0.09 ID NLV NLV 1.66E+7 ID Polychlorinated biphenyls (PCBs) 0.2 (M); (J,T) 1336363 0.5 (A) 0.5 (A) 2.6E-5 45 (S) 45 (S) 44.7 ID Prometon 1610180 160 460 NA NLV NLV 7.50E+5 ID Propachlor 1918167 95 270 NA NLV NLV 6.55E+5 ID Propazine 139402 200 560 NA NLV NLV 8,600 ID Propionic acid 79094 12,000 35,000 ID NLV NLV 1.00E+9 1.0E+9 (D) Propyl alcohol (I) 71238 1,400 4,000 NA NLV NLV 1.00E+9 7.1E+7 n-Propylbenzene (I) 103651 80 230 ID ID ID NA ID Propylene glycol 57556 1.5E+5 4.2E+5 2.9E+5 NLV NLV 1.00E+9 ID Pyrene 129000 140 (S) 140 (S) ID 140 (S) 140 (S) 135 ID Pyridine (I) 110861 20 (M); 7.3 21 NA 5,500 12,000 3.00E+5 81,000 Selenium (B) 7782492 50 (A) 50 (A) 5 NLV NLV NA ID Silver (B) 7440224 34 98 0.2 (M); NLV NLV NA ID

168 2017 MR 22 – December 15, 2017 0.06 Silvex (2,4,5-TP) 93721 50 (A) 50 (A) 30 NLV NLV 1.40E+5 ID Simazine 122349 4.0 (A) 4.0 (A) 17 NLV NLV 4,470 ID Sodium 17341252 2.3E+S(HH) 3.5E+5 NA NLV NLV NA ID Sodium azide 26628228 88 250 50 (M); 7.3 ID ID NA ID Strontium (B) 7440246 4,600 13,000 21,000 NLV NLV NA ID Styrene 100425 100 (A) 100 (A) 80 (X) 1.7E+5 3.1E+5 (S) 3.10E+5 1.4E+5 Sulfate 14808798 2.5E+5 (E) 2.5E+5 (E) NA NLV NLV NA ID Tebuthiuron 34014181 510 1,500 NA NLV NLV 2.50E+6 ID 2,3,7,8- Tetrabromodibenzo- p-dioxin (O) 50585416 (O) (O) (O) NLV NLV 0.00996 ID 1,2,4,5- Tetrachlorobenzene 95943 1,300 (S) 1,300 (S) 2.9 (X) 1,300 (S) 1,300 (S) 1,300 ID 2,3,7,8- Tetrachlorodibenzo- 1.0E-5 (M); p-dioxin (O) 1746016 3.0E-5 (A) 3.0E-5 (A) 3.1E-9 NLV NLV 0.019 ID 1,1,1,2- Tetrachloroethane 630206 77 320 ID 15,000 96,000 1.10E+6 ID

169 2017 MR 22 – December 15, 2017

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Chemical Residential Surface Volatilization Volatilization Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air Flammability Service Water Drinking Interface Inhalation Inhalation Water and Explosivity Hazardous Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Screening Level 1,1,2,2- Tetrachloroethane 79345 8.5 35 78 (X) 12,000 77,000 2.97E+6 ID Tetrachloroethylene 127184 5.0 (A) 5.0 (A) 60 (X) 25,000 1.7E+5 2.00E+5 ID Tetrahydrofuran 109999 95 270 11,000 (X) 6.9E+6 1.6E+7 1.00E+9 60,000 Tetranitromethane 509148 ID ID NA 580 3,200 85,000 ID Thallium (B) 7440280 2.0 (A) 2.0 (A) 3.7 (X) NLV NLV NA ID Toluene (I) 108883 790 (E) 790 (E) 270 5.3E+5 (S) 5.3E+5 (S) 5.26E+5 61,000 p-Toluidine 106490 15 62 NA NLV NLV 7.60E+6 NA Total dissolved solids (TDS) NA 5.0E+5 (E) 5.0E+5 (E) (EE) ID ID NA NA 1.0 (M); Toxaphene 8001352 3.0 (A) 3.0 (A) 6.8E-5 NLV NLV 740 ID Triallate 2303175 95 270 NA ID ID 4,000 ID Tributylamine 102829 10 29 ID 14,000 32,000 75,400 ID 1,2,4-Trichlorobenzene 120821 70 (A) 70 (A) 99 (X) 3.0E+5 (S) 3.0E+5 (S) 3.00E+5 NA 1,1,1-Trichloroethane 71556 200 (A) 200 (A) 89 6.6E+5 1.3E+6 (S) 1.33E+6 ID 1,1,2-Trichloroethane 79005 5.0 (A) 5.0 (A) 330 (X) 17,000 1.1E+5 4.42E+6 NA Trichloroethylene 79016 5.0 (A) 5.0 (A) 200 (X) 2,200 4,900 1.10E+6 ID Trichlorofluoromethane 75694 2,600 7,300 NA 1.1E+6 (S) 1.1E+6 (S) 1.10E+6 ID 2,4,5-Trichlorophenol 95954 730 2,100 NA NLV NLV 1.20E+6 ID

170 2017 MR 22 – December 15, 2017 2,4,6-Trichlorophenol 88062 120 470 5 NLV NLV 8.00E+5 ID 1,2,3-Trichloropropane 96184 42 120 NA 8,300 18,000 1.90E+6 NA 1,1,2-Trichloro-1,2,2- trifluoroethane 76131 1.7E+5 (S) 1.7E+5 (S) 32 1.7E+5 (S) 1.7E+5 (S) 1.70E+5 ID Triethanolamine 102716 3,700 10,000 NA NLV NLV 1.00E+9 ID Triethylene glycol 112276 4,300 12,000 NA NLV NLV 1.00E+6 ID 3-Trifluoromethyl-4- nitrophenol 88302 4,500 13,000 NA NLV NLV 5.00E+6 ID Trifluralin 1582098 37 110 NA ID ID 8,100 ID 2,2,4-Trimethyl pentane 540841 ID ID NA 2,300 (S) 2,300 (S) 2,330 160 2,4,4-Trimethyl-2- pentene (I) 107404 ID ID NA ID ID 11,900 ID 1,2,4-Trimethylbenzene (I) 95636 63 (E) 63 (E) 17 56,000 (S) 56,000 (S) 55,890 56,000 (S) 1,3,5-Trimethylbenzene (I) 108678 72 (E) 72 (E) 45 61,000 (S) 61,000 (S) 61,150 ID

171 2017 MR 22 – December 15, 2017

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (ug/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based or solubility value, whichever is lower. Residential Nonresidential Groundwater Groundwater Groundwater Chemical Residential Surface Volatilization Volatilization Abstract Drinking Nonresidential Water to Indoor Air to Indoor Air Flammability Service Water Drinking Interface Inhalation Inhalation Water and Explosivity Hazardous Substance Number Criteria Water Criteria Criteria Criteria Criteria Solubility Screening Level Triphenyl phosphate 115866 1,200 1,400 (S) NA NLV NLV 1,430 ID tris(2,3- 10 (M); Dibromopropyl)phosphate 126727 0.71 10 (M); 2.9 ID 4,700 (S) 4,700 (S) 4,700 ID Urea 57136 ID ID NA NLV NLV NA ID Vanadium 7440622 4.5 62 27 NLV NLV NA ID Vinyl acetate (I) 108054 640 1,800 NA 4.1E+6 8.9E+6 2.00E+7 1.8E+6 Vinyl chloride 75014 2.0 (A) 2.0 (A) 13 (X) 1,100 13,000 2.76E+6 33,000 White phosphorus (R) 12185103 0.11 0.31 NA NLV NLV NA ID Xylenes (I) 1330207 280 (E) 280 (E) 41 1.9E+5 (S) 1.9E+5 (S) 1.86E+5 70,000 Zinc (B) 7440666 2,400 5,000 (E) (G) NLV NLV NA ID

172 2017 MR 22 – December 15, 2017

R 299.46 Generic soil cleanup criteria and screening levels for residential catergory. Rule 46 (1) The generic groundwater cleanup criteria is as shown in table 1. The cleanup criteria designated as residential are the cleanup criteria for unrestricted residential use as defined by sections 20101(1)(i) and 20120e(1)(a) of the act. (2) The generic soil cleanup criteria for residential category shall beis as shown in table 2. These cleanup criteria are the cleanup criteria for unrestricted residential use as defined by sections 20101(1)(i) and 20120e(1)(a) of the act. (3) The generic soil cleanup criteria for nonresidential category is as shown in table 3. (4) The VIAP screening levels for groundwater, soil, and soil gas is shown as table 4. (5) Abbreviations and definitions have the following meanings when used in the tables of this rule: (a) “aes” means the criterion is based on aesthetic value pursuant to R 299.9. (b) “ca” means the criterion is based on carcinogenic health effects. (c) “dev” means the criterion is based on developmental health effects. (d) “max” means the criterion is based on the maximum ceiling concentration pursuant to R 299.6(5). (e) “mut” means the criterion is based on mutagenic cancer effects. (f) “nc” means the criterion is based on noncarcinogenic health effects. (g) “sdws” means the criterion is based on the state drinking water standard. (h) “sol” means the criterion is based on solubility. (i) “st” means the criterion is based on short-term toxicity. (j) “swpv” means the criterion is based on the soil water partition value. (k) “20x” means the criterion is based on the groundwater criterion multiplied by 20. (6) Tables 1 to 4 of this rule read as follows:

173 2017 MR 22 – December 15, 2017

TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 360 1,100 3.90E+03 NA Acenaphthene 83329 nc nc 360 1,100 1.61E+04 NA Acenaphthylene 208968 nc nc 770 2,500 1.00E+09 1.1E+07 Acetaldehyde (I) 75070 nc nc 3,400 11,000 1.00E+09 NA Acetate 71501 nc nc 3,400 11,000 1.00E+09 1.0E+09 (S) Acetic acid 64197 nc nc sol 5,300 17,000 1.00E+09 1.7E+07 Acetone (I) 67641 nc nc 360 1,100 1.00E+09 1.4E+07 Acetonitrile 75058 nc nc 3,200 (DD) 13,000 (DD) 6.13E+06 NA Acetophenone (DD) 98862 dev dev 24 76 2.1E+08 5.1E+06 Acrolein (I) 107028 nc nc 0.0005 mg/l (A) 0.0005 mg/l (A) 3.90E+08 NA Acrylamide (MM) 79061 sdws sdws 800 (DD) 3,800 1.00E+09 1.0E+09 (S) Acrylic acid (DD) 79107 dev nc sol 1.3 (M) 6.8 7.45E+07 4.6E+06 Acrylonitrile (I) 107131 ca ca 0.002 mg/l (A) 0.002 mg/l (A) 2.40E+05 NA Alachlor 15972608 sdws sdws 0.003 mg/l (A) 0.003 mg/l (A) 6.03E+06 NA Aldicarb 116063 sdws sdws 0.002 mg/l (A) 0.002 mg/l(A) 1.00E+07 NA Aldicarb sulfone 1646884 sdws sdws 0.004 mg/l (A) 0.004 mg/l (A) 2.80E+07 NA Aldicarb sulfoxide 1646873 sdws sdws

174 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 0.043 0.22 1.70E+01 NA Aldrin 309002 ca ca 0.05 mg/l (E,V) 0.05 mg/l (E,V) NA NA Aluminum (B, DD) 7429905 aes aes 10,000 (N) 10,000 (N) 4.82E+08 NA Ammonia (N) 7664417 na na 190 (E) 190 (E) 1.07E+07 3.4E+05 t-Amyl methyl ether (TAME) 994058 aes aes 42 130 3.60E+07 NA Aniline 62533 nc nc 43 (S) 43 (S) 4.34E+01 NA Anthracene 120127 sol sol 0.006 mg/l (A) 0.006 mg/l (A) NA NA Antimony 7440360 sdws sdws 0.010 mg/l (A) 0.010 mg/l (A) NA NA Arsenic (B,KK) 7440382 sdws sdws 7 MFL (A,BB) 7 MFL (A,BB) NA NA Asbestos (BB) 1332214 sdws sdws 0.003 mg/l (A) 0.003 mg/l (A) 3.47E+04 NA Atrazine 1912249 sdws sdws 6.6 33 6.40E+03 NA Azobenzene 103333 ca ca 2 mg/l (A) 2 mg/l (A) NA NA Barium (B,KK) 7440393 sdws sdws 0.005 mg/l (A) 0.005 mg/l (A) 1.79E+06 68,000 Benzene (I,KK) 71432 sdws sdws 0.0010 (M) 0.016 (M) 3.22E+05 NA Benzidine (MM) 92875 mut ca 2.3 (MM) 9.4 (S) 9.4E+00 NA Benzo(a)anthracene (Q,MM) 56553 mut sol 1.5 (S) 1.5 (S) 1.5E+00 NA Benzo(b)fluoranthene (Q,MM) 205992 sol sol

175 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 0.80 (M,S) 0.80 (M,S) 8.0E-01 NA Benzo(k)fluoranthene (Q,MM) 207089 sol sol 0.26 (M,S) 0.26 (M,S) 2.60E-01 NA Benzo(g,h,i)perylene 191242 sol sol 0.0002 mg/l (A) 0.0002 mg/l (A) 1.6E+00 NA Benzo(a)pyrene (Q,DD,MM) 50328 sdws sdws 24,000 76,000 3.40E+06 NA Benzoic acid 65850 nc nc 830 2,600 4.29E+07 NA Benzyl alcohol 100516 nc nc 4.3 (M) 22 5.25E+05 NA Benzyl chloride 100447 ca ca 0.004 mg/l (A) 0.004 mg/l (A) NA NA Beryllium (B) 7440417 sdws sdws 1.5 (M) 4.7 (M) 1.89E+07 NA bis(2-Chloroethoxy)ethane 112265 nc nc 0.66 (M) 3.3 1.72E+07 1.7E+07 (S) bis-2-Chloroethylether (I) 111444 ca ca sol 0.006 mg/l (A) 0.006 mg/l (A) 2.70E+02 NA bis(2-Ethylhexyl) phthalate (DD) 117817 sdws sdws 800 (F,DD) 3,300 (F,DD) NA NA Boron (DD) 7440428 dev dev 0.010 mg/l (A) 0.010 mg/l (A) NA NA Bromate 15541454 sdws sdws 47 150 4.46E+05 4.5E+05 (S) Bromobenzene (I) 108861 nc nc sol 0.080 mg/l (A,W) 0.080 mg/l (A,W) 3.03E+06 NA Bromodichloromethane (DD) 75274 sdws sdws 0.080 mg/l (A,W) 0.080 mg/l (A,W) 3.10E+06 NA Bromoform 75252 sdws sdws 120 380 1.52E+07 NA Bromomethane 74839 nc nc

176 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 590 (M) 1,900 6.30E+07 4.7E+07 n-Butanol (I) 71363 nc nc 2,400 (DD) 11,000 2.23E+08 7.1E+06 2-Butanone (MEK) (I,DD,KK) 78933 dev nc 590 1,900 8.40E+06 2.8E+06 n-Butyl acetate 123864 nc nc 1,100 3,400 1.00E+09 7.9E+07 t-Butyl alcohol 75650 nc nc 80 (DD) 330 (DD) 2.69E+03 NA Butyl benzyl phthalate (DD) 85687 dev dev 270 870 1.18E+03 NA n-Butylbenzene 104518 nc nc 590 1,900 1.76E+04 18,000 (S) sec-Butylbenzene 135988 nc nc sol 590 1,900 2.95E+04 NA t-Butylbenzene (I) 98066 nc nc 0.005 mg/l (A) 0.005 mg/l (A) NA NA Cadmium (B,KK) 7440439 sdws sdws NA NA 4.60E+03 NA Camphene (I) 79925

2,000 (DD) 9,400 7.72E+08 NA Caprolactam (DD) 105602 dev nc 40 (DD) 170 (DD) 1.10E+05 NA Carbaryl (DD) 63252 dev dev 7.4 (M) 38 1.80E+03 NA Carbazole 86748 ca ca 0.04 mg/l (A) 0.04 mg/l (A) 3.20E+05 NA Carbofuran (DD) 1563662 sdws sdws 440 (DD) 1,800 (DD) 2.16E+06 27,000 Carbon disulfide (I,R,DD) 75150 dev dev 0.005 mg/l (A) 0.005 mg/l (A) 7.93E+05 NA Carbon tetrachloride (KK) 56235 sdws sdws

177 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 0.002 mg/l (A) 0.002 mg/l (A) 5.60E+01 NA Chlordane (J,KK) 57749 sdws sdws 250 mg/l (E) 250 mg/l (E) NA NA Chloride 16887006 aes aes 18 57 8.16E+06 NA 2-Chloroaniline 95512 nc nc 3.0 9.4 3.90E+06 NA 4-Chloroaniline 106478 nc nc 0.1 mg/l (A) 0.1 mg/l (A) 4.98E+05 1.9E+05 Chlorobenzene (I,KK) 108907 sdws sdws 4,700 15,000 3.06E+08 NA p-Chlorobenzene sulfonic acid 98668 nc nc 12,000 40,000 1.40E+06 NA 1-Chloro-1,1-difluoroethane 75683 nc nc 240 760 6.71E+06 88,000 Chloroethane (DD) 75003 nc nc NA NA 4.29E+05 NA 2-Chloroethyl vinyl ether 110758

0.080 mg/l (A,W) 0.080 mg/l (A,W) 7.95E+06 NA Chloroform (KK) 67663 sdws sdws 220 1,100 5.32E+06 NA Chloromethane (I) 74873 ca ca 400 (DD) 1,700 (DD) 3.83E+06 NA 4-Chloro-3-methylphenol (DD) 59507 dev dev 470 1,500 1.17E+04 NA beta-Chloronaphthalene 91587 nc nc 32 (DD) 130 (DD) 1.13E+07 NA 2-Chlorophenol (DD) 95578 dev dev 40 130 3.74E+05 1.4E+05 o-Chlorotoluene (I) 95498 nc nc 19 (DD) 78 (DD) 1.12E+03 NA Chlorpyrifos (DD) 2921882 dev dev

178 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 0.1 mg/l (A) 0.1 mg/l (A) NA NA Chromium (III) (B,H,KK) 16065831 sdws sdws 0.1 mg/l (A) 0.1 mg/l (A) NA NA Chromium (VI) (H,KK,MM) 18540299 sdws sdws 2.0 (S) 2.0 (S) 2.0E+00 NA Chrysene (Q,MM) 218019 sol sol 1.8 (M) 5.7 (M) NA NA Cobalt (B) 7440484 nc nc 1.0 mg/l (E) 1.0 mg/l (E) NA NA Copper (B) 7440508 aes aes 1.2 (M) 3.8 1.70E+05 NA Cyanazine 21725462 nc nc 0.2 mg/l (A) 0.2 mg/l (A) 1.0E+09 4.6E+06 Cyanide (P,R,DD) Varies sdws sdws NA NA 5.50E+04 2,900 Cyclohexane (DD) 110827

1,200 3,800 2.50E+07 2.5E+07 (S) Cyclohexanone 108941 nc nc sol 59 190 5.00E+02 NA Dacthal 1861321 nc nc 0.2 mg/l (A) 0.2 mg/l (A) 5.02E+08 NA Dalapon 75990 sdws sdws 3.0 15 9.00E+01 NA 4-4'-DDD 72548 ca ca 2.1 11 4.00E+01 NA 4-4'-DDE 72559 ca ca 2.0 (DD) 5.5 (S) 5.50E+00 NA 4-4'-DDT (DD) 50293 dev sol 0.10 (M,S) 0.10 (M,S) 1.00E-01 NA Decabromodiphenyl ether (DD) 1163195 sol sol 27 (DD) 110 (DD) 1.12E+04 NA Di-n-butyl phthalate (DD) 84742 dev dev

179 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 0.4 mg/l (A) 0.4 mg/l (A) 7.80E+02 NA Di(2-ethylhexyl) adipate (DD) 103231 sdws sdws 22 (S) 22 (S) 2.20E+01 NA Di-n-octyl phthalate 117840 sol sol NA NA 1.00E+09 1.0E+09 (S) Diacetone alcohol (I) 123422 sol 4.2 13 4.00E+04 NA Diazinon 333415 nc nc 0.23 (M) 2.5 (S) 2.5E+00 NA Dibenzo(a,h)anthracene (Q,MM) 53703 mut sol 5.9 19 3.10E+03 NA Dibenzofuran 132649 nc nc 0.080 mg/l (A,W) 0.080 mg/l (A,W) 2.70E+06 NA Dibromochloromethane (MM) 124481 sdws sdws 0.0002 mg/l (A) 0.0002 mg/l (A) 1.23E+06 NA Dibromochloropropane (MM) 96128 sdws sdws 18 57 1.19E+07 NA Dibromomethane 74953 nc nc 1,800 (DD) 8,500 8.31E+06 NA Dicamba (DD) 1918009 dev nc 0.6 mg/l (A) 0.6 mg/l (A) 1.56E+05 NA 1,2-Dichlorobenzene 95501 sdws sdws 12 38 1.25E+05 NA 1,3-Dichlorobenzene 541731 nc nc 0.075 mg/l (A) 0.075 mg/l (A) 8.13E+04 NA 1,4-Dichlorobenzene (KK) 106467 sdws sdws 1.6 8.2 3.10E+03 NA 3,3`-Dichlorobenzidine 91941 ca ca 30 94 2.80E+05 NA Dichlorodifluoromethane 75718 nc nc 130 650 5.04E+06 3.8E+05 1,1-Dichloroethane 75343 ca ca

180 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 0.005 mg/l (A) 0.005 mg/l (A) 8.60E+06 2.1E+06 1,2-Dichloroethane (I,KK) 107062 sdws sdws 0.007 mg/l (A) 0.007 mg/l (A) 2.42E+06 97,000 1,1-Dichloroethylene (I,KK) 75354 sdws sdws 0.07 mg/l (A) 0.07 mg/l (A) 6.41E+06 2.9E+05 cis-1,2-Dichloroethylene 156592 sdws sdws 0.1 mg/l (A) 0.1 mg/l (A) 4.52E+06 2.5E+05 trans-1,2-Dichloroethylene 156605 sdws sdws 15 47 7.00E+03 NA 2,6-Dichloro-4-nitroaniline 99309 nc nc 80 (DD) 380 5.55E+06 NA 2,4-Dichlorophenol (DD) 120832 dev nc 0.07 mg/l (A) 0.07 mg/l (A) 6.77E+05 NA 2,4-Dichlorophenoxyacetic acid (KK) 94757 sdws sdws 0.005 mg/l (A) 0.005 mg/l (A) 2.80E+06 5.4E+05 1,2-Dichloropropane (I) 78875 sdws sdws 7.2 37 2.80E+06 6.6E+05 1,3-Dichloropropene (J) 542756 ca ca 0.78 (M) 9.4 8.00E+06 NA Dichlorvos (MM) 62737 mut nc NA NA 4.00E+03 NA Dicyclohexyl phthalate 84617

0.045 0.23 1.95E+02 NA Dieldrin 60571 ca ca 1.2 (E,M) 1.2 (E, M) 6.00E+07 4.6E+05 Diethyl ether 60297 aes aes 4,700 15,000 1.08E+06 NA Diethyl phthalate 84662 nc nc 180 570 1.00E+09 NA Diethylene glycol monobutyl ether 112345 nc nc 1,100 (DD) 4,500 (DD) 8.80E+06 2.2E+05 Diisopropyl ether (DD) 108203 dev dev

181 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 4.6 15 1.10E+08 4.6E+06 Diisopropylamine (I) 108189 nc nc 590 1,900 4.00E+06 NA Dimethyl phthalate 131113 nc nc 150 470 1.00E+09 NA N,N-Dimethylacetamide 127195 nc nc 12 38 1.45E+06 NA N,N-Dimethylaniline 121697 nc nc 590 1,900 1.00E+09 1.0E+09 (S) Dimethylformamide (I) 68122 nc nc sol 120 380 7.87E+06 NA 2,4-Dimethylphenol 105679 nc nc 3.6 (M) 11 6.05E+06 NA 2,6-Dimethylphenol 576261 nc nc 5.9 19 4.76E+06 NA 3,4-Dimethylphenol 95658 nc nc 5,900 19,000 1.00E+09 NA Dimethylsulfoxide 67685 nc nc 12 38 2.79E+06 NA 2,4-Dinitrophenol 51285 nc nc 1.1 5.5 2.00E+05 NA 2,4-Dinitrotoluene (KK) 121142 ca ca 0.007 mg/l (A) 0.007 mg/l (A) 5.20E+04 NA Dinoseb (DD) 88857 sdws sdws 7.2 37 1.00E+09 1.5E+08 1,4-Dioxane (I) 123911 ca ca 0.02 mg/l (A) 0.02 mg/l (A) 7.08E+08 NA Diquat 85007 sdws sdws NA NA NA NA Dissolved oxygen (DO) NA

18 57 4.20E+04 NA Diuron 330541 nc nc

182 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 30 94 3.25E+02 NA Endosulfan (J) 115297 nc nc 0.1 mg/l (A) 0.1 mg/l (A) 1.00E+08 NA Endothall 145733 sdws sdws 0.002 mg/l (A) 0.002 mg/l (A) 2.50E+02 NA Endrin (KK) 72208 sdws sdws 0.002 mg/l (A) 0.002 mg/l (A) 6.59E+07 4.8E+07 Epichlorohydrin (I) 106898 sdws sdws 1.2E+06 (DD) 5.2E+06 (DD) 1.00E+09 1.2E+08 Ethanol (I,DD) 64175 dev dev 430 1,400 8.00E+07 5.3E+06 Ethyl acetate (I) 141786 nc nc 49 (E) 49 (E) 1.2E+07 3.1E+05 Ethyl-tert-butyl ether (ETBE) 637923 aes aes 74 (E) 74 (E) 1.69E+05 43,000 Ethylbenzene (I) 100414 aes aes 0.00005 mg/l (A) 0.00005 mg/l (A) 3.91E+06 NA Ethylene dibromide 106934 sdws sdws 3,200 (M) 13,000 (DD) 1.00E+09 NA Ethylene glycol (DD) 107211 dev dev 590 1,900 1.00E+09 NA Ethylene glycol monobutyl ether 111762 nc nc NA NA 1.00E+06 NA Ethylenediaminetetraacetic acid (EDTA) (II) 60004

240 260 (S) 2.60E+02 NA Fluoranthene 206440 nc sol 240 760 1.69E+03 NA Fluorene 86737 nc nc 1,700 (S) 1,700 (S) 1.69E+03 NA Fluorine (soluble fluoride) (DD) 7782414 sol sol 1,200 3,800 4.0E+08 NA Formaldehyde (MM) 50000 nc nc

183 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 5,300 17,000 1.00E+09 1.0E+9 (S) Formic acid (I,U) 64186 nc nc sol 4,400 (DD) 18,000 (DD) 9.58E+07 NA 1-Formylpiperidine (DD) 2591868 dev dev 13 67 4.00E+06 NA Gentian violet 548629 ca ca 0.7 mg/l (A) 0.7 mg/l (A) 1.05E+07 NA Glyphosate (DD) 1071836 sdws sdws 0.0004 mg/l (A) 0.0004 mg/l (A) 1.80E+02 NA Heptachlor (DD,KK) 76448 sdws sdws 0.0002 mg/l (A) 0.0002 mg/l (A) 2.00E+02 NA Heptachlor epoxide (KK) 1024573 sdws sdws 3,400 (S) 3,400 (S) 3.40E+03 210 n-Heptane 142825 sol sol 0.16 (S) 0.16 (S) 1.60E-01 NA Hexabromobenzene 87821 sol sol 0.001 mg/l (A) 0.001 mg/l (A) 6.20E+00 NA Hexachlorobenzene (C-66) (KK) 118741 sdws sdws 5.9 19 3.20E+03 NA Hexachlorobutadiene (C-46) (KK) 87683 nc nc 0.11 0.58 2.00E+03 NA alpha-Hexachlorocyclohexane 319846 ca ca 0.36 1.1 2.40E+02 NA beta-Hexachlorocyclohexane 319857 nc nc 0.05 mg/l (A) 0.05 mg/l (A) 1.80E+03 NA Hexachlorocyclopentadiene (C-56) 77474 sdws sdws 4.2 (M) 13 5.00E+04 NA Hexachloroethane (KK) 67721 nc nc 1,800 5,700 9.50E+03 210 n-Hexane 110543 nc nc 30 (M) 94 1.72E+07 4.3E+06 2-Hexanone 591786 nc nc

184 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 0.19 (M,S) 0.19 (M,S) 1.9E-01 NA Indeno(1,2,3-cd)pyrene (Q,MM) 193395 sol sol 0.3 mg/l (E) 0.3 mg/l (E) NA NA Iron (B) 7439896 aes aes 1,800 5,700 8.50E+07 5.2E+07 Isobutyl alcohol (I) 78831 nc nc 760 3,800 1.20E+07 NA Isophorone (DD) 78591 ca nc 8,000 (DD) 38,000 1.00E+09 5.9E+07 Isopropyl alcohol (I,DD) 67630 dev nc 590 1,900 6.13E+04 38,000 Isopropyl benzene 98828 nc nc 1.0 (L,DD) 1.0 (L,DD) NA NA Lead (B,L,DD,KK) 7439921 dev dev 0.0002 mg/l (A) 0.0002 mg/l (A) 7.30E+03 NA Lindane (KK) 58899 sdws sdws 8.0 (M) 33 (DD) NA NA Lithium (B,DD) 7439932 dev dev 3.3E+05 1.0E+06 NA NA Magnesium 7439954 nc nc 0.05 mg/l (E) 0.05 mg/l (E) NA NA Manganese (B) 7439965 aes aes 0.002 mg/l (A) 0.002 mg/l (A) 6.00E+02 NA Mercury (Total) (Z,DD,KK) Varies sdws sdws NA NA NA 10,000 (AA) Methane (K,AA) 74828

8,000 (DD) 33,000 (DD) 1.00E+09 1.7E+08 Methanol (DD) 67561 dev dev 0.04 mg/l (A) 0.04 mg/l (A) 1.00E+02 NA Methoxychlor (DD,KK) 72435 sdws sdws 20 (DD) 83 (DD) 1.00E+09 1.0E+9 (S) 2-Methoxyethanol (I,DD) 109864 dev dev sol

185 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 26 83 6.30E+05 NA 2-Methyl-4-chlorophenoxyacetic acid 94746 nc nc 2.4 (M) 7.6 (M) 1.98E+05 NA 2-Methyl-4,6-dinitrophenol 534521 nc nc 420 1,300 1.00E+09 NA N-Methyl-morpholine (I) 109024 nc nc 1.2 3.8 3.77E+04 NA Methyl parathion 298000 nc nc 300 940 1.90E+07 3.5E+06 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 nc nc 40 (E) 40 (E) 5.10E+07 9.6E+05 Methyl-tert-butyl ether (MTBE) 1634044 aes aes 12 38 5.62E+06 NA N-methylaniline 100618 nc nc NA NA 4.20E+04 930 Methylcyclopentane (I) 96377

12 38 1.39E+04 NA 4,4`-Methylene-bis-2- chloroaniline (MBOCA) (MM) 101144 nc nc 0.005 mg/l (A) 0.005 mg/l (A) 1.30E+07 NA Methylene chloride (MM) 75092 sdws sdws 24 76 2.46E+04 NA 2-Methylnaphthalene 91576 nc nc 30 94 2.20E+07 NA Methylphenols (JJ,KK) 1319773 nc nc 800 (DD) 3,800 2.59E+07 NA 2-Methylphenol (DD,KK) 95487 dev nc 590 1,900 5.30E+05 NA Metolachlor 51218452 nc nc 77 250 1.05E+06 NA Metribuzin 21087649 nc nc 0.78 3.8 8.50E+01 NA Mirex 2385855 ca nc

186 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 59 190 NA NA Molybdenum 7439987 nc nc 590 1,900 3.10E+04 NA Naphthalene 91203 nc nc 36 110 NA NA Nickel (B) 7440020 nc nc 10 mg/l (A,N) 10 mg/l (A,N) NA NA Nitrate (N,DD) 14797558 sdws sdws 1 mg/l (A,N) 1 mg/l (A,N) NA NA Nitrite (N,DD) 14797650 sdws sdws 12 38 2.09E+06 NA Nitrobenzene (I,KK) 98953 nc nc 12 38 2.50E+06 NA 2-Nitrophenol 88755 nc nc 0.10 (M) 0.53 (M) 1.30E+07 NA n-Nitroso-di-n-propylamine 621647 ca ca 150 750 3.50E+04 NA N-Nitrosodiphenylamine 86306 ca ca 0.2 mg/l (A) 0.2 mg/l (A) 2.80E+08 NA Oxamyl 23135220 sdws sdws 59 190 NA NA Oxo-hexyl acetate 88230357 nc nc 330 (S) 330 (S) 3.30E+02 NA Pendimethalin (DD) 40487421 sol sol 4.7 (M) 15 8.31E+02 NA Pentachlorobenzene 608935 nc nc 18 (M) 57 4.40E+02 NA Pentachloronitrobenzene 82688 nc nc 0.001 mg/l (A) 0.001 mg/l (A) 1.40E+04 NA Pentachlorophenol (KK) 87865 sdws sdws NA NA 3.80E+04 320 Pentane 109660

187 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level NA NA 2.03E+05 NA 2-Pentene (I) 109682

2.8 (M) 12 (DD) NA NA Perchlorate (DD) 14797730 dev dev 0.070 (NN) 0.070 (NN) 9.50E+06 NA Perfluorooctanoic acid (DD) 335671 dev dev 0.070 (NN) 0.070 (NN) 3.1E+00 NA Perfluorooctane sulfonic acid (DD) 1763231 dev dev 6.5-8.5 (E) 6.5-8.5 (E) NA NA pH NA aes aes 180 570 1.15E+03 NA Phenanthrene 85018 nc nc 1,200 (DD) 5,700 8.28E+07 NA Phenol (DD) 108952 dev nc 14 (M) 72 3.20E+04 NA Phenytoin (DD) 57410 ca ca NA NA NA NA Phosphorus, Total Varies

0.08 (M) 0.33 (M) 3.30E+03 NA Phosphorus, White (R,DD) 7723140 dev dev 11,000 36,000 6.97E+06 NA o-Phthalic acid 88993 nc nc 12,000 38,000 6.20E+06 NA Phthalic anhydride 85449 nc nc 0.5 mg/l (A) 0.5 mg/l (A) 4.30E+05 NA Picloram 1918021 sdws sdws 2.6 8.3 1.00E+09 NA Piperidine 110894 nc nc 0.10 0.51 1.10E+01 NA Polybrominated biphenyls (J,DD) 67774327 ca ca 0.0005 mg/l (A) 0.0005 mg/l (A) 7.00E+02 NA Polychlorinated biphenyls (PCBs) (J,T,DD) 1336363 sdws sdws

188 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level (O) (O) NA NA Polychlorinated biphenyls (PCBs) congeners (O) Varies

300 940 7.50E+05 NA Prometon 1610180 nc nc 23 (M) 120 5.80E+05 NA Propachlor 1918167 ca ca 110 340 8.60E+03 NA Propazine 139402 nc nc 11,000 34,000 1.00E+09 1.0E+09 (S) Propionic acid 79094 nc nc sol 8,000 (DD) 33,000 (DD) 1.00E+09 7.1E+07 Propyl alcohol (I,DD) 71238 dev dev 590 1,900 5.22E+04 37,000 n-Propylbenzene (I,DD) 103651 nc nc 1.2E+05 3.8E+05 1.00E+09 NA Propylene glycol 57556 nc nc 140 (S) 140 (S) 1.35E+02 NA Pyrene 129000 sol sol 5.9 (M) 19 (M) 1.00E+09 5.2E+07 Pyridine (I,KK) 110861 nc nc 0.05 mg/l (A) 0.05 mg/l (A) NA NA Selenium (B,KK) 7782492 sdws sdws 0.1 mg/l (E) 0.1 mg/l (E) NA NA Silver (KK) 7440224 aes aes 0.05 mg/l (A) 0.05 mg/l (A) 7.10E+04 NA Silvex (2,4,5-TP) (KK) 93721 sdws sdws 0.004 mg/l (A) 0.004 mg/l (A) 6.20E+03 NA Simazine 122349 sdws sdws 2.3E+5 (HH) 1.8E+05 NA NA Sodium 17341252 nc 71 230 NA NA Sodium azide 26628228 nc nc

189 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 240 760 9.46E+08 NA Sodium bromide 7647156 nc nc 2,400 (DD) 11,000 NA NA Strontium (B,DD) 7440246 dev nc 0.1 mg/l (A) 0.1 mg/l (A) 3.10E+05 1.4E+05 Styrene 100425 sdws sdws 250 mg/l (E) 250 mg/l (E) NA NA Sulfate 14808798 aes aes 5.9 (M) 19 1.0E+09 NA Sulfolane 126330 nc nc 280 (DD) 1,300 2.50E+06 NA Tebuthiuron (DD) 34014181 dev nc (O) (O) 9.96E-03 NA 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416

28 (DD) 120 (DD) 5.95E+02 NA 1,2,4,5-Tetrachlorobenzene (DD) 95943 dev dev 3E-08 mg/l (A,O) 3E-08 mg/l (A,O) 2.00E-01 NA 2,3,7,8-Tetrachlorodibenzo-p-dioxin (O,DD) 1746016 sdws sdws 28 140 1.07E+06 NA 1,1,1,2-Tetrachloroethane 630206 ca ca 3.6 18 2.83E+06 NA 1,1,2,2-Tetrachloroethane 79345 ca ca 0.005 mg/l (A) 0.005 mg/l (A) 2.06E+05 NA Tetrachloroethylene (KK) 127184 sdws sdws 3,600 (DD) 17,000 1.00E+09 8.2E+06 Tetrahydrofuran (DD) 109999 dev nc NA NA 1.00E+09 NA 1,1,3,3-Tetramethylurea 632224

NA NA 9.00E+05 NA Tetranitromethane 509148

0.002 mg/l (A) 0.002 mg/l (A) NA NA Thallium 7440280 sdws sdws

190 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 790 (E) 790 (E) 5.26E+05 61,000 Toluene (I) 108883 aes aes 24 76 6.50E+06 NA p-Toluidine 106490 nc nc 500 mg/l (E) 500 mg/l (E) NA NA Total dissolved solids (TDS) NA aes aes 0.003 mg/l (A) 0.003 mg/l (A) 5.50E+2 NA Toxaphene (KK) 8001352 sdws sdws 10 (M) 51 4.00E+03 NA Triallate (DD) 2303175 ca ca 21 66 1.42E+05 NA Tributylamine 102829 nc nc 16 51 1.80E+04 NA 1,2,3-Trichlorobenzene 87616 nc nc 0.07 mg/l (A) 0.07 mg/l (A) 4.90E+04 NA 1,2,4-Trichlorobenzene 120821 sdws sdws 0.20 mg/l (A) 0.20 mg/l (A) 1.29E+06 NA 1,1,1-Trichloroethane 71556 sdws sdws 0.005 mg/l (A) 0.005 mg/l (A) 4.59E+06 3.9E+06 1,1,2-Trichloroethane 79005 sdws sdws 0.005 mg/l (A) 0.005 mg/l (A) 1.28E+06 NA Trichloroethylene (DD,KK,MM,NN) 79016 sdws sdws 1,800 5,700 1.10E+06 NA Trichlorofluoromethane 75694 nc nc 180 570 1.20E+06 NA 2,4,5-Trichlorophenol (KK) 95954 nc nc 40 (DD) 170 (DD) 8.00E+05 NA 2,4,6-Trichlorophenol (DD,KK) 88062 dev dev 0.0075 (M) 0.12 (M) 1.75E+06 NA 1,2,3-Trichloropropane (MM) 96184 mut ca 1.6E+05 1.7E+05 (S) 1.70E+05 NA 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 nc sol

191 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 3,000 9,400 1.00E+09 NA Triethanolamine 102716 nc nc 24,000 (DD) 1.1E+05 1.00E+09 NA Triethylene glycol (DD) 112276 dev nc 2,500 (DD) 12,000 5.00E+06 NA 3-Trifluoromethyl-4-nitrophenol (DD) 88302 dev nc 140 180 (S) 1.84E+02 NA Trifluralin 1582098 nc sol NA NA 2.44E+03 170 2,2,4-Trimethyl pentane 540841

NA NA 1.29E+04 NA 2,4,4-Trimethyl-2-pentene (I) 107404

130 (E) 130 (E) 7.52E+04 75,000 (S) 1,2,3-Trimethylbenzene (I) 526738 aes aes sol 63 (E) 63 (E) 5.70E+04 57,000 (S) 1,2,4-Trimethylbenzene (I) 95636 aes aes sol 72 (E) 72 (E) 4.82E+04 48,000 (S) 1,3,5-Trimethylbenzene (I) 108678 aes aes sol 950 1,900 (S) 1.90E+03 NA Triphenyl phosphate 115866 nc sol 0.66 (M) 3.3 (M) 8.00E+03 NA tris(2,3-Dibromopropyl)phosphate 126727 ca ca NA NA 5.45E+08 NA Urea 57136

0.42 (M) 1.3 (M) NA NA Vanadium (B) 7440622 nc nc 3,500 (DD) 15,000 (DD) 2.00E+07 1.8E+06 Vinyl acetate (I,DD) 108054 dev dev 0.002 mg/l (A) 0.002 mg/l (A) 8.80E+06 32,000 Vinyl chloride (KK,LL,MM) 75014 sdws sdws 280 (E) 280 (E) 1.06E+05 58,000 Xylenes (I,J) 1330207 aes aes

192 2017 MR 22 – December 15, 2017 TABLE 1. GROUNDWATER: RESIDENTIAL AND NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per liter (µg/L). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Chemical Abstract Nonresidential Flammability and Hazardous Substance Service Residential Drinking Drinking Water Water Explosivity Number Water Criteria Criteria Solubility Screening Level 5 mg/l (E) 5 mg/l (E) NA NA Zinc (B) 7440666 aes aes

193 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 58,000 1.2E+07 1.2E+07 9.2E+06 1.1E+10 1.5E+07 NA Acenaphthene 83329 swpv nc nc nc nc nc NA 58,000 1.6E+07 1.6E+07 1.6E+07 1.1E+10 1.5E+07 NA Acenaphthylene 208968 swpv nc nc nc nc nc NA 15,000 31,000 1.3E+05 61,000 4.7E+08 3.2E+07 NA Acetaldehyde (I) 75070 20x nc nc nc nc nc NA 68,000 NA NA NA NA 1.0E+08 (D) NA Acetate 71501 20x max NA 68,000 2.1E+07 2.2E+07 2.2E+07 1.3E+10 1.0E+08 (C,D) 3.5E+07 Acetic acid 64197 20x nc nc nc nc max NA 1.1E+05 1.6E+08 4.6E+08 2.3E+08 1.6E+12 1.0E+08 (C,D) 3.7E+07 Acetone (I) 67641 20x st st st st max NA 7,200 3.0E+05 9.3E+05 4.7E+05 3.1E+09 1.5E+07 4.2E+07 Acetonitrile 75058 20x nc nc nc nc nc NA 64,000 7.3E+07 8.1E+07 7.3E+07 1.6E+11 5.3E+07 (C,DD) 8.4E+05 Acetophenone (DD) 98862 (DD) (DD) (DD) (DD) 20x dev dev dev dev dev NA 480 54 290 130 1.1E+06 1.0E+06 7.4E+06 Acrolein (I) 107028 20x nc nc nc nc nc NA 10 NA NA NA 5.2E+06 2,200 (MM) NA Acrylamide (MM) 79061 (MM) 20x mut mut NA 16,000 10,000 10,000 10,000 1.0E+07 1.3E+07 (DD) 3.5E+07 Acrylic acid (DD) 79107 20x nc nc nc nc dev NA 26 (M) 1,100 5,200 2,300 1.9E+07 11,000 3.7E+06 Acrylonitrile (I) 107131 20x ca ca ca ca ca

194 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 40 NA NA NA NA 63,000 NA Alachlor 15972608 20x ca NA 60 NA NA NA NA 67,000 NA Aldicarb 116063 20x nc NA 40 (M) NA NA NA NA 2.5E+05 NA Aldicarb sulfone 1646884 20x nc NA 80 (M) NA NA NA NA NA NA Aldicarb sulfoxide 1646873 20x NA 110 3,400 3,500 3,500 2.6E+05 570 NA Aldrin 309002 swpv ca ca ca ca ca 5.7E+06 1,000 NA NA NA 2.9E+08 1.0E+08 (D) NA Aluminum (B,DD) 7429905 20x nc max NA 2.0E+05 (N) NA NA NA 2.6E+10 NA NA Ammonia (N) 7664417 20x nc NA 3,800 1.0E+05 8.7E+05 3.7E+05 3.2E+09 3.2E+07 (C) 8.9E+05 t-Amyl methyl ether (TAME) 994058 20x nc nc nc nc nc NA 840 NA NA NA 5.2E+07 1.1E+06 6.2E+06 Aniline 62533 20x nc ca NA 23,000 2.1E+08 2.1E+08 2.1E+08 5.2E+10 7.5E+07 NA Anthracene 120127 swpv nc nc nc nc nc NA 4,300 NA NA NA 1.0E+07 1.8E+05 NA Antimony 7440360 swpv nc nc 5,500 4,700 NA NA NA 3.0E+05 9,000 NA Arsenic (B,KK) 7440382 swpv ca ca NA NA NA NA NA (BB) NA NA Asbestos (BB) 1332214

NA 60 NA NA NA 1.1E+09 4.5E+06 NA Atrazine 1912249 20x nc nc

195 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 800 1.6E+05 1.7E+05 1.7E+05 4.1E+07 55,000 NA Azobenzene 103333 swpv ca ca ca ca ca 45,000 1.3E+06 NA NA NA 2.6E+08 6.8E+07 NA Barium (B,KK) 7440393 swpv nc nc NA 100 4,400 44,000 18,000 1.6E+08 1.1E+05 6.2E+05 Benzene (I,KK) 71432 20x ca ca ca ca ca NA 0.04 (M) NA NA NA 7,800 (MM) 4.8 (M) NA Benzidine (MM) 92875 swpv mut mut

NA 13,000 3.0E+05 3.1E+05 3.1E+05 8.7E+06 (Q) NA Benzo(a)anthracene (Q,MM) 56553 (MM) (MM) (MM) (MM) mut swpv mut mut mut NA 29,000 NA NA NA 8.7E+06 (Q) NA Benzo(b)fluoranthene (Q,MM) 205992 (MM) swpv mut NA 15,000 NA NA NA 8.7E+07 (Q) NA Benzo(k)fluoranthene (Q,MM) 207089 (MM) swpv mut NA 16,000 NA NA NA 3.7E+08 7.1E+05 NA Benzo(g,h,i)perylene 191242 swpv nc nc NA 3,800 NA NA NA 1.0E+05 (DD) 1,600 (MM) NA Benzo(a)pyrene (Q,DD,MM) 50328 swpv dev mut

NA 4.8E+05 NA NA NA 3.7E+07 1.0E+08 (D) NA Benzoic acid 65850 20x nc max NA 17,000 NA NA NA 2.6E+11 3.5E+07 (C) 3.2E+06 Benzyl alcohol 100516 20x nc nc NA 86 (M) 4,900 8,500 5,300 2.5E+07 36,000 4.9E+05 Benzyl chloride 100447 20x ca ca ca ca ca 196 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels 1,000 51,000 NA NA NA 5.3E+05 1.3E+05 NA Beryllium (B) 7440417 swpv ca nc NA 30 (M) NA NA NA NA 62,000 1.6E+06 bis(2-Chloroethoxy)ethane 112265 20x nc NA 13 (M) 940 1,400 970 3.9E+06 5,500 1.7E+06 bis-2-Chloroethylether (I) 111444 20x ca ca ca ca ca NA 23,000 NA NA NA 8.0E+08 6.9E+05 (C) 65,000 bis(2-Ethylhexyl) phthalate (DD) 117817 swpv ca ca NA 10,000 (F) NA NA NA 1.6E+09 3.3E+07 (DD) NA Boron (DD) 7440428 20x nc dev NA 200 NA NA NA NA 22,000 NA Bromate 15541454 20x ca NA 940 2.0E+05 8.8E+05 4.0E+05 3.1E+09 2.0E+06 (C) 2.3E+05 Bromobenzene (I) 108861 20x nc nc nc nc nc NA 1,600 (W) 2,200 19,000 8,200 7.2E+07 98,000 3.2E+05 Bromodichloromethane (DD) 75274 20x ca ca ca ca ca NA 1,600 (W) 85,000 3.3E+05 1.5E+05 1.2E+09 7.7E+05 (C) 3.0E+05 Bromoform 75252 20x ca ca ca ca ca NA 2,400 5,800 1.4E+05 56,000 5.2E+08 5.0E+06 NA Bromomethane 74839 20x nc nc nc nc nc NA 12,000 4.2E+06 6.5E+06 4.3E+06 1.8E+10 2.5E+07 (C) 2.5E+06 n-Butanol (I) 71363 20x nc nc nc nc nc NA 48,000 2.3E+07 7.3E+07 3.5E+07 2.5E+11 3.9E+07 (C,DD) 9.3E+06 2-Butanone (MEK) (I,DD,KK) 78933 (DD) (DD) (DD) (DD) 20x dev dev dev dev dev NA 12,000 1.3E+06 5.8E+06 2.7E+06 2.1E+10 2.5E+07 (C) 5.9E+05 n-Butyl acetate 123864 20x nc nc nc nc nc NA 22,000 8.2E+05 1.3E+06 8.6E+05 3.8E+09 4.5E+07 NA t-Butyl alcohol 75650 20x nc nc nc nc nc 197 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 18,000 NA NA NA 4.1E+10 1.3E+06 (DD) NA Butyl benzyl phthalate (DD) 85687 swpv nc dev NA 13,000 7.1E+05 2.9E+06 1.4E+06 1.0E+10 1.2E+07 (C) 36,000 n-Butylbenzene 104518 swpv nc nc nc nc nc NA 26,000 1,100 5,800 2,600 2.1E+07 2.5E+07 (C) 49,000 sec-Butylbenzene 135988 swpv nc nc nc nc nc NA 20,000 1,200 5,800 2,600 2.1E+07 2.5E+07 (C) 61,000 t-Butylbenzene (I) 98066 swpv nc nc nc nc nc 2,000 6,000 NA NA NA 7.1E+05 59,000 NA Cadmium (B,KK) 7440439 swpv ca nc NA NA 65,000 1.1E+06 4.5E+05 4.2E+09 NA NA Camphene (I) 79925 nc nc nc nc NA 40,000 NA NA NA 1.2E+08 3.3E+07 (DD) NA Caprolactam (DD) 105602 20x nc dev NA 800 NA NA NA NA 6.6E+05 (DD) NA Carbaryl (DD) 63252 20x dev NA 2,200 NA NA NA 4.6E+08 62,000 NA Carbazole 86748 swpv ca ca NA 800 NA NA NA NA 4,000 (DD) NA Carbofuran (DD) 1563662 20x dev NA 8,800 3.5E+05 9.5E+06 3.9E+06 3.7E+10 7.3E+06 (C,DD) 2.9E+05 Carbon disulfide (I,R,DD) 75150 20x nc nc nc nc dev NA 100 2,800 59,000 24,000 2.3E+08 93,000 1.8E+05 Carbon tetrachloride (KK) 56235 20x ca ca ca ca ca NA 4,300 1.2E+05 1.2E+05 1.2E+05 1.0E+07 37,000 NA Chlordane (J,KK) 57749 swpv st st st st ca NA 5.0E+06 NA NA NA NA NA NA Chloride 16887006 20x

198 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 360 NA NA NA 5.2E+08 7.5E+05 2.1E+06 2-Chloroaniline 95512 20x nc nc NA 60 NA NA NA NA 30,000 NA 4-Chloroaniline 106478 20x ca NA 2,000 1.3E+05 7.2E+05 3.2E+05 2.6E+09 5.0E+06 (C) 2.6E+05 Chlorobenzene (I,KK) 108907 20x nc nc nc nc nc NA 94,000 NA NA NA NA 1.0E+08 (D) NA p-Chlorobenzene sulfonic acid 98668 20x max NA 2.4E+05 2.3E+07 6.8E+08 2.8E+08 2.6E+12 1.0E+08 (D) NA 1-Chloro-1,1-difluoroethane 75683 20x nc nc nc nc max NA 4,800 2.2E+06 5.5E+07 2.2E+07 2.1E+11 3.0E+06 NA Chloroethane (DD) 75003 20x nc nc nc nc ca NA NA NA NA NA NA NA 44,000 2-Chloroethyl vinyl ether 110758

NA 1,600 (W) 1,100 15,000 6,100 5.5E+07 2.5E+06 (C) 8.8E+05 Chloroform (KK) 67663 20x ca ca ca ca nc NA 4,400 44,000 1.2E+06 5.0E+05 4.7E+09 1.8E+06 NA Chloromethane (I) 74873 20x nc nc nc nc ca NA 8,000 NA NA NA NA 6.6E+06 (DD) NA 4-Chloro-3-methylphenol (DD) 59507 20x dev NA 38,000 NA NA NA NA 2.0E+07 NA beta-Chloronaphthalene 91587 swpv nc NA 640 8.6E+05 8.6E+05 8.6E+05 9.0E+08 5.3E+05 (DD) 7.3E+06 2-Chlorophenol (DD) 95578 (DD) (DD) (DD) (DD) 20x dev dev dev dev dev NA 800 2.6E+05 1.2E+06 5.3E+05 4.2E+09 1.7E+06 (C) 3.0E+05 o-Chlorotoluene (I) 95498 20x nc nc nc nc nc

199 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 4,400 NA NA NA 5.2E+07 5.0E+05 (DD) NA Chlorpyrifos (DD) 2921882 swpv nc dev 15,000 1.0E+08 (D) NA NA NA 5.2E+06 1.0E+08 (D) NA Chromium (III) (B,H,KK) 16065831 max nc max NA 31,000 NA NA NA 44,000 1,700 (M, MM) NA Chromium (VI) (H,KK,MM) 18540299 (MM) swpv mut mut NA 25,000 NA NA NA 8.7E+08(MM) (Q) NA Chrysene (Q,MM) 218019 swpv mut 10,000 36 (M) NA NA NA 1.4E+05 1.9E+05 NA Cobalt (B) 7440484 20x ca nc 14,000 5.8E+06 NA NA NA 1.0E+08 6.2E+05 NA Copper (B) 7440508 swpv nc nc NA 24 (M) NA NA NA NA 16,000 NA Cyanazine 21725462 20x ca NA 4,000 1,700 11,000 5,100 4.2E+07 53,000 (DD) NA Cyanide (P,R,DD) Varies 20x nc nc nc nc dev NA NA 2.8E+06 8.2E+07 3.3E+07 3.1E+11 NA 50,000 Cyclohexane (DD) 110827 nc nc nc nc NA 24,000 1.2E+07 1.5E+07 1.2E+07 3.7E+10 5.0E+07 (C) 1.7E+06 Cyclohexanone 108941 20x nc nc nc nc nc NA 1,200 NA NA NA NA 2.5E+06 NA Dacthal 1861321 20x nc NA 4,000 NA NA NA NA 7.5E+06 2.0E+07 Dalapon 75990 20x nc NA 11,000 NA NA NA 1.8E+07 41,000 NA 4-4'-DDD 72548 swpv ca ca

200 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 7,900 1.6E+05 1.6E+05 1.6E+05 1.3E+07 29,000 NA 4-4'-DDE 72559 swpv ca ca ca ca ca NA 11,000 NA NA NA 1.3E+07 40,000 NA 4-4'-DDT (DD) 50293 swpv ca ca NA 880 NA NA NA 1.3E+09 7.5E+05 (DD) NA Decabromodiphenyl ether (DD) 1163195 (DD) swpv dev dev NA 1,000 NA NA NA 1.0E+09 4.4E+05 (C,DD) 26,000 Di-n-butyl phthalate (DD) 84742 (DD) swpv dev dev NA 4.6E+05 (C) NA NA NA 3.7E+09 8.1E+06 (C) 56,000 Di(2-ethylhexyl) adipate (DD) 103231 swpv ca ca NA 99,000 3.9E+08 4.0E+08 4.0E+08 2.5E+10 4.8E+06 NA Di-n-octyl phthalate 117840 swpv nc nc nc nc nc NA NA 1.8E+08 1.8E+08 1.8E+08 1.3E+11 NA 3.5E+07 Diacetone alcohol (I) 123422 nc nc nc nc NA 410 NA NA NA 5.2E+07 1.7E+05 NA Diazinon 333415 swpv nc nc NA 14,000 NA NA NA 8.7E+05 (Q) NA Dibenzo(a,h)anthracene (Q,MM) 53703 swpv (MM) mut NA 1,700 3.5E+05 3.5E+05 3.5E+05 2.1E+08 2.5E+05 NA Dibenzofuran 132649 swpv nc nc nc nc nc NA 1,600 (W) 1,300 6,100 (MM) 2,700 (MM) 2.2E+07 13,000 (MM) 2.7E+05 Dibromochloromethane (MM) 124481 (MM) mut mut (MM) 20x mut mut mut NA 4.0 (M) 23 (MM) 34 (MM) 23 (MM) 93,000 (MM) 1,400 (MM) 3.3E+05 Dibromochloropropane (MM) 96128 20x mut mut mut mut mut

201 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 360 8,900 57,000 25,000 2.1E+08 7.5E+05 9.4E+05 Dibromomethane 74953 20x nc nc nc nc nc NA 36,000 NA NA NA NA 3.0E+07 (DD) NA Dicamba (DD) 1918009 20x dev NA 12,000 1.4E+06 4.5E+06 2.2E+06 1.6E+10 7.5E+07 (C) 1.3E+05 1,2-Dichlorobenzene 95501 20x nc nc nc nc nc NA 240 12,000 44,000 21,000 1.6E+08 5.0E+05 (C) 99,000 1,3-Dichlorobenzene 541731 20x nc nc nc nc nc NA 1,500 26,000 93,000 44,000 3.3E+08 4.7E+05 NA 1,4-Dichlorobenzene (KK) 106467 20x ca ca ca ca ca NA 160 (M) NA NA NA 3.8E+06 14,000 NA 3,3`-Dichlorobenzidine 91941 swpv ca ca NA 710 1.3E+05 4.5E+06 1.8E+06 1.7E+10 1.2E+06 NA Dichlorodifluoromethane 75718 swpv nc nc nc nc nc NA 2,600 13,000 2.1E+05 86,000 8.0E+08 1.0E+06 (C) 6.0E+05 1,1-Dichloroethane 75343 20x ca ca ca ca ca NA 100 1,700 13,000 5,600 4.9E+07 67,000 1.0E+06 1,2-Dichloroethane (I,KK) 107062 20x ca ca ca ca ca NA 140 1.0E+05 2.7E+06 1.1E+06 1.0E+10 1.2E+07 (C) 4.8E+05 1,1-Dichloroethylene (I,KK) 75354 20x nc nc nc nc nc NA 1,400 8,000 1.1E+05 46,000 4.2E+08 5.0E+05 8.2E+05 cis-1,2-Dichloroethylene 156592 20x nc nc nc nc nc NA 2,000 200,000 3.6E+06 1.5E+06 1.4E+10 5.0E+06 (C) 7.9E+05 trans-1,2-Dichloroethylene 156605 20x nc nc nc nc nc NA 940 NA NA NA 4.6E+08 6.2E+05 NA 2,6-Dichloro-4-nitroaniline 99309 swpv nc nc

202 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 1,600 NA NA NA 5.8E+08 1.3E+06 (DD) NA 2,4-Dichlorophenol (DD) 120832 20x nc dev NA 1,400 NA NA NA 9.2E+09 1.4E+07 NA 2,4-Dichlorophenoxyacetic acid (KK) 94757 20x nc nc NA 100 6,000 56,000 24,000 2.1E+08 1.7E+05 4.6E+05 1,2-Dichloropropane (I) 78875 20x nc nc nc nc ca NA 140 8,600 85,000 36,000 3.2E+08 61,000 5.3E+05 1,3-Dichloropropene (J) 542756 20x ca ca ca ca ca NA 16 (M) NA NA NA 1.0E+08 3,800 (MM) 1.1E+06 Dichlorvos (MM) 62737 20x nc mut NA NA NA NA NA NA NA NA Dicyclohexyl phthalate 84617

NA 29 3,700 3,800 3,800 2.8E+05 610 NA Dieldrin 60571 swpv ca ca ca ca ca NA 24 (M) 1.2E+06 1.4E+07 5.8E+06 5.2E+10 5.0E+07 (C) 3.4E+06 Diethyl ether 60297 20x nc nc nc nc nc NA 94,000 NA NA NA 1.5E+11 1.0E+08 (C,D) 2.6E+05 Diethyl phthalate 84662 20x nc max NA 3,600 NA NA NA 5.2E+06 7.5E+06 5.3E+07 Diethylene glycol monobutyl ether 112345 20x nc nc NA 22,000 8.2E+05 9.3E+06 3.9E+06 3.5E+10 1.8E+07 (C,DD) 7.8E+05 Diisopropyl ether (DD) 108203 (DD) (DD) (DD) (DD) 20x dev dev dev dev dev NA 92 1.7E+06 3.4E+06 1.9E+06 1.0E+10 1.9E+05 1.8E+07 Diisopropylamine (I) 108189 20x nc nc nc nc nc NA 12,000 NA NA NA 2.6E+09 2.5E+07 (C) 3.8E+05 Dimethyl phthalate 131113 20x nc nc

203 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 3,000 2.2E+07 2.2E+07 2.2E+07 5.2E+09 6.2E+06 3.9E+07 N,N-Dimethylacetamide 127195 20x nc nc nc nc nc NA 240 25,000 38,000 26,000 1.1E+08 1.2E+05 2.8E+05 N,N-Dimethylaniline 121697 20x ca ca ca ca ca NA 12,000 7.5E+05 7.5E+05 7.5E+05 3.7E+08 2.5E+07 3.5E+07 Dimethylformamide (I) 68122 20x nc nc nc nc nc NA 2,400 NA NA NA 3.7E+09 5.0E+06 NA 2,4-Dimethylphenol 105679 20x nc nc NA 72 (M) NA NA NA 1.0E+08 1.5E+05 NA 2,6-Dimethylphenol 576261 20x nc nc NA 120 (M) NA NA NA 1.8E+08 2.5E+05 NA 3,4-Dimethylphenol 95658 20x nc nc NA 1.2E+05 NA NA NA 1.0E+09 1.0E+08 (C,D) 3.7E+07 Dimethylsulfoxide 67685 20x nc max NA 240 (M) NA NA NA 3.7E+08 5.0E+05 NA 2,4-Dinitrophenol 51285 20x nc nc NA 22 NA NA NA 1.4E+07 9,100 NA 2,4-Dinitrotoluene (KK) 121142 20x ca ca NA 970 NA NA NA 2.1E+08 66,000 (DD) NA Dinoseb (DD) 88857 swpv nc dev NA 140 (M) 78,000 1.0E+05 79,000 2.5E+08 61,000 3.8E+07 1,4-Dioxane (I) 123911 20x ca ca ca ca ca NA 400 NA NA NA NA 1.2E+06 NA Diquat 85007 20x nc NA 360 (M) NA NA NA 1.7E+08 3.2E+05 NA Diuron 330541 20x nc ca NA 6,500 NA NA NA NA 1.2E+06 NA Endosulfan (J) 115297 swpv nc

204 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 2,000 NA NA NA 3.7E+09 1.7E+06 NA Endothall 145733 20x nc nc NA 790 NA NA NA NA 1.2E+05 NA Endrin (KK) 72208 swpv nc NA 40 (M) 7,500 16,000 9,000 5.2E+07 6.1E+05 3.5E+06 Epichlorohydrin (I) 106898 20x nc nc nc nc ca NA 2.4E+07 2.3E+08 3.5E+08 2.4E+08 9.5E+11 1.0E+08 (C,D) 3.5E+07 Ethanol (I,DD) 64175 20x st nc nc st max NA 8,600 2.4E+05 1.0E+06 4.7E+05 3.7E+09 1.8E+07 (C) 3.5E+06 Ethyl acetate (I) 141786 20x nc nc nc nc nc NA 980 5.4E+05 5.2E+06 2.2E+06 1.9E+10 2.3E+07 (C) 9.7E+05 Ethyl-tert-butyl ether (ETBE) 637923 20x nc nc nc nc nc NA 1,500 22,000 1.4E+05 60,000 5.1E+08 5.5E+05 (C) 1.6E+05 Ethylbenzene (I) 100414 20x ca ca ca ca ca NA 1.0 (M) 140 590 270 2.1E+06 3,000 4.5E+05 Ethylene dibromide 106934 20x ca ca ca ca ca NA 64,000 NA NA NA 1.0E+09 5.3E+07 (C,DD) 3.5E+07 Ethylene glycol (DD) 107211 20x nc dev NA 12,000 NA NA NA 8.4E+10 2.5E+07 3.8E+07 Ethylene glycol monobutyl ether 111762 20x nc nc NA NA NA NA NA NA NA NA Ethylenediaminetetraacetic acid (EDTA) (II) 60004

NA 4.3E+05 NA NA NA 7.3E+09 1.6E+07 NA Fluoranthene 206440 swpv nc nc NA 70,000 1.3E+07 1.3E+07 1.3E+07 7.3E+09 1.0E+07 NA Fluorene 86737 swpv nc nc nc nc nc NA 40,000 NA NA NA NA 9.9E+06 (DD) NA Fluorine (soluble fluoride) (DD) 7782414 20x dev

205 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 24,000 28,000 37,000 37,000 4.0E+07 5.0E+07 NA Formaldehyde (MM) 50000 (MM) (MM) (MM) (MM) 20x mut mut mut mut nc NA 1.1E+05 18,000 20,000 20,000 1.6E+07 1.0E+08 (C,D) 3.5E+07 Formic acid (I,U) 64186 20x nc nc nc nc max NA 88,000 NA NA NA NA 7.3E+07 (C,DD) 3.9E+06 1-Formylpiperidine (DD) 2591868 20x dev NA 2.8E+05 NA NA NA NA 1.1E+05 NA Gentian violet 548629 swpv ca NA 14,000 NA NA NA NA 6.6E+06 (DD) NA Glyphosate (DD) 1071836 20x dev NA 18,000 20,000 21,000 21,000 9.8E+05 8,100 NA Heptachlor (DD,KK) 76448 swpv ca ca ca ca ca NA 65 2,600 2,600 2,600 4.9E+05 2,700 NA Heptachlor epoxide (KK) 1024573 swpv ca ca ca ca ca NA 4.6E+05 (C) 1.5E+06 4.8E+07 1.9E+07 1.8E+11 1.0E+08 (C,D) 29,000 n-Heptane 142825 swpv nc nc nc nc max NA 14 (M) NA NA NA NA 8.0E+05 NA Hexabromobenzene 87821 swpv nc NA 200 (M) 940 1,000 940 1.8E+06 4,000 NA Hexachlorobenzene (C-66) (KK) 118741 swpv nc nc nc nc nc NA 170 4,700 17,000 7,900 5.8E+07 78,000 (C) 5,600 Hexachlorobutadiene (C-46) (KK) 87683 swpv ca ca ca ca ca NA 9.9 (M) NA NA NA 7.1E+05 960 NA alpha-Hexachlorocyclohexane 319846 swpv ca ca NA 33 NA NA NA 2.4E+06 3,400 NA beta-Hexachlorocyclohexane 319857 swpv ca ca

206 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 2,400 670 2,900 1,300 1.0E+07 2.4E+06 (C) 5,300 Hexachlorocyclopentadiene (C-56) 77474 swpv nc nc nc nc nc NA 84 (M) 7,700 35,000 16,000 1.3E+08 1.5E+05 NA Hexachloroethane (KK) 67721 20x ca ca ca ca ca NA 2.1E+05 (C) 2.8E+05 9.5E+06 3.9E+06 3.7E+10 7.5E+07 (C) 70,000 n-Hexane 110543 swpv nc nc nc nc nc NA 600 (M) 1.6E+05 4.6E+05 2.3E+05 1.6E+09 1.2E+06 (C) 1.1E+06 2-Hexanone 591786 20x nc nc nc nc nc NA 12,000 NA NA NA 8.7E+06 (Q) NA Indeno(1,2,3-cd)pyrene (Q,MM) 193395 (MM) swpv mut 1.125E+07 6,000 NA NA NA NA 1.0E+08 (D) NA Iron (B) 7439896 20x max NA 36,000 1.7E+07 2.7E+07 1.8E+07 7.8E+10 7.5E+07 (C) 3.3E+06 Isobutyl alcohol (I) 78831 20x nc nc nc nc nc NA 15,000 NA NA NA 4.7E+09 6.4E+06 (C) 2.0E+06 Isophorone (DD) 78591 20x ca ca NA 1.6E+05 2.2E+06 3.6E+06 2.3E+06 1.0E+10 1.0E+08 (C,D) 3.6E+07 Isopropyl alcohol (I,DD) 67630 20x nc nc nc nc max NA 14,000 5,700 33,000 15,000 1.2E+08 2.5E+07 (C) 90,000 Isopropyl benzene 98828 swpv ca ca ca ca nc 11,000 1.8E+05 (L) NA NA NA 7.8E+06 (L) 1.9E+05 (L,DD) NA Lead (B,L,DD,KK) 7439921 swpv nc dev NA 18 (M) NA NA NA NA 6,500 NA Lindane (KK) 58899 swpv ca 11,000 160 (M) NA NA NA 1.8E+09 3.3E+05 (DD) NA Lithium (B,DD) 7439932 20x nc dev 207 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 6.6E+06 NA NA NA 5.2E+09 1.0E+08 (D) NA Magnesium 7439954 20x nc max 3.6E+05 1,000 NA NA NA 1.6E+07 1.2E+07 NA Manganese (B) 7439965 20x nc nc NA 40 160 4,100 1,700 1.6E+07 16,000 (DD) NA Mercury (Total) (Z,DD,KK) Varies 20x nc nc nc nc dev NA NA NA NA NA NA NA NA Methane (K) 74828

NA 1.6E+05 2.2E+08 3.7E+08 2.7E+08 1.0E+12 1.0E+08 (C,D) 3.5E+07 Methanol (DD) 67561 (DD) (DD) (DD) (DD) 20x dev dev dev dev max NA 34,000 NA NA NA NA 5.4E+05 (DD) NA Methoxychlor (DD,KK) 72435 swpv dev NA 400 60,000 60,000 60,000 5.8E+07 3.3E+05 (DD) 3.5E+07 2-Methoxyethanol (I,DD) 109864 20x nc nc nc nc dev NA 520 NA NA NA 9.4E+08 1.1E+06 NA 2-Methyl-4-chlorophenoxyacetic acid 94746 20x nc nc NA 59 (M) NA NA NA 1.0E+08 1.0E+05 NA 2-Methyl-4,6-dinitrophenol 534521 swpv nc nc NA 8,400 NA NA NA NA 1.7E+07 4.7E+07 N-Methyl-morpholine (I) 109024 20x nc NA 29 (M) NA NA NA NA 50,000 NA Methyl parathion 298000 swpv nc NA 6,000 1.2E+07 4.3E+07 2.0E+07 1.5E+11 1.2E+07 (C) 1.1E+06 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 (DD) (DD) (DD) (DD) 20x dev dev dev dev nc NA 800 1.8E+05 1.3E+06 5.7E+05 4.9E+09 1.8E+06 3.0E+06 Methyl-tert-butyl ether (MTBE) 1634044 20x ca ca ca ca ca

208 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 240 NA NA NA NA 5.0E+05 1.1E+06 N-methylaniline 100618 20x nc NA NA 2.9E+05 9.5E+06 3.9E+06 3.7E+10 NA 72,000 Methylcyclopentane (I) 96377 nc nc nc nc NA 2,200 NA NA NA NA 1.6E+05 (MM) NA 4,4`-Methylene-bis-2- chloroaniline (MBOCA) (MM) 101144 swpv mut NA 100 5.3E+05 8.2E+06 3.4E+06 3.1E+10 5.5E+05 (MM) 1.2E+06 Methylene chloride (MM) 75092 20x nc nc nc nc mut NA 1,900 2.3E+05 2.5E+05 2.3E+05 5.2E+08 1.0E+06 NA 2-Methylnaphthalene 91576 swpv nc nc nc nc nc NA 600 NA NA NA 5.2E+09 1.2E+6 NA Methylphenols (JJ,KK) 1319773 20x nc nc NA 16,000 NA NA NA 5.2E+09 1.3E+07 (DD) NA 2-Methylphenol (DD,KK) 95487 20x nc dev NA 12,000 NA NA NA NA 2.5E+07 (C) 5.4E+05 Metolachlor 51218452 20x nc NA 1,500 NA NA NA NA 3.2E+06 NA Metribuzin 21087649 20x nc NA 8,900 NA NA NA NA 10,000 NA Mirex 2385855 swpv ca NA 1,200 NA NA NA 1.6E+09 3.1E+06 NA Molybdenum 7439987 20x nc nc NA 29,000 13,000 16,000 13,000 3.7E+07 2.5E+07 NA Naphthalene 91203 swpv ca ca ca ca nc 15,000 38,000 NA NA NA 4.7E+06 1.5E+06 NA Nickel (B) 7440020 swpv nc nc

209 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 2.0E+05 (N) NA NA NA NA 1.0E+08 (D) NA Nitrate (N,DD) 14797558 20x max NA 20,000 (N) NA NA NA NA 1.6E+07 (DD) NA Nitrite (N,DD) 14797650 20x dev NA 240 (M) 18,000 19,000 18,000 3.2E+07 5.0E+05 1.0E+06 Nitrobenzene (I,KK) 98953 20x ca ca ca ca nc NA 240 (M) 2,300 2,300 2,300 2.6E+06 5.0E+05 NA 2-Nitrophenol 88755 20x nc nc nc nc nc NA 2.0 (M) NA NA NA 6.4E+05 870 7.6E+06 n-Nitroso-di-n-propylamine 621647 20x ca ca NA 13,000 NA NA NA NA 1.2E+06 NA N-Nitrosodiphenylamine 86306 swpv ca NA 4,000 NA NA NA 1.3E+09 1.7E+06 NA Oxamyl 23135220 20x nc nc NA 1,200 NA NA NA 4.2E+09 2.5E+06 NA Oxo-hexyl acetate 88230357 20x nc nc NA 59,000 NA NA NA NA 3.2E+07 (DD) NA Pendimethalin (DD) 40487421 swpv dev NA 560 3,200 3,300 3,200 5.2E+06 3.2E+05 NA Pentachlorobenzene 608935 swpv nc nc nc nc nc NA 3,500 1.9E+06 1.9E+06 1.9E+06 5.8E+08 7.5E+05 NA Pentachloronitrobenzene 82688 swpv nc nc nc nc nc NA 160 NA NA NA 1.2E+07 15,000 NA Pentachlorophenol (KK) 87865 swpv ca ca NA NA 3.8E+05 1.4E+07 5.5E+06 5.2E+10 NA 1.9E+05 Pentane 109660 nc nc nc nc NA NA NA NA NA NA NA 2.3E+05 2-Pentene (I) 109682

210 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 56 (M) NA NA NA NA 1.2E+05 (DD) NA Perchlorate (DD) 14797730 20x dev NA 59 (NN) NA NA NA NA 2,100 (DD) NA Perfluorooctanoic acid (DD) 335671 swpv dev NA 1.4 (NN) NA NA NA NA 2,100 (DD) NA Perfluorooctane sulfonic acid (DD) 1763231 20x dev NA 96,000 24,000 25,000 25,000 5.2E+06 7.5E+06 NA Phenanthrene 85018 swpv nc nc nc nc nc NA 24,000 NA NA NA 1.0E+10 2.0E+07 (DD) NA Phenol (DD) 108952 20x nc dev NA 670 NA NA NA 9.1E+07 1.2E+05 NA Phenytoin (DD) 57410 swpv ca ca NA NA NA NA NA NA NA NA Phosphorus, Total Varies

NA 2 NA NA NA 1.0E+07 2,100 (DD) NA Phosphorus, White (R,DD) 7723140 20x nc dev NA 2.2E+05 NA NA NA NA 1.0E+08 (D) NA o-Phthalic acid 88993 20x max NA 2.4E+05 NA NA NA 1.0E+09 1.0E+08 (D) NA Phthalic anhydride 85449 20x nc max NA 10,000 NA NA NA NA 1.7E+07 NA Picloram 1918021 20x nc NA 52 2.3E+08 2.4E+08 2.3E+08 3.7E+11 1.1E+05 1.4E+08 Piperidine 110894 20x nc nc nc nc nc NA 2 (M) NA NA NA NA 1,400 NA Polybrominated biphenyls (J,DD) 67774327 20x ca NA 1,200 38,000 39,000 39,000 1.3E+07 1,900 (T,DD) NA Polychlorinated biphenyls (PCBs) (J,T,DD) 1336363 swpv ca ca ca ca dev

211 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA (O) (O) (O) (O) (O) (O) NA Polychlorinated biphenyls (PCBs) congeners (O) Varies

NA 6,000 NA NA NA NA 1.2E+07 NA Prometon 1610180 20x nc NA 460 NA NA NA NA 1.9E+05 NA Propachlor 1918167 20x ca NA 2,200 NA NA NA NA 4.5E+06 NA Propazine 139402 20x nc NA 2.2E+05 1.4E+07 1.4E+07 1.4E+07 1.6E+10 1.0E+08 (C,D) 3.5E+07 Propionic acid 79094 20x nc nc nc nc max NA 1.6E+05 8.1E+06 1.3E+07 8.5E+06 3.7E+10 1.0E+08 (C,D) 3.6E+07 Propyl alcohol (I,DD) 71238 (DD) (DD) (DD) (DD) 20x dev dev dev dev max NA 16,000 2.6E+06 1.4E+07 6.2E+06 5.0E+10 2.5E+07 (C) 89,000 n-Propylbenzene (I,DD) 103651 (DD) (DD) (DD) (DD) swpv dev dev dev dev nc NA 2.4E+06 NA NA NA NA 1.0E+08 (C,D) 3.5E+07 Propylene glycol 57556 20x max NA 2.4E+05 9.6E+07 9.9E+07 9.9E+07 5.2E+09 1.2E+07 NA Pyrene 129000 swpv nc nc nc nc nc NA 120 77,000 87,000 77,000 1.8E+08 2.5E+05 1.8E+08 Pyridine (I,KK) 110861 20x nc nc nc nc nc 610 4,200 NA NA NA 1.0E+09 3.1E+06 NA Selenium (B,KK) 7782492 swpv nc nc NA 14,000 NA NA NA 1.6E+08 2.5E+05 NA Silver (KK) 7440224 swpv nc nc NA 1,000 NA NA NA NA 2.0E+06 NA Silvex (2,4,5-TP) (KK) 93721 20x nc

212 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 80 NA NA NA NA 1.2E+06 NA Simazine 122349 20x nc NA 1.1E+06 NA NA NA NA 1.0E+08 (D) NA Sodium 17341252 20x max NA 1,400 (M) NA NA NA NA 7.5E+06 NA Sodium azide 26628228 20x nc NA 4,800 NA NA NA 7.3E+09 2.5E+07 NA Sodium bromide 7647156 20x nc nc 1.29E+05 48,000 NA NA NA NA 9.9E+07 (DD) NA Strontium (B,DD) 7440246 20x dev NA 2,000 1.6E+05 6.3E+05 2.9E+05 2.2E+09 4.7E+05 (C) 2.9E+05 Styrene 100425 20x ca ca ca ca ca NA 5.0E+06 NA NA NA NA NA NA Sulfate 14808798 20x NA 120 (M) NA NA NA 3.3E+08 2.5E+05 NA Sulfolane 126330 20x nc nc NA 5,600 NA NA NA NA 4.6E+06 (DD) NA Tebuthiuron (DD) 34014181 20x dev NA (O) NA NA NA NA (O) NA 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416

NA 2,000 20,000 23,000 20,000 5.2E+07 4.6E+05 (DD) NA 1,2,4,5-Tetrachlorobenzene (DD) 95943 swpv nc nc nc nc dev NA 0.24 (O) 0.58 (O) 0.6 (O) 0.6 (O) 29 (O) 0.1 (O,DD) NA 2,3,7,8-Tetrachlorodibenzo-p-dioxin (O,DD) 1746016 swpv ca ca ca ca dev NA 560 7,400 47,000 20,000 1.7E+08 2.3E+05 2.3E+05 1,1,1,2-Tetrachloroethane 630206 20x ca ca ca ca ca NA 72 2,500 6,600 3,400 2.2E+07 30,000 6.3E+05 1,1,2,2-Tetrachloroethane 79345 20x ca ca ca ca ca 213 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 100 38,000 5.4E+05 2.2E+05 2.1E+09 1.5E+06 (C) 60,000 Tetrachloroethylene (KK) 127184 20x st nc nc st nc NA 72,000 9.6E+06 3.0E+07 1.5E+07 1.0E+11 6.0E+07 (C,DD) 5.4E+07 Tetrahydrofuran (DD) 109999 20x nc nc nc nc dev NA NA 2.1E+05 2.1E+05 2.1E+05 4.2E+07 NA 4.0E+07 1,1,3,3-Tetramethylurea 632224 nc nc nc nc NA NA 29 36 29 85,000 NA 8.0E+05 Tetranitromethane 509148 ca ca ca ca NA 2,300 NA NA NA 1.0E+07 6,200 NA Thallium 7440280 swpv nc nc NA 16,000 8.5E+06 7.0E+07 3.0E+07 2.6E+11 2.0E+07 (C) 2.8E+05 Toluene (I) 108883 20x nc nc nc nc nc NA 480 (M) NA NA NA 4.1E+07 2.0E+05 NA p-Toluidine 106490 20x ca ca NA 25,000 NA NA NA 4.0E+06 8,800 NA Toxaphene (KK) 8001352 swpv ca ca NA 330 (M) 2.8E+07 2.8E+07 2.8E+07 1.0E+10 84,000 NA Triallate (DD) 2303175 (DD) (DD) (DD) (DD) swpv dev dev dev dev ca NA 1,300 3.4E+05 3.4E+05 3.4E+05 3.7E+08 8.7E+05 (C) 5.3E+05 Tributylamine 102829 swpv nc nc nc nc nc NA 720 3.4E+05 5.1E+05 3.5E+05 1.4E+09 6.7E+05 NA 1,2,3-Trichlorobenzene 87616 swpv nc nc nc nc nc NA 3,100 24,000 37,000 25,000 1.0E+08 2.1E+05 (C) 1.3E+05 1,2,4-Trichlorobenzene 120821 swpv nc nc nc nc ca NA 4,000 3.3E+06 6.6E+07 2.7E+07 2.5E+11 1.0E+08 (C,D) 2.4E+05 1,1,1-Trichloroethane 71556 20x st nc nc st max NA 100 0.57 2.9 1.3 10,000 1.0E+05 7.2E+05 1,1,2-Trichloroethane 79005 20x nc nc nc nc nc 214 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 100 1,700 26,000 11,000 1.0E+08 33,000 (DD) 2.5E+05 Trichloroethylene (DD,KK,MM,NN) 79016 (DD) (DD) (DD) (DD) 20x dev dev dev dev dev NA 36,000 2.1E+05 6.0E+06 2.4E+06 2.3E+10 7.5E+07 (C) 5.5E+05 Trichlorofluoromethane 75694 20x nc nc nc nc nc NA 10,000 NA NA NA 1.8E+10 7.5E+06 NA 2,4,5-Trichlorophenol (KK) 95954 swpv nc nc NA 2,300 NA NA NA 4.1E+08 5.5E+05 NA 2,4,6-Trichlorophenol (DD,KK) 88062 swpv ca ca NA 0.16 (M) 1,900 4,700 2,500 1.6E+07 37 (MM) 4.6E+05 1,2,3-Trichloropropane (MM) 96184 20x nc nc nc nc mut NA 4.3E+06 (C) 1.2E+07 2.6E+08 1.1E+08 9.9E+11 1.0E+08 (C,D) 2.8E+05 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 swpv nc nc nc nc max NA 60,000 NA NA NA 2.5E+08 1.0E+08 (C,D) 5.3E+07 Triethanolamine 102716 20x nc max NA 4.8E+05 NA NA NA NA 1.0E+08 (C,D) 5.3E+07 Triethylene glycol (DD) 112276 20x max NA 1.6E+05 NA NA NA NA 4.1E+07 (DD) NA 3-Trifluoromethyl-4-nitrophenol (DD) 88302 swpv dev NA 74,000 6.1E+08 6.2E+08 6.2E+08 1.6E+11 3.3E+06 NA Trifluralin 1582098 swpv nc nc nc nc ca NA NA 1.6E+06 4.8E+07 1.9E+07 1.8E+11 NA 30,000 2,2,4-Trimethyl pentane 540841 nc nc nc nc NA NA NA NA NA NA NA 52,000 2,4,4-Trimethyl-2-pentene (I) 107404

NA 2,700 2.2E+05 8.9E+05 4.1E+05 3.1E+09 2.5E+06 (C) 98,000 1,2,3-Trimethylbenzene (I) 526738 swpv nc nc nc nc nc NA 1,300 1.9E+05 8.7E+05 3.9E+05 3.1E+09 2.5E+06 (C) 73,000 1,2,4-Trimethylbenzene (I) 95636 swpv nc nc nc nc nc 215 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C, D, M,Y) Contact Csat Protection

Infinite Source Volatile Soil Hazardous Substance Chemical Statewide Residential Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Drinking Water Inhalation for 2 Meter for 5 Meter Soil Concentration Service Background Protection Criteria Source Source Inhalation Direct Contact Screening Number Level Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 1,500 1.6E+05 8.6E+05 3.8E+05 3.1E+09 2.5E+06 (C) 61,000 1,3,5-Trimethylbenzene (I) 108678 swpv nc nc nc nc nc NA 3.3E+05 NA NA NA NA 4.0E+07 NA Triphenyl phosphate 115866 swpv nc NA 210 17,000 17,000 17,000 2.4E+06 5,500 1.6E+05 tris(2,3-Dibromopropyl)phosphate 126727 swpv ca ca ca ca ca NA NA NA NA NA NA NA NA Urea 57136

27,000 6,700 NA NA NA 5.2E+06 13,000 NA Vanadium (B) 7440622 swpv nc nc NA 70,000 3.5E+05 2.8E+06 1.2E+06 1.0E+10 5.8E+07 (C,DD) 9.1E+05 Vinyl acetate (I,DD) 108054 20x nc nc nc nc dev NA 40 660 21,000 8,600 8.2E+07 760 (LL,MM) NA Vinyl chloride (KK,LL,MM) 75014 (LL,MM) (LL,MM) (LL,MM) (LL,MM) 20x mut mut mut mut mut NA 5,600 5.0E+05 3.1E+06 1.4E+06 1.2E+10 5.0E+07 (C) 87,000 Xylenes (I,J) 1330207 20x nc nc nc nc nc 39,000 5.0E+06 NA NA NA NA 1.0E+08 (D) NA Zinc (B) 7440666 swpv max

216 2017 MR 22 – December 15, 2017

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 58,000 1.8E+05 1.4E+07 1.4E+07 1.4E+07 1.6E+10 5.1E+07 NA Acenaphthene 83329 swpv swpv nc nc nc nc nc NA 58,000 1.8E+05 1.8E+07 1.8E+07 1.8E+07 1.6E+10 5.1E+07 NA Acenaphthylene 208968 swpv swpv nc nc nc nc nc NA 15,000 50,000 36,000 1.2E+05 60,000 6.9E+08 1.0E+08 (D) NA Acetaldehyde (I) 75070 20x 20x nc nc nc nc max NA 68,000 2.2E+05 NA NA NA NA 1.0E+08 (D) NA Acetate 71501 20x 20x max NA 68,000 2.2E+05 2.5E+07 2.5E+07 2.5E+07 1.9E+10 1.0E+08 (C,D) 3.5E+07 Acetic acid 64197 20x 20x nc nc nc nc max NA 1.1E+05 3.4E+05 1.3E+08 3.0E+08 1.6E+08 1.6E+12 1.0E+08 (C,D) 3.7E+07 Acetone (I) 67641 20x 20x st st st st max NA 7,200 22,000 3.5E+05 8.9E+05 4.8E+05 4.6E+09 5.1E+07 (C) 4.2E+07 Acetonitrile 75058 20x 20x nc nc nc nc nc NA 64,000 2.6E+05 5.8E+07 6.0E+07 5.8E+07 1.6E+11 1.0E+08 (C,D) 8.4E+05 Acetophenone (DD) 98862 (DD) (DD) (DD) (DD) 20x 20x dev dev dev dev max NA 480 1,500 63 270 120 1.5E+06 3.4E+06 7.4E+06 Acrolein (I) 107028 20x 20x nc nc nc nc nc NA 10 10 NA NA NA 3.0E+07 65,000 NA Acrylamide (MM) 79061 20x 20x ca ca NA 16,000 76,000 12,000 12,000 12,000 1.5E+07 1.0E+08 (C,D) 3.5E+07 Acrylic acid (DD) 79107 20x 20x nc nc nc nc max NA 26 (M) 140 2,000 7,800 3,600 4.4E+07 61,000 3.7E+06 Acrylonitrile (I) 107131 20x 20x ca ca ca ca ca NA 40 40 NA NA NA NA 3.5E+05 NA Alachlor 15972608 20x 20x ca

217 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 60 60 NA NA NA NA 2.3E+05 NA Aldicarb 116063 20x 20x nc NA 40 (M) 40 (M) NA NA NA NA 8.5E+05 NA Aldicarb sulfone 1646884 20x 20x nc NA 80 (M) 80 (M) NA NA NA NA NA NA Aldicarb sulfoxide 1646873 20x 20x NA 110 580 6,300 6,500 6,500 6.1E+05 2,800 NA Aldrin 309002 swpv swpv ca ca ca ca ca 5.7E+06 1,000 1,000 NA NA NA 4.2E+08 1.0E+08 (D) NA Aluminum (B,DD) 7429905 20x 20x nc max NA 2.0E+05 (N) 2.0E+05 (N) NA NA NA 6.0E+10 NA NA Ammonia (N) 7664417 20x 20x st NA 3,800 3,800 1.2E+05 8.1E+05 3.5E+05 4.8E+09 1.0E+08 (C,D) 8.9E+05 t-Amyl methyl ether (TAME) 994058 20x 20x nc nc nc nc max NA 840 2,600 NA NA NA 7.7E+07 5.8E+06 6.2E+06 Aniline 62533 20x 20x nc ca NA 23,000 23,000 2.4E+08 2.4E+08 2.4E+08 7.7E+10 1.0E+08 (D) NA Anthracene 120127 swpv swpv nc nc nc nc max NA 4,300 4,300 NA NA NA 1.5E+07 6.0E+05 NA Antimony 7440360 swpv swpv nc nc 5,500 4,700 4,700 NA NA NA 7.0E+05 52,000 NA Arsenic (B,KK) 7440382 swpv swpv ca ca NA NA NA NA NA NA (BB) NA NA Asbestos (BB) 1332214

NA 60 60 NA NA NA 1.6E+09 1.5E+07 NA Atrazine 1912249 20x 20x nc nc NA 800 4,000 3.1E+05 3.1E+05 3.1E+05 9.7E+07 3.0E+05 NA Azobenzene 103333 swpv swpv ca ca ca ca ca

218 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels 45,000 1.3E+06 1.3E+06 NA NA NA 3.8E+08 1.0E+08 (D) NA Barium (B,KK) 7440393 swpv swpv nc max NA 100 100 8,200 65,000 28,000 3.8E+08 4.3E+05 6.2E+05 Benzene (I,KK) 71432 20x 20x ca ca ca ca nc NA 0.040 (M) 0.62(M) NA NA NA 45,000 140 (M) NA Benzidine (MM) 92875 swpv swpv ca ca NA 13,000 53,000 1.3E+06 1.4E+06 1.4E+06 5.0E+07 (Q) NA Benzo(a)anthracene (Q,MM) 56553 swpv swpv ca ca ca ca NA 29,000 29,000 NA NA NA 5.0E+07 (Q) NA Benzo(b)fluoranthene (Q,MM) 205992 swpv swpv ca NA 15,000 15,000 NA NA NA 5.0E+08 (Q) NA Benzo(k)fluoranthene (Q,MM) 207089 swpv swpv ca NA 16,000 16,000 NA NA NA 5.4E+08 2.1E+06 NA Benzo(g,h,i)perylene 191242 swpv swpv nc nc NA 3,800 3,800 NA NA NA 1.0E+05 (DD) 41,000 NA Benzo(a)pyrene (Q,DD,MM) 50328 swpv swpv dev ca NA 4.8E+05 1.5E+06 NA NA NA 5.4E+07 1.0E+08 (D) NA Benzoic acid 65850 20x 20x nc max NA 17,000 52,000 NA NA NA 3.8E+11 1.0E+08 (C,D) 3.2E+06 Benzyl alcohol 100516 20x 20x nc max NA 86 (M) 440 9,100 14,000 9,400 6.0E+07 2.0E+05 4.9E+05 Benzyl chloride 100447 20x 20x ca ca ca ca ca 1,000 51,000 51,000 NA NA NA 1.3E+06 2.9E+05 NA Beryllium (B) 7440417 swpv swpv ca nc NA 30 (M) 94 (M) NA NA NA NA 2.1E+05 1.6E+06 bis(2-Chloroethoxy)ethane 112265 20x 20x nc NA 13 (M) 66 (M) 1,800 2,300 1,800 9.1E+06 30,000 1.7E+06 bis-2-Chloroethylether (I) 111444 20x 20x ca ca ca ca ca 219 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 23,000 23,000 NA NA NA 1.9E+09 3.4E+06 (C) 65,000 bis(2-Ethylhexyl) phthalate (DD) 117817 swpv swpv ca ca NA 10,000 (F) 10,000 (F) NA NA NA 2.3E+09 1.0E+08 (D) NA Boron (DD) 7440428 20x 20x nc max NA 200 200 NA NA NA NA 1.4E+05 NA Bromate 15541454 20x 20x ca NA 940 3,000 2.3E+05 8.2E+05 3.9E+05 4.6E+09 6.8E+06 (C) 2.3E+05 Bromobenzene (I) 108861 20x 20x nc nc nc nc nc NA 1,600 (W) 1,600 (W) 3,700 26,000 11,000 1.5E+08 5.3E+05 (C) 3.2E+05 Bromodichloromethane (DD) 75274 20x 20x nc nc nc nc ca NA 1,600 (W) 1,600 (W) 1.6E+05 4.9E+05 2.4E+05 2.7E+09 4.2E+06 (C) 3.0E+05 Bromoform 75252 20x 20x ca ca ca ca ca NA 2,400 7,600 6,800 1.3E+05 52,000 7.7E+08 1.7E+07 NA Bromomethane 74839 20x 20x nc nc nc nc nc NA 12,000 38,000 4.8E+06 6.5E+06 4.9E+06 2.7E+10 8.5E+07 (C) 2.5E+06 n-Butanol (I) 71363 20x 20x nc nc nc nc nc NA 48,000 2.2E+05 1.8E+07 4.7E+07 2.4E+07 2.5E+11 1.0E+08 (C,D) 9.3E+06 2-Butanone (MEK) (I,DD,KK) 78933 (DD) (DD) (DD) (DD) 20x 20x dev dev dev dev max NA 12,000 38,000 1.6E+06 5.5E+06 2.6E+06 3.1E+10 8.5E+07 (C) 5.9E+05 n-Butyl acetate 123864 20x 20x nc nc nc nc nc NA 22,000 68,000 9.5E+05 1.3E+06 9.7E+05 5.5E+09 1.0E+08 (D) NA t-Butyl alcohol 75650 20x 20x nc nc nc nc max NA 18,000 76,000 NA NA NA 6.0E+10 9.9E+06 (DD) NA Butyl benzyl phthalate (DD) 85687 swpv swpv nc dev NA 13,000 42,000 (C) 8.2E+05 2.8E+06 1.3E+06 1.5E+10 3.9E+07 (C) 36,000 n-Butylbenzene 104518 swpv swpv nc nc nc nc nc NA 26,000 84,000 (C) 1,300 5,400 2,500 3.1E+07 8.5E+07 (C) 49,000 sec-Butylbenzene 135988 swpv swpv nc nc nc nc nc 220 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 20,000 63,000 (C) 1,400 5,400 2,500 3.1E+07 8.5E+07 (C) 61,000 t-Butylbenzene (I) 98066 swpv swpv nc nc nc nc nc 2,000 6,000 6,000 NA NA NA 1.7E+06 2.2E+05 NA Cadmium (B,KK) 7440439 swpv swpv ca nc NA NA NA 76,000 1.0E+06 4.2E+05 6.2E+09 NA NA Camphene (I) 79925 nc nc nc nc NA 40,000 1.9E+05 NA NA NA 1.7E+08 1.0E+08 (D) NA Caprolactam (DD) 105602 20x 20x nc max NA 800 3,400 NA NA NA NA 5.0E+06 (DD) NA Carbaryl (DD) 63252 20x 20x dev NA 2,200 11,000 NA NA NA 1.1E+09 3.4E+05 NA Carbazole 86748 swpv swpv ca ca NA 800 800 NA NA NA NA 30,000 (DD) NA Carbofuran (DD) 1563662 20x 20x dev NA 8,800 36,000 4.0E+05 8.8E+06 3.6E+06 5.4E+10 5.5E+07 (C,DD) 2.9E+05 Carbon disulfide (I,R,DD) 75150 20x 20x nc nc nc nc dev NA 100 100 5,200 88,000 36,000 5.4E+08 5.1E+05 (C) 1.8E+05 Carbon tetrachloride (KK) 56235 20x 20x ca ca ca ca ca NA 4,300 4,300 1.3E+05 1.3E+05 1.3E+05 1.4E+07 2.1E+05 NA Chlordane (J,KK) 57749 swpv swpv st st st st ca NA 5.0E+06 5.0E+06 NA NA NA NA NA NA Chloride 16887006 20x 20x NA 360 1,100 NA NA NA 7.7E+08 2.6E+06 (C) 2.1E+06 2-Chloroaniline 95512 20x 20x nc nc NA 60 190 NA NA NA NA 1.7E+05 NA 4-Chloroaniline 106478 20x 20x ca NA 2,000 2,000 1.5E+05 6.7E+05 3.0E+05 3.8E+09 1.7E+07 (C) 2.6E+05 Chlorobenzene (I,KK) 108907 20x 20x nc nc nc nc nc

221 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 94,000 3.0E+05 NA NA NA NA 1.0E+08 (D) NA p-Chlorobenzene sulfonic acid 98668 20x 20x max NA 2.4E+05 8.0E+05 2.7E+07 6.3E+08 2.6E+08 3.8E+12 1.0E+08 (D) NA 1-Chloro-1,1-difluoroethane 75683 20x 20x nc nc nc nc max NA 4,800 15,000 2.5E+06 5.0E+07 2.1E+07 3.1E+11 1.7E+07 NA Chloroethane (DD) 75003 20x 20x nc nc nc nc ca NA NA NA NA NA NA NA NA 44,000 2-Chloroethyl vinyl ether 110758

NA 1,600 (W) 1,600 (W) 2,100 22,000 9,100 1.3E+08 8.5E+06 (C) 8.8E+05 Chloroform (KK) 67663 20x 20x ca ca ca ca nc NA 4,400 22,000 52,000 1.1E+06 4.6E+05 6.9E+09 1.0E+07 NA Chloromethane (I) 74873 20x 20x nc nc nc nc ca NA 8,000 34,000 NA NA NA NA 5.0E+07 (DD) NA 4-Chloro-3-methylphenol (DD) 59507 20x 20x dev NA 38,000 1.2E+05 NA NA NA NA 6.8E+07 NA beta-Chloronaphthalene 91587 swpv swpv nc NA 640 2,600 6.8E+05 6.8E+05 6.8E+05 9.0E+08 4.0E+06 (DD) 7.3E+06 2-Chlorophenol (DD) 95578 (DD) (DD) (DD) (DD) 20x 20x dev dev dev dev dev NA 800 2,600 3.0E+05 1.1E+06 5.2E+05 6.2E+09 5.7E+06 (C) 3.0E+05 o-Chlorotoluene (I) 95498 20x 20x nc nc nc nc nc NA 4,400 18,000 NA NA NA 7.7E+07 3.3E+06 (DD) NA Chlorpyrifos (DD) 2921882 swpv swpv nc dev 15,000 1.0E+08 (D) 1.0E+08 (D) NA NA NA 7.7E+06 1.0E+08 (D) NA Chromium (III) (B,H,KK) 16065831 max max nc max NA 31,000 31,000 NA NA NA 2.5E+05 36,000 NA Chromium (VI) (H,KK,MM) 18540299 swpv swpv ca ca NA 25,000 25,000 NA NA NA 5.0E+09 (Q) NA Chrysene (Q,MM) 218019 swpv swpv ca 222 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels 10,000 36 (M) 110 (M) NA NA NA 3.3E+05 7.4E+05 NA Cobalt (B) 7440484 20x 20x ca nc 14,000 5.8E+06 5.8E+06 NA NA NA 1.5E+08 2.5E+06 NA Copper (B) 7440508 swpv swpv nc nc NA 24 (M) 76 (M) NA NA NA NA 90,000 NA Cyanazine 21725462 20x 20x ca NA 4,000 4,000 1,900 11,000 4,900 6.2E+07 8.2E+05 3.9E+07 Cyanide (P,R,DD) Varies 20x 20x nc nc nc nc nc NA NA NA 3.2E+06 7.5E+07 3.1E+07 4.6E+11 NA 50,000 Cyclohexane (DD) 110827 nc nc nc nc NA 24,000 76,000 1.4E+07 1.6E+07 1.4E+07 5.4E+10 1.0E+08 (C,D) 1.7E+06 Cyclohexanone 108941 20x 20x nc nc nc nc max NA 1,200 3,800 NA NA NA NA 8.5E+06 NA Dacthal 1861321 20x 20x nc NA 4,000 4,000 NA NA NA NA 2.6E+07 (C) 2.0E+07 Dalapon 75990 20x 20x nc NA 11,000 56,000 NA NA NA 4.3E+07 2.0E+05 NA 4-4'-DDD 72548 swpv swpv ca ca NA 7,900 41,000 2.9E+05 3.0E+05 3.0E+05 3.1E+07 1.4E+05 NA 4-4'-DDE 72559 swpv swpv ca ca ca ca ca NA 11,000 30,000 NA NA NA 3.1E+07 2.3E+05 NA 4-4'-DDT (DD) 50293 swpv swpv ca ca NA 880 880 NA NA NA 1.3E+09 4.9E+06 (DD) NA Decabromodiphenyl ether (DD) 1163195 (DD) swpv swpv dev dev NA 1,000 4,100 NA NA NA 1.0E+09 3.3E+06 (C,DD) 26,000 Di-n-butyl phthalate (DD) 84742 (DD) swpv swpv dev dev

223 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 4.6E+05 (C) 4.6E+05 (C) NA NA NA 8.8E+09 4.0E+07 (C) 56,000 Di(2-ethylhexyl) adipate (DD) 103231 swpv swpv ca ca NA 99,000 99,000 4.5E+08 4.7E+08 4.7E+08 3.6E+10 1.5E+07 NA Di-n-octyl phthalate 117840 swpv swpv nc nc nc nc nc NA NA NA 2.1E+08 2.1E+08 2.1E+08 1.8E+11 NA 3.5E+07 Diacetone alcohol (I) 123422 nc nc nc nc NA 410 1,300 NA NA NA 7.7E+07 6.0E+05 NA Diazinon 333415 swpv swpv nc nc NA 1.4E+04 1.5E+05 NA NA NA 5.0E+06 (Q) NA Dibenzo(a,h)anthracene (Q,MM) 53703 swpv swpv ca NA 1,700 5,600 4.1E+05 4.1E+05 4.1E+05 3.1E+08 8.5E+05 NA Dibenzofuran 132649 swpv swpv nc nc nc nc nc NA 1,600 (W) 1,600 (W) 5,900 22,000 10,000 1.2E+08 3.9E+05 (C) 2.7E+05 Dibromochloromethane (MM) 124481 20x 20x ca ca ca ca ca NA 4 (M) 4 (M) 100 130 100 5.4E+05 41,000 3.3E+05 Dibromochloropropane (MM) 96128 20x 20x ca ca ca ca ca NA 360 1,100 10,000 53,000 24,000 3.1E+08 2.6E+06 (C) 9.4E+05 Dibromomethane 74953 20x 20x nc nc nc nc nc NA 36,000 1.7E+05 NA NA NA NA 1.0E+08 (D) NA Dicamba (DD) 1918009 20x 20x max NA 12,000 12,000 1.6E+06 4.3E+06 2.2E+06 2.3E+10 1.0E+08 (C,D) 1.3E+05 1,2-Dichlorobenzene 95501 20x 20x nc nc nc nc max NA 240 760 14,000 42,000 21,000 2.3E+08 1.7E+06 (C) 99,000 1,3-Dichlorobenzene 541731 20x 20x nc nc nc nc nc NA 1,500 1,500 48,000 1.4E+05 70,000 7.7E+08 2.6E+06 NA 1,4-Dichlorobenzene (KK) 106467 20x 20x ca ca ca ca ca NA 160 (M) 840 (M) NA NA NA 8.8E+06 74,000 NA 3,3`-Dichlorobenzidine 91941 swpv swpv ca ca

224 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 710 2,200 1.6E+05 4.1E+06 1.7E+06 2.5E+10 4.3E+06 NA Dichlorodifluoromethane 75718 swpv swpv nc nc nc nc nc NA 2,600 13,000 24,000 3.1E+05 1.3E+05 1.9E+09 5.8E+06 (C) 6.0E+05 1,1-Dichloroethane 75343 20x 20x ca ca ca ca ca NA 100 100 3,100 20,000 8,600 1.2E+08 3.6E+05 1.0E+06 1,2-Dichloroethane (I,KK) 107062 20x 20x ca ca ca ca ca NA 140 140 1.2E+05 2.5E+06 1.0E+06 1.5E+10 4.3E+07 (C) 4.8E+05 1,1-Dichloroethylene (I,KK) 75354 20x 20x nc nc nc nc nc NA 1,400 1,400 9,300 1.0E+05 43,000 6.2E+08 1.7E+06 (C) 8.2E+05 cis-1,2-Dichloroethylene 156592 20x 20x nc nc nc nc nc NA 2,000 2,000 4.6E+05 6.5E+06 2.7E+06 4.0E+10 1.7E+07 (C) 7.9E+05 trans-1,2-Dichloroethylene 156605 20x 20x st st st st nc NA 940 3,000 NA NA NA 6.8E+08 2.1E+06 NA 2,6-Dichloro-4-nitroaniline 99309 swpv swpv nc nc NA 1,600 7,600 NA NA NA 8.5E+08 1.7E+07 NA 2,4-Dichlorophenol (DD) 120832 20x 20x nc nc NA 1,400 1,400 NA NA NA 1.3E+10 5.3E+07 NA 2,4-Dichlorophenoxyacetic acid (KK) 94757 20x 20x nc nc NA 100 100 7,000 52,000 22,000 3.1E+08 9.2E+05 (C) 4.6E+05 1,2-Dichloropropane (I) 78875 20x 20x nc nc nc nc ca NA 140 740 16,000 1.3E+05 54,000 7.5E+08 3.3E+05 5.3E+05 1,3-Dichloropropene (J) 542756 20x 20x ca ca ca ca ca NA 16 (M) 190 NA NA NA 1.5E+08 1.1E+05 1.1E+06 Dichlorvos (MM) 62737 20x 20x nc ca NA NA NA NA NA NA NA NA NA Dicyclohexyl phthalate 84617

NA 29 150 6,900 7,100 7,100 6.5E+05 3,000 NA Dieldrin 60571 swpv swpv ca ca ca ca ca

225 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 24 (M) 24 (M) 1.4E+06 1.3E+07 5.5E+06 7.7E+10 1.0E+08 (C,D) 3.4E+06 Diethyl ether 60297 20x 20x nc nc nc nc max NA 94,000 3.0E+05 (C) NA NA NA 2.2E+11 1.0E+08 (C,D) 2.6E+05 Diethyl phthalate 84662 20x 20x nc max NA 3,600 11,000 NA NA NA 7.7E+06 2.6E+07 5.3E+07 Diethylene glycol monobutyl ether 112345 20x 20x nc nc NA 22,000 90,000 6.5E+05 5.9E+06 2.5E+06 3.5E+10 1.0E+08 (C,D) 7.8E+05 Diisopropyl ether (DD) 108203 (DD) (DD) (DD) (DD) 20x 20x dev dev dev dev max NA 92 300 2.0E+06 3.3E+06 2.1E+06 1.5E+10 6.5E+05 1.8E+07 Diisopropylamine (I) 108189 20x 20x nc nc nc nc nc NA 12,000 38,000 NA NA NA 3.8E+09 8.5E+07 (C) 3.8E+05 Dimethyl phthalate 131113 20x 20x nc nc NA 3,000 9,400 2.6E+07 2.5E+07 2.5E+07 7.7E+09 2.1E+07 3.9E+07 N,N-Dimethylacetamide 127195 20x 20x nc nc nc nc nc NA 240 760 47,000 61,000 47,000 2.5E+08 6.8E+05 (C) 2.8E+05 N,N-Dimethylaniline 121697 20x 20x ca ca ca ca ca NA 12,000 38,000 8.7E+05 8.7E+05 8.7E+05 5.4E+08 8.5E+07 (C) 3.5E+07 Dimethylformamide (I) 68122 20x 20x nc nc nc nc nc NA 2,400 7,600 NA NA NA 5.4E+09 1.7E+07 NA 2,4-Dimethylphenol 105679 20x 20x nc nc NA 72 (M) 220 (M) NA NA NA 1.5E+08 5.1E+05 NA 2,6-Dimethylphenol 576261 20x 20x nc nc NA 120 (M) 380 NA NA NA 2.7E+08 8.5E+05 NA 3,4-Dimethylphenol 95658 20x 20x nc nc NA 1.2E+05 3.8E+05 NA NA NA 1.5E+09 1.0E+08 (C,D) 3.7E+07 Dimethylsulfoxide 67685 20x 20x nc max NA 240 (M) 760 NA NA NA 5.4E+08 1.7E+06 NA 2,4-Dinitrophenol 51285 20x 20x nc nc 226 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 22 110 NA NA NA 3.4E+07 49,000 NA 2,4-Dinitrotoluene (KK) 121142 20x 20x ca ca NA 970 970 NA NA NA 3.1E+08 8.5E+05 NA Dinoseb (DD) 88857 swpv swpv nc nc NA 140 (M) 740 1.4E+05 1.7E+05 1.4E+05 6.0E+08 3.3E+05 3.8E+07 1,4-Dioxane (I) 123911 20x 20x ca ca ca ca ca NA 400 400 NA NA NA NA 4.3E+06 NA Diquat 85007 20x 20x nc NA 360 (M) 1,100 NA NA NA 2.5E+08 1.7E+06 NA Diuron 330541 20x 20x nc ca NA 6,500 20,000 NA NA NA NA 4.3E+06 NA Endosulfan (J) 115297 swpv swpv nc NA 2,000 2,000 NA NA NA 5.4E+09 6.0E+06 NA Endothall 145733 20x 20x nc nc NA 790 790 NA NA NA NA 3.7E+05 NA Endrin (KK) 72208 swpv swpv nc NA 40 (M) 40 (M) 8,700 16,000 9,600 7.7E+07 3.7E+05 3.5E+06 Epichlorohydrin (I) 106898 20x 20x nc nc nc nc ca NA 2.4E+07 1.0E+08 (C,D) 1.8E+08 2.4E+08 1.9E+08 9.5E+11 1.0E+08 (C,D) 3.5E+07 Ethanol (I,DD) 64175 20x max st st st st max NA 8,600 28,000 2.7E+05 9.6E+05 4.6E+05 5.4E+09 6.1E+07 (C) 3.5E+06 Ethyl acetate (I) 141786 20x 20x nc nc nc nc nc NA 980 980 6.3E+05 4.8E+06 2.1E+06 2.8E+10 7.8E+07 (C) 9.7E+05 Ethyl-tert-butyl ether (ETBE) 637923 20x 20x nc nc nc nc nc NA 1,500 1,500 41,000 2.1E+05 92,000 1.2E+09 3.0E+06 (C) 1.6E+05 Ethylbenzene (I) 100414 20x 20x ca ca ca ca ca NA 1.0 (M) 1.0 (M) 260 890 430 5.0E+06 17,000 4.5E+05 Ethylene dibromide 106934 20x 20x ca ca ca ca ca

227 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 6.4E+04 2.6E+05 NA NA NA 1.5E+09 1.0E+08 (C,D) 3.5E+07 Ethylene glycol (DD) 107211 20x 20x nc max NA 12,000 38,000 NA NA NA 1.2E+11 8.5E+07 (C) 3.8E+07 Ethylene glycol monobutyl ether 111762 20x 20x nc nc Ethylenediaminetetraacetic acid NA NA NA NA NA NA NA NA NA 60004 (EDTA) (II) NA 4.3E+05 4.6E+05 NA NA NA 1.1E+10 4.9E+07 NA Fluoranthene 206440 swpv swpv nc nc NA 70,000 2.2E+05 1.5E+07 1.5E+07 1.5E+07 1.1E+10 3.4E+07 NA Fluorene 86737 swpv swpv nc nc nc nc nc NA 40,000 40,000 NA NA NA NA 1.0E+08 (D) NA Fluorine (soluble fluoride) (DD) 7782414 20x 20x max NA 24,000 76,000 1.3E+05 1.7E+05 1.7E+05 2.3E+08 1.0E+08 (D) NA Formaldehyde (MM) 50000 20x 20x ca ca ca ca max NA 1.1E+05 3.4E+05 21,000 24,000 24,000 2.3E+07 1.0E+08 (C,D) 3.5E+07 Formic acid (I,U) 64186 20x 20x nc nc nc nc max NA 88,000 3.6E+05 NA NA NA NA 1.0E+08 (C,D) 3.9E+06 1-Formylpiperidine (DD) 2591868 20x 20x max NA 2.8E+05 1.4E+06 NA NA NA NA 6.0E+05 NA Gentian violet 548629 swpv swpv ca NA 14,000 14,000 NA NA NA NA 5.0E+07 (DD) NA Glyphosate (DD) 1071836 20x 20x dev NA 18,000 18,000 38,000 40,000 40,000 2.3E+06 40,000 NA Heptachlor (DD,KK) 76448 swpv swpv ca ca ca ca ca NA 65 65 4,800 4,900 4,900 1.2E+06 13,000 NA Heptachlor epoxide (KK) 1024573 swpv swpv ca ca ca ca ca NA 4.6E+05 (C) 4.6E+05 (C) 1.7E+06 4.4E+07 1.8E+07 2.7E+11 1.0E+08 (C,D) 29,000 n-Heptane 142825 swpv swpv nc nc nc nc max

228 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 14 (M) 14 (M) NA NA NA NA 2.5E+06 NA Hexabromobenzene 87821 swpv swpv nc NA 200 (M) 200 (M) 1,100 1,100 1,100 2.7E+06 12,000 NA Hexachlorobenzene (C-66) (KK) 118741 swpv swpv nc nc nc nc nc NA 170 540 8,800 25,000 13,000 1.4E+08 4.3E+05 (C) 5,600 Hexachlorobutadiene (C-46) (KK) 87683 swpv swpv ca ca ca ca ca NA 9.9 (M) 52 NA NA NA 1.7E+06 5,300 NA alpha-Hexachlorocyclohexane 319846 swpv swpv ca ca NA 33 99 NA NA NA 5.7E+06 18,000 NA beta-Hexachlorocyclohexane 319857 swpv swpv ca ca NA 2,400 2,400 780 2,800 1,300 1.5E+07 7.4E+06 (C) 5,300 Hexachlorocyclopentadiene (C-56) 77474 swpv swpv nc nc nc nc nc NA 84 (M) 260 (M) 14,000 53,000 25,000 3.0E+08 6.0E+05 NA Hexachloroethane (KK) 67721 20x 20x ca ca ca ca nc NA 2.1E+05 (C) 6.8E+05 (C) 3.2E+05 8.8E+06 3.6E+06 5.4E+10 1.0E+08 (C,D) 70,000 n-Hexane 110543 swpv swpv nc nc nc nc max NA 600 (M) 1,900 (M) 1.8E+05 4.4E+05 2.3E+05 2.3E+09 4.3E+06 (C) 1.1E+06 2-Hexanone 591786 20x 20x nc nc nc nc nc NA 1.2E+04 1.2E+04 NA NA NA 5.0E+07 (Q) NA Indeno(1,2,3-cd)pyrene (Q,MM) 193395 swpv swpv ca 1.125E+07 6,000 6,000 NA NA NA NA 1.0E+08 (D) NA Iron (B) 7439896 20x 20x max NA 36,000 1.1E+05 1.9E+07 2.7E+07 2.0E+07 1.2E+11 1.0E+08 (C,D) 3.3E+06 Isobutyl alcohol (I) 78831 20x 20x nc nc nc nc max NA 15,000 76,000 NA NA NA 1.1E+10 3.5E+07 (C) 2.0E+06 Isophorone (DD) 78591 20x 20x ca ca

229 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 1.6E+05 7.6E+05 2.6E+06 3.6E+06 2.6E+06 1.5E+10 1.0E+08 (C,D) 3.6E+07 Isopropyl alcohol (I,DD) 67630 20x 20x nc nc nc nc max NA 14,000 45,000 11,000 50,000 22,000 2.9E+08 8.5E+07 (C) 90,000 Isopropyl benzene 98828 swpv swpv ca ca ca ca nc 11,000 1.8E+05 (L) 1.8E+05 (L) NA NA NA 1.2E+07 (L) 7.6E+05 NA Lead (B,L,DD,KK) 7439921 swpv swpv nc (L,DD) NA 18 (M) 18 (M) NA NA NA NA 39,000 NA Lindane (KK) 58899 swpv swpv ca 11,000 160 (M) 660 NA NA NA 2.7E+09 3.0E+06 (DD) NA Lithium (B,DD) 7439932 20x 20x nc dev NA 6.6E+06 2.0E+07 NA NA NA 7.7E+09 1.0E+08 (D) NA Magnesium 7439954 20x 20x nc max 3.6E+05 1,000 1,000 NA NA NA 2.3E+07 3.2E+07 NA Manganese (B) 7439965 20x 20x nc nc NA 40 40 190 3,800 1,500 2.3E+07 1.5E+05 (DD) NA Mercury (Total) (Z,DD,KK) Varies 20x 20x nc nc nc nc dev NA NA NA NA NA NA NA NA NA Methane (K) 74828

NA 1.6E+05 6.6E+05 1.8E+08 2.6E+08 2.1E+08 1.0E+12 1.0E+08 (C,D) 3.5E+07 Methanol (DD) 67561 (DD) (DD) (DD) (DD) 20x 20x dev dev dev dev max NA 34,000 34,000 NA NA NA NA 3.5E+06 (DD) NA Methoxychlor (DD,KK) 72435 swpv swpv dev NA 400 1,700 70,000 70,000 70,000 8.5E+07 2.5E+06 (DD) 3.5E+07 2-Methoxyethanol (I,DD) 109864 20x 20x nc nc nc nc dev NA 520 1,700 NA NA NA 1.4E+09 3.7E+06 NA 2-Methyl-4-chlorophenoxyacetic acid 94746 20x 20x nc nc NA 59 (M) 190 (M) NA NA NA 1.5E+08 3.4E+05 NA 2-Methyl-4,6-dinitrophenol 534521 swpv swpv nc nc

230 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 8,400 26,000 NA NA NA NA 6.0E+07 (C) 4.7E+07 N-Methyl-morpholine (I) 109024 20x 20x nc NA 29 (M) 91 NA NA NA NA 1.7E+05 NA Methyl parathion 298000 swpv swpv nc NA 6,000 19,000 9.4E+06 2.8E+07 1.4E+07 1.5E+11 4.3E+07 (C) 1.1E+06 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 (DD) (DD) (DD) (DD) nc 20x 20x dev dev dev dev NA 800 800 3.4E+05 2.0E+06 8.7E+05 1.2E+10 9.8E+06 (C) 3.0E+06 Methyl-tert-butyl ether (MTBE) 1634044 20x 20x ca ca ca ca ca NA 240 760 NA NA NA NA 1.7E+06 (C) 1.1E+06 N-methylaniline 100618 20x 20x nc NA NA NA 3.4E+05 8.8E+06 3.6E+06 5.4E+10 NA 72,000 Methylcyclopentane (I) 96377 nc nc nc nc 4,4`-Methylene-bis-2- chloroaniline NA 2,200 6,900 NA NA NA NA 1.7E+06 NA 101144 (MBOCA) (MM) swpv swpv nc NA 100 100 6.1E+05 7.6E+06 3.2E+06 4.6E+10 5.1E+06 (C) 1.2E+06 Methylene chloride (MM) 75092 20x 20x nc nc nc nc nc NA 1,900 6,100 2.7E+05 2.8E+05 2.7E+05 7.7E+08 3.4E+06 NA 2-Methylnaphthalene 91576 swpv swpv nc nc nc nc nc NA 600 1,900 NA NA NA 7.7E+09 4.3E+06 NA Methylphenols (JJ,KK) 1319773 20x 20x nc nc NA 16,000 76,000 NA NA NA 7.7E+09 1.0E+08 (D) NA 2-Methylphenol (DD,KK) 95487 20x 20x nc max NA 12,000 38,000 NA NA NA NA 8.5E+07 (C) 5.4E+05 Metolachlor 51218452 20x 20x nc NA 1,500 5,000 NA NA NA NA 1.1E+07 NA Metribuzin 21087649 20x 20x nc NA 8,900 43,000 NA NA NA NA 52,000 NA Mirex 2385855 swpv swpv ca 231 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 1,200 3,800 NA NA NA 2.3E+09 1.2E+07 NA Molybdenum 7439987 20x 20x nc nc NA 29,000 95,000 24,000 27,000 24,000 8.8E+07 8.5E+07 NA Naphthalene 91203 swpv swpv ca ca ca ca nc 15,000 38,000 1.1E+05 NA NA NA 6.9E+06 4.0E+06 NA Nickel (B) 7440020 swpv swpv nc nc NA 2.0E+05 (N) 2.0E+05 (N) NA NA NA NA 1.0E+08 (D) NA Nitrate (N,DD) 14797558 20x 20x max NA 20,000 (N) 20,000 (N) NA NA NA NA 1.0E+08 (D) NA Nitrite (N,DD) 14797650 20x 20x max NA 240 (M) 760 33,000 33,000 33,000 7.5E+07 1.7E+06 (C) 1.0E+06 Nitrobenzene (I,KK) 98953 20x 20x ca ca ca ca nc NA 240 (M) 760 2,700 2,700 2,700 3.9E+06 1.7E+06 NA 2-Nitrophenol 88755 20x 20x nc nc nc nc nc NA 2 (M) 11 (M) NA NA NA 1.5E+06 4,700 7.6E+06 n-Nitroso-di-n-propylamine 621647 20x 20x ca ca NA 13,000 64,000 NA NA NA NA 6.8E+06 NA N-Nitrosodiphenylamine 86306 swpv swpv ca NA 4,000 4,000 NA NA NA 1.9E+09 5.9E+06 NA Oxamyl 23135220 20x 20x nc nc NA 1,200 3,800 NA NA NA 6.2E+09 8.5E+06 NA Oxo-hexyl acetate 88230357 20x 20x nc nc NA 59,000 59,000 NA NA NA NA 1.0E+08 (D) NA Pendimethalin (DD) 40487421 swpv swpv max NA 560 1,800 3,700 3,700 3,700 7.7E+06 9.8E+05 NA Pentachlorobenzene 608935 swpv swpv nc nc nc nc nc NA 3,500 11,000 2.2E+06 2.2E+06 2.2E+06 8.5E+08 2.6E+06 NA Pentachloronitrobenzene 82688 swpv swpv nc nc nc nc nc

232 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 160 160 NA NA NA 2.7E+07 65,000 NA Pentachlorophenol (KK) 87865 swpv swpv ca ca NA NA NA 4.4E+05 1.3E+07 5.1E+06 7.7E+10 NA 1.9E+05 Pentane 109660 nc nc nc nc NA NA NA NA NA NA NA NA 2.3E+05 2-Pentene (I) 109682

NA 56 (M) 240 NA NA NA NA 1.0E+06 (DD) NA Perchlorate (DD) 14797730 20x 20x dev NA 59 (NN) 59 (NN) NA NA NA NA 25,000 NA Perfluorooctanoic acid (DD) 335671 swpv swpv nc NA 1.4 (NN) 1.4 (NN) NA NA NA NA 25,000 NA Perfluorooctane sulfonic acid (DD) 1763231 20x 20x nc NA 96,000 3.0E+05 28,000 29,000 29,000 7.7E+06 2.6E+07 NA Phenanthrene 85018 swpv swpv nc nc nc nc nc NA 24,000 1.1E+05 NA NA NA 1.5E+10 1.0E+08 (D) NA Phenol (DD) 108952 20x 20x nc max NA 670 3,400 NA NA NA 2.1E+08 6.5E+05 NA Phenytoin (DD) 57410 swpv swpv ca ca NA NA NA NA NA NA NA NA NA Phosphorus, Total Varies

NA 2 7 NA NA NA 1.5E+07 14,000 (DD) NA Phosphorus, White (R,DD) 7723140 20x 20x nc dev NA 2.2E+05 7.2E+05 NA NA NA NA 1.0E+08 (D) NA o-Phthalic acid 88993 20x 20x max NA 2.4E+05 7.6E+05 NA NA NA 1.5E+09 1.0E+08 (D) NA Phthalic anhydride 85449 20x 20x nc max NA 10,000 10,000 NA NA NA NA 6.0E+07 NA Picloram 1918021 20x 20x nc

233 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 52 170 2.7E+08 2.7E+08 2.7E+08 5.4E+11 3.7E+05 1.4E+08 Piperidine 110894 20x 20x nc nc nc nc nc NA 2 (M) 10 (M) NA NA NA NA 6,700 NA Polybrominated biphenyls (J,DD) 67774327 20x 20x ca Polychlorinated biphenyls (PCBs) NA 1,200 1,200 71,000 72,000 72,000 3.0E+07 20,000 (T) NA 1336363 (J,T,DD) swpv swpv ca ca ca ca ca Polychlorinated biphenyls (PCBs) NA (O) (O) (O) (O) (O) (O) (O) NA Varies congeners (O) NA 6,000 19,000 NA NA NA NA 4.3E+07 NA Prometon 1610180 20x 20x nc NA 460 2,400 NA NA NA NA 1.0E+06 NA Propachlor 1918167 20x 20x ca NA 2,200 6,800 NA NA NA NA 1.5E+07 NA Propazine 139402 20x 20x nc NA 2.2E+05 6.8E+05 1.6E+07 1.7E+07 1.7E+07 2.3E+10 1.0E+08 (C,D) 3.5E+07 Propionic acid 79094 20x 20x nc nc nc nc max NA 1.6E+05 6.6E+05 6.4E+06 8.7E+06 6.5E+06 3.7E+10 1.0E+08 (C,D) 3.6E+07 Propyl alcohol (I,DD) 71238 (DD) (DD) (DD) (DD) 20x 20x dev dev dev dev max NA 16,000 52,000 2.1E+06 8.8E+06 4.0E+06 5.0E+10 8.5E+07 (C) 89,000 n-Propylbenzene (I,DD) 103651 (DD) (DD) (DD) (DD) swpv swpv dev dev dev dev nc NA 2.4E+06 7.6E+06 NA NA NA NA 1.0E+08 (C,D) 3.5E+07 Propylene glycol 57556 20x 20x max NA 2.4E+05 2.4E+05 1.1E+08 1.2E+08 1.2E+08 7.7E+09 3.7E+07 NA Pyrene 129000 swpv swpv nc nc nc nc nc NA 120 380 90,000 95,000 90,000 2.7E+08 8.5E+05 1.8E+08 Pyridine (I,KK) 110861 20x 20x nc nc nc nc nc

234 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels 610 4,200 4,200 NA NA NA 1.5E+09 1.2E+07 NA Selenium (B,KK) 7782492 swpv swpv nc nc NA 14,000 14,000 NA NA NA 2.3E+08 6.7E+05 NA Silver (KK) 7440224 swpv swpv nc nc NA 1,000 1,000 NA NA NA NA 6.8E+06 NA Silvex (2,4,5-TP) (KK) 93721 20x 20x nc NA 80 80 NA NA NA NA 4.3E+06 NA Simazine 122349 20x 20x nc NA 1.1E+06 3.6E+06 NA NA NA NA 1.0E+08 (D) NA Sodium 17341252 20x 20x max NA 1,400 (M) 4,600 NA NA NA NA 2.9E+07 NA Sodium azide 26628228 20x 20x nc NA 4,800 15,000 NA NA NA 1.1E+10 9.8E+07 NA Sodium bromide 7647156 20x 20x nc nc 1.29E+05 48,000 2.2E+05 NA NA NA NA 1.0E+08 (D) NA Strontium (B,DD) 7440246 20x 20x max NA 2,000 2,000 2.9E+05 9.5E+05 4.6E+05 5.3E+09 2.6E+06 (C) 2.9E+05 Styrene 100425 20x 20x ca ca ca ca ca NA 5.0E+06 5.0E+06 NA NA NA NA NA NA Sulfate 14808798 20x 20x NA 120 (M) 380 NA NA NA 4.9E+08 8.5E+05 NA Sulfolane 126330 20x 20X nc nc NA 5,600 26,000 NA NA NA NA 6.0E+07 NA Tebuthiuron (DD) 34014181 20x 20x nc 2,3,7,8-Tetrabromodibenzo-p-dioxin NA (O) (O) NA NA NA NA (O) NA 50585416 (O)

235 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 2,000 8,600 23,000 25,000 23,000 7.7E+07 3.5E+06 (DD) NA 1,2,4,5-Tetrachlorobenzene (DD) 95943 swpv swpv nc nc nc nc dev 2,3,7,8-Tetrachlorodibenzo-p-dioxin NA 0.24 (O) 0.24 (O) 1.1 (O) 1.1 (O) 1.1 (O) 68 (O) 1.0 (O) NA 1746016 (O,DD) swpv swpv ca ca ca ca ca NA 560 2,800 14,000 70,000 31,000 4.1E+08 1.3E+06 (C) 2.3E+05 1,1,1,2-Tetrachloroethane 630206 20x 20x ca ca ca ca ca NA 72 360 4,600 10,000 5,600 5.2E+07 1.7E+05 6.3E+05 1,1,2,2-Tetrachloroethane 79345 20x 20x ca ca ca ca ca NA 100 100 30,000 3.4E+05 1.4E+05 2.1E+09 5.1E+06 (C) 60,000 Tetrachloroethylene (KK) 127184 20x 20x st st st st nc NA 72,000 3.4E+05 1.1E+07 2.9E+07 1.5E+07 1.5E+11 1.0E+08 (C,D) 5.4E+07 Tetrahydrofuran (DD) 109999 20x 20x nc nc nc nc max NA NA NA 2.4E+05 2.5E+05 2.5E+05 6.2E+07 NA 4.0E+07 1,1,3,3-Tetramethylurea 632224 nc nc nc nc NA NA NA 53 60 54 2.0E+05 NA 8.0E+05 Tetranitromethane 509148 ca ca ca ca NA 2,300 2,300 NA NA NA 1.5E+07 25,000 NA Thallium 7440280 swpv swpv nc nc NA 16,000 16,000 9.7E+06 6.4E+07 2.8E+07 3.8E+11 6.7E+07 (C) 2.8E+05 Toluene (I) 108883 20x 20x st st st st nc NA 480 (M) 1,500 NA NA NA 9.7E+07 1.1E+06 NA p-Toluidine 106490 20x 20x ca ca NA 25,000 25,000 NA NA NA 9.4E+06 44,000 NA Toxaphene (KK) 8001352 swpv swpv ca ca NA 330 (M) 1,700 (M) 2.2E+07 2.2E+07 2.2E+07 1.0E+10 4.6E+05 NA Triallate (DD) 2303175 (DD) (DD) (DD) (DD) swpv swpv dev dev dev dev ca

236 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 1,300 4,000 4.0E+05 4.0E+05 4.0E+05 5.4E+08 3.0E+06 (C) 5.3E+05 Tributylamine 102829 swpv swpv nc nc nc nc nc NA 720 2,300 4.0E+05 5.2E+05 4.0E+05 2.1E+09 2.3E+06 NA 1,2,3-Trichlorobenzene 87616 swpv swpv nc nc nc nc nc NA 3,100 3,100 27,000 37,000 28,000 1.5E+08 1.1E+06 (C) 1.3E+05 1,2,4-Trichlorobenzene 120821 swpv swpv nc nc nc nc ca NA 4,000 4,000 3.7E+06 5.8E+07 2.4E+07 3.5E+11 1.0E+08 (C,D) 2.4E+05 1,1,1-Trichloroethane 71556 20x 20x st st st st max NA 100 100 0.66 2.7 1.2 15,000 3.4E+05 7.2E+05 1,1,2-Trichloroethane 79005 20x 20x nc nc nc nc nc NA 100 100 1,400 17,000 6,900 1.0E+08 2.5E+05 2.5E+05 Trichloroethylene (DD,KK,MM,NN) 79016 (DD) (DD) (DD) (DD) (DD) 20x 20x dev dev dev dev dev NA 36,000 1.1E+05 2.4E+05 5.5E+06 2.3E+06 3.4E+10 1.0E+08 (C,D) 5.5E+05 Trichlorofluoromethane 75694 20x 20x nc nc nc nc max NA 10,000 33,000 NA NA NA 2.7E+10 2.6E+07 NA 2,4,5-Trichlorophenol (KK) 95954 swpv swpv nc nc NA 2,300 9,800 NA NA NA 9.7E+08 3.0E+06 NA 2,4,6-Trichlorophenol (DD,KK) 88062 swpv swpv ca ca NA 0.16 (M) 2.4 (M) 2,200 4,500 2,500 2.3E+07 1,100 4.6E+05 1,2,3-Trichloropropane (MM) 96184 20x 20x nc nc nc nc ca NA 4.3E+06 (C) 4.6E+06 (C) 1.4E+07 2.4E+08 9.9E+07 1.5E+12 1.0E+08 (C,D) 2.8E+05 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 swpv swpv nc nc nc nc max NA 60,000 1.9E+05 NA NA NA 3.6E+08 1.0E+08 (C,D) 5.3E+07 Triethanolamine 102716 20x 20x nc max NA 4.8E+05 2.2E+06 NA NA NA NA 1.0E+08 (C,D) 5.3E+07 Triethylene glycol (DD) 112276 20x 20x max NA 1.6E+05 7.9E+05 NA NA NA NA 1.0E+08 (D) NA 3-Trifluoromethyl-4-nitrophenol (DD) 88302 swpv swpv max

237 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (µg/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the criterion. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)).

Groundwater Ambient Air (C,D,M,Y) Contact Csat Protection

Infinite Residential Nonresidential Source Chemical Statewide Drinking Drinking Volatile Soil Finite VSIC Finite VSIC Particulate Soil Saturation Hazardous Substance Abstract Default Water Water Inhalation for 2 Meter for 5 Meter Soil Direct Concentration Service Background Protection Protection Criteria Source Source Inhalation Contact Screening Number Level Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels NA 74,000 95,000 7.1E+08 7.2E+08 7.2E+08 2.3E+11 1.6E+07 NA Trifluralin 1582098 swpv swpv nc nc nc nc ca NA NA NA 1.8E+06 4.4E+07 1.8E+07 2.7E+11 NA 30,000 2,2,4-Trimethyl pentane 540841 nc nc nc nc NA NA NA NA NA NA NA NA 52,000 2,4,4-Trimethyl-2-pentene (I) 107404

NA 2,700 2,700 2.6E+05 8.3E+05 4.1E+05 4.6E+09 8.5E+06 (C) 98,000 1,2,3-Trimethylbenzene (I) 526738 swpv swpv nc nc nc nc nc NA 1,300 1,300 2.2E+05 8.2E+05 3.8E+05 4.6E+09 8.5E+06 (C) 73,000 1,2,4-Trimethylbenzene (I) 95636 swpv swpv nc nc nc nc nc NA 1,500 1,500 1.8E+05 8.0E+05 3.7E+05 4.6E+09 8.5E+06 (C) 61,000 1,3,5-Trimethylbenzene (I) 108678 swpv swpv nc nc nc nc nc NA 3.3E+05 6.5E+05 NA NA NA NA 1.0E+08 (D) NA Triphenyl phosphate 115866 swpv swpv max NA 210 1,000 31,000 31,000 31,000 5.7E+06 30,000 1.6E+05 tris(2,3-Dibromopropyl)phosphate 126727 swpv swpv ca ca ca ca ca NA NA NA NA NA NA NA NA NA Urea 57136

27,000 6,700 21,000 NA NA NA 7.7E+06 33,000 NA Vanadium (B) 7440622 swpv swpv nc nc NA 70,000 3.0E+05 4.0E+05 2.6E+06 1.1E+06 1.5E+10 1.0E+08 (C,D) 9.1E+05 Vinyl acetate (I,DD) 108054 20x 20x nc nc nc nc max NA 40 40 4,300 110,000 45,000 6.8E+08 46,000 NA Vinyl chloride (KK,LL,MM) 75014 20x 20x ca ca ca ca ca NA 5,600 5,600 5.8E+05 2.9E+06 1.3E+06 1.7E+10 1.0E+08 (C,D) 87,000 Xylenes (I,J) 1330207 20x 20x nc nc nc nc max 39,000 5.0E+06 5.0E+06 NA NA NA NA 1.0E+08 (D) NA Zinc (B) 7440666 swpv swpv max

238 2017 MR 22 – December 15, 2017

TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

3,900 (S) 3,900 NA 2.0E+05 NA 7,300 NA Acenaphthene 83329 sol nc nc 65 16,000 NA NA NA 7,300 NA Acenaphthylene (CC) 208968 nc nc 190 1.0E+09 1.1E+07 34 (M) NA 310 4.0 Acetaldehyde (I) 75070 nc nc nc NA 1.0E+09 NA NA NA NA NA Acetate 71501

3.6E+06 1.0E+09 1.0E+09 (S) 6.5E+05 3.5E+07 8,700 4.0 Acetic acid (CC) 64197 nc sol nc nc 50,000 (FF) 1.0E+09 1.7E+07 2.6E+05 (EE) 3.7E+07 1.1E+06 (EE) 2.5 Acetone (I,EE,FF) 67641 st st st 2,800 1.0E+09 1.4E+07 620 (M) 4.2E+07 2,100 3.0 Acetonitrile 75058 nc nc nc 8,700 (DD) 6.1E+06 NA 6.2E+05 (DD) 8.4E+05 1.1E+05 (DD) NA Acetophenone (DD) 98862 dev dev dev 0.25 (M) 2.1E+08 5.1E+06 0.046 (M) 7.4E+06 0.70 2.8 Acrolein (I) 107028 nc nc nc NA 3.9E+08 NA NA NA NA NA Acrylamide (MM) 79061

1,400 1.0E+09 1.0E+09 (S) 260 3.5E+07 7.0 2.4 Acrylic acid (DD) 79107 nc sol nc nc 4.6 7.5E+07 4.6E+06 1.2 (M) 3.7E+06 12 3.0 Acrylonitrile (I) 107131 ca ca ca NA 2.4E+05 NA NA NA NA NA Alachlor 15972608

NA 6.0E+06 NA NA NA NA NA Aldicarb 116063

NA 1.0E+07 NA NA NA NA NA Aldicarb sulfone 1646884

NA 2.8E+07 NA NA NA NA NA Aldicarb sulfoxide 1646873

0.61 17 NA 520 NA 0.17 NA Aldrin 309002 ca ca ca 239 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA NA NA NA NA NA NA Aluminum (B,DD) 7429905

1,900 (FF) 4.8E+08 NA NA NA 17,000 (EE) 15 Ammonia (EE,FF) 7664417 st nc 3.9 (M) 1.1E+07 3.4E+05 NA 8.9E+05 2,200 1.1 t-Amyl methyl ether (TAME) (CC) 994058 nc nc NA 3.6E+07 NA NA 6.2E+06 NA 1.3 Aniline 62533

43 (S) 43 NA 1.3E+07 NA 35,000 0.6 Anthracene 120127 sol nc nc NA NA NA NA NA NA NA Antimony 7440360

NA NA NA NA NA NA 5.1 Arsenic (B,KK) 7440382

NA NA NA NA NA NA NA Asbestos (BB) 1332214

NA 35,000 NA NA NA NA NA Atrazine 1912249

1.8 (M) 6,400 NA NA NA 27 NA Azobenzene (CC) 103333 ca ca NA NA NA NA NA NA NA Barium (B,KK) 7440393

1.0 1.8E+06 68,000 1.7 (M) 6.2E+05 110 1.2 Benzene (I,KK) 71432 ca ca ca NA 3.2E+05 NA NA NA NA NA Benzidine (MM) 92875

9.4 (S) 9.4 NA 1.6E+05 (MM) NA 5.8 (MM) NA Benzo(a)anthracene (Q,MM) 56553 sol mut mut NA 1.5 NA NA NA NA NA Benzo(b)fluoranthene (Q,MM) 205992

NA 0.80 NA NA NA NA NA Benzo(k)fluoranthene (Q,MM) 207089

NA 0.26 NA NA NA NA NA Benzo(g,h,i)perylene 191242

240 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 1.6 NA NA NA NA NA Benzo(a)pyrene (Q,DD,MM) 50328

NA 3.4E+06 NA NA NA NA NA Benzoic acid 65850

NA 4.3E+07 NA NA 3.2E+06 NA NA Benzyl alcohol 100516

2.5 (M) 5.3E+05 NA 12 (M) 4.9E+05 17 1.1 Benzyl chloride 100447 ca ca ca NA NA NA NA NA NA NA Beryllium (B) 7440417

NA 1.9E+07 NA NA 1.6E+06 NA NA bis(2-Chloroethoxy)ethane 112265

6.8 1.7E+07 1.7E+07 (S) 3.4 (M) 1.7E+06 2.6 2.7 bis-2-Chloroethylether (I) 111444 ca sol ca ca NA 270 NA NA 65,000 NA 0.3 bis(2-Ethylhexyl) phthalate (DD) 117817

NA NA NA NA NA NA NA Boron (DD) 7440428

NA NA NA NA NA NA NA Bromate 15541454

62 4.5E+05 4.5E+05 (S) 160 2.3E+05 2,100 6.0 Bromobenzene (I) 108861 nc sol nc nc 1.2 3.0E+06 NA 0.61 (M) 3.2E+05 48 NA Bromodichloromethane (DD) 75274 ca ca ca 89 3.1E+06 NA 45 (M) 3.0E+05 770 NA Bromoform 75252 ca ca ca 2.1 (M) 1.5E+07 NA 0.90 (M) NA 350 10 Bromomethane 74839 nc nc nc 98,000 6.3E+07 4.7E+07 20,000 2.5E+06 12,000 1.4 n-Butanol (I) 71363 nc nc nc 2,600 (DD) 2.2E+08 7.1E+06 31,000 (DD) 9.3E+06 1.7E+05 (DD) 1.4 2-Butanone (MEK) (I,DD,KK) 78933 dev dev dev 2,900 8.4E+06 2.8E+06 1,100 5.9E+05 14,000 1.7 n-Butyl acetate 123864 nc nc nc

241 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

230 1.0E+09 7.9E+07 NA NA 2,500 2.4 t-Butyl alcohol (CC) 75650 nc nc NA 2,700 NA NA NA NA NA Butyl benzyl phthalate (DD) 85687

44 12,000 NA 550 36,000 7,000 0.8 n-Butylbenzene 104518 nc nc nc 270 18,000 18,000 (S) 3,800 49,000 14 0.8 sec-Butylbenzene 135988 nc sol nc nc 0.077 (M) 30,000 NA 0.64 (M) 61,000 14 0.7 t-Butylbenzene (I) 98066 nc nc nc NA NA NA NA NA NA NA Cadmium (B,KK) 7440439

3.2 4,600 NA NA NA 2,800 NA Camphene (I,CC) 79925 nc nc NA 7.7E+08 NA NA NA NA 1.4 Caprolactam (DD) 105602

NA 1.1E+05 NA NA NA NA NA Carbaryl (DD) 63252

NA 1,800 NA NA NA NA NA Carbazole 86748

NA 3.2E+05 NA NA NA NA NA Carbofuran (DD) 1563662

92 2.2E+06 27,000 52 (M) 2.9E+05 24,000 1.3 Carbon disulfide (I,R,DD) 75150 nc nc nc 0.41 (M) 7.9E+05 NA 0.31 (M) 1.8E+05 150 NA Carbon tetrachloride (KK) 56235 ca ca ca 18 (EE) 56 NA 13,000 (EE) NA 6.7 (EE) NA Chlordane (J,KK,EE) 57749 st st st NA NA NA NA NA NA NA Chloride 16887006

NA 8.2E+06 NA NA 2.1E+06 NA NA 2-Chloroaniline 95512

NA 3.9E+06 NA NA NA NA NA 4-Chloroaniline 106478

242 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

33 5.0E+05 1.9E+05 82 2.6E+05 1,700 1.3 Chlorobenzene (I,KK) 108907 nc nc nc NA 3.1E+08 NA NA NA NA NA p-Chlorobenzene sulfonic acid 98668

2,800 1.4E+06 NA 2,400 NA 1.7E+06 6.0 1-Chloro-1,1-difluoroethane 75683 nc nc nc 620 6.7E+06 88,000 330 NA 1.4E+05 3.8 Chloroethane (DD) 75003 nc nc nc NA 4.3E+05 NA NA 44,000 NA NA 2-Chloroethyl vinyl ether 110758

0.49 (M) 8.0E+06 NA 0.26 (M) 8.8E+05 37 NA Chloroform (KK) 67663 ca ca ca 15 5.3E+06 NA 6.9 (M) NA 3,100 8.1 Chloromethane (I) 74873 nc nc nc NA 3.8E+06 NA NA NA NA NA 4-Chloro-3-methylphenol (DD) 59507

NA 12,000 NA NA NA NA NA beta-Chloronaphthalene 91587

45 (DD) 1.1E+07 NA 12,000 (DD) 7.3E+06 600 (DD) NA 2-Chlorophenol (DD) 95578 dev dev dev 50 3.7E+05 1.4E+05 200 3.0E+05 2,800 1.0 o-Chlorotoluene (I) 95498 nc nc nc NA 1,100 NA NA NA NA NA Chlorpyrifos (DD) 2921882

NA NA NA NA NA NA NA Chromium (III) (B,H,KK) 16065831

NA NA NA NA NA NA NA Chromium (VI) (H,KK,MM) 18540299

NA 2.0 NA NA NA NA NA Chrysene (Q,MM) 218019

NA NA NA NA NA NA NA Cobalt (B) 7440484

NA NA NA NA NA NA NA Copper (B) 7440508

243 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 1.7E+05 NA NA NA NA NA Cyanazine 21725462

9.0 1.0E+09 4.6E+06 1.8 (M) 3.9E+07 28 6.0 Cyanide (P,R,DD) Varies nc nc nc 290 55,000 2,900 320 (M) 50,000 2.1E+05 1.3 Cyclohexane (DD) 110827 nc nc nc 2,300 2.5E+07 2.5E+07 (S) NA 1.7E+06 24,000 1.1 Cyclohexanone (CC) 108941 nc sol nc NA 500 NA NA NA NA NA Dacthal 1861321

NA 5.0E+08 NA NA 2.0E+07 NA NA Dalapon 75990

NA 90 NA NA NA NA NA 4-4`-DDD 72548

32 40 NA 39,000 NA 8.7 NA 4-4`-DDE 72559 ca ca ca NA 5.5 NA NA NA NA NA 4-4`-DDT (DD) 50293

NA 0.10 NA NA NA NA NA Decabromodiphenyl ether (DD) 1163195

NA 11,000 NA NA 26,000 NA 0.5 Di-n-butyl phthalate (DD) 84742

NA 780 NA NA 56,000 NA 0.4 Di(2-ethylhexyl) adipate (DD) 103231

22 (S) 22 NA NA NA 16,000 NA Di-n-octyl phthalate (CC) 117840 sol nc 2.9E+07 1.0E+09 1.0E+09 (S) 5.2E+06 3.5E+07 83,000 1.8 Diacetone alcohol (I) 123422 nc sol nc nc NA 40,000 NA NA NA NA NA Diazinon 333415

NA 2.5 NA NA NA NA NA Dibenzo(a,h)anthracene (Q,MM) 53703

3,100 (S) 3,100 NA 7.1E+06 NA 140 NA Dibenzofuran 132649 sol nc nc

244 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

0.78 (M,MM) 2.7E+06 NA 0.40 (M,MM) 2.7E+05 14 (MM) NA Dibromochloromethane (MM) 124481 mut mut mut 0.00045 (M,MM) 1.2E+06 NA NA 3.3E+05 0.062 (MM) NA Dibromochloropropane (MM,CC) 96128 mut mut 8.8 1.2E+07 NA 3.5 (M) 9.4E+05 140 NA Dibromomethane 74953 nc nc nc NA 8.3E+06 NA NA NA NA NA Dicamba (DD) 1918009

370 1.6E+05 NA 1,500 1.3E+05 10,000 2.2 1,2-Dichlorobenzene 95501 nc nc nc 2.6 1.3E+05 NA 10 (M) 99,000 100 NA 1,3-Dichlorobenzene 541731 nc nc nc 5.9 81,000 NA 23 (M) NA 220 2.5 1,4-Dichlorobenzene (KK) 106467 ca ca ca NA 3,100 NA NA NA NA NA 3,3`-Dichlorobenzidine 91941

13 2.8E+05 NA 12 (M) NA 11,000 NA Dichlorodifluoromethane 75718 nc nc nc 4.7 5.0E+06 3.8E+05 2.6 (M) 6.0E+05 530 5.4 1,1-Dichloroethane 75343 ca ca ca 1.4 8.6E+06 2.1E+06 0.82 (M) 1.0E+06 33 6.2 1,2-Dichloroethane (I,KK) 107062 ca ca ca 18 2.4E+06 97,000 12 (M) 4.8E+05 7,000 6.5 1,1-Dichloroethylene (I,KK) 75354 nc nc nc 3.4 6.4E+06 2.9E+05 2.1 (M) 8.2E+05 280 3.0 cis-1,2-Dichloroethylene 156592 nc nc nc 27 (FF) 4.5E+06 2.5E+05 39 (M, EE) 7.9E+05 9,000 (EE) 6.0 trans-1,2-Dichloroethylene (EE,FF) 156605 st nc nc NA 7,000 NA NA NA NA NA 2,6-Dichloro-4-nitroaniline 99309

NA 5.6E+06 NA NA NA NA NA 2,4-Dichlorophenol (DD) 120832

NA 6.8E+05 NA NA NA NA NA 2,4-Dichlorophenoxyacetic acid (KK) 94757

245 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

2.6 2.8E+06 5.4E+05 2.1 (M) 4.6E+05 140 3.4 1,2-Dichloropropane (I) 78875 nc nc nc 3.3 2.8E+06 6.6E+05 3.1 (M) 5.3E+05 210 5.3 1,3-Dichloropropene (J) 542756 ca ca ca NA 8.0E+06 NA NA 1.1E+06 NA NA Dichlorvos (MM) 62737

NA 4,000 NA NA NA NA NA Dicyclohexyl phthalate 84617

3.7 200 NA 770 NA 0.18 NA Dieldrin 60571 ca ca ca 1,200 6.0E+07 4.6E+05 350 3.4E+06 35,000 1.9 Diethyl ether 60297 nc nc nc NA 1.1E+06 NA NA 2.6E+05 NA 0.7 Diethyl phthalate 84662

NA 1.0E+09 NA NA 5.3E+07 NA 0.8 Diethylene glycol monobutyl ether 112345

36 (DD) 8.8E+06 2.2E+05 190 (M,DD) 7.8E+05 23,000 (DD) 1.4 Diisopropyl ether (DD) 108203 dev dev dev 3,500 1.1E+08 4.6E+06 2,900 1.8E+07 7,000 1.1 Diisopropylamine (I) 108189 nc nc nc NA 4.0E+06 NA NA 3.8E+05 NA 0.9 Dimethyl phthalate 131113

1.9+07 1.0E+09 NA 3.8E+06 3.9E+07 3,500 1.8 N,N-Dimethylacetamide 127195 nc nc nc 1.1 (M) 1.5E+06 NA NA 2.8E+05 71 NA N,N-Dimethylaniline (CC) 121697 ca ca 2,700 1.0E+09 1.0E+09 (S) NA 3.5E+07 240 2.2 Dimethylformamide (I,CC) 68122 nc sol nc NA 7.9E+06 NA NA NA NA 1.1 2,4-Dimethylphenol 105679

NA 6.1E+06 NA NA NA NA NA 2,6-Dimethylphenol 576261

NA 4.8E+06 NA NA NA NA NA 3,4-Dimethylphenol 95658

246 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 1.0E+09 NA NA 3.7E+07 NA 2.6 Dimethylsulfoxide 67685

NA 2.8E+06 NA NA NA NA NA 2,4-Dinitrophenol 51285

NA 2.0E+05 NA NA NA NA NA 2,4-Dinitrotoluene (KK) 121142

NA 52,000 NA NA NA NA NA Dinoseb (DD) 88857

1,900 1.0E+09 1.5E+08 360 (M) 3.8E+07 170 2.0 1,4-Dioxane (I) 123911 ca ca ca NA 7.1E+08 NA NA NA NA NA Diquat 85007

NA 42,000 NA NA NA NA NA Diuron 330541

NA 330 NA NA NA NA NA Endosulfan (J) 115297

NA 1.0E+08 NA NA NA NA NA Endothall 145733

NA 250 NA NA NA NA NA Endrin (KK) 72208

0.99 (M) 6.6E+07 4.8E+07 NA 3.5E+06 35 3.8 Epichlorohydrin (I,OOCC) 106898 nc nc 1.0E+05 (FF) 1.0E+09 1.2E+08 1.3E+06 (EE) 3.5E+07 6.3E+05 (EE) 3.3 Ethanol (I,DD,EE,FF) 64175 st st st 910 8.0E+07 5.3E+06 210 3.5E+06 2,400 2.0 Ethyl acetate (I) 141786 nc nc nc 22 1.2E+07 3.1E+05 NA 9.7E+05 13,000 1.2 Ethyl-tert-butyl ether (ETBE) (CC) 637923 nc nc 2.8 1.7E+05 43,000 12 (M) 1.6E+05 340 0.8 Ethylbenzene (I) 100414 ca ca ca 0.13 3.9E+06 NA 0.074 (M) 4.5E+05 1.4 NA Ethylene dibromide 106934 ca ca ca NA 1.0E+09 NA NA 3.5E+07 NA 3.2 Ethylene glycol (DD) 107211

247 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 1.0E+09 NA NA 3.8E+07 NA 4.0 Ethylene glycol monobutyl ether 111762

Ethylenediaminetetraacetic acid (EDTA) NA 1.0E+06 NA NA NA NA NA 60004 (II) NA 260 NA NA NA NA NA Fluoranthene 206440

1,700 (S) 1,700 NA 4.7E+05 NA 4,900 NA Fluorene 86737 sol nc nc NA 1,700 NA NA NA NA NA Fluorine (soluble fluoride) (DD) 7782414

3,000 (MM) 4.0E+08 NA 530 (M,MM) NA 27 (MM) 7.0 Formaldehyde (MM) 50000 mut mut mut 2,500 1.0E+09 1.0E+09 (S) 440 (M) 3.5E+07 10 18 Formic acid (I,U) 64186 nc sol nc nc NA 9.6E+07 NA NA 3.9E+06 NA NA 1-Formylpiperidine (DD) 2591868

NA 4.0E+06 NA NA NA NA NA Gentian violet 548629

NA 1.1E+07 NA NA NA NA NA Glyphosate (DD) 1071836

0.25 180 NA 3,600 NA 0.65 NA Heptachlor (DD,KK) 76448 ca ca ca 0.014 200 NA NA NA 0.33 NA Heptachlor epoxide (KK,CC) 1024573 ca ca 150 3,400 210 130 29,000 1.2E+05 1.1 n-Heptane 142825 nc nc nc NA 0.16 NA NA NA NA NA Hexabromobenzene 87821

0.11 (M) 6.2 NA 6.7 (M) NA 1.2 NA Hexachlorobenzene (C-66) (KK) 118741 nc nc nc 0.32 3,200 NA 2.5 (M) 5,600 39 NA Hexachlorobutadiene (C-46) (KK) 87683 ca ca ca NA 2,000 NA NA NA NA NA alpha-Hexachlorocyclohexane 319846

248 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 240 NA NA NA NA NA beta-Hexachlorocyclohexane 319857

0.030 (M) 1,800 NA 0.32 (M) 5,300 7.0 NA Hexachlorocyclopentadiene (C-56) 77474 nc nc nc 1.5 (M) 50,000 NA 3.2 (M) NA 85 NA Hexachloroethane (KK) 67721 ca ca ca 29 9,500 210 25 70,000 24,000 1.1 n-Hexane 110543 nc nc nc 660 1.7E+07 4.3E+06 210 (M) 1.1E+06 1,000 1.0 2-Hexanone 591786 nc nc nc NA 0.19 NA NA NA NA NA Indeno(1,2,3-cd)pyrene (Q,MM) 193395

NA NA NA NA NA NA NA Iron (B) 7439896

4.0E+05 8.5E+07 5.2E+07 79,000 3.3E+06 52,000 1.7 Isobutyl alcohol (I) 78831 nc nc nc NA 1.2E+07 NA NA 2.0E+06 NA 0.8 Isophorone (DD) 78591

53,000 1.0E+09 5.9E+07 9,800 3.6E+07 7,000 2.0 Isopropyl alcohol (I,DD) 67630 nc nc nc 0.60 (M) 61,000 38,000 3.8 (M)ca 90,000 81 0.9 Isopropyl benzene 98828 ca ca NA NA NA NA NA NA NA Lead (B,L, DD,KK) 7439921

NA 7,300 NA NA NA NA NA Lindane (KK) 58899

NA NA NA NA NA NA NA Lithium (B,DD) 7439932

NA NA NA NA NA NA NA Magnesium 7439954

NA NA NA NA NA NA NA Manganese (B) 7439965

0.088 60 NA 0.027 nc NA 10 NA Mercury (Total) (Z,DD,KK) Varies nc nc

249 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

(AA) NA 10,000 (AA) NA NA 8.4E+06 (GG) 5.0 Methane (K) 74828

1.2E+05 (DD) 1.0E+09 1.7E+08 1.4E+06 (DD) 3.5E+07 6.7E+05 (DD) 6.0 Methanol (DD) 67561 dev dev dev NA 100 NA NA NA NA NA Methoxychlor (DD,KK) 72435

8,400 1.0E+09 1.0E+09 (S) 1,500 3.5E+07 38 1.8 2-Methoxyethanol (I,DD) 109864 nc sol nc nc NA 6.3E+05 NA NA NA NA NA 2-Methyl-4-chlorophenoxyacetic acid 94746

NA 2.0E+05 NA NA NA NA NA 2-Methyl-4,6-dinitrophenol 534521

NA 1.0E+09 NA NA 4.7E+07 NA NA N-Methyl-morpholine (I) 109024

NA 38,000 NA NA NA NA NA Methyl parathion 298000

720 (DD) 1.9E+07 3.5E+06 12,000 (DD) 1.1E+06 1.0E+05 (DD) 1.2 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 dev dev dev 250 5.1E+07 9.6E+05 74 (M) 3.0E+06 3,300 1.6 Methyl-tert-butyl ether (MTBE) 1634044 ca ca ca NA 5.6E+06 NA NA 1.1E+06 NA NA N-methylaniline 100618

30 (M) 42,000 930 29 (M) 72,000 24,000 1.0 Methylcyclopentane (I) 96377 nc nc nc 4,4`-Methylene-bis-2- chloroaniline NA 14,000 NA NA NA NA NA 101144 (MBOCA) (MM) 79 (FF) 1.3E+07 NA 130 1.2E+06 21,000 13 Methylene chloride (MM,FF) 75092 st nc nc 66 25,000 NA 1,700 NA 350 NA 2-Methylnaphthalene 91576 nc nc nc NA 2.2E+07 NA NA NA NA 1.1 Methylphenols (JJ,KK) 1319773

NA 2.6E+07 NA NA NA NA 1.4 2-Methylphenol (DD,KK) 95487

250 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 5.3E+05 NA NA 5.4E+05 NA NA Metolachlor 51218452

NA 1.1E+06 NA NA NA NA NA Metribuzin 21087649

NA 85 NA NA NA NA NA Mirex 2385855

NA NA NA NA NA NA NA Molybdenum 7439987

4.2 (M) 31,000 NA 67 (M) NA 25 0.9 Naphthalene 91203 ca ca ca NA NA NA NA NA NA NA Nickel (B) 7440020

NA NA NA NA NA NA NA Nitrate (N,DD) 14797558

NA NA NA NA NA NA NA Nitrite (N,DD) 14797650

68 2.1E+06 NA 170 (M) 1.0E+06 21 1.8 Nitrobenzene (I,KK) 98953 ca ca ca 0.12 (M,CC) 2.5E+06 NA NA NA 1.7 NA 2-Nitrophenol (CC) 88755 nc nc NA 1.3E+07 NA NA 7.6E+06 NA NA n-Nitroso-di-n-propylamine 621647

NA 35,000 NA NA NA NA NA N-Nitrosodiphenylamine 86306

NA 2.8E+08 NA NA NA NA NA Oxamyl 23135220

NA NA NA NA NA NA NA Oxo-hexyl acetate 88230357

NA 330 NA NA NA NA NA Pendimethalin (DD) 40487421

0.0086 (M) 830 NA NA NA 3.5 NA Pentachlorobenzene (CC) 608935 nc nc 8.5 (M) 440 NA NA NA 380 NA Pentachloronitrobenzene (CC) 82688 nc nc

251 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 14,000 NA NA NA NA NA Pentachlorophenol (KK) 87865

40 (M) 38,000 320 36 (M) 1.9E+05 35,000 1.4 Pentane 109660 nc nc nc NA 2.0E+05 NA NA 2.3E+05 NA NA 2-Pentene (I) 109682

NA NA NA NA NA NA NA Perchlorate (DD) 14797730

NA 9.5E+06 NA NA NA NA NA Perfluorooctanoic acid 335671

NA 3.1 NA NA NA NA NA Perfluorooctane sulfonic acid (DD) 1763231

0.077 (M) 1,200 NA NA NA 3.5 NA Phenanthrene (CC) 85018 nc nc NA 8.3E+07 NA NA NA NA 1.8 Phenol (DD) 108952

NA 32,000 NA NA NA NA NA Phenytoin (DD) 57410

NA 3,300 NA NA NA NA NA Phosphorus, White (R,DD) 7723140

NA 7.0E+06 NA NA NA NA NA o-Phthalic acid 88993

NA 6.2E+06 NA NA NA NA 1.7 Phthalic anhydride 85449

NA 4.3E+05 NA NA NA NA NA Picloram 1918021

45,000 1.0E+09 NA NA 1.4E+08 2.4E+05 NA Piperidine (OOCC) 110894 nc nc NA 11 NA NA NA NA NA Polybrominated biphenyls (J,DD) 67774327

Polychlorinated biphenyls (PCBs) 0.031 (M) 700 NA NA NA 8.5 NA 1336363 (J,T,CC,DD) ca ca Polychlorinated biphenyls (PCBs) (O) (O) (O) (O) (O) (O) NA varies congeners (O)

252 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 7.5E+05 NA NA NA NA NA Prometon 1610180

NA 5.8E+05 NA NA NA NA NA Propachlor 1918167

NA 8,600 NA NA NA NA NA Propazine 139402

1.2E+06 1.0E+09 1.0E+09 (S) 2.2E+05 3.5E+07 10,000 2.9 Propionic acid 79094 nc sol nc nc 2,700 (DD) 1.0E+09 7.1E+07 40,000 (DD) 3.6E+07 24,000 (DD) 2.2 Propyl alcohol (I,DD) 71238 dev dev dev 43 (DD) 52,000 37,000 1,800 (DD) 89,000 33,300 (DD) 0.8 n-Propylbenzene (I,DD) 103651 dev dev dev NA 1.0E+09 NA NA 3.5E+07 NA 2.6 Propylene glycol 57556

140 (S) 140 NA 2.5E+07 NA 3,500 NA Pyrene 129000 sol nc nc 600 1.0E+09 5.2E+07 540 1.8E+08 120 1.8 Pyridine (I,KK) 110861 nc nc nc NA NA NA NA NA NA NA Selenium (B,KK) 7782492

NA NA NA NA NA NA NA Silver (KK) 7440224

NA 71,000 NA NA NA NA NA Silvex (2,4,5-TP) (KK) 93721

NA 6,200 NA NA NA NA NA Simazine 122349

NA NA NA NA NA NA NA Sodium 17341252

NA NA NA NA NA NA NA Sodium azide 26628228

NA 9.5E+08 NA NA NA NA NA Sodium bromide 7647156

NA NA NA NA NA NA NA Strontium (B,DD) 7440246

253 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

33 3.1E+05 1.4E+05 150 2.9E+05 1,500 0.9 Styrene 100425 ca ca ca NA NA NA NA NA NA NA Sulfate 14808798

NA 1.0E+09 NA NA NA NA NA Sulfolane 126330

NA 2.5E+06 NA NA NA NA NA Tebuthiuron (DD) 34014181

NA 1.0E-02 NA NA NA NA NA 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416

3.1 600 NA 70 (M) NA 35 NA 1,2,4,5-Tetrachlorobenzene (DD) 95943 nc nc nc 2,3,7,8-Tetrachlorodibenzo-p-dioxin 3.8E-07 (M,O) 0.20 NA NA NA 1.9E-05 NA 1746016 (O,CC,DD) ca ca 3.1 1.1E+06 NA 3.2 (M) 2.3E+05 110 NA 1,1,1,2-Tetrachloroethane 630206 ca ca ca 2.4 2.8E+06 NA 2.7 (M) 6.3E+05 15 NA 1,1,2,2-Tetrachloroethane 79345 ca ca ca 1.5 (FF) 2.1E+05 NA 6.2 (M, EE) 60,000 1,400 (EE) NA Tetrachloroethylene (KK,EE,FF) 127184 st st st 45,000 1.0E+09 8.2E+06 13,000 5.4E+07 70,000 2.0 Tetrahydrofuran (DD) 109999 nc nc nc 2,700 1.0E+09 NA NA 4.0E+07 28 NA 1,1,3,3-Tetramethylurea (CC) 632224 nc nc 0.00027 (M) 9.0E+05 NA NA 8.0E+05 0.056 NA Tetranitromethane (CC) 509148 ca ca NA NA NA NA NA NA NA Thallium 7440280

300 (FF) 5.3E+05 61,000 3,700 (EE) 2.8E+05 1.7E+05 (EE) 1.1 Toluene (I,EE,FF) 108883 st nc nc NA 6.5E+06 NA NA NA NA 1.1 p-Toluidine 106490

NA 550 NA NA NA NA NA Toxaphene (KK) 8001352

254 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

530 (DD) 4,000 NA NA NA 6,700 (DD) NA Triallate (CC,DD) 2303175 dev dev 170 1.4E+05 NA 3,300 5.3E+05 240 1.4 Tributylamine 102829 nc nc nc 58 18,000 NA 830 NA 940 NA 1,2,3-Trichlorobenzene 87616 nc nc nc 3.8 (M) 49,000 NA 53 (M) 1.3E+05 70 2.5 1,2,4-Trichlorobenzene 120821 nc nc nc 180 (FF) 1.3E+06 NA 450 (EE) 2.4E+05 1.7E+05 (EE) 8.0 1,1,1-Trichloroethane (EE,FF) 71556 st st st 0.00047 (M) 4.6E+06 3.9E+06 0.00037 (M) 7.2E+05 0.0070 6.0 1,1,2-Trichloroethane 79005 nc nc nc 0.073 (M,DD) 1.3E+06 NA 0.33 (M,DD) 2.5E+05 67 (DD) 8.0 Trichloroethylene (G,DD,KK,MM) 79016 dev dev dev 22 1.1E+06 NA 19 (M) 5.5E+05 15,000 NA Trichlorofluoromethane 75694 nc nc nc NA 1.2E+06 NA NA NA NA NA 2,4,5-Trichlorophenol (KK) 95954

NA 8.0E+05 NA NA NA NA NA 2,4,6-Trichlorophenol (DD,KK) 88062

1.9 1.8E+06 NA 2.6 (M) 4.6E+05 10 3.2 1,2,3-Trichloropropane (MM) 96184 nc nc nc 840 1.7E+05 NA 860 2.8E+05 6.6E+05 NA 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 nc nc nc NA 1.0E+09 NA NA 5.3E+07 NA 1.0 Triethanolamine 102716

NA 1.0E+09 NA NA 5.3E+07 NA 0.9 Triethylene glycol (DD) 112276

NA 5.0E+06 NA NA NA NA NA 3-Trifluoromethyl-4-nitrophenol (DD) 88302

180 (S) 180 NA NA NA 1.0E+05 NA Trifluralin (CC) 1582098 sol nc 160 2,400 170 130 (M) 30,000 1.2E+05 1.1 2,2,4-Trimethyl pentane 540841 nc nc nc

255 2017 MR 22 – December 15, 2017 TABLE 4. VI TIER 1 GROUNDWATER, SOIL AND VAPOR SCREENING LEVELS PART 201 GENERIC SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS The VI Tier 1 screening levels serve as the basis for the development of VI Tier 2 generic residential and VI Tier 3A generic restricted categorical criteria. A person may elect to use the VI Tier 1 screening levels as the generic residential clean‐up criteria. All soil and groundwater values, unless otherwise noted, are expressed in units of parts per billion (ppb). All vapor values, unless otherwise noted, are expressed in micrograms per meter cubed (µg/m3). One ppb is equivalent to 1 µg per liter (µg/L) for groundwater and 1 µg per kilogram (µg/kg) for soil. For vapor 1 µg/m3 is not equal to 1 part per billion by volume (ppbv). The lower explosive limit is expressed as % by volume in air. Some screening levels are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by one or more letters in parentheses and is defined in R 299.49(1). The abbreviation beneath the value represents the basis for the screening level. When the health‐based value is less than the target detection limit (TDL), the TDL is the criterion (MCL 324.20120a(10)). Groundwater Water Solubility Flammability and Soil Soil Saturation Vapor Chemical Screening Levels Explosivity Screening Concentration Screening Lower Explosive Hazardous Substance Abstract Service Screening Level Screening Levels Level (X) Number Levels Levels

NA 13,000 NA NA 52,000 NA NA 2,4,4-Trimethyl-2-pentene (I) 107404

43 75,000 75,000 (S) 270 98,000 2,100 0.8 1,2,3-Trimethylbenzene (I) 526738 nc sol nc nc 25 57,000 57,000 (S) 150 73,000 2,100 0.9 1,2,4-Trimethylbenzene (I) 95636 nc sol nc nc 18 48,000 48,000 (S) 100 61,000 2,100 1.0 1,3,5-Trimethylbenzene (I) 108678 nc sol nc nc NA 1,900 NA NA NA NA NA Triphenyl phosphate 115866

0.074 (M) 8,000 NA NA 1.6E+05 1.6 NA tris(2,3-Dibromopropyl)phosphate (CC) 126727 ca ca NA 5.5E+08 NA NA NA NA NA Urea 57136

NA NA NA NA NA NA NA Vanadium (B) 7440622

690 2.0E+07 1.8E+06 160 (M) 9.1E+05 7,000 2.6 Vinyl acetate (I,DD) 108054 nc nc nc 0.12 (M,MM) 8.8E+06 32,000 0.082 (M,MM) NA 54 (MM) 3.6 Vinyl chloride (KK,LL,MM) 75014 mut mut mut 75 1.1E+05 58,000 280 87,000 7,600 0.9 Xylenes (I,J) 1330207 nc nc nc NA NA NA NA NA NA NA Zinc (B) 7440666

256 2017 MR 22 – December 15, 2017 TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Chemica Residential Groundwater Soil Source Finite l Statewide Drinking Surface Water Volatilization Volatile Soil Finite VSIC VSIC for 2 Particulate Soil Saturation Abstract Default Water Interface to Indoor Air Inhalation for 5 Meter Meter Soil Direct Concentration Hazardous Service Backgrou Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Substance Number nd Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels Acenaphthene 83329 NA 3.0E+5 8,700 1.9E+8 8.1E+7 8.1E+7 8.1E+7 1.4E+10 4.1E+7 NA Acenaphthylene 208968 NA 5,900 ID 1.6E+6 2.2E+6 2.2E+6 2.2E+6 2.3E+9 1.6E+6 NA Acetaldehyde (I) 75070 NA 19,000 2,600 2.2E+5 1.7E+5 1.7E+5 2.8E+5 6.0E+8 2.9E+7 1.1E+8 Acetate 71501 NA ID (G) ID ID ID ID ID ID ID Acetic acid 64197 NA 84,000 (G) NLV NLV NLV NLV 1.7E+10 1.3E+8 6.5E+8 Acetone (I) 67641 NA 15,000 34,000 2.9E+8 (C) 1.3E+8 1.3E+8 1.9E+8 3.9E+11 2.3E+7 1.1E+8 Acetonitrile 75058 NA 2,800 NA 4.8E+6 1.6E+6 1.6E+6 2.1E+6 4.0E+9 4.3E+6 2.2E+7 Acetophenone 98862 NA 30,000 ID 1.2E+8 (C) 4.4E+7 4.4E+7 4.4E+7 3.3E+10 4.7E+7 (C) 1.1E+6 Acrolein (I) 107028 NA 2,400 NA 410 310 310 610 1.3E+6 3.6E+6 2.3E+7 Acrylamide 79061 NA 10 200 (X) NLV NLV NLV NLV 2.4E+6 1,900 NA Acrylic acid 79107 NA 78,000 NA 2.4E+6 1.9E+5 2.3E+5 2.3E+5 6.7E+7 3.5E+7 (DD) 1.1E+8 100 (M); Acrylonitrile (I) 107131 NA 52 100 (M); 40 6,600 5,000 5,100 10,000 4.6E+7 16,000 8.3E+6 1597260 Alachlor 8 NA 52 290 (X) NLV NLV NLV NLV ID 93,000 NA Aldicarb 116063 NA 60 NA NLV NLV NLV NLV ID 2.3E+5 NA 200 (M); Aldicarb sulfone 1646884 NA 40 NA NLV NLV NLV NLV ID 2.5E+5 NA Aldicarb sulfoxide 1646873 NA 200(M); 80 NA NLV NLV NLV NLV ID 2.9E+5 NA Aldrin 309002 NA NLL NLL 1.3E+6 58,000 58,000 58,000 6.4E+5 1,000 NA Aluminum (B) 7429905 6.9E+6 1,000 NA NLV NLV NLV NLV ID 5.0E+7 (DD) NA Ammonia 7664417 NA ID (CC) ID ID ID ID 6.7E+9 ID 1.0E+7 t-Amyl methyl ether (TAME) 994058 NA 3,900 NA 58,000 3.4E+5 7.6E+5 1.8E+6 4.1E+9 2.9E+7 (C) 4.4E+5 Aniline 62533 NA 1,100 330 (M); 80 NLV NLV NLV NLV 6.7E+7 3.3E+5 4.5E+6 Anthracene 120127 NA 41,000 ID 1.0E+9 (D) 1.4E+9 1.4E+9 1.4E+9 6.7E+10 2.3E+8 NA Antimony 7440360 NA 4,300 94,000 (X) NLV NLV NLV NLV 1.3E+7 1.8E+5 NA Arsenic 7440382 5,800 4,600 4,600 NLV NLV NLV NLV 7.2E+5 7,600 NA

257 2017 MR 22 – December 15, 2017 1.0E+7 (M); Asbestos (BB) 1332214 NA NLL NLL NLV NLV NLV NLV 68,000 ID NA Atrazine 1912249 NA 60 150 NLV NLV NLV NLV ID 71,000 (DD) NA Azobenzene 103333 NA 4,200 ID 6.1E+6 6.3E+5 6.3E+5 6.3E+5 1.0E+8 1.4E+5 NA

258 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Surface Soil Source Soil Chemical Statewide Drinking Water Volatilization Volatile Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Water Interface to Indoor Air Inhalation for 5 Meter for 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels Barium (B) 7440393 75,000 1.3E+6 (G) NLV NLV NLV NLV 3.3E+8 3.7E+7 NA Benzene (I) 71432 NA 100 4,000 (X) 1,600 13,000 34,000 79,000 3.8E+8 1.8E+5 4.0E+5 1,000 (M); 1,000 (M); Benzidine 92875 NA 6.0 6.0 NLV NLV NLV NLV 46,000 1,000 (M); 23 NA Benzo(a)anthracene (Q) 56553 NA NLL NLL NLV NLV NLV NLV ID 20,000 NA Benzo(b)fluoranthene (Q) 205992 NA NLL NLL ID ID ID ID ID 20,000 NA Benzo(k)fluoranthene (Q) 207089 NA NLL NLL NLV NLV NLV NLV ID 2.0E+5 NA Benzo(g,h,i)perylene 191242 NA NLL NLL NLV NLV NLV NLV 8.0E+8 2.5E+6 NA Benzo(a)pyrene (Q) 50328 NA NLL NLL NLV NLV NLV NLV 1.5E+6 2,000 NA Benzoic acid 65850 NA 6.4E+5 NA NLV NLV NLV NLV ID 9.9E+8 NA Benzyl alcohol 100516 NA 2.0E+5 NA NLV NLV NLV NLV 3.3E+11 3.2E+8 (C) 5.8E+6 Benzyl chloride 100447 NA 150 NA 6,300 14,000 14,000 17,000 6.2E+7 48,000 2.3E+5 Beryllium 7440417 NA 51,000 (G) NLV NLV NLV NLV 1.3E+6 4.1E+5 NA bis(2- Chloroethoxy)ethane 112265 NA ID ID NLV NLV NLV NLV ID ID 2.7E+6 bis(2-Chloroethyl)ether (I) 111444 NA 100 100 (M); 20 8,300 3,800 3,800 3,800 9.4E+6 13,000 2.2E+6 bis(2- Ethylhexyl)phthalate 117817 NA NLL NLL NLV NLV NLV NLV 7.0E+8 2.8E+6 1.0E+7 Boron (B) 7440428 NA 10,000 1.4E+5 (X) NLV NLV NLV NLV ID 4.8E+7 (DD) NA Bromate 15541454 NA 200 800 (X) NLV NLV NLV NLV ID 17,000 NA Bromobenzene (I) 108861 NA 550 NA 3.1E+5 4.5E+5 4.5E+5 4.5E+5 5.3E+8 5.4E+5 7.6E+5 Bromodichloromethane 75274 NA 1,600 (W) ID 1,200 9,100 9,700 19,000 8.4E+7 1.1E+5 1.5E+6 Bromoform 75252 NA 1,600 (W) ID 1.5E+5 9.0E+5 9.0E+5 9.0E+5 2.8E+9 8.2E+5 8.7E+5 Bromomethane 74839 NA 200 700 860 11,000 57,000 1.4E+5 3.3E+8 3.2E+5 2.2E+6 n-Butanol (I) 71363 NA 19,000 2.0E+5 NLV NLV NLV NLV 2.3E+10 2.9E+7 (C) 8.7E+6

259 2017 MR 22 – December 15, 2017 1.2E+8 (C, 2-Butanone (MEK) (I) 78933 NA 2.6E+5 44,000 5.4E+7 (C) 2.9E+7 2.9E+7 3.5E+7 6.7E+10 DD) 2.7E+7 n-Butyl acetate 123864 NA 11,000 NA 5.6E+7 (C) 1.1E+8 2.6E+8 3.2E+8 4.7E+11 1.7E+7 (C) 1.1E+6 t-Butyl alcohol 75650 NA 78,000 NA 3.1E+8 (C) 9.7E+7 2.0E+8 2.0E+8 1.3E+11 1.2E+8 (C) 1.1E+8 Butyl benzyl phthalate 85687 NA 2.2E+6 (C) 1.2E+5 (X) NLV NLV NLV NLV 4.7E+10 3.6E+7 (C) 3.1E+5 n-Butylbenzene 104518 NA 1,600 ID ID ID ID ID 2.0E+9 2.5E+6 1.0E+7

260 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Surface Soil Source Soil Chemical Statewide Drinking Water Volatilization Volatile Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Water Interface to Indoor Air Inhalation for 5 Meter for 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels sec-Butylbenzene 135988 NA 1,600 ID ID ID ID ID 4.0E+8 2.5E+6 1.0E+7 t-Butylbenzene (I) 98066 NA 1,600 ID ID ID ID ID 6.7E+8 2.5E+6 1.0E+7 Cadmium (B) 7440439 1,200 6,000 (G,X) NLV NLV NLV NLV 1.7E+6 5.5E+5 NA Camphene (I) 79925 NA ID NA 3,700 1.5E+5 9.1E+5 2.2E+6 5.3E+9 ID NA Caprolactam 105602 NA 1.2E+5 NA NLV NLV NLV NLV 6.7E+8 5.3E+7 (DD) NA Carbaryl 63252 NA 14,000 NA ID ID ID ID ID 2.2E+7 NA Carbazole 86748 NA 9,400 1,100 NLV NLV NLV NLV 6.2E+7 5.3E+5 NA Carbofuran 1563662 NA 800 NA NLV NLV NLV NLV ID 1.1E+6 NA Carbon disulfide 7.2E+6 (C, (I,R) 75150 NA 16,000 ID 76,000 1.3E+6 7.9E+6 1.9E+7 4.7E+10 DD) 2.8E+5 Carbon tetrachloride 56235 NA 100 900 (X) 190 3,500 12,000 28,000 1.3E+8 96,000 3.9E+5 Chlordane (J) 57749 NA NLL NLL 1.1E+7 1.2E+6 1.2E+6 1.2E+6 3.1E+7 31,000 NA Chloride 16887006 NA 5.0E+6 (X) NLV NLV NLV NLV ID 5.0E+5 (F) NA Chlorobenzene (I) 108907 NA 2,000 500 1.2E+5 7.7E+5 9.9E+5 2.1E+6 4.7E+9 4.3E+6 (C) 2.6E+5 p-Chlorobenzene sulfonic acid 98668 NA 1.5E+5 ID ID ID ID ID ID 2.3E+8 ID 1-Chloro-1,1- difluoroethane 75683 NA 3.0E+5 NA 2.9E+6 (C) 7.9E+7 5.6E+8 1.4E+9 3.3E+12 4.7E+8 (C) 9.6E+5 Chloroethane 75003 NA 8,600 22,000 (X) 2.9E+6 (C) 3.00E+07 1.2E+8 2.8E+8 6.7E+11 2.6E+6 (C) 9.5E+5 2-Chloroethyl vinyl ether 110758 NA ID NA ID ID ID ID ID ID 1.9E+6 Chloroform 67663 NA 1,600 (W) 7,000 7,200 45,000 1.2E+5 2.7E+5 1.3E+9 1.2E+6 1.5E+6 Chloromethane (I) 74873 NA 5,200 ID 2,300 40,000 4.1E+5 1.0E+6 4.9E+9 1.6E+6 (C) 1.1E+6 4-Chloro-3- methylphenol 59507 NA 5,800 280 NLV NLV NLV NLV ID 4.5E+6 NA beta- Chloronaphthalene 91587 NA 6.2E+5 NA ID ID ID ID ID 5.6E+7 NA 2-Chlorophenol 95578 NA 900 360 4.3E+5 9.6E+5 9.6E+5 9.6E+5 1.2E+9 1.4E+6 1.9E+7 o-Chlorotoluene (I) 95498 NA 3,300 ID 2.7E+5 1.2E+6 2.9E+6 6.3E+6 4.7E+9 4.5E+6 (C) 5.0E+5 Chlorpyrifos 2921882 NA 17,000 1,500 130 4,600 23,000 55,000 1.3E+8 1.1E+7 NA 261 2017 MR 22 – December 15, 2017 Chromium (III) 18,000 (B,H) 16065831 (total) 1.0E+9 (D) (G,X) NLV NLV NLV NLV 3.3E+8 7.9E+8 NA Chromium (VI) 18540299 NA 30,000 3,300 NLV NLV NLV NLV 2.6E+5 2.5E+6 NA Chrysene (Q) 218019 NA NLL NLL ID ID ID ID ID 2.0E+6 NA

262 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Surface Soil Source Soil Chemical Statewide Drinking Water Volatilization Volatile Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Water Interface to Indoor Air Inhalation for 5 Meter for 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels Cobalt 7440484 6,800 800 2,000 NLV NLV NLV NLV 1.3E+7 2.6E+6 NA Copper (B) 7440508 32,000 5.8E+6 (G) NLV NLV NLV NLV 1.3E+8 2.0E+7 NA Cyanazine 21725462 NA 200 1,100 (X) NLV NLV NLV NLV ID 14,000 NA Cyanide (P,R) 57125 390 (total) 4,000 100 NLV NLV NLV NLV 2.5E+5 12,000 NA Cyclohexanone 108941 NA 5.2E+6 NA 17,000 1.0E+6 1.1E+7 2.7E+7 6.7E+10 1.0E+9 (C,D) 2.2E+8 Dacthal 1861321 NA 50,000 NA NLV NLV NLV NLV ID 2.3E+6 NA Dalapon 75990 NA 4,000 NA NLV NLV NLV NLV ID 1.9E+7 5.9E+7 4-4'-DDD 72548 NA NLL NLL NLV NLV NLV NLV 4.4E+7 95,000 NA 4-4'-DDE 72559 NA NLL NLL NLV NLV NLV NLV 3.2E+7 45,000 NA 4-4'-DDT 50293 NA NLL NLL NLV NLV NLV NLV 3.2E+7 57,000 NA Decabromodiphenyl ether 1163195 NA 1.4E+5 NA 1.0E+9 (D) 8.6E+7 8.6E+7 8.6E+7 2.3E+9 3.8E+6 NA Di-n-butyl phthalate 84742 NA 9.6E+5 (C) 11,000 NLV NLV NLV NLV 3.3E+9 2.7E+7 (C) 7.6E+5 1.5E+7 (C, Di(2-ethylhexyl) adipate 103231 NA 1.3E+7 (C) ID NLV NLV NLV NLV 9.2E+9 DD) 9.6E+5 Di-n-octyl phthalate 117840 NA 1.0E+8 ID NLV NLV NLV NLV 3.1E+10 6.9E+6 1.4E+8 Diacetone alcohol (I) 123422 NA ID NA NLV NLV NLV NLV 1.6E+11 ID 1.1E+8 Diazinon 333415 NA 95 72 NLV NLV NLV NLV ID 12,000 (DD) 3.1E+5 Dibenzo(a,h)anthracene (Q) 53703 NA NLL NLL NLV NLV NLV NLV ID 2,000 NA Dibenzofuran 132649 NA ID 1,700 2.0E+6 1.3E+5 1.3E+5 1.3E+5 6.7E+6 ID NA Dibromochloromethane 124481 NA 1,600 (W) ID 3,900 24,000 24,000 33,000 1.3E+8 1.1E+5 6.1E+5 Dibromochloropropane 96128 NA 10 (M); 4.0 ID 220 260 260 260 5.6E+5 4,400 (C) 1,200 Dibromomethane 74953 NA 1,600 NA ID ID ID ID ID 2.5E+6 (C) 2.0E+6 Dicamba 1918009 NA 4,400 NA NA NLV NLV NLV ID 3.4E+6 NA 1,2-Dichlorobenzene 95501 NA 14,000 280 1.1E+7 (C) 3.9E+7 3.9E+7 5.2E+7 1.0E+11 1.9E+7 (C) 2.1E+5 1,3-Dichlorobenzene 541731 NA 170 680 26,000 79,000 79,000 1.1E+5 2.0E+8 2.0E+5 (C) 1.7E+5 1,4-Dichlorobenzene 106467 NA 1,700 360 19,000 77,000 77,000 1.1E+5 4.5E+8 4.0E+5 NA

263 2017 MR 22 – December 15, 2017 2,000 (M); 3,3'-Dichlorobenzidine 91941 NA 2,000 (M); 28 7.4 NLV NLV NLV NLV 6.5E+6 6,600 NA Dichlorodifluoromethane 75718 NA 95,000 ID 9.0E+5 5.3E+7 5.5E+8 1.4E+9 3.3E+12 5.2E+7 (C) 1.0E+6

264 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Surface Soil Source Soil Chemical Statewide Drinking Water Volatilization Volatile Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Water Interface to Indoor Air Inhalation for 5 Meter for 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels 1,1-Dichloroethane 75343 NA 18,000 15,000 2.3E+5 2.1E+6 5.9E+6 1.4E+7 3.3E+10 2.7E+7 (C) 8.9E+5 1,2-Dichloroethane (I) 107062 NA 100 7,200 (X) 2,100 6,200 11,000 26,000 1.2E+8 91,000 1.2E+6 1,1-Dichloroethylene (I) 75354 NA 140 2,600 62 1,100 5,300 13,000 6.2E+7 2.0E+5 5.7E+5 cis-1,2- Dichloroethylene 156592 NA 1,400 12,000 22,000 1.8E+5 4.2E+5 9.9E+5 2.3E+9 2.5E+6 (C) 6.4E+5 trans-1,2- Dichloroethylene 156605 NA 2,000 30,000 (X) 23,000 2.8E+5 8.3E+5 2.0E+6 4.7E+9 3.8E+6 (C) 1.4E+6 2,6-Dichloro-4- nitroaniline 99309 NA 44,000 NA NLV NLV NLV NLV ID 6.8E+7 NA 330 (M); 2,4-Dichlorophenol 120832 NA 1,500 220 NLV NLV NLV NLV 5.1E+9 6.6E+5 (DD) 1.8E+6 2,4-Dichlorophenoxy acetic acid 94757 NA 1,400 4,400 NLV NLV NLV NLV 6.7E+9 2.5E+6 NA 1,2-Dichloropropane (I) 78875 NA 100 4,600 (X) 4,000 25,000 50,000 1.1E+5 2.7E+8 1.4E+5 5.5E+5 1,3-Dichloropropene 542756 NA 170 180 (X) 1,000 18,000 68,000 1.6E+5 7.8E+8 10,000 6.2E+5 Dichlorovos 62737 NA 50 (M); 32 NA NLV NLV NLV NLV 3.3E+7 10,000 2.2E+6 Dicyclohexyl phthalate 84617 NA ID NA ID ID ID ID ID ID NA Dieldrin 60571 NA NLL NLL 1.4E+5 19,000 19,000 19,000 6.8E+5 1,100 NA Diethyl ether 60297 NA 200 ID 2.8E+7 (C) 8.5E+7 1.5E+8 3.4E+8 8.0E+11 1.1E+8 (C) 7.4E+6 Diethyl phthalate 84662 NA 1.1E+5 2,200 NLV NLV NLV NLV 3.3E+9 1.7E+8 (C) 7.4E+5 Diethylene glycol monobutyl ether 112345 NA 1,800 NA NLV NLV NLV NLV 1.3E+9 2.7E+6 1.1E+8 Diisopropyl ether 108203 NA 600 ID 6.7E+5 (C) 3.4E+5 7.6E+5 1.8E+6 4.1E+9 9.2E+5 (C) 1,300 Diisopropylamine (I) 108189 NA 110 NA 5.5E+6 6.2E+6 6.2E+6 7.3E+6 1.3E+10 1.7E+5 6.7E+6 Dimethyl phthalate 131113 NA 1.5E+6 (C) NA NLV NLV NLV NLV 3.3E+9 1.0E+9 (C,D) 7.9E+5 N,N- Dimethylacetamide 127195 NA 3,600 82,000 (X) NLV NLV NLV NLV ID 5.6E+6 1.1E+8

265 2017 MR 22 – December 15, 2017 N,N-Dimethylaniline 121697 NA 320 NA 1.7E+5 1.5E+5 1.5E+5 1.5E+5 2.6E+8 5.0E+5 8.0E+5 Dimethylformamide (I) 68122 NA 14,000 NA NLV NLV NLV NLV 2.0E+9 2.2E+7 1.1E+8 2,4-Dimethylphenol 105679 NA 7,400 7,600 NLV NLV NLV NLV 4.7E+9 1.1E+7 NA 2,6-Dimethylphenol 576261 NA 330 (M); 88 NA NLV NLV NLV NLV 1.3E+8 1.4E+5 NA 3,4-Dimethylphenol 95658 NA 330 (M); 200 500 NLV NLV NLV NLV 2.3E+8 3.2E+5 NA Dimethylsulfoxide 67685 NA 4.4E+6 3.8E+6 NLV NLV NLV NLV 1.3E+9 1.0E+9 (C,D) 1.8E+7 2,4-Dinitrotoluene 121142 NA 430 NA NLV NLV NLV NLV 1.6E+7 48,000 NA

266 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Surface Soil Source Soil Chemical Statewide Drinking Water Volatilization Volatile Soil Finite VSIC Finite VSIC Particulate Saturation Abstract Default Water Interface to Indoor Air Inhalation for 5 Meter for 2 Meter Soil Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Direct Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels Dinoseb 88857 NA 300 200 (M); 43 NLV NLV NLV NLV 2.7E+8 66,000 (DD) 1.4E+5 1,4-Dioxane (I) 123911 NA 1,700 56,000 (X) NLV NLV NLV NLV 5.7E+8 5.3E+5 9.7E+7 Diquat 85007 NA 400 400 NLV NLV NLV NLV ID 5.0E+5 NA Diuron 330541 NA 620 NA NLV NLV NLV NLV 4.7E+8 9.7E+5 NA Endosulfan (J) 115297 NA NLL NLL ID ID ID ID ID 1.4E+6 NA Endothall 145733 NA NLL NLL NLV NLV NLV NLV 2.3E+9 3.8E+6 NA Endrin 72208 NA NLL NLL NLV NLV NLV NLV ID 65,000 NA Epichlorohydrin (I) 106898 NA 100 NA 64,000 31,000 31,000 35,000 6.7E+7 8,900 7.3E+6 1.0E+9 Ethanol (I) 64175 NA 3.8E+7 ID NLV NLV NLV NLV 1.3E+12 (C,D,DD) 1.1E+8 Ethyl acetate (I) 141786 NA 1.3E+5 NA 3.8E+7 (C) 4.9E+7 4.9E+7 9.8E+7 2.1E+11 2.0E+8 (C) 7.5E+6 Ethyl-tert-butyl ether (ETBE) 637923 NA 980 ID 5.4E+5 1.9E+6 4.5E+6 1.1E+7 2.5E+10 ID 6.5E+5 Ethylbenzene (I) 100414 NA 1,500 360 87,000 7.2E+5 1.0E+6 2.2E+6 1.0E+10 2.2E+7 (C) 1.4E+5 Ethylene dibromide 106934 NA 20 (M); 1.0 110 (X) 670 1,700 1,700 3,300 1.4E+7 92 8.9E+5 Ethylene glycol 107211 NA 3.0E+5 3.8E+6 (X) NLV NLV NLV NLV 6.7E+10 4.5E+8 (C) 1.1E+8 Ethylene glycol monobutyl ether 111762 NA 74,000 NA 7.4E+5 1.8E+7 1.5E+8 3.6E+8 8.7E+11 1.1E+8 (C) 4.1E+7 Fluoranthene 206440 NA 7.3E+5 5,500 1.0E+9 (D) 7.4E+8 7.4E+8 7.4E+8 9.3E+9 4.6E+7 NA Fluorene 86737 NA 3.9E+5 5,300 5.8E+8 1.3E+8 1.3E+8 1.3E+8 9.3E+9 2.7E+7 NA Fluorine (soluble fluoride) (B) 7782414 NA 40,000 ID NLV NLV NLV NLV ID 9.0E+6 (DD) NA Formaldehyde 50000 NA 26,000 2,400 12,000 13,000 23,000 52,000 2.4E+8 4.1E+7 6.0E+7 Formic acid (I,U) 64186 NA 2.0E+5 ID 1.5E+6 2.1E+5 1.4E+5 1.4E+5 1.3E+8 3.2E+8 (C) 1.1E+8 1-Formylpiperidine 2591868 NA 1,600 NA ID ID ID ID ID 2.5E+6 1.0E+7 Gentian violet 548629 NA 300 NA NLV NLV NLV NLV ID 96,000 NA Glyphosate 1071836 NA NLL NLL NLV NLV NLV NLV ID 1.1E+7 (DD) NA Heptachlor 76448 NA NLL NLL 3.5E+5 62,000 62,000 62,000 2.4E+6 5,600 NA 267 2017 MR 22 – December 15, 2017 Heptachlor epoxide 1024573 NA NLL NLL NLV NLV NLV NLV 1.2E+6 3,100 NA n-Heptane 142825 NA 4.6E+7 (C) NA 1.5E+6 (C) 2.1E+7 4.4E+7 1.0E+8 2.3E+11 9.9E+8 (C) 2.4E+5 Hexabromobenzene 87821 NA 5,400 ID ID ID ID ID ID 1.1E+6 NA

268 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Groundwater Source Residential Surface Soil Volatile Finite Soil Chemical Statewide Drinking Water Volatilization to Soil VSIC for Finite VSIC Particulate Saturation Abstract Default Water Interface Indoor Air Inhalation 5 Meter for 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels Hexachlorobenzene (C-66) 118741 NA 1,800 350 41,000 17,000 17,000 17,000 6.8E+6 8,900 NA Hexachlorobutadiene (C-46) 87683 NA 26,000 91 1.3E+5 1.3E+5 1.3E+5 1.3E+5 1.4E+8 1.0E+5 3.5E+5 alpha-Hexachlorocyclohexane 319846 NA 18 ID 30,000 12,000 22,000 25,000 1.7E+6 2,600 NA beta-Hexachlorocyclohexane 319857 NA 37 ID NLV NLV NLV NLV 5.9E+6 5,400 NA Hexachlorocyclopentadiene (C- 56) 77474 NA 3.2E+5 ID 30,000 50,000 50,000 50,000 1.3E+7 2.3E+6 (C) 7.2E+5 Hexachloroethane 67721 NA 430 1,800 (X) 40,000 5.5E+5 9.3E+5 9.3E+5 2.3E+8 2.3E+5 NA n-Hexane 110543 NA 1.8E+5 (C) NA 5.1E+5 (C) 3.0E+6 3.2E+6 6.2E+6 1.3E+10 9.2E+7 (C) 44,000 2-Hexanone 591786 NA 20,000 ID 9.9E+5 1.1E+6 1.1E+6 1.4E+6 2.7E+9 3.2E+7 (C) 2.5E+6 Indeno(1,2,3-cd) pyrene (Q) 193395 NA NLL NLL NLV NLV NLV NLV ID 20,000 NA Iron (B) 7439896 1.2E+7 6,000 NA NLV NLV NLV NLV ID 1.6E+8 NA Isobutyl alcohol (I) 78831 NA 46,000 NA 2.3E+8 (C) 7.9E+7 7.9E+7 7.9E+7 1.0E+11 7.2E+7 (C) 8.9E+6 Isophorone 78591 NA 15,000 26,000 (X) NLV NLV NLV NLV 1.2E+10 4.8E+6 (C) 2.4E+6 Isopropyl alcohol (I) 67630 NA 9,400 1.1E+6 (X) NLV NLV NLV NLV 1.5E+10 1.4E+7 1.1E+8 Isopropyl benzene 98828 NA 91,000 3,200 4.0E+5 (C) 1.7E+6 1.7E+6 2.8E+6 5.8E+9 2.5E+7 (C) 3.9E+5 Lead (B) 7439921 21,000 7.0E+5 (G,X) NLV NLV NLV NLV 1.0E+8 4.0E+5 NA 20 (M); Lindane 58899 NA 7.0 20 (M); 1.1 ID ID ID ID ID 8,300 NA 4.2E+6 Lithium (B) 7439932 9,800 3,400 8,800 NLV NLV NLV NLV 2.3E+9 (DD) NA Magnesium (B) 7439954 NA 8.0E+6 NA NLV NLV NLV NLV 6.7E+9 1.0E+9 (D) NA Manganese (B) 7439965 4.4E+5 1,000 (G,X) NLV NLV NLV NLV 3.3E+6 2.5E+7 NA Mercury (Total) (B,Z) Varies 130 1,700 50 (M); 1.2 48,000 52,000 52,000 52,000 2.0E+7 1.6E+5 NA 8.4E+6 ug/m3 Methane 74828 NA ID NA (GG) ID ID ID ID ID ID Methanol 67561 NA 74,000 1.2E+7 (C) 3.7E+7 (C) 3.1E+7 4.4E+7 9.6E+7 2.2E+11 1.1E+8 (C) 3.1E+6 Methoxychlor 72435 NA 16,000 NA ID ID ID ID ID 1.9E+6 NA

269 2017 MR 22 – December 15, 2017 2-Methoxyethanol (I) 109864 NA 150 NA NLV NLV NLV NLV 1.3E+9 2.3E+5 1.1E+8 2-Methyl-4-chlorophenoxyacetic acid 94746 NA 390 NA NLV NLV NLV NLV ID 2.3E+5 NA 830 (M); 2-Methyl-4,6-dinitrophenol 534521 NA 400 NA NLV NLV NLV NLV 1.3E+8 79,000 NA N-Methyl-morpholine (I) 109024 NA 400 NA NLV NLV NLV NLV ID 6.1E+5 1.1E+8

270 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Groundwater Source Residential Surface Soil Volatile Finite Soil Chemical Statewide Drinking Water Volatilization to Soil VSIC for Finite VSIC Particulate Saturation Abstract Default Water Interface Indoor Air Inhalation 5 Meter for 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels Methyl parathion 298000 NA 46 NA NLV NLV NLV NLV ID 56,000 NA 4-Methyl-2-pentanone (MIBK) (I) 108101 NA 36,000 ID 3.7E+7 (C) 4.5E+7 4.5E+7 6.7E+7 1.4E+11 5.6E+7 (C) 2.7E+6 Methyl-tert-butyl ether (MTBE) 1634044 NA 800 1.4E+5 (X) 9.9E+6 (C) 2.5E+7 3.9E+7 8.7E+7 2.0E+11 1.5E+6 5.9E+6 Methylcyclopentane (I) 96377 NA ID NA 92,000 2.3E+6 8.2E+6 2.0E+7 4.7E+10 ID 3.5E+5 4,4'-Methylene-bis-2- chloroaniline (MBOCA) 101144 NA NLL NLL NLV NLV NLV NLV 8.4E+7 6,800 NA Methylene chloride 75092 NA 100 30,000 (X) 45,000 2.1E+5 5.9E+5 1.4E+6 6.6E+9 1.3E+6 2.3E+6 2-Methylnaphthalene 91576 NA 57,000 4,200 2.7E+6 1.5E+6 1.5E+6 1.5E+6 6.7E+8 8.1E+6 NA 1,000 (M); Methylphenols (J) 1319773 NA 7,400 600 NLV NLV NLV NLV 6.7E+9 1.1E+7 NA 1.5E+6 (C, Metolachlor 51218452 NA 4,800 300 NLV NLV NLV NLV ID DD) 4.4E+5 Metribuzin 21087649 NA 3,600 NA ID ID ID ID ID 9.6E+6 NA Mirex 2385855 NA NLL NLL ID ID ID ID ID 9,600 NA Molybdenum (B) 7439987 NA 1,500 64,000 (X) NLV NLV NLV NLV ID 2.6E+6 NA Naphthalene 91203 NA 35,000 730 2.5E+5 3.0E+5 3.0E+5 3.0E+5 2.0E+8 1.6E+7 NA Nickel (B) 7440020 20,000 1.0E+5 (G) NLV NLV NLV NLV 1.3E+7 4.0E+7 NA 2.0E+5 Nitrate (B,N) 14797558 NA (N) ID NLV NLV NLV NLV ID ID NA Nitrite (B,N) 14797650 NA 20,000 (N) NA NLV NLV NLV NLV ID ID NA 330 (M); Nitrobenzene (I) 98953 NA 68 3,600 (X) 91,000 54,000 54,000 54,000 4.7E+7 1.0E+5 4.9E+5 2-Nitrophenol 88755 NA 400 ID NLV NLV NLV NLV ID 6.3E+5 NA 330 (M); n-Nitroso-di-n-propylamine 621647 NA 100 NA NLV NLV NLV NLV 1.6E+6 1,200 1.5E+6 N-Nitrosodiphenylamine 86306 NA 5,400 NA NLV NLV NLV NLV 2.2E+9 1.7E+6 NA Oxamyl 23135220 NA 4,000 NA NLV NLV NLV NLV ID 8.6E+6 NA Oxo-hexyl acetate 88230357 NA 1,500 NA ID ID ID ID 5.4E+9 2.3E+6 1.0E+7 271 2017 MR 22 – December 15, 2017 Pendimethalin 40487421 NA 1.1E+6 NA NLV NLV NLV NLV ID 4.6E+7 NA Pentachlorobenzene 608935 NA 29,000 9,500 ID ID ID ID ID 3.2E+5 (C) 1.9E+5 Pentachloronitrobenzene 82688 NA 37,000 NA 1.2E+5 2.3E+5 2.3E+5 2.3E+5 3.3E+8 1.7E+6 NA Pentachlorophenol 87865 NA 22 (G,X) NLV NLV NLV NLV 1.0E+8 90,000 NA Pentane 109660 NA ID NA 9.7E+5 (C) 3.7E+7 3.1E+8 5.8E+8 1.2E+12 ID 2.4E+5

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Groundwater Source Residential Surface Soil Volatile Finite Soil Chemical Statewide Drinking Water Volatilization to Soil VSIC for Finite VSIC Particulate Saturation Abstract Default Water Interface Indoor Air Inhalation 5 Meter for 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels 2-Pentene (I) 109682 NA ID NA ID ID ID ID ID ID 2.2E+5 Phenanthrene 85018 NA 56,000 2,100 2.8E+6 1.6E+5 1.6E+5 1.6E+5 6.7E+6 1.6E+6 NA 4.0E+7 (C, Phenol 108952 NA 88,000 9,000 NLV NLV NLV NLV 4.0E+10 DD) 1.2E+7 Phenytoin 57410 NA 830 4300 (X) NLV NLV NLV NLV 2.2E+8 1.0E+5 NA Phosphorus (Total) 7723140 NA 1.3E+6 (EE) NLV NLV NLV NLV 6.7E+7 1.0E+9 (D) NA Phthalic acid 88993 NA 2.8E+5 NA NLV NLV NLV NLV ID 4.3E+8 (C) 1.7E+6 Phthalic anhydride 85449 NA 3.0E+5 NA NLV NLV NLV NLV ID 4.7E+8 (C) 1.1E+6 Picloram 1918021 NA 10,000 920 NLV NLV NLV NLV ID 1.6E+7 NA Piperidine 110894 NA 64 NA NLV NLV NLV NLV 9.3E+9 99,000 1.2E+8 Polybrominated biphenyls (J) 67774327 NA NLL NLL NLV NLV NLV NLV ID 1,200 NA Polychlorinated biphenyls (PCBs) (J,T) 1336363 NA NLL NLL 3.0E+6 2.4E+5 7.9E+6 7.9E+6 5.2E+6 (T) NA Prometon 1610180 NA 4,900 NA NLV NLV NLV NLV ID 5.0E+6 NA Propachlor 1918167 NA 1,900 NA NLV NLV NLV NLV ID 2.9E+6 NA Propazine 139402 NA 4,000 NA NLV NLV NLV NLV ID 6.1E+6 NA Propionic acid 79094 NA 2.4E+5 ID NLV NLV NLV NLV 2.0E+10 3.8E+8 (C) 1.1E+8 Propyl alcohol (I) 71238 NA 28,000 NA NLV NLV NLV NLV 4.9E+10 1.3E+7 (DD) 1.1E+8 n-Propylbenzene (I) 103651 NA 1,600 ID ID ID ID ID 1.3E+9 2.5E+6 1.0E+7 1.0E+9 Propylene glycol 57556 NA 3.0E+6 5.8E+6 NLV NLV NLV NLV 4.0E+11 (C,D) 1.1E+8 Pyrene 129000 NA 4.8E+5 ID 1.0E+9 (D) 6.5E+8 6.5E+8 6.5E+8 6.7E+9 2.9E+7 NA Pyridine (I) 110861 NA 400 NA 1,100 8,200 40,000 97,000 2.3E+8 2.3E+5 (C) 37,000 272 2017 MR 22 – December 15, 2017 Selenium (B) 7782492 410 4,000 400 NLV NLV NLV NLV 1.3E+8 2.6E+6 NA Silver (B) 7440224 1,000 4,500 100 (M); 27 NLV NLV NLV NLV 6.7E+6 2.5E+6 NA Silvex (2,4,5-TP) 93721 NA 3,600 2,200 NLV NLV NLV NLV ID 1.7E+6 NA Simazine 122349 NA 80 340 NLV NLV NLV NLV ID 1.2E+6 NA Sodium 17341252 NA 4.6E+6 NA NLV NLV NLV NLV ID 1.0E+9 (D) NA Sodium azide 26628228 NA 1,800 1,000 ID ID ID ID ID 2.7E+6 NA Strontium (B) 7440246 NA 92,000 4.2E+5 NLV NLV NLV NLV ID 3.3E+8 NA

273 2017 MR 22 – December 15, 2017

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Groundwater Source Residential Surface Soil Volatile Finite Finite Soil Chemical Statewide Drinking Water Volatilization Soil VSIC for 5 VSIC for Particulate Saturation Abstract Default Water Interface to Indoor Air Inhalation Meter 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels Styrene 100425 NA 2,700 2,100 (X) 2.5E+5 9.7E+5 9.7E+5 1.4E+6 5.5E+9 4.0E+5 5.2E+5 Sulfate 14808798 NA 5.0E+6 NA NLV NLV NLV NLV ID ID NA Tebuthiuron 34014181 NA 10,000 NA NLV NLV NLV NLV ID 4.6E+6 (DD) NA 2,3,7,8-Tetrabromodibenzo-p- dioxin (O) 50585416 NA NLL NLL NLV NLV NLV NLV (O) (O) NA 1,2,4,5-Tetrachlorobenzene 95943 NA 1.5E+6 3,400 (X) 5.8E+5 2.3E+5 2.3E+5 2.3E+5 6.7E+7 7.7E+7 NA 2,3,7,8-Tetrachlorodibenzo-p- dioxin (O) 1746016 NA NLL NLL NLV NLV NLV NLV 71 (O) 0.09 (O) NA 1,1,1,2-Tetrachloroethane 630206 NA 1,500 ID 6,200 36,000 54,000 1.0E+5 4.2E+8 4.8E+5 (C) 4.4E+5 1,1,2,2-Tetrachloroethane 79345 NA 170 1,600 (X) 4,300 10,000 10,000 14,000 5.4E+7 53,000 8.7E+5 Tetrachloroethylene 127184 NA 100 1,200 (X) 11,000 1.7E+5 4.8E+5 1.1E+6 2.7E+9 2.0E+5 (C) 88,000 Tetrahydrofuran 109999 NA 1,900 2.2E+5 (X) 1.3E+6 1.3E+7 6.7E+7 1.6E+8 3.9E+11 2.9E+6 1.2E+8 500 (M); Tetranitromethane 509148 NA ID NA 500(M); 110 51 ID ID 2.1E+5 ID ID Thallium (B) 7440280 NA 2,300 4,200 (X) NLV NLV NLV NLV 1.3E+7 35,000 NA Toluene (I) 108883 NA 16,000 5,400 3.3E+5 (C) 2.8E+6 5.1E+6 1.2E+7 2.7E+10 5.0E+7 (C) 2.5E+5 660 (M); p-Toluidine 106490 NA 300 NA NLV NLV NLV NLV 1.0E+8 94,000 1.2E+6 Toxaphene 8001352 NA 24,000 8,200 NLV NLV NLV NLV 9.7E+6 20,000 NA Triallate 2303175 NA 95,000 NA ID ID ID ID ID 2.9E+6 (C) 2.5E+5 Tributylamine 102829 NA 7,800 ID 5.8E+5 6.0E+5 6.0E+5 6.0E+5 4.7E+8 7.9E+5 3.7E+6 1,2,4-Trichlorobenzene 120821 NA 4,200 5,900 (X) 9.6E+6 (C) 2.8E+7 2.8E+7 2.8E+7 2.5E+10 9.9E+5 (DD) 1.1E+6 1,1,1-Trichloroethane 71556 NA 4,000 1,800 2.5E+5 3.8E+6 1.2E+7 2.8E+7 6.7E+10 5.0E+8 (C) 4.6E+5 1,1,2-Trichloroethane 79005 NA 100 6,600 (X) 4,600 17,000 21,000 44,000 1.9E+8 1.8E+5 9.2E+5 Trichloroethylene 79016 NA 100 4,000 (X) 1,000 11,000 25,000 57,000 1.3E+8 1.1E+5 (DD) 5.0E+5 Trichlorofluoromethane 75694 NA 52,000 NA 2.8E+6 (C) 9.2E+7 6.3E+8 1.5E+9 3.8E+12 7.9E+7 (C) 5.6E+5 2,4,5-Trichlorophenol 95954 NA 39,000 NA NLV NLV NLV NLV 2.3E+10 2.3E+7 NA

274 2017 MR 22 – December 15, 2017 330 (M); 2,4,6-Trichlorophenol 88062 NA 2,400 100 NLV NLV NLV NLV 1.0E+9 7.1E+5 NA 1,2,3-Trichloropropane 96184 NA 840 NA 4,000 9,200 9,200 11,000 2.0E+7 1.3E+6 (C) 8.3E+5 1,1,2-Trichloro-1,2,2- 1.0E+9 trifluoroethane 76131 NA 9.0E+6 (C) 1,700 5.1E+6 (C) 1.8E+8 8.8E+8 2.1E+9 5.1E+12 (C,D) 5.5E+5 Triethanolamine 102716 NA 74,000 NA NLV NLV NLV NLV 3.3E+9 1.1E+8 1.1E+8

TABLE 2. SOIL: RESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Groundwater Source Residential Surface Soil Volatile Finite Finite Soil Chemical Statewide Drinking Water Volatilization Soil VSIC for 5 VSIC for Particulate Saturation Abstract Default Water Interface to Indoor Air Inhalation Meter 2 Meter Soil Direct Concentration Service Background Protection Protection Inhalation Criteria Source Source Inhalation Contact Screening Hazardous Substance Number Level Criteria Criteria Criteria (VSIC) Thickness Thickness Criteria Criteria Levels 3.9E+7 Triethylene glycol 112276 NA 86,000 NA NLV NLV NLV NLV ID (C,DD) 1.1E+5 3-Trifluoromethyl-4-nitrophenol 88302 NA 1.1E+5 NA NLV NLV NLV NLV ID 4.1E+7 (DD) NA Trifluralin 1582098 NA 1.9E+5 NA ID ID ID ID ID 2.0E+6 NA 2,2,4-Trimethyl pentane 540841 NA ID NA 1.1E+5 (C) 5.2E+6 3.9E+7 9.6E+7 2.3E+11 ID 19,000 2,4,4-Trimethyl-2-pentene (I) 107404 NA ID NA ID ID ID ID ID ID 56,000 1,2,4-Trimethylbenzene (I) 95636 NA 2,100 570 4.3E+6 (C) 2.1E+7 5.0E+8 5.0E+8 8.2E+10 3.2E+7 (C) 1.1E+5 1,3,5-Trimethylbenzene (I) 108678 NA 1,800 1,100 2.6E+6 (C) 1.6E+7 3.8E+8 3.8E+8 8.2E+10 3.2E+7 (C) 94,000 Triphenyl phosphate 115866 NA 1.5E+6 (C) NA NLV NLV NLV NLV ID 3.6E+7 (C) 1.1E+5 tris(2,3- Dibromopropyl)phosphate 126727 NA 930 ID 82,000 (C) 18,000 18,000 18,000 5.9E+6 4,400 27,000 Urea 57136 NA ID NA NLV NLV NLV NLV ID ID NA Vanadium 7440622 NA 72,000 4.3E+5 NLV NLV NLV NLV ID 7.5E+5 (DD) NA 5.8E+6 Vinyl acetate (I) 108054 NA 13,000 NA 7.9E+5 1.7E+6 2.6E+6 5.8E+6 1.3E+10 (C,DD) 2.4E+6 Vinyl chloride 75014 NA 40 260 (X) 270 4,200 30,000 73,000 3.5E+8 3,800 4.9E+5 White phosphorus (R) 12185103 NA 2.2 NA NLV NLV NLV NLV ID 2,300 (DD) NA Xylenes (I) 1330207 NA 5,600 820 6.3E+6 (C) 4.6E+7 6.1E+7 1.3E+8 2.9E+11 4.1E+8 (C) 1.5E+5 Zinc (B) 7440666 47,000 2.4E+6 (G) NLV NLV NLV NLV ID 1.7E+8 NA

275 2017 MR 22 – December 15, 2017 R 299.48 Rescinded.Generic soil cleanup criteria for nonresidential category. Rule 48. Generic soil cleanup criteria for nonresidential category shall be as shown in table 3.

276 2017 MR 22 – December 15, 2017 TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Source Groundwat Soil Volatile Finite Finite Chemica Residential Nonresidenti er Surface Volatilizati Soil VSIC for VSIC for Soil l Statewide Drinking al Drinking Water on to Inhalatio 5 Meter 2 Meter Saturation Abstract Default Water Water Interface Indoor Air n Source Source Particulate Soil Direct Concentratio Service Backgrou Protection Protection Protection Inhalation Criteria Thicknes Thicknes Inhalation Contact n Screening Hazardous Substance Number nd Levels Criteria Criteria Criteria Criteria (VSIC) s s Criteria Criteria Levels Acenaphthene 83329 NA 3.0E+5 8.8E+5 8,700 3.5E+8 9.7E+7 9.7E+7 9.7E+7 6.2E+9 1.3E+8 NA Acenaphthylene 208968 NA 5,900 17,000 ID 3.0E+6 2.7E+6 2.7E+6 2.7E+6 1.0E+9 5.2E+6 NA Acetaldehyde (I) 75070 NA 19,000 54,000 2,600 4.0E+5 2.1E+5 2.1E+5 2.9E+5 2.6E+8 9.5E+7 1.1E+8 Acetate 71501 NA ID ID (G) ID ID ID ID ID ID ID Acetic acid 64197 NA 84,000 2.4E+5 (G) NLV NLV NLV NLV 7.4E+9 4.2E+8 6.5E+8 Acetone (I) 67641 NA 15,000 42,000 34,000 5.4E+8 (C) 1.6E+8 1.6E+8 2.0E+8 1.7E+11 7.3E+7 1.1E+8 Acetonitrile 75058 NA 2,800 8,000 NA 8.8E+6 1.9E+6 1.9E+6 2.2E+6 1.8E+9 1.4E+7 2.2E+7 Acetophenone 98862 NA 30,000 88,000 ID 2.1E+8 (C) 5.2E+7 5.2E+7 5.2E+7 1.4E+10 1.5E+8 (C) 1.1E+6 Acrolein (I) 107028 NA 2,400 6,600 NA 760 370 370 630 5.9E+5 1.2E+7 2.3E+7 Acrylamide 79061 NA 10 10 200 (X) NLV NLV NLV NLV 3.0E+6 8,700 NA 2.1E+8 Acrylic acid 79107 NA 78,000 2.2E+5 NA 5.5E+6 2.2E+5 2.7E+5 2.7E+5 2.9E+7 (C,DD) 1.1E+8 100 (M); 100 (M); Acrylonitrile (I) 107131 NA 52 220 40 35,000 17,000 17,000 31,000 5.8E+7 74,000 8.3E+6 1597260 Alachlor 8 NA 52 52 290 (X) NLV NLV NLV NLV ID 3.9E+5 NA Aldicarb 116063 NA 60 60 NA NLV NLV NLV NLV ID 7.3E+5 NA 200 (M); Aldicarb sulfone 1646884 NA 40 200 (M); 40 NA NLV NLV NLV NLV ID 8.0E+5 NA Aldicarb sulfoxide 1646873 NA 200(M); 80 200 (M); 80 NA NLV NLV NLV NLV ID 9.5E+5 NA Aldrin 309002 NA NLL NLL NLL 7.1E+6 2.0E+5 2.0E+5 2.0E+5 8.0E+5 4,300 NA Aluminum (B) 7429905 6.9E+6 1,000 1,000 NA NLV NLV NLV NLV ID 3.7E+8 (DD) NA Ammonia 7664417 NA ID ID (CC) ID ID ID ID 2.9E+9 ID 1.0E+7 t-Amyl methyl ether (TAME) 994058 NA 3,900 3,900 NA 1.1E+5 4.0E+5 7.8E+5 1.8E+6 1.8E+9 9.5E+7 (C) 4.4E+5 330 (M); Aniline 62533 NA 1,100 4,400 80 NLV NLV NLV NLV 2.9E+7 1.5E+6 4.5E+6 Anthracene 120127 NA 41,000 41,000 ID 1.0E+9 (D) 1.6E+9 1.6E+9 1.6E+9 2.9E+10 7.3E+8 NA Antimony 7440360 NA 4,300 4,300 94,000 (X) NLV NLV NLV NLV 5.9E+6 6.7E+5 NA

277 2017 MR 22 – December 15, 2017 Arsenic 7440382 5,800 4,600 4,600 4,600 NLV NLV NLV NLV 9.1E+5 37,000 NA 1.0E+7 (M); Asbestos (BB) 1332214 NA NLL NLL NLL NLV NLV NLV NLV 85,000 ID NA Atrazine 1912249 NA 60 60 150 NLV NLV NLV NLV ID 3.3E+5 (DD) NA Azobenzene 103333 NA 4,200 17,000 ID 3.2E+7 2.1E+6 2.1E+6 2.1E+6 1.3E+8 6.6E+5 NA

278 2017 MR 22 – December 15, 2017

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Nonresidential Surface Soil Source Drinking Drinking Water Volatilization Volatile Soil Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for Finite VSIC Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter for 2 Meter Inhalation Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels Barium (B) 7440393 75,000 1.3E+6 1.3E+6 (G) NLV NLV NLV NLV 1.5E+8 1.3E+8 NA Benzene (I) 71432 NA 100 100 4,000 (X) 8,400 45,000 99,000 2.3E+5 4.7E+8 8.4E+5 (C) 4.0E+5 1,000 (M); 1,000 (M); 1,000 (M); Benzidine 92875 NA 6.0 1,000 (M); 6.0 6.0 NLV NLV NLV NLV 59,000 110 NA Benzo(a)anthracene (Q) 56553 NA NLL NLL NLL NLV NLV NLV NLV ID 80,000 NA Benzo(b)fluoranthene (Q) 205992 NA NLL NLL NLL ID ID ID ID ID 80,000 NA Benzo(k)fluoranthene (Q) 207089 NA NLL NLL NLL NLV NLV NLV NLV ID 8.0E+5 NA Benzo(g,h,i)perylene 191242 NA NLL NLL NLL NLV NLV NLV NLV 3.5E+8 7.0E+6 NA Benzo(a)pyrene (Q) 50328 NA NLL NLL NLL NLV NLV NLV NLV 1.9E+6 8,000 NA Benzoic acid 65850 NA 6.4E+5 1.8E+6 NA NLV NLV NLV NLV ID 1.0E+9 (D) NA 1.0E+9 Benzyl alcohol 100516 NA 2.0E+5 5.8E+5 NA NLV NLV NLV NLV 1.5E+11 (C,D) 5.8E+6 Benzyl chloride 100447 NA 150 640 NA 33,000 48,000 48,000 52,000 7.8E+7 2.2E+5 2.3E+5 Beryllium 7440417 NA 51,000 51,000 (G) NLV NLV NLV NLV 5.9E+5 1.6E+6 NA bis(2- Chloroethoxy)ethane 112265 NA ID ID ID NLV NLV NLV NLV ID ID 2.7E+6 bis(2-Chloroethyl)ether (I) 111444 NA 100 170 100 (M); 20 44,000 13,000 13,000 13,000 1.2E+7 58,000 2.2E+6 bis(2- Ethylhexyl)phthalate 117817 NA NLL NLL NLL NLV NLV NLV NLV 8.9E+8 1.2E+7 (C) 1.0E+7 Boron (B) 7440428 NA 10,000 10,000 1.4E+5 (X) NLV NLV NLV NLV ID 3.5E+8 (DD) NA Bromate 15541454 NA 200 200 800 (X) NLV NLV NLV NLV ID 91,000 NA Bromobenzene (I) 108861 NA 550 1,500 NA 5.8E+5 5.4E+5 5.4E+5 5.4E+5 2.4E+8 1.7E+6 (C) 7.6E+5 Bromodichloromethane 75274 NA 1,600 (W) 1,600 (W) ID 6,400 31,000 31,000 57,000 1.1E+8 4.9E+5 1.5E+6 Bromoform 75252 NA 1,600 (W) 1,600 (W) ID 7.7E+5 3.1E+6 3.1E+6 3.1E+6 3.6E+9 3.8E+6 (C) 8.7E+5 Bromomethane 74839 NA 200 580 700 1,600 13,000 57,000 1.4E+5 1.5E+8 1.0E+6 2.2E+6

279 2017 MR 22 – December 15, 2017 n-Butanol (I) 71363 NA 19,000 54,000 2.00E+05 NLV NLV NLV NLV 1.0E+10 9.5E+7 (C) 8.7E+6 7.0E+8 2-Butanone (MEK) (I) 78933 NA 2.6E+5 7.6E+5 44,000 9.9E+7 (C) 3.5E+7 3.5E+7 3.6E+7 2.9E+10 (C,DD) 2.7E+7 n-Butyl acetate 123864 NA 11,000 32,000 NA 1.0E+8 (C) 1.4E+8 3.1E+8 3.5E+8 2.1E+11 5.5E+7 (C) 1.1E+6 t-Butyl alcohol 75650 NA 78,000 2.2E+5 NA 5.8E+8 (C) 1.2E+8 2.4E+8 2.4E+8 5.6E+10 3.9E+8 (C) 1.1E+8 Butyl benzyl phthalate 85687 NA 2.2E+6 (C) 5.0E+6 (C) 1.2E+5 (X) NLV NLV NLV NLV 2.1E+10 1.2E+8 (C) 3.1E+5 n-Butylbenzene 104518 NA 1,600 4,600 ID ID ID ID ID 8.8E+8 8.0E+6 1.0E+7

280 2017 MR 22 – December 15, 2017

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Nonresidential Surface Soil Source Drinking Drinking Water Volatilization Volatile Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for VSIC for Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels sec-Butylbenzene 135988 NA 1,600 4,600 ID ID ID ID ID 1.8E+8 8.0E+6 1.0E+7 t-Butylbenzene (I) 98066 NA 1,600 4,600 ID ID ID ID ID 2.9E+8 8.0E+6 1.0E+7 Cadmium (B) 7440439 1,200 6,000 6,000 (G,X) NLV NLV NLV NLV 2.2E+6 2.1E+6 NA Camphene (I) 79925 NA ID ID NA 6,700 1.8E+5 9.1E+5 2.2E+6 2.4E+9 ID NA 3.1E+8 Caprolactam 105602 NA 1.2E+5 3.4E+5 NA NLV NLV NLV NLV 2.9E+8 (DD) NA Carbaryl 63252 NA 14,000 40,000 NA ID ID ID ID ID 7.0E+7 NA Carbazole 86748 NA 9,400 39,000 1,100 NLV NLV NLV NLV 7.8E+7 2.4E+6 NA Carbofuran 1563662 NA 800 800 NA NLV NLV NLV NLV ID 3.6E+6 NA 4.3E+7 Carbon disulfide (I,R) 75150 NA 16,000 46,000 ID 1.4E+5 1.6E+6 8.0E+6 1.9E+7 2.1E+10 (C,DD) 2.8E+5 Carbon tetrachloride 56235 NA 100 100 900 (X) 990 12,000 34,000 79,000 1.7E+8 4.4E+5 (C) 3.9E+5 Chlordane (J) 57749 NA NLL NLL NLL 5.9E+7 4.2E+6 4.2E+6 4.2E+6 2.1E+7 1.5E+5 NA Chloride 16887006 NA 5.0E+6 5.0E+6 (X) NLV NLV NLV NLV ID 5.0E+5 (F) NA Chlorobenzene (I) 108907 NA 2,000 2,000 500 2.2E+5 9.2E+5 1.1E+6 2.1E+6 2.1E+9 1.4E+7 (C) 2.6E+5 p-Chlorobenzene sulfonic acid 98668 NA 1.5E+5 4.2E+5 ID ID ID ID ID ID 7.3E+8 ID 1-Chloro-1,1- 1.0E+9 difluoroethane 75683 NA 3.0E+5 8.8E+5 NA 5.4E+6 (C) 9.4E+7 5.7E+8 1.4E+9 1.5E+12 (C,D) 9.6E+5 Chloroethane 75003 NA 8,600 34,000 22,000 (X) 5.3E+6 (C) 3.6E+7 1.2E+8 2.8E+8 2.9E+11 1.2E+7 (C) 9.5E+5 2-Chloroethyl vinyl ether 110758 NA ID ID NA ID ID ID ID ID ID 1.9E+6 Chloroform 67663 NA 1,600 (W) 1,600 (W) 7,000 38,000 1.5E+5 3.4E+5 7.9E+5 1.6E+9 5.5E+6 (C) 1.5E+6 Chloromethane (I) 74873 NA 5,200 22,000 ID 10,000 1.2E+5 1.0E+6 2.5E+6 2.6E+9 7.4E+6 (C) 1.1E+6 4-Chloro-3-methylphenol 59507 NA 5,800 16,000 280 NLV NLV NLV NLV ID 1.5E+7 NA beta-Chloronaphthalene 91587 NA 6.2E+5 1.8E+6 NA ID ID ID ID ID 1.8E+8 NA 2-Chlorophenol 95578 NA 900 2,600 360 8.0E+5 1.1E+6 1.1E+6 1.1E+6 5.3E+8 4.5E+6 1.9E+7 o-Chlorotoluene (I) 95498 NA 3,300 9,300 ID 5.0E+5 1.5E+6 3.1E+6 6.4E+6 2.1E+9 1.5E+7 (C) 5.0E+5

281 2017 MR 22 – December 15, 2017 Chlorpyrifos 2921882 NA 17,000 48,000 1,500 240 5,500 23,000 56,000 5.9E+7 3.4E+7 NA 18,000 1.0E+9 Chromium (III) (B,H) 16065831 (total) (D) 1.0E+9 (D) (G,X) NLV NLV NLV NLV 1.5E+8 1.0E+9 (D) NA Chromium (VI) 18540299 NA 30,000 30,000 3,300 NLV NLV NLV NLV 2.4E+5 9.2E+6 NA Chrysene (Q) 218019 NA NLL NLL NLL ID ID ID ID ID 8.0E+6 NA

282 2017 MR 22 – December 15, 2017

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Groundwater Source Residential Nonresidential Surface Soil Volatile Drinking Drinking Water Volatilization Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for VSIC for Soil Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Direct Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels Cobalt 7440484 6,800 800 2,000 2,000 NLV NLV NLV NLV 5.9E+6 9.0E+6 NA Copper (B) 7440508 32,000 5.8E+6 5.8E+6 (G) NLV NLV NLV NLV 5.9E+7 7.3E+7 NA Cyanazine 21725462 NA 200 200 1,100 (X) NLV NLV NLV NLV ID 66,000 NA Cyanide (P,R) 57125 390 (total) 4,000 4,000 100 NLV NLV NLV NLV 2.5E+5 2.5E+5 NA Cyclohexanone 108941 NA 5.2E+6 1.5E+7 NA 32,000 1.3E+6 1.1E+7 2.7E+7 2.9E+10 1.0E+9 (C,D) 2.2E+8 Dacthal 1861321 NA 50,000 1.4E+5 NA NLV NLV NLV NLV ID 7.3E+6 NA Dalapon 75990 NA 4,000 4,000 NA NLV NLV NLV NLV ID 6.2E+7 (C) 5.9E+7 4-4'-DDD 72548 NA NLL NLL NLL NLV NLV NLV NLV 5.6E+7 4.0E+5 NA 4-4'-DDE 72559 NA NLL NLL NLL NLV NLV NLV NLV 4.0E+7 1.9E+5 NA 4-4'-DDT 50293 NA NLL NLL NLL NLV NLV NLV NLV 4.0E+7 2.8E+5 NA Decabromodiphenyl ether 1163195 NA 1.4E+5 1.4E+5 NA 1.0E+9 (D) 1.0E+8 1.0E+8 1.0E+8 1.0E+9 1.1E+7 NA Di-n-butyl phthalate 84742 NA 9.6E+5 (C) 2.7E+6 (C) 11,000 NLV NLV NLV NLV 1.5E+9 8.7E+7 (C) 7.6E+5 6.3E+7 Di(2-ethylhexyl) adipate 103231 NA 1.3E+7 (C) 1.3E+7 (C) ID NLV NLV NLV NLV 1.2E+10 (C,DD) 9.6E+5 Di-n-octyl phthalate 117840 NA 1.0E+8 2.9E+8 (C) ID NLV NLV NLV NLV 1.4E+10 2.0E+7 1.4E+8 Diacetone alcohol (I) 123422 NA ID ID NA NLV NLV NLV NLV 7.1E+10 ID 1.1E+8 Diazinon 333415 NA 95 280 72 NLV NLV NLV NLV ID 70,000 (DD) 3.1E+5 Dibenzo(a,h)anthracene (Q) 53703 NA NLL NLL NLL NLV NLV NLV NLV ID 8,000 NA Dibenzofuran 132649 NA ID ID 1,700 3.6E+6 1.6E+5 1.6E+5 1.6E+5 2.9E+6 ID NA Dibromochloromethane 124481 NA 1,600 (W) 1,600 (W) ID 21,000 80,000 80,000 98,000 1.6E+8 5.0E+5 6.1E+5 Dibromochloropropane 96128 NA 10 (M); 4.0 10 (M); 4.0 ID 1,200 900 900 900 7.0E+5 20,000 (C) 1,200 Dibromomethane 74953 NA 1,600 4,600 NA ID ID ID ID ID 8.0E+6 (C) 2.0E+6 Dicamba 1918009 NA 4,400 13,000 NA NLV NLV NLV NLV ID 1.7E+7 NA 1,2-Dichlorobenzene 95501 NA 14,000 14,000 280 2.0E+7 (C) 4.6E+7 4.6E+7 5.5E+7 4.4E+10 6.3E+7 (C) 2.1E+5

283 2017 MR 22 – December 15, 2017 1,3-Dichlorobenzene 541731 NA 170 480 680 48,000 94,000 94,000 1.1E+5 8.8E+7 6.6E+5 (C) 1.7E+5 1,4-Dichlorobenzene 106467 NA 1,700 1,700 360 1.0E+5 2.6E+5 2.6E+5 3.4E+5 5.7E+8 1.9E+6 NA 2,000 (M); 2,000 (M); 2,000 (M); 3,3'-Dichlorobenzidine 91941 NA 28 110 7.4 NLV NLV NLV NLV 8.2E+6 30,000 NA Dichlorodifluoromethane 75718 NA 95,000 2.7E+5 ID 1.7E+6 6.3E+7 5.5E+8 1.4E+9 1.5E+12 1.7E+8 (C) 1.0E+6

284 2017 MR 22 – December 15, 2017

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Nonresidential Surface Soil Source Drinking Drinking Water Volatilization Volatile Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for VSIC for Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels 1,1-Dichloroethane 75343 NA 18,000 50,000 15,000 4.3E+5 2.5E+6 6.0E+6 1.4E+7 1.5E+10 8.7E+7 (C) 8.9E+5 1,2-Dichloroethane (I) 107062 NA 100 100 7,200 (X) 11,000 21,000 33,000 74,000 1.5E+8 4.2E+5 1.2E+6 1,1-Dichloroethylene (I) 75354 NA 140 140 2,600 330 3,700 15,000 37,000 7.8E+7 6.6E+5 (C) 5.7E+5 cis-1,2- Dichloroethylene 156592 NA 1,400 1,400 12,000 41,000 2.1E+5 4.3E+5 1.0E+6 1.0E+9 8.0E+6 (C) 6.4E+5 trans-1,2- Dichloroethylene 156605 NA 2,000 2,000 30,000 (X) 43,000 3.3E+5 8.4E+5 2.0E+6 2.1E+9 1.2E+7 (C) 1.4E+6 2,6-Dichloro-4- nitroaniline 99309 NA 44,000 1.3E+5 NA NLV NLV NLV NLV ID 2.2E+8 NA 3.9E+6 2,4-Dichlorophenol 120832 NA 1,500 4,200 330 (M); 220 NLV NLV NLV NLV 2.3E+9 (C,DD) 1.8E+6 2,4- Dichlorophenoxyacetic acid 94757 NA 1,400 1,400 4,400 NLV NLV NLV NLV 2.9E+9 8.6E+6 NA 1,2-Dichloropropane (I) 78875 NA 100 100 4,600 (X) 7,400 30,000 51,000 1.2E+5 1.2E+8 6.6E+5 (C) 5.5E+5 1,3-Dichloropropene 542756 NA 170 700 180 (X) 5,400 60,000 2.0E+5 4.7E+5 5.9E+8 2.4E+5 6.2E+5 Dichlorovos 62737 NA 50 (M); 32 130 NA NLV NLV NLV NLV 1.5E+7 47,000 2.2E+6 Dicyclohexyl phthalate 84617 NA ID ID NA ID ID ID ID ID ID NA Dieldrin 60571 NA NLL NLL NLL 7.2E+5 64,000 64,000 64,000 8.5E+5 4,700 NA Diethyl ether 60297 NA 200 200 ID 5.2E+7 (C) 1.0E+8 1.6E+8 3.5E+8 3.5E+11 3.6E+8 (C) 7.4E+6 Diethyl phthalate 84662 NA 1.1E+5 3.2E+5 2,200 NLV NLV NLV NLV 1.5E+9 5.5E+8 (C) 7.4E+5 Diethylene glycol monobutyl ether 112345 NA 1,800 5,000 NA NLV NLV NLV NLV 5.9E+8 8.7E+6 1.1E+8 Diisopropyl ether 108203 NA 600 1,700 (C) ID 1.2E+6 (C) 3.2E+6 4.8E+6 1.0E+7 1.1E+10 3.0E+6 (C) 1,300 Diisopropylamine (I) 108189 NA 110 320 NA 1.0E+7 (C) 7.4E+6 7.4E+6 7.7E+6 5.9E+9 5.6E+5 6.7E+6 1.0E+9 Dimethyl phthalate 131113 NA 1.5E+6 (C) 4.2E+6 (C) NA NLV NLV NLV NLV 1.5E+9 (C,D) 7.9E+5 N,N-Dimethylacetamide 127195 NA 3,600 10,000 82,000 (X) NLV NLV NLV NLV ID 1.8E+7 1.1E+8

285 2017 MR 22 – December 15, 2017 N,N-Dimethylaniline 121697 NA 320 920 NA 8.9E+5 (C) 5.2E+5 5.2E+5 5.2E+5 3.3E+8 1.6E+6 (C) 8.0E+5 Dimethylformamide (I) 68122 NA 14,000 40,000 NA NLV NLV NLV NLV 8.8E+8 7.0E+7 1.1E+8 2,4-Dimethylphenol 105679 NA 7,400 20,000 7,600 NLV NLV NLV NLV 2.1E+9 3.6E+7 NA 2,6-Dimethylphenol 576261 NA 330 (M); 88 330 (M); 260 NA NLV NLV NLV NLV 5.9E+7 4.4E+5 NA 3,4-Dimethylphenol 95658 NA 330 (M); 200 580 500 NLV NLV NLV NLV 1.0E+8 1.0E+6 NA 1.0E+9 Dimethylsulfoxide 67685 NA 4.4E+6 1.3E+7 3.8E+6 NLV NLV NLV NLV 5.9E+8 (C,D) 1.8E+7 2,4-Dinitrotoluene 121142 NA 430 640 NA NLV NLV NLV NLV 2.0E+7 2.2E+5 NA

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Residential Nonresidential Groundwater Soil Source Drinking Drinking Surface Water Volatilization Volatile Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for VSIC for Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Contact Concentration Hazardous Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels 3.9E+5 Dinoseb 88857 NA 300 300 200 (M); 43 NLV NLV NLV NLV 1.2E+8 (C,DD) 1.4E+5 1,4-Dioxane (I) 123911 NA 1,700 7,000 56,000 (X) NLV NLV NLV NLV 7.1E+8 2.4E+6 9.7E+7 Diquat 85007 NA 400 400 400 NLV NLV NLV NLV ID 1.6E+6 NA Diuron 330541 NA 620 1,800 NA NLV NLV NLV NLV 2.1E+8 3.1E+6 NA Endosulfan (J) 115297 NA NLL NLL NLL ID ID ID ID ID 4.4E+6 NA Endothall 145733 NA NLL NLL NLL NLV NLV NLV NLV 1.0E+9 1.2E+7 NA Endrin 72208 NA NLL NLL NLL NLV NLV NLV NLV ID 1.9E+5 NA Epichlorohydrin (I) 106898 NA 100 100 NA 1.2E+5 37,000 37,000 37,000 2.9E+7 41,000 7.3E+6 1.0E+9 Ethanol (I) 64175 NA 3.8E+7 7.6E+7 ID NLV NLV NLV NLV 5.6E+11 (C,D,DDD) 1.1E+8 Ethyl acetate (I) 141786 NA 1.3E+5 3.8E+5 NA 7.0E+7 (C) 5.9E+7 5.9E+7 1.0E+8 9.4E+10 6.6E+8 (C) 7.5E+6 Ethyl-tert-butyl ether (ETBE) 637923 NA 980 980 ID 1.7E+6 (C) 2.3E+6 4.6E+6 1.1E+7 1.1E+10 ID 6.5E+5 Ethylbenzene (I) 100414 NA 1,500 1,500 360 4.6E+5 (C) 2.4E+6 3.1E+6 6.5E+6 1.3E+10 7.1E+7 (C) 1.4E+5 Ethylene dibromide 106934 NA 20 (M); 1.0 20 (M); 1.0 110 (X) 3,600 5,800 5,800 9,800 1.8E+7 430 8.9E+5 1.0E+9 Ethylene glycol 107211 NA 3.0E+5 8.4E+5 3.8E+6 (X) NLV NLV NLV NLV 2.9E+10 (C,D) 1.1E+8 Ethylene glycol monobutyl ether 111762 NA 74,000 2.0E+5 NA 1.4E+6 2.1E+7 1.5E+8 3.6E+8 3.8E+11 3.6E+8 (C) 4.1E+7 286 2017 MR 22 – December 15, 2017 Fluoranthene 206440 NA 7.3E+5 7.3E+5 5,500 1.0E+9 (D) 8.9E+8 8.8E+8 8.8E+8 4.1E+9 1.3E+8 NA Fluorene 86737 NA 3.9E+5 8.9E+5 5,300 1.0E+9 (D) 1.5E+8 1.5E+8 1.5E+8 4.1E+9 8.7E+7 NA Fluorine (soluble 6.7E+7 fluoride) (B) 7782414 NA 40,000 40,000 ID NLV NLV NLV NLV ID (DD) NA Formaldehyde 50000 NA 26,000 76,000 2,400 65,000 43,000 69,000 1.5E+5 2.6E+8 1.3E+8 (C) 6.0E+7 Formic acid 1.0E+9 (I,U) 64186 NA 2.0E+5 5.8E+5 ID 2.8E+6 2.6E+5 1.6E+5 1.6E+5 5.9E+7 (C,D) 1.1E+8 1- Formylpiperidine 2591868 NA 1,600 4,600 NA ID ID ID ID ID 8.0E+6 1.0E+7 Gentian violet 548629 NA 300 1,300 NA NLV NLV NLV NLV ID 4.4E+5 NA 5.7E+7 Glyphosate 1071836 NA NLL NLL NLL NLV NLV NLV NLV ID (DD) NA Heptachlor 76448 NA NLL NLL NLL 1.9E+6 2.1E+5 2.1E+5 2.1E+5 3.0E+6 23,000 NA Heptachlor epoxide 1024573 NA NLL NLL NLL NLV NLV NLV NLV 1.5E+6 9,500 NA 1.0E+9 n-Heptane 142825 NA 4.6E+7 (C) 1.3E+8 (C) NA 2.7E+6 (C) 2.5E+7 4.5E+7 1.0E+8 1.0E+11 (C,D) 2.4E+5

287 2017 MR 22 – December 15, 2017

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Nonresidential Surface Soil Source Drinking Drinking Water Volatilization to Volatile Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface Indoor Air Inhalation VSIC for VSIC for Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels Hexabromobenzene 87821 NA 5,400 5,400 ID ID ID ID ID ID 3.1E+6 NA Hexachlorobenzene (C-66) 118741 NA 1,800 1,800 350 2.2E+5 56,000 56,000 56,000 8.5E+6 37,000 NA Hexachlorobutadiene (C- 4.7E+5 46) 87683 NA 26,000 72,000 91 7.1E+5 (C) 4.6E+5 4.6E+5 4.6E+5 1.8E+8 (C) 3.5E+5 alpha- Hexachlorocyclohexane 319846 NA 18 71 ID 1.6E+5 41,000 86,000 86,000 2.1E+6 12,000 NA beta- Hexachlorocyclohexane 319857 NA 37 150 ID NLV NLV NLV NLV 7.4E+6 25,000 NA Hexachlorocyclopentadiene 6.7E+6 (C-56) 77474 NA 3.2E+5 3.2E+5 ID 56,000 60,000 60,000 60,000 5.9E+6 (C) 7.2E+5 Hexachloroethane 67721 NA 430 1,200 1,800 (X) 79,000 6.6E+5 1.4E+6 1.4E+6 1.0E+8 7.3E+5 NA 3.0E+8 n-Hexane 110543 NA 1.8E+5 (C) 5.1E+5 (C) NA 9.5E+5 (C) 3.5E+6 3.5E+6 6.4E+6 5.9E+9 (C) 44,000 1.0E+8 2-Hexanone 591786 NA 20,000 58,000 ID 1.8E+6 1.3E+6 1.3E+6 1.5E+6 1.2E+9 (C) 2.5E+6 Indeno(1,2,3-cd)pyrene (Q) 193395 NA NLL NLL NLL NLV NLV NLV NLV ID 80,000 NA Iron (B) 7439896 1.2E+7 6,000 6,000 NA NLV NLV NLV NLV ID 5.8E+8 NA 2.3E+8 Isobutyl alcohol (I) 78831 NA 46,000 1.3E+5 NA 4.3E+8 (C) 9.5E+7 9.5E+7 9.5E+7 4.4E+10 (C) 8.9E+6 2.2E+7 Isophorone 78591 NA 15,000 62,000 26,000 (X) NLV NLV NLV NLV 8.2E+9 (C) 2.4E+6 Isopropyl alcohol (I) 67630 NA 9,400 26,000 1.1E+6 (X) NLV NLV NLV NLV 6.5E+9 4.7E+7 1.1E+8 8.0E+7 Isopropyl benzene 98828 NA 91,000 2.6E+5 3,200 7.3E+5 (C) 2.0E+6 2.0E+6 3.0E+6 2.6E+9 (C) 3.9E+5 9.0E+5 Lead (B) 7439921 21,000 7.0E+5 7.0E+5 (G,X) NLV NLV NLV NLV 4.4E+7 (DD) NA 20 (M); Lindane 58899 NA 7.0 20 (M); 7.0 20 (M); 1.1 ID ID ID ID ID 42,000 NA 3.1E+7 Lithium (B) 7439932 9,800 3,400 7,000 8,800 NLV NLV NLV NLV 1.0E+9 (DD) NA

288 2017 MR 22 – December 15, 2017 1.0E+9 Magnesium (B) 7439954 NA 8.0E+6 2.2E+7 NA NLV NLV NLV NLV 2.9E+9 (D) NA Manganese (B) 7439965 4.4E+5 1,000 1,000 (G,X) NLV NLV NLV NLV 1.5E+6 9.0E+7 NA Mercury (Total) (B,Z) Varies 130 1,700 1,700 50 (M); 1.2 89,000 62,000 62,000 62,000 8.8E+6 5.8E+5 NA 8.4E+6 ug/m3 Methane 74828 NA ID ID NA (GG) ID ID ID ID ID ID 3.6E+8 Methanol 67561 NA 74,000 2.0E+5 1.2E+7 (C) 6.7E+7 (C) 3.7E+7 4.6E+7 9.7E+7 9.6E+10 (C) 3.1E+6 Methoxychlor 72435 NA 16,000 16,000 NA ID ID ID ID ID 5.6E+6 NA 2-Methoxyethanol (I) 109864 NA 150 420 NA NLV NLV NLV NLV 5.9E+8 7.3E+5 1.1E+8 2-Methyl-4- chlorophenoxyacetic acid 94746 NA 390 1,100 NA NLV NLV NLV NLV ID 7.3E+5 NA 830 (M); 2-Methyl-4,6-dinitrophenol 534521 NA 400 830 (M); 400 NA NLV NLV NLV NLV 5.9E+7 2.6E+5 NA

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Nonresidential Surface Soil Source Drinking Drinking Water Volatilization Volatile Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for VSIC for Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels N-Methyl-morpholine (I) 109024 NA 400 1,100 NA NLV NLV NLV NLV ID 2.0E+6 1.1E+8 Methyl parathion 298000 NA 46 130 NA NLV NLV NLV NLV ID 1.8E+5 NA 4-Methyl-2-pentanone (MIBK) (I) 108101 NA 36,000 1.0E+5 ID 6.9E+7 (C) 5.3E+7 5.3E+7 7.0E+7 6.0E+10 1.8E+8 (C) 2.7E+6 Methyl-tert-butyl ether (MTBE) 1634044 NA 800 800 1.4E+5 (X) 1.8E+7 (C) 3.0E+7 4.1E+7 8.9E+7 8.8E+10 7.1E+6 (C) 5.9E+6 Methylcyclopentane (I) 96377 NA ID ID NA 1.7E+5 2.8E+6 8.3E+6 2.0E+7 2.1E+10 ID 3.5E+5 4,4'-Methylene-bis-2- chloroaniline 101144 NA NLL NLL NLL NLV NLV NLV NLV 1.1E+8 32,000 NA Methylene chloride 75092 NA 100 100 30,000 (X) 2.4E+5 7.0E+5 1.7E+6 4.0E+6 8.3E+9 5.8E+6 (C) 2.3E+6 2-Methylnaphthalene 91576 NA 57,000 1.7E+5 4,200 4.9E+6 1.8E+6 1.8E+6 1.8E+6 2.9E+8 2.6E+7 NA 1,000 (M); Methylphenols (J) 1319773 NA 7,400 20,000 600 NLV NLV NLV NLV 2.9E+9 3.6E+7 NA 6.9E+6 Metolachlor 51218452 NA 4,800 20,000 300 NLV NLV NLV NLV ID (C,DD) 4.4E+5 Metribuzin 21087649 NA 3,600 10,000 NA ID ID ID ID ID 2.8E+7 NA Mirex 2385855 NA NLL NLL NLL ID ID ID ID ID 40,000 NA 289 2017 MR 22 – December 15, 2017 Molybdenum (B) 7439987 NA 1,500 4,200 64,000 (X) NLV NLV NLV NLV ID 9.6E+6 NA Naphthalene 91203 NA 35,000 1.0E+5 730 4.7E+5 3.5E+5 3.5E+5 3.5E+5 8.8E+7 5.2E+7 NA Nickel (B) 7440020 20,000 1.0E+5 1.0E+5 (G) NLV NLV NLV NLV 1.6E+7 1.5E+8 NA Nitrate (B,N) 14797558 NA 2.0E+5 (N) 2.0E+5 (N) ID NLV NLV NLV NLV ID ID NA Nitrite (B,N) 14797650 NA 20,000 (N) 20,000 (N) NA NLV NLV NLV NLV ID ID NA 330 (M); Nitrobenzene (I) 98953 NA 68 330 (M); 190 3,600 (X) 1.7E+5 64,000 64,000 64,000 2.1E+7 3.4E+5 4.9E+5 2-Nitrophenol 88755 NA 400 1,200 ID NLV NLV NLV NLV ID 2.0E+6 NA n-Nitroso-di-n- 330 (M); propylamine 621647 NA 100 330 (M); 100 NA NLV NLV NLV NLV 2.0E+6 5,400 1.5E+6 N-Nitrosodiphenylamine 86306 NA 5,400 22,000 NA NLV NLV NLV NLV 2.8E+9 7.8E+6 NA Oxamyl 23135220 NA 4,000 4,000 NA NLV NLV NLV NLV ID 2.8E+7 NA Oxo-hexyl acetate 88230357 NA 1,500 4,200 NA ID ID ID ID 2.4E+9 7.3E+6 1.0E+7 Pendimethalin 40487421 NA 1.1E+6 1.1E+6 NA NLV NLV NLV NLV ID 1.3E+8 NA Pentachlorobenzene 608935 NA 29,000 81,000 9,500 ID ID ID ID ID 9.3E+5 (C) 1.9E+5 Pentachloronitrobenzene 82688 NA 37,000 37,000 NA 2.2E+5 2.8E+5 2.8E+5 2.8E+5 1.5E+8 5.5E+6 NA

290 2017 MR 22 – December 15, 2017

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Groundwater Infinite Residential Nonresidential Surface Soil Source Drinking Drinking Water Volatilization Volatile Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for VSIC for Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels Pentachlorophenol 87865 NA 22 22 (G,X) NLV NLV NLV NLV 1.3E+8 3.2E+5 NA Pentane 109660 NA ID ID NA 1.8E+5 4.4E+7 3.4E+8 6.0E+8 5.3E+11 ID 2.4E+5 2-Pentene (I) 109682 NA ID ID NA ID ID ID ID ID ID 2.2E+5 Phenanthrene 85018 NA 56,000 1.6E+5 2,100 5.1E+6 1.9E+5 1.9E+5 1.9E+5 2.9E+6 5.2E+6 NA 2.3E+8 Phenol 108952 NA 88,000 2.6E+5 9,000 NLV NLV NLV NLV 1.8E+10 (C,DD) 1.2E+7 Phenytoin 57410 NA 830 3300 4300 (X) NLV NLV NLV NLV 2.8E+8 4.8E+5 NA Phosphorus (Total) 7723140 NA 1.3E+6 4.8E+6 (EE) NLV NLV NLV NLV 2.9E+7 1.0E+9 (D) NA 1.0E+9 Phthalic acid 88993 NA 2.8E+5 8.0E+5 NA NLV NLV NLV NLV ID (C,D) 1.7E+6 1.0E+9 Phthalic anhydride 85449 NA 3.0E+5 8.8E+5 NA NLV NLV NLV NLV ID (C,D) 1.1E+6 Picloram 1918021 NA 10,000 10,000 920 NLV NLV NLV NLV ID 5.1E+7 NA Piperidine 110894 NA 64 180 NA NLV NLV NLV NLV 4.1E+9 3.2E+5 1.2E+8 Polybrominated biphenyls (J) 67774327 NA NLL NLL NLL NLV NLV NLV NLV ID 4,800 NA Polychlorinated biphenyls (PCBs) (J,T) 1336363 NA NLL NLL NLL 1.6E+7 8.1E+5 2.8E+7 2.8E+7 6.5E+6 (T) NA Prometon 1610180 NA 4,900 14,000 NA NLV NLV NLV NLV ID 1.6E+7 NA Propachlor 1918167 NA 1,900 5,400 NA NLV NLV NLV NLV ID 9.5E+6 NA Propazine 139402 NA 4,000 11,000 NA NLV NLV NLV NLV ID 2.0E+7 NA 1.0E+9 Propionic acid 79094 NA 2.4E+5 7.0E+5 ID NLV NLV NLV NLV 8.8E+9 (C,D) 1.1E+8 Propyl alcohol (I) 71238 NA 28,000 80,000 NA NLV NLV NLV NLV 2.1E+10 7.4E+7 (DD) 1.1E+8 n-Propylbenzene (I) 103651 NA 1,600 4,600 ID ID ID ID ID 5.9E+8 8.0E+6 1.0E+7 1.0E+9 Propylene glycol 57556 NA 3.0E+6 8.4E+6 5.8E+6 NLV NLV NLV NLV 1.8E+11 (C,D) 1.1E+8 Pyrene 129000 NA 4.8E+5 4.8E+5 ID 1.0E+9 (D) 7.8E+8 7.8E+8 7.8E+8 2.9E+9 8.4E+7 NA Pyridine (I) 110861 NA 400 420 NA 2,000 9,800 40,000 97,000 1.0E+8 7.3E+5 (C) 37,000 291 2017 MR 22 – December 15, 2017 Selenium (B) 7782492 410 4,000 4,000 400 NLV NLV NLV NLV 5.9E+7 9.6E+6 NA Silver (B) 7440224 1,000 4,500 13,000 100 (M); 27 NLV NLV NLV NLV 2.9E+6 9.0E+6 NA Silvex (2,4,5-TP) 93721 NA 3,600 3,600 2,200 NLV NLV NLV NLV ID 5.5E+6 NA Simazine 122349 NA 80 80 340 NLV NLV NLV NLV ID 3.8E+6 NA Sodium 17341252 NA 4.6E+6 7.0E+6 NA NLV NLV NLV NLV ID 1.0E+9 (D) NA

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Groundwater Source Residential Nonresidential Surface Soil Volatile Drinking Drinking Water Volatilization Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for VSIC for Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels Sodium azide 26628228 NA 1,800 5,000 1,000 ID ID ID ID ID 8.7E+6 NA Strontium (B) 7440246 NA 92,000 2.6E+5 4.2E+5 NLV NLV NLV NLV ID 1.0E+9 (D) NA Styrene 100425 NA 2,700 2,700 2,100 (X) 1.3E+6 (C) 3.3E+6 3.3E+6 4.2E+6 6.9E+9 1.9E+6 (C) 5.2E+5 Sulfate 14808798 NA 5.0E+6 5.0E+6 NA NLV NLV NLV NLV ID ID NA Tebuthiuron 34014181 NA 10,000 30,000 NA NLV NLV NLV NLV ID 2.7E+7 (DD) NA 2,3,7,8- Tetrabromodibenzo-p- dioxin (O) 50585416 NA NLL NLL NLL NLV NLV NLV NLV (O) (O) NA 1,2,4,5- Tetrachlorobenzene 95943 NA 1.5E+6 1.5E+6 3,400 (X) 1.1E+6 2.7E+5 2.7E+5 2.7E+5 2.9E+7 2.5E+8 NA 2,3,7,8- Tetrachlorodibenzo-p- dioxin (O) 1746016 NA NLL NLL NLL NLV NLV NLV NLV 59 (O) 0.99 (O) NA 1,1,1,2- Tetrachloroethane 630206 NA 1,500 6,400 ID 33,000 1.2E+5 2.1E+5 3.3E+5 5.3E+8 2.2E+6 (C) 4.4E+5 1,1,2,2- Tetrachloroethane 79345 NA 170 700 1,600 (X) 23,000 34,000 34,000 34,000 6.8E+7 2.4E+5 8.7E+5 Tetrachloroethylene 127184 NA 100 100 1,200 (X) 21,000 2.1E+5 4.9E+5 1.1E+6 1.2E+9 9.3E+5 (C) 88,000 Tetrahydrofuran 109999 NA 1,900 5,400 2.2E+5 (X) 2.4E+6 1.5E+7 6.7E+7 1.6E+8 1.7E+11 9.5E+6 1.2E+8 500 (M); Tetranitromethane 509148 NA ID ID NA 600 180 ID ID 2.6E+5 ID ID Thallium (B) 7440280 NA 2,300 2,300 4,200 (X) NLV NLV NLV NLV 5.9E+6 1.3E+5 NA Toluene (I) 108883 NA 16,000 16,000 5,400 6.1E+5 (C) 3.3E+6 3.6E+7 3.6E+7 1.2E+10 1.6E+8 (C) 2.5E+5 p-Toluidine 106490 NA 660 (M); 1,200 NA NLV NLV NLV NLV 1.3E+8 4.3E+5 1.2E+6 292 2017 MR 22 – December 15, 2017 300 Toxaphene 8001352 NA 24,000 24,000 8,200 NLV NLV NLV NLV 1.2E+7 85,000 NA Triallate 2303175 NA 95,000 2.7E+5 (C) NA ID ID ID ID ID 9.5E+6 (C) 2.5E+5 Tributylamine 102829 NA 7,800 23,000 ID 1.1E+6 7.2E+5 7.2E+5 7.2E+5 2.1E+8 2.6E+6 3.7E+6 5.8E+6 1,2,4-Trichlorobenzene 120821 NA 4,200 4,200 5,900 (X) 1.8E+7 (C) 3.4E+7 3.4E+7 3.4E+7 1.1E+10 (C,DD) 1.1E+6 1.0E+9 1,1,1-Trichloroethane 71556 NA 4,000 4,000 1,800 4.6E+5 4.5E+6 1.5E+7 3.1E+7 2.9E+10 (C,D) 4.6E+5 1,1,2-Trichloroethane 79005 NA 100 100 6,600 (X) 24,000 57,000 57,000 1.2E+5 2.5E+8 8.4E+5 9.2E+5 6.6E+5 Trichloroethylene 79016 NA 100 100 4,000 (X) 1,900 14,000 25,000 58,000 5.9E+7 (C,DD) 5.0E+5 Trichlorofluoromethane 75694 NA 52,000 1.5E+5 NA 5.1E+6(C) 1.1E+8 1.4E+11 1.4E+11 1.7E+12 2.6E+8 (C) 5.6E+5 2,4,5-Trichlorophenol 95954 NA 39,000 1.1E+5 NA NLV NLV NLV NLV 1.0E+10 7.3E+7 NA 330 (M); 2,4,6-Trichlorophenol 88062 NA 2,400 9,400 100 NLV NLV NLV NLV 1.3E+9 3.3E+6 NA

293 2017 MR 22 – December 15, 2017

TABLE 3. SOIL: NONRESIDENTIAL PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS; All criteria, unless otherwise noted, are expressed in units of parts per billion (ppb). One ppb is equivalent to 1 microgram per kilogram (ug/kg). Criteria with 6 or more digits are expressed in scientific notation. For example, 200,000 is presented as 2.0E+5. A footnote is designated by a letter in parentheses and is explained in the footnote pages that follow the criteria tables. When the risk-based criterion is less than the target detection limit (TDL), the TDL is listed as the criterion (§324.20120a(10)). In these cases, 2 numbers are present in the cell. The first number is the criterion (i.e., TDL), and the second number is the risk-based value. Groundwater Protection Indoor Air Ambient Air (Y) (C) Contact Csat Infinite Groundwater Source Residential Nonresidential Surface Soil Volatile Drinking Drinking Water Volatilization Soil Finite Finite Particulate Soil Chemical Statewide Water Water Interface to Indoor Air Inhalation VSIC for VSIC for Soil Direct Saturation Abstract Default Protection Protection Protection Inhalation Criteria 5 Meter 2 Meter Inhalation Contact Concentration Service Background Criteria & Criteria & Criteria & Criteria & (VSIC) & Source Source Criteria & Criteria & Screening Hazardous Substance Number Levels RBSLs RBSLs RBSLs RBSLs RBSLs Thickness Thickness RBSLs RBSLs Levels 1,2,3-Trichloropropane 96184 NA 840 2,400 NA 7,500 11,000 11,000 12,000 8.8E+6 4.2E+6 (C) 8.3E+5 1,1,2-Trichloro-1,2,2- 1.0E+9 trifluoroethane 76131 NA 9.0E+6 (C) 9.0E+6 (C) 1,700 9.3E+6 (C) 2.1E+8 8.9E+8 2.1E+9 2.3E+12 (C,D) 5.5E+5 Triethanolamine 102716 NA 74,000 2.0E+5 NA NLV NLV NLV NLV 1.5E+9 3.6E+8 (C) 1.1E+8 2.3E+8 Triethylene glycol 112276 NA 86,000 2.4E+5 (C) NA NLV NLV NLV NLV ID (C,DD) 1.1E+5 3-Trifluoromethyl-4- nitrophenol 88302 NA 1.1E+5 3.1E+5 NA NLV NLV NLV NLV ID 2.4E+8 (DD) NA Trifluralin 1582098 NA 1.9E+5 5.7E+5 NA ID ID ID ID ID 5.7E+6 NA 2,2,4-Trimethyl pentane 540841 NA ID ID NA 2.0E+5 (C) 6.3E+6 4.0E+7 9.6E+7 1.0E+11 ID 19,000 2,4,4-Trimethyl-2-pentene (I) 107404 NA ID ID NA ID ID ID ID ID ID 56,000 1,2,4-Trimethylbenzene (I) 95636 NA 2,100 2,100 570 8.0E+6 (C) 2.5E+7 6.0E+8 6.0E+8 3.6E+10 1.0E+8 (C) 1.1E+5 1,3,5-Trimethylbenzene (I) 108678 NA 1,800 1,800 1,100 4.8E+6 (C) 1.9E+7 4.6E+8 4.6E+8 3.6E+10 1.0E+8 (C) 94,000 Triphenyl phosphate 115866 NA 1.5E+6 (C) 1.8E+6 (C) NA NLV NLV NLV NLV ID 1.2E+8 (C) 1.1E+5 tris(2,3- Dibromopropyl)phosphate 126727 NA 930 930 ID 4.3E+5 (C) 60,000 60,000 60,000 7.4E+6 20,000 27,000 Urea 57136 NA ID ID NA NLV NLV NLV NLV ID ID NA Vanadium 7440622 NA 72,000 9.9E+5 4.3E+5 NLV NLV NLV NLV ID 5.5E+6 (DD) NA 3.4E+7 Vinyl acetate (I) 108054 NA 13,000 36,000 NA 1.5E+6 2.0E+6 2.7E+6 5.9E+6 5.9E+9 (C,DD) 2.4E+6 Vinyl chloride 75014 NA 40 40 260 (X) 2,800 29,000 1.7E+5 4.2E+5 8.9E+8 34,000 4.9E+5 White phosphorus (R) 12185103 NA 2.2 6 NA NLV NLV NLV NLV ID 17,000 (DD) NA 1.0E+9 Xylenes (I) 1330207 NA 5,600 5,600 820 1.2E+7 (C) 5.4E+7 6.5E+7 1.3E+8 1.3E+11 (C,D) 1.5E+5 Zinc (B) 7440666 47,000 2.4E+6 5.0E+6 (G) NLV NLV NLV NLV ID 6.3E+8 NA

294 2017 MR 22 – December 15, 2017 R 299.49 Footnotes for generic cleanup criteria tables. Rule 49. (1) The footnotes that apply to the generic criteria tables in R 299.44, R 299.46, and R 299.48 are as follows: (A) Criterion is the state of Michigan drinking water standard established pursuant to section 5 of 1976 PA 399, MCL 325.1005. The state drinking water standards are in units of milligam per liter (mg/l) of water. (B) Background, as defined in R 299.1(b) section 20101(1)(e) of the act, may be substituted if higher it has a greater numeric value than the calculated cleanup criterion. Background levels may be less than criteria for some inorganic compounds. (C) The criterion developed under R 299.20 to R 299.267 exceeds the chemical-specific soil saturation screening level (Csat). The person proposing or implementing response activity shall document whether additional response activity is required to control free-phase liquids or NAPL to protect against risks associated with free-phase liquidsNAPL by using methods appropriate for the free-phase liquidsNAPL present. Development of a site-specific Csat or methods presented in R 299.22, R 299.24(5), and R 299.26(8) may be conducted for the relevant exposure pathways. (D) Calculated criterion health-based soil value exceeds 100 percent% by dry weight, hence it is reduced to the maximum ceiling concentration of 100 percent% or 1.0E+98 parts per billion (ppb). (E) Criterion is the aesthetic drinking water value, as required by section 20120a(5) of the Natural Resources and Environmental Protection Act, 1994 PA 451, as amended (NREPA)act. The criteria based on national secondary drinking water levels are in units of milligram per liter (mg/l) of water. A notice of aesthetic impact may be employedused as an institutional control mechanismland or resource use restriction if groundwater concentrations exceed the aesthetic drinking water criterion, but do not exceed the applicable health-based drinking water value provided in the following table:

Aesthetic Residential Non-Residential Chemical Hazardous Substance Abstract Drinking Health-Based Health-Based Service Water Drinking Water Drinking Water CAS Number Value Value* Value µg/L µg/L µg/L

Aluminum 7429905 50 3004,000 (V) 4,100 16,000 (V) tertiary-Amyl methyl ether (TAME) 994058 190 910770 2,6002,400 Copper 7440508 1,000 1,40030 4,00095 Chloride 16887006 2.5E+5 NA NA Diethyl ether 60297 5.0 (M); 1.2 3,7001,200 10,0003,800 Ethyl-tert-butyl ether (ETBE) 637923 49 550 1,700 Ethylbenzene 100414 74 70066 700330 Fluorine (soluble floride) 7782414 1,700 (S) 1,200 1,700 (S) Iron 7439896 300 2,0004,200 5,60013,000 Manganese 7439965 50 860700 2,5002,200 Methyl-tert-butyl ether (MTBE) 1634044 40 240210 6901,100 Silver 7440224 100 5.9 19 Sulfate 14808798 2.5E+5 NA NA Toluene 108883 790 1,000470 1,0001,500 Total Dissolved Solids NA 5.0E+5 NA NA 1,2,3-Trimethylbenzene 526738 130 60 190 1,2,4-Trimethylbenzene 95636 63 1,00060 2,900190 1,3,5-Trimethylbenzene 108678 72 1,00060 2,900190

Xylenes 1330207 280 10,0001,200 10,0003,800 Zinc 7440666 5,000 1,800 5,700 For this comparison all values are in units of micrograms per liter (µg/L).

295 2017 MR 22 – December 15, 2017

(F) Criterion is based on adverse impacts to plant life and phytotoxicity. Boron drinking water criteria listed are health-based values and do not protect for adverse impacts to plant life and phytotoxicity from irrigation water. Pursuant to R 299.28, when irrigation water is a reasonable and relevant use of groundwater the potential for phytotoxicity and injury to the groundwater resource that may impair its use for irrigation require consideration. The department has determined 500 µg/L is necessary to address the risks to plant life and groundwater resources not otherwise accounted for with the generic criterion. Boron soil criteria protective of drinking water are based upon adverse impacts to plant life and phytotoxicity from soil conditions. The boron phytotoxicity values are not calculated using the generic equations and generic input values for the pathway-specific rules. (G) Groundwater surface water interface (GSI) criterion depends on the pH or water hardness, or both, of the receiving surface water. The final chronic value (FCV) for the protection of aquatic life shall be calculated based on the pH or hardness of the receiving surface water. Where water hardness exceeds 400 mg CaCO3/L, use 400 mg CaCO3/L for the FCV calculation. The FCV formula provides values in units of ug/L or ppb. The generic GSI criterion is the lesser of the calculated FCV, the wildlife value (WV), and the surface water human non-drinking water value (HNDV). The soil GSI protection criteria for these hazardous substances are the greater of the 20 times the GSI criterion or the GSI soil-water partition values using the GSI criteria developed with the procedure described in this footnote.

FCV Formula WV HNDV Hazardous Substance FCV Conversion Factor (CF) where, ug/L ug/L ug/L Acetate EXP(0.2732*×(pH) + 7.0362) NA NA 1.3E+6

Acetic Acid EXP(0.2732*×(pH) + 7.0362) NA NA 1.3E+6

Barium EXP(1.0629*×(LnH)+1.1869) NA NA 1.6E+5

Beryllium EXP(2.5279*×(LnH)-10.7689) NA NA 1,200

FCV Formula WV HNDV Hazardous Substance FCV Conversion Factor (CF) ug/L ug/L ug/L

Cadmium (EXP(0.7852*×(LnH)-2.715))*×CF 1.101672-((LnH)*×(0.041838)) NA 130

Chromium (total)  (EXP(0.819*×(LnH)+0.6848))*×CF 0.86 NA 9,400

Copper (EXP(0.8545*×(LnH)-1.702)) *×CF 0.96 NA 38,000

Lead (EXP(0.9859*×(LnH)-1.270))*×CF 1.46203-((LnH)*×(0.14571)) NA 190

Manganese EXP(0.8784*×(LnH)+3.5385) NA NA 59,000

Nickel (EXP(0.846*×(LnH)+0.0584))*×CF 0.997 NA 2.1E+5

Pentachlorophenol EXP(1.005*×(pH)-5.134) NA NA 2.8

Zinc (EXP(0.8473*×(LnH)+0.884))*×CF 0.986 NA 16,000 EXP(x) = The base of the natural logarithm raised to power x (ex). LnH = The natural logarithm of water hardness in mg CaCO3/L. * = The multiplication symbol.  = The GSI criterion developed here may not be protective for surface water that is used as a drinking 296 2017 MR 22 – December 15, 2017 water source. Refer to footnote (X) for further guidance.

A spreadsheet that may be used to calculate GSI and GSI protection criteria for (G)-footnoted hazardous substances is available on the Department of Environmental Quality (DEQ) internet web site. The mutagenic cancer health-based values for trichloroethylene are not calculated using the toxicological input values shown in the tables of R 299.50 without adjustments. These values are calculated using cancer adjustment factors (CAF) and mutagenic adjustment factors (MAF) to adjust the cancer potency values for combined risk for mutagenic and non-mutagenic cancer effects.

Mutagenic health-based values: CAF MAF Adult-based cancer potency values Ingestion and dermal 0.804 0.202 Cancer Slope Factor = (Drinking Water Value; 4.6E-2 ((mg/kg-day)-1) Direct Contact Value) Inhalation 0.756 0.244 Inhalation Unit Risk Factor = (Acceptable Air Value; 4.1E-6 ((µg/kg-day)-1) Volatilization to Indoor Air Value; Particulate Soil Inhalation Value)

(H) Valence-specific chromium data (Cr III and Cr VI) shall be compared to the corresponding valence-specific cleanup criteria for soil. If both Cr III and Cr VI are present in groundwater, tThe total concentration of both chromium cannot exceed the drinking water criterion of 1000.1 ug/Lmg/L. If analytical data are provided for total chromium only, they shall be compared to the cleanup criteria for Cr VI. Cr III soil cleanup criterion for protection of drinking water can only be used at sites where groundwater is prevented from being used as a public water supply, currently and in the future, through an approved land or resource use restriction. (I) Hazardous substance may exhibit the characteristic of ignitability as defined 40 C.F.R. §261.21 (revised as of July 1, 2001), which is adopted by reference in these rules. and is available for inspection at the DEQ, 525 West Allegan Street, Lansing, Michigan. Copies of the regulation may be purchased, at a cost as of the time of adoption of these rules of $45, from the Superintendent of Documents, Government Printing Office, Washington, DC 20401 (stock number 869-044-00155-1), or from the DEQ, Remediation and Redevelopment Division (RRD), 525 West Allegan Street, Lansing, Michigan 48933, at cost under part 111 of the act in R 299.9212(1). (J) Hazardous substance may be present in several isomer forms. Isomer-specific concentrations shall be added together for comparison to criteria. (K) Hazardous substance may be flammable or explosive, or both. (L) Drinking water, soils protective of drinking water, and direct contact Ccriteria for lead are derived using a biologically based model, as allowed for under section 20120a(9) of the NREPAact, and are not calculated using the algorithmsequations and generic input values in pathway-specific rules. While the derivation for the criteria is not the generic developmental equations, the basis for the criteria is the developmental effects of lead. A higher concentration than the generic residential drinking water criterion of 1 µg/l, up to 3 µg/l, may be allowed as a site- specific remedy and still allow for residential drinking water use, under sections 20120a(2) and 20120b of the act, if soil concentrations are appropriately lower than 190 mg/kg. A higher concentration than the generic nonresidential drinking water criterion of 1 µg/l, up to 10 µg/l, may be allowed as a site-specific remedy and still allow for nonresidential drinking water use, under sections 20120a(2) and 20120b of the act, if soil concentrations are appropriately lower than 760 mg/kg. If a site-specific criterion is approved based on this subdivision, a notice shall be filed on the deed for all property where the groundwater concentrations will exceed 1 µg/l to provide notice of the potential for unacceptable risk if soil or groundwater concentrations increase. Total lead and both fine and coarse lead fractions analysis may be required for comparison to lead soil criteria.The generic residential drinking water criterion of 4 ug/L is linked to the generic residential soil direct contact criterion of 400 mg/kg. A higher concentration in the drinking water, up to the state action level of 15 ug/L, may be allowed as a site-specific remedy and still allow for drinking water use, under Section 20120a(2) and 20120b of the NREPA if soil concentrations are appropriately lower than 400 mg/kg. If a site-specific criterion is approved based on this 297 2017 MR 22 – December 15, 2017 subdivision, a notice shall be filed on the deed for all property where the groundwater concentrations will exceed 4 ug/L to provide notice of the potential for unacceptable risk if soil or groundwater concentrations increase. Acceptable combinations of site-specific soil and drinking water concentrations are presented in the following table: Acceptable Combinations of Lead in Drinking Water and Soil Drinking Water Concentration Soil Concentration (ug/L) (mg/kg) 5 386-395 6 376-385 7 376-385 8 366-375 9 356-365 10 346-355 11 336-345 12 336-345 13 326-335 14 316-325 15 306-315 (M) Calculated criterion health-based value is below the analytical target detection limit, therefore, the criterion defaults to the target detection limit is the criterion. The target detection limit is established specific for an individual environmental medium. The volatilization to indoor air pathway is evaluated using criterion for soil, groundwater, and vapor pursuant to R 299.27. When a volatilization to indoor air criterion is the target detection limit for 1 or more medium, further evaluation of the remaining media shall demonstrate compliance for the pathway. (N) The concentrations of all potential sources of nitrate-nitrogen (e.g., ammonia-N, nitrite-N, and nitrate-N) in groundwater that is used as a source of drinking water shall not, when added together, exceed the nitrate drinking water criterion of 10,000 ug/Lmg/L. Where leaching to groundwater is a relevant pathway, soil concentrations of all potential sources of nitrate-nitrogen shall not, when added together, exceed the nitrate drinking water protection criterion of 2.0E+5 uµg/kg. (O) The concentration of all polychlorinated and polybrominated dibenzodioxin and dibenzofuran isomersand polychlorinated biphenyl congeners listed in the table below present at a facility, expressed as an equivalent concentration of 2,3,7,8-tetrachlorodibenzo-p-dioxin based upon their relative potency toxicity equivalence factors (TEF), shall be added together and compared to the criteria for 2,3,7,8-tetrachlorodibenzo-p-dioxin. Soil direct contact criteria for these hazardous substances are not protective for the human consumption of eggs from chickens with access to soil at these concentrations. In addition, the soil direct contact criteria may not be protective for other livestock products raised or produced on soils at these concentrations. Exposure from livestock products is an injury which requires consideration pursuant to R 299.28. The generic cleanup criteria for 2,3,7,8- tetrachlorodibenzo-p-dioxin are not calculated according to the algorithms presented in R 299.14 to R 299.26. The generic cleanup criteria are being held at the values that the DEQ has used since August 1998, in recognition of the fact that national efforts to reassess risks posed by dioxin are not yet complete. Until these studies are complete, it is premature to select a revised slope factor and/or reference dose for calculation of generic cleanup criteria. Toxicity equivalence factors for dibenzodioxins, dibenzofurans, and dioxin-like polychlorinated biphenyls are identified as follows:

Dioxin Congener CAS Number TEF 2,3,7,8-TCDD 1746016 1.0 1,2,3,7,8-PeCDD 40321764 1.0 1,2,3,4,7,8-HxCDD 39227286 0.1 1,2,3,6,7,8-HxCDD 57653857 0.1 1,2,3,7,8,9-HxCDD 19408743 0.1 1,2,3,4,6,7,8-HpCDD 35822469 0.01 1,2,3,4,6,7,8,9-OCDD 3268879 0.0003

298 2017 MR 22 – December 15, 2017 Furan Congener CAS Number TEF 2,3,7,8-TCDF 51207319 0.1 1,2,3,7,8-PeCDF 57117416 0.03 2,3,4,7,8-PeCDF 57117314 0.3 1,2,3,4,7,8-HxCDF 70648269 0.1 1,2,3,6,7,8-HxCDF 57117449 0.1 1,2,3,7,8,9-HxCDF 72918219 0.1 2,3,4,6,7,8-HxCDF 60851345 0.1 1,2,3,4,6,7,8-HpCDF 67562394 0.01 1,2,3,4,7,8,9-HpCDF 55673897 0.01 1,2,3,4,5,7,7,9-OCDF 39001020 0.0003

PCB Congener CAS Number TEF 3,3,4,4’-TCB (77) 32598133 0.0001 3,4,4’,5-TCB (81) 70362604 0.0003 3,3’,4,4’,5-PeCB (126) 57465288 0.1 3,3’,4,4’,5,5’,-HxCB (169) 32774166 0.03 2,3,3’,4,4’-PeCB (105) 32598144 0.00003 2,3,4,4’,5-PeCB (114) 74472370 0.00003 2,3,4,4’,5-PeCB (118) 31508006 0.00003 2’,3,4,4’5-PeCB (123), 65510443 0.00003 2,3,3’,4,4’,5-HxCB (156) 38380084 0.00003 2,3,3’,4,4’,5-HxCB (157) 69782907 0.00003 2,3,4,4’,5,5’-HxCB (167) 52663726 0.00003 2,3,3’,4,4’,5,5’,-HxCB (189) 39635319 0.00003

(P) Amenable cyanide methods or method OIA-1677 shall be used to quantify cyanide concentrations for compliance with all groundwater criteria. Total cyanide methods or method OIA-1677 shall be used to quantify cyanide concentrations for compliance with soil criteria. The generic cleanup criteria consider different chemical species of cyanide. The generic criteria presented in the criteria tables represent the lower of the values calculated for each chemical species of cyanide for a pathway. The residential direct contact criterion for cyanide is also protective of acute toxicity resulting in fatality; therefore, the concentrations of individual discrete samples are required for comparison to this criterion. Nonresidential direct contact criteria may not be protective of the potential for release of hydrogen cyanide gas. Additional land or resource use restrictions may be necessary to protect for the acute inhalation concerns associated with hydrogen cyanide gas. (Q) Criteria for carcinogenic polycyclic aromatic hydrocarbons were developed using relative potential potencies to benzo(a)pyrene. The soil direct contact criteria for the carcinogenic polynuclear aromatic hydrocarbons (cPAH) are developed using the oral cancer slope factor (SFo) for benzo(a)pyrene. The soil concentration of each cPAH detected at a facility shall be expressed as its equivalent concentration of benzo(a)pyrene by multiplying the soil concentration by its respective benzo(a)pyrene relative potency factor (RPF). All RPF-adjusted cPAH soil concentrations shall then be added together and the total RPF-adjusted cPAH soil concentration compared to the applicable soil direct contact criterion for benzo(a)pyrene. Compliance with cPAH groundwater and soil criteria, other than soil direct contact criteria, are not based on the RPF-cumulative approach because the final benzo(a)pyrene criteria for these pathways are not based on a cancer endpoint. The drinking water criteria for benzo(a)pyrene are based on the state drinking water standard and the particulate soil inhalation criteria are based on noncancer, developmental endpoints. The drinking water criteria for the other cPAHs are developed using the

299 2017 MR 22 – December 15, 2017 RPF-adjusted SFo for benzo(a)pyrene and are presented individually in the groundwater criteria table. The particulate soil inhalation criteria for the other cPAHs are developed using the RPF- adjusted inhalation unit risk factor (IURF) for benzo(a)pyrene and are presented individually in the soil criteria tables. The cPAHs, their benzo(a)pyrene RPFs, and their respective RPF-based toxicity values are presented in the following table. The SFo and IURF values are the cancer endpoints for benzo(a)pyrene adjusted by the respective RPFs for the other cPAHs.

Carcinogenic PAH CAS Number RPF SFo IURF Benzo(a)pyrene 50328 1.0 1.0E+0 6.0E-4 Benzo(a)anthracene 56553 0.1 1.0E-1 6.0E-5 Benzo(b)fluoranthene 205992 0.1 1.0E-1 6.0E-5 Benzo(k)fluoranthene 207089 0.01 1.0E-2 6.0E-6 Chrysene 218019 0.001 1.0E-3 6.0E-7 Dibenz(a,h)anthracene 53703 1.0 1.0E+0 6.0E-4 Indeno(1,2,3-cd)pyrene 193395 0.1 1.0E-1 6.0E-5

(R) Hazardous substance may exhibit the characteristic of reactivity as defined 40 C.F.R. §261.23 (revised as of July 1, 2001), which is adopted by reference in these rules. and is available for inspection at the DEQ, 525 West Allegan Street, Lansing, Michigan. Copies of the regulation may be purchased, at a cost as of the time of adoption of these rules of $45, from the Superintendent of Documents, Government Printing Office, Washington, DC 20401 (stock number 869-044-00155-1), or from the DEQ, RRD, 525 West Allegan Street, Lansing, Michigan 48933, at cost under part 111 of the act in R 299.9212(3). (S) Criterion defaults to Calculated health-based value exceeds the hazardous substance-specific water solubility limit, therefore, the water solubility limit is the criterion. (T) Refer to the federal Toxic Substances Control Act (TSCA), 40 C.F.R. §761, Subpart D and 40 C.F.R. §761, Subpart G, to determine the applicability of TSCA cleanup standards. Subpart D and Subpart G of 40 C.F.R. §761 (July 1, 2001 September 29, 2014) are adopted by reference in these rules and are available for inspection at the Michigan Department of Environmental Quality (MDEQ), 525 West Allegan Street, Lansing, Michigan. Copies of the regulations may be purchased, at a cost as of the time of adoption of these rules of $55, from the Superintendent of Documents, Government Printing Office, Washington, DC 20401, or from the MDEQ, RRD, 525 West Allegan Street, Lansing, Michigan 48933, at cost. Alternatives to compliance with the TSCA standards listed below are possible under 40 C.F.R. §761 Subpart D. New releases may be subject to the standards identified in 40 C.F.R. §761, Subpart G. Use Part 201the soil direct contact cleanup criteria in the following table if TSCA standards are not applicable.

Part 201 Soil Direct TSCA, Subpart D Land Use Category Contact Cleanup Standards Cleanup Criteria 4,000 1,000 ppbµg/kg, or Residential 1,900 10,000 ppbµg/kg if capped ppbµg/kg 1,000 ppbµg/kg, or 16,000 Nonresidential 20,000 10,000 ppbµg/kg if capped ppbµg/kg

(U) Hazardous substance may exhibit the characteristic of corrosivity as defined 40 C.F.R. §261.22 (revised as of July 1, 2001), which is adopted by reference in these rules. and is available for inspection at the DEQ, 525 West Allegan Street, Lansing, Michigan. Copies of the regulation may be purchased, at a cost as of the time of adoption of these rules of $45, from the Superintendent of Documents, Government Printing Office, Washington, DC 20401 (stock number 869-044-00155-1), or from the DEQ, RRD, 525 West Allegan Street,

300 2017 MR 22 – December 15, 2017 Lansing, Michigan 48933, at cost under part 111 of the act in R 299.9212(2), as it may result in an aqueous mixture that has a pH less than or equal to 2 or greater than or equal to 12.5. (V) Criterion is the aesthetic drinking water value as required by section 20120(a)(5) of the NREPAact. Concentrations up to 200 ug/Lµg/L may be acceptable, and still allow for drinking water use, as part of an unrestricted site-specific cleanup under sections 20120a(2) and 20120b of the NREPAact. (W) Concentrations of trihalomethanes disinfection by-products in groundwater shall be added together to determine compliance with the Michigan drinking water standard of 80 ug/Lµg/L. Concentrations of trihalomethanes in soil shall be added together to determine compliance with the drinking water protection criterion of 1,600 uµg/kg. The trihalomethanes are: bromodichloromethane (CAS No. 75274), bromoform (CAS No. 75252), chloroform (CAS No. 67663), and dibromochloromethane (CAS No. 74953). (X) The GSI criterion shown in the generic cleanup criteria tables is not protective for surface water that is used as a drinking water source. For a groundwater discharge to the Great Lakes and their connecting waters or discharge in close proximity to a water supply intake in inland surface waters, the generic GSI criterion shall be the surface water human drinking water value (HDV) listed in the table in this footnote, except for those HDV indicated with an asterisk. For HDV with an asterisk, the generic GSI criterion shall be the lowest of the HDV, the WV, and the calculated FCV. See formulas in footnote (G). Soil protection criteria based on the HDV shall be as listed in the table in this footnote, except for those values with an asterisk. Soil GSI protection criteria based on the HDV shall be as listed in the table in this footnote, except for those values with an asterisk. Soil GSI protection criteria for compounds with an asterisk shall be the greater of 20 times the GSI criterion or the GSI soil-water partition values using the GSI criteria developed with the procedure described in this footnote.

Surface Water Human Soil GSI Protection Chemical Drinking Water Values Criteria Abstract (HDV) for HDV Hazardous Substance Service (ug/L) (µug/kg) Number Acrylamide 79061 0.5 (M); 0.12 10 Alachlor 15972608 3.5 88 Antimony 7440360 2.0 (M); 1.7 1,200 Benzene 71432 12 240 Boron 7440428 4,000 80,000 Bromate 15541454 10 (M); 0.5 200 n-Butanol 71363 3,500 70,000 Butyl benzyl phthalate 85687 6.9 13,000 Cadmium 7440439 2.5* * Carbon tetrachloride 56235 5.6 110 Chloride 16887006 50,000 1.0E+6 Chloroethane 75003 170 3,400 Chromium (III) 16065831 120* * Cyanazine 21725462 2.0 (M); 0.93 200 (M); 40 1,2-Dichloroethane 107062 6.0 120 trans-1,2-Dichloroethylene 156605 470 9,400 1,2-Dichloropropane 78875 9.1 180 1,3-Dichloropropene 542756 3.3 100 (M); 66 N,N-Dimethylacetamide 127195 700 14,000 1,4-Dioxane 123911 34 680 Ethylene dibromide 106934 0.17 20 (M); 3.4 Ethylene glycol 107211 56,000 1.1E+6 Hexachloroethane 67721 5.3 310 Isophorone 78591 310 6,200 Isopropyl alcohol 67630 28,000 5.6E+5 Lead 7439921 14* * Manganese 7439965 1,300* * Methanol 67561 14,000 2.8E+5 Methyl-tert-butyl ether (MTBE) 1634044 100 2,000 Methylene chloride 75092 47 940 301 2017 MR 22 – December 15, 2017

Surface Water Human Soil GSI Protection Chemical Drinking Water Values Criteria Abstract (HDV) for HDV Hazardous Substance Service (ug/L) (µug/kg) Number Molybdenum 7439987 120 2,400 Nitrobenzene 98953 4.7 330 (M); 94 Pentachlorophenol 87865 1.8* * Styrene 100425 20 530 1,2,4,5-Tetrachlorobenzene 95943 2.8 3,300 1,1,2,2-Tetrachloroethane 79345 3.2 64 Tetrachloroethylene 127184 11 220 Tetrahydrofuran 109999 350 7,000 Thallium 7440280 2.0 (M); 1.2 1,400 1,2,4-Trichlorobenzene 120821 80 4,700 1,1,2-Trichloroethane 79005 12 240 Trichloroethylene 79016 29 580 Vinyl chloride 75014 1.0 (M); 0.25 40 (M); 20 The lower explosive level represents a % by volume in air, at room temperature unless noted otherwise in the source document identified in table 3 of R 299.50. (Y) Source size modifiers shown in the following table shall be used to determine soil inhalation criteria for ambient air when the source size is not one-half1/2 acre. The modifier shall be multiplied by the generic soil inhalation criteria shown in the table of generic cleanup criteria shall be multiplied by the modifier to determine the applicable criterionhealth-based value. If the resulting value exceeds the maximum ceiling concentration then that concentration becomes the criterion [Footnote (D)]. If the resulting value is less than the target detection limit the target detection limit becomes the criterion [Footnote (M)]. The modified criterion may exceed the chemical-specific Csat. See Footnote (C) and R 299.4(6).

Source Size sq. feet or acres Modifier 400 sq feet 3.17 1000 sq feet 2.2 2000 sq feet 1.76 1/4 acre 1.15 1/2 acre 1 1 acre 0.87 2 acre 0.77 5 acre 0.66 10 acre 0.6 32 acre 0.5 100 acre 0.43 Source Size Modifiers: Contamination Source Modifier for Area Size deriving final (ft2 or acres) VSIC/PSIC 100 ft2 6.97 400 ft2 3.05 1000 ft2 2.14 2000 ft2 1.74 ½ acre 1.00 1 acre 0.88 2 acres 0.77 5 acres 0.66 10 acres 0.59 20 acres 0.52 302 2017 MR 22 – December 15, 2017 Contamination Source Modifier for Area Size deriving final (ft2 or acres) VSIC/PSIC 30 acres 0.49 50 acres 0.45 75 acres 0.43 100 acres 0.41 150 acres 0.38 200 acres 0.36 300 acres 0.34 400 acres 0.33 500 acres 0.32 1000 acres 0.28 1500 acres 0.26

(Z) Mercury is typically measured as total mercury. The generic cleanup criteria, however, are based on data for consider different chemical species of mercury. The generic criteria presented in the criteria tables represent the lower of the values calculated for each chemical species of mercury for a pathway. Total mercury analytical results are compared to criteria. Specifically, data for elemental mercury, chemical abstract service (CAS) number 7439976, serve as the basis for the soil volatilization to indoor air criteria, groundwater volatilization to indoor air, and soil inhalation criteria. Data for methyl mercury, CAS number 22967926, serve as the basis for the GSI criterion; and data for mercuric chloride, CAS number 7487947, serve as the basis for the drinking water, groundwater contact, soil direct contact, and the groundwater protection criteria. Comparison to criteria shall be based on species-specific analytical data only if sufficient facility characterization has been conducted to rule out the presence of other species of mercury. (AA) Use 10,000 ug/l where groundwater enters a structure through the use of a water well, sump or other device. Use 28,000 ug/l for all other uses. The methane FESL is not calculated using the equation of R 299.16 or the toxicological, chemical-specific, and chemical-physical input values from the tables of R 299.50. Dissolved-phase methane in groundwater is not explosive; however, if liberated and allowed to accumulate in an enclosed structure the principal health and safety concerns are the explosive, flammable, and asphyxiant properties of gas phase methane. Concentrations of dissolved-phase methane in groundwater that exceed the flammability and explosivity screening level of 10,000 μg/L require evaluation of potential fire and explosion risk pursuant to R 299.4(7) with respect to gas-phase methane that could be released from groundwater. The evaluation shall include consideration of other sources of gas-phase methane generation in the vadose zone and the presence of above or below grade enclosed structures with the potential for gas-phase methane to pose a fire and explosion risk.

Health-based VI groundwater screening levels are not available for methane dissolved in groundwater due to insufficient data. In addition to the evaluation required pursuant to R 299.4(7), an exceedance of the flammability and explosivity screening levels shall require evaluation of the methane source for vapor intrusion potential pursuant to R 299.27(8)(c). For this purpose, dissolved-phase methane in groundwater is not subject to generic cleanup criteria, and shall be considered solely for purposes of evaluating the potential for gas-phase methane generation as well as potential risks associated with any generated gas-phase methane. (BB) The state drinking water standard for asbestos (fibers greater than 10 micrometers in length) is in units of a million fibers per liter of water (MFL). Soil concentrations of asbestos are determined by polarized light microscopymust be evaluated on a site-specific basis. United States Environmental Protection Agency asbestos technical resources provide applicable information for a site-specific evaluation. (CC) Groundwater: The generic GSI criteria are based on the toxicity of unionized ammonia (NH3); the criteria are 29 ug/L and 53 ug/L for cold water and warm water surface water, respectively. As a result, the GSI criterion shall be compared to the percent% of the total ammonia concentration in the groundwater that will become NH3 in the surface water. This percent% NH3 is a function of the pH and temperature of the receiving surface water

303 2017 MR 22 – December 15, 2017 and can be estimated using the following table, taken from Emerson, et al., (Journal of the Fisheries Research Board of Canada, Volume 32(12):2382, 1975). o Percent NH3 in Aqueous Ammonia Solutions for 0-30 C and pH 6-10 Temp Temp pH (◦F) (◦C) 6.0 6.5 7.0 7.5 8.0 8.5 9.0 9.5 10.0 32.0 0 0.00827 0.0261 0.0826 0.261 0.820 2.55 7.64 20.7 45.3 33.8 1 0.00899 0.0284 0.0898 0.284 0.891 2.77 8.25 22.1 47.3 35.6 2 0.00977 0.0309 0.0977 0.308 0.968 3.00 8.90 23.6 49.4 37.4 3 0.0106 0.0336 0.106 0.335 1.05 3.25 9.60 25.1 51.5 39.2 4 0.0115 0.0364 0.115 0.363 1.14 3.52 10.3 26.7 53.5 41.0 5 0.0125 0.0395 0.125 0.394 1.23 3.80 11.1 28.3 55.6 42.8 6 0.0136 0.0429 0.135 0.427 1.34 4.11 11.9 30.0 57.6 44.6 7 0.0147 0.0464 0.147 0.462 1.45 4.44 12.8 31.7 59.5 46.4 8 0.0159 0.0503 0.159 0.501 1.57 4.79 13.7 33.5 61.4 48.2 9 0.0172 0.0544 0.172 0.542 1.69 5.16 14.7 35.3 63.3 50.0 10 0.0186 0.0589 0.186 0.586 1.83 5.56 15.7 37.1 65.1 51.8 11 0.0201 0.0637 0.201 0.633 1.97 5.99 16.8 38.9 66.8 53.6 12 0.0218 0.0688 0.217 0.684 2.13 6.44 17.9 40.8 68.5 55.4 13 0.0235 0.0743 0.235 0.738 2.30 6.92 19.0 42.6 70.2 57.2 14 0.0254 0.0802 0.253 0.796 2.48 7.43 20.2 44.5 71.7 59.0 15 0.0274 0.0865 0.273 0.859 2.67 7.97 21.5 46.4 73.3 60.8 16 0.0295 0.0933 0.294 0.925 2.87 8.54 22.8 48.3 74.7 62.6 17 0.0318 0.101 0.317 0.996 3.08 9.14 24.1 50.2 76.1 64.4 18 0.0343 0.108 0.342 1.07 3.31 9.78 25.5 52.0 77.4 66.2 19 0.0369 0.117 0.368 1.15 3.56 10.5 27.0 53.9 78.7 68.0 20 0.0397 0.125 0.396 1.24 3.82 11.2 28.4 55.7 79.9 69.5 21 0.0427 0.135 0.425 1.33 4.10 11.9 29.9 57.5 81.0 71.6 22 0.0459 0.145 0.457 1.43 4.39 12.7 31.5 59.2 82.1 73.4 23 0.0493 0.156 0.491 1.54 4.70 13.5 33.0 60.9 83.2 75.2 24 0.0530 0.167 0.527 1.65 5.03 14.4 34.6 62.6 84.1 77.0 25 0.0569 0.180 0.566 1.77 5.38 15.3 36.3 64.3 85.1 78.8 26 0.0610 0.193 0.607 1.89 5.75 16.2 37.9 65.9 85.9 80.6 27 0.0654 0.207 0.651 2.03 6.15 17.2 39.6 67.4 86.8 82.4 28 0.0701 0.221 0.697 2.17 6.56 18.2 41.2 68.9 87.3 84.2 29 0.0752 0.237 0.747 2.32 7.00 19.2 42.9 70.4 88.3 86.0 30 0.0805 0.254 0.799 2.48 7.46 20.3 44.6 71.8 89.0

The generic approach for estimating NH3 assumes a default pH of 8 and default temperatures of 68F and 85F for cold water and warm water surface water, respectively. The resulting percent% NH3 is 3.8 percent% and 7.2 percent% for cold water and warm water, respectively. This default percentage shall be multiplied by the total ammonia-nitrogen (NH3-N) concentration in the groundwater and the resulting NH3 concentration compared to the applicable GSI criterion. As an alternative, the maximum pH and temperature data from the specific receiving surface water can be used to estimate, from the table in this footnote, a lower percent% unionized ammonia concentration for comparison to the generic GSI. Soil: The generic soil GSI protection criteria for unionized ammonia are 580 uµg/kg and 1,100 uµg/kg for cold water and warm water surface water, respectively. Hazardous substance does not have sufficient chemical-physical generic input values to allow the development of a generic screening level or criterion using the equations of R 299.27. The generic screening level or criterion for groundwater, pursuant to R 299.27(7)(a) is based solely on the equations of R 299.27(13)(b). The generic screening level or criterion for vapor is based on R 299.27(7)(b). Alternatively, a person may evaluate the VIAP using a VI Tier 3B site-specific criterion. 304 2017 MR 22 – December 15, 2017

Hazardous Substance CAS Number Acenaphthylene 208968 t-Amyl methyl ether (TAME) 994058 Azobenzene 103333 t-Butyl alcohol 75650 Camphene 79925 Cyclohexanone 108941 Di-n-octyl phthalate 117840 Dibromochloropropane 96128 N, N-Dimethylaniline 121697 Dimethylformamide 68122 Epichlorohydrin 106898 Ethyl-tert-butyl ether (ETBE) 637923 Heptachlor epoxide 1024573 2-Nitrophenol 88755 Pentachlorobenzene 608935 Pentachloronitrobenzene 82688 Phenanthrene 85018 Piperidine 110894 Polychlorinated biphenyls (PCBs) 1336363 2,3,7,8-Tetrachlorodibenzo-p-dioxin 1746016 1,1,3,3-Tetramethylurea 632224 Tetranitromethane 509148 Triallate 2303175 Trifluralin 1582098 tris(2,3-Dibromopropyl)phosphate 126727

(DD) Hazardous substance causes developmental effects. Residential direct contact criteria are protective of both prenatal exposure using a pregnant female receptor and postnatal exposure using a child receptor. Nonresidential direct contact criteria are protective for aof prenatal exposure using a pregnant adultfemale receptor. Prenatal developmental effects may occur after a single exposure (SE) or full-term (FT) exposure. Oral exposure pathways are drinking water and soil direct contact. Inhalation exposure pathways are ambient air and volatilization to indoor air.

Categorization of the Developmental Toxicants Oral Inhalation CAS Hazardous Substance Exposure Exposure Number Pathways Pathways Acetophenone 98862 SE SE1 Acrylic acid 79107 FT -- Aluminum 7429905 SE -- Benzo(a)pyrene 50328 SE SE bis(2-Ethylhexyl)phthalate 117817 SE -- Boron 7440428 SE -- Bromodichloromethane 75274 SE -- 2-Butanone (MEK) 78933 FT SE Butyl benzyl phthalate 85687 SE -- Caprolactam 105602 FT -- Carbaryl 63252 SE -- Carbofuran 1563662 SE -- Carbon Disulfide 75150 SE -- Chloroethane 75003 -- FT

305 2017 MR 22 – December 15, 2017 Oral Inhalation CAS Hazardous Substance Exposure Exposure Number Pathways Pathways 4-Chloro-3-methylphenol 59507 SE -- 2-Chlorophenol 95578 SE SE Chlorpyrifos 2921882 SE -- Cyanide 57125 FT -- Cyclohexane 110827 -- FT 4-4'-DDT 50293 FT -- Decabromodiphenyl ether 1163195 SE SE1 Di-n-butyl phthalate 84742 SE SE Di(2-ethylhexyl) adipate 103231 SE -- Dicamba 1918009 FT -- 2,4-Dichlorophenol 120832 FT -- Diisopropyl ether 108203 SE SE Dinoseb 88857 FT FT Ethanol 64175 SE -- Ethylene glycol 107211 SE -- Fluorine (soluble fluoride) 7782414 FT -- 1-Formylpiperidine 2591868 SE -- Glyphosate 1071836 SE -- Heptachlor 76448 SE -- Isophorone 78591 -- SE Isopropyl alcohol 67630 FT -- Lead 7439921 FT FT Lithium 7439932 SE FT Mercury , organic (CH3Hg) 22967926 FT -- Methanol 67561 SE SE Methoxychlor 72435 SE -- 2-Methoxyethanol 109864 SE -- 4-Methyl-2-pentanone (MIBK) 108101 -- SE 2-Methylphenol 95487 FT -- Nitrate 14797558 FT -- Nitrite 14797650 FT -- Pendimethalin 40487421 SE -- Perchlorate 14797730 FT -- Percluorooctanic acid 335671 FT -- Perfluorooctane sulfonic acid 1763231 FT -- Phenol 108952 FT -- Phenytoin 57410 SE -- Phosphorus, White 7723140 SE -- Polybrominated biphenyls 67774327 FT -- 306 2017 MR 22 – December 15, 2017 Oral Inhalation CAS Hazardous Substance Exposure Exposure Number Pathways Pathways Polychlorinated biphenyls (PCBs) 1336363 FT -- PCB dioxin-like congeners varies FT FT Propyl alcohol 71238 SE SE n-Propylbenzene 103651 -- SE1 Strontium 7440246 FT -- Tebuthiuron 34014181 FT -- 1,2,4,5-Tetrachlorobenzene 95943 SE -- 2,3,7,8-Tetrachlorodibenzo-p-dioxin 1746016 FT FT Tetrahydrofuran 109999 FT -- Triallate 2303175 -- SE1 Trichloroethylene 79016 SE SE 2,4,6-Trichlorophenol 88062 SE -- Triethylene glycol 112276 FT -- 3-Trifluoromethyl-4-nitrophenol 88302 FT -- Vinyl acetate 108054 SE -- 1 Toxicity value is based on less than a 12-hour exposure; therefore, the nonresidential value shall not be adjusted for a 12-hour work day.

(EE) The following are applicable generic GSI criteria as required by section 20120e of the NREPA.

Hazardous Substance GSI Notes (ug/L) Phosphorus 1,000 Criteria applicable unless receiving water is a surface water that has a phosphorus waste load allocation or is an inland lake. In those cases, contact the department for applicable values. Total dissolved solids 5.0E+5 If TDS data are not available, the TDS criterion (TDS) may be used as a screening level for the sum of the concentrations of the following substances: calcium, chlorides, iron, magnesium, POTASSIUM, SODIUM, SULFATE.

Dissolved Oxygen (DO): Since a low level of DO can be harmful to Cold receiving waters  7,000 aquatic life, the criterion represents a minimum level that on-site samples must Warm receiving waters  5,000 exceed. This is in contrast to other criteria which represent “not to exceed” concentrations. DO criteria are not applicable if groundwater Carbonaceous Biochemical Oxygen Demand (CBOD) is less than 10,000 ug/L and groundwater ammonia concentration is less than 2,000 ug/L. The residential or nonresidential acceptable air concentration (AAC) for the following hazardous substances is not derived pursuant to the equations of R 299.26 and R 299.27. The identified hazardous substance may cause adverse human health effects for less than chronic exposures. The AAC for these hazardous substances is the acute or intermediate minimum risk level (MRL) developed by the Agency for Toxic Substances and Disease Registry (ATSDR), a United States Environmental Protection Agency Integrated Risk Information System (IRIS) acute reference concentration, or an acute initial threshold screening level (ITSL) by the department as follows:

307 2017 MR 22 – December 15, 2017 Nonresidential CAS Residential AAC Hazardous Substance AAC Number µg/m3 µg/m3 Acetoned 67641 31,000 31,000c Ammoniae 7664417 not applicable 1,200c Chlordaned 57749 0.20 0.28b trans-1,2-Dichloroethylenee 156605 not applicable 790c Ethanolg 64175 19,000 19,000c Tetrachloroethylenee 127184 41a 41a,b Toluenee 108883 not applicable 7,500a,c 1,1,1-Trichloroethanef 71556 5,000a 7,000a,c a Toxicity value for acute exposures or short-term exposures shall not be adjusted for generic exposure frequency, duration, and averaging time. b ATSDR has adjusted the acute or intermediate MRL for continuous exposure; therefore, the nonresidential value may be adjusted for a 12- hour work day. c Acute toxicity value is based on less than a 12-hour exposure; therefore, the nonresidential value shall not be adjusted for a 12-hour work day. d ATSDR intermediate MRL e ATSDR acute MRL f US EPA IRIS short-term reference concentration gDepartment acute Initial Threshold Screening Level

TR  ATca For R 299.26 equations, the AAC is the health-based cancer ( IURF  ED  EF ) or noncancer THQ  AT  RfC  RSC ( ED  EF ) component of the residential and nonresidential equations 1-8 and 12-19. For R 299.27 the AAC substitutes as the health-based value rather than the equations of R 299.27(14). (FF) The chloride GSI criterion shall be 125 mg/l when the discharge is to surface waters of the state designated as public water supply sources or 50 mg/l when the discharge is to the Great Lakes or connecting waters. Chloride GSI criteria shall not apply for surface waters of the state that are not designated as a public water supply source, however, the total dissolved solids criterion is applicable. The residential or nonresidential acceptable air concentration (AAC) for the following volatile hazardous substances are based on toxicity values that have been identified to have the potential to cause adverse human health effects for less than chronic exposures. The short-term exposure for shallow groundwater screening levels or criterion is based solely on the equations of R 299.27(13)(b).

Nonresidential CAS Residential AAC Hazardous Substance AAC Number µg/m3 µg/m3 Acetoned 67641 62,000 62,000c Ammoniad 7664417 1,200 1,200c trans-1,2-Dichloroethylened 156605 790 790c Ethanolf 64175 19,000 19,000c Methylene Chlorided 75092 2,100 not applicable Tetrachloroethylened 127184 41a 41a,b Toluened 108883 7,500a 7,500a,c 1,1,1-Trichloroethanee 71556 5,000a 7,000a,c a Toxicity value for acute exposures or short-term exposures shall not be adjusted for generic exposure frequency, duration, and averaging time. b ATSDR has adjusted the acute or intermediate MRL for continuous exposure; therefore, the nonresidential value may be adjusted for a 12- hour work day. c Acute toxicity value is based on less than a 12-hour exposure; therefore, the nonresidential value shall not be adjusted for a 12-hour work day. d ATSDR acute MRL e US EPA IRIS short-term reference concentration f Department acute Initial Threshold Screening Levels

(GG) RiskHealth-based criteria are not available for gas-phase methane due to insufficient toxicity data. Methane is not known to be toxic; the principal health and safety concerns are its explosive, flammable, and asphyxiant properties. The VI screening level for vapor addresses the risk that gas- phase methane can enter an enclosed structure and create a fire and explosion risk, or displace oxygen

308 2017 MR 22 – December 15, 2017 and present a risk of asphyxia or anoxia, or both, in an enclosed structure. Concentrations protective of the fire and explosion risk are also protective for asphyxia or anoxia for all VI tiers. An acceptable soil gas concentration (presented for both residential and nonresidential land uses) was derived utilizing 25 percent% of the lower explosive level for methane. This equates to 1.25 percent% by volume gas-phase methane or 8.4E+6 µug/m3. (HH) The residential drinking water criterion for sodium is not calculated using the equations of R 299.10 or the toxicological, chemical-specific, or chemical-physical input values as shown in the tables of R 299.50. The criterion is 230,000 ug/lµg/L pursuant toin accordance with the department’s Sodium Advisory Council recommendation and revised Groundwater Discharge Standards. (II) The residential drinking water criterion for 1,4-dioxane is not calculated using the equations of R 299.10 or the toxicological and chemical-physical data as shown in table 4 of R 299.50. The drinking water criterion is calculated using the United States Environmental Protection Agency’s (U.S. EPA) “Toxicological Review of 1,4-Dioxane,” EPA/635/R-11/003F, September 2013, and the department’s residential exposure algorithms to protect both children and adults from unsafe levels of the chemical. A copy of the U.S. EPA’s “Toxicological Review of 1,4-dioxane,” may be obtained on the U.S. EPA website, www.epa.gov, free of charge as of the time of adoption of these rules. A copy of the department’s residential exposure algorithms may be obtained without charge from the DEQ, RRD, 525 West Allegan Street, Lansing, Michigan 48933.This hazardous substance belongs to a class of chemicals known as chelating agents. The department’s experience with the behavior of chelating agents in the environment comes from ethylene diamine tetraacetic acid (EDTA) and the sodium and calcium salts of EDTA. The ability of EDTA and other chelating agents to mobilize more toxic hazardous substances, such as inorganics in soil, sediment, and groundwater, poses a greater concern than the toxicity of the individual chelating agents. As such, generic groundwater cleanup criteria are not presented for hazardous substances in this class. Rather, inorganic concentrations in groundwater must be evaluated at sites where chelating agents are known or suspected to have been released. Concentrations of inorganics in groundwater must satisfy applicable cleanup criteria. (JJ) 3- and 4-Methylphenol cannot be analyzed separately. Environmental concentrations are reported as 3- and 4-methylphenol. As a result, both isomers are listed together as a single hazardous substance in the criteria tables. To protect for the adverse effects of both isomers, the criteria presented in the tables is the lower of the criteria generated for each isomer. (KK) Hazardous substance may exhibit the characteristic of toxicity as defined under part 111 of the act in R 299.9212(4).

EPA TCLP Total CAS Hazardous Extract Concentration Hazardous Substance Number Waste Concentration Screening Level Number (µg/L) (µg/kg)

Arsenic 440382 D004 5,000 100,000 Barium 7440393 D005 100,000 2,000,000 Benzene 71432 D018 500 10,000 2-Butanone (MEK) 78933 D035 200,000 4,000,000 Cadmium 7440439 D006 1,000 20,000 Carbon tetrachloride 56235 D019 500 10,000 Chlordane 57749 D020 30 600 Chlorobenzene 108907 D021 100,000 2,000,000 Chloroform 67663 D022 6,000 120,000 Chromium, total 7440473 D007 5,000 100,000 Cresol ------D026 200,000 4,000,000 2,4-Dichlorophenoxyacetic Acid (2,4-D) 94757 D016 10,000 200,000 1,4-Dichlorobenzene 106467 D027 7,500 150,000 1,2-Dichloroethane 107062 D028 500 10,000 309 2017 MR 22 – December 15, 2017 EPA TCLP Total CAS Hazardous Extract Concentration Hazardous Substance Number Waste Concentration Screening Level Number (µg/L) (µg/kg)

1,1-Dichloroethylene 75354 D029 700 14,000 2,4-Dinitrotoluene 121142 D030 130 2,600 Endrin 72208 D012 20 400 76448 Heptachlor and Heptachlor Epoxide D031 8 160 1024573 Hexachlorobenzene (C-66) 118741 D032 130 2,600 Hexachlorobutadiene (C-46) 87683 D033 500 10,000 Hexachloroethane 67721 D034 3,000 60,000 Lead 7439921 D008 5,000 100,000 Lindane 58899 D013 400 8,000 Mercury 7439976 D009 200 4,000 Methoxychlor 72435 D014 10,000 200,000 2-Methylphenol 95487 D023 200,000 4,000,000 3-Methylphenol 108394 D024 200,000 4,000,000 4-Methylphenol 106445 D025 200,000 4,000,000 Nitrobenzene 98953 D036 2,000 40,000 Pentachlorophenol 87865 D037 100,000 2,000,000 Pyridine 110861 D038 5,000 100,000 Selenium 7782492 D010 1,000 20,000 Silver 7440224 D011 5,000 100,000 Tetrachloroethylene 127184 D039 700 14,000 Toxaphene 8001352 D015 500 10,000 Trichloroethylene 79016 D040 500 10,000 2,4,5-Trichlorophenol 95954 D041 400,000 8,000,000 2,4,6-Trichlorophenol 41026 D042 2,000 40,000 Silvex (2,4,5 TP) 93721 D017 1,000 20,000 Vinyl chloride 050518 D043 200 4,000

(LL) The residential mutagenic cancer health-based values for vinyl chloride are not calculated using the equations and generic input values in the pathway-specific rules. The residential mutagenic cancer health-based values are calculated using the following equations. The equations take into account the greater sensitivity to vinyl chloride during early life by using lifetime averaging of continuous exposure from birth to adulthood and no averaging for childhood exposure. The equations are based on those currently used for deriving the United States Environmental Protection Agency cancer based regional screening levels.

Residential drinking water mutagenic cancer health-based value for vinyl chloride:

TR  CF DWVmut,VC   SFo EFres IFdw   SFo IRdw,child        ATca   BWchild  where, DWVmut,V (Drinking water value) = 2.1E-01 µg/L or ppb

310 2017 MR 22 – December 15, 2017 C TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days CF (Conversion factor) = 1,000 µg/L -1 SFo (Oral cancer slope factor) = 7.2E-01 (mg/kg-day) EFres (Exposure frequency) = 350 days/year IFdw (Age-adjusted drinking = 1.1245 L-year/kg-day water ingestion factor) IRdw, child (Drinking water ingestion = 0.78 L/day rate) BWchild (Body weight) = 15 kg

Residential direct contact mutagenic cancer health-based value for vinyl chloride:

TR  CF DCV  mut,VC  SFo EFi,res IFs  AEi   SFo IRs,child  AEi         AT   BW   ca   child 

 SF EF DF  AE   SF  SA EV  AF  AE   d d,res d d child child d        ATca   BW child  where, DCVmut,V (Direct contact value for vinyl = 7.56E+02 µg/kg C chloride) TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days CF (Conversion factor) = 1E+9 µg/kg -1 SFo (Oral cancer slope factor) = 7.2E-01 (mg/kg-day) EFi,res (Ingestion exposure frequency) = 350 days/year IFs (Age-adjusted soil ingestion = 100.525 mg-year/kg-day factor) AEi (Ingestion absorption efficiency) = 1 -1 SFd (Dermal cancer slope factor) = 7.2E-01 (mg/kg-day) EFd,res (Dermal exposure frequency) = 275 days/year DF (Age-adjusted soil dermal = 424.5 mg-year/kg-day factor) AEd (Dermal absorption efficiency) = 0.1 IRs,child (Soil ingestion rate, child) = 179 mg/day BWchild (Body Weight, child) = 15 kg 2 SAchild (Skin surface area, child) = 2,400 cm EV (Event frequency) = 1 event/day 2 AFchild (Soil adherence factor, child) = 0.3 mg/cm -event

Residential volatile soil inhalation mutagenic cancer health-based value for vinyl chloride:

TR VSIVmut,VC  IURFEDres EFres  IURF       ATca  VFres   VFres  311 2017 MR 22 – December 15, 2017 where, VSIVmut,V (Volatile soil inhalation = 6.576E+02 µg/kg or ppb C value for infinite source, ½ acre source size) TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk = 4.4E-06 (µg/m3)-1 factor) EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year 3 VFres,inf (Volatilization factor for = 4.0316E+02 m /kg infinite source, ½ acre source size) VF for finite sources: 3 VFres,2m (Volatilization factor for = 1.303E+04 m /kg infinite source, ½ acre source size) 3 VFres,5m (Volatilization factor for = 5.294E+03 m /kg infinite source, ½ acre source size)

Residential particulate soil inhalation mutagenic cancer health-based value for vinyl chloride:

TR PSIVmut,VC   IURF  EDres  EFres   IURF        ATca  PEFres   PEFres  where, PSIVmut,V (Particulate soil inhalation = 8.179E+07 µg/kg or ppb C value for ½ acre source) -5 TR (Target risk level) = 10 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = 4.4E-06 (µg/m3)-1 EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year 3 PEFres (Particulate emission factor = 5.014E+07 m /kg for ½ acre source size, no emissions due to vehicle)

Residential mutagenic cancer acceptable air value (AAV) for vinyl chloride:

TR AAVmut,VC   IURF  EDres  EFres     IURF  ATca  where, 3 AAVmut,V (Acceptable air value for vinyl = 1.631 µg/m C chloride)

312 2017 MR 22 – December 15, 2017 TR (Target risk level) = 10-5 ATca (Averaging time) = 28,470 days IURF (Inhalation unit risk factor) = 4.4E-06 (µg/m3)-1 EDres (Exposure duration) = 32 years EFres (Exposure frequency) = 350 days/year

(MM) Hazardous substance is a carcinogen with a mutagenic mode of action. The cancer potency values used in calculating health-based values shall be modified using age-dependent adjustment factors for those carcinogenic chemicals identified as mutagenic. (NN) The residential and nonresidential drinking water criteria for perfluorooctanoic acid (PFOA) and perfluorooctane sulfonic acid (PFOS) are not calculated using the equations of R 299.10 or the toxicological, chemical-specific, or chemical-physical input values as shown in the tables of R 299.50. The PFOA drinking water criteria are the health advisory value as presented in the United States Environmental Protection Agency Drinking Water Health Advisory for Perfluorooctanoic Acid (PFOA), EPA 822-R-16-005, May 2016. The PFOS drinking water criteria are the health advisory value as presented in the United States Environmental Protection Agency Drinking Water Health Advisory for Perfluorooctane Sulfonate (PFOS), EPA 822-R-16-004, May 2016. Compliance with the drinking water criteria shall require comparing the sum of the PFOA and PFOS groundwater concentrations to the drinking water criterion of 0.07 μg/L. The drinking water criteria for PFOA and PFOS protect for both short-term developmental and chronic exposure. (2) Abbreviations have the following meanings when used in the tables of this rule: (a) “ATSDR” means Agency for Toxic Substances and Disease Registry. (b) “CAF” means cancer adjustment factor. (c) “CAS Number” means Chemical Abstract Service Number. (d) “IRIS” means United States Environmental Protection Agency’s Integrated Risk Information System. (e) “MAF” means mutagenic adjustment factors. (f) “MRL” means minimum risk level. (g) “TEF” means toxicity equivalence factor. (h) “TEMP” means temperature. (i) “TSCA” means Toxic Substance Control Act, 15 U.S.C. §2601 et seq. “ID” means insufficient data to develop criterion. “NA” means a criterion or value is not available or, in the case of background and CAS numbers, not applicable. “NLL” means hazardous substance is not likely to leach under most soil conditions. “NLV” means hazardous substance is not likely to volatilize under most conditions.

R 299.50 Toxicological and, chemical-specific, and chemical-physical properties. Rule 50. (1) The toxicological and chemical-physical properties used to calculate generic criteria shall be asare shown in table 41, except as provided in section 20120a(9) of the act, R 299.49(1)(l) and R 299.49(1)(o).the footnotes of the generic cleanup criteria tables in R 299.49. (2) Abbreviations used in table 14 have the following meanings when used in this rule: (a) “ATSDR” means Agency for Toxic Substances and Disease Registry. (b) “CAEPA” means California environmental protection agency. (c) “ECHA” means European Chemicals Agency. (d) “HEAST” means USEPA’s Health Effects Assessment Summary Tables. (e) “IRIS” means USEPA’s Integrated Risk Information System. (f) “MADEP” means Massachusetts department of environmental protection. (g) “MDEQ” means Michigan department of environmental quality. (h) “MNDOH” means Minnesota department of health. (i) “NYDEC” means New York state department of environmental conservation. (j) “OPP” means USEPA’s Office of Pesticide Programs. 313 2017 MR 22 – December 15, 2017 (k) “PPRTV” means USEPA’s Provisional Peer Reviewed Toxicity Values. (l) “TCEQ” means Texas commission on environmental quality. (m) “USEPA” means United States Environmental Protection Agency. (n) “WHO” means World Health Organization. (o) “A/MDEQ” means ATSDR value has been modified by MDEQ. (p) “C/MDEQ” means CAEPA value has been modified by MDEQ. (q) “E/MDEQ” means ECHA value has been modified by MDEQ. (r) “I/MDEQ” means IRIS value has been modified by MDEQ. (s) “O/MDEQ” means OPP value has been modified by MDEQ. (t) “P/MDEQ” means PPRTV value has been modified by MDEQ. (u) “W/MDEQ” means WHO value has been modified by MDEQ. (v) (a)“NA” means not available. (b) “NR” means not relevant. (3) The chemical-specific properties used to calculate generic criteria are shown in table 2, except as provided in the footnotes of the generic cleanup criteria tables in R 299.49. (4) Abbreviations used in table 2 have the following meanings when used in this rule: (a) “MDEQ” means Michigan department of environmental quality. (b) “USEPA” means United States Environmental Protection Agency’s Risk Assessment Guidance for Superfund Volume I: Human Health Evaluation Manual (Part E, Supplemental Guidance for Dermal Risk Assessment). July, 2004. (5) The chemical-physical properties used to calculate generic criteria are shown in table 3, except as provided in the footnotes of the generic cleanup criteria tables in R 299.49. (6) Abbreviations used in table 3 have the following meanings when used in this rule: (a) Source abbreviations are as follows: (i) “CRC” means Chemical Rubber Company Handbook of Chemistry and Physics, 95th edition, 2014-2015. (ii) “EPA1” means USEPA (2001) Fact Sheet, Correcting the Henry’s Law Constant for Soil Temperature. Office of Solid Waste and Emergency Response, Washington, D.C. (iii) “EPA4” means USEPA (2004) User’s Guide for Evaluating Subsurface Vapor Intrusion into Buildings. February 22, 2004. (iv) “EPI” means USEPA’s Estimation Programs Interface SUITE 4.1, Copyright 2000-2012. (v) “HSDB” means Hazardous Substances Data Bank. (vi) “NPG” means National Institute for Occupational Safety and Health Pocket Guide to Chemical Hazards. (vii) “PC” means National Center for Biotechnology Information’s PubChem database. (viii) “PP” means Syracuse Research Corporation’s PhysProp database. (ix) “SCDM” means USEPA’s Superfund Chemical Data Matrix. (x) “SSG” means USEPA’s Soil Screening Guidance: Technical Background Document, Second Edition, 1996. (xi) “W9” means USEPA’s User Guide for Water9 Software, Version 2.0.0, 2001. (b) Basis abbreviations are as follows: (i) “EST” means estimated. (ii) “EXP” means experimental. (iii) “EXT” means extrapolated. (iv) “NA” means not available. (v) “NR” means not relevant. (7) Tables 1 to 3 of this rule read as follows:

314 2017 MR 22 – December 15, 2017

TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Acenaphthene 83329 6.0E-02 IRIS NA MDEQ 2.1E+02 MDEQ NA MDEQ No No No No Acenaphthylene 208968 6.0E-02 TCEQ NA PPRTV 2.1E+02 NYDEC NA MDEQ No No No No Acetaldehyde (I) 75070 1.3E-01 MDEQ NA MDEQ 9.0E+00 IRIS 2.2E-06 IRIS No No No No Acetate 71501 5.7E-01 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Acetic acid (OO) 64197 5.7E-01 MDEQ NA MDEQ 2.5E+02 MDEQ NA MDEQ No No No No Acetone (I) 67641 9.0E-01 IRIS NA MDEQ 3.1E+04 ATSDR NA MDEQ No No No No Acetonitrile 75058 6.0E-02 HEAST NA MDEQ 6.0E+01 IRIS NA MDEQ No No No No Acetophenone (DD) 98862 8.0E-01 P/MDEQ NA MDEQ 3.2E+03 MDEQ NA MDEQ No No Yes Yes Acrolein (I) 107028 4.0E-03 ATSDR NA MDEQ 2.0E-02 IRIS NA MDEQ No No No No Acrylamide (MM) 79061 2.0E-03 IRIS 5.1E-01 IRIS 6.0E+00 IRIS 1.0E-04 IRIS Yes Yes No No Acrylic acid (DD,OO) 79107 2.0E-01 PPRTV NA MDEQ 2.0E-01 PPRTV NA MDEQ No No No Yes Acrylonitrile (I) 107131 1.0E-02 ATSDR 5.4E-01 IRIS 2.0E+00 IRIS 6.8E-05 IRIS No No No No Alachlor 15972608 1.0E-02 IRIS 9.6E-02 MDEQ NA MDEQ NA MDEQ No No No No Aldicarb 116063 2.7E-04 OPP NA MDEQ NA MDEQ NA MDEQ No No No No Aldicarb sulfone 1646884 1.0E-03 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No Aldicarb sulfoxide 1646873 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Aldrin 309002 3.0E-05 ATSDR 1.7E+01 IRIS NA MDEQ 4.9E-03 IRIS No No No No Aluminum (B,DD) 7429905 1.0E+00 ATSDR NA MDEQ 5.5E+00 PPRTV NA MDEQ No No No Yes Ammonia 7664417 NA MDEQ NA MDEQ 5.0E+02 IRIS NA MDEQ No No No No t-Amyl methyl ether (TAME) 994058 1.3E-01 MDEQ NA MDEQ 6.2E+01 MDEQ NA MDEQ No No No No Aniline 62533 7.0E-03 PPRTV 5.7E-03 IRIS 1.0E+00 IRIS 1.6E-06 MDEQ No No No No Anthracene 120127 3E-01 IRIS NA MDEQ 1.0E+03 MDEQ NA MDEQ No No No No Antimony 7440360 4.0E-04 IRIS NA MDEQ 2.0E-01 MDEQ NA MDEQ No No No No Arsenic (B,KK) 7440382 3.0E-04 ATSDR 1.5E+00 IRIS NA MDEQ 4.3E-03 IRIS No No No No 9.0E-05 2.3E-01 Asbestos (BB) 1332214 NA MDEQ NA MDEQ IRIS IRIS No No No No fibers/cc fibers/ml Atrazine 1912249 1.8E-02 OPP NA MDEQ 2.1E+01 O/MDEQ NA MDEQ No No No No Azobenzene 103333 NA MDEQ 1.1E-01 IRIS NA MDEQ 3.1E-05 IRIS No No No No Barium (B,KK) 7440393 2.0E-01 IRIS NA MDEQ 5.0E+00 MDEQ NA MDEQ No No No No

315 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Benzene (I,KK) 71432 5.0E-04 ATSDR 5.5E-02 IRIS 1.0E+01 ATSDR 7.80E-06 IRIS No No No No Benzidine (MM) 92875 3.0E-03 IRIS 2.3E+02 IRIS NA MDEQ 6.7E-02 IRIS Yes Yes No No Benzo(a)anthracene (Q,MM) 56553 NA MDEQ 1.0E-01 IRIS NA MDEQ 6.0E-05 IRIS Yes Yes No No Benzo(b)fluoranthene (Q,MM) 205992 NA MDEQ 1.0E-01 IRIS NA MDEQ 6.0E-05 IRIS Yes Yes No No Benzo(k)fluoranthene (Q,MM) 207089 NA MDEQ 1.0E-02 IRIS NA MDEQ 6.0E-06 IRIS Yes Yes No No Benzo(g,h,i)perylene 191242 2E-03 MDEQ NA MDEQ 7E+00 MDEQ NA MDEQ No No No No Benzo(a)pyrene (Q,DD,MM) 50328 3.0E-04 IRIS 1.0E+00 IRIS 2.0E-03 IRIS 6.0E-04 IRIS Yes Yes Yes Yes Benzoic acid 65850 4.0E+00 IRIS NA MDEQ 7.0E-01 PPRTV NA MDEQ No No No No Benzyl alcohol 100516 1.4E-01 PPRTV NA MDEQ 5.0E+03 MDEQ NA MDEQ No No No No Benzyl chloride 100447 2.0E-03 PPRTV 1.7E-01 IRIS 1.0E+00 PPRTV 5.0E-05 MDEQ No No No No Beryllium (B) 7440417 2.0E-03 ATSDR NA MDEQ 2.0E-02 IRIS 2.4E-03 IRIS No No No No bis(2-Chloroethoxy)ethane 112265 2.5E-04 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No bis-2-Chloroethylether (I) 111444 NA MDEQ 1.1E+00 IRIS 1.2E+02 ATSDR 3.3E-04 IRIS No No No No bis(2-Ethylhexyl) phthalate (DD) 117817 6.0E-02 ATSDR 1.4E-02 IRIS 7.0E+01 MDEQ 1.6E-06 MDEQ No No No Yes Boron (DD) 7440428 2.0E-01 IRIS NA MDEQ 3.0E+01 ATSDR NA MDEQ No No No Yes Bromate 15541454 4.0E-03 IRIS 7E-01 IRIS NA MDEQ NA MDEQ No No No No Bromobenzene (I) 108861 8.0E-03 IRIS NA MDEQ 6.0E+01 IRIS NA MDEQ No No No No Bromodichloromethane (DD) 75274 8.0E-03 PPRTV 6.2E-02 IRIS 2.0E+00 PPRTV 1.77E-05 MDEQ No No No Yes Bromoform 75252 2.0E-02 ATSDR 7.9E-03 IRIS NA MDEQ 1.1E-06 IRIS No No No No Bromomethane 74839 2.0E-02 OPP NA MDEQ 1.0E+01 PPRTV NA MDEQ No No No No n-Butanol (I,OO) 71363 1.0E-01 IRIS NA MDEQ 3.5E+02 MDEQ NA MDEQ No No No No 2-Butanone (MEK) (I,DD,KK) 78933 5.9E-01 IRIS NA MDEQ 5.0E+03 IRIS NA MDEQ No No Yes Yes n-Butyl acetate 123864 1.0E-01 W/MDEQ NA MDEQ 4.0E+02 WHO NA MDEQ No No No No t-Butyl alcohol (OO) 75650 1.8E-01 MADEP NA MDEQ 7.2E+01 E/MDEQ NA MDEQ No No No No Butyl benzyl phthalate (DD) 85687 2.0E-02 CAEPA 1.9E-03 PPRTV 7.8E+02 ECHA NA MDEQ No No No Yes n-Butylbenzene 104518 0.046 PPRTV NA MDEQ 2.0E+02 CAEPA NA MDEQ No No No No sec-Butylbenzene 135988 1.0E-01 PPRTV NA MDEQ 4.0E-01 CAEPA NA MDEQ No No No No t-Butylbenzene (I) 98066 1.0E-01 PPRTV NA MDEQ 4.0E-01 CAEPA NA MDEQ No No No No Cadmium (B,KK) 7440439 1E-04 ATSDR NA MDEQ NA MDEQ 1.8E-03 IRIS No No No No Camphene (I) 79925 NA MDEQ NA MDEQ 8.0E+01 MDEQ NA MDEQ No No No No

316 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Caprolactam (DD) 105602 5.0E-01 IRIS NA MDEQ 2.2E+00 CAEPA NA MDEQ No No No Yes Carbaryl (DD) 63252 1.0E-02 OPP 8.7E-04 OPP NA MDEQ NA MDEQ No No No Yes Carbazole 86748 5.0E-03 MDEQ 9.8E-02 MDEQ NA MDEQ 2.8E-06 MDEQ No No No No Carbofuran (DD) 1563662 6.0E-05 OPP NA MDEQ NA MDEQ NA MDEQ No No No Yes Carbon disulfide (I,R,DD) 75150 1.1E-01 IRIS NA MDEQ 7.0E+02 IRIS NA MDEQ No No No Yes Carbon tetrachloride (KK) 56235 4.0E-03 IRIS 6.5E-2 IRIS 1.0E+02 IRIS 5.6E-06 IRIS No No No No Chlordane (J,KK) 57749 5.0E-04 IRIS 3.5E-01 IRIS 7.0E-01 IRIS 1.0E-04 IRIS No No No No Chloride 16887006 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No 2-Chloroaniline 95512 3.0E-03 MDEQ NA MDEQ 1.0E+01 MDEQ NA MDEQ No No No No 4-Chloroaniline 106478 5.0E-04 PPRTV 2.0E-01 PPRTV NA MDEQ NA MDEQ No No No No Chlorobenzene (I,KK) 108907 2.0E-02 IRIS NA MDEQ 5.0E+01 PPRTV NA MDEQ No No No No p-Chlorobenzene sulfonic acid 98668 8.0E-01 C/MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No 1-Chloro-1,1-difluoroethane 75683 2.1E+00 MDEQ NA MDEQ 5.0E+04 IRIS NA MDEQ No No No No Chloroethane (DD) 75003 4E-02 P/MDEQ 2.0E-03 MDEQ 4.0E+03 PPRTV NA MDEQ No No Yes No 2-Chloroethyl vinyl ether 110758 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Chloroform (KK) 67663 1.0E-02 IRIS NA MDEQ 9.8E+01 ATSDR 2.3E-05 IRIS No No No No Chloromethane (I) 74873 NA MDEQ 3.3E-03 MDEQ 9.0E+01 IRIS NA MDEQ No No No No 4-Chloro-3-methylphenol (DD) 59507 1.0E-01 PPRTV NA MDEQ NA MDEQ NA MDEQ No No No Yes beta-Chloronaphthalene 91587 8.0E-02 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No 2-Chlorophenol (DD) 95578 8.0E-03 PPRTV NA MDEQ 1.8E+01 MDEQ NA MDEQ No No Yes Yes o-Chlorotoluene (I) 95498 6.7E-03 P/MDEQ NA MDEQ 8.0E+01 CAEPA NA MDEQ No No No No Chlorpyrifos (DD) 2921882 4.7E-03 OPP NA MDEQ 1E+00 MDEQ NA MDEQ No No No Yes Chromium (III) (B,H,KK) 16065831 1.5E+00 IRIS NA MDEQ 1.0E-01 ATSDR NA MDEQ No No No No Chromium (VI) (H,KK,MM) 18540299 9.0E-04 ATSDR 5.0E-01 CAEPA 5.0E-03 ATSDR 1.2E-02 IRIS Yes Yes No No Chrysene (Q,MM) 218019 NA MDEQ 1.0E-03 USEPA NA MDEQ 6.0E-07 USEPA Yes Yes No No Cobalt (B) 7440484 3.0E-04 P/MDEQ NA MDEQ 6.0E-03 PPRTV 9.0E-03 PPRTV No No No No Copper (B) 7440508 1.0E-03 ATSDR NA MDEQ 2.0E+00 MDEQ NA MDEQ No No No No Cyanazine 21725462 2.0E-04 WHO 3.7E-01 MDEQ NA MDEQ NA MDEQ No No No No Cyanide (P,R,DD) 57125 6.3E-04 IRIS NA MDEQ 8.0E-01 IRIS NA MDEQ No No No Yes Cyclohexane (DD) 110827 NA MDEQ NA MDEQ 6.0E+03 IRIS NA MDEQ No No Yes No

317 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Cyclohexanone (OO) 108941 2.0E-01 P/MDEQ NA MDEQ 7.0E+02 PPRTV NA MDEQ No No No No Dacthal 1861321 1.0E-02 OPP 1.49E-03 OPP NA MDEQ NA MDEQ No No No No Dalapon 75990 3.0E-02 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No 4-4'-DDD 72548 3.0E-03 MDEQ 2.4E-01 IRIS NA MDEQ 7.0E-05 MDEQ No No No No 4-4'-DDE 72559 7.0E-04 MDEQ 3.4E-01 IRIS NA MDEQ 9.7E-05 MDEQ No No No No 4-4'-DDT (DD) 50293 5.0E-04 ATSDR 3.4E-01 IRIS NA MDEQ 9.7E-05 IRIS No No No Yes Decabromodiphenyl ether (DD) 1163195 7.0E-03 IRIS 7.0E-04 IRIS 2.5E+01 MDEQ 2.0E-07 MDEQ No No Yes Yes Di-n-butyl phthalate (DD) 84742 6.7E-03 ECHA NA MDEQ 2.0E+01 ECHA NA MDEQ No No Yes Yes Di(2-ethylhexyl) adipate (DD) 103231 6.0E-01 IRIS 1.2E-03 IRIS NA MDEQ 3.4E-07 MDEQ No No No Yes Di-n-octyl phthalate 117840 1.2E-02 PPRTV NA MDEQ 4.7E+02 MDEQ NA MDEQ No No No No Diacetone alcohol (I,OO) 123422 NA MDEQ NA MDEQ 2.4E+03 MDEQ NA MDEQ No No No No Diazinon 333415 7.0E-04 ATSDR NA MDEQ 1.0E+00 ATSDR NA MDEQ No No No No Dibenzo(a,h)anthracene (Q,MM) 53703 NA MDEQ 1.0E+00 IRIS NA MDEQ 6.0E-04 IRIS Yes Yes No No Dibenzofuran 132649 1.0E-03 PPRTV NA MDEQ 4.0E+00 MDEQ NA MDEQ No No No No Dibromochloromethane (MM) 124481 7.0E-03 P/MDEQ 8.4E-02 IRIS NA MDEQ 2.4E-05 MDEQ Yes Yes No No Dibromochloropropane (MM) 96128 2.0E-04 PPRTV 8.0E-01 PPRTV 2.0E-01 IRIS 5.6E-03 PPRTV Yes Yes No No Dibromomethane 74953 3.0E-03 P/MDEQ NA MDEQ 4.0E+00 PPRTV NA MDEQ No No No No Dicamba (DD) 1918009 4.5E-01 OPP NA MDEQ NA MDEQ NA MDEQ No No No Yes 1,2-Dichlorobenzene 95501 3.0E-01 ATSDR NA MDEQ 3.0E+02 MDEQ NA MDEQ No No No No 1,3-Dichlorobenzene 541731 2.0E-03 A/MDEQ NA MDEQ 3.0E+00 MDEQ NA MDEQ No No No No 1,4-Dichlorobenzene (KK) 106467 7.0E-02 ATSDR 1.3E-02 MDEQ 6.0E+01 ATSDR 3.9E-06 MDEQ No No No No 3,3`-Dichlorobenzidine 91941 7.3E-03 MDEQ 4.5E-01 IRIS NA MDEQ 3.4E-04 CAEPA No No No No Dichlorodifluoromethane 75718 5.0E-03 P/MDEQ NA MDEQ 3.3E+02 P/MDEQ NA MDEQ No No No No 1,1-Dichloroethane 75343 2.0E-01 PPRTV 5.7E-03 CAEPA 5.0E+02 MDEQ 1.6E-06 CAEPA No No No No 1,2-Dichloroethane (I,KK) 107062 2.0E-02 PPRTV 9.1E-02 IRIS 7.0E+00 PPRTV 2.6E-05 IRIS No No No No 1,1-Dichloroethylene (I,KK) 75354 5.0E-02 IRIS NA MDEQ 2.0E+02 IRIS NA MDEQ No No No No cis-1,2-Dichloroethylene 156592 2.0E-03 IRIS NA MDEQ 8.0E+00 CAEPA NA MDEQ No No No No trans-1,2-Dichloroethylene 156605 2.0E-02 IRIS NA MDEQ 2.6E+02 A/MDEQ NA MDEQ No No No No 2,6-Dichloro-4-nitroaniline 99309 2.5E-03 OPP NA MDEQ 8.8E+00 O/MDEQ NA MDEQ No No No No 2,4-Dichlorophenol (DD) 120832 2.0E-02 P/MDEQ NA MDEQ 1.1E+01 MDEQ NA MDEQ No No No Yes

318 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route 2,4-Dichlorophenoxyacetic acid (KK) 94757 5.0E-02 OPP NA MDEQ 1.75E+02 OPP NA MDEQ No No No No 1,2-Dichloropropane (I) 78875 9.0E-02 ATSDR 3.6E-02 CAEPA 4.0E+00 IRIS 5.0E-06 MDEQ No No No No 1,3-Dichloropropene (J) 542756 3.0E-02 ATSDR 1.0E-01 IRIS 3.0E+01 ATSDR 4.0E-06 IRIS No No No No Dichlorvos (MM) 62737 5.0E-04 OPP 2.9E-01 IRIS 2.0E+00 O/MDEQ NA MDEQ Yes Yes No No Dicyclohexyl phthalate 84617 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Dieldrin 60571 5.0E-05 ATSDR 1.6E+01 IRIS NA MDEQ 4.6E-03 IRIS No No No No Diethyl ether 60297 2.0E-01 IRIS NA MDEQ 1.0E+03 P/MDEQ NA MDEQ No No No No Diethyl phthalate 84662 8.0E-01 IRIS NA MDEQ 2.8E+03 MDEQ NA MDEQ No No No No Diethylene glycol monobutyl ether 112345 3.0E-02 PPRTV NA MDEQ 1.0E-01 PPRTV NA MDEQ No No No No Diisopropyl ether (DD) 108203 2.7E-01 MDEQ NA MDEQ 7.0E+02 PPRTV NA MDEQ No No Yes Yes Diisopropylamine (I) 108189 7.7E-04 MDEQ NA MDEQ 2.0E+02 MDEQ NA MDEQ No No No No Dimethyl phthalate 131113 1.0E-01 PPRTV NA MDEQ 5.0E+01 MDEQ NA MDEQ No No No No N,N-Dimethylacetamide (OO) 127195 2.5E-02 MDEQ NA MDEQ 1.0E+02 MDEQ NA MDEQ No No No No N,N-Dimethylaniline 121697 2.0E-03 IRIS 4.9E-02 MDEQ NA MDEQ 1.2E-05 MDEQ No No No No Dimethylformamide (I,OO) 68122 1.0E-01 PPRTV NA MDEQ 7.0E+00 P/MDEQ NA MDEQ No No No No 2,4-Dimethylphenol 105679 2.0E-02 P/MDEQ NA MDEQ 7.0E+01 MDEQ NA MDEQ No No No No 2,6-Dimethylphenol 576261 6.0E-04 IRIS NA MDEQ 2.0E+00 MDEQ NA MDEQ No No No No 3,4-Dimethylphenol 95658 1.0E-03 IRIS NA MDEQ 3.5E+00 MDEQ NA MDEQ No No No No Dimethylsulfoxide 67685 1.0E+00 O/MDEQ NA MDEQ 2.0E+01 MDEQ NA MDEQ No No No No 2,4-Dinitrophenol 51285 2.0E-03 PPRTV NA MDEQ 7.0E+00 MDEQ NA MDEQ No No No No 2,4-Dinitrotoluene (KK) 121142 1.0E-03 ATSDR 6.7E-01 USEPA 2.0E+00 MDEQ 8.9E-05 CAEPA No No No No Dinoseb (DD) 88857 1.0E-03 IRIS NA MDEQ 4.0E+00 MDEQ NA MDEQ No No Yes Yes 1,4-Dioxane (I,OO) 123911 3.0E-02 IRIS 1.0E-01 IRIS 3.0E+01 IRIS 5.0E-06 IRIS No No No No Diquat 85007 5.0E-03 OPP NA MDEQ NA MDEQ NA MDEQ No No No No Dissolved oxygen (DO) NA NA MDEQ NA MDEQ NA MDEQ NA MDEQ NA NA No No Diuron 330541 3.0E-03 OPP 1.9E-02 OPP 3.3E+00 OPP NA MDEQ No No No No Endosulfan (J) 115297 5.0E-03 ATSDR NA MDEQ NA MDEQ NA MDEQ No No No No Endothall 145733 7.0E-03 OPP NA MDEQ 7.0E+01 OPP NA MDEQ No No No No Endrin (KK) 72208 3.0E-04 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No Epichlorohydrin (I) 106898 6.0E-03 PPRTV 9.9E-03 IRIS 1.0E+00 IRIS 1.2E-06 IRIS No No No No

319 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Ethanol (I,DD,OO) 64175 6.2E+01 MDEQ NA MDEQ 1.9E+04 MDEQ NA MDEQ No No No Yes Ethyl acetate (I) 141786 7.2E-02 P/MDEQ NA MDEQ 7.0E+01 PPRTV NA MDEQ No No No No Ethyl-tert-butyl ether (ETBE) 637923 9.2E-02 MDEQ NA MDEQ 3.7E+02 MDEQ NA MDEQ No No No No Ethylbenzene (I) 100414 4.0E-02 ATSDR 1.1E-02 CAEPA 2.6E+02 ATSDR 2.5E-06 CAEPA No No No No Ethylene dibromide 106934 9.0E-03 IRIS 2.0E+00 IRIS 9.0E+00 IRIS 6.0E-04 IRIS No No No No Ethylene glycol (DD) 107211 8.0E-01 ATSDR NA MDEQ 2.0E+01 A/MDEQ NA MDEQ No No No Yes Ethylene glycol monobutyl ether 111762 1.0E-01 IRIS NA MDEQ 1.6E+03 IRIS NA MDEQ No No No No Ethylenediaminetetraacetic acid (EDTA) (II) 60004 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Fluoranthene 206440 4.0E-02 P/MDEQ NA MDEQ 1.4E+02 MDEQ NA MDEQ No No No No Fluorene 86737 4.0E-02 A/MDEQ NA MDEQ 1.4E+02 MDEQ NA MDEQ No No No No Fluorine (soluble fluoride) (DD) 7782414 6.0E-02 IRIS NA MDEQ NA MDEQ NA MDEQ No No No Yes Formaldehyde (MM,OO) 50000 2.0E-01 IRIS NA MDEQ 9.8E+00 ATSDR 1.3E-05 IRIS Yes Yes No No Formic acid (I,U,OO) 64186 9E-01 PPRTV NA MDEQ 3E-01 PPRTV NA MDEQ No No No No 1-Formylpiperidine (DD) 2591868 1.1E+00 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No Yes Gentian violet 548629 1.4E-01 MDEQ 5.5E-02 MDEQ NA MDEQ NA MDEQ No No No No Glyphosate (DD) 1071836 1E-01 IRIS NA MDEQ NA MDEQ NA MDEQ No No No Yes Heptachlor (DD,KK) 76448 1E-04 ATSDR 1.2E+00 MDEQ NA MDEQ 1.30E-03 IRIS No No No Yes Heptachlor epoxide (KK) 1024573 1.3E-05 IRIS 3.6E+00 MDEQ NA MDEQ 2.6E-03 IRIS No No No No n-Heptane 142825 4.4E+00 MDEQ NA MDEQ 3.5E+03 MDEQ NA MDEQ No No No No Hexabromobenzene 87821 2E-03 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No Hexachlorobenzene (C-66) (KK) 118741 1.0E-05 PPRTV 1.6E+00 IRIS 3.5E-02 MDEQ 4.6E-04 IRIS No No No No Hexachlorobutadiene (C-46) (KK) 87683 1.0E-03 PPRTV 7.8E-02 IRIS NA MDEQ 2.2E-05 IRIS No No No No alpha-Hexachlorocyclohexane 319846 8.0E-03 ATSDR 6.3E+00 IRIS NA MDEQ 1.8E-03 IRIS No No No No beta-Hexachlorocyclohexane 319857 6E-05 A/MDEQ 1.8E+00 IRIS NA MDEQ 5.3E-04 IRIS No No No No Hexachlorocyclopentadiene (C-56) 77474 6E-03 IRIS NA MDEQ 2E-01 IRIS NA MDEQ No No No No Hexachloroethane (KK) 67721 7.0E-04 IRIS 4E-02 IRIS 3E+01 IRIS 1.0E-05 MDEQ No No No No n-Hexane 110543 3E-01 PPRTV NA MDEQ 7E+02 MDEQ NA MDEQ No No No No 2-Hexanone 591786 5E-03 IRIS NA MDEQ 3E+01 IRIS NA MDEQ No No No No Indeno(1,2,3-cd)pyrene (Q,MM) 193395 NA MDEQ 1.0E-01 IRIS NA MDEQ 6.0E-05 IRIS Yes Yes No No Iron (B) 7439896 7E-01 PPRTV NA MDEQ NA MDEQ NA MDEQ No No No No

320 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Isobutyl alcohol (I,OO) 78831 3E-01 IRIS NA MDEQ 1.5E+03 MDEQ NA MDEQ No No No No Isophorone (DD) 78591 2E-01 IRIS 9.5E-04 IRIS 2E+03 CAEPA 2.7E-07 MDEQ No No Yes No Isopropyl alcohol (I,DD,OO) 67630 2E+00 PPRTV NA MDEQ 2E+02 PPRTV NA MDEQ No No No Yes Isopropyl benzene 98828 1.0E-01 IRIS NA MDEQ 4E+02 IRIS 1.05E-05 MDEQ No No No No Lead (B,L,DD,KK) 7439921 NA MDEQ NA MDEQ 1.5E-01 USEPA NA MDEQ No No Yes Yes Lindane (KK) 58899 4.7E-03 OPP 1.1E+00 CAEPA NA MDEQ NA MDEQ No No No No Lithium (B,DD) 7439932 0.002 PPRTV NA MDEQ 3.5E+01 MDEQ NA MDEQ No No Yes Yes Magnesium 7439954 1.1E+01 MDEQ NA MDEQ 1.0E+02 MDEQ NA MDEQ No No No No Manganese (B) 7439965 4.7E-02 I/MDEQ NA MDEQ 3.0E-01 ATSDR NA MDEQ No No No No Mercury (Total) (Z,DD,KK) Varies Mercury, elemental 7439976 6.0E-05 MDEQ NA MDEQ 3.0E-01 IRIS NA MDEQ No No No No Mercuric chloride 7487947 3.0E-04 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No Methyl mercury (DD) 22967926 1.0E-04 IRIS NA MDEQ NA MDEQ NA MDEQ No No No Yes Methane (K) 74828 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Methanol (DD,OO) 67561 2.0E+00 IRIS NA MDEQ 2.0E+04 IRIS NA MDEQ No No Yes Yes Methoxychlor (DD,KK) 72435 5.0E-03 ATSDR NA MDEQ NA MDEQ NA MDEQ No No No Yes 2-Methoxyethanol (I,DD,OO) 109864 5E-03 PPRTV NA MDEQ 1.1E+00 PPRTV NA MDEQ No No No Yes 2-Methyl-4-chlorophenoxyacetic acid 94746 4.4E-03 OPP NA MDEQ 1.8E+01 O/MDEQ NA MDEQ No No No No 2-Methyl-4,6-dinitrophenol 534521 4.0E-04 A/MDEQ NA MDEQ 2.0E+00 MDEQ NA MDEQ No No No No N-Methyl-morpholine (I,OO) 109024 7.0E-02 E/MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Methyl parathion 298000 2E-04 OPP NA MDEQ NA MDEQ NA MDEQ No No No No 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 5.0E-02 MDEQ NA MDEQ 3E+03 IRIS NA MDEQ No No Yes No Methyl-tert-butyl ether (MTBE) 1634044 1.4E-01 MNDOH 3.4E-03 MDEQ 3E+03 IRIS 2.60E-07 CAEPA No No No No N-methylaniline 100618 2.0E-03 PPRTV NA MDEQ NA MDEQ NA MDEQ No No No No Methylcyclopentane (I) 96377 NA MDEQ NA MDEQ 7E+02 MDEQ NA MDEQ No No No No 4,4`-Methylene-bis-2-chloroaniline 101144 2E-03 PPRTV 7E-03 PPRTV NA MDEQ NA MDEQ Yes Yes No No (MBOCA) (MM) Methylene chloride (MM) 75092 6.0E-03 IRIS 2E-03 IRIS 6E+02 IRIS 1E-08 IRIS Yes Yes No No 2-Methylnaphthalene 91576 4E-03 IRIS NA MDEQ 1.0E+01 MDEQ NA MDEQ No No No No Methylphenols (JJ,KK) 1319773

321 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route 2-Methylphenol (DD,KK) 95487 2.0E-01 PPRTV NA MDEQ 1.0E+02 MDEQ NA PPRTV No No No Yes 3-Methylphenol (KK) 108394 5.0E-02 IRIS NA MDEQ 1.0E+02 MDEQ NA MDEQ No No No No 4-Methylphenol (KK) 106445 5.0E-03 P/MDEQ NA MDEQ 1.0E+02 MDEQ NA MDEQ No No No No Metolachlor 51218452 1.0E-01 OPP NA MDEQ NA MDEQ NA MDEQ No No No No Metribuzin 21087649 1.3E-02 OPP NA MDEQ NA MDEQ NA MDEQ No No No No Mirex 2385855 2E-04 IRIS 9.3E-01 MDEQ NA MDEQ NA MDEQ No No No No Molybdenum 7439987 5.0E-03 IRIS NA MDEQ 3.0E+01 MDEQ NA MDEQ No No No No Naphthalene 91203 1.0E-01 OPP NA MDEQ 3.0E+00 IRIS 3.4E-05 CAEPA No No No No Nickel (B) 7440020 6.0E-03 MDEQ NA MDEQ 9E-02 ATSDR 2.4E-04 IRIS No No No No Nitrate (N,DD) 14797558 1.6E+00 IRIS NA MDEQ NA MDEQ NA MDEQ No No No Yes Nitrite (N,DD) 14797650 1.0E-01 IRIS NA MDEQ NA MDEQ NA MDEQ No No No Yes Nitrobenzene (I,KK) 98953 2E-03 IRIS NA MDEQ 9.0E+00 IRIS 4E-05 IRIS No No No No 2-Nitrophenol 88755 2.0E-03 TCEQ NA MDEQ 5.0E-02 P/MDEQ NA MDEQ No No No No n-Nitroso-di-n-propylamine 621647 NA MDEQ 7.0E+00 IRIS NA MDEQ 2E-03 MDEQ No No No No N-Nitrosodiphenylamine 86306 2.5E-01 MDEQ 4.9E-03 IRIS NA MDEQ NA MDEQ No No No No Oxamyl 23135220 6.9E-03 OPP NA MDEQ 2.5E+01 MDEQ NA MDEQ No No No No Oxo-hexyl acetate (OO) 88230357 1.0E-02 MDEQ NA MDEQ 8.1E+01 MDEQ NA MDEQ No No No No Pendimethalin (DD) 40487421 3.0E-01 OPP NA MDEQ NA MDEQ NA MDEQ No No No Yes Pentachlorobenzene 608935 8.0E-04 IRIS NA MDEQ 1.0E-01 MDEQ NA MDEQ No No No No Pentachloronitrobenzene 82688 3.0E-03 IRIS NA MDEQ 1.1E+01 MDEQ NA MDEQ No No No No Pentachlorophenol (KK) 87865 5.0E-03 IRIS 4.0E-01 IRIS 2.0E+01 MDEQ 1.1E-04 MDEQ No No No No Pentane 109660 NA MDEQ NA MDEQ 1.0E+03 PPRTV NA MDEQ No No No No 2-Pentene (I) 109682 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Perchlorate (DD) 14797730 7.0E-04 IRIS NA MDEQ NA MDEQ NA MDEQ No No No Yes Perfluorooctanoic acid (DD) 335671 2.0E-05 USEPA 7.00E-02 USEPA NA MDEQ NA MDEQ No No No Yes Perfluorooctane sulfonic acid (DD) 1763231 2.0E-05 USEPA NA MDEQ NA MDEQ NA MDEQ No No No Yes pH NA NA MDEQ NA MDEQ NA MDEQ NA MDEQ NA NA No No Phenanthrene 85018 3.0E-02 TCEQ NA MDEQ 1.0E-01 MDEQ NA MDEQ No No No No Phenol (DD) 108952 3.0E-01 IRIS NA MDEQ 2.0E+02 MDEQ NA MDEQ No No No Yes Phenytoin (DD) 57410 3.0E-02 MDEQ 5.1E-02 MDEQ NA MDEQ 1.4E-05 MDEQ No No No Yes

322 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Phosphorus, Total Varies NA MDEQ NA MDEQ NA MDEQ NA MDEQ NA NA No No Phosphorus, White (R,DD) 7723140 2.0E-05 IRIS NA MDEQ 2.0E-01 A/MDEQ NA MDEQ No No No Yes o-Phthalic acid 88993 1.9E+00 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Phthalic anhydride 85449 2.0E+00 IRIS NA MDEQ 2.0E+01 MDEQ NA MDEQ No No No No Picloram 1918021 7.0E-02 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No Piperidine (OO) 110894 4.4E-04 MDEQ NA MDEQ 7.0E+03 ECHA NA MDEQ No No No No Polybrominated biphenyls (J,DD) 67774327 1.0E-02 ATSDR 7.2E+00 MDEQ NA MDEQ NA MDEQ No No No Yes Polychlorinated biphenyls (PCBs) 1336363 2.0E-05 IRIS 2.0E+00 IRIS NA MDEQ 1.0E-04 IRIS No No No Yes (J,T,DD) Polychlorinated biphenyls (PCBs) congeners (O) (O) (O) (O) (O) No No Yes Yes (DD,O) Prometon 1610180 5.0E-2 OPP NA MDEQ NA MDEQ NA MDEQ No No No No Propachlor 1918167 5.4E-2 OPP 3.2E-2 OPP NA MDEQ NA MDEQ No No No No Propazine 139402 1.8E-2 OPP NA MDEQ NA MDEQ NA MDEQ No No No No Propionic acid (OO) 79094 1.8E+0 MDEQ NA MDEQ 3.0E+2 MDEQ NA MDEQ No No No No Propyl alcohol (I,DD,OO) 71238 2.0E+00 MDEQ NA MDEQ 7.3E+2 MDEQ NA MDEQ No No Yes Yes n-Propylbenzene (I,DD) 103651 1.0E-1 PPRTV NA MDEQ 1.0E+03 PPRTV NA MDEQ No No Yes No Propylene glycol 57556 2E+1 PPRTV NA MDEQ NA MDEQ NA MDEQ No No No No Pyrene 129000 3.0E-2 IRIS NA MDEQ 1.0E+2 MDEQ NA MDEQ No No No No Pyridine (I,KK) 110861 1.0E-3 IRIS NA MDEQ 3.5E+0 MDEQ NA MDEQ No No No No Selenium (B,KK) 7782492 5.0E-3 IRIS NA MDEQ 2.0E+1 CAEPA NA MDEQ No No No No Silver (KK) 7440224 1.0E-3 OPP NA MDEQ 3.0E+0 OPP NA MDEQ No No No No Silvex (2,4,5-TP) (KK) 93721 8E-3 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No Simazine 122349 5.0E-3 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No Sodium 17341252 1.9E+1 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Sodium azide 26628228 1.2E-2 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Sodium bromide 7647156 4.0E-2 MDEQ NA MDEQ 1.4E+2 MDEQ NA MDEQ No No No No Strontium (B,DD) 7440246 6.0E-1 IRIS NA MDEQ NA MDEQ NA MDEQ No No No Yes Styrene 100425 2.0E-1 IRIS 1.3E-2 MDEQ 9.0E+2 ATSDR 5.7E-7 MDEQ No No No No Sulfate 14808798 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No

323 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Sulfolane 126330 0.001 PPRTV NA MDEQ 6.4 P/MDEQ NA MDEQ No No No No Tebuthiuron (DD) 34014181 7.0E-2 IRIS NA MDEQ NA MDEQ NA MDEQ No No No Yes 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416 NA MDEQ 7.5E+4 MDEQ NA MDEQ NA MDEQ No No No No 1,2,4,5-Tetrachlorobenzene (DD) 95943 7.0E-3 P/MDEQ NA MDEQ 1.0E+0 MDEQ NA MDEQ No No No Yes 2,3,7,8-Tetrachlorodibenzo-p-dioxin 1746016 7E-10 IRIS 7.5E+4 MDEQ 2.0E-6 MDEQ 4.4E+1 MDEQ No No Yes Yes (O,DD) 1,1,1,2-Tetrachloroethane 630206 3.0E-2 IRIS 2.6E-2 IRIS NA MDEQ 7.4E-6 IRIS No No No No 1,1,2,2-Tetrachloroethane 79345 2.0E-2 IRIS 2.0E-1 IRIS NA MDEQ 5.8E-5 MDEQ No No No No Tetrachloroethylene (KK) 127184 6.0E-3 IRIS 2.1E-3 IRIS 4.0E+1 IRIS 3.0E-7 IRIS No No No No Tetrahydrofuran (DD) 109999 9.0E-1 IRIS NA MDEQ 2.0E+3 IRIS NA MDEQ No No No Yes 1,1,3,3-Tetramethylurea (OO) 632224 NA MDEQ NA MDEQ 8.0E-1 MDEQ NA MDEQ No No No No Tetranitromethane 509148 NA MDEQ NA MDEQ 4.0E-1 MDEQ 1.5E-2 MDEQ No No No No Thallium 7440280 1.0E-5 PPRTV NA MDEQ 2.0E-1 MDEQ NA MDEQ No No No No Toluene (I) 108883 7.9E-2 IRIS NA MDEQ 5.0E+3 IRIS NA MDEQ No No No No p-Toluidine 106490 4E-3 PPRTV 3E-2 PPRTV 2 MDEQ 3.1E-5 MDEQ No No No No Total dissolved solids (TDS) NA NA MDEQ NA MDEQ NA MDEQ NA MDEQ NA NA No No Toxaphene (KK) 8001352 2.0E-4 A/MDEQ 1.1E+0 IRIS NA MDEQ 3.2E-4 IRIS No No No No Triallate (DD) 2303175 2.5E-2 OPP 7.2E-2 OPP 2.0E+2 O/MDEQ NA MDEQ No No Yes No Tributylamine 102829 3.5E-3 MDEQ NA MDEQ 7.0E+00 MDEQ NA MDEQ No No No No 1,2,3-Trichlorobenzene 87616 2.7E-3 P/MDEQ NA MDEQ 2.7E+1 MDEQ NA MDEQ No No No No 1,2,4-Trichlorobenzene 120821 1.0E-1 ATSDR 2.9E-02 PPRTV 2.0E+0 PPRTV NA MDEQ No No No No 1,1,1-Trichloroethane 71556 2.0E+0 IRIS NA MDEQ 5.0E+3 IRIS NA MDEQ No No No No 1,1,2-Trichloroethane 79005 4.0E-4 P/MDEQ 5.7E-2 IRIS 2.0E-4 PPRTV 1.6E-5 IRIS No No No No Trichloroethylene (DD,KK,MM,NN) 79016 5.0E-4 IRIS 4.6E-2 IRIS 2.0E+0 IRIS 4.1E-6 IRIS Yes Yes Yes Yes Trichlorofluoromethane 75694 3.0E-1 IRIS NA MDEQ 4.4E+2 P/MDEQ NA MDEQ No No No No 2,4,5-Trichlorophenol (KK) 95954 3.0E-2 PPRTV NA MDEQ 3.5E+2 MDEQ NA MDEQ No No No No 2,4,6-Trichlorophenol (DD,KK) 88062 1.0E-02 P/MDEQ 1.1E-02 IRIS NA MDEQ 3.1E-6 IRIS No No No Yes 1,2,3-Trichloropropane (MM) 96184 4.0E-3 IRIS 3.0E+1 IRIS 3.0E-1 IRIS NA MDEQ Yes Yes No No 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 2.7E+1 IRIS NA MDEQ 1.9E+4 MDEQ NA MDEQ No No No No Triethanolamine 102716 5.0E-1 MDEQ NA MDEQ 4.7E+0 ECHA NA MDEQ No No No No

324 2017 MR 22 – December 15, 2017 TABLE 1. TOXICOLOGICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(2).

Chemical Chronic Abstract Oral Inhalation Inhalation Developmental or Hazardous Substance Service Reference RfD Oral Slope SF Reference RfC Unit Risk IURF Mutagenic Reproductive Number Dose Source Factor Source Concentration Source Factor Source Carcinogen? Toxicant? RfD SF RfC IURF Inhalation Oral Inhalation Oral 3 3 -1 mg/kg-day (mg/kg-day)-1 µg/m (µg/m ) Route Route Route Route Triethylene glycol (DD) 112276 5.9E+0 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No Yes 3-Trifluoromethyl-4-nitrophenol (DD) 88302 6.2E-1 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No Yes Trifluralin 1582098 2.4E-2 OPP 2.96E-3 OPP 3.0E+3 OPP NA MDEQ No No No No 2,2,4-Trimethyl pentane 540841 NA MDEQ NA MDEQ 3.5E+3 MDEQ NA MDEQ No No No No 2,4,4-Trimethyl-2-pentene (I) 107404 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No 1,2,3-Trimethylbenzene (I, J) 526738 1.0E-2 IRIS NA MDEQ 6.0E+1 IRIS NA MDEQ No No No No 1,2,4-Trimethylbenzene (I, J) 95636 1.0E-2 IRIS NA MDEQ 6.0E+1 IRIS NA MDEQ No No No No 1,3,5-Trimethylbenzene (I, J) 108678 1.0E-2 IRIS NA MDEQ 6.0E+1 IRIS NA MDEQ No No No No Triphenyl phosphate 115866 1.6E-1 MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No tris(2,3-Dibromopropyl)phosphate 126727 NA MDEQ 1.1E+0 MDEQ NA MDEQ 5.3E-4 MDEQ No No No No Urea 57136 NA MDEQ NA MDEQ NA MDEQ NA MDEQ No No No No Vanadium (B) 7440622 7.0E-05 PPRTV NA MDEQ 1.0E-1 ATSDR NA MDEQ No No No No Vinyl acetate (I,DD) 108054 8.8E-1 MDEQ NA MDEQ 2.0E+2 IRIS NA MDEQ No No No Yes Vinyl chloride (KK,LL,MM) 75014 3.0E-3 ATSDR 7.2E-1 IRIS 8.0E+1 ATSDR 4.4E-6 IRIS Yes Yes No No Xylenes (I,J) 1330207 2.0E-1 ATSDR NA MDEQ 2.2E+2 ATSDR NA MDEQ No No No No Zinc (B) 7440666 3.0E-01 IRIS NA MDEQ NA MDEQ NA MDEQ No No No No

325 2017 MR 22 – December 15, 2017

TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Acenaphthene 83329 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acenaphthylene 208968 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acetaldehyde (I) 75070 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acetate 71501 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acetic acid (OO) 64197 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acetone (I) 67641 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acetonitrile 75058 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acetophenone (DD) 98862 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acrolein (I) 107028 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acrylamide (MM) 79061 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acrylic acid (DD,OO) 79107 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Acrylonitrile (I) 107131 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Alachlor 15972608 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Aldicarb 116063 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Aldicarb sulfone 1646884 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Aldicarb sulfoxide 1646873 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Aldrin 309002 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Aluminum (B,DD) 7429905 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Ammonia 7664417 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ t-Amyl methyl ether (TAME) 994058 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Aniline 62533 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Anthracene 120127 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Antimony 7440360 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.15 USEPA Arsenic (B,KK) 7440382 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.03 USEPA 1.0 MDEQ Asbestos (BB) 1332214 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0 MDEQ 1.0 MDEQ Atrazine 1912249 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Azobenzene 103333 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Barium (B,KK) 7440393 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.07 USEPA Benzene (I,KK) 71432 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ

326 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Benzidine (MM) 92875 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Benzo(a)anthracene (Q,MM) 56553 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.13 USEPA 1.0 MDEQ Benzo(b)fluoranthene (Q,MM) 205992 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.13 USEPA 1.0 MDEQ Benzo(k)fluoranthene (Q,MM) 207089 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.13 USEPA 1.0 MDEQ Benzo(g,h,i)perylene 191242 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.13 USEPA 1.0 MDEQ Benzo(a)pyrene (Q,DD,MM) 50328 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.13 USEPA 1.0 MDEQ Benzoic acid 65850 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Benzyl alcohol 100516 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Benzyl chloride 100447 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Beryllium (B) 7440417 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.007 USEPA bis(2-Chloroethoxy)ethane 112265 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ bis-2-Chloroethylether (I) 111444 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ bis(2-Ethylhexyl) phthalate (DD) 117817 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Boron (DD) 7440428 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Bromate 15541454 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Bromobenzene (I) 108861 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Bromodichloromethane (DD) 75274 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Bromoform 75252 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Bromomethane 74839 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ n-Butanol (I,OO) 71363 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Butanone (MEK) (I,DD,KK) 78933 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ n-Butyl acetate 123864 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ t-Butyl alcohol (OO) 75650 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Butyl benzyl phthalate (DD) 85687 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ n-Butylbenzene 104518 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ sec-Butylbenzene 135988 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ t-Butylbenzene (I) 98066 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Cadmium (B,KK) 7440439 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.001 USEPA 0.05 USEPA Camphene (I) 79925 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Caprolactam (DD) 105602 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Carbaryl (DD) 63252 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ

327 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Carbazole 86748 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Carbofuran (DD) 1563662 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Carbon disulfide (I,R,DD) 75150 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Carbon tetrachloride (KK) 56235 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Chlordane (J,KK) 57749 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.04 USEPA 1.0 MDEQ Chloride 16887006 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ 2-Chloroaniline 95512 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 4-Chloroaniline 106478 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Chlorobenzene (I,KK) 108907 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ p-Chlorobenzene sulfonic acid 98668 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1-Chloro-1,1-difluoroethane 75683 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Chloroethane (DD) 75003 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Chloroethyl vinyl ether 110758 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Chloroform (KK) 67663 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Chloromethane (I) 74873 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 4-Chloro-3-methylphenol (DD) 59507 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ beta-Chloronaphthalene 91587 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Chlorophenol (DD) 95578 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ o-Chlorotoluene (I) 95498 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Chlorpyrifos (DD) 2921882 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Chromium (III) (B,H,KK) 16065831 0.7 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.013 USEPA Chromium (VI) (H,KK,MM) 18540299 0.7 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.025 USEPA Chrysene (Q,MM) 218019 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.13 USEPA 1.0 MDEQ Cobalt (B) 7440484 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Copper (B) 7440508 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Cyanazine 21725462 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Cyanide (P,R,DD) 57125 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.01 MDEQ 1.0 MDEQ Cyclohexane (DD) 110827 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Cyclohexanone (OO) 108941 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dacthal 1861321 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dalapon 75990 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ

328 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless 4-4'-DDD 72548 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ 4-4'-DDE 72559 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ 4-4'-DDT (DD) 50293 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.03 USEPA 1.0 MDEQ Decabromodiphenyl ether (DD) 1163195 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Di-n-butyl phthalate (DD) 84742 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Di(2-ethylhexyl) adipate (DD) 103231 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Di-n-octyl phthalate 117840 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Diacetone alcohol (I,OO) 123422 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Diazinon 333415 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dibenzo(a,h)anthracene (Q,MM) 53703 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.13 USEPA 1.0 MDEQ Dibenzofuran 132649 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dibromochloromethane (MM) 124481 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dibromochloropropane (MM) 96128 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dibromomethane 74953 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dicamba (DD) 1918009 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,2-Dichlorobenzene 95501 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,3-Dichlorobenzene 541731 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,4-Dichlorobenzene (KK) 106467 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 3,3`-Dichlorobenzidine 91941 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dichlorodifluoromethane 75718 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,1-Dichloroethane 75343 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,2-Dichloroethane (I,KK) 107062 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,1-Dichloroethylene (I,KK) 75354 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ cis-1,2-Dichloroethylene 156592 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ trans-1,2-Dichloroethylene 156605 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,6-Dichloro-4-nitroaniline 99309 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,4-Dichlorophenol (DD) 120832 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,4-Dichlorophenoxyacetic acid (KK) 94757 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.05 USEPA 1.0 MDEQ 1,2-Dichloropropane (I) 78875 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,3-Dichloropropene (J) 542756 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dichlorvos (MM) 62737 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ

329 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Dicyclohexyl phthalate 84617 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Dieldrin 60571 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Diethyl ether 60297 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Diethyl phthalate 84662 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Diethylene glycol monobutyl ether 112345 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Diisopropyl ether (DD) 108203 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Diisopropylamine (I) 108189 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dimethyl phthalate 131113 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ N,N-Dimethylacetamide (OO) 127195 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ N,N-Dimethylaniline 121697 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dimethylformamide (I,OO) 68122 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,4-Dimethylphenol 105679 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,6-Dimethylphenol 576261 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 3,4-Dimethylphenol 95658 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dimethylsulfoxide 67685 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,4-Dinitrophenol 51285 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,4-Dinitrotoluene (KK) 121142 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dinoseb (DD) 88857 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,4-Dioxane (I,OO) 123911 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Diquat 85007 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Dissolved oxygen (DO) NA NR MDEQ NR MDEQ NR MDEQ NR MDEQ NR MDEQ NR MDEQ Diuron 330541 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Endosulfan (J) 115297 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Endothall 145733 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Endrin (KK) 72208 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Epichlorohydrin (I) 106898 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Ethanol (I,DD,OO) 64175 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Ethyl acetate (I) 141786 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Ethyl-tert-butyl ether (ETBE) 637923 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Ethylbenzene (I) 100414 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Ethylene dibromide 106934 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ

330 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Ethylene glycol (DD) 107211 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Ethylene glycol monobutyl ether 111762 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Ethylenediaminetetraacetic acid (EDTA) (II) 60004 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Fluoranthene 206440 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Fluorene 86737 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Fluorine (soluble fluoride) (DD) 7782414 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Formaldehyde (MM,OO) 50000 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Formic acid (I,U,OO) 64186 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1-Formylpiperidine (DD) 2591868 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Gentian violet 548629 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Glyphosate (DD) 1071836 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Heptachlor (DD,KK) 76448 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Heptachlor epoxide (KK) 1024573 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ n-Heptane 142825 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Hexabromobenzene 87821 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Hexachlorobenzene (C-66) (KK) 118741 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Hexachlorobutadiene (C-46) (KK) 87683 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ alpha-Hexachlorocyclohexane 319846 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ beta-Hexachlorocyclohexane 319857 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Hexachlorocyclopentadiene (C-56) 77474 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Hexachloroethane (KK) 67721 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ n-Hexane 110543 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Hexanone 591786 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Indeno(1,2,3-cd)pyrene (Q,MM) 193395 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.13 USEPA 1.0 MDEQ Iron (B) 7439896 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Isobutyl alcohol (I,OO) 78831 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Isophorone (DD) 78591 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Isopropyl alcohol (I,DD,OO) 67630 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Isopropyl benzene 98828 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Lead (B,L,DD,KK) 7439921 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Lindane (KK) 58899 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.04 USEPA 1.0 MDEQ

331 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Lithium (B,DD) 7439932 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Magnesium 7439954 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Manganese (B) 7439965 0.5 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.04 USEPA Mercury (Total) (Z,DD,KK) Varies Mercury, elemental 7439976 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Mercuric chloride 7487947 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.07 USEPA Methyl mercury (DD) 22967926 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Methane (K) 74828 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Methanol (DD,OO) 67561 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Methoxychlor (DD,KK) 72435 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Methoxyethanol (I,DD,OO) 109864 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Methyl-4-chlorophenoxyacetic acid 94746 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Methyl-4,6-dinitrophenol 534521 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ N-Methyl-morpholine (I,OO) 109024 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Methyl parathion 298000 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Methyl-tert-butyl ether (MTBE) 1634044 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ N-methylaniline 100618 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Methylcyclopentane (I) 96377 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 4,4`-Methylene-bis-2-chloroaniline 101144 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ (MBOCA) (MM) Methylene chloride (MM) 75092 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Methylnaphthalene 91576 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Methylphenols (JJ,KK) 1319773 2-Methylphenol (DD,KK) 95487 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 USEPA 3-Methylphenol (KK) 108394 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 USEPA 4-Methylphenol (KK) 106445 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 USEPA Metolachlor 51218452 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Metribuzin 21087649 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Mirex 2385855 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Molybdenum 7439987 0.4 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ

332 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Naphthalene 91203 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Nickel (B) 7440020 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.04 USEPA Nitrate (N,DD) 14797558 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Nitrite (N,DD) 14797650 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Nitrobenzene (I,KK) 98953 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Nitrophenol 88755 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ n-Nitroso-di-n-propylamine 621647 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ N-Nitrosodiphenylamine 86306 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Oxamyl 23135220 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Oxo-hexyl acetate (OO) 88230357 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Pendimethalin (DD) 40487421 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Pentachlorobenzene 608935 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Pentachloronitrobenzene 82688 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Pentachlorophenol (KK) 87865 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.25 USEPA 1.0 MDEQ Pentane 109660 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2-Pentene (I) 109682 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Perchlorate (DD) 14797730 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Perfluorooctanoic acid 335671 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Perfluorooctane sulfonic acid (DD) 1763231 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ pH NA NR MDEQ NR MDEQ NR MDEQ NR MDEQ NR MDEQ NR MDEQ Phenanthrene 85018 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Phenol (DD) 108952 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Phenytoin (DD) 57410 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Phosphorus, Total Varies 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Phosphorus, White (R,DD) 7723140 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ o-Phthalic acid 88993 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Phthalic anhydride 85449 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Picloram 1918021 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Piperidine (OO) 110894 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Polybrominated biphenyls (J,DD) 67774327 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ

333 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Polychlorinated biphenyls (PCBs) (J,T,DD) 1336363 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.14 USEPA 1.0 MDEQ Polychlorinated biphenyls (PCBs) congeners (O) (O) 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.03 USEPA 1.0 MDEQ Prometon 1610180 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Propachlor 1918167 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Propazine 139402 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Propionic acid (OO) 79094 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Propyl alcohol (I,DD,OO) 71238 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ n-Propylbenzene (I,DD) 103651 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Propylene glycol 57556 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Pyrene 129000 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Pyridine (I,KK) 110861 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Selenium (B,KK) 7782492 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Silver (KK) 7440224 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.04 USEPA Silvex (2,4,5-TP) (KK) 93721 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Simazine 122349 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Sodium 17341252 0.1 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Sodium azide 26628228 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Sodium bromide 7647156 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Strontium (B,DD) 7440246 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Styrene 100425 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Sulfate 14808798 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Sulfolane 126330 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Tebuthiuron (DD) 34014181 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.03 USEPA 1.0 MDEQ 1,2,4,5-Tetrachlorobenzene (DD) 95943 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,3,7,8-Tetrachlorodibenzo-p-dioxin (O,DD) 1746016 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.03 USEPA 1.0 MDEQ 1,1,1,2-Tetrachloroethane 630206 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,1,2,2-Tetrachloroethane 79345 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Tetrachloroethylene (KK) 127184 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Tetrahydrofuran (DD) 109999 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,1,3,3-Tetramethylurea (OO) 632224 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ

334 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Tetranitromethane 509148 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Thallium 7440280 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ Toluene (I) 108883 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ p-Toluidine 106490 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Total dissolved solids (TDS) NA NR MDEQ NR MDEQ NR MDEQ NR MDEQ NR MDEQ NR MDEQ Toxaphene (KK) 8001352 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ Triallate (DD) 2303175 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Tributylamine 102829 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,2,3-Trichlorobenzene 87616 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,2,4-Trichlorobenzene 120821 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,1,1-Trichloroethane 71556 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,1,2-Trichloroethane 79005 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Trichloroethylene (DD,KK,MM,NN) 79016 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Trichlorofluoromethane 75694 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,4,5-Trichlorophenol (KK) 95954 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,4,6-Trichlorophenol (DD,KK) 88062 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,2,3-Trichloropropane (MM) 96184 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Triethanolamine 102716 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Triethylene glycol (DD) 112276 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 3-Trifluoromethyl-4-nitrophenol (DD) 88302 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Trifluralin 1582098 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.1 MDEQ 1.0 MDEQ 2,2,4-Trimethyl pentane 540841 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 2,4,4-Trimethyl-2-pentene (I) 107404 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,2,3-Trimethylbenzene (I, J) 526738 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,2,4-Trimethylbenzene (I, J) 95636 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ 1,3,5-Trimethylbenzene (I, J) 108678 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Triphenyl phosphate 115866 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ tris(2,3-Dibromopropyl)phosphate 126727 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Urea 57136 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Vanadium (B) 7440622 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 0.026 USEPA

335 2017 MR 22 – December 15, 2017 TABLE 2. CHEMICAL‐SPECIFIC DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Hazardous substance footnotes are defined in R 299.49. Data sources are as defined in R 299.50(4) Relative Chemical Source Relative Relative Abstract Contribution Source Source Ingestion Dermal Gastrointestinal Service for Drinking RSCw Contribution RSCs Contribution RSCa Absorption AEi Absorption AEd Absorption ABSgi Number Water Source for Soil Source for Air Source Efficiency Source Efficiency Source Efficiency Source RSCw RSCs RSCa AEi AEd ABSgi Hazardous Substance unitless unitless unitless unitless unitless unitless Vinyl acetate (I,DD) 108054 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Vinyl chloride (KK,LL,MM) 75014 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Xylenes (I,J) 1330207 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 1.0 MDEQ 0.1 MDEQ 1.0 MDEQ Zinc (B) 7440666 0.2 MDEQ 1.0 MDEQ 1.0 MDEQ 0.5 MDEQ 0.01 MDEQ 1.0 MDEQ

336 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless Acenaphthene 83329 154.21 EPI Solid MDEQ 279 EXP EPI 93.4 EXP EPI 3.92 EXP EPI Acenaphthylene 208968 152.20 EPI Solid MDEQ 280 EXP EPI 92.5 EXP EPI 3.94 EXP EPI Acetaldehyde (I) 75070 44.05 EPI Gas MDEQ 20.1 EXP EPI -123.37 EXP EPI -0.34 EXP EPI Acetate 71501 59.04402 PC Liquid MDEQ 117.9 NA PC 16.6 EXP PC NA NA NA Acetic acid (OO) 64197 60.05 EPI Liquid MDEQ 117.9 EXP EPI 16.6 EXP EPI -0.17 EXP EPI Acetone (I) 67641 58.08 EPI Liquid MDEQ 56 EXP EPI -94.8 EXP EPI -0.24 EXP EPI Acetonitrile 75058 41.05 EPI Liquid MDEQ 81.6 EXP EPI -43.8 EXP EPI -0.34 EXP EPI Acetophenone (DD) 98862 120.15 EPI Liquid MDEQ 202 EXP EPI 20 EXP EPI 1.58 EXP EPI Acrolein (I) 107028 56.06 EPI Liquid MDEQ 52.6 EXP EPI -87.7 EXP EPI -0.01 EXP EPI Acrylamide (MM) 79061 71.08 EPI Solid MDEQ 192.6 EXP EPI 84.5 EXP EPI -0.67 EXP EPI Acrylic acid (DD,OO) 79107 72.06 EPI Liquid MDEQ 141 EXP EPI 12.5 EXP EPI 0.35 EXP EPI Acrylonitrile (I) 107131 53.06 EPI Liquid MDEQ 77.3 EXP EPI -83.5 EXP EPI 0.25 EXP EPI Alachlor 15972608 269.77 EPI Solid MDEQ 400 EXP PC 40 EXP EPI 3.52 EXP EPI Aldicarb 116063 190.26 EPI Solid MDEQ NA NA NA 99 EXP EPI 1.13 EXP EPI Aldicarb sulfone 1646884 222.26 EPI Solid MDEQ NA NA NA 140 EXP EPI -0.57 EXP EPI Aldicarb sulfoxide 1646873 206.26 EPI Solid MDEQ NA NA NA NA NA NA -0.78 EST PP Aldrin 309002 364.92 EPI Solid MDEQ 329.86 EXP EPA4 104 EXP EPI 6.50 EXP EPI Aluminum (B,DD) 7429905 30.01 EPI Inorganic MDEQ 2519 EXP CRC 660.323 EXP CRC NR NA NA Ammonia 7664417 17.03 EPI Gas MDEQ -33.35 EXP EPI -77.7 EXP EPI 0.23 EST PP t-Amyl methyl ether (TAME) 994058 102.18 EPI Liquid MDEQ 86.3 EXP EPI -80 EXP PC 1.55 EXP PP Aniline 62533 93.13 EPI Liquid MDEQ 184.17 EXP EPI -6.02 EXP EPI 0.90 EXP EPI Anthracene 120127 178.24 EPI Solid MDEQ 339.9 EXP EPI 215 EXP EPI 4.45 EXP EPI Antimony 7440360 124.78 EPI Inorganic MDEQ 1635 EXP PP 630 EXP PP NR NA NA Arsenic (B,KK) 7440382 77.95 EPI Inorganic MDEQ NA NA NA NA NA NA NR NA NA Asbestos (BB) 1332214 NA NA Inorganic MDEQ NA NA NA NA NA NA NR NA NA Atrazine 1912249 215.69 EPI Solid MDEQ NA NA NA 173 EXP EPI 2.61 EXP EPI Azobenzene 103333 182.23 EPI Solid MDEQ 293 EXP EPI 68 EXP EPI 3.82 EXP EPI Barium (B,KK) 7440393 137.33 EPI Inorganic MDEQ 1600 EXP PP 710 EXP PP NR NA NA Benzene (I,KK) 71432 78.11 EPI Liquid MDEQ 80 EXP EPI 5.5 EXP EPI 2.13 EXP EPI

337 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless Benzidine (MM) 92875 184.24 EPI Solid MDEQ 401 EXP EPI 120 EXP EPI 1.34 EXP EPI Benzo(a)anthracene (Q,MM) 56553 228.3 EPI Solid MDEQ 437.6 EXP EPI 84 EXP EPI 5.76 EXP EPI Benzo(b)fluoranthene (Q,MM) 205992 252.32 EPI Solid MDEQ 481 EXP PC 168 EXP EPI 5.78 EXP EPI Benzo(k)fluoranthene (Q,MM) 207089 252.32 EPI Solid MDEQ 480 EXP EPI 217 EXP EPI 6.11 EXP EPI Benzo(g,h,i)perylene 191242 276.34 EPI Solid MDEQ 500 EXP EPI 278 EXP EPI 6.63 EXP EPI Benzo(a)pyrene (Q,DD,MM) 50328 252.32 EPI Solid MDEQ 495 EXP EPI 176.5 EXP EPI 6.13 EXP EPI Benzoic acid 65850 122.12 EPI Solid MDEQ 249.2 EXP EPI 122.4 EXP EPI 1.87 EXP EPI Benzyl alcohol 100516 108.14 EPI Liquid MDEQ 205.3 EXP EPI -15.2 EXP EPI 1.10 EXP EPI Benzyl chloride 100447 126.59 EPI Liquid MDEQ 179 EXP EPI -45 EXP EPI 2.30 EXP EPI Beryllium (B) 7440417 9.01 EPI Inorganic MDEQ 2468 EXP HSDB 986 EXP PP NR NA NA bis(2-Chloroethoxy)ethane 112265 187.07 EPI Liquid MDEQ 232 EXP EPI -31.5 EXP EPI 1.28 EST PP bis-2-Chloroethylether (I) 111444 143.01 EPI Liquid MDEQ 178.5 EXP EPI -51.9 EXP EPI 1.29 EXP EPI bis(2-Ethylhexyl) phthalate (DD) 117817 390.57 EPI Liquid MDEQ 384 EXP EPI -55 EXP EPI 7.60 EXP EPI Boron (DD) 7440428 10.806 CRC Inorganic MDEQ 4000 EXP CRC 2077 EXP CRC NR NA NA Bromate 15541454 127.9022 PC Inorganic MDEQ NA NA NA NA NA NA NR NA NA Bromobenzene (I) 108861 157.01 EPI Liquid MDEQ 156 EXP EPI -30.6 EXP EPI 2.99 EXP EPI Bromodichloromethane (DD) 75274 163.83 EPI Liquid MDEQ 90 EXP EPI -57 EXP EPI 2.00 EXP EPI Bromoform 75252 252.73 EPI Liquid MDEQ 149.1 EXP EPI 8 EXP EPI 2.40 EXP EPI Bromomethane 74839 94.94 EPI Gas MDEQ 3.5 EXP EPI -93.7 EXP EPI 1.19 EXP EPI n-Butanol (I,OO) 71363 74.12 EPI Liquid MDEQ 117.7 EXP EPI -89.8 EXP EPI 0.88 EXP EPI 2-Butanone (MEK) (I,DD,KK) 78933 72.11 EPI Liquid MDEQ 79.5 EXP EPI -86.6 EXP EPI 0.29 EXP EPI n-Butyl acetate 123864 116.16 EPI Liquid MDEQ 126.1 EXP EPI -78 EXP EPI 1.78 EXP EPI t-Butyl alcohol (OO) 75650 74.12 EPI Solid MDEQ 82.4 EXP EPI 25.4 EXP EPI 0.35 EXP EPI Butyl benzyl phthalate (DD) 85687 312.37 EPI Solid MDEQ 370 EXP EPI 25 EXP EPI 4.73 EXP EPI n-Butylbenzene 104518 134.22 EPI Liquid MDEQ 183.3 EXP EPI -87.9 EXP EPI 4.38 EXP EPI sec-Butylbenzene 135988 134.22 EPI Liquid MDEQ 173.5 EXP EPI -82.7 EXP EPI 4.57 EXP EPI t-Butylbenzene (I) 98066 134.22 EPI Liquid MDEQ 169.1 EXP EPI -57.8 EXP EPI 4.11 EXP EPI Cadmium (B,KK) 7440439 112.4 PP Inorganic MDEQ 765 EXP PP 321 EXP PP NR NA NA Camphene (I) 79925 136.24 EPI Solid MDEQ 160 EXP EPI 51.2 EXP EPI 4.22 EXP PP

338 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless Caprolactam (DD) 105602 113.16 EPI Solid MDEQ 270 EXP EPI 69.3 EXP EPI 0.66 EST PP Carbaryl (DD) 63252 201.23 EPI Solid MDEQ 315 EXP EPI 145 EXP EPI 2.36 EXP EPI Carbazole 86748 167.21 EPI Solid MDEQ 354.7 EXP EPI 346.2 EXP EPI 3.72 EXP EPI Carbofuran (DD) 1563662 221.26 EPI Solid MDEQ NA NA NA 151 EXP EPI 2.32 EXP EPI Carbon disulfide (I,R,DD) 75150 76.13 EPI Liquid MDEQ 46 EXP EPI -111.5 EXP EPI 1.94 EXP EPI Carbon tetrachloride (KK) 56235 153.82 EPI Liquid MDEQ 76.8 EXP EPI -23 EXP EPI 2.83 EXP EPI Chlordane (J,KK) 57749 409.78 EPI Solid MDEQ 351.1 EXP EPA4 106 EXP EPI 6.16 EXP EPI Chloride 16887006 35.45 EPI Inorganic MDEQ NA NA NA NA NA NA NR NA NA 2-Chloroaniline 95512 127.57 EPI Liquid MDEQ 208.8 EXP EPI -14 EXP EPI 1.90 EXP EPI 4-Chloroaniline 106478 127.57 EPI Solid MDEQ 232 EXP EPI 72.5 EXP EPI 1.83 EXP EPI Chlorobenzene (I,KK) 108907 112.56 EPI Liquid MDEQ 131.7 EXP EPI -45.31 EXP EPI 2.84 EXP EPI p-Chlorobenzene sulfonic acid 98668 192.62 EPI Solid MDEQ NA NA NA 67 EXP EPI -0.52 EST PP 1-Chloro-1,1-difluoroethane 75683 100.5 EPI Gas MDEQ -9.1 EXP EPI -130.8 EXP EPI 2.05 EST PP Chloroethane (DD) 75003 64.52 EPI Gas MDEQ 12.3 EXP EPI -138.7 EXP EPI 1.43 EXP EPI 2-Chloroethyl vinyl ether 110758 106.55 EPI Liquid MDEQ 108 EXP EPI -70 EXP EPI 1.17 EST PP Chloroform (KK) 67663 119.38 EPI Liquid MDEQ 61.1 EXP EPI -63.6 EXP EPI 1.97 EXP EPI Chloromethane (I) 74873 50.49 EPI Gas MDEQ -24 EXP EPI -97.7 EXP EPI 0.91 EXP EPI 4-Chloro-3-methylphenol (DD) 59507 142.59 EPI Solid MDEQ 235 EXP EPI 67 EXP EPI 3.10 EXP EPI beta-Chloronaphthalene 91587 162.62 EPI Solid MDEQ 256 EXP EPI 61 EXP EPI 3.90 EXP EPI 2-Chlorophenol (DD) 95578 128.56 EPI Liquid MDEQ 174.9 EXP EPI 9.8 EXP EPI 2.15 EXP EPI o-Chlorotoluene (I) 95498 126.59 EPI Liquid MDEQ 159 EXP EPI -35.6 EXP EPI 3.42 EXP EPI Chlorpyrifos (DD) 2921882 350.59 EPI Solid MDEQ 160 EXP HSDB 42 EXP EPI 4.96 EXP EPI Chromium (III) (B,H,KK) 16065831 51.996 PP Inorganic MDEQ 2642 EXP PP 1900 EXP PP NR NA NA Chromium (VI) (H,KK,MM) 18540299 51.996 PP Inorganic MDEQ 2642 EXP PP 1900 EXP PP NR NA NA Chrysene (Q,MM) 218019 228.3 PP Solid MDEQ 448 EXP PP 258.2 EXP PP 5.81 EXP PP Cobalt (B) 7440484 58.93 EPI Inorganic MDEQ 2927 EXP HSDB 1495 EXP HSDB NR NA NA Copper (B) 7440508 63.55 EPI Inorganic MDEQ 2595 EXP PP 1083 EXP PP NR NA NA Cyanazine 21725462 240.70 EPI Solid MDEQ NA NA NA 168 EXP EPI 2.22 EXP EPI Cyanide (P,R,DD) 57125 26.018 PP Inorganic MDEQ NA NA NA NA NA NA NR NA NA

339 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless Cyclohexane (DD) 110827 84.16 EPI Liquid MDEQ 80.7 EXP EPI 6.6 EXP EPI 3.44 EXP EPI Cyclohexanone (OO) 108941 98.15 EPI Liquid MDEQ 155.4 EXP EPI -31 EXP EPI 0.81 EXP EPI Dacthal 1861321 331.97 EPI Solid MDEQ 365 EXP EPI 155 EXP EPI 4.28 EXP EPI Dalapon 75990 142.97 EPI Liquid MDEQ 187.5 EXP EPI -5 EXP EPI 0.78 EXP EPI 4-4'-DDD 72548 320.05 EPI Solid MDEQ 350 EXP EPI 109.5 EXP EPI 6.02 EXP EPI 4-4'-DDE 72559 318.03 EPI Solid MDEQ 336 EXP EPI 89 EXP EPI 6.51 EXP EPI 4-4'-DDT (DD) 50293 354.49 EPI Solid MDEQ 260 EXP EPI 108.5 EXP EPI 6.91 EXP EPI Decabromodiphenyl ether (DD) 1163195 959.17 EPI Solid MDEQ 530 EXP EPI 305 EXP EPI 12.11 EST PP Di-n-butyl phthalate (DD) 84742 278.35 EPI Liquid MDEQ 340 EXP EPI -35 EXP EPI 4.50 EXP EPI Di(2-ethylhexyl) adipate (DD) 103231 370.58 EPI Liquid MDEQ 417 EXP EPI -67.8 EXP EPI 6.11 EST PP Di-n-octyl phthalate 117840 390.57 EPI Solid MDEQ NA NA NA 25 EXP EPI 8.10 EXP EPI Diacetone alcohol (I,OO) 123422 116.16 EPI Liquid MDEQ 167.9 EXP EPI -44 EXP EPI -0.34 EST PP Diazinon 333415 304.35 EPI Solid MDEQ NA NA NA 25 EXP EPI 3.81 EXP EPI Dibenzo(a,h)anthracene (Q,MM) 53703 278.36 EPI Solid MDEQ 524 EXP EPI 269.5 EXP EPI 6.75 EXP EPI Dibenzofuran 132649 168.20 EPI Solid MDEQ 287 EXP EPI 86.5 EXP EPI 4.12 EXP EPI Dibromochloromethane (MM) 124481 208.28 EPI Liquid MDEQ 120 EXP EPI -20 EXP EPI 2.16 EXP EPI Dibromochloropropane (MM) 96128 236.33 EPI Liquid MDEQ 196 EXP EPI 6 EXP EPI 2.96 EXP EPI Dibromomethane 74953 173.84 EPI Liquid MDEQ 97 EXP EPI -52.5 EXP EPI 1.70 EXP EPI Dicamba (DD) 1918009 221.04 EPI Solid MDEQ NA NA NA 115 EXP EPI 2.21 EXP EPI 1,2-Dichlorobenzene 95501 147.00 EPI Liquid MDEQ 180 EXP EPI -16.7 EXP EPI 3.43 EXP EPI 1,3-Dichlorobenzene 541731 147.00 EPI Liquid MDEQ 173 EXP EPI -24.8 EXP EPI 3.53 EXP EPI 1,4-Dichlorobenzene (KK) 106467 147.00 EPI Solid MDEQ 174 EXP EPI 52.09 EXP EPI 3.44 EXP EPI 3,3`-Dichlorobenzidine 91941 253.13 EPI Solid MDEQ 368 EXP EPI 132 EXP EPI 3.51 EXP EPI Dichlorodifluoromethane 75718 120.91 EPI Gas MDEQ -29.8 EXP EPI -158 EXP EPI 2.16 EXP EPI 1,1-Dichloroethane 75343 98.96 EPI Liquid MDEQ 57.4 EXP EPI -96.9 EXP EPI 1.79 EXP EPI 1,2-Dichloroethane (I,KK) 107062 98.96 EPI Liquid MDEQ 83.5 EXP EPI -35.5 EXP EPI 1.48 EXP EPI 1,1-Dichloroethylene (I,KK) 75354 96.94 EPI Liquid MDEQ 31.7 EXP EPI -122.5 EXP EPI 2.13 EXP EPI cis-1,2-Dichloroethylene 156592 96.94 EPI Liquid MDEQ 60.1 EXP EPI -80 EXP EPI 1.86 EXP EPI trans-1,2-Dichloroethylene 156605 96.94 EPI Liquid MDEQ 48.7 EXP PP -49.8 EXP PP 2.09 EXP PP

340 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless 2,6-Dichloro-4-nitroaniline 99309 207.02 EPI Solid MDEQ NA NA NA 191 EXP EPI 2.80 EXP EPI 2,4-Dichlorophenol (DD) 120832 163.00 EPI Solid MDEQ 210 EXP EPI 45 EXP EPI 3.06 EXP EPI 2,4-Dichlorophenoxyacetic acid (KK) 94757 221.04 EPI Solid MDEQ NA NA NA 140.5 EXP EPI 2.81 EXP EPI 1,2-Dichloropropane (I) 78875 112.99 EPI Liquid MDEQ 95.5 EXP EPI -100 EXP EPI 1.98 EXP EPI 1,3-Dichloropropene (J) 542756 110.97 EPI Liquid MDEQ 112 EXP EPI -50 EXP EPI 2.04 EXP EPI Dichlorvos (MM) 62737 220.98 EPI Liquid MDEQ 234.1 EXP EPI -60 EXP EPI 1.43 EXP EPI Dicyclohexyl phthalate 84617 330.43 EPI Solid MDEQ NA NA NA 66 EXP EPI NA NA NA Dieldrin 60571 380.91 EPI Solid MDEQ 330 EXP EPI 175.5 EXP EPI 5.40 EXP EPI Diethyl ether 60297 74.12 EPI Liquid MDEQ 34.6 EXP EPI -116.3 EXP EPI 0.89 EXP EPI Diethyl phthalate 84662 222.24 EPI Liquid MDEQ 295 EXP EPI -40.5 EXP EPI 2.42 EXP EPI Diethylene glycol monobutyl ether 112345 162.23 EPI Liquid MDEQ 231 EXP EPI -68 EXP EPI 0.56 EXP EPI Diisopropyl ether (DD) 108203 102.18 EPI Liquid MDEQ 68.5 EXP EPI -86.8 EXP EPI 1.52 EXP EPI Diisopropylamine (I) 108189 101.19 EPI Liquid MDEQ 83.9 EXP EPI -61 EXP EPI 1.40 EXP EPI Dimethyl phthalate 131113 194.19 EPI Liquid MDEQ 283.7 EXP EPI 5.5 EXP EPI 1.60 EXP EPI N,N-Dimethylacetamide (OO) 127195 87.12 EPI Liquid MDEQ 165 EXP EPI -20 EXP EPI -0.77 EXP EPI N,N-Dimethylaniline 121697 121.18 EPI Liquid MDEQ 193.45 EXP EPI 2.5 EXP EPI 2.31 EXP EPI Dimethylformamide (I,OO) 68122 73.10 EPI Liquid MDEQ 153 EXP EPI -60.4 EXP EPI -1.01 EXP EPI 2,4-Dimethylphenol 105679 122.17 EPI Solid MDEQ 210.9 EXP EPI 24.5 EXP EPI 2.30 EXP EPI 2,6-Dimethylphenol 576261 122.17 EPI Solid MDEQ 201 EXP EPI 45.7 EXP EPI 2.36 EXP EPI 3,4-Dimethylphenol 95658 122.17 EPI Solid MDEQ 227 EXP EPI 60.8 EXP EPI 2.23 EXP EPI Dimethylsulfoxide 67685 78.13 EPI Liquid MDEQ 189 EXP EPI 18.5 EXP EPI -1.35 EXP EPI 2,4-Dinitrophenol 51285 184.11 EPI Solid MDEQ NA NA NA 115.5 EXP EPI 1.67 EXP EPI 2,4-Dinitrotoluene (KK) 121142 182.14 EPI Solid MDEQ 300 EXP EPI 71 EXP EPI 1.98 EXP EPI Dinoseb (DD) 88857 240.22 EPI Solid MDEQ 332 EXP EPI 40 EXP EPI 3.56 EXP EPI 1,4-Dioxane (I,OO) 123911 88.11 EPI Liquid MDEQ 101.5 EXP EPI 11.8 EXP EPI -0.27 EXP EPI Diquat 85007 344.05 EPI Solid MDEQ NA NA NA 337 EXP PP -4.60 EXP PP Dissolved oxygen (DO) NA NA NA NA MDEQ NA NA NA NA NA NA NR NA NA Diuron 330541 233.10 EPI Solid MDEQ NA NA NA 158 EXP EPI 2.68 EXP EPI Endosulfan (J) 115297 406.92 EPI Solid MDEQ NA NA NA 106 EXP EPI 3.83 EXP EPI

341 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless Endothall 145733 186.17 EPI Solid MDEQ NA NA NA 144 EXP EPI 1.91 EXP EPI Endrin (KK) 72208 380.91 PP Solid MDEQ NA NA NA 228 EXP PP 5.20 EXP PP Epichlorohydrin (I) 106898 92.53 EPI Liquid MDEQ 116.11 EXP EPI -57.2 EXP EPI 0.45 EXP EPI Ethanol (I,DD,OO) 64175 46.07 EPI Liquid MDEQ 78.2 EXP EPI -114.1 EXP EPI -0.31 EXP EPI Ethyl acetate (I) 141786 88.11 EPI Liquid MDEQ 77.1 EXP EPI -83.6 EXP EPI 0.73 EXP EPI Ethyl-tert-butyl ether (ETBE) 637923 102.18 EPI Liquid MDEQ 73.1 EXP EPI -94 EXP EPI 1.92 EST PP Ethylbenzene (I) 100414 106.17 EPI Liquid MDEQ 136.1 EXP EPI -94.9 EXP EPI 3.15 EXP EPI Ethylene dibromide 106934 187.86 EPI Liquid MDEQ 131.6 EXP EPI 9.9 EXP EPI 1.96 EXP EPI Ethylene glycol (DD) 107211 62.07 EPI Liquid MDEQ 197.3 EXP EPI -13 EXP EPI -1.36 EXP EPI Ethylene glycol monobutyl ether 111762 118.18 EPI Liquid MDEQ 168.4 EXP EPI -74.8 EXP EPI 0.83 EXP EPI Ethylenediaminetetraacetic acid (EDTA) (II) 60004 292.25 EPI Solid MDEQ NA NA NA 245 EXP EPI -3.86 EST PP Fluoranthene 206440 202.26 EPI Solid MDEQ 384 EXP EPI 107.8 EXP EPI 5.16 EXP EPI Fluorene 86737 166.22 EPI Solid MDEQ 295 EXP EPI 114.8 EXP EPI 4.18 EXP EPI Fluorine (soluble fluoride) (DD) 7782414 38.00 EPI Inorganic MDEQ -188.13 EXP EPI -219.61 EXP EPI NR NA NA Formaldehyde (MM,OO) 50000 30.03 EPI Gas MDEQ -19.5 EXP EPI -92 EXP EPI 0.35 EXP EPI Formic acid (I,U,OO) 64186 46.03 EPI Liquid MDEQ 101 EXP EPI 8.3 EXP EPI -0.54 EXP EPI 1-Formylpiperidine (DD) 2591868 113.16 EPI Liquid MDEQ 222.5 EXP EPI -30.8 EXP EPI 0.43 EST PP Gentian violet 548629 407.99 EPI Solid MDEQ NA NA NA 215 EXP EPI 0.96 EXP EPI Glyphosate (DD) 1071836 169.07 EPI Solid MDEQ NA NA NA 189.5 EXP EPI -3.40 EXP EPI Heptachlor (DD,KK) 76448 373.32 EPI Solid MDEQ 310 EXP PP 95.5 EXP PP 6.10 EXP PP Heptachlor epoxide (KK) 1024573 389.32 EPI Solid MDEQ NA NA NA 160 EXP EPI 4.98 EXP EPI n-Heptane 142825 100.21 EPI Liquid MDEQ 98.5 EXP EPI -90.6 EXP EPI 4.66 EXP EPI Hexabromobenzene 87821 551.49 EPI Solid MDEQ NA NA NA 326 EXP EPI 6.07 EXP EPI Hexachlorobenzene (C-66) (KK) 118741 284.78 EPI Solid MDEQ 325 EXP EPI 231.8 EXP EPI 5.73 EXP EPI Hexachlorobutadiene (C-46) (KK) 87683 260.76 EPI Liquid MDEQ 215 EXP EPI -21 EXP EPI 4.78 EXP EPI alpha-Hexachlorocyclohexane 319846 290.83 EPI Solid MDEQ 288 EXP PP 159.5 EXP PP 3.80 EXP PP beta-Hexachlorocyclohexane 319857 290.83 EPI Solid MDEQ 323.4 EXP PC 314.5 EXP PP 3.78 EXP PP Hexachlorocyclopentadiene (C-56) 77474 272.77 EPI Liquid MDEQ 239 EXP EPI -9 EXP EPI 5.40 EXP EPI Hexachloroethane (KK) 67721 236.74 EPI Solid MDEQ 184.85 EXP EPA4 187 EXP EPI 4.14 EXP EPI

342 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless n-Hexane 110543 86.18 EPI Liquid MDEQ 68.7 EXP EPI -95.3 EXP EPI 3.90 EXP EPI 2-Hexanone 591786 100.16 EPI Liquid MDEQ 127.6 EXP EPI -55.5 EXP EPI 1.38 EXP EPI Indeno(1,2,3-cd)pyrene (Q,MM) 193395 276.34 EPI Solid MDEQ 536 EXP EPI 163.6 EXP EPI 6.54 EXP SSG Iron (B) 7439896 55.85 EPI Inorganic MDEQ 2861 EXP CRC 1538 EXP CRC NR NA NA Isobutyl alcohol (I,OO) 78831 74.12 EPI Liquid MDEQ 107.8 EXP EPI -108 EXP EPI 0.76 EXP EPI Isophorone (DD) 78591 138.21 EPI Liquid MDEQ 215.2 EXP EPI -8.1 EXP EPI 1.70 EXP EPI Isopropyl alcohol (I,DD,OO) 67630 60.10 EPI Liquid MDEQ 82.3 EXP EPI -89.5 EXP EPI 0.05 EXP EPI Isopropyl benzene 98828 120.20 EPI Liquid MDEQ 152.4 EXP EPI -96 EXP EPI 3.66 EXP EPI Lead (B,L,DD,KK) 7439921 207.20 EPI Inorganic MDEQ 1749 EXP CRC 327.462 EXP CRC NR NA NA Lindane (KK) 58899 290.83 EPI Solid MDEQ 323.4 EXP EPI 112.5 EXP EPI 3.72 EXP EPI Lithium (B,DD) 7439932 6.94 EPI Inorganic MDEQ 1342 EXP CRC 180.5 EXP CRC NR NA NA Magnesium 7439954 24.304 CRC Inorganic MDEQ 1090 EXP CRC 650 EXP CRC NR NA NA Manganese (B) 7439965 54.94 EPI Inorganic MDEQ 2061 EXP CRC 1246 EXP CRC NR NA NA Mercury (Total) (Z,DD,KK) Varies Mercury, elemental 7439976 200.59 EPI Inorganic MDEQ 356.619 EXP CRC -38.8 EXP PP 0.62 EST SCDM Mercuric chloride 7487947 271.50 EPI Inorganic MDEQ 302 EXP HSDB 277 EXP EPI NR NA NA Methyl mercury (DD) 22967926 215.63 EPI Inorganic MDEQ NA NA NA NA NA NA NA NA NA Methane (K) 74828 16.04 EPI Gas MDEQ -161.5 EXP EPI -182.4 EXP EPI 1.09 EXP EPI Methanol (DD,OO) 67561 32.04 EPI Liquid MDEQ 64.7 EXP EPI -97.6 EXP EPI -0.77 EXP EPI Methoxychlor (DD,KK) 72435 345.66 EPI Solid MDEQ 346 EXP EPI 87 EXP EPI 5.08 EXP EPI 2-Methoxyethanol (I,DD,OO) 109864 76.10 EPI Liquid MDEQ 124.1 EXP EPI -85.1 EXP EPI -0.77 EXP EPI 2-Methyl-4-chlorophenoxyacetic acid 94746 200.62 EPI Solid MDEQ 286.74 EXP EPI 120 EXP EPI 3.25 EXP EPI 2-Methyl-4,6-dinitrophenol 534521 198.14 EPI Solid MDEQ 378 EXP EPI 86.6 EXP EPI 2.13 EXP EPI N-Methyl-morpholine (I,OO) 109024 101.15 EPI Liquid MDEQ 116 EXP EPI -64.4 EXP CRC -0.33 EXP EPI Methyl parathion 298000 263.21 EPI Solid MDEQ NA NA NA 35.5 EXP EPI 2.86 EXP EPI 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 100.16 EPI Liquid MDEQ 116.5 EXP EPI -84 EXP EPI 1.31 EXP EPI Methyl-tert-butyl ether (MTBE) 1634044 88.15 EPI Liquid MDEQ 55.2 EXP EPI -108.6 EXP EPI 0.94 EXP EPI N-methylaniline 100618 107.16 EPI Liquid MDEQ 196.2 EXP EPI -57 EXP EPI 1.66 EXP EPI Methylcyclopentane (I) 96377 84.16 EPI Liquid MDEQ 71.8 EXP EPI -142.5 EXP EPI 3.37 EXP EPI

343 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless 4,4`-Methylene-bis-2-chloroaniline (MBOCA) (MM) 101144 267.16 EPI Solid MDEQ 378.9 EXP EPI 110 EXP EPI 3.91 EXP EPI Methylene chloride (MM) 75092 84.93 EPI Liquid MDEQ 40 EXP EPI -95.1 EXP EPI 1.25 EXP EPI 2-Methylnaphthalene 91576 142.20 EPI Solid MDEQ 241.1 EXP EPI 34.4 EXP EPI 3.86 EXP EPI Methylphenols (JJ,KK) 1319773 2-Methylphenol (DD,KK) 95487 108.14 EPI Solid MDEQ 191 EXP EPI 29.8 EXP EPI 1.95 EXP EPI 3-Methylphenol (KK) 108394 108.14 EPI Liquid MDEQ 202.2 EXP EPI 11.8 EXP EPI 1.96 EXP EPI 4-Methylphenol (KK) 106445 108.14 EPI Solid MDEQ 201.9 EXP EPI 35.5 EXP EPI 1.94 EXP EPI Metolachlor 51218452 283.80 EPI Liquid MDEQ NA NA NA -62.1 EXP EPI 3.13 EXP EPI Metribuzin 21087649 214.29 EPI Solid MDEQ NA NA NA 126 EXP EPI 1.70 EXP EPI Mirex 2385855 545.55 EPI Solid MDEQ NA NA NA NA NA NA 6.89 EXP EPI Molybdenum 7439987 95.94 EPI Inorganic MDEQ 4639 EXP CRC 2622 EXP PP NR NA NA Naphthalene 91203 128.18 EPI Solid MDEQ 217.9 EXP EPI 80.2 EXP EPI 3.30 EXP EPI Nickel (B) 7440020 58.69 EPI Inorganic MDEQ 2913 EXP CRC 1455 EXP CRC NR NA NA Nitrate (N,DD) 14797558 62.00 EPI Inorganic MDEQ NA NA NA NA NA NA NR NA NA Nitrite (N,DD) 14797650 47.01 EPI Inorganic MDEQ NA NA NA NA NA NA NR NA NA Nitrobenzene (I,KK) 98953 123.11 EPI Liquid MDEQ 210.8 EXP EPI 5.7 EXP EPI 1.85 EXP EPI 2-Nitrophenol 88755 139.11 EPI Solid MDEQ 216 EXP EPI 44.8 EXP EPI 1.79 EXP EPI n-Nitroso-di-n-propylamine 621647 130.19 EPI Liquid MDEQ 206 EXP EPI NA NA NA 1.36 EXP EPI N-Nitrosodiphenylamine 86306 198.23 EPI Solid MDEQ 101 EXP PC 66.5 EXP EPI 3.13 EXP EPI Oxamyl 23135220 219.26 EPI Solid MDEQ NA NA NA 101 EXP EPI -0.47 EXP EPI Oxo-hexyl acetate (OO) 88230357 144.22 EPI Liquid MDEQ NA NA NA NA NA NA NA NA NA Pendimethalin (DD) 40487421 281.31 EPI Solid MDEQ 330 EXP EPI 56 EXP EPI 5.20 EXP EPI Pentachlorobenzene 608935 250.34 EPI Solid MDEQ 277 EXP EPI 86 EXP EPI 5.17 EXP EPI Pentachloronitrobenzene 82688 295.34 EPI Solid MDEQ 328 EXP EPI 144 EXP EPI 4.64 EXP EPI Pentachlorophenol (KK) 87865 266.34 EPI Solid MDEQ 310 EXP EPI 174 EXP EPI 5.12 EXP EPI Pentane 109660 72.15 EPI Liquid MDEQ 36 EXP EPI -129.7 EXP EPI 3.39 EXP EPI 2-Pentene (I) 109682 70.14 EPI Liquid MDEQ 37 EXP EPI -151.4 EXP PC 2.58 EST PP Perchlorate (DD) 14797730 99.4506 PC Inorganic MDEQ NA NA NA NA NA NA NR NA NA Perfluorooctanoic acid 335671 414.07 EPI Solid MDEQ 192.4 EXP PP 55 EXP EPI 6.30 EST PP

344 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless Perfluorooctane sulfonic acid (DD) 1763231 500.13 EPI Liquid MDEQ 258 EXP EPI NA NA NA 6.28 EST PC pH NA NA NA NA MDEQ NA NA NA NA NA NA NR NA NA Phenanthrene 85018 178.24 EPI Solid MDEQ 340 EXP EPI 99.24 EXP EPI 4.46 EXP EPI Phenol (DD) 108952 94.11 EPI Solid MDEQ 181.8 EXP EPI 40.9 EXP EPI 1.46 EXP EPI Phenytoin (DD) 57410 252.27 EPI Solid MDEQ NA NA NA 295 EXP EPI 2.47 EXP EPI Phosphorus, Total Varies NA NA NA MDEQ NA NA NA NA NA NA NA NA NA Phosphorus, White (R,DD) 7723140 34 EPI Inorganic MDEQ 280 EXP EPI 44.1 EXP EPI NR NA NA o-Phthalic acid 88993 166.13 EPI Solid MDEQ NA NA NA 230 EXP EPI 0.73 EXP EPI Phthalic anhydride 85449 148.12 EPI Solid MDEQ 295 EXP EPI 130.8 EXP EPI 1.60 EXP EPI Picloram 1918021 241.46 EPI Solid MDEQ NA NA NA 218.5 EXP EPI 1.90 EXP EPI Piperidine (OO) 110894 85.15 EPI Liquid MDEQ 106 EXP EPI -7 EXP EPI 0.84 EXP EPI Polybrominated biphenyls (J,DD) 67774327 627.58416 PC Solid MDEQ 72 EXP PC NA NA NA 6.39 EXP PC Polychlorinated biphenyls (PCBs) (J,T,DD) 1336363 291.99 EPI Solid MDEQ 357.5 EXP HSDB NA NA NA 7.10 EXP EPI Polychlorinated biphenyls (PCBs) congeners (O) (O) Prometon 1610180 225.30 EPI Solid MDEQ NA NA NA 91 EXP EPI 2.99 EXP EPI Propachlor 1918167 211.69 EPI Solid MDEQ 110 EXP PP 77 EXP EPI 2.18 EXP EPI Propazine 139402 229.71 EPI Solid MDEQ NA NA NA 213 EXP EPI 2.93 EXP EPI Propionic acid (OO) 79094 74.08 EPI Liquid MDEQ 141.1 EXP EPI -21.1 EXP EPI 0.33 EXP EPI Propyl alcohol (I,DD,OO) 71238 60.10 EPI Liquid MDEQ 97.2 EXP EPI -126.1 EXP EPI 0.25 EXP EPI n-Propylbenzene (I,DD) 103651 120.20 EPI Liquid MDEQ 159.2 EXP EPI -99.5 EXP EPI 3.69 EXP EPI Propylene glycol 57556 76.10 EPI Liquid MDEQ 187.6 EXP EPI -60 EXP EPI -0.92 EXP EPI Pyrene 129000 202.26 EPI Solid MDEQ 404 EXP EPI 151.2 EXP EPI 4.88 EXP EPI Pyridine (I,KK) 110861 79.10 EPI Liquid MDEQ 115.2 EXP EPI -41.6 EXP EPI 0.65 EXP EPI Selenium (B,KK) 7782492 78.96 CRC Inorganic MDEQ 685 EXP CRC 221 EXP PP NR NA NA Silver (KK) 7440224 107.87 EPI Inorganic MDEQ 2162 EXP CRC 960.5 EXP PP NR NA NA Silvex (2,4,5-TP) (KK) 93721 269.51 EPI Solid MDEQ NA NA NA 181.6 EXP EPI 3.80 EXP EPI Simazine 122349 201.66 EPI Solid MDEQ NA NA NA 226 EXP EPI 2.18 EXP EPI Sodium 17341252 22.99 EPI Inorganic MDEQ 882.94 EXP CRC 97.79 EXP CRC NR NA NA Sodium azide 26628228 65.01 EPI Inorganic MDEQ NA NA NA 275 EXP PC NR NA NA

345 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless Sodium bromide 7647156 102.89 EPI Inorganic MDEQ 1390 EXP CRC 747 EXP CRC NR NA NA Strontium (B,DD) 7440246 87.62 EPI Inorganic MDEQ 1377 EXP CRC 777 EXP PP NR NA NA Styrene 100425 104.15 EPI Liquid MDEQ 145 EXP EPI -31 EXP EPI 2.95 EXP EPI Sulfate 14808798 96.0626 PC Inorganic MDEQ NA NA NA NA NA NA NR NA NA Sulfolane 126330 120.17 EPI Solid MDEQ 285 EXP EPI 27.60 EXP EPI -0.77 EXP EPI Tebuthiuron (DD) 34014181 228.31 EPI Solid MDEQ NA NA NA 162.85 EXP EPI 1.79 EXP EPI 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416 499.78 EPI Solid MDEQ NA NA NA 334 EXP EPI 7.90 EST PP 1,2,4,5-Tetrachlorobenzene (DD) 95943 215.89 EPI Solid MDEQ 244.5 EXP EPI 139.5 EXP EPI 4.64 EXP EPI 2,3,7,8-Tetrachlorodibenzo-p-dioxin (O,DD) 1746016 321.98 EPI Solid MDEQ NA NA NA 305 EXP EPI 6.80 EXP EPI 1,1,1,2-Tetrachloroethane 630206 167.85 EPI Liquid MDEQ 130.2 EXP EPI -70.2 EXP EPI 2.93 EST PP 1,1,2,2-Tetrachloroethane 79345 167.85 EPI Liquid MDEQ 146.5 EXP EPI -43.8 EXP EPI 2.39 EXP EPI Tetrachloroethylene (KK) 127184 165.83 EPI Liquid MDEQ 121.3 EXP EPI -22.3 EXP EPI 3.40 EXP EPI Tetrahydrofuran (DD) 109999 72.11 EPI Liquid MDEQ 65 EXP EPI -108.44 EXP EPI 0.46 EXP EPI 1,1,3,3-Tetramethylurea (OO) 632224 116.16 EPI Liquid MDEQ 176.5 EXP EPI -1.2 EXP EPI 0.19 EXP EPI Tetranitromethane 509148 196.03 EPI Liquid MDEQ 126.1 EXP EPI 13.8 EXP EPI -2.05 EST PP Thallium 7440280 204.38 EPI Inorganic MDEQ 1473 EXP CRC 303.5 EXP PP NR NA NA Toluene (I) 108883 92.14 EPI Liquid MDEQ 110.6 EXP EPI -94.9 EXP EPI 2.73 EXP EPI p-Toluidine 106490 107.16 EPI Solid MDEQ 200.4 EXP EPI 43.6 EXP EPI 1.39 EXP EPI Total dissolved solids (TDS) NA NA NA NA MDEQ NA NA NA NA NA NA NR NA NA Toxaphene (KK) 8001352 414 HSDB Solid MDEQ NA NA NA 77 EXP PP 5.90 EXP PP Triallate (DD) 2303175 304.66 EPI Solid MDEQ NA NA NA 29 EXP EPI 4.60 EXP EPI Tributylamine 102829 185.36 EPI Liquid MDEQ 216.5 EXP EPI -70 EXP EPI 4.46 EST PP 1,2,3-Trichlorobenzene 87616 181.45 EPI Solid MDEQ 218.5 EXP EPI 53.5 EXP EPI 4.05 EXP EPI 1,2,4-Trichlorobenzene 120821 181.45 EPI Liquid MDEQ 213.5 EXP EPI 17 EXP EPI 4.02 EXP EPI 1,1,1-Trichloroethane 71556 133.41 EPI Liquid MDEQ 74 EXP EPI -30.41 EXP EPI 2.49 EXP EPI 1,1,2-Trichloroethane 79005 133.41 EPI Liquid MDEQ 113.8 EXP EPI -36.6 EXP EPI 1.89 EXP EPI Trichloroethylene (DD,KK,MM,NN) 79016 131.39 EPI Liquid MDEQ 87.2 EXP EPI -84.7 EXP EPI 2.42 EXP EPI Trichlorofluoromethane 75694 137.37 EPI Liquid MDEQ 23.7 EXP EPI -111.1 EXP EPI 2.53 EXP EPI 2,4,5-Trichlorophenol (KK) 95954 197.45 EPI Solid MDEQ 247 EXP EPI 69 EXP EPI 3.72 EXP EPI

346 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Log Chemical Physical State Octanol- Abstract at Standard Physical Water Log Log Service Molecular MW Temperature State Boiling BP BP Melting MP MP Partition Kow Kow Hazardous Substance Number Weight Source and Pressure Source Point Basis Source Point Basis Source Coefficient Basis Source MW BP MP Log Kow g/mol unitless ºC ºC unitless 2,4,6-Trichlorophenol (DD,KK) 88062 197.45 EPI Solid MDEQ 246 EXP EPI 69 EXP EPI 3.69 EXP EPI 1,2,3-Trichloropropane (MM) 96184 147.43 EPI Liquid MDEQ 157 EXP EPI -14.7 EXP EPI 2.27 EXP EPI 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 187.38 EPI Liquid MDEQ 47.7 EXP EPI -35 EXP EPI 3.16 EXP EPI Triethanolamine 102716 149.19 EPI Liquid MDEQ 335.4 EXP EPI 20.5 EXP EPI -1.00 EXP EPI Triethylene glycol (DD) 112276 150.18 EPI Liquid MDEQ 285 EXP EPI -7 EXP EPI -1.75 EXP EPI 3-Trifluoromethyl-4-nitrophenol (DD) 88302 207.11 EPI Solid MDEQ NA NA NA 76 EXP EPI 2.87 EST PP Trifluralin 1582098 335.29 EPI Solid MDEQ NA NA NA 49 EXP EPI 5.34 EXP EPI 2,2,4-Trimethyl pentane 540841 114.23 EPI Liquid MDEQ 99.2 EXP EPI -107.3 EXP EPI 1.09 EST PP 2,4,4-Trimethyl-2-pentene (I) 107404 112.22 EPI Liquid MDEQ 104.9 EXP EPI -106.3 EXP EPI 4.00 EST PP 1,2,3-Trimethylbenzene (I, J) 526738 120.20 EPI Liquid MDEQ 176.1 EXP EPI -25.4 EXP EPI 3.66 EXP EPI 1,2,4-Trimethylbenzene (I, J) 95636 120.20 EPI Liquid MDEQ 169.3 EXP EPI -43.8 EXP EPI 3.63 EXP EPI 1,3,5-Trimethylbenzene (I, J) 108678 120.20 EPI Liquid MDEQ 164.7 EXP EPI -44.7 EXP EPI 3.42 EXP EPI Triphenyl phosphate 115866 326.29 EPI Solid MDEQ 370 EXP PC 50.5 EXP EPI 4.59 EXP EPI tris(2,3-Dibromopropyl)phosphate 126727 697.62 EPI Liquid MDEQ NA NA NA 5.5 EXP EPI 4.29 EXP EPI Urea 57136 60.06 EPI Solid MDEQ NA NA NA 132.7 EXP EPI -2.11 EXP EPI Vanadium (B) 7440622 50.94 EPI Inorganic MDEQ 3407 EXP CRC 1910 EXP CRC NR NA NA Vinyl acetate (I,DD) 108054 86.09 EPI Liquid MDEQ 72.8 EXP EPI -93.2 EXP EPI 0.73 EXP EPI Vinyl chloride (KK,LL,MM) 75014 62.50 EPI Gas MDEQ -13.3 EXP EPI -153.7 EXP EPI 1.27 EXP SSG Xylenes (I,J) 1330207 106.17 EPI Liquid MDEQ 138.23 EXP EPI 13.25 EXP EPI 3.16 EXP PP Zinc (B) 7440666 65.37 EPI Inorganic MDEQ 908 EXP PP 419.5 EXP PP NR NA NA

347 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol Acenaphthene 83329 5027 EST EPI NR NA NA NR NA NA 1.84E-04 EXP EPI Acenaphthylene 208968 5027 EST EPI NR NA NA NR NA NA 1.14E-04 EXP EPI Acetaldehyde (I) 75070 1 EST EPI NR NA NA NR NA NA 6.67E-05 EXP EPI Acetate 71501 NA NA NA NR NA NA NR NA NA NA NA NA Acetic acid (OO) 64197 1 EST EPI NR NA NA NR NA NA 1.00E-07 EXP EPI Acetone (I) 67641 2.364 EST EPI NR NA NA NR NA NA 3.50E-05 EXP EPI Acetonitrile 75058 4.67 EST EPI NR NA NA NR NA NA 3.45E-05 EXP EPI Acetophenone (DD) 98862 51.85 EST EPI NR NA NA NR NA NA 1.04E-05 EXP EPI Acrolein (I) 107028 1 EST EPI NR NA NA NR NA NA 1.22E-04 EXP EPI Acrylamide (MM) 79061 5.694 EST EPI NR NA NA NR NA NA 1.70E-09 EST PP Acrylic acid (DD,OO) 79107 1.44 EST EPI NR NA NA NR NA NA 3.70E-07 EST PP Acrylonitrile (I) 107131 8.511 EST EPI NR NA NA NR NA NA 1.38E-04 EXP EPI Alachlor 15972608 312.3 EST EPI NR NA NA NR NA NA 8.32E-09 EXP EPI Aldicarb 116063 24.64 EST EPI NR NA NA NR NA NA 1.44E-09 EST PP Aldicarb sulfone 1646884 10 EST EPI NR NA NA NR NA NA 3.37E-09 EST PP Aldicarb sulfoxide 1646873 10 EST EPI NR NA NA NR NA NA 9.69E-10 EST PP Aldrin 309002 8.202E+04 EST EPI NR NA NA NR NA NA 4.40E-05 EXP EPI Aluminum (B,DD) 7429905 NR NA NA NR NA NA NA NA NA NR NA NA Ammonia 7664417 NA NA NA NR NA NA NR NA NA 1.61E-05 EXP EPI t-Amyl methyl ether (TAME) 994058 22.66 EST EPI NR NA NA NR NA NA 1.32E-03 EXP EPI Aniline 62533 70.23 EST EPI NR NA NA NR NA NA 2.02E-06 EXP EPI Anthracene 120127 1.636E+04 EST EPI NR NA NA NR NA NA 5.56E-05 EXP EPI Antimony 7440360 NR NA NA NR NA NA 4.5E+01 EST SSG NR NA NA Arsenic (B,KK) 7440382 NR NA NA NR NA NA 2.9E+01 EST SSG NR NA NA Asbestos (BB) 1332214 NR NA NA NR NA NA NR NA NA NR NA NA Atrazine 1912249 224.5 EST EPI NR NA NA NR NA NA 2.60E-09 EXP HSDB

348 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol Azobenzene 103333 3759 EST EPI NR NA NA NR NA NA 1.35E-05 EST PP Barium (B,KK) 7440393 NR NA NA NR NA NA 4.1E+01 EST SSG NR NA NA Benzene (I,KK) 71432 145.8 EST EPI NR NA NA NR NA NA 5.55E-03 EXP EPI Benzidine (MM) 92875 1190 EST EPI NR NA NA NR NA NA 5.17E-11 EST PP Benzo(a)anthracene (Q,MM) 56553 1.769E+05 EST EPI NR NA NA NR NA NA 1.20E-05 EXP EPI Benzo(b)fluoranthene (Q,MM) 205992 5.994E+05 EST EPI NR NA NA NR NA NA 6.57E-07 EXP EPI Benzo(k)fluoranthene (Q,MM) 207089 5.874E+05 EST EPI NR NA NA NR NA NA 5.84E-07 EXP EPI Benzo(g,h,i)perylene 191242 1.951E+06 EST EPI NR NA NA NR NA NA 3.31E-07 EXP EPI Benzo(a)pyrene (Q,DD,MM) 50328 5.874E+05 EST EPI NR NA NA NR NA NA 4.57E-07 EXP EPI Benzoic acid 65850 16.55 EST EPI 0.6 EST SSG NR NA NA 3.81E-08 EST PP Benzyl alcohol 100516 21.46 EST EPI NR NA NA NR NA NA 3.37E-07 EXP EPI Benzyl chloride 100447 446.1 EST EPI NR NA NA NR NA NA 4.12E-04 EST PP Beryllium (B) 7440417 NR NA NA NR NA NA 7.9E+02 EST SSG NR NA NA bis(2-Chloroethoxy)ethane 112265 26.21 EST EPI NR NA NA NR NA NA 7.81E-07 EST PP bis-2-Chloroethylether (I) 111444 32.21 EST EPI NR NA NA NR NA NA 2.96E-05 EXP CRC bis(2-Ethylhexyl) phthalate (DD) 117817 1.196E+05 EST EPI NR NA NA NR NA NA 1.02E-07 EXP SSG Boron (DD) 7440428 NR NA NA NR NA NA NA NA NA NR NA NA Bromate 15541454 NR NA NA NR NA NA NR NA NA NR NA NA Bromobenzene (I) 108861 233.9 EST EPI NR NA NA NR NA NA 2.47E-03 EXP EPI Bromodichloromethane (DD) 75274 31.82 EST EPI NR NA NA NR NA NA 2.12E-03 EXP EPI Bromoform 75252 31.82 EST EPI NR NA NA NR NA NA 5.35E-04 EXP EPI Bromomethane 74839 13.22 EST EPI NR NA NA NR NA NA 7.34E-03 EXP EPI n-Butanol (I,OO) 71363 3.471 EST EPI NR NA NA NR NA NA 8.81E-06 EXP EPI 2-Butanone (MEK) (I,DD,KK) 78933 4.51 EST EPI NR NA NA NR NA NA 5.69E-05 EXP EPI n-Butyl acetate 123864 18.54 EST EPI NR NA NA NR NA NA 2.81E-04 EXP EPI t-Butyl alcohol (OO) 75650 2.111 EST EPI NR NA NA NR NA NA 9.05E-06 EXP EPI

349 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol Butyl benzyl phthalate (DD) 85687 7155 EST EPI NR NA NA NR NA NA 1.26E-06 EXP SSG n-Butylbenzene 104518 1482 EST EPI NR NA NA NR NA NA 1.31E-02 EXP CRC sec-Butylbenzene 135988 1331 EST EPI NR NA NA NR NA NA 1.87E-02 EXP CRC t-Butylbenzene (I) 98066 1001 EST EPI NR NA NA NR NA NA 1.26E-02 EXP CRC Cadmium (B,KK) 7440439 NR NA NA NR NA NA 7.5E+01 EST SSG NR NA NA Camphene (I) 79925 1020 EST EPI NR NA NA NR NA NA 1.61E-01 EST PP Caprolactam (DD) 105602 24.5 EST EPI NR NA NA NR NA NA 2.53E-08 EST PP Carbaryl (DD) 63252 354.8 EST EPI NR NA NA NR NA NA 2.80E-09 EXP HSDB Carbazole 86748 9161 EST EPI NR NA NA NR NA NA 1.16E-07 EXP EPI Carbofuran (DD) 1563662 95.25 EST EPI NR NA NA NR NA NA 3.09E-09 EST PP Carbon disulfide (I,R,DD) 75150 21.73 EST EPI NR NA NA NR NA NA 1.44E-02 EXP EPI Carbon tetrachloride (KK) 56235 43.89 EST EPI NR NA NA NR NA NA 2.76E-02 EXP EPI Chlordane (J,KK) 57749 6.754E+04 EST EPI NR NA NA NR NA NA 4.86E-05 EXP EPI Chloride 16887006 NR NA NA NR NA NA NA NA NA NR NA NA 2-Chloroaniline 95512 115 EST EPI NR NA NA NR NA NA 5.39E-06 EST PP 4-Chloroaniline 106478 112.7 EST EPI NR NA NA NR NA NA 3.31E-07 EXP SSG Chlorobenzene (I,KK) 108907 233.9 EST EPI NR NA NA NR NA NA 3.11E-03 EXP EPI p-Chlorobenzene sulfonic acid 98668 16.06 EST EPI NR NA NA NR NA NA 1.86E-09 EST PP 1-Chloro-1,1-difluoroethane 75683 43.89 EST EPI NR NA NA NR NA NA 5.88E-02 EXP EPI Chloroethane (DD) 75003 21.73 EST EPI NR NA NA NR NA NA 1.11E-02 EXP EPI 2-Chloroethyl vinyl ether 110758 17.68 EST EPI NR NA NA NR NA NA 8.76E-03 EST PP Chloroform (KK) 67663 31.82 EST EPI NR NA NA NR NA NA 3.67E-03 EXP EPI Chloromethane (I) 74873 13.22 EST EPI NR NA NA NR NA NA 8.82E-03 EXP EPI 4-Chloro-3-methylphenol (DD) 59507 491.8 EST EPI NR NA NA NR NA NA 2.45E-06 EST PP beta-Chloronaphthalene 91587 2478 EST EPI NR NA NA NR NA NA 3.20E-04 EXP EPI 2-Chlorophenol (DD) 95578 306.5 EST EPI 388 EST SSG NR NA NA 1.12E-05 EXP EPI

350 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol o-Chlorotoluene (I) 95498 382.9 EST EPI NR NA NA NR NA NA 3.57E-03 EXP EPI Chlorpyrifos (DD) 2921882 7283 EST EPI NR NA NA NR NA NA 2.93E-06 EXP EPI Chromium (III) (B,H,KK) 16065831 NR NA NA NR NA NA 1.8E+06 EST SSG NR NA NA Chromium (VI) (H,KK,MM) 18540299 NR NA NA NR NA NA 1.9E+01 EST SSG NR NA NA Chrysene (Q,MM) 218019 3.98E+05 EST SSG NR NA NA NR NA NA 5.23E-06 EXP PP Cobalt (B) 7440484 NR NA NA NR NA NA NA NA NA NR NA NA Copper (B) 7440508 NR NA NA NR NA NA 3.6E+02 EST MDEQ NR NA NA Cyanazine 21725462 134.1 EST EPI NR NA NA NR NA NA 2.57E-10 EXP HSDB Cyanide (P,R,DD) 57125 NR NA NA NR NA NA 9.9E+00 EST SSG NR NA NA Cyclohexane (DD) 110827 145.8 EST EPI NR NA NA NR NA NA 1.50E-01 EXP EPI Cyclohexanone (OO) 108941 17.38 EST EPI NR NA NA NR NA NA 9.00E-06 EXP EPI Dacthal 1861321 511.1 EST EPI NR NA NA NR NA NA 2.18E-06 EST PP Dalapon 75990 3.231 EST EPI NR NA NA NR NA NA 5.66E-08 EST PP 4-4'-DDD 72548 1.175E+05 EST EPI NR NA NA NR NA NA 6.60E-06 EXP EPI 4-4'-DDE 72559 1.175E+05 EST EPI NR NA NA NR NA NA 4.16E-05 EXP EPI 4-4'-DDT (DD) 50293 1.686E+05 EST EPI NR NA NA NR NA NA 8.32E-06 EXP EPI Decabromodiphenyl ether (DD) 1163195 2.762E+05 EST EPI NR NA NA NR NA NA 1.19E-08 EST PP Di-n-butyl phthalate (DD) 84742 1157 EST EPI NR NA NA NR NA NA 1.81E-06 EXP EPI Di(2-ethylhexyl) adipate (DD) 103231 3.6E+04 EST EPI NR NA NA NR NA NA 4.34E-07 EXP EPI Di-n-octyl phthalate 117840 1.408E+05 EST EPI NR NA NA NR NA NA 6.68E-05 EXP SSG Diacetone alcohol (I,OO) 123422 1 EST EPI NR NA NA NR NA NA 2.61E-07 EST PP Diazinon 333415 3034 EST EPI NR NA NA NR NA NA 1.13E-07 EXP EPI Dibenzo(a,h)anthracene (Q,MM) 53703 1.912E+06 EST EPI NR NA NA NR NA NA 1.47E-08 EXP SSG Dibenzofuran 132649 9161 EST EPI NR NA NA NR NA NA 1.09E-04 EXP CRC Dibromochloromethane (MM) 124481 31.82 EST EPI NR NA NA NR NA NA 7.83E-04 EXP EPI Dibromochloropropane (MM) 96128 115.8 EST EPI NR NA NA NR NA NA 1.47E-04 EST PP

351 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol Dibromomethane 74953 21.73 EST EPI NR NA NA NR NA NA 8.22E-04 EXP EPI Dicamba (DD) 1918009 29.01 EST EPI NR NA NA NR NA NA 4.38E-10 EST PP 1,2-Dichlorobenzene 95501 382.9 EST EPI NR NA NA NR NA NA 1.92E-03 EXP EPI 1,3-Dichlorobenzene 541731 375.3 EST EPI NR NA NA NR NA NA 2.63E-03 EXP EPI 1,4-Dichlorobenzene (KK) 106467 375.3 EST EPI NR NA NA NR NA NA 2.41E-03 EXP EPI 3,3`-Dichlorobenzidine 91941 3190 EST EPI NR NA NA NR NA NA 4.00E-09 EXP SSG Dichlorodifluoromethane 75718 43.89 EST EPI NR NA NA NR NA NA 3.43E-01 EXP EPI 1,1-Dichloroethane 75343 31.82 EST EPI NR NA NA NR NA NA 5.62E-03 EXP EPI 1,2-Dichloroethane (I,KK) 107062 39.6 EST EPI NR NA NA NR NA NA 1.18E-03 EXP EPI 1,1-Dichloroethylene (I,KK) 75354 31.82 EST EPI NR NA NA NR NA NA 2.61E-02 EXP EPI cis-1,2-Dichloroethylene 156592 39.6 EST EPI NR NA NA NR NA NA 4.08E-03 EXP EPI trans-1,2-Dichloroethylene 156605 52.5 EST SSG NR NA NA NR NA NA 9.38E-03 EXP PP 2,6-Dichloro-4-nitroaniline 99309 1947 EST EPI NR NA NA NR NA NA 4.67E-08 EST PP 2,4-Dichlorophenol (DD) 120832 491.8 EST EPI 147 EST SSG NR NA NA 3.48E-06 EST PP 2,4-Dichlorophenoxyacetic acid (KK) 94757 29.63 EST EPI NR NA NA NR NA NA 9.75E-08 EXP HSDB 1,2-Dichloropropane (I) 78875 60.7 EST EPI NR NA NA NR NA NA 2.82E-03 EXP EPI 1,3-Dichloropropene (J) 542756 72.17 EST EPI NR NA NA NR NA NA 3.55E-03 EXP EPI Dichlorvos (MM) 62737 53.96 EST EPI NR NA NA NR NA NA 5.74E-07 EST PP Dicyclohexyl phthalate 84617 1.332E+04 EST EPI NR NA NA NR NA NA 1.00E-07 EST PP Dieldrin 60571 2.009E+04 EST EPI NR NA NA NR NA NA 1.00E-05 EXP EPI Diethyl ether 60297 9.699 EST EPI NR NA NA NR NA NA 1.23E-03 EXP EPI Diethyl phthalate 84662 104.9 EST EPI NR NA NA NR NA NA 6.10E-07 EST PP Diethylene glycol monobutyl ether 112345 10 EST EPI NR NA NA NR NA NA 7.20E-09 EXP EPI Diisopropyl ether (DD) 108203 22.79 EST EPI NR NA NA NR NA NA 2.56E-03 EXP EPI Diisopropylamine (I) 108189 63.66 EST EPI NR NA NA NR NA NA 9.60E-05 EST PP Dimethyl phthalate 131113 31.59 EST EPI NR NA NA NR NA NA 1.97E-07 EST PP

352 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol N,N-Dimethylacetamide (OO) 127195 3.344 EST EPI NR NA NA NR NA NA 1.31E-08 EXP EPI N,N-Dimethylaniline 121697 78.67 EST EPI NR NA NA NR NA NA 5.68E-05 EST PP Dimethylformamide (I,OO) 68122 1 EST EPI NR NA NA NR NA NA 7.39E-08 EXP EPI 2,4-Dimethylphenol 105679 491.8 EST EPI NR NA NA NR NA NA 9.51E-07 EXP EPI 2,6-Dimethylphenol 576261 501.9 EST EPI NR NA NA NR NA NA 6.65E-06 EXP EPI 3,4-Dimethylphenol 95658 491.8 EST EPI NR NA NA NR NA NA 4.15E-07 EXP EPI Dimethylsulfoxide 67685 2.082 EST EPI NR NA NA NR NA NA 1.51E-09 EXP EPI 2,4-Dinitrophenol 51285 460.8 EST EPI 0.01 EST SSG NR NA NA 8.60E-08 EXP EPI 2,4-Dinitrotoluene (KK) 121142 575.6 EST EPI NR NA NA NR NA NA 5.40E-08 EXP EPI Dinoseb (DD) 88857 4294 EST EPI NR NA NA NR NA NA 4.56E-07 EST PP 1,4-Dioxane (I,OO) 123911 2.633 EST EPI NR NA NA NR NA NA 4.80E-06 EXP EPI Diquat 85007 NA NA NA NR NA NA NR NA NA 1.42E-13 EST PP Dissolved oxygen (DO) NA NR NA NA NR NA NA NR NA NA NR NA NA Diuron 330541 109.1 EST EPI NR NA NA NR NA NA 5.04E-10 EST PP Endosulfan (J) 115297 6761 EST EPI NR NA NA NR NA NA 6.50E-05 EXP EPI Endothall 145733 19.41 EST EPI NR NA NA NR NA NA 3.85E-16 EST PP Endrin (KK) 72208 12300 EST SSG NR NA NA NR NA NA 6.36E-06 EXP PP Epichlorohydrin (I) 106898 9.907 EST EPI NR NA NA NR NA NA 2.96E-05 EXP CRC Ethanol (I,DD,OO) 64175 1.045 EST EPI NR NA NA NR NA NA 5.00E-06 EXP EPI Ethyl acetate (I) 141786 5.583 EST EPI NR NA NA NR NA NA 1.34E-04 EXP EPI Ethyl-tert-butyl ether (ETBE) 637923 21.07 EST EPI NR NA NA NR NA NA 1.64E-03 EXP EPI Ethylbenzene (I) 100414 446.1 EST EPI NR NA NA NR NA NA 7.88E-03 EXP EPI Ethylene dibromide 106934 39.6 EST EPI NR NA NA NR NA NA 6.50E-04 EXP EPI Ethylene glycol (DD) 107211 1 EST EPI NR NA NA NR NA NA 6.00E-08 EXP EPI Ethylene glycol monobutyl ether 111762 2.823 EST EPI NR NA NA NR NA NA 1.60E-06 EXP EPI Ethylenediaminetetraacetic acid (EDTA) (II) 60004 312.7 EST EPI NR NA NA NR NA NA 5.77E-16 EST PP

353 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol Fluoranthene 206440 5.545E+04 EST EPI NR NA NA NR NA NA 8.86E-06 EXP EPI Fluorene 86737 9160 EST EPI NR NA NA NR NA NA 9.62E-05 EXP EPI Fluorine (soluble fluoride) (DD) 7782414 NR NA NA NR NA NA NA NA NA NR NA NA Formaldehyde (MM,OO) 50000 1 EST EPI NR NA NA NR NA NA 3.37E-07 EXP EPI Formic acid (I,U,OO) 64186 1 EST EPI NR NA NA NR NA NA 1.67E-07 EXP EPI 1-Formylpiperidine (DD) 2591868 4.162 EST EPI NR NA NA NR NA NA 7.61E-08 EST PP Gentian violet 548629 6.711E+05 EST EPI NR NA NA NR NA NA 3.06E-16 EST PP Glyphosate (DD) 1071836 1 EST EPI NR NA NA NR NA NA 2.10E-12 EST PP Heptachlor (DD,KK) 76448 1.41E+06 EST SSG NR NA NA NR NA NA 2.94E-04 EXP PP Heptachlor epoxide (KK) 1024573 1.011E+04 EST EPI NR NA NA NR NA NA 2.10E-05 EXP EPI n-Heptane 142825 239.7 EST EPI NR NA NA NR NA NA 2.00E+00 EST PP Hexabromobenzene 87821 2807 EST EPI NR NA NA NR NA NA 2.81E-05 EST PP Hexachlorobenzene (C-66) (KK) 118741 6195 EST EPI NR NA NA NR NA NA 1.70E-03 EXP EPI Hexachlorobutadiene (C-46) (KK) 87683 845.2 EST EPI NR NA NA NR NA NA 1.03E-02 EXP EPI alpha-Hexachlorocyclohexane 319846 2807 EXT EPI NR NA NA NR NA NA 6.70E-06 EXP PP beta-Hexachlorocyclohexane 319857 2807 EXT EPI NR NA NA NR NA NA 4.40E-07 EXP PP Hexachlorocyclopentadiene (C-56) 77474 1404 EST EPI NR NA NA NR NA NA 2.70E-02 EXP EPI Hexachloroethane (KK) 67721 196.8 EST EPI NR NA NA NR NA NA 3.89E-03 EXP EPI n-Hexane 110543 131.5 EST EPI NR NA NA NR NA NA 1.80E+00 EST PP 2-Hexanone 591786 14.98 EST EPI NR NA NA NR NA NA 9.32E-05 EST PP Indeno(1,2,3-cd)pyrene (Q,MM) 193395 1.951E+06 EST EPI NR NA NA NR NA NA 3.48E-07 EXP EPI Iron (B) 7439896 NR NA NA NR NA NA NA NA NA NR NA NA Isobutyl alcohol (I,OO) 78831 2.919 EST EPI NR NA NA NR NA NA 9.78E-06 EXP EPI Isophorone (DD) 78591 65.15 EST EPI NR NA NA NR NA NA 6.64E-06 EXP SSG Isopropyl alcohol (I,DD,OO) 67630 1.53 EST EPI NR NA NA NR NA NA 8.10E-06 EXP EPI Isopropyl benzene 98828 697.8 EST EPI NR NA NA NR NA NA 1.15E-02 EXP EPI

354 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol Lead (B,L,DD,KK) 7439921 NR NA NA NR NA NA 1.1E+04 EST MDEQ NR NA NA Lindane (KK) 58899 2807 EST EPI NR NA NA NR NA NA 5.14E-06 EXP EPI Lithium (B,DD) 7439932 NR NA NA NR NA NA NA NA NA NR NA NA Magnesium 7439954 NR NA NA NR NA NA NA NA NA NR NA NA Manganese (B) 7439965 NR NA NA NR NA NA NA NA NA NR NA NA Mercury (Total) (Z,DD,KK) Varies Mercury, elemental 7439976 3.449 EST EPI NR NA NA NA NA NA 1.14E-02 EXP SSG Mercuric chloride 7487947 NR NA NA NR NA NA 5.2E+01 EST SSG NR NA NA Methyl mercury (DD) 22967926 NA NA NA NR NA NA NA NA NA NA NA NA Methane (K) 74828 3.979 EST EPI NR NA NA NR NA NA 6.65E-01 EXP CRC Methanol (DD,OO) 67561 1 EST EPI NR NA NA NR NA NA 4.55E-06 EXP EPI Methoxychlor (DD,KK) 72435 26890 EST EPI NR NA NA NR NA NA 2.03E-07 EXP EPI 2-Methoxyethanol (I,DD,OO) 109864 1 EST EPI NR NA NA NR NA NA 3.30E-07 EXP EPI 2-Methyl-4-chlorophenoxyacetic acid 94746 29.63 EST EPI NR NA NA NR NA NA 1.33E-09 EST PP 2-Methyl-4,6-dinitrophenol 534521 754.4 EST EPI NR NA NA NR NA NA 1.40E-06 EXP EPI N-Methyl-morpholine (I,OO) 109024 7.231 EST EPI NR NA NA NR NA NA 2.50E-07 EST PP Methyl parathion 298000 729.3 EST EPI NR NA NA NR NA NA 1.00E-07 EXP EPI 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 12.6 EST EPI NR NA NA NR NA NA 1.38E-04 EST PP Methyl-tert-butyl ether (MTBE) 1634044 11.56 EST EPI NR NA NA NR NA NA 5.87E-04 EXP EPI N-methylaniline 100618 82.08 EST EPI NR NA NA NR NA NA 8.88E-06 EXP EPI Methylcyclopentane (I) 96377 128.3 EST EPI NR NA NA NR NA NA 3.62E-01 EXP CRC 4,4`-Methylene-bis-2-chloroaniline (MBOCA) (MM) 101144 5698 EST EPI NR NA NA NR NA NA 4.06E-11 EST PP Methylene chloride (MM) 75092 21.73 EST EPI NR NA NA NR NA NA 3.25E-03 EXP EPI 2-Methylnaphthalene 91576 2478 EST EPI NR NA NA NR NA NA 5.18E-04 EXP EPI Methylphenols (JJ,KK) 1319773 2-Methylphenol (DD,KK) 95487 306.5 EST EPI 9.12E+01 EST SSG NR NA NA 1.20E-06 EXP EPI

355 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol 3-Methylphenol (KK) 108394 300.4 EST EPI NR NA NA NR NA NA 8.56E-07 EXP EPI 4-Methylphenol (KK) 106445 300.4 EST EPI NR NA NA NR NA NA 1.00E-06 EXP EPI Metolachlor 51218452 488.5 EST EPI NR NA NA NR NA NA 9.00E-09 EXP EPI Metribuzin 21087649 53.13 EST EPI NR NA NA NR NA NA 1.17E-10 EST PP Mirex 2385855 3.566E+05 EST EPI NR NA NA NR NA NA 8.11E-04 EXP EPI Molybdenum 7439987 NR NA NA NR NA NA NA NA NA NR NA NA Naphthalene 91203 1544 EST EPI NR NA NA NR NA NA 4.40E-04 EXP EPI Nickel (B) 7440020 NR NA NA NR NA NA 6.5E+01 EST SSG NR NA NA Nitrate (N,DD) 14797558 NR NA NA NR NA NA NA NA NA NR NA NA Nitrite (N,DD) 14797650 NR NA NA NR NA NA NA NA NA NR NA NA Nitrobenzene (I,KK) 98953 226.4 EST EPI NR NA NA NR NA NA 2.40E-05 EXP EPI 2-Nitrophenol 88755 296.7 EST EPI NR NA NA NR NA NA 1.28E-05 EXP EPI n-Nitroso-di-n-propylamine 621647 275.4 EST EPI NR NA NA NR NA NA 5.38E-06 EXP EPI N-Nitrosodiphenylamine 86306 2632 EST EPI NR NA NA NR NA NA 5.00E-06 EXP SSG Oxamyl 23135220 10 EST EPI NR NA NA NR NA NA 2.37E-10 EST PP Oxo-hexyl acetate (OO) 88230357 NA NA NA NR NA NA NR NA NA NA NA NA Pendimethalin (DD) 40487421 5615 EST EPI NR NA NA NR NA NA 8.56E-07 EXP HSDB Pentachlorobenzene 608935 3708 EST EPI NR NA NA NR NA NA 7.03E-04 EXP EPI Pentachloronitrobenzene 82688 5996 EST EPI NR NA NA NR NA NA 4.42E-05 EST PP Pentachlorophenol (KK) 87865 4959 EST EPI 592 EST SSG NR NA NA 2.45E-08 EXP EPI Pentane 109660 72.17 EST EPI NR NA NA NR NA NA 1.25E+00 EXP EPI 2-Pentene (I) 109682 72.17 EST EPI NR NA NA NR NA NA 2.40E-01 EST PP Perchlorate (DD) 14797730 NR NA NA NR NA NA NA NA NA NR NA NA Perfluorooctanoic acid 335671 2.625E+04 EST EPI NR NA NA NR NA NA 3.01E-05 EST PP Perfluorooctane sulfonic acid (DD) 1763231 7.168E+04 EST EPI NR NA NA NR NA NA NA NA NA pH NA NR NA NA NR NA NA NR NA NA NR NA NA

356 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol Phenanthrene 85018 1.669E+04 EST EPI NR NA NA NR NA NA 4.23E-05 EXP EPI Phenol (DD) 108952 187.2 EST EPI NR NA NA NR NA NA 3.33E-07 EXP EPI Phenytoin (DD) 57410 1473 EST EPI NR NA NA NR NA NA 1.02E-11 EST PP Phosphorus, Total Varies NA NA NA NR NA NA NA NA NA NA NA NA Phosphorus, White (R,DD) 7723140 NR NA NA NR NA NA NA NA NA 2.44E-02 EST PP o-Phthalic acid 88993 80.85 EST EPI NR NA NA NR NA NA 2.00E-11 EST PP Phthalic anhydride 85449 10 EST EPI NR NA NA NR NA NA 1.63E-08 EST PP Picloram 1918021 38.77 EST EPI NR NA NA NR NA NA 5.33E-14 EST PP Piperidine (OO) 110894 54.73 EST EPI NR NA NA NR NA NA 4.45E-06 EXP EPI Polybrominated biphenyls (J,DD) 67774327 NA NA NA NR NA NA NR NA NA NA NA NA Polychlorinated biphenyls (PCBs) (J,T,DD) 1336363 7.810E+04 EST EPI NR NA NA NR NA NA 4.15E-04 EXP EPI Polychlorinated biphenyls (PCBs) congeners (O) (O) Prometon 1610180 137.4 EST EPI NR NA NA NR NA NA 9.09E-10 EST PP Propachlor 1918167 204.50 EST EPI NR NA NA NR NA NA 3.60E-07 EST PP Propazine 139402 344.1 EST EPI NR NA NA NR NA NA 4.60E-09 EST PP Propionic acid (OO) 79094 1.44 EST EPI NR NA NA NR NA NA 4.45E-07 EXP EPI Propyl alcohol (I,DD,OO) 71238 1.904 EST EPI NR NA NA NR NA NA 7.41E-06 EXP EPI n-Propylbenzene (I,DD) 103651 813.1 EST EPI NR NA NA NR NA NA 1.05E-02 EXP EPI Propylene glycol 57556 1 EST EPI NR NA NA NR NA NA 1.29E-08 EST PP Pyrene 129000 5.434E+04 EST EPI NR NA NA NR NA NA 1.19E-05 EXP EPI Pyridine (I,KK) 110861 71.72 EST EPI NR NA NA NR NA NA 1.10E-05 EXP EPI Selenium (B,KK) 7782492 NR NA NA NR NA NA 5.0E+00 EST SSG 9.74E-03 EST PP Silver (KK) 7440224 NR NA NA NR NA NA 8.3E+00 EST SSG NR NA NA Silvex (2,4,5-TP) (KK) 93721 175.3 EST EPI NR NA NA NR NA NA 9.06E-09 EST PP Simazine 122349 146.5 EST EPI NR NA NA NR NA NA 9.42E-10 EST PP Sodium 17341252 NR NA NA NR NA NA NA NA NA NR NA NA

357 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol Sodium azide 26628228 NR NA NA NR NA NA NA NA NA NR NA NA Sodium bromide 7647156 NR NA NA NR NA NA NA NA NA NR NA NA Strontium (B,DD) 7440246 NR NA NA NR NA NA NA NA NA NR NA NA Styrene 100425 446.1 EST EPI NR NA NA NR NA NA 2.75E-03 EXP EPI Sulfate 14808798 NR NA NA NR NA NA NR NA NA NR NA NA Sulfolane 126330 9.079 EST EPI NA NA NA NA NA NA 4.85E-06 EST PP Tebuthiuron (DD) 34014181 42.35 EST EPI NR NA NA NR NA NA 1.20E-10 EXP EPI 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416 1.129E+05 EST EPI NR NA NA NR NA NA 2.95E-07 EST PP 1,2,4,5-Tetrachlorobenzene (DD) 95943 2220 EST EPI NR NA NA NR NA NA 1.00E-03 EXP EPI 2,3,7,8-Tetrachlorodibenzo-p-dioxin (O,DD) 1746016 2.491E+05 EST EPI NR NA NA NR NA NA 5.00E-05 EST PP 1,1,1,2-Tetrachloroethane 630206 86.03 EST EPI NR NA NA NR NA NA 2.50E-03 EXP EPI 1,1,2,2-Tetrachloroethane 79345 94.94 EST EPI NR NA NA NR NA NA 3.67E-04 EXP EPI Tetrachloroethylene (KK) 127184 94.94 EST EPI NR NA NA NR NA NA 1.77E-02 EXP EPI Tetrahydrofuran (DD) 109999 10.75 EST EPI NR NA NA NR NA NA 7.05E-05 EXP EPI 1,1,3,3-Tetramethylurea (OO) 632224 3.958 EST EPI NR NA NA NR NA NA 8.48E-09 EST PP Tetranitromethane 509148 428.3 EST EPI NR NA NA NR NA NA 2.40E-04 EST PP Thallium 7440280 NR NA NA NR NA NA 7.1E+01 EST SSG 2.45E-02 EST PP Toluene (I) 108883 233.9 EST EPI NR NA NA NR NA NA 6.64E-03 EXP EPI p-Toluidine 106490 112.7 EST EPI NR NA NA NR NA NA 2.02E-06 EXP EPI Total dissolved solids (TDS) NA NR NA NA NR NA NA NR NA NA NR NA NA Toxaphene (KK) 8001352 2.57E+05 EST SSG NR NA NA NR NA NA 6.00E-06 EXP PP Triallate (DD) 2303175 1008 EST EPI NR NA NA NR NA NA 1.20E-05 EST PP Tributylamine 102829 1861 EST EPI NR NA NA NR NA NA 1.60E-04 EST PP 1,2,3-Trichlorobenzene 87616 1383 EST EPI NR NA NA NR NA NA 1.25E-03 EXP EPI 1,2,4-Trichlorobenzene 120821 1356 EST EPI NR NA NA NR NA NA 1.42E-03 EXP EPI 1,1,1-Trichloroethane 71556 43.89 EST EPI NR NA NA NR NA NA 1.72E-02 EXP EPI

358 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Soil Organic Soil-Water Carbon-Water Soil Koc for Distribution Chemical Partition Ionizing Coefficients for Hazardous Substance Abstract Coefficients for Organic Ion Inorganic Henry's Law Service Organic Koc Koc Compounds Koc Ion Koc Compounds at Kd Kd Constant at HLC HLC Number Compounds Basis Source at pH=6.8 Basis Source pH=6.8 Basis Source 25ºC Basis Source Koc IonKoc Kd HLC L/kg L/kg L/kg atm-m3 /mol 1,1,2-Trichloroethane 79005 60.7 EST EPI NR NA NA NR NA NA 8.24E-04 EXP EPI Trichloroethylene (DD,KK,MM,NN) 79016 60.7 EST EPI NR NA NA NR NA NA 9.85E-03 EXP EPI Trichlorofluoromethane 75694 43.89 EST EPI NR NA NA NR NA NA 9.70E-02 EXP EPI 2,4,5-Trichlorophenol (KK) 95954 1777 EST EPI 2365 EST SSG NR NA NA 4.33E-06 EXP SSG 2,4,6-Trichlorophenol (DD,KK) 88062 1777 EST EPI 1040 EST SSG NR NA NA 7.79E-06 EXP SSG 1,2,3-Trichloropropane (MM) 96184 115.8 EST EPI NR NA NA NR NA NA 3.43E-04 EXP EPI 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 196.8 EST EPI NR NA NA NR NA NA 3.16E-01 EXP CRC Triethanolamine 102716 10 EST EPI NR NA NA NR NA NA 7.05E-13 EST PP Triethylene glycol (DD) 112276 10 EST EPI NR NA NA NR NA NA 3.16E-11 EST PP 3-Trifluoromethyl-4-nitrophenol (DD) 88302 2038 EST EPI NR NA NA NR NA NA 1.92E-08 EST PP Trifluralin 1582098 1.639E+04 EST EPI NR NA NA NR NA NA 1.03E-04 EXP EPI 2,2,4-Trimethyl pentane 540841 240.3 EST EPI NR NA NA NR NA NA 3.03E+00 EXP CRC 2,4,4-Trimethyl-2-pentene (I) 107404 240.3 EST EPI NR NA NA NR NA NA 8.81E-01 EST PP 1,2,3-Trimethylbenzene (I, J) 526738 626.9 EST EPI NR NA NA NR NA NA 4.36E-03 EXP EPI 1,2,4-Trimethylbenzene (I, J) 95636 614.3 EST EPI NR NA NA NR NA NA 6.16E-03 EXP EPI 1,3,5-Trimethylbenzene (I, J) 108678 602.1 EST EPI NR NA NA NR NA NA 8.77E-03 EXP EPI Triphenyl phosphate 115866 1.074E+04 EST EPI NR NA NA NR NA NA 3.31E-06 EST PP tris(2,3-Dibromopropyl)phosphate 126727 9706 EST EPI NR NA NA NR NA NA 2.18E-05 EST PP Urea 57136 3.154 EST EPI NR NA NA NR NA NA NR NA NA Vanadium (B) 7440622 NR NA NA NR NA NA 1.0E+03 EST SSG NR NA NA Vinyl acetate (I,DD) 108054 5.583 EST EPI NR NA NA NR NA NA 5.11E-04 EXP SSG Vinyl chloride (KK,LL,MM) 75014 21.73 EST EPI NR NA NA NR NA NA 2.78E-02 EXP EPI Xylenes (I,J) 1330207 382.9 EST EPI NR NA NA NR NA NA 6.63E-03 EXP PP Zinc (B) 7440666 NR NA NA NR NA NA 6.2E+01 EST SSG NR NA NA

359 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L Acenaphthene 83329 5.06E-02 EST W9 8.33E-06 EST W9 NA NA NA 135 EXPPC 3.90E+03 EXP EPI Acenaphthylene 208968 4.50E-02 EST W9 6.98E-06 EST W9 NA NA NA NA NA NA 1.61E+04 EXP EPI Acetaldehyde (I) 75070 1.28E-01 EST W9 1.35E-05 EST W9 0.04 EXP CRC -39 EXP CRC 1.00E+09 EXP EPI Acetate 71501 1.25E-01 EST W9 1.46E-05 EST W9 NA NA NA NA NA NA 1.00E+09 EXP PC Acetic acid (OO) 64197 1.17E-01 EST W9 1.34E-05 EST W9 0.04 EXP CRC 39 EXP CRC 1.00E+09 EXP EPI Acetone (I) 67641 1.06E-01 EST W9 1.15E-05 EST W9 0.025 EXP CRC -20 EXP CRC 1.00E+09 EXP EPI Acetonitrile 75058 1.34E-01 EST W9 1.41E-05 EST W9 0.03 EXP CRC 6 EXP CRC 1.00E+09 EXP EPI Acetophenone (DD) 98862 6.52E-02 EST W9 8.72E-06 EST W9 NA NA NA 77 EXP CRC 6.13E+06 EXP EPI Acrolein (I) 107028 1.12E-01 EST W9 1.22E-05 EST W9 0.028 EXP CRC -26 EXP CRC 2.12E+08 EXP EPI Acrylamide (MM) 79061 1.07E-01 EST W9 1.26E-05 EST W9 NA NA NA 138 EXP NPG 3.90E+08 EXP EPI Acrylic acid (DD,OO) 79107 1.03E-01 EST W9 1.20E-05 EST W9 0.024 EXP CRC 50 EXP CRC 1.00E+09 EXP EPI Acrylonitrile (I) 107131 1.14E-01 EST W9 1.23E-05 EST W9 0.03 EXP CRC 0 EXP CRC 7.45E+07 EXP EPI Alachlor 15972608 2.26E-02 EST W9 5.69E-06 EST W9 NA NA NA 137 EXP PC 2.40E+05 EXP EPI Aldicarb 116063 3.19E-02 EST W9 7.25E-06 EST W9 NA NA NA NA NA NA 6.03E+06 EXP EPI Aldicarb sulfone 1646884 5.18E-02 EST W9 6.05E-06 EST W9 NA NA NA NA NA NA 1.00E+07 EXP EPI Aldicarb sulfoxide 1646873 5.44E-02 EST W9 6.36E-06 EST W9 NA NA NA NA NA NA 2.80E+07 EXP EPI Aldrin 309002 2.28E-02 EST W9 5.84E-06 EST W9 NA NA NA NA NA NA 1.70E+01 EXP EPI Aluminum (B,DD) 7429905 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Ammonia 7664417 2.87E-01 EST W9 3.35E-05 EST W9 0.15 EXP PC NA NA NA 4.82E+08 EXP EPI t-Amyl methyl ether (TAME) 994058 6.73E-02 EST W9 8.06E-06 EST W9 0.011 EXP PC -7 EXP PC 1.07E+07 EXP PP Aniline 62533 8.30E-02 EST W9 1.01E-05 EST W9 0.013 EXP CRC 70 EXP CRC 3.60E+07 EXP EPI Anthracene 120127 3.90E-02 EST W9 7.85E-06 EST W9 0.006 EXP CRC 121 EXP CRC 4.34E+01 EXP EPI Antimony 7440360 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Arsenic (B,KK) 7440382 NR NA NA NR NA NA 0.051 EXP PC NA NA NA NA NA NA Asbestos (BB) 1332214 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Atrazine 1912249 2.65E-02 EST W9 6.84E-06 EST W9 NA NA NA NA NA NA 3.47E+04 EXP EPI Azobenzene 103333 3.59E-02 EST W9 7.47E-06 EST W9 NA NA NA NA NA NA 6.40E+03 EXP EPI

360 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L Barium (B,KK) 7440393 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Benzene (I,KK) 71432 8.95E-02 EST W9 1.03E-05 EST W9 0.012 EXP CRC -11 EXP CRC 1.79E+06 EXP EPI Benzidine (MM) 92875 3.55E-02 EST W9 7.59E-06 EST W9 NA NA NA NA NA NA 3.22E+05 EXP EPI Benzo(a)anthracene (Q,MM) 56553 2.61E-02 EST W9 6.75E-06 EST W9 NA NA NA NA NA NA 9.40E+00 EXP EPI Benzo(b)fluoranthene (Q,MM) 205992 4.76E-02 EST W9 5.56E-06 EST W9 NA NA NA NA NA NA 1.50E+00 EXP EPI Benzo(k)fluoranthene (Q,MM) 207089 4.76E-02 EST W9 5.56E-06 EST W9 NA NA NA NA NA NA 8.00E-01 EXP EPI Benzo(g,h,i)perylene 191242 2.39E-02 EST W9 6.09E-06 EST W9 NA NA NA NA NA NA 2.60E-01 EXP EPI Benzo(a)pyrene (Q,DD,MM) 50328 2.55E-02 EST W9 6.58E-06 EST W9 NA NA NA NA NA NA 1.62E+00 EXP EPI Benzoic acid 65850 7.02E-02 EST W9 9.79E-06 EST W9 NA NA NA 121 EXP CRC 3.40E+06 EXP EPI Benzyl alcohol 100516 7.31E-02 EST W9 9.37E-06 EST W9 NA NA NA 93 EXP CRC 4.29E+07 EXP EPI Benzyl chloride 100447 6.34E-02 EST W9 8.81E-06 EST W9 0.011 EXP CRC 67 EXP CRC 5.25E+05 EXP EPI Beryllium (B) 7440417 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA bis(2-Chloroethoxy)ethane 112265 3.34E-02 EST W9 7.32E-06 EST W9 NA NA NA 121 EXP CRC 1.89E+07 EXP EPI bis-2-Chloroethylether (I) 111444 5.67E-02 EST W9 8.71E-06 EST W9 0.027 EXP CRC 55 EXP CRC 1.72E+07 EXP EPI bis(2-Ethylhexyl) phthalate (DD) 117817 1.73E-02 EST W9 4.18E-06 EST W9 0.003 EXP PC 218 EXP CRC 2.70E+02 EXP EPI Boron (DD) 7440428 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Bromate 15541454 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Bromobenzene (I) 108861 5.37E-02 EST W9 9.30E-06 EST W9 0.06 EXP PC 51 EXP CRC 4.46E+05 EXP EPI Bromodichloromethane (DD) 75274 5.63E-02 EST W9 1.07E-05 EST W9 NA NA NA NA NA NA 3.03E+06 EXP EPI Bromoform 75252 3.57E-02 EST W9 1.04E-05 EST W9 NA NA NA 83 EXP CRC 3.10E+06 EXP EPI Bromomethane 74839 1.00E-01 EST W9 1.35E-05 EST W9 0.1 EXP CRC 194 EXP PC 1.52E+07 EXP EPI n-Butanol (I,OO) 71363 9.00E-02 EST W9 1.01E-05 EST W9 0.014 EXP CRC 37 EXP CRC 6.32E+07 EXP EPI 2-Butanone (MEK) (I,DD,KK) 78933 9.14E-02 EST W9 1.02E-05 EST W9 0.014 EXP CRC -9 EXP CRC 2.23E+08 EXP EPI n-Butyl acetate 123864 6.32E-02 EST W9 8.12E-06 EST W9 0.017 EXP CRC 22 EXP CRC 8.40E+06 EXP EPI t-Butyl alcohol (OO) 75650 8.90E-02 EST W9 9.94E-06 EST W9 0.024 EXP CRC 11 EXP CRC 1.00E+09 EXP EPI Butyl benzyl phthalate (DD) 85687 2.08E-02 EST W9 5.17E-06 EST W9 NA NA NA 199 EXP PC 2.69E+03 EXP EPI n-Butylbenzene 104518 5.28E-02 EST W9 7.33E-06 EST W9 0.008 EXP CRC 71 EXP CRC 1.18E+04 EXP EPI sec-Butylbenzene 135988 5.27E-02 EST W9 7.32E-06 EST W9 0.008 EXP CRC 52 EXP CRC 1.76E+04 EXP EPI

361 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L t-Butylbenzene (I) 98066 5.30E-02 EST W9 7.37E-06 EST W9 0.007 EXP CRC 60 EXP CRC 2.95E+04 EXP EPI Cadmium (B,KK) 7440439 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Camphene (I) 79925 7.18E-02 EST W9 8.38E-06 EST W9 NA NA NA 33 EXP PC 4.60E+03 EXP EPI Caprolactam (DD) 105602 6.89E-02 EST W9 8.95E-06 EST W9 0.014 EXP NPG 125 EXP CRC 7.72E+08 EXP EPI Carbaryl (DD) 63252 2.74E-02 EST W9 7.12E-06 EST W9 NA NA NA 193 EXP PC 1.10E+05 EXP EPI Carbazole 86748 4.50E-02 EST W9 8.22E-06 EST W9 NA NA NA NA NA NA 1.80E+03 EXP EPI Carbofuran (DD) 1563662 2.56E-02 EST W9 6.57E-06 EST W9 NA NA NA NA NA NA 3.20E+05 EXP EPI Carbon disulfide (I,R,DD) 75150 1.06E-01 EST W9 1.30E-05 EST W9 0.013 EXP CRC -30 EXP CRC 2.16E+06 EXP EPI Carbon tetrachloride (KK) 56235 5.71E-02 EST W9 9.78E-06 EST W9 NA NA NA NA NA NA 7.93E+05 EXP EPI Chlordane (J,KK) 57749 2.15E-02 EST W9 5.45E-06 EST W9 NA NA NA 55.6 EXP PC 5.60E+01 EXP EPI Chloride 16887006 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA 2-Chloroaniline 95512 6.55E-02 EST W9 9.29E-06 EST W9 NA NA NA 39.4 EXP NPG 8.16E+06 EXP EPI 4-Chloroaniline 106478 7.04E-02 EST W9 1.03E-05 EST W9 NA NA NA 104 EXP NPG 3.90E+06 EXP EPI Chlorobenzene (I,KK) 108907 7.21E-02 EST W9 9.48E-06 EST W9 0.013 EXP CRC 28 EXP CRC 4.98E+05 EXP EPI p-Chlorobenzene sulfonic acid 98668 5.70E-02 EST W9 6.66E-06 EST W9 NA NA NA NA NA NA 3.06E+08 EST PP 1-Chloro-1,1-difluoroethane 75683 8.04E-02 EST W9 1.01E-05 EST W9 0.06 EXP CRC NA NA NA 1.40E+06 EXP EPI Chloroethane (DD) 75003 1.05E-01 EST W9 1.18E-05 EST W9 0.038 EXP CRC -50 EXP CRC 6.71E+06 EXP EPI 2-Chloroethyl vinyl ether 110758 7.44E-02 EST W9 9.49E-06 EST W9 NA NA NA 27 EXP CRC 4.29E+05 EXP EPI Chloroform (KK) 67663 7.69E-02 EST W9 1.09E-05 EST W9 NA NA NA NA NA NA 7.95E+06 EXP EPI Chloromethane (I) 74873 1.24E-01 EST W9 1.36E-05 EST W9 0.081 EXP CRC NA NA NA 5.32E+06 EXP EPI 4-Chloro-3-methylphenol (DD) 59507 4.96E-02 EST W9 7.27E-06 EST W9 NA NA NA 118 EXP PC 3.83E+06 EXP EPI beta-Chloronaphthalene 91587 6.38E-02 EST W9 7.45E-06 EST W9 NA NA NA NA NA NA 1.17E+04 EXP EPI 2-Chlorophenol (DD) 95578 6.61E-02 EST W9 9.48E-06 EST W9 NA NA NA 64 EXP CRC 1.13E+07 EXP EPI o-Chlorotoluene (I) 95498 6.29E-02 EST W9 8.72E-06 EST W9 0.01 EXP PC 35.6 EXP NPG 3.74E+05 EXP EPI Chlorpyrifos (DD) 2921882 2.21E-02 EST W9 5.62E-06 EST W9 NA NA NA 27.8 EXP PC 1.12E+03 EXP EPI Chromium (III) (B,H,KK) 16065831 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Chromium (VI) (H,KK,MM) 18540299 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Chrysene (Q,MM) 218019 2.61E-02 EST W9 6.75E-06 EST W9 NA NA NA NA NA NA 2.00E+00 EXP PP

362 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L Cobalt (B) 7440484 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Copper (B) 7440508 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Cyanazine 21725462 4.91E-02 EST W9 5.74E-06 EST W9 NA NA NA NA NA NA 1.70E+05 EXP EPI Cyanide (P,R,DD) 57125 2.16E-01 EST W9 2.53E-05 EST W9 0.06 EXP CRC NA NA NA NA NA NA Cyclohexane (DD) 110827 8.00E-02 EST W9 9.11E-06 EST W9 0.013 EXP CRC -20 EXP CRC 5.50E+04 EXP EPI Cyclohexanone (OO) 108941 7.68E-02 EST W9 9.38E-06 EST W9 0.011 EXP CRC 44 EXP CRC 2.50E+07 EXP EPI Dacthal 1861321 3.96E-02 EST W9 4.63E-06 EST W9 NA NA NA NA NA NA 5.00E+02 EXP EPI Dalapon 75990 6.03E-02 EST W9 9.46E-06 EST W9 NA NA NA NA NA NA 5.02E+08 EXP EPI 4-4'-DDD 72548 2.35E-02 EST W9 6.02E-06 EST W9 NA NA NA NA NA NA 9.00E+01 EXP EPI 4-4'-DDE 72559 4.08E-02 EST W9 4.76E-06 EST W9 NA NA NA NA NA NA 4.00E+01 EXP EPI 4-4'-DDT (DD) 50293 2.29E-02 EST W9 5.85E-06 EST W9 NA NA NA 72.2 EXP NPG 5.50E+00 EXP EPI Decabromodiphenyl ether (DD) 1163195 1.89E-02 EST W9 4.77E-06 EST W9 NA NA NA NA NA NA 1.00E-01 EXP EPI Di-n-butyl phthalate (DD) 84742 2.14E-02 EST W9 5.33E-06 EST W9 0.005 EXP CRC 157 EXP CRC 1.12E+04 EXP EPI Di(2-ethylhexyl) adipate (DD) 103231 1.73E-02 EST W9 4.16E-06 EST W9 0.004 EXP CRC 206 EXP CRC 7.80E+02 EXP EPI Di-n-octyl phthalate 117840 1.73E-02 EST W9 4.17E-06 EST W9 NA NA NA NA NA NA 2.20E+01 EXP EPI Diacetone alcohol (I,OO) 123422 6.49E-02 EST W9 8.43E-06 EST W9 0.018 EXP CRC 58 EXP CRC 1.00E+09 EXP EPI Diazinon 333415 2.10E-02 EST W9 5.23E-06 EST W9 NA NA NA 82.8 EXP NPG 4.00E+04 EXP EPI Dibenzo(a,h)anthracene (Q,MM) 53703 2.36E-02 EST W9 6.02E-06 EST W9 NA NA NA NA NA NA 2.49E+00 EXP EPI Dibenzofuran 132649 6.24E-02 EST W9 7.29E-06 EST W9 NA NA NA NA NA NA 3.10E+03 EXP EPI Dibromochloromethane (MM) 124481 3.66E-02 EST W9 1.06E-05 EST W9 NA NA NA NA NA NA 2.70E+06 EXP EPI Dibromochloropropane (MM) 96128 3.20E-02 EST W9 8.87E-06 EST W9 NA NA NA NA NA NA 1.23E+06 EXP EPI Dibromomethane 74953 5.51E-02 EST W9 1.19E-05 EST W9 NA NA NA NA NA NA 1.19E+07 EXP EPI Dicamba (DD) 1918009 2.92E-02 EST W9 7.80E-06 EST W9 NA NA NA NA NA NA 8.31E+06 EXP EPI 1,2-Dichlorobenzene 95501 5.62E-02 EST W9 8.92E-06 EST W9 0.022 EXP CRC 66 EXP CRC 1.56E+05 EXP EPI 1,3-Dichlorobenzene 541731 5.58E-02 EST W9 8.85E-06 EST W9 NA NA NA 72 EXP CRC 1.25E+05 EXP EPI 1,4-Dichlorobenzene (KK) 106467 5.50E-02 EST W9 8.68E-06 EST W9 0.025 EXP NPG 66 EXP CRC 8.13E+04 EXP EPI 3,3`-Dichlorobenzidine 91941 4.75E-02 EST W9 5.55E-06 EST W9 NA NA NA NA NA NA 3.10E+03 EXP EPI Dichlorodifluoromethane 75718 7.30E-02 EST W9 1.02E-05 EST W9 NA NA NA NA NA NA 2.80E+05 EXP EPI

363 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L 1,1-Dichloroethane 75343 8.36E-02 EST W9 1.06E-05 EST W9 0.054 EXP CRC -17 EXP CRC 5.04E+06 EXP EPI 1,2-Dichloroethane (I,KK) 107062 8.57E-02 EST W9 1.10E-05 EST W9 0.062 EXP CRC 13 EXP CRC 8.60E+06 EXP EPI 1,1-Dichloroethylene (I,KK) 75354 8.63E-02 EST W9 1.10E-05 EST W9 0.065 EXP CRC -28 EXP CRC 2.42E+06 EXP EPI cis-1,2-Dichloroethylene 156592 8.84E-02 EST W9 1.13E-05 EST W9 0.03 EXP CRC 6 EXP CRC 6.41E+06 EXP EPI trans-1,2-Dichloroethylene 156605 8.76E-02 EST W9 1.12E-05 EST W9 0.06 EXP CRC 2 EXP CRC 4.52E+06 EXP PP 2,6-Dichloro-4-nitroaniline 99309 1.30E-02 EST W9 2.88E-06 EST W9 NA NA NA NA NA NA 7.00E+03 EXP EPI 2,4-Dichlorophenol (DD) 120832 4.88E-02 EST W9 8.74E-06 EST W9 NA NA NA 114 EXP CRC 5.55E+06 EXP EPI 2,4-Dichlorophenoxyacetic acid (KK) 94757 2.79E-02 EST W9 7.34E-06 EST W9 NA NA NA NA NA NA 6.77E+05 EXP EPI 1,2-Dichloropropane (I) 78875 7.33E-02 EST W9 9.71E-06 EST W9 0.034 EXP CRC 21 EXP CRC 2.80E+06 EXP EPI 1,3-Dichloropropene (J) 542756 7.65E-02 EST W9 1.02E-05 EST W9 0.053 EXP NPG 25 EXP NPG 2.80E+06 EXP EPI Dichlorvos (MM) 62737 2.79E-02 EST W9 7.33E-06 EST W9 NA NA NA NA NA NA 8.00E+06 EXP EPI Dicyclohexyl phthalate 84617 2.24E-02 EST W9 5.68E-06 EST W9 NA NA NA 185 EXP PC 4.00E+03 EXP EPI Dieldrin 60571 2.33E-02 EST W9 6.01E-06 EST W9 NA NA NA NA NA NA 1.95E+02 EXP EPI Diethyl ether 60297 8.52E-02 EST W9 9.36E-06 EST W9 0.019 EXP CRC -45 EXP CRC 6.00E+07 EXP EPI Diethyl phthalate 84662 2.49E-02 EST W9 6.35E-06 EST W9 0.007 EXP CRC 161 EXP CRC 1.08E+06 EXP EPI Diethylene glycol monobutyl ether 112345 4.14E-02 EST W9 6.97E-06 EST W9 0.008 EXP PC 78 EXP PC 1.00E+09 EXP EPI Diisopropyl ether (DD) 108203 6.54E-02 EST W9 7.76E-06 EST W9 0.014 EXP CRC -28 EXP CRC 8.80E+06 EXP EPI Diisopropylamine (I) 108189 6.59E-02 EST W9 7.78E-06 EST W9 0.011 EXP CRC -1 EXP CRC 1.10E+08 EXP EPI Dimethyl phthalate 131113 2.99E-02 EST W9 7.14E-06 EST W9 0.009 EXP CRC 146 EXP CRC 4.00E+06 EXP EPI N,N-Dimethylacetamide (OO) 127195 8.45E-02 EST W9 1.00E-05 EST W9 0.018 EXP CRC 70 EXP CRC 1.00E+09 EXP EPI N,N-Dimethylaniline 121697 6.25E-02 EST W9 8.31E-06 EST W9 NA NA NA 63 EXP CRC 1.45E+06 EXP EPI Dimethylformamide (I,OO) 68122 9.72E-02 EST W9 1.12E-05 EST W9 0.022 EXP CRC 58 EXP CRC 1.00E+09 EXP EPI 2,4-Dimethylphenol 105679 6.22E-02 EST W9 8.31E-06 EST W9 0.011 EXP PC 112 EXP PC 7.87E+06 EXP EPI 2,6-Dimethylphenol 576261 6.35E-02 EST W9 8.54E-06 EST W9 NA NA NA 73 EXP PC 6.05E+06 EXP EPI 3,4-Dimethylphenol 95658 6.28E-02 EST W9 8.41E-06 EST W9 NA NA NA NA NA NA 4.76E+06 EXP EPI Dimethylsulfoxide 67685 9.86E-02 EST W9 1.18E-05 EST W9 0.026 EXP CRC 95 EXP CRC 1.00E+09 EXP EPI 2,4-Dinitrophenol 51285 4.07E-02 EST W9 9.08E-06 EST W9 NA NA NA NA NA NA 2.79E+06 EXP EPI 2,4-Dinitrotoluene (KK) 121142 3.82E-02 EST W9 8.11E-06 EST W9 NA NA NA 207 EXP CRC 2.00E+05 EXP EPI

364 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L Dinoseb (DD) 88857 4.92E-02 EST W9 5.74E-06 EST W9 NA NA NA 15.6 EXP PC 5.20E+04 EXP EPI 1,4-Dioxane (I,OO) 123911 8.74E-02 EST W9 1.05E-05 EST W9 0.02 EXP CRC 12 EXP CRC 1.00E+09 EXP EPI Diquat 85007 2.08E-02 EST W9 5.19E-06 EST W9 NA NA NA NA NA NA 7.08E+08 EXP PP Dissolved oxygen (DO) NA NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Diuron 330541 2.77E-02 EST W9 7.29E-06 EST W9 NA NA NA NA NA NA 4.20E+04 EXP EPI Endosulfan (J) 115297 2.25E-02 EST W9 5.76E-06 EST W9 NA NA NA NA NA NA 3.25E+02 EXP EPI Endothall 145733 3.67E-02 EST W9 8.18E-06 EST W9 NA NA NA NA NA NA 1.00E+08 EXP EPI Endrin (KK) 72208 2.30E-02 EST W9 5.90E-06 EST W9 NA NA NA NA NA NA 2.50E+02 EXP PP Epichlorohydrin (I) 106898 8.88E-02 EST W9 1.11E-05 EST W9 0.038 EXP CRC 31 EXP CRC 6.59E+07 EXP EPI Ethanol (I,DD,OO) 64175 1.24E-01 EST W9 1.32E-05 EST W9 0.033 EXP CRC 13 EXP CRC 1.00E+09 EXP EPI Ethyl acetate (I) 141786 8.23E-02 EST W9 9.70E-06 EST W9 0.02 EXP CRC -4 EXP CRC 8.00E+07 EXP EPI Ethyl-tert-butyl ether (ETBE) 637923 6.61E-02 EST W9 7.87E-06 EST W9 0.0124 EXP PC -19 EXP PC 1.20E+07 EXP EPI Ethylbenzene (I) 100414 6.85E-02 EST W9 8.46E-06 EST W9 0.008 EXP CRC 21 EXP CRC 1.69E+05 EXP EPI Ethylene dibromide 106934 4.30E-02 EST W9 1.04E-05 EST W9 NA NA NA NA NA NA 3.91E+06 EXP EPI Ethylene glycol (DD) 107211 1.17E-01 EST W9 1.36E-05 EST W9 0.032 EXP CRC 111 EXP CRC 1.00E+09 EXP EPI Ethylene glycol monobutyl ether 111762 6.26E-02 EST W9 8.14E-06 EST W9 0.04 EXP CRC 69 EXP CRC 1.00E+09 EXP EPI Ethylenediaminetetraacetic acid (EDTA) (II) 60004 1.90E-02 EST W9 4.60E-06 EST W9 NA NA NA NA NA NA 1.00E+06 EXP EPI Fluoranthene 206440 5.51E-02 EST W9 6.44E-06 EST W9 NA NA NA NA NA NA 2.60E+02 EXP EPI Fluorene 86737 6.28E-02 EST W9 7.34E-06 EST W9 NA NA NA NA NA NA 1.69E+03 EXP EPI Fluorine (soluble fluoride) (DD) 7782414 NR NA NA NR NA NA NA NA NA NA NA NA 1.69E+03 EXP EPI Formaldehyde (MM,OO) 50000 2.07E-01 EST W9 2.47E-05 EST W9 0.07 EXP CRC 85 EXP CRC 4.00E+08 EXP EPI Formic acid (I,U,OO) 64186 1.48E-01 EST W9 1.72E-05 EST W9 0.18 EXP CRC 50 EXP CRC 1.00E+09 EXP EPI 1-Formylpiperidine (DD) 2591868 6.91E-02 EST W9 8.98E-06 EST W9 NA NA NA NA NA NA 9.58E+07 EST PP Gentian violet 548629 3.45E-02 EST W9 4.04E-06 EST W9 NA NA NA NA NA NA 4.00E+06 EXP EPI Glyphosate (DD) 1071836 4.96E-02 EST W9 9.63E-06 EST W9 NA NA NA NA NA NA 1.05E+07 EXP EPI Heptachlor (DD,KK) 76448 2.29E-02 EST W9 5.89E-06 EST W9 NA NA NA NA NA NA 1.80E+02 EXP PP Heptachlor epoxide (KK) 1024573 3.56E-02 EST W9 4.16E-06 EST W9 NA NA NA NA NA NA 2.00E+02 EXP EPI n-Heptane 142825 6.49E-02 EST W9 7.59E-06 EST W9 0.0105 EXP CRC -4 EXP CRC 3.40E+03 EXP EPI

365 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L Hexabromobenzene 87821 2.83E-02 EST W9 3.30E-06 EST W9 NA NA NA NA NA NA 1.60E-01 EXP EPI Hexachlorobenzene (C-66) (KK) 118741 2.90E-02 EST W9 7.85E-06 EST W9 NA NA NA 242 EXP PC 6.20E+00 EXP EPI Hexachlorobutadiene (C-46) (KK) 87683 2.67E-02 EST W9 7.03E-06 EST W9 NA NA NA 90 EXP PC 3.20E+03 EXP EPI alpha-Hexachlorocyclohexane 319846 2.75E-02 EST W9 7.35E-06 EST W9 NA NA NA 65.6 EXP PC 2.00E+03 EXP PP beta-Hexachlorocyclohexane 319857 2.77E-02 EST W9 7.40E-06 EST W9 NA NA NA 65.6 EXP PC 2.40E+02 EXP PP Hexachlorocyclopentadiene (C-56) 77474 2.72E-02 EST W9 7.22E-06 EST W9 NA NA NA NA NA NA 1.80E+03 EXP EPI Hexachloroethane (KK) 67721 3.21E-02 EST W9 8.89E-06 EST W9 NA NA NA NA NA NA 5.00E+04 EXP EPI n-Hexane 110543 7.31E-02 EST W9 8.17E-06 EST W9 0.011 EXP CRC -22 EXP CRC 9.50E+03 EXP EPI 2-Hexanone 591786 7.04E-02 EST W9 8.44E-06 EST W9 0.01 EXP CRC 25 EXP CRC 1.72E+07 EXP EPI Indeno(1,2,3-cd)pyrene (Q,MM) 193395 4.48E-02 EST W9 5.23E-06 EST W9 NA NA NA NA NA NA 1.90E-01 EXP EPI Iron (B) 7439896 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Isobutyl alcohol (I,OO) 78831 8.97E-02 EST W9 1.00E-05 EST W9 0.017 EXP CRC 28 EXP CRC 8.50E+07 EXP EPI Isophorone (DD) 78591 5.25E-02 EST W9 7.53E-06 EST W9 0.008 EXP CRC 84 EXP CRC 1.20E+07 EXP EPI Isopropyl alcohol (I,DD,OO) 67630 1.03E-01 EST W9 1.12E-05 EST W9 0.02 EXP CRC 12 EXP CRC 1.00E+09 EXP EPI Isopropyl benzene 98828 6.03E-02 EST W9 7.86E-06 EST W9 0.009 EXP CRC 36 EXP CRC 6.13E+04 EXP EPI Lead (B,L,DD,KK) 7439921 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Lindane (KK) 58899 2.75E-02 EST W9 7.35E-06 EST W9 NA NA NA 65.6 EXP PC 7.30E+03 EXP EPI Lithium (B,DD) 7439932 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Magnesium 7439954 NR NA NA NR NA NA NA NA NA 500 EXP PC NA NA NA Manganese (B) 7439965 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Mercury (Total) (Z,DD,KK) Varies Mercury, elemental 7439976 7.09E-02 EST W9 3.01E-05 EST W9 NA NA NA NA NA NA 6.00E+01 EXP PP Mercuric chloride 7487947 NR NA NA NR NA NA NA NA NA NA NA NA 6.90E+07 EXP EPI Methyl mercury (DD) 22967926 5.28E-02 EST W9 6.17E-06 EST W9 NA NA NA NA NA NA NA NA NA Methane (K) 74828 2.21E-01 EST W9 2.01E-05 EST W9 0.05 EXP CRC -188 EXP NPG 2.20E+04 EXP EPI Methanol (DD,OO) 67561 1.58E-01 EST W9 1.65E-05 EST W9 0.06 EXP CRC 11 EXP CRC 1.00E+09 EXP EPI Methoxychlor (DD,KK) 72435 2.21E-02 EST W9 5.59E-06 EST W9 NA NA NA NA NA NA 1.00E+02 EXP EPI 2-Methoxyethanol (I,DD,OO) 109864 9.52E-02 EST W9 1.10E-05 EST W9 0.018 EXP CRC 39 EXP CRC 1.00E+09 EXP EPI

366 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L 2-Methyl-4-chlorophenoxyacetic acid 94746 3.03E-02 EST W9 8.24E-06 EST W9 NA NA NA NA NA NA 6.30E+05 EXP EPI 2-Methyl-4,6-dinitrophenol 534521 3.19E-02 EST W9 8.36E-06 EST W9 NA NA NA NA NA NA 1.98E+05 EXP EPI N-Methyl-morpholine (I,OO) 109024 7.32E-02 EST W9 8.96E-06 EST W9 NA NA NA 24 EXP CRC 1.00E+09 EXP EPI Methyl parathion 298000 2.50E-02 EST W9 6.44E-06 EST W9 NA NA NA 42 EXP PC 3.77E+04 EXP EPI 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 6.98E-02 EST W9 8.35E-06 EST W9 0.012 EXP CRC 18 EXP CRC 1.90E+07 EXP EPI Methyl-tert-butyl ether (MTBE) 1634044 7.53E-02 EST W9 8.59E-06 EST W9 0.016 EXP PC -33 EXP PC 5.10E+07 EXP EPI N-methylaniline 100618 7.21E-02 EST W9 9.13E-06 EST W9 NA NA NA 79.4 EXP NPG 5.62E+06 EXP EPI Methylcyclopentane (I) 96377 7.88E-02 EST W9 8.93E-06 EST W9 0.01 EXP CRC -29 EXP CRC 4.20E+04 EXP EPI 4,4`-Methylene-bis-2-chloroaniline (MBOCA) (MM) 101144 2.55E-02 EST W9 6.61E-06 EST W9 NA NA NA 113 EXP PC 1.39E+04 EXP EPI Methylene chloride (MM) 75092 9.99E-02 EST W9 1.25E-05 EST W9 0.13 EXP CRC NA NA NA 1.30E+07 EXP EPI 2-Methylnaphthalene 91576 5.24E-02 EST W9 7.78E-06 EST W9 NA NA NA 97 EXP PC 2.46E+04 EXP EPI Methylphenols (JJ,KK) 1319773 2-Methylphenol (DD,KK) 95487 7.04E-02 EST W9 9.39E-06 EST W9 0.014 EXP CRC 81 EXP CRC 2.59E+07 EXP EPI 3-Methylphenol (KK) 108394 7.08E-02 EST W9 9.32E-06 EST W9 0.011 EXP CRC 86 EXP CRC 2.27E+07 EXP EPI 4-Methylphenol (KK) 106445 7.08E-02 EST W9 9.32E-06 EST W9 0.011 EXP CRC 86 EXP CRC 2.15E+07 EXP EPI Metolachlor 51218452 2.19E-02 EST W9 5.48E-06 EST W9 NA NA NA 93.3 EXP PC 5.30E+05 EXP EPI Metribuzin 21087649 2.73E-02 EST W9 7.13E-06 EST W9 NA NA NA NA NA NA 1.05E+06 EXP EPI Mirex 2385855 2.85E-02 EST W9 3.33E-06 EST W9 NA NA NA NA NA NA 8.50E+01 EXP EPI Molybdenum 7439987 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Naphthalene 91203 6.05E-02 EST W9 8.38E-06 EST W9 0.009 EXP CRC 79 EXP CRC 3.10E+04 EXP EPI Nickel (B) 7440020 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Nitrate (N,DD) 14797558 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Nitrite (N,DD) 14797650 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Nitrobenzene (I,KK) 98953 6.81E-02 EST W9 9.45E-06 EST W9 0.018 EXP CRC 88 EXP CRC 2.09E+06 EXP EPI 2-Nitrophenol 88755 6.43E-02 EST W9 9.98E-06 EST W9 NA NA NA 108 EXP PC 2.50E+06 EXP EPI n-Nitroso-di-n-propylamine 621647 5.64E-02 EST W9 7.76E-06 EST W9 NA NA NA NA NA NA 1.30E+07 EXP EPI N-Nitrosodiphenylamine 86306 2.84E-02 EST W9 7.19E-06 EST W9 NA NA NA NA NA NA 3.50E+04 EXP EPI Oxamyl 23135220 2.35E-02 EST W9 5.87E-06 EST W9 NA NA NA NA NA NA 2.80E+08 EXP EPI

367 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L Oxo-hexyl acetate (OO) 88230357 4.83E-02 EST W9 7.11E-06 EST W9 NA NA NA 45 EXP PC NA NA NA Pendimethalin (DD) 40487421 2.27E-02 EST W9 5.72E-06 EST W9 NA NA NA 33 EXP PC 3.30E+02 EXP EPI Pentachlorobenzene 608935 2.94E-02 EST W9 7.95E-06 EST W9 NA NA NA NA NA NA 8.31E+02 EXP EPI Pentachloronitrobenzene 82688 2.63E-02 EST W9 6.92E-06 EST W9 NA NA NA NA NA NA 4.40E+02 EXP EPI Pentachlorophenol (KK) 87865 2.95E-02 EST W9 8.01E-06 EST W9 NA NA NA NA NA NA 1.40E+04 EXP EPI Pentane 109660 8.21E-02 EST W9 8.80E-06 EST W9 0.014 EXP CRC -40 EXP CRC 3.80E+04 EXP EPI 2-Pentene (I) 109682 8.49E-02 EST W9 9.09E-06 EST W9 NA NA NA -20 EXP PC 2.03E+05 EXP EPI Perchlorate (DD) 14797730 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Perfluorooctanoic acid 335671 2.26E-02 EST W9 5.79E-06 EST W9 NA NA NA NA NA NA 9.50E+06 EST PP Perfluorooctane sulfonic acid (DD) 1763231 3.02E-02 EST W9 3.52E-06 EST W9 NA NA NA NA NA NA 3.10E+00 EST PC pH NA NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Phenanthrene 85018 3.75E-02 EST W9 7.47E-06 EST W9 NA NA NA 171 EXP CRC 1.15E+03 EXP EPI Phenol (DD) 108952 8.40E-02 EST W9 1.04E-05 EST W9 0.018 EXP CRC 79 EXP CRC 8.28E+07 EXP EPI Phenytoin (DD) 57410 4.76E-02 EST W9 5.56E-06 EST W9 NA NA NA NA NA NA 3.20E+04 EXP EPI Phosphorus, Total Varies NA NA NA NR NA NA NA NA NA NA NA NA NA NA NA Phosphorus, White (R,DD) 7723140 NR NA NA NR NA NA NA NA NA NA NA NA 3.30E+03 EXP EPI o-Phthalic acid 88993 4.99E-02 EST W9 9.34E-06 EST W9 NA NA NA 168 EXP CRC 6.97E+06 EXP EPI Phthalic anhydride 85449 5.95E-02 EST W9 9.77E-06 EST W9 0.017 EXP CRC 152 EXP CRC 6.20E+06 EXP EPI Picloram 1918021 4.90E-02 EST W9 5.73E-06 EST W9 NA NA NA NA NA NA 4.30E+05 EXP EPI Piperidine (OO) 110894 8.30E-02 EST W9 9.64E-06 EST W9 NA NA NA 16 EXP CRC 1.00E+09 EXP EPI Polybrominated biphenyls (J,DD) 67774327 2.59E-02 EST W9 3.03E-06 EST W9 NA NA NA NA NA NA 1.10E+01 EXP PC Polychlorinated biphenyls (PCBs) (J,T,DD) 1336363 4.32E-02 EST W9 5.04E-06 EST W9 NA NA NA NA NA NA 7.00E+02 EXP EPI Polychlorinated biphenyls (PCBs) congeners (O) (O) Prometon 1610180 5.13E-02 EST W9 6.00E-06 EST W9 NA NA NA NA NA NA 7.50E+05 EXP EPI Propachlor 1918167 2.68E-02 EST W9 6.96E-06 EST W9 NA NA NA NA NA NA 5.80E+05 EXP EPI Propazine 139402 2.49E-02 EST W9 6.36E-06 EST W9 NA NA NA NA NA NA 8.60E+03 EXP EPI Propionic acid (OO) 79094 9.81E-02 EST W9 1.14E-05 EST W9 0.029 EXP CRC 52 EXP CRC 1.00E+09 EXP EPI Propyl alcohol (I,DD,OO) 71238 1.04E-01 EST W9 1.14E-05 EST W9 0.022 EXP CRC 23 EXP CRC 1.00E+09 EXP EPI

368 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L n-Propylbenzene (I,DD) 103651 6.02E-02 EST W9 7.83E-06 EST W9 0.008 EXP CRC 30 EXP CRC 5.22E+04 EXP EPI Propylene glycol 57556 9.81E-02 EST W9 1.15E-05 EST W9 0.026 EXP CRC 99 EXP CRC 1.00E+09 EXP EPI Pyrene 129000 2.78E-02 EST W9 7.25E-06 EST W9 NA NA NA NA NA NA 1.35E+02 EXP EPI Pyridine (I,KK) 110861 9.31E-02 EST W9 1.09E-05 EST W9 0.018 EXP CRC 20 EXP CRC 1.00E+09 EXP EPI Selenium (B,KK) 7782492 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Silver (KK) 7440224 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Silvex (2,4,5-TP) (KK) 93721 2.34E-02 EST W9 5.92E-06 EST W9 NA NA NA NA NA NA 7.10E+04 EXP EPI Simazine 122349 2.81E-02 EST W9 7.37E-06 EST W9 NA NA NA NA NA NA 6.20E+03 EXP EPI Sodium 17341252 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Sodium azide 26628228 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Sodium bromide 7647156 NR NA NA NR NA NA NA NA NA NA NA NA 9.46E+08 EXP PC Strontium (B,DD) 7440246 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Styrene 100425 7.11E-02 EST W9 8.78E-06 EST W9 0.009 EXP CRC 31 EXP CRC 3.10E+05 EXP EPI Sulfate 14808798 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Sulfolane 126330 7.16E-02 EST W9 9.91E-06 EST W9 NA NA NA 177 EXP CRC 1.0E+09 EXP PP Tebuthiuron (DD) 34014181 5.09E-02 EST W9 5.94E-06 EST W9 NA NA NA NA NA NA 2.50E+06 EXP EPI 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416 3.77E-02 EST W9 3.53E-06 EST W9 NA NA NA NA NA NA 9.96E-03 EST PP 1,2,4,5-Tetrachlorobenzene (DD) 95943 3.19E-02 EST W9 8.75E-06 EST W9 NA NA NA 155 EXP CRC 5.95E+02 EXP EPI 2,3,7,8-Tetrachlorodibenzo-p-dioxin (O,DD) 1746016 2.57E-02 EST W9 6.76E-06 EST W9 NA NA NA 4 EXP PC 2.00E-01 EXP EPI 1,1,1,2-Tetrachloroethane 630206 4.82E-02 EST W9 9.10E-06 EST W9 NA NA NA NA NA NA 1.07E+06 EXP EPI 1,1,2,2-Tetrachloroethane 79345 4.89E-02 EST W9 9.29E-06 EST W9 NA NA NA NA NA NA 2.83E+06 EXP EPI Tetrachloroethylene (KK) 127184 5.05E-02 EST W9 9.46E-06 EST W9 NA NA NA NA NA NA 2.06E+05 EXP EPI Tetrahydrofuran (DD) 109999 9.54E-02 EST W9 1.08E-05 EST W9 0.02 EXP CRC -14 EXP CRC 1.00E+09 EXP EPI 1,1,3,3-Tetramethylurea (OO) 632224 6.59E-02 EST W9 8.59E-06 EST W9 NA NA NA 77 EXP CRC 1.00E+09 EXP EPI Tetranitromethane 509148 3.35E-02 EST W9 8.60E-06 EST W9 NA NA NA NA NA NA 9.00E+05 EXP EPI Thallium 7440280 NR NA NA NR NA NA NA NA NA 216 EXP PC NA NA NA Toluene (I) 108883 7.78E-02 EST W9 9.20E-06 EST W9 0.011 EXP CRC 4 EXP CRC 5.26E+05 EXP EPI p-Toluidine 106490 7.12E-02 EST W9 8.98E-06 EST W9 0.011 EXP PC 87 EXP CRC 6.50E+06 EXP EPI

369 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L Total dissolved solids (TDS) NA NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Toxaphene (KK) 8001352 3.42E-02 EST W9 4.00E-06 EST W9 NA NA NA NA NA NA 5.50E+02 EXP PP Triallate (DD) 2303175 2.25E-02 EST W9 5.67E-06 EST W9 NA NA NA 90 EXP PC 4.00E+03 EXP EPI Tributylamine 102829 2.80E-02 EST W9 5.68E-06 EST W9 0.014 EXP PC 63 EXP CRC 1.42E+05 EXP EPI 1,2,3-Trichlorobenzene 87616 3.95E-02 EST W9 8.38E-06 EST W9 NA NA NA 112.7 EXP NPG 1.80E+04 EXP EPI 1,2,4-Trichlorobenzene 120821 3.96E-02 EST W9 8.40E-06 EST W9 0.025 EXP CRC 105 EXP CRC 4.90E+04 EXP EPI 1,1,1-Trichloroethane 71556 6.48E-02 EST W9 9.60E-06 EST W9 0.08 EXP CRC NA NA NA 1.29E+06 EXP EPI 1,1,2-Trichloroethane 79005 6.69E-02 EST W9 1.00E-05 EST W9 0.06 EXP CRC 32 EXP CRC 4.59E+06 EXP EPI Trichloroethylene (DD,KK,MM,NN) 79016 6.87E-02 EST W9 1.02E-05 EST W9 0.08 EXP CRC 90 EXP PC 1.28E+06 EXP EPI Trichlorofluoromethane 75694 6.54E-02 EST W9 1.00E-05 EST W9 NA NA NA NA NA NA 1.10E+06 EXP EPI 2,4,5-Trichlorophenol (KK) 95954 3.31E-02 EST W9 8.69E-06 EST W9 NA NA NA 133 EXP PC 1.20E+06 EXP EPI 2,4,6-Trichlorophenol (DD,KK) 88062 3.31E-02 EST W9 8.68E-06 EST W9 NA NA NA 99 EXP PC 8.00E+05 EXP EPI 1,2,3-Trichloropropane (MM) 96184 5.75E-02 EST W9 9.24E-06 EST W9 0.032 EXP CRC 71 EXP CRC 1.75E+06 EXP EPI 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 3.76E-02 EST W9 8.59E-06 EST W9 NA NA NA NA NA NA 1.70E+05 EXP EPI Triethanolamine 102716 5.14E-02 EST W9 8.08E-06 EST W9 0.01 EXP CRC 179 EXP CRC 1.00E+09 EXP EPI Triethylene glycol (DD) 112276 5.09E-02 EST W9 8.06E-06 EST W9 0.009 EXP CRC 177 EXP CRC 1.00E+09 EXP EPI 3-Trifluoromethyl-4-nitrophenol (DD) 88302 5.43E-02 EST W9 6.34E-06 EST W9 NA NA NA NA NA NA 5.00E+06 EXP EPI Trifluralin 1582098 2.15E-02 EST W9 5.41E-06 EST W9 NA NA NA 151 EXP PC 1.84E+02 EXP EPI 2,2,4-Trimethyl pentane 540841 5.74E-02 EST W9 7.06E-06 EST W9 0.011 EXP PC -12 EXP CRC 2.44E+03 EXP EPI 2,4,4-Trimethyl-2-pentene (I) 107404 5.98E-02 EST W9 7.35E-06 EST W9 NA NA NA 2 EXP CRC 1.29E+04 EST PP 1,2,3-Trimethylbenzene (I, J) 526738 6.13E-02 EST W9 8.02E-06 EST W9 0.008 EXP CRC 44 EXP CRC 7.52E+04 EXP EPI 1,2,4-Trimethylbenzene (I, J) 95636 6.07E-02 EST W9 7.92E-06 EST W9 0.009 EXP CRC 44 EXP CRC 5.70E+04 EXP EPI 1,3,5-Trimethylbenzene (I, J) 108678 6.02E-02 EST W9 7.84E-06 EST W9 0.01 EXP CRC 50 EXP CRC 4.82E+04 EXP EPI Triphenyl phosphate 115866 2.11E-02 EST W9 5.27E-06 EST W9 NA NA NA 220 EXP CRC 1.90E+03 EXP EPI tris(2,3-Dibromopropyl)phosphate 126727 1.94E-02 EST W9 4.88E-06 EST W9 NA NA NA 112 EXP PC 8.00E+03 EXP EPI Urea 57136 1.28E-01 EST W9 1.54E-05 EST W9 NA NA NA NA NA NA 5.45E+08 EXP EPI Vanadium (B) 7440622 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA Vinyl acetate (I,DD) 108054 8.49E-02 EST W9 1.00E-05 EST W9 0.026 EXP CRC -8 EXP CRC 2.00E+07 EXP EPI

370 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Lower Abstract Explosive S Hazardous Substance Service Air Da Da Water Dw Dw Limit in LEL LEL Flash FP FP Water S Sourc Number Diffusivity Basis Source Diffusivity Basis Source Air Basis Source Point Basis Source Solubility Basis e D D LEL FP S a w cm2 /s cm2 /s unitless ºC µg/L Vinyl chloride (KK,LL,MM) 75014 1.07E-01 EST W9 1.20E-05 EST W9 0.036 EXP CRC -78 EXP CRC 8.80E+06 EXP EPI Xylenes (I,J) 1330207 6.91E-02 EST W9 8.56E-06 EST W9 0.009 EXP CRC 27 EXP CRC 1.06E+05 EXP PP Zinc (B) 7440666 NR NA NA NR NA NA NA NA NA NA NA NA NA NA NA

371 2017 MR 22 – December 15, 2017

TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol Acenaphthene 83329 1.222 EXP CRC 2.15E-03 EXP EPI 8.03E+02 EXP EPA4 1.22E+04 EXP EPA4 Acenaphthylene 208968 0.8987 EXP CRC 6.68E-03 EXP EPI NA NA NA NA NA NA Acetaldehyde (I) 75070 0.7834 EXP CRC 9.02E+02 EXP EPI 466.00 EXP EPA4 6.16E+03 EXP EPA4 Acetate 71501 NA NA NA NA NA NA NA NA NA NA NA NA Acetic acid (OO) 64197 1.0446 EXP CRC 1.57E+01 EXP EPI 593 EXP CRC 5.66E+03 EXP CRC Acetone (I) 67641 0.7845 EXP CRC 2.32E+02 EXP EPI 508.10 EXP EPA1 6.96E+03 EXP EPA1 Acetonitrile 75058 0.7857 EXP CRC 8.88E+01 EXP EPI 545.50 EXP EPA4 7.11E+03 EXP EPA4 Acetophenone (DD) 98862 1.0281 EXP CRC 3.97E-01 EXP EPI 709.50 EXP EPA4 1.17E+04 EXP EPA4 Acrolein (I) 107028 0.84 EXP CRC 2.74E+02 EXP EPI 506.00 EXP EPA4 6.73E+03 EXP EPA4 Acrylamide (MM) 79061 1.13 EXP PC 7.00E-03 EXP EPI NA NA NA NA NA NA Acrylic acid (DD,OO) 79107 1.0511 EXP CRC 3.97E+00 EXP EPI 615.15 EXP HSDB 1.10E+04 EXP HSDB Acrylonitrile (I) 107131 0.8007 EXP CRC 1.09E+02 EXP EPI 519.00 EXP EPA4 7.79E+03 EXP EPA4 Alachlor 15972608 1.133 EXP CRC 2.20E-05 EXP PP NA NA NA NA NA NA Aldicarb 116063 1.195 EXP CRC 3.47E-05 EXP EPI NA NA NA NA NA NA Aldicarb sulfone 1646884 NA NA NA 9.00E-05 EXP EPI NA NA NA NA NA NA Aldicarb sulfoxide 1646873 NA NA NA 1.00E-04 EXP EPI NA NA NA NA NA NA Aldrin 309002 1.6 EXP PC 1.20E-04 EXP EPI 8.39E+02 EXP EPA4 1.50E+04 EST EPA4 Aluminum (B,DD) 7429905 NR NA NA NR NA NA NR NA NA NR NA NA Ammonia 7664417 NA NA NA 7.51E+03 EXP EPI 405.55 EXP HSDB 5.58E+03 EXP CRC t-Amyl methyl ether (TAME) 994058 0.766 EXP CRC 7.52E+01 EXP EPI 536 EXP CRC NA NA NA Aniline 62533 1.0217 EXP CRC 6.67E-01 EXP EPI 704 EXP CRC 1.01E+04 EXP CRC Anthracene 120127 1.28 EXP CRC 6.53E-06 EXP EPI 873.00 EXP EPA1 1.31E+04 EXP EPA1 Antimony 7440360 NR NA NA NR NA NA NR NA NA NR NA NA Arsenic (B,KK) 7440382 NR NA NA NR NA NA NR NA NA NA NA NA Asbestos (BB) 1332214 NR NA NA NR NA NA NR NA NA NR NA NA Atrazine 1912249 1.23 EXP PC 2.89E-07 EXP EPI NA NA NA NA NA NA Azobenzene 103333 1.203 EXP PC 3.61E-04 EXP EPI NA NA NA NA NA NA Barium (B,KK) 7440393 NR NA NA NR NA NA NR NA NA NR NA NA Benzene (I,KK) 71432 0.8765 EXP CRC 9.48E+01 EXP EPI 562.16 EXP EPA1 7.34E+03 EXP EPA1 372 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol Benzidine (MM) 92875 1.25 EXP PC 8.98E-07 EST PP NA NA NA NA NA NA Benzo(a)anthracene (Q,MM) 56553 1.274 EXP PC 2.10E-07 EXP EPI 1004.79 EXP EPA1 1.60E+04 EST EPA1 Benzo(b)fluoranthene (Q,MM) 205992 NA NA NA 5.00E-07 EXP EPI 9.69E+02 EXP EPA4 1.70E+04 EST EPA4 Benzo(k)fluoranthene (Q,MM) 207089 NA NA NA 9.65E-10 EXP EPI 1019.70 EXP EPA1 1.80E+04 EST EPA1 Benzo(g,h,i)perylene 191242 1.3 EXP PC 1.00E-10 EXP EPI NA NA NA NA NA NA Benzo(a)pyrene (Q,DD,MM) 50328 1.351 EXP PC 5.49E-09 EXP EPI 969.27 EXP EPA1 1.90E+04 EST EPA1 Benzoic acid 65850 1.2659 EXP CRC 7.00E-04 EXP EPI 751.00 EXP EPA1 1.21E+04 EXP EPA1 Benzyl alcohol 100516 1.0419 EXP CRC 9.40E-02 EXP EPI 715 EXP CRC 1.21E+04 EXP CRC Benzyl chloride 100447 1.1004 EXP CRC 1.23E+00 EXP EPI 685.00 EXP EPA4 8.77E+03 EXP EPA4 Beryllium (B) 7440417 NR NA NA NR NA NA NR NA NA NR NA NA bis(2-Chloroethoxy)ethane 112265 1.195 EXP CRC 6.00E-02 EXP EPI NA NA NA NA NA NA bis-2-Chloroethylether (I) 111444 1.22 EXP CRC 1.55E+00 EXP EPI 6.60E+02 EXP EPA4 1.08E+04 EXP EPA4 bis(2-Ethylhexyl) phthalate (DD) 117817 0.981 EXP CRC 1.42E-07 EXP EPI 806.00 EXP EPA1 1.60E+04 EXP EPA1 Boron (DD) 7440428 NR NA NA NR NA NA NR NA NA NR NA NA Bromate 15541454 NR NA NA NR NA NA NR NA NA NR NA NA Bromobenzene (I) 108861 1.495 EXP CRC 4.18E+00 EXP EPI 670.15 EXP HSDB 1.06E+04 EXP HSDB Bromodichloromethane (DD) 75274 1.98 EXP CRC 5.00E+01 EXP PP 5.86E+02 EXP EPA4 7.80E+03 EST EPA4 Bromoform 75252 2.8788 EXP CRC 5.60E+00 EXP PC 6.96E+02 EXP EPA4 9.48E+03 EXP EPA4 Bromomethane 74839 1.6755 EXP CRC 1.62E+03 EXP EPI 467.00 EXP EPA4 5.71E+03 EXP EPA4 n-Butanol (I,OO) 71363 0.8095 EXP CRC 6.70E+00 EXP EPI 563.05 EXP EPA1 1.03E+04 EXP EPA1 2-Butanone (MEK) (I,DD,KK) 78933 0.7999 EXP CRC 9.06E+01 EXP EPI 536.78 EXP EPA4 7.48E+03 EXP EPA4 n-Butyl acetate 123864 0.8825 EXP CRC 1.15E+01 EXP EPI 578 EXP CRC 8.67E+03 EXP CRC t-Butyl alcohol (OO) 75650 0.7887 EXP CRC 4.07E+01 EXP EPI NA NA NA 9.34E+03 EXP HSDB Butyl benzyl phthalate (DD) 85687 1.119 EXP CRC 8.25E-06 EXP EPI 839.68 EXP EPA1 1.40E+04 EST EPA1 n-Butylbenzene 104518 0.8601 EXP CRC 1.06E+00 EXP EPI 660.50 EXP EPA4 9.29E+03 EXP EPA4 sec-Butylbenzene 135988 0.858 EXP PC 1.75E+00 EXP EPI 679.00 EXP EPA4 8.87E+04 EXP EPA4 t-Butylbenzene (I) 98066 0.8665 EXP CRC 2.20E+00 EXP EPI 1220.00 EXP EPA4 8.98E+03 EXP EPA4 Cadmium (B,KK) 7440439 NR NA NA NR NA NA NR NA NA NR NA NA Camphene (I) 79925 NA NA NA 2.51E+00 EXP EPI NA NA NA NA NA NA 373 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol Caprolactam (DD) 105602 1.01 EXP PC 1.90E-03 EXP HSDB NA NA NA 1.31E+04 EXP HSDB Carbaryl (DD) 63252 1.228 EXP CRC 1.36E-06 EXP EPI NA NA NA NA NA NA Carbazole 86748 1.297 EXP CRC 1.37E-06 EST HSDB 899.00 EXP EPA1 1.40E+04 EXP EPA1 Carbofuran (DD) 1563662 1.18 EXP CRC 4.85E-06 EXP EPI NA NA NA NA NA NA Carbon disulfide (I,R,DD) 75150 1.2632 EXP CRC 3.59E+02 EXP EPI 5.52E+02 EXP EPA4 6.39E+03 EXP EPA4 Carbon tetrachloride (KK) 56235 1.594 EXP CRC 1.15E+02 EXP EPI 556.60 EXP EPA1 7.13E+03 EXP EPA1 Chlordane (J,KK) 57749 1.6 EXP CRC 9.75E-06 EXP EPI 885.73 EXP EPA1 1.40E+04 EST EPA1 Chloride 16887006 NR NA NA NR NA NA NR NA NA NR NA NA 2-Chloroaniline 95512 1.2114 EXP PC 2.04E-01 EXP EPI NA NA NA 1.06E+04 EXP CRC 4-Chloroaniline 106478 1.429 EXP CRC 2.70E-02 EXP EPI 754.00 EXP EPA1 1.17E+04 EXP EPA1 Chlorobenzene (I,KK) 108907 1.1058 EXP CRC 1.20E+01 EXP EPI 6.32E+02 EXP EPA4 8.41E+03 EXP EPA4 p-Chlorobenzene sulfonic acid 98668 NA NA NA 4.28E-06 EST PP NA NA NA NA NA NA 1-Chloro-1,1-difluoroethane 75683 1.107 EXP CRC 2.54E+03 EXP EPI 410.31 EXP CRC 5.36E+03 EXP HSDB Chloroethane (DD) 75003 0.918 EXP PC 1.01E+03 EXP EPI 460.40 EXP EPA4 5.88E+03 EXP EPA4 2-Chloroethyl vinyl ether 110758 1.0495 EXP CRC 2.68E+01 EXP EPI NA NA NA NA NA NA Chloroform (KK) 67663 1.4788 EXP CRC 1.97E+02 EXP EPI 536.40 EXP EPA1 6.99E+03 EXP EPA1 Chloromethane (I) 74873 0.911 EXP PC 4.30E+03 EXP EPI 416.25 EXP EPA4 5.11E+03 EXP EPA4 4-Chloro-3-methylphenol (DD) 59507 0.9 EXP PC 5.00E-02 EXP EPI NA NA NA NA NA NA beta-Chloronaphthalene 91587 NA NA NA 1.22E-02 EXT EPI NA NA NA NA NA NA 2-Chlorophenol (DD) 95578 1.2634 EXP CRC 2.53E+00 EXP EPI 6.75E+02 EXP EPA4 9.57E+03 EXP EPA4 o-Chlorotoluene (I) 95498 1.0825 EXP CRC 3.43E+00 EXP EPI 654.25 EXP HSDB 8.96E+03 EXP CRC Chlorpyrifos (DD) 2921882 1.44 EXP PC 2.03E-05 EXP EPI NA NA NA NA NA NA Chromium (III) (B,H,KK) 16065831 NR NA NA NR NA NA NR NA NA NR NA NA Chromium (VI) (H,KK,MM) 18540299 NR NA NA NR NA NA NR NA NA NR NA NA Chrysene (Q,MM) 218019 1.274 EXP CRC 6.23E-09 EXP PP 9.79E+02 EXP EPA4 1.65E+04 EXP EPA4 Cobalt (B) 7440484 NR NA NA NR NA NA NR NA NA NR NA NA Copper (B) 7440508 NR NA NA NR NA NA NR NA NA NR NA NA Cyanazine 21725462 NA NA NA 1.38E-07 EXP EPI NA NA NA NA NA NA Cyanide (P,R,DD) 57125 NR NA NA NR NA NA NR NA NA NR NA NA 374 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol Cyclohexane (DD) 110827 0.7739 EXP CRC 9.69E+01 EXP EPI 553.4 EXP CRC 7.16E+03 EXP CRC Cyclohexanone (OO) 108941 0.9478 EXP CRC 4.33E+00 EXP EPI 665 EXP CRC NA NA NA Dacthal 1861321 NA NA NA 2.50E-06 EXP EPI NA NA NA 2.50E+04 EXP HSDB Dalapon 75990 1.4014 EXP PC 1.51E-01 EXT EPI NA NA NA NA NA NA 4-4'-DDD 72548 1.476 EXP PC 1.35E-06 EXP EPI 863.77 EXP EPA1 1.70E+04 EST EPA1 4-4'-DDE 72559 NA NA NA 6.00E-06 EXT EPI 860.38 EXP EPA1 1.50E+04 EST EPA1 4-4'-DDT (DD) 50293 1.56 EXP PC 1.60E-07 EXP EPI 720.75 EXP EPA1 2.20E+04 EST EPA1 Decabromodiphenyl ether (DD) 1163195 3.0 EXP PC 4.67E-12 EST PP NA NA NA NA NA NA Di-n-butyl phthalate (DD) 84742 1.0465 EXP CRC 2.01E-05 EXP EPI 798.67 EXP EPA1 1.48E+04 EXP EPA1 Di(2-ethylhexyl) adipate (DD) 103231 0.922 EXP CRC 8.50E-07 EXP EPI 845 EXP HSDB NA NA NA Di-n-octyl phthalate 117840 0.978 EXP PC 1.00E-07 EXP EPI 862.22 EXP EPA1 1.40E+04 EST EPA1 Diacetone alcohol (I,OO) 123422 0.9387 EXP CRC 1.71E+00 EXP EPI 607 EXP HSDB 1.17E+04 EXP HSDB Diazinon 333415 1.1088 EXP CRC 9.01E-05 EXP EPI NA NA NA NA NA NA Dibenzo(a,h)anthracene (Q,MM) 53703 1.282 EXP PC 9.55E-10 EXT EPI 990.41 EXP EPA1 3.00E+04 EXP EPA1 Dibenzofuran 132649 NA NA NA 2.48E-03 EXP EPI 824.00 EXP EPA4 6.64E+04 EXP EPA4 Dibromochloromethane (MM) 124481 2.451 EXP PC 5.54E+00 EST PP 6.78E+02 EXP EPA4 5.90E+03 EXP EPA4 Dibromochloropropane (MM) 96128 2.08 EXP PC 5.80E-01 EXP EPI NA NA NA NA NA NA Dibromomethane 74953 2.4969 EXP CRC 4.44E+01 EXP EPI 583.00 EXP EPA4 7.87E+03 EXP EPA4 Dicamba (DD) 1918009 1.57 EXP CRC 1.25E-05 EXP EPI NA NA NA NA NA NA 1,2-Dichlorobenzene 95501 1.3059 EXP CRC 1.36E+00 EXP EPI 7.05E+02 EXP EPA4 9.70E+03 EXP EPA4 1,3-Dichlorobenzene 541731 1.2884 EXP CRC 2.15E+00 EXP EPI 684.00 EXP EPA4 9.23E+03 EXP EPA4 1,4-Dichlorobenzene (KK) 106467 1.2475 EXP PC 1.74E+00 EXP EPI 6.85E+02 EXP EPA4 9.27E+03 EXP EPA4 3,3`-Dichlorobenzidine 91941 NA NA NA 2.56E-07 EST PP 754.03 EXP EPA1 2.00E+04 EST EPA1 Dichlorodifluoromethane 75718 1.35 EXP PC 4.85E+03 EXP EPI 384.95 EXP EPA4 9.42E+03 EXP EPA4 1,1-Dichloroethane 75343 1.1757 EXP CRC 2.27E+02 EXP EPI 5.23E+02 EXP EPA4 6.90E+03 EXP EPA4 1,2-Dichloroethane (I,KK) 107062 1.2454 EXP CRC 7.89E+01 EXP EPI 5.61E+02 EXP EPA4 7.64E+03 EXP EPA4 1,1-Dichloroethylene (I,KK) 75354 1.213 EXP CRC 6.00E+02 EXP EPI 5.76E+02 EXP EPA4 6.25E+03 EXP EPA4 cis-1,2-Dichloroethylene 156592 1.2837 EXP CRC 2.00E+02 EXP PP 5.44E+02 EXP EPA4 7.19E+03 EXP EPA4 trans-1,2-Dichloroethylene 156605 1.2565 EXP CRC 3.31E+02 EXT PP 5.17E+02 EXP EPA4 6.72E+03 EXP EPA4 375 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol 2,6-Dichloro-4-nitroaniline 99309 0.28 EXP PC 1.20E-06 EXP EPI NA NA NA NA NA NA 2,4-Dichlorophenol (DD) 120832 1.4 EXP PC 9.00E-02 EXP EPI 708.17 EXP EPA1 1.50E+04 EST EPA1 2,4-Dichlorophenoxyacetic acid (KK) 94757 1.42 EXP PC 8.25E-05 EXP EPI NA NA NA NA NA NA 1,2-Dichloropropane (I) 78875 1.156 EXP CRC 5.33E+01 EXP EPI 5.72E+02 EXP EPA4 7.59E+03 EXP EPA4 1,3-Dichloropropene (J) 542756 1.224 EXP CRC 3.40E+01 EXP EPI 5.87E+02 EXP EPA4 7.90E+03 EST EPA4 Dichlorvos (MM) 62737 1.415 EXP CRC 1.58E-02 EXP EPI NA NA NA NA NA NA Dicyclohexyl phthalate 84617 1.383 EXP CRC 8.69E-07 EXP HSDB NA NA NA NA NA NA Dieldrin 60571 1.75 EXP CRC 5.89E-06 EXP EPI 842.25 EXP EPA1 1.70E+04 EST EPA1 Diethyl ether 60297 0.7138 EXP CRC 5.38E+02 EXP EPI 466.8 EXP CRC 6.34E+03 EXP CRC Diethyl phthalate 84662 1.120 EXP PC 2.10E-03 EXP EPI 757.00 EXP EPA1 1.37E+04 EXP EPA1 Diethylene glycol monobutyl ether 112345 0.9553 EXP CRC 2.19E-02 EXP EPI 692 EXP CRC NA NA NA Diisopropyl ether (DD) 108203 0.7192 EXP CRC 1.49E+02 EXP EPI 500.2 EXP CRC 6.96E+03 EXP CRC Diisopropylamine (I) 108189 0.7153 EXP CRC 7.94E+01 EXP EPI 523.1 EXP CRC 7.27E+03 EXP CRC Dimethyl phthalate 131113 1.1905 EXP CRC 3.08E-03 EXP EPI NA NA NA 1.81E+04 EXP HSDB N,N-Dimethylacetamide (OO) 127195 0.9372 EXP CRC 2.00E+00 EXP EPI 658.15 EXP HSDB 1.04E+04 EXP HSDB N,N-Dimethylaniline 121697 0.9557 EXP CRC 7.00E-01 EXP EPI 687.7 EXP CRC NA NA NA Dimethylformamide (I,OO) 68122 0.9445 EXP CRC 3.87E+00 EXP EPI 649.6 EXP CRC NA NA NA 2,4-Dimethylphenol 105679 0.965 EXP CRC 1.02E-01 EXP EPI 707.60 EXP EPA1 1.13E+04 EXP EPA1 2,6-Dimethylphenol 576261 1.01 EXP PC 2.74E-01 EXP HSDB 701 EXP CRC NA NA NA 3,4-Dimethylphenol 95658 0.983 EXP CRC 3.56E-02 EXP EPI 730 EXP CRC 1.40E+04 EXP HSDB Dimethylsulfoxide 67685 1.101 EXP CRC 6.10E-01 EXP EPI 707 EXP CRC 1.03E+04 EXP CRC 2,4-Dinitrophenol 51285 1.683 EXP CRC 3.90E-04 EXP EPI 827.85 EXP EPA1 2.50E+04 EXP EPA1 2,4-Dinitrotoluene (KK) 121142 1.379 EXP PC 1.47E-04 EXP EPI 814.00 EXP EPA1 1.35E+04 EXP EPA1 Dinoseb (DD) 88857 NA NA NA 5.25E-05 EXP PC NA NA NA NA NA NA 1,4-Dioxane (I,OO) 123911 1.0337 EXP CRC 3.81E+01 EXP EPI 587.3 EXP CRC 8.16E+03 EXP CRC Diquat 85007 1.24 EXP CRC 1.81E-06 EST PP NA NA NA NA NA NA Dissolved oxygen (DO) NA NR NA NA NR NA NA NR NA NA NR NA NA Diuron 330541 1.48 EXP PC 6.90E-08 EXP EPI NA NA NA NA NA NA Endosulfan (J) 115297 1.745 EXP CRC 1.73E-07 EXP EPI 9.43E+02 EXP EPA4 1.40E+04 EST EPA4 376 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol Endothall 145733 1.431 EXP PC 1.57E-10 EXP EPI NA NA NA NA NA NA Endrin (KK) 72208 1.7 EXP PC 3.00E-06 EXP PP 986.20 EXP EPA1 1.50E+04 EST EPA1 Epichlorohydrin (I) 106898 1.1812 EXP CRC 1.64E+01 EXP EPI NA NA NA 9.06E+03 EXP HSDB Ethanol (I,DD,OO) 64175 0.7893 EXP CRC 5.93E+01 EXP EPI 515 EXP CRC 9.22E+03 EST CRC Ethyl acetate (I) 141786 0.9003 EXP CRC 9.32E+01 EXP EPI 523.30 EXP EPA4 7.63E+03 EXP EPA4 Ethyl-tert-butyl ether (ETBE) 637923 0.736 EXP CRC 1.24E+02 EXP EPI NA NA NA 7.50E+03 EXP HSDB Ethylbenzene (I) 100414 0.8626 EXP CRC 9.60E+00 EXP EPI 6.17E+02 EXP EPA4 8.50E+03 EXP EPA4 Ethylene dibromide 106934 2.1683 EXP CRC 1.12E+01 EXP EPI 583.00 EXP EPA4 8.31E+03 EXP EPA4 Ethylene glycol (DD) 107211 1.1135 EXP CRC 9.20E-02 EXP EPI 719 EXP CRC 1.21E+04 EXP CRC Ethylene glycol monobutyl ether 111762 0.9015 EXP CRC 8.80E-01 EXP EPI 633.9 EXP CRC NA NA NA Ethylenediaminetetraacetic acid (EDTA) (II) 60004 0.86 EXP PC 1.50E-12 EXT EPI NA NA NA NA NA NA Fluoranthene 206440 NA NA NA 9.22E-06 EXP EPI 905.00 EXP EPA1 1.38E+04 EXP EPA1 Fluorene 86737 NA NA NA 6.00E-04 EXP EPI 8.70E+02 EXP EPA4 1.27E+04 EXP EPA4 Fluorine (soluble fluoride) (DD) 7782414 NR NA NA NR NA NA NR NA NA NR NA NA Formaldehyde (MM,OO) 50000 1.46 EXP PC 3.89E+03 EXP EPI 410.35 EXP HSDB 5.92E+03 EXP HSDB Formic acid (I,U,OO) 64186 1.22 EXP CRC 4.26E+01 EXP EPI 588 EXP CRC 5.42E+03 EXP CRC 1-Formylpiperidine (DD) 2591868 1.0158 EXP CRC 1.15E-01 EST PP NA NA NA NA NA NA Gentian violet 548629 NA NA NA 1.93E-14 EST PP NA NA NA NA NA NA Glyphosate (DD) 1071836 1.705 EXP PC 9.80E-08 EXP EPI NA NA NA NA NA NA Heptachlor (DD,KK) 76448 1.66 EXP PC 4.00E-04 EXP PP 8.46E+02 EXP EPA4 1.30E+04 EST EPA4 Heptachlor epoxide (KK) 1024573 NA NA NA 1.95E-05 EXP EPI 848.76 EXP EPA1 1.60E+04 EST EPA1 n-Heptane 142825 0.6795 EXP CRC 4.60E+01 EXP EPI 540.1 EXP CRC 7.59E+03 EXP CRC Hexabromobenzene 87821 NA NA NA 1.63E-08 EST PP NA NA NA NA NA NA Hexachlorobenzene (C-66) (KK) 118741 2.044 EXP CRC 1.80E-05 EXP EPI 8.25E+02 EXP EPA4 1.44E+04 EXP EPA4 Hexachlorobutadiene (C-46) (KK) 87683 1.556 EXP CRC 2.20E-01 EXP EPI 7.38E+02 EXP EPA4 1.02E+04 EXP EPA4 alpha-Hexachlorocyclohexane 319846 1.87 EXP PC 3.50E-05 EXP PC 8.39E+02 EXP EPA4 1.50E+04 EXP EPA4 beta-Hexachlorocyclohexane 319857 1.89 EXP CRC 3.60E-07 EXP PP 839.36 EXP EPA1 1.90E+04 EST EPA1 Hexachlorocyclopentadiene (C-56) 77474 1.7019 EXP CRC 6.00E-02 EXP EPI 7.46E+02 EXP EPA4 1.09E+04 EXP EPA4 Hexachloroethane (KK) 67721 2.091 EXP CRC 2.10E-01 EXP EPI 695.00 EXP EPA1 9.51E+03 EXP EPA1 377 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol n-Hexane 110543 0.6606 EXP CRC 1.51E+02 EXP EPI 508.00 EXP EPA4 6.90E+03 EXP EPA4 2-Hexanone 591786 0.8113 EXP CRC 1.16E+01 EXP EPI 586.7 EXP CRC 8.69E+03 EXP CRC Indeno(1,2,3-cd)pyrene (Q,MM) 193395 NA NA NA 1.25E-10 EST PP 1078.24 EXP EPA1 1.90E+04 EST EPA1 Iron (B) 7439896 NR NA NA NR NA NA NR NA NA NR NA NA Isobutyl alcohol (I,OO) 78831 0.8018 EXP CRC 1.05E+01 EXP EPI 547.78 EXP EPA4 1.09E+04 EXP EPA4 Isophorone (DD) 78591 0.9255 EXP CRC 4.38E-01 EXP EPI 715.00 EXP EPA1 1.03E+04 EXP EPA1 Isopropyl alcohol (I,DD,OO) 67630 0.7809 EXP CRC 4.54E+01 EXP EPI 508.3 EXP CRC 9.52E+03 EXP CRC Isopropyl benzene 98828 0.864 EXP CRC 4.50E+00 EXP EPI 631.10 EXP EPA4 1.03E+04 EXP EPA4 Lead (B,L,DD,KK) 7439921 NR NA NA NR NA NA NR NA NA NR NA NA Lindane (KK) 58899 1.87 EXP PC 4.20E-05 EXP EPI 839.36 EXP EPA1 1.50E+04 EST EPA1 Lithium (B,DD) 7439932 NR NA NA NR NA NA NR NA NA NR NA NA Magnesium 7439954 NR NA NA NR NA NA NR NA NA NR NA NA Manganese (B) 7439965 NR NA NA NR NA NA NR NA NA NR NA NA Mercury (Total) (Z,DD,KK) Varies Mercury, elemental 7439976 13.534 EXP PC 1.96E-03 EXP PP 1.75E+03 EXP EPA4 1.41E+04 EXP EPA4 Mercuric chloride 7487947 NR NA NA NR NA NA NR NA NA NR NA NA Methyl mercury (DD) 22967926 NR NA NA NA NA NA NR NA NA NR NA NA Methane (K) 74828 0.554 EXP PC 4.66E+05 EXP EPI 190.56 EXP CRC 1.96E+03 EXP CRC Methanol (DD,OO) 67561 0.7914 EXP CRC 1.27E+02 EXP EPI 512.7 EXP CRC 8.42E+03 EXP CRC Methoxychlor (DD,KK) 72435 1.41 EXP CRC 2.58E-06 EST PP 848.49 EXP EPA1 1.60E+04 EST EPA1 2-Methoxyethanol (I,DD,OO) 109864 0.9647 EXP CRC 9.50E+00 EXP EPI 598 EXP CRC 1.08E+04 EXP HSDB 2-Methyl-4-chlorophenoxyacetic acid 94746 1.56 EXP PC 5.90E-06 EXP EPI NA NA NA NA NA NA 2-Methyl-4,6-dinitrophenol 534521 1.58 EXP PC 1.20E-04 EXP EPI NA NA NA NA NA NA N-Methyl-morpholine (I,OO) 109024 0.9051 EXP CRC 1.32E+01 EST PP NA NA NA NA NA NA Methyl parathion 298000 1.358 EXP CRC 3.50E-06 EXP EPI NA NA NA NA NA NA 4-Methyl-2-pentanone (MIBK) (I,DD) 108101 0.7965 EXP CRC 1.99E+01 EXP EPI 571.00 EXP EPA4 8.24E+03 EXP EPA4 Methyl-tert-butyl ether (MTBE) 1634044 0.7353 EXP CRC 2.50E+02 EXP EPI 497.10 EXP EPA4 6.68E+03 EXP EPA4 N-methylaniline 100618 0.9891 EXP CRC 4.53E-01 EXP EPI 702 EXP CRC 1.27E+04 EXP HSDB Methylcyclopentane (I) 96377 0.7486 EXP CRC 1.38E+02 EXP EPI 532.78 EXP CRC 6.95E+03 EXP CRC 378 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol 4,4`-Methylene-bis-2- chloroaniline (MBOCA) 101144 1.44 EXP PC 2.86E-07 EST PP NA NA NA NA NA NA Methylene(MM) chloride (MM) 75092 1.3266 EXP CRC 4.35E+02 EXP EPI 510 EXP EPA4 6.71E+03 EXP EPA4 2-Methylnaphthalene 91576 1.0058 EXP CRC 5.50E-02 EXP EPI 761.00 EXP EPA4 1.26E+04 EXP EPA4 Methylphenols (JJ,KK) 1319773 2-Methylphenol (DD,KK) 95487 1.047 EXP PC 3.10E-01 EXP CRC 697.60 EXP CRC 1.08E+01 EXP CRC 3-Methylphenol (KK) 108394 1.0339 EXP CRC 1.10E-01 EXP EPI 705.80 EXP CRC 1.14E+01 EXP CRC 4-Methylphenol (KK) 106445 1.034 EXP PC 1.10E-01 EXP EPI 704.60 EXP CRC 1.13E+01 EXP CRC Metolachlor 51218452 1.12 EXP CRC 3.14E-05 EXP EPI NA NA NA NA NA NA Metribuzin 21087649 1.31 EXP CRC 4.35E-07 EXP EPI NA NA NA NA NA NA Mirex 2385855 NA NA NA 8.00E-07 EXP EPI NA NA NA NA NA NA Molybdenum 7439987 NR NA NA NR NA NA NR NA NA NR NA NA Naphthalene 91203 1.0253 EXP CRC 8.50E-02 EXP EPI 7.48E+02 EXP EPA4 1.04E+04 EXP EPA4 Nickel (B) 7440020 NR NA NA NR NA NA NR NA NA NR NA NA Nitrate (N,DD) 14797558 NR NA NA NR NA NA NR NA NA NR NA NA Nitrite (N,DD) 14797650 NR NA NA NR NA NA NR NA NA NR NA NA Nitrobenzene (I,KK) 98953 1.2037 EXP CRC 2.45E-01 EXP EPI 719 EXP EPA4 1.06E+04 EXP EPA4 2-Nitrophenol 88755 1.49 EXP PC 1.13E-01 EXP EPI NA NA NA 1.25E+04 EXP HSDB n-Nitroso-di-n-propylamine 621647 0.9163 EXP CRC 8.60E-02 EST PP 746.87 EXP EPA1 6.10E+03 EST EPA1 N-Nitrosodiphenylamine 86306 1.23 EXP PC 1.00E-01 EST PP 890.45 EXP EPA1 7.30E+03 EST EPA1 Oxamyl 23135220 0.97 EXP CRC 2.30E-04 EXP EPI NA NA NA NA NA NA Oxo-hexyl acetate (OO) 88230357 0.8779 EXP PC 1.32E+00 EXP PC NA NA NA NA NA NA Pendimethalin (DD) 40487421 1.19 EXP CRC 1.46E-05 EXP EPI NA NA NA NA NA NA Pentachlorobenzene 608935 1.8342 EXP CRC 2.00E-03 EXP PC NA NA NA 1.51E+04 EXP HSDB Pentachloronitrobenzene 82688 1.718 EXP CRC 5.00E-05 EXP EPI NA NA NA NA NA NA Pentachlorophenol (KK) 87865 1.978 EXP CRC 1.10E-04 EXP EPI 813.20 EXP EPA1 1.61E+04 EXP EPA1 Pentane 109660 0.6262 EXP CRC 5.14E+02 EXP EPI 469.7 EXP CRC 6.16E+03 EXP CRC 2-Pentene (I) 109682 0.6431 EXP PC 5.28E+02 EXP EPI NA NA NA NA NA NA Perchlorate (DD) 14797730 NR NA NA NR NA NA NR NA NA NR NA NA Perfluorooctanoic acid 335671 1.792 EXP HSDB 5.25E-01 EXP EPI NA NA NA NA NA NA 379 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol Perfluorooctane sulfonic acid (DD) 1763231 NA NA NA 2.00E-03 EST PC NA NA NA NA NA NA pH NA NR NA NA NR NA NA NR NA NA NR NA NA Phenanthrene 85018 1.179 EXP PC 1.21E-04 EXP EPI 869 EXP HSDB NA NA NA Phenol (DD) 108952 1.0722 EXP PC 3.50E-01 EXP EPI 694.20 EXP EPA1 1.09E+04 EXP EPA1 Phenytoin (DD) 57410 NA NA NA 1.20E-10 EST PP NA NA NA NA NA NA Phosphorus, Total Varies NR NA NA NA NA NA NA NA NA NA NA NA Phosphorus, White (R,DD) 7723140 NR NA NA NR NA NA NR NA NA NR NA NA o-Phthalic acid 88993 1.593 EXP PC 6.36E-07 EXP PC 800.00 EXP HSDB NA NA NA Phthalic anhydride 85449 1.53 EXP PC 5.17E-04 EXP PC NA NA NA 1.39E+04 EXP HSDB Picloram 1918021 NA NA NA 7.21E-11 EXP EPI NA NA NA NA NA NA Piperidine (OO) 110894 0.8606 EXP CRC 3.21E+01 EXP EPI 594.14 EXP CRC NA NA NA Polybrominated biphenyls (J,DD) 67774327 NA NA NA 5.20E-08 EXP PC NA NA NA NA NA NA Polychlorinated biphenyls (PCBs) (J,T,DD) 1336363 NA NA NA 4.94E-04 EST PP NA NA NA NA NA NA Polychlorinated biphenyls (PCBs) congeners (O) (O) Prometon 1610180 NA NA NA 2.30E-06 EXP EPI NA NA NA NA NA NA Propachlor 1918167 1.242 EXP CRC 2.30E-04 EXP EPI NA NA NA NA NA NA Propazine 139402 1.162 EXP CRC 1.31E-07 EXP EPI NA NA NA NA NA NA Propionic acid (OO) 79094 0.9882 EXP CRC 3.53E+00 EXP EPI 603 EXP CRC 7.41E+03 EXP HSDB Propyl alcohol (I,DD,OO) 71238 0.7997 EXP CRC 2.10E+01 EXP EPI 536.8 EXP CRC 9.90E+03 EXP CRC n-Propylbenzene (I,DD) 103651 0.8593 EXP CRC 3.42E+00 EXP EPI 630.00 EXP EPA4 9.12E+03 EXP EPA4 Propylene glycol 57556 1.0361 EXP CRC 1.29E-01 EXP EPI NA NA NA 1.28E+04 EXP HSDB Pyrene 129000 1.271 EXP CRC 4.50E-06 EXP EPI 9.36E+02 EXP EPA4 1.44E+04 EXP EPA4 Pyridine (I,KK) 110861 0.9819 EXP CRC 2.08E+01 EXP EPI 619 EXP CRC 8.39E+03 EXP CRC Selenium (B,KK) 7782492 NR NA NA NR NA NA NR NA NA NR NA NA Silver (KK) 7440224 NR NA NA NR NA NA NR NA NA NR NA NA Silvex (2,4,5-TP) (KK) 93721 1.2085 EXP PC 9.97E-06 EST PP NA NA NA NA NA NA Simazine 122349 1.302 EXP PC 2.21E-08 EXP EPI NA NA NA NA NA NA Sodium 17341252 NR NA NA NR NA NA NR NA NA NR NA NA Sodium azide 26628228 NR NA NA NR NA NA NR NA NA NR NA NA 380 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol Sodium bromide 7647156 NR NA NA NR NA NA NR NA NA NR NA NA Strontium (B,DD) 7440246 NR NA NA NR NA NA NR NA NA NR NA NA Styrene 100425 0.9016 EXP CRC 6.40E+00 EXP EPI 6.36E+02 EXP EPA4 8.74E+03 EXP EPA4 Sulfate 14808798 NR NA NA NR NA NA NR NA NA NR NA NA Sulfolane 126330 1.2723 EXP CRC 6.20E-03 EXP EPI NA NA NA NA NA NA Tebuthiuron (DD) 34014181 NA NA NA 3.00E-07 EXP EPI NA NA NA NA NA NA 2,3,7,8-Tetrabromodibenzo-p-dioxin (O) 50585416 NA NA NA 4.80E-09 EXT EPI NA NA NA NA NA NA 1,2,4,5-Tetrachlorobenzene (DD) 95943 1.858 EXP CRC 5.40E-03 EXP PC 762.95 EXP HSDB 1.14E+04 EXP HSDB 2,3,7,8-Tetrachlorodibenzo-p-dioxin (O,DD) 1746016 1.8 EXP PC 1.50E-09 EXP EPI NA NA NA NA NA NA 1,1,1,2-Tetrachloroethane 630206 1.5406 EXP CRC 1.20E+01 EXP EPI 6.24E+02 EXP EPA4 9.77E+03 EXP EPA4 1,1,2,2-Tetrachloroethane 79345 1.5953 EXP CRC 4.62E+00 EXP EPI 6.61E+02 EXP EPA4 9.00E+03 EXP EPA4 Tetrachloroethylene (KK) 127184 1.623 EXP CRC 1.85E+01 EXP EPI 6.20E+02 EXP EPA4 8.29E+03 EXP EPA4 Tetrahydrofuran (DD) 109999 0.8833 EXP CRC 1.62E+02 EXP EPI 540 EXP CRC 7.12E+03 EXP CRC 1,1,3,3-Tetramethylurea (OO) 632224 0.9687 EXP CRC 1.39E+01 EXP EPI NA NA NA NA NA NA Tetranitromethane 509148 1.638 EXP CRC 8.42E+00 EXP EPI NA NA NA 9.74E+03 EXP CRC Thallium 7440280 NR NA NA NR NA NA NR NA NA NR NA NA Toluene (I) 108883 0.8623 EXP CRC 2.84E+01 EXP EPI 5.92E+02 EXP EPA4 7.93E+03 EXP EPA4 p-Toluidine 106490 0.9619 EXP CRC 2.86E-01 EXP EPI 667 EXP CRC 1.06E+04 EXP CRC Total dissolved solids (TDS) NA NR NA NA NR NA NA NR NA NA NR NA NA Toxaphene (KK) 8001352 NA NA NA 6.69E-06 EXP PP 873.31 EXP EPA1 1.50E+04 EST EPA1 Triallate (DD) 2303175 1.273 EXP CRC 1.20E-04 EXP EPI NA NA NA NA NA NA Tributylamine 102829 0.777 EXP CRC 9.34E-02 EXP EPI 638.35 EXP HSDB 1.24E+04 EXP HSDB 1,2,3-Trichlorobenzene 87616 1.4533 EXP CRC 2.10E-01 EXP EPI 762.65 EXP HSDB 1.09E+04 EXP HSDB 1,2,4-Trichlorobenzene 120821 1.459 EXP CRC 4.60E-01 EXP EPI 7.25E+02 EXP EPA4 1.05E+04 EXP EPA4 1,1,1-Trichloroethane 71556 1.339 EXP CRC 1.24E+02 EXP EPI 545.00 EXP EPA1 7.14E+03 EXP EPA1 1,1,2-Trichloroethane 79005 1.4397 EXP CRC 2.30E+01 EXP EPI 6.02E+02 EXP EPA4 8.32E+03 EXP EPA4 Trichloroethylene (DD,KK,MM,NN) 79016 1.4642 EXP CRC 6.90E+01 EXP EPI 5.44E+02 EXP EPA4 7.51E+03 EXP EPA4 Trichlorofluoromethane 75694 1.4879 EXP CRC 8.03E+02 EXP EPI 471.00 EXP EPA4 6.00E+03 EXP EPA4 2,4,5-Trichlorophenol (KK) 95954 1.678 EXP PC 7.50E-03 EXP PC 759.13 EXP EPA1 1.10E+04 EST EPA1 381 2017 MR 22 – December 15, 2017 TABLE 3. CHEMICAL‐PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS/PART 213 RISK‐BASED SCREENING LEVELS Developed pursuant to R 299.50 of the Administrative Rules for Part 201, Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, MCL 324.20101 to 324.20142. Scientific notation is represented by E+ or E‐ a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The data set for each hazardous substance consists of 17 columns (excluding basis and source columns) across 4 pages. Review all 17 columns when evaluating data for a specific hazardous substance. Hazardous substance footnotes are defined in R 299.49. The data basis and sources are defined in R 299.50(6). Chemical Abstract Hazardous Substance Service Dens Dens Vapor VP VP Critical Tc Tc Enthalpy of ΔH Δ H Number Density Basis Source Pressure Basis Source Temperature Basis Source Vaporization Basis Source Dens VP Tc ΔH g/cm3 (mmHg) K cal/mol 2,4,6-Trichlorophenol (DD,KK) 88062 1.675 EXP PC 8.00E-03 EXP PC 749.03 EXP EPA1 1.20E+04 EST EPA1 1,2,3-Trichloropropane (MM) 96184 1.3889 EXP CRC 3.69E+00 EXP EPI 652.00 EXP EPA4 9.17E+03 EXP EPA4 1,1,2-Trichloro-1,2,2-trifluoroethane 76131 1.5635 EXP CRC 3.63E+02 EXP EPI 487.30 EXP EPA4 6.46E+03 EXP EPA4 Triethanolamine 102716 1.1242 EXP CRC 3.59E-06 EXP EPI 787.45 EXP HSDB 1.61E+04 EXP HSDB Triethylene glycol (DD) 112276 1.1274 EXP CRC 1.32E-03 EXP EPI 775 EXP CRC 1.71E+04 EXP CRC 3-Trifluoromethyl-4-nitrophenol (DD) 88302 NA NA NA 1.33E-03 EST PP NA NA NA NA NA NA Trifluralin 1582098 1.294 EXP PC 4.58E-05 EXP EPI NA NA NA NA NA NA 2,2,4-Trimethyl pentane 540841 0.6878 EXP CRC 4.93E+01 EXP EPI 543.9 EXP CRC 7.36E+03 EXP CRC 2,4,4-Trimethyl-2-pentene (I) 107404 0.7218 EXP CRC 3.59E+01 EXP EPI 555 EXP HSDB NA NA NA 1,2,3-Trimethylbenzene (I, J) 526738 0.8944 EXP CRC 1.69E+00 EXP EPI 664.50 EXP HSDB 1.17E+04 EXP HSDB 1,2,4-Trimethylbenzene (I, J) 95636 0.8758 EXP CRC 2.10E+00 EXP EPI 649.17 EXP EPA4 9.37E+03 EXP EPA4 1,3,5-Trimethylbenzene (I, J) 108678 0.8615 EXP CRC 2.48E+00 EXP EPI 637.25 EXP EPA4 9.32E+03 EXP EPA4 Triphenyl phosphate 115866 1.2055 EXP PC 6.28E-06 EXP PC NA NA NA NA NA NA tris(2,3-Dibromopropyl)phosphate 126727 2.27 EXP PC 1.90E-04 EXP EPI NA NA NA NA NA NA Urea 57136 1.323 EXP CRC 1.20E-05 EXP PC NA NA NA NA NA NA Vanadium (B) 7440622 NR NA NA NR NA NA NR NA NA NR NA NA Vinyl acetate (I,DD) 108054 0.9256 EXP CRC 9.02E+01 EXP EPI 5.19E+02 EXP EPA4 7.80E+03 EXP EPA4 Vinyl chloride (KK,LL,MM) 75014 0.9106 EXP CRC 2.98E+03 EXP EPI 432 EXP EPA4 5.25E+03 EXP EPA4 Xylenes (I,J) 1330207 0.8801 EXP PC 7.99E+00 EXP PP 621 EXP MDEQ 8.57E+03 EXP MDEQ Zinc (B) 7440666 NR NA NA NR NA NA NR NA NA NR NA NA

382 2017 MR 22 – December 15, 2017

TABLE 4. TOXICOLOGICAL AND CHEMICAL-PHYSICAL DATA FOR PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS Scientific notation is represented by E+ or E- a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The dataset for each hazardous substance requires 22 columns across two pages. Review all 22 columns when evaluating data for a specific hazardous substance. Soil Organic Relative Log Chemical Chronic Relative Carbon-Water Oral Inhalation Occupational Source Ingestion Dermal Octanol- Abstract Oral Slope Inhalation Source Partition Hazardous Substance Reference Unit Risk Short Term Contribution Absorption Absorption Water Service Factor Reference Contribution Coefficients for Dose Factor Exposure Level for Drinking Efficiency Efficiency Partition Number Concentration for Soil Organic Water Coefficient Compounds RfD SF RfC IURF STEL RSC AEi AEd RSC Log Kow Koc

mg/kg-day (mg/kg-day)-1 ug/m3 (ug/m3)-1 ug/m3 unitless unitless unitless unitless unitless L/kg Acenaphthene 83329 1.80E-01 NA 2.10E+02 NA NA 0.2 1 0.1 1 3.92 7,140 Acenaphthylene 208968 7.10E-03 NA 3.50E+01 NA NA 0.2 1 0.1 1 3.6 3,460 Acetaldehyde (I) 75070 1.30E-01 NA 9.00E+00 2.20E-06 4.50E+04 0.2 1 0.1 1 -0.367 0.613 Acetate 71501 5.70E-01 NA NA NA NA 0.2 NA NA NA NA NA Acetic acid 64197 5.70E-01 NA 2.50E+02 NA 3.70E+04 0.2 1 0.1 1 -0.23 0.595 Acetone (I) 67641 1.00E-01 NA 5.90E+03 NA 1.70E+06 0.2 1 0.1 1 -0.24 0.581 Acetonitrile 75058 1.90E-02 NA 6.00E+01 NA 1.01E+05 0.2 1 0.1 1 -0.337 0.648 Acetophenone 98862 2.10E-01 NA 4.90E+02 NA NA 0.2 1 0.1 1 1.6 37.4 Acrolein (I) 107028 1.60E-02 NA 2.00E-02 NA 6.90E+02 0.2 1 0.1 1 -0.01 1.18 Acrylamide 79061 2.00E-04 2.80E+00 6 1.30E-03 NA 0.2 1 0.1 1 -0.96 0.114 Acrylic acid 79107 5.30E-01 NA 1.00E+00 NA NA 0.2 1 0.1 1 0.35 2.21 Acrylonitrile (I) 107131 NA 3.30E-01 2.00E+00 6.80E-05 NA 0.2 1 0.1 1 0.255 1.78 Alachlor 15972608 1.00E-02 9.60E-02 NA NA NA 0.2 0.5 0.1 1 3.52 734 Aldicarb 116063 1.00E-03 NA NA NA NA 0.2 1 0.1 1 1.1 12.1 Aldicarb sulfone 1646884 1.10E-03 NA NA NA NA 0.2 1 0.1 1 -0.57 0.275 Aldicarb sulfoxide 1646873 1.30E-03 NA NA NA NA 0.2 1 0.1 1 -0.67 0.22 Aldrin 309002 2.50E-05 8.70E+00 NA 4.90E-03 NA 0.2 0.5 0.1 1 6.5 2.45E+06 Aluminum (B) 7429905 3.30E-01 NA NA NA NA 0.2 0.5 0.01 1 NR NR Ammonia 7664417 NA NA 1.00E+02 NA 2.40E+04 0.2 1 0.1 1 NA NA t-Amyl methyl ether (TAME) 994058 1.30E-01 NA 6.20E+01 NA NA 0.2 1 0.1 1 1.73 28.1 Aniline 62533 NA 1.60E-02 1.00E+00 1.60E-06 NA 0.2 1 0.1 1 0.978 9.15 Anthracene 120127 1.00E+00 NA 1.00E+03 NA NA 0.2 1 0.1 1 4.55 29,700 Antimony 7440360 3.50E-04 NA 2.00E-01 NA NA 0.2 0.5 0.01 1 NR NR Arsenic 7440382 2.70E-04 1.50E+00 NA 4.30E-03 NA 0.2 0.5 0.03 1 NR NR Asbestos (BB) 1332214 NA NA NA 4.60E-02 NA 1 1 0 1 NR NR

383 2017 MR 22 – December 15, 2017 TABLE 4. TOXICOLOGICAL AND CHEMICAL-PHYSICAL DATA FOR PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS Scientific notation is represented by E+ or E- a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The dataset for each hazardous substance requires 22 columns across two pages. Review all 22 columns when evaluating data for a specific hazardous substance. Soil Organic Relative Log Chemical Chronic Relative Carbon-Water Oral Inhalation Occupational Source Ingestion Dermal Octanol- Abstract Oral Slope Inhalation Source Partition Hazardous Substance Reference Unit Risk Short Term Contribution Absorption Absorption Water Service Factor Reference Contribution Coefficients for Dose Factor Exposure Level for Drinking Efficiency Efficiency Partition Number Concentration for Soil Organic Water Coefficient Compounds Atrazine 1912249 3.50E-02 7.40E-02 NA NA NA 0.2 1 0.1 1 2.7 451 Azobenzene 103333 NA 3.70E-02 NA 3.10E-05 NA 0.2 1 0.1 1 3.82 5,690 Barium (B) 7440393 7.00E-02 NA 5.00E+00 NA NA 1 0.5 0.01 1 NR NR

384 2017 MR 22 – December 15, 2017 TABLE 4. TOXICOLOGICAL AND CHEMICAL-PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS

Scientific notation is represented by E+ or E- a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The dataset for each hazardous substance consists of 22 columns across two pages. Review all 22 columns when evaluating data for a specific hazardous substance.

Soil-Water Distribution Physical Soil Koc for Coefficients for State at Ionizing Organic Inorganic Henry's Law Lower Standard Hazardous Substance Chemical Abstract Compounds at Compounds at Constant at Air Water Explosive Flash Water Temperature Molecular Service Number pH=6.8 pH=6.8 25C Diffusivity Diffusivity Limit in Air Point Solubility and Pressure Weight Di or Da or Kd HLC Dair D LEL FP S MW w

L/kg L/kg atm-m3/mol cm2/s cm2/s unitless F ug/L unitless g/mol Acenaphthene 83329 NR NR 1.55E-04 0.0421 7.69E-06 NA NA 4,240 Solid 154.2 Acenaphthylene 208968 NR NR 1.48E-03 0.08 8.00E-06 NA NA 3,930 Solid 152.271 Acetaldehyde (I) 75070 NR NR 7.95E-05 0.08 8.00E-06 0.04 -36 1.00E+09 Liquid 44.1 Acetate 71501 NA NA NA NA NA NA NA ID NA NA Acetic acid 64197 NR NR 1.00E-07 0.08 8.00E-06 0.04 103 6.00E+09 Liquid 60.05 Acetone (I) 67641 NR NR 3.88E-05 0.124 1.14E-05 0.025 0 1.00E+09 Liquid 58.08 Acetonitrile 75058 NR NR 2.40E-05 0.13 1.70E-05 0.03 42 2.00E+08 Liquid 41.05 Acetophenone 98862 NR NR 1.10E-05 0.08 8.00E-06 NA NA 6.10E+06 Liquid 120.2 Acrolein (I) 107028 NR NR 9.40E-05 0.11 1.20E-05 0.028 -15 2.10E+08 Liquid 56.06 Acrylamide 79061 NR NR 3.22E-10 0.097 1.10E-04 NA 280 2.20E+09 Solid 71.08 Acrylic acid 79107 NR NR 3.20E-07 0.08 8.00E-06 0.024 121 1.00E+09 Liquid 72.06 Acrylonitrile (I) 107131 NR NR 1.00E-04 0.12 1.30E-05 0.03 30 7.50E+07 Liquid 53.06 Alachlor 15972608 NR NR 8.32E-09 0.08 8.00E-06 NA NA 1.83E+05 Solid 269.77 Aldicarb 116063 NR NR 4.17E-09 0.08 8.00E-06 NA NA 6.00E+06 Solid 190.25 Aldicarb sulfone 1646884 NR NR 3.37E-09 0.08 8.00E-06 NA NA 7.80E+06 Solid 222.27 Aldicarb sulfoxide 1646873 NR NR 9.69E-10 0.08 8.00E-06 NA NA 2.80E+07 Solid 206.27 Aldrin 309002 NR NR 1.70E-04 0.0132 4.86E-06 NA NA 180 Solid 364.9 Aluminum (B) 7429905 NR NA NR NR NR NA NA NA Inorganic 26.982 Ammonia 7664417 NR NR 3.20E-04 0.08 8.00E-06 0.15 NA 5.30E+08 Liquid 17.04 t-Amyl methyl ether (TAME) 994058 NR NR 2.68E-03 0.08 8.00E-06 NA NA 2.64E+06 Liquid 102.18 Aniline 62533 NR NR 2.30E-06 0.07 8.30E-06 0.013 158 3.60E+07 Liquid 93.13 Anthracene 120127 NR NR 6.50E-05 0.0324 7.74E-06 NA NA 43.4 Solid 178.24 Antimony 7440360 NR 45 NR NR NR NA NA NA Inorganic 121.76 Arsenic 7440382 NR 29 NR NR NR NA NA NA Inorganic 74.922 Asbestos (BB) 1332214 NR NA NR NR NR NR NR NA Inorganic NA 385 Atrazine 1912249 NR NR 2.63E-09 0.08 8.00E-06 NA NA 70,000 Solid 215.72 Azobenzene 103333 NR NR 1.35E-05 0.08 8.00E-06 NA NA 6,400 Solid 182.23 Barium (B) 7440393 NR 41 NR NR NR NA NA NA Inorganic 137.327 2017 MR 22 – December 15, 2017 TABLE 4. TOXICOLOGICAL AND CHEMICAL-PHYSICAL DATA PART 201 GENERIC CLEANUP CRITERIA AND SCREENING LEVELS

Scientific notation is represented by E+ or E- a value, for example 200,000 is presented as 2.0E+5. Units are as indicated in each column heading. The dataset for each hazardous substance consists of 22 columns across two pages. Review all 22 columns when evaluating data for a specific hazardous substance.

Soil-Water Distribution Physical Soil Koc for Coefficients for State at Ionizing Organic Inorganic Henry's Law Lower Standard Hazardous Substance Chemical Abstract Compounds at Compounds at Constant at Air Water Explosive Flash Water Temperature Molecular Service Number pH=6.8 pH=6.8 25C Diffusivity Diffusivity Limit in Air Point Solubility and Pressure Weight Di or Da or Kd HLC Dair D LEL FP S MW w

L/kg L/kg atm-m3/mol cm2/s cm2/s unitless F ug/L unitless g/mol Acenaphthene 83329 NR NR 1.55E-04 0.0421 7.69E-06 NA NA 4,240 Solid 154.2 Acenaphthylene 208968 NR NR 1.48E-03 0.08 8.00E-06 NA NA 3,930 Solid 152.271 Acetaldehyde (I) 75070 NR NR 7.95E-05 0.08 8.00E-06 0.04 -36 1.00E+09 Liquid 44.1 Acetate 71501 NA NA NA NA NA NA NA ID NA NA Acetic acid 64197 NR NR 1.00E-07 0.08 8.00E-06 0.04 103 6.00E+09 Liquid 60.05 Acetone (I) 67641 NR NR 3.88E-05 0.124 1.14E-05 0.025 0 1.00E+09 Liquid 58.08 Acetonitrile 75058 NR NR 2.40E-05 0.13 1.70E-05 0.03 42 2.00E+08 Liquid 41.05 Acetophenone 98862 NR NR 1.10E-05 0.08 8.00E-06 NA NA 6.10E+06 Liquid 120.2 Acrolein (I) 107028 NR NR 9.40E-05 0.11 1.20E-05 0.028 -15 2.10E+08 Liquid 56.06 Acrylamide 79061 NR NR 3.22E-10 0.097 1.10E-04 NA 280 2.20E+09 Solid 71.08 Acrylic acid 79107 NR NR 3.20E-07 0.08 8.00E-06 0.024 121 1.00E+09 Liquid 72.06 Acrylonitrile (I) 107131 NR NR 1.00E-04 0.12 1.30E-05 0.03 30 7.50E+07 Liquid 53.06 Alachlor 15972608 NR NR 8.32E-09 0.08 8.00E-06 NA NA 1.83E+05 Solid 269.77 Aldicarb 116063 NR NR 4.17E-09 0.08 8.00E-06 NA NA 6.00E+06 Solid 190.25 Aldicarb sulfone 1646884 NR NR 3.37E-09 0.08 8.00E-06 NA NA 7.80E+06 Solid 222.27 Aldicarb sulfoxide 1646873 NR NR 9.69E-10 0.08 8.00E-06 NA NA 2.80E+07 Solid 206.27 Aldrin 309002 NR NR 1.70E-04 0.0132 4.86E-06 NA NA 180 Solid 364.9 Aluminum (B) 7429905 NR NA NR NR NR NA NA NA Inorganic 26.982 Ammonia 7664417 NR NR 3.20E-04 0.08 8.00E-06 0.15 NA 5.30E+08 Liquid 17.04 t-Amyl methyl ether (TAME) 994058 NR NR 2.68E-03 0.08 8.00E-06 NA NA 2.64E+06 Liquid 102.18 Aniline 62533 NR NR 2.30E-06 0.07 8.30E-06 0.013 158 3.60E+07 Liquid 93.13 Anthracene 120127 NR NR 6.50E-05 0.0324 7.74E-06 NA NA 43.4 Solid 178.24 Antimony 7440360 NR 45 NR NR NR NA NA NA Inorganic 121.76 Arsenic 7440382 NR 29 NR NR NR NA NA NA Inorganic 74.922 Asbestos (BB) 1332214 NR NA NR NR NR NR NR NA Inorganic NA 386 Atrazine 1912249 NR NR 2.63E-09 0.08 8.00E-06 NA NA 70,000 Solid 215.72 Azobenzene 103333 NR NR 1.35E-05 0.08 8.00E-06 NA NA 6,400 Solid 182.23 Barium (B) 7440393 NR 41 NR NR NR NA NA NA Inorganic 137.327 2017 MR 22 – December 15, 2017

PROPOSED ADMINISTRATIVE RULES

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY REMEDIATION AND REDEVELOPMENT DIVISION

CLEANUP CRITERIA REQUIREMENTS FOR RESPONSE ACTIVITY Rule Set 2015-094 EQ

NOTICE OF PUBLIC HEARING THURSDAY, January 18, 2018 Constitution Hall 525 West Allegan Street, Lansing ConCon Conference Room, Atrium, 2:00 p.m. – 4:00 p.m.

The Michigan Department of Environmental Quality (MDEQ), Remediation and Redevelopment Division (RRD), will hold a public hearing on Thursday, January 18, 2018 at Constitution Hall from 2:00 p.m. – 4:00 p.m. The hearing will be held to receive public comments on proposed changes to the Cleanup Criteria Requirements for Response Activity rules.

The proposed rule set (2015-094 EQ) will amend the current rules to revise the generic cleanup criteria established under Section 20120a which are also the risk-based screening levels for regulated substances under Section 21304a of the Natural Resources and Environmental Protection Act, Act 451 of 1994, as amended (NREPA), MCL 324.20120a and MCL 324.21304a.

The authority to propose rules for promulgation is conferred on the Director of the MDEQ by Sections 20104(1) and 20120a(17) of the NREPA, MCL 324.20104(1) and 324.20120a(17). At the conclusion of the promulgation process, these rules will take effect 180 days after filing with the Secretary of State.

The rules (2015-094 EQ) are published on the Office of Regulatory Reinvention’s website at www.michigan.gov/orr. Click on “Latest Rules Activity” and then “Pending Rule Changes.” Under “Rules by Department,” click on “Environmental Quality.” Scroll to ORR 2015-094 EQ and click on “Revision Text.”

Any interested person is invited to attend and present his or her views. It is requested that all statements be submitted in writing for the hearing record. Anyone unable to attend may submit comments in writing to the following address by 5:00 P.M. on Wednesday, January 24, 2018. Copies of the draft rules may also be obtained by mail or electronic transmission at the following address:

Remediation and Redevelopment Division Michigan Department of Environmental Quality (Attention: Dan Yordanich) P.O. Box 30426 Lansing, Michigan 48909-7926 Phone: 517-284-5174 Fax: 517-241-9581 E-Mail: [email protected]

Persons needing accommodations for effective participation in the meeting should contact the Remediation and Redevelopment Division at 517-284-5174 one week in advance to request mobility, visual hearing, or other assistance. The hearing location is handicap accessible.

387 2017 MR 22 – December 15, 2017

ADMINISTRATIVE RULES

DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

DIRECTOR’S OFFICE

GENERAL INDUSTRY SAFETY AND HEALTH STANDARD STANDARDS

Filed with the Secretary of State on

These rules become effective immediately upon filing with the Secretary of State unless adopted under section 33, 44, or 45a(6) of 1969 PA 306. Rules adopted under these sections become effective 7 days after filing with the Secretary of State.

(By authority conferred on the director of the department of licensing and regulatory affairs by sections 16 and 21 of 1974 PA 154, MCL 408.1016 and 408.1021, and Executive Reorganization Order Nos. 1996-2, 2003-18 2003-1, 2008-4, and 2011-4, MCL 408.1016, 408.1021, 445.2001, 445.2011, 445.2025, and 445.2030)

R 408.16301, R 408.16302, R 408.16309, R 408.16311, R 408.16312, R 408.16313, R 408.16321, R 408.16322, R 408.16323, R 408.16325, R 408.16331, R 408.16333, R 408.16335, R 408.16338, R 408.16343, R 408.16345, R 408.16346, R 408.16347, R 408.16350, R 408.16351, R 408.16353, R 408.16354, R 408.16356, R 408.16361, R 408.16362, R 408.16364, R 408.16372, R 408.16375, R 408.16377, and R 408.16387 of the Michigan Administrative Code are amended, and R 408.16318 is added, as follows:

PART 63. PULP, PAPER, AND PAPERBOARD MILLS

GENERAL PROVISIONS

R 408.16301 Scope. Rule 6301. (1) This standard part sets forth rules to protect the life, limb, and health of the employee in, about, or around places of employment where pulp, paper, and paperboard are manufactured and converted. (2) These rules apply to establishments where pulp, paper, and paperboard are manufactured and converted. These rules do not apply to logging and the transportation of logs to pulp, paper, and paperboard mills (3) Respiratory protection shall be in compliance with Occupational Health Standard Part 451 “Respiratory Protection,” as referenced in R 408.16302.

R 408.16302 Adopted and referenced standards. Rule 6302. (1) This standard is adopted by reference in these rules, National Fire Protection Association NFPA 91 “Blower and Exhaust Systems for Dust, Stock, and Vapor Removal or Conveying,” 1961 edition. This standard is available from NFPA, 1 Batterymarch Park, Quincy, Massachusetts, USA, 02169-7471, telephone number: 1-617-770-3000 or via the internet at website: www.nfpa.org; at a cost as of the time of adoption of these rules of $27.00. (2) The following standards are adopted by reference in these rules and are available from IHS Global, 15 Inverness Way East, Englewood, Colorado, 80112, USA, telephone number: 1-800-854-7179 or via the internet at website: http://global.ihs.com, at a cost as of the time of adoption of these rules, as stated in this subrule. (a) American National Standard Institute (ANSI) Standard Z9.1 “Open Surface Tanks-Ventilation and Operations,” 1951 edition. Cost: $20.00. (b) ANSI Z9.2 “Fundamentals Governing the Design and Operation of Local Exhaust Ventilation Systems,” 1960 edition. Cost $32.00. (c) American Society of Mechanical Engineers(ASME) Boiler and Pressure Vessel Code, Section VIII, “Unfired Pressure Vessels,” 1989 edition with addenda. Cost: $514.00. 388 2017 MR 22 – December 15, 2017 (3) The standards adopted in these rules subrules(1) and(2) of this rule are also available for inspection at the Department of Licensing and Regulatory Affairs, MIOSHA Regulatory Services Section, 530 West Allegan Street, 7150 Harris Drive, P.O. Box 30643, Lansing, Michigan, 48909-8143. (4) Copies of the standards adopted in these rules subrules (1) and (2) of this rule may be obtained from the publisher or may also be obtained from the Department of Licensing and Regulatory Affairs, MIOSHA Regulatory Services Section, 530 West Allegan Street, 7150 Harris Drive, P.O. Box 30643, Lansing, Michigan, 48909-8143, at the cost charged in this rule, plus $20.00 for shipping and handling. (5) The following Michigan Occupational Safety and Health Administration (MIOSHA) occupational safety and health standards are referenced in these rules. Up to 5 copies of these standards may be obtained at no charge from the Michigan Department of Licensing and Regulatory Affairs, MIOSHA Regulatory Services Section, regulatory services section, 530 West Allegan Street, 7150 Harris Drive, P.O. Box 30643, Lansing, MI, 48909-8143 or via the internet at website: www.michigan.gov/mioshastandards. For quantities greater than 5, the cost, at the time of adoption of these rules, is 4 cents per page. (a) General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” Standard Part 2 “Floor and Wall Openings, Stairways, and Skylights,” R 408.10201 to R 408.10241. (b) General Industry Safety Standard Part 7 “Guards for Power Transmission,” R 408.17201 to R 408.10765. (c) General Industry Safety Standard Part 23 “Hydraulic Power Presses,” R 408.12301 to R 408.12373. (d) General Industry Safety and Health Standard Part 27 “Woodworking Machinery,” R 408.12701 to R 408.12799. (e) General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” R 408.13301 to R 408.13398. (f) General Industry Safety and Health Standard Part 52 “Sawmills,” R 408.15201 to R 408.15284. R 408.15277. (g) Occupational Health Standard Part 301 “Air Contaminants,” Contaminants for General Industry,” R 325.51101 to R 325.51108. (h) Occupational Health Standard Part 380 “Occupational Noise Exposure in General Industry,” R 325.60101 to R 325.60128. (i) Occupational Health Standard Part 451 “Respiratory Protection,” R 325.60051 to R 325.60052.

R 408.16309 Definitions; T to V. Rule 6309. (1) "Tipple" means a device by which a loaded railcar or truck is emptied. (2) “Travel restraint system” means a combination of an anchorage, anchorage connector, lanyard or other means of connection, and body support that an employer uses to eliminate the possibility of an employee going over the edge of a walking-working surface. (3) (2) "Vessel" means a tank or vat used for storage or mixing of pulp or chemicals.

R 408.16311 Employer responsibility. Rule 6311. An employer shall do all of the following: (a) Provide training to each employee regarding the hazards and safeguards before starting an assigned job. (b) Provide personal protective equipment that is necessary to protect an employee from the hazards of the job according to the requirements of R 408.16313 and General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302. (c) Prevent the operation of a machine that is not guarded according to Michigan Occupational Safety and Health Administration (MIOSHA) standards, that has a defective guard, or that is otherwise unsafe. (d) Establish and maintain a lockout procedure as prescribed in R 408.16323(4). (e) Comply with the requirements of this standard. part.

R 408.16312 Employee responsibility. Rule 6312. An employee shall do all of the following: (a) Use personal protective equipment furnished by the employer. (b) Report to his or her supervisor any machine or safeguard that which is defective.

389 2017 MR 22 – December 15, 2017 (c) Not remove a guard except for authorized operational or maintenance purposes. The guard shall be replaced or equivalent guarding installed before the machine is returned to production. (d) Not operate any machine or equipment until he is trained in the operating procedures, hazards, and hazards and safeguards and has been authorized to do so.

R 408.16313 Personal protective equipment. Rule 6313. (1) A deluge shower and eye fountain shall be provided within 25 feet of an area where caustics or acids are used or mixed at a strength that could cause injury to an exposed employee. (2) An approved life jacket shall be provided to the employee, at no expense to the employee, and shall be used when an employee works above water where a protective standard barrier or lifeline and safety belt is not provided. (3) Personal protective equipment used by more than 1 employee shall be cleaned or sanitized after each usage where body contact has been made. (4) Eye protection, as prescribed specified in General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302, shall be provided to, and used by, employees who are in the wood yard and employees who are involved in any of the following operations: (a) Maintenance. (b) Barking. (c) Knot cleaning. (d) Digesting. (e) Pulp grinding. (f) Banding. (g) Chemical handling (5) Head protection, as prescribed specified in General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302, shall be provided to, and used by, employees who are in the wood yard and employees who are included in any of the following operations: (a) Barking. (b) Maintenance. (c) Digesting. (d) Pulp grinding. (6) Foot protection, as prescribed specified in General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302 shall be provided to, and used by, employees who are in the wood yard and employees who are involved in any of the following operations: (a) Pulp grinding. (b) Maintenance. (c) Hazardous chemical handling and mixing operations (7) Personal protective equipment such as aprons, gloves, rubber boots, and metal or plastic toe or metatarsal foot protection shall be provided and used as prescribed in General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302. (8) Respiratory equipment shall be provided to the employee, at no expense to the employee, and shall be available and maintained in an operable and sanitary condition where toxic fumes may be encountered above the maximum threshold limits as prescribed by Occupational Health Standard Part 301 “Air Contaminants,” Contaminants for General Industry,” and Part 451 “Respiratory Protection,” as referenced in R 408.16302.

R 408.16318 Belt conveyors. Rule 6318. (1) When conveyors cross passageways or roadways, an employer shall provide a horizontal platform under the conveyor, extended out from the sides of the conveyor a distance equal to 1 1∕2 times the length of the wood handled. (2) An employer shall provide the platform that shall extend the width of the road plus 2 feet (61 cm) on each side, and shall be kept free of wood and rubbish.

390 2017 MR 22 – December 15, 2017 (3) An employer shall provide the edges of the platform with toeboards or other protection that meet the requirements of General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” as referenced in R 408.16302.

R 408.16321 Illumination. Rule 6321. (1) An employer stall furnish natural Natural or artificial lighting shall be furnished to provide the following: (a) A minimum of 25 foot candles intensity at the machine operator’s work station. (b) A minimum of 5 foot candles along a means of egress. (c) A minimum of 2 foot candles in an inside active storage area. (2) An employee who is entering a vessel for the purpose of cleaning or inspecting the vessel shall be provided with an appropriate and intrinsically safe emergency portable illumination device. (3) Emergency lighting shall be provided where it is necessary for employees to remain at their machines or stations to shut down equipment in case of power failure. Emergency lighting shall be provided at stairways and passageways or aisle ways used by employees for emergency exit in case of power failure. Emergency lighting shall be provided in all plant first aid and medical facilities. (4) Emergency lighting shall be provided at stairways and passageways or aisle ways used by employees for emergency exit in case of power failure. (5) Emergency lighting shall be provided in all plant first aid and medical facilities.

R 408.16322 Walking-working surfaces. Floors, aisles and catwalks. Rule 6322. (1) An aisle or floor work area shall be free of protruding objects, holes, and loose boards. (2) An aisle shall be 3 feet wider than the widest load transported in the aisle and the outline of the aisle marked. (3) A slip-resistant surface shall be provided on platforms, at work stations, on walk ramps, plank walks, and catwalks. (4) A stair tread leading to a catwalk or platform shall have a slip-resistant surface. (5) A catwalk 4 feet or more above the floor, ground, or platform shall be guarded by a guardrail system standard barrier and toeboard on the open side as prescribed in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” as referenced in R 408.16302. R 408.10211, R 408.10231 and R 408.10233 of General Industry Safety Standard, Part 2 “Floor and Wall Openings, Stairways and Skylights,” as referenced in R 408.16302. However, a catwalk, regardless of height, above or adjacent to dangerous equipment shall be guarded with a guardrail system standard barrier and toeboard. (6) In the machine room, steps of uniform rise and tread with non-slip surfaces that meet the requirements in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces” shall be provided at each press.

R 408.16323 Power controls. Rule 6323.(1) A machine shall be equipped with an emergency stop device, distinguished by its size or color, which can be activated from the operator's or crew member's work station. In addition, a rotary cutter, paper machine, and calender shall have an emergency stop device which will provide a braking action to stop the machine quickly in an emergency. This device shall be tested periodically by making use of it when stopping the machine. (2) A machine attended by more than 1 operator shall be equipped with a control for each operator exposed to a point of operation hazard. These controls shall be interlocked to prevent operation until each operator operates his or her control concurrently. (3) A machine control shall be designed and installed to prevent unintentional activation by contact with objects or parts of the body. (4) A power source of any equipment to be repaired, serviced or set-up shall be locked out by each employee doing the work where unexpected startup would cause injury, except when motion is necessary during set-up or adjustment. Such motion shall be achieved by a manually held constant pressure control device. Residual pressure shall be relieved prior to and during such work when the equipment is locked out.

391 2017 MR 22 – December 15, 2017 (5) Upon power failure, provisions shall be made to prevent machines from automatically restarting upon restoration of power.

R 408.16325. Lubrication. Rule 6325. (1) An employer shall ensure that lubrication is Lubrication shall be accomplished by 1 of the following: (a) Manually, when the machine can be shut off and locked out. (b) Automatic pressure or gravity feed system. (c) Extension pipe leading to an area outside of guards or away from any hazards. (d) A means which would provide equal or greater protection than subdivision (a), (b) or (c) of this subrule for the employee. (2) An employer shall ensure that General Industry Safety Standard Part 7 “Guards for Power Transmission,” as referenced in R 408.16302, is shall be followed.

R 408.16331 Material handling. Rule 6331. (1) A mechanical lifting device shall be provided and used to place and remove rolls of paper and paperboard from a machine. (2) An escape hatch shall be provided where doors on an enclosed cab provided on a powered industrial truck may be blocked by special equipment. (3) A crane, powered industrial truck, or other wood handling equipment, except over the road vehicles, having a cab with windows shall have all windows protected by a screen made of steel rods not less than 7/16 inch in diameter with openings not more than 4 by 4 inches or 2 by 6 inches. (4) Where a hooker or hatch tender is used, the operator of a cab style crane shall respond to the hooker’s or hatch tender’s signals. The signals for an overhead crane shall be as prescribed in Table 1 ‘Standard Hand Signals for For Controlling Overhead and And Gantry Cranes.’ The signals for a boom type crane shall be as prescribed in Table 2 ‘Hand Signals for Boom-Type Cranes.’ (5) A blower used to transport rags shall be provided a feed hopper with the opening not less than 48 inches from the fan. The blower outlet must shall not allow material to fall on an employee. (6) Railroad cars shall not be spotted on tracks adjacent to the locomotive cranes unless a 24-inch clearance is maintained, as prescribed in R 408.16342(1). (7) The handling and storage of other materials shall conform to R 408.16342(1) and (2) with respect to clearance. (8) Handles of wood hooks shall be locked to the shank to prevent them from rotating. (9) An employee shall not ride on a powered hand truck unless it is so designed by the manufacturer. A limit switch shall be on the operating handle —30 degrees each way from a 45-degree angle up and down beyond which the drive motor is electrically disconnected and braking action commences. (10) Whenever possible, all dust, fumes, and gases incident to handling materials shall be controlled at the source, in accordance with ANSI Standard Z9.2 “Fundamentals Governing the The Design and Operation of Local Exhaust Ventilation Systems,” 1960 edition, as adopted in R 408.16302. Where control at the source is not possible, an employer shall provide respirators with goggles or protective masks, masks shall be provided, and employees shall wear them when handling alum, clay, soda, ash, lime, bleach powder, sulfur, chlorine, and similar materials, and when opening rag bales. (11) Hoods of cutters, shredders, and dusters shall have exhaust ventilation in accordance with ANSI Standard Z9.2 “Fundamentals Governing the The Design and Operation of Local Exhaust Ventilation Systems,” 1960 edition, as adopted in R 408.16302.

392 2017 MR 22 – December 15, 2017 TABLE 1 STANDARD HAND SIGNALS FOR CONTROLLING OVERHEAD AND GANTRY CRANE

BRIDGE TRAVEL. HOIST. LOWER. Arm extended forward, hand With forearm vertical, With arm extended downward, open and slightly raised, make forefinger pointing up, move forefinger pointing down, move pushing motion in direction of hand in small horizontal circle. hand in small horizontal circles. travel.

TROLLEY TRAVEL. Palm up, fingers closed, thumb STOP. EMERGENCY STOP. pointing in direction of motion, Arm extended, palm down, hold Arm extended, palm down, jerk hand horizontally. position rigidly. move hand rapidly right and left.

MOVE SLOWLY.

MULTIPLE TROLLEYS. Use one hand to give any MAGNET IS Hold up one finger for block motion signal and place other DISCONNECTED. marked “1” and two fingers for hand motionless in front of Crane operator spreads both block marked “2”, Regular hand giving the motion signal. hands apart – palms up. signals follow. (Hoist slowly shown as example.) TABLE 2 HAND SIGNALS FOR BOOM-TYPE CRANES

393 2017 MR 22 – December 15, 2017 TABLE 1 STANDARD HAND SIGNALS FOR CONTROLLING OVERHEAD AND GANTRY CRANE

HOIST. LOWER. USE MAIN HOIST. With forearm vertical, With arm extended downward, Tap fist on head; then use forefinger pointing up, move forefinger pointing down, move regular signals. hand in small horizontal circle. hand in small horizontal circles.

USE WHIPLINE. (Auxiliary Hoist). RAISE BOOM. LOWER BOOM. Tap elbow with one hand; then Arm Extended, fingers closed, Arm extended, fingers closed, use regular signals. thumb pointing upward. thumb pointing downward.

7 MOVE SLOWLY. RAISE THE BOOM AND LOWER THE BOOM AND Use one hand to give any LOWER THE LOAD. RAISE THE LOAD. motion signal and place other With arm extended, thumb With arm extended, thumb hand motionless in front of hand pointing up, flex fingers in and pointing down, flex fingers in giving the motion signal. (Hoist out as long as load movement is and out as long as load slowly shown as example.) desired. movement is desired.

394 2017 MR 22 – December 15, 2017 TABLE 1 STANDARD HAND SIGNALS FOR CONTROLLING OVERHEAD AND GANTRY CRANE

SWING. EMERGENCY STOP. STOP. Arm extended, palm down, Arm extended, point with finger Arm Extended, palm down, in direction of swing of boom. move hand rapidly right and hold position rigidly. left.

TRAVEL. TRAVEL.(Both Tracks) Arm extended forward, hand DOG EVERYTHING. Use both fists in front of body, open and slightly raised, make Clasp hand in front of body. making a circular motion about pushing motion in direction of each other, indicating direction travel. of travel, forward or backward. (For crawler cranes only.)

Extracted from American National Standard, Safety Code for Crawler, Locomotive and Truck Cranes, B 30.5-1968 with the permission of the publisher, The American Society of Mechanical Engineers, TRAVEL. (One Track.) United Engineering Center, Lock the track on side indicated 345 East 47th Street, New York, N.Y. 10017. by raised fist. Travel opposite track in direction indicated by circular motion of other fist, rotated vertically in front of body. (For crawler cranes only.) R 408.16333 Vessels, bin, and cooker entry. Rule 6333.(1) A lifeline and safety harness or safety belt shall be provided and used by an employee entering a vessel, tank, digester, bin, or cooker without an access door at ground or floor level, as prescribed in General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302. An 395 2017 MR 22 – December 15, 2017 employee shall be stationed outside with a self-contained respirator in a position to handle the lifeline and summon assistance. (2) An employer shall ensure that the The air inside the vessel, tank, or bin is shall be tested prior to entry. Atmospheres containing toxic gas or vapor, or which are deficient in oxygen must shall be purged and fresh air forced inside while the tank or vessel is occupied, or a self-contained or a constant-flow type supplied air respirator shall be worn. An employee shall not enter a vessel or tank containing an explosive atmosphere (3) An employer shall ensure that controls Controls to equipment supplying or operating a closed vessel, tank, digester, bin, or cooker are shall be locked out or blanked before entry by an employee. (4) An employer shall ensure that valves Valves to supply pipes for a closed vessel, tank, digester, bin, or cooker are shall be closed and locked out or blanked before entry by an employee. (5) Tanks shall be free of acid and shall be washed out with water, and fresh air shall be blown into them, before allowing an employee to enter. An employer shall provide an An employee entering the tanks shall be provided with a supplied air respirator, lifebelt, and attached lifeline, lifeline by the employer, at no expense to the employee. (6) Any lines or sewers shall be blanked off to protect workers from air contaminants. (7) When cleaning, inspection, or other work requires that employees must enter the cooker, 1 employee shall be stationed outside in a position to observe and assist in case of emergency. (8) All intake valves to a tank shall be blanked off or disconnected.

R 408.16335 Skip hoists. Rule 6335. An employer shall ensure that a A skip hoist, unless completely enclosed, is shall be equipped with all of the following: (a) A warning device to announce movement. (b) An interlocking gate across the bucket loading opening. (c) A standard barrier across any open side.

R 408.16338 Blue flag warning. Rule 6338. (1) An employer shall ensure that a A locomotive or locomotive crane uses shall use a blue flag, blue light or derailer when either of the following occur: (a) An employee may be endangered by railcars being pushed into an area in which they are working. (b) Loading or unloading railcars, oiling or servicing a railcar, locomotive or locomotive crane. (2) When it is not possible to place a blue flag or blue light at a switch, a blue flag or blue light must it shall be placed at least 50 feet from the end of the last car at both ends of the car or cars. At stub-end tracks a blue flag or blue light is necessary only at the open end. (3) A blue flag and blue light shall be marked with the name of the department placing it.

(4) A blue flag or blue light shall not be removed except by the person who places it, except if an employee does not remove his or her blue flag or blue light and cannot be located, his or her supervisor after making a thorough check of the track area in question, in company with an operating man or woman, may remove the blue flag or blue light. (5) Where 2 or more groups are working in the same location, a responsible employee or supervisor from each group shall each place a blue flag or blue light as specified in subrules (1) and (2) of this rule.

R 408.16343. Flumes, runways and jack ladders. Rule 6343. (1) A flume or water runway used to transport logs shall have a guardrail system standard barrier along the exposed sides. The height of the sides of a flume or runway extending above ground, floor, or platform level may be counted as part of the 42 inches as prescribed for a guardrail system standard barrier in R 408.10231 of General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” Standard Part 2 “Floor and Wall Openings, Stairways and Skylights,” as referenced in R 408.16302. (2) An inclined walkway along an inclined portion of a jack ladder and the inclined portion of a runway to the jack ladder shall have cleats or a slip-resistant surface that complies with General Industry Safety and Health 396 2017 MR 22 – December 15, 2017 Standard Part 2 “Walking-Working Surfaces.” and the The walkway shall be equipped with a stair rail railing on both sides as prescribed in R 408.10221 of the General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces.” Standard Part 2 “Floor and Wall Openings, Stairways and Skylights,” as referenced in R 408.16302. (3) For a runway to the jack ladder, the runway from the pond or unloading dock to the table shall be protected with standard handrails and toeboards. (4) On a runway to the jack ladder, an employer shall provide protective equipment for persons working over water.

R 408.16345. Saws. Rule 6345. (1) A guard shall be provided in front of a slasher saw to protect an employee from thrown pieces. (2) An employee shall not mount a slasher saw table unless the machine is stopped and locked out as prescribed in R 408.16323(4). (3) The exposed portion of a slasher saw blade below the table shall be enclosed. (4) A saw and other equipment more commonly found in a sawmill shall be guarded and used as prescribed in General Industry Safety and Health Standard Part Standard, Part 52 “Sawmills,” as referenced in R 408.16302.

R 408.16346. Barkers. Rule 6346. (1) An employee shall not hold or have physical contact with the pulpwood during the barking operation. (2) An employer shall provide barrier Barrier guards or enclosures shall be provided to protect an employee in the area from flying particles from the barker. (3) Two or more continuous barking drums installed side by side shall be provided with a walkway between each set with a guardrail system standard barrier as prescribed in R 408.10231 of General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” Standard Part 2 “Floor and Wall Openings, Stairways and Skylights,” as referenced in R 408.16302. (4) When a platform or floor allows access to the sides of a drum barker, a guardrail system standard barrier shall be installed as prescribed in R 408.10231 of General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” Standard Part 2 “Floor and Wall Openings, Stairways and Skylights,” as referenced in R 408.16302. (5) In-running nip points exposed to contact of trunnion rollers on a drum barker shall be guarded. (6) An intermittent barking drum shall be equipped with a device that locks the drum while being loaded or unloaded. (7) The loading and unloading ends of a hydraulic barker shall be equipped with baffles. The operator shall be protected by a barrier of 1/2 inch plexiglas or material of equivalent strength. A high pressure hose to a hydraulic barker shall be secured at the hose connection ends to prevent whipping if a connection fails.

R 408.16347 Chippers. Rule 6347. (1) An employer shall ensure that an An employee feeding a chipper does shall not have a work station in direct line with the chipper hopper. (2) The in-feed conveyor shall be guarded for its entire length by an enclosure or guardrail system standard barrier as prescribed in R 408.10231 and R 408.10233 of General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” Standard Part 2 “Floor and Wall Openings, Stairways and Skylights,” as referenced in R 408.16302. (3) The chipper hopper shall be enclosed not less than 40 inches from the blades to the opening and be baffled to prevent wood from being thrown from the hopper. (4) An employee feeding a chipper within 42 inches of the hopper shall wear a safety belt and line designed to prevent falling into the hopper. (5) Where jam-ups cannot be cleared, the in-feed equipment shall be stopped and locked out. The employee clearing the jam shall wear a safety belt and line which will prevent contact with the blades before additional

397 2017 MR 22 – December 15, 2017 clearing is done. If it is necessary to remove or loosen a blade hood, the power must shall be shut off and locked out. (6) Chipper knives shall be transported on a carrier. (7) Hearing protection equipment shall be worn by the operator and others in the immediate area if there is any possibility that the noise level may be harmful and shall be in compliance with Occupational Health Standard Part 380 “Occupational Noise Exposure,” Exposure in General Industry,” as referenced in R 408.16302.

R 408.16350 Bleaching. Rule 6350.(1) An employer shall ensure that the The bleach-mixing rooms in which the bleach powder is mixed is shall be provided with adequate exhaust ventilation, located at the floor level, as prescribed in ANSI Standard Z9.1 “Open Surface Tanks-Ventilation and And Operations,” 1951 edition, as adopted in R 408.16302 (2) Chlorine gas shall be carried away from the work place and breathing area by an exhaust system. The gas shall be rendered neutral or harmless before being discharged into the atmosphere as prescribed in ANSI Standard Z9.2 “Fundamentals Governing the The Design and Operation of Local Exhaust Ventilation Systems,” 1960 edition, as adopted in R 408.16302. (3) For emergency and rescue operations, the employer must provide employees with self-contained breathing apparatuses or supplied-air respirators and ensure that employees use these respirators as prescribed in Occupational Health Standard Part 451 “Respiratory Protection,” as referenced in R 408.16302.

R 408.16351 Acid rooms, acid towers, and acid tanks. Rule 6351. (1) An employer shall ensure that the employee is provided with eye protection, a supplied air respirator, and a personal fall protection system that meets the requirements of General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302, during inspection, repairs or maintenance of acid towers. The line shall be extended to an attendant stationed outside the tower opening. During inspection, repairs, or maintenance of acid towers, the employees shall be provided with eye protection, a supplied air respirator, a safety belt, and an attached lifeline. The line shall be extended to an attendant stationed outside the tower opening. Personal protective equipment as prescribed in General Industry Safety Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302, shall be worn. (2) Walkways, stairs, and other equipment in acid rooms, acid towers, and acid tanks shall be inspected monthly for corrosion and replaced or repaired where any part shows a defect affecting employee safety. (3) Where hoops are used on acid tanks, the hoops must they shall be made of rods rather than flat strip stock and shall be inspected and maintained as prescribed in subrule (2) of this rule. (4) Pressure tanks-accumulators shall be inspected semiannually as prescribed in the ASME Boiler and And Pressure Vessel Code, Section VIII, “Unfired Pressure Vessels,” 1989 with addenda, as adopted in R 408.16302. (5) An employer shall ensure that when When lead burning is performed within tanks, fresh air is shall be forced into the tanks so that fresh air will reach the face of the employee first and the direction of the current will never be from the source of the fumes toward the face of the employees. Supplied air respirators, such as constant-flow type, (constant-flow type) shall be provided as required in Occupational Health Standard Part 451 “Respiratory Protection,” as referenced in R 408.16302.

R 408.16353 Sulfur burning and drying. Rule 6353.(1) A sulfur burning or drying house shall be safely and adequately provided with an exhaust system as prescribed by ANSI Standard Z9.2 “Fundamentals Governing the Design and Operation of Local Exhaust Ventilation Systems,” 1960 edition, as adopted in R 408.16302, to reduce the chance of dust explosion hazards and fires. (2) Pipes, beams, and other overhead objects shall be cleaned off not less than once a month to remove dust accumulations. (3) Sulfur storage bins shall be kept free of sulfur dust accumulation, in accordance with ANSI Standard Z9.2 “Fundamentals Governing the Design and Operation of Local Exhaust Ventilation Systems,” 1960 edition, as adopted in R 408.16302.

398 2017 MR 22 – December 15, 2017 (4) Exhaust ventilation shall be provided where niter cake is fed into a rotary furnace and shall be so designed and maintained as to keep the concentration of hydrogen sulfide gas below the parts per million listed in Occupational Health Standard Part 301 “Air Contaminants,” Contaminants for General Industry,” as referenced in R 408.16302. (5) Non-sparking tools and equipment shall be used in handling dry sulfur. Smoking shall be prohibited and “No Smoking” signs shall be posted. (6) Sulfur melting equipment shall not be located in the burner room. (7) Explosion-proof electric equipment shall be used where dry sulfur burning is done. (8) Supplied-air respirators shall be strategically located for emergency and rescue use. (9) Gas masks shall be available. These masks shall furnish adequate protection against sulfurous acid and chlorine gases, and shall be inspected and repaired in accordance with Occupational Health Standard Part 451 “Respiratory Protection,” as referenced in R 408.16302. (10) Where as the processes of the sulfate and soda operations are similar to those of the sulfite processes, subrules (8) and (9) of this rule apply.

R 408.16354 Digesters and blow pits, general. Rule 6354. (1) An employer shall ensure that a A means of egress is shall be provided at each end of the room at every floor level of a digester building. (2) An employer shall ensure that a A batch type digester has shall have all of the following: (a) A blowoff valve located so it can be operated from another room, remote from safety valve. (b) Blow valves on rotary digesters pinned or locked in a closed position during the cooking period. (c) Pipes, valves, and fittings classified as heavy duty between the digester and blow pit. These pipes, valves, and fittings shall be inspected at least semiannually to determine the degree of deterioration and shall be replaced when necessary. (d) Through bolts instead of cap bolts on pipe joints. (3) A side opening to a blow pit is preferred on the side of the pit instead of on the top. . If the opening is on top, the The opening shall be as small as possible when located on the top, and shall be protected by a standard barrier as prescribed in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” Standard Part 2 “Floor and Wall Openings, Stairways, and Skylights,” as referenced in R 408.16302. Access to a blow pit shall be by a ladder designed to keep the door open when the ladder is in place, or an employee is within the pit. (4) Access to a blow pit shall be by a ladder designed to keep the door open when the ladder is in place, or an employee is within the pit. (5) (4) Blow-pit hoops shall be maintained in a safe condition. (6) (5) Personal protective equipment as prescribed in R 408.16313 and General Industry Safety and Health Standard Part 33 “Personal Protective Equipment,” as referenced in R 408.16302, shall be provided and worn when repairing or removing old brick lining from a digester. (7) (6) An employer shall ensure that fresh Fresh air is shall be blown constantly into the digester while employees are inside. Supplied-air respirators shall be available if the fresh air supply fails or is inadequate. (8) (7) An inspector shall not enter a digester unless a lifeline is securely fastened to his or her body by means of a safety belt and at least 1 other experienced employee is stationed outside the digester to handle the line and to summon assistance. All ladders and lifelines shall be inspected before each use.

R 408.16356 Safety valves. Rule 6356. (1) A safety valve shall be installed between the steam regulating valve and the vessel on a separate pipe line for each pressure vessel. The safety device shall conform to paragraph U-2 in the ASME Boiler and Pressure Vessel Code, Section VIII, “Unfired Pressure Vessels,” 1989, with addenda, as referenced in R 408.16302. Also see Rule R 408.4025 of the Michigan Boiler Rules. Rules, at web-site: http://www.michigan.gov/budget/0,4538,7-157-76309_35738_5698---,00.html. (2) A safety valve shall be checked between each cook to ensure it has not become plugged or corroded to the point of being inoperative. 399 2017 MR 22 – December 15, 2017 (3) A safety valve shall be inspected not less than annually and repaired if necessary to ensure its ability to operate, and shall be set at not more than the rated capacity of the pressure vessel. (4) The vent for a safety valve shall discharge into an area that does not create a hazard for an employee.

R 408.16361 Pulpers and beaters. Rule 6361.(1) When beaters are fed from the floor above, the chute opening, if less than 42 inches (1.06 m) from the floor, shall be provided with a guardrail system that meets the requirements in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” as referenced in R 408.16302, or other equivalent enclosures. The top of a pulper vessel or beater tub less than 42 inches from the floor or platform shall have a barrier erected around the exposed edge to a height of 42 inches to guard the opening, or a beater or pulper fed from a floor above by a chute shall have the chute extend to a height of 42 inches or the opening guarded by the standard barrier as prescribed in General Industry Safety Standard Part 2 “Floor and Wall Openings, Stairways, and Skylights,” as referenced in R 408.16302. (2) All pulpers having the top or any other opening of a vessel less than 42 inches (107 cm) from the floor or work platform shall have such openings guarded by guardrail systems that meet the requirements in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” as referenced in R 408.16302, or other equivalent enclosures (3) When beaters have openings for manual feeding or with pulpers have openings for manual changings, openings shall be sufficient only to permit the entry of stock, and shall be provided with at least 2 permanently secured crossrails or other fall protection system that meet the requirements in in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” as referenced in R 408.16302, (4) (2) Beater rolls shall be provided with covers. (5) (3) The floor around a beater shall be provided with sufficient drainage to remove wastes. (6) (4) When cleaning, inspecting, or other work requires that employees enter the pulpers, they shall be equipped with safety belt and lifeline, and 1 employee shall be stationed outside at a position to observe and assist in case of emergency. (7) (5) When cleaning, inspecting, or other work requires that employees enter pulpers, all steam, water, or other control devices shall be locked or tagged out. Blank flanging and tagging of pipe lines is acceptable in place of closed and locked or tagged valves. Blank flanging of steam and water lines is acceptable in place of valve locks.

R 408.16362 Bleaching. Rule 6362. A bleaching engine, except the Bellmer type, shall have the top covered with the exception of an opening large enough to permit filling but too small to admit an employee. This opening shall be covered with a door. The opening and a platform connecting 1 engine with another shall have standard guardrails be guarded with standard barriers as prescribed that meet the requirements in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” Standard Part 2 “Floor and Wall Openings, Stairways and Skylights,” as referenced in R 408.16302.

R 408.16364 Dust. Rule 6364. (1) Measures for the control of dust shall be provided, in accordance with General Industry Safety and Health Standard Part 33 “Personal Protective Equipment” and Occupational Health Standard Part 451 “Respiratory Protection,” as referenced in R 408.16302. (2) Installation of blower and exhaust systems for dust, stock, and vapor removal or conveying, shall be provided, in accordance with NFPA 91 “Blower and Exhaust Systems for Dust, Stock, and Vapor Removal or Conveying,” 1961 edition, as adopted in R 408.16302.

R 408.16372 Dryer. Rule 6372. (1) A barrier guard or a guardrail system standard barrier, as prescribed in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” standard, Part 2. “Floor and Wall Openings, Stairways, and Skylights,” as referenced in R 408.16302, shall be installed in front of the first dryer of each section of a paper machine, if the area is accessible to an employee. 400 2017 MR 22 – December 15, 2017 (2) In starting a dryer section, steam to heat the drums shall be introduced slowly while the drums are turning. (3) A broken carrier rope shall not be removed from a dryer while the section is running at operating speed. (4) The end of a "yankee" type dryer exposed to contact shall be guarded by a barrier to prevent entry to the turning drum.

R 408.16375 Broke hole. Rule 6375. (1) A guardrail that complies with A broke hole of such dimensions that an employee could fall through shall be guarded on all sides by a standard barrier as prescribed in General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” standard, Part 2 “Floor and Wall Openings, Stairways and Skylights.” as referenced in R 408.16302, shall be provided at broke holes. (2) Where a broke hole of such dimensions that an employee could fall through is located over a pulper or pulper conveyor system which is manually fed, the employee feeding into the hole shall wear a travel restraint system that safety belt and line which will restrict the employee from falling through the hole. (3) (2) A warning device shall be used to alert an employee working below a broke hole when broke is discharged into the hole.

R 408.16377 Calenders and platers. Rule 6377. (1) A calender roll shall be cleaned on the outrunning side. An alloy steel scraper not less than 3 x 5 inches shall be used to remove deposits from the rolls. (2) Platers. A guard shall be arranged across the face of the rolls to serve as a warning that the operator's hand is approaching the danger zone. (3) An employer shall provide steps or ladders that comply with General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” as referenced in R 408.16302, and tread with nonslip surfaces at each calendar stack. (4) Handrails and hand grips complying with General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” as referenced in R 408.16302, shall be provided at each calendar stack.

R 408.16387 Cores. Rule 6387. (1) A core notcher shall be guarded pursuant to the General Industry Safety Standard Part 23 “Hydraulic Power Presses,” as referenced in R 408.16302. (2) A core cutter shall be guarded pursuant to General Industry Safety and Health Standard Part 27 “Woodworking Machinery,” as referenced in R 408.16302. (3) A set screw for securing a core collar to winding and unwinding shafts shall not protrude above the face of the collar. Sharp corners on the collar shall be beveled. (4) A core shaft weighing more than 50 pounds shall have a mechanical device such as a dolly to support all or part of the weight when removing the shaft from the set of paper and placing it in the dressing brackets on the winder.

401 2017 MR 22 – December 15, 2017

ADMINISTRATIVE RULES

DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

DIRECTOR’S OFFICE

GENERAL INDUSTRY SAFETY AND HEALTH STANDARD

Filed with the Secretary of State on

These rules become effective immediately upon filing with the Secretary of State unless adopted under section 33, 44, or 45a(6) of 1969 PA 306. Rules adopted under these sections become effective 7 days after filing with the Secretary of State.

(By authority conferred on the director of the Department of Licensing and Regulatory Affairs by sections 16 and 21 of 1974 PA 154, MCL 408.1016 and 408.1021, and Executive Reorganization Order Nos. 1996-2, 2003-18 2003-1, 2008-4, and 2011-4, MCL 408.1016, 408.1021, 445.2001, 445.2011, 445.2025, and 445.2030)

R 408.19401, R 408.19403, and R 408.19405 of the Michigan Administrative Code are amended, and R 408.19410 is added, as follows:

PART 94 TEXTILES

R 408.19401 Scope. Rule 9401. This standard applies to the design, installation, processes, operation and maintenance of textile machinery, equipment, and other plant facilities in all plants engaged in the manufacture and processing of textiles, except those processes used exclusively in the manufacture of synthetic fibers.

R 408.19403 Adoption of a federal standard. Rule 9403. (1) The federal Occupational Safety and Health Administration (OSHA) regulation 29 C.F.R. §1910.262, “Textiles,” as amended November 18, 2016, is adopted by reference in these rules. (2) A reference to §1910.264, “Laundry machinery and operations,” means General Industry Safety Standard Part 71 “Laundry and Dry Cleaning Machinery and Operations.” (3) A reference to §1910.144, “Safety color code for marking physical hazards,” means General Industry Safety Standard Part 37 “Accident Prevention Signs and Tags.” (4) A reference to §1910 Subpart D, “Walking-Working Surfaces,” means General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces.” (5) The availability information for the standards adopted in these rules is in R 408.19405 and MIOSHA standards referenced in these rules is in R 408.19410. (6) The adopted federal regulations shall have the same force and effect as a rule promulgated under the Michigan Occupational Safety and Health Act, 1974 PA 154, MCL 408.1001 to 408.1094.

R 408.19405 Adopted standards. Rule 9405. (1) The OSHA regulation 29 C.F.R. §1910.262, “Textiles,” adopted in these rules is available from the United States Department of Labor, Occupational Safety and Health Administration, website www.osha.gov, at no charge, as of the time of adoption of these rules. (2) The following standards are adopted in these rules and are available from IHS Global, 15 Inverness Way East, Englewood, Colorado, 80112, USA, telephone number: 1-800-854-7179 or via the internet at website: http://global.ihs.com at a cost as of the time of adoption of these rules, as stated in this subrule.

402 2017 MR 22 – December 15, 2017 (a) American National Safety Institute ANSI Standard Z9.2 “Fundamentals Governing the Design and Operation of Local Exhaust Ventilation Systems,” 1960 edition. Cost $32.00. (b) American Society of Mechanical Engineers ASME Boiler and Pressure Vessel Code, Section VIII, “Unfired Pressure Vessels,” 1968 edition. Cost: $514.00. (3) The standards adopted in these rules are available for inspection at the Department of Licensing and Regulatory Affairs, MIOSHA Regulatory Services Section, 530 West Allegan Street, P.O. Box 30643, Lansing, Michigan, 48909-8143. (4) The standards adopted in these rules may be obtained from the publisher or may be obtained from the Department of Licensing and Regulatory Affairs, MIOSHA Regulatory Services Section, 530 West Allegan Street, P.O. Box 30643, Lansing, Michigan, 48909-8143, at the cost charged in this rule, plus $20.00 for shipping and handling.

R 408.19410 Availability of MIOSHA referenced standards. Rule 9410. The following Michigan Occupational Safety and Health Administration (MIOSHA) standards are referenced in these rules. Up to 5 copies of these standards may be obtained at no charge from the Michigan Department of Licensing and Regulatory Affairs, MIOSHA Regulatory Services Section, 530 West Allegan Street, P.O. Box 30643, Lansing, MI, 48909-8143 or via the internet at website: www.michigan.gov/mioshastandards. For quantities greater than 5, the cost, at the time of adoption of these rules, is 4 cents per page. (a) General Industry Safety and Health Standard Part 2 “Walking-Working Surfaces,” R 408.10201 to R 408.10241. (b) General Industry Safety Standard Part 37 “Accident Prevention Signs and Tags,” R 408.13701 to R 408.13738. (c) General Industry Safety Standard Part 71 “Laundry and Dry Cleaning Machinery and Operations,” R 408.17101 to R 408.17163.

403 2017 MR 22 – December 15, 2017

CERTIFICATE OF NEED REVIEW STANDARDS

MCL 24.208 states in part:

Sec. 8. The State Office of Administrative Hearings and Rules shall publish the Michigan register at least once each month. The Michigan register shall contain all of the following:

* * *

(k) All of the items in section 7(l) after final approval by the certificate of need commission or the statewide health coordinating council under section 22215 or 22217 of the public health code, 1978 PA 368, MCL 333.22215 and 333.2217.

MCL 24.207 states in part:

Sec. 7. “Rule” means an agency regulation, statement, standard, policy, ruling, or instruction of general applicability that implements or applies law enforced or administered by the agency, or that prescribes the organization, procedure, or practice of the agency, including the amendment, suspension, or rescission of the law enforced or administered by the agency. Rule does not include any of the following:

* * *

(l) All of the following, after final approval by the certificate of need commission or the statewide health coordinating council under section 22215 or 22217 of the public health code, 1978 PA 368, MCL 333.22215 and 333.22217: (i) The designation, deletion, or revision of covered medical equipment and covered clinical services. (ii) Certificate of need review standards (iii) Data reporting requirements and criteria for determining health facility viability. (iv) Standards used by the department of community health in designating a regional certificate of need review agency. (v) The modification of the 100 licensed bed limitation for short-term nursing care programs set forth in section 22210 of the public health code, 1978 PA 368, MCL 333.22210.

404 2017 MR 22 – December 15, 2017

CERTIFICATE OF NEED REVIEW STANDARDS

CERTIFICATE OF NEED (CON) REVIEW STANDARDS SYNOPSIS FOR PUBLICATION IN THE MICHIGAN REGISTER PURSUANT TO THE ADMINISTRATIVE PROCEDURES ACT, 1969 PA 306, MCL 24.208(1)(k)

SURGICAL SERVICES Final Approval by the CON Commission 9/21/17 and Effective 11/17/17

The language changes include the following:

1. Updated the Department name throughout the document. 2. Section 4(3)(a): Added language regarding commitment letters and the use of historical surgical cases for initiation. 3. Section 11(2)(e): Added new language regarding commitment letters and the use of historical surgical cases for initiation as shown below. Less regulation will ease the process for the applicant when using its own data to initiate: • (e) SUBSECTION 11(2)(d) SHALL NOT APPLY IF THE PROPOSED PROJECT INVOLVES THE INITIATION OF A SURGICAL SERVICE AT A NEW FSOF OR A NEW ASC AT A NEW GEOGRAPHICAL SITE UTILIZING THE HISTORICAL SURGICAL CASES OF THE APPLICANT AND THE NEW SERVICE IS OWNED BY THE SAME APPLICANT. THE APPLICANT FACILITY COMMITTING SURGICAL DATA HAS COMPLETED THE DEPARTMENTAL FORM THAT CERTIFIES THE SURGICAL CASES WERE PERFORMED AT THE COMMITTING FACILITY AND THE SURGICAL CASES WILL BE TRANSFERRED TO THE PROPOSED SURGICAL FACILITY FOR NO LESS THAN 3 YEARS SUBSEQUENT TO THE INITIATION OF THE SURGICAL SERVICE PROPOSED BY THE APPLICANT. 4. Other technical edits.

Complete Standards

A complete set of the approved language can be found at http://www.michigan.gov/mdhhs/0,5885,7-339- 71551_2945_5106-25558--,00.html. A hard copy may be obtained, for a fee, by sending a written request to:

Michigan Department of Health and Human Services Policy, Planning and Legislative Services Planning and Access to Care Section P.O. Box 30195 Lansing, MI 48909 (517) 335-6708

Email address: [email protected]

405 2017 MR 22 – December 15, 2017 EMERGENCY RULES

MCL 24.248 states:

“Sec. 48. (1) If an agency finds that preservation of the public health, safety, or welfare requires promulgation of an emergency rule without following the notice and participation procedures required by sections 41 and 42 and states in the rule the agency's reasons for that finding, and the governor concurs in the finding of emergency, the agency may dispense with all or part of the procedures and file in the office of the secretary of state the copies prescribed by section 46 indorsed as an emergency rule, to 3 of which copies shall be attached the certificates prescribed by section 45 and the governor's certificate concurring in the finding of emergency. The emergency rule is effective on filing and remains in effect until a date fixed in the rule or 6 months after the date of its filing, whichever is earlier. The rule may be extended once for not more than 6 months by the filing of a governor's certificate of the need for the extension with the office of the secretary of state before expiration of the emergency rule. An emergency rule shall not be numbered and shall not be compiled in the Michigan Administrative Code, but shall be noted in the annual supplement to the code. The emergency rule shall be published in the Michigan register pursuant to section 8. (2) If the agency desires to promulgate an identical or similar rule with an effectiveness beyond the final effective date of an emergency rule, the agency shall comply with the procedures prescribed by this act for the processing of a rule which is not an emergency rule. The rule shall be published in the Michigan register and in the code.”

406 2017 MR 22 – December 15, 2017

EMERGENCY RULES

DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

BUREAU OF PROFESSIONAL LICENSING FOR A STANDING ORDER FOR DISPENSING OPIOID ANTAGONISTS EMERGENCY RULES

CERTIFICATE OF NEED FOR EXTENSION OF EMERGENCY RULES

Pursuant to Section 48(1) of 1969 PA 306, as amended, MCL 24.248(1), I hereby certify that it is necessary to extend the effectiveness of the Standing Order for Dispensing Opioid Antagonists Rules, which were filed with the Secretary of State on May 27, 2017, for an additional 6 months, therefore, “Standing Order for Dispensing Opioid Antagonists” Rules shall remain effective until May 27, 2018.

______Rick Snyder, Governor Date

407 2017 MR 22 – December 15, 2017

DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS BUREAU OF PROFESSIONAL LICENSING EMERGENCY RULES FOR A STANDING ORDER FOR DISPENSING OPIOID ANTAGONISTS Filed with the Secretary of State on These rules take effect upon filing with the Secretary of State and shall remain in effect for 6 months

(By the authority conferred on the Department of Licensing and Regulatory Affairs by section 17744e, of 1978 PA 368, being MCL 333.17744e and on the Department of Health and Human Services by sections 2221, 2226, and 2233, of 1978 PA 368, being MCL 333.2221, 333.2226 and 333.2233) FINDING OF EMERGENCY These rules are promulgated by the Department of Licensing and Regulatory Affairs (LARA) to establish emergency rules for the implementation of provisions from 2016 PA 383 (Act), effective March 28, 2017, which allows the Office of the Chief Medical Executive to issue a standing order that does not identify particular patients at the time it is issued for the purpose of a pharmacist dispensing opioid antagonists. The Act requires LARA, in consultation with the Michigan Department of Health and Human Services and local health departments, to promulgate rules regarding dispensing, training, and referral to implement the Act. Michigan has been experiencing a persistently growing opioid abuse problem over the last several years. Opioids, in the form of powerful painkillers that are highly addictive, have led to rising numbers of opioid dependence among Michigan’s citizens. Moreover, prescribed opioids have lead to an uncontrollable increase in the use of highly addictive and dangerous illegal substances, especially heroin. According to the 2015 statistics from Center for Disease Control, Michigan saw its third consecutive year of record drug overdose deaths. In 2015, 1,981 people died from drug overdoses, up 13.5% from 2014. Furthermore, over the last 17 years, deaths from drug overdoses in Michigan quadrupled, compounded by the fact that the state was ranked 10th in the nation in per capita prescribing rates of opioid pain relievers in 2012. The Act allows for the dispensing of opioid antagonists, such as Naloxone, to family members, acquaintances, and health professionals capable of assisting individuals in the throes of opioid addiction. Opioids antagonists are drugs used to bind to the opioid receptors in the body, resulting in the blocking of the body’s opiate receptors, preventing the body from having an adverse response to drugs such as heroin and other opiates. Prior to the statute becoming law, drug abusers themselves could obtain opioid antagonists to self-administer in the event of an overdose. However, for a variety of reasons, it is unrealistic to believe that an individual in the midst of an accidental opioid overdose would have the faculties to recognize the onset of an overdose and take appropriate action. Most importantly, permanent administrative rules cannot be promulgated quickly enough to stem the loss of life which is increasing on a daily basis. Time is of the essence, and 2016 PA 383 presents an opportunity to rapidly place life-saving opioid antagonists within the hands of those most readily able to stop and reverse opioid overdoses, and immediately save lives. LARA, in consultation with the Department of Health and Human Services and local health departments, finds an urgency exists to prevent continued death and to preserve the public health, safety, and welfare from the opioid overdose epidemic which requires the promulgation of emergency rules without following the notice and participation procedures required by sections 41, 42, and 48 of 1969 PA 306, as amended, being MCL 24.241, MCL 24.242, and MCL 24.248 of the Michigan Compiled Laws. Rule 1. Definitions.

As used in these rules: (1) "Code" means the public health code, 1978 PA 368, MCL 333.1101 to 333.25211. (2) “Department" means the Michigan Department of Health and Human Services. (3) “Eligible individuals” means individuals within the State of Michigan, who are seeking opioid antagonists. (4) “Standing order” means a standing order issued by the Office of the Chief Medical Executive pursuant to section 17744e of the Code, being MCL 333.17744e. 408 2017 MR 22 – December 15, 2017

Rule 2. Dispensing opioid antagonists; standing order; requirements.

(1) Upon issuance of the standing order, a pharmacy shall register with the department prior to dispensing opioid antagonists under the standing order. (2) A pharmacy dispensing an opioid antagonist pursuant to the standing order, shall submit the following information, without individual identifiers, to the department on a quarterly basis, in a manner established by the department: (a) The total number of doses of opioid antagonist dispensed under the standing order. (b)The total number of doses of opioid antagonists dispensed under any type of prescription, including the standing order. (c) The number of each type of formulation dispensed.

Rule 3. Training for the administration of opioid antagonists; requirements.

(1) Pharmacists who dispense opioid antagonists pursuant to the standing order shall obtain training in the proper use and administration of opioid antagonists and in opioid overdose response. The training programs can be obtained on-line, in person, or in writing. (2) Pharmacists who dispense opioid antagonists pursuant to the standing order shall provide educational material, approved by the Office of the Chief Medical Executive, on the administration of opioid antagonists to eligible individuals.

Rule 4. Referral to resource information.

(1) Pharmacists who dispense opioid antagonists pursuant to the standing order shall provide the eligible individual with resource information regarding referral for treatment services.

MICHIGAN DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

______Shelly Edgerton, Director Department of Licensing and Regulatory Affairs

Pursuant to Section 48(1) of 1969 PA 306, as amended, being MCL 24.248(1), I hereby concur in the finding of the Department of Licensing and Regulatory Affairs that the circumstances creating an emergency have occurred and the promulgation of the above rules is required for the preservation of the public health, safety, and welfare.

______Rick Snyder, Governor Date

409 2017 MR 22 – December 15, 2017

EMERGENCY RULES

DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

BUREAU OF MEDICAL MARIHUANA REGULATION

MEDICAL MARIHUANA FACILITIES LICENSING ACT

EMERGENCY RULES

Filed with the Secretary of State on These rules take effect upon filing with the Secretary of State and shall remain in effect for 6 months.

(By authority conferred on the department of licensing and regulatory affairs by section 206 of 2016 PA 281, MCL 333.27206, enacting section 2 of Act 281 of 2016, by section 3 of 2016 PA 282, MCL 333.27903, and by section 6 of MCL 333.26426, 2008, Initiated Law 1.)

FINDING OF EMERGENCY

These rules are promulgated by the department of Licensing and Regulatory Affairs (department) to establish emergency rules for the purpose of implementing the Medical Marihuana Facilities Licensing Act (act), 2016 PA 281, MCL 333.27101 et seq., which took effect December 20, 2016. The act provides for a state regulatory structure to license and regulate medical marihuana growers, processors, provisioning centers, secure transporters, and safety compliance facilities that interacts with the statewide monitoring system for commercial marihuana transactions; establishes a medical marihuana licensing board (Board) created within the department and appointed by the governor; and prescribes civil fines and sanctions and provides remedies.

The act includes an enacting section specifying that the legislature found it necessary for the promulgation of emergency rules to preserve the public health, safety, or welfare for access to safe sources of marihuana for medical use and the immediate need for growers, processors, secure transporters, provisioning centers, and safety compliance facilities to operate under clear requirements. In addition, section 206 of the act requires the department, in consultation with the Board, to promulgate administrative rules and emergency rules as necessary to implement, administer, and enforce the act. Furthermore, section 206 specifies that the rules shall ensure the safety, security, and integrity of the operation of marihuana facilities.

To date, no administrative rules have been promulgated under the authority granted to the department, in consultation with the Board that has been created within the department. Specifically, there are no current administrative rules to ensure the safety, security, and integrity of the operation of marihuana facilities. Pursuant to section 401 of the act, beginning December 15, 2017, persons may apply to the Board created within the department for state operating licenses in the categories of class A, B, or C grower, processor, provisioning center, secure transporter, and safety compliance facility. The Board is required to review all applications for licensure, issue or deny issuance of a license, and inform each applicant of the Board’s decision. If issuance is denied, the Board is required, upon request, to provide a public investigative hearing. In addition, any party aggrieved by an action of the Board suspending, revoking, restricting, or refusing to renew a license, or imposing a fine, shall be given a hearing before the Board upon request. There are no administrative rules currently in place that will provide for the implementation of these requirements as specified in the act.

In addition, the act requires the promulgation of administrative rules to prescribe the use of the statewide monitoring system to track all marihuana transfers, as provided in the Marihuana Tracking Act, 2016 PA 282, MCL 333.27901 et seq. To date, these administrative rules have not been promulgated. The statewide monitoring system is used to 410 2017 MR 22 – December 15, 2017 track and inventory marihuana and is a key component to preserving the integrity of the operation of marihuana facilities, monitoring the industry, investigating, and supporting compliance with the act to promote the public health, safety, or welfare.

The lack of administrative rules to implement the act will have a detrimental effect on the necessity for access to a safe source of marihuana for medical use and the immediate need for growers, processors, secure transporters, provision centers, and safety compliance facilities to operate under clear requirements. Furthermore, the use of the statewide monitoring system to track all marihuana transfers is integral to the safety and compliance requirements of the act. The emergency administrative rules are needed to enable the department, through its Bureau of Medical Marihuana Regulation, to implement the act to provide a safe environment for the state operating licensees and Michigan communities, as well as access to medical marihuana that has been tested for safety for sale to registered qualifying patients and registered primary caregivers.

If the complete process specified in the Administrative Procedures Act of 1969, 1969 PA 306, MCL 24.201 et seq. for the promulgation of rules were followed, the process would not be completed in time for the department to comply with the act’s requirements to process applications according to the timelines specified in the act, provide administrative hearing procedures, or implement the tracking requirements. Furthermore, the administrative rules would not be promulgated prior to the issuance of state operating licenses, thus causing uncertainty and financial hardship to individuals or businesses that plan to apply for commercial state operating licenses.

The department, in consultation with the Board, therefore, finds that the preservation of the public health, safety, and welfare requires the promulgation of emergency rules as provided in section 48 without following the notice and participation procedure required by sections 41 and 42 of 1969 PA 306, as amended, being MCL 24.241, and MCL 24.242 of the Michigan Compiled Laws.

Rule 1. Definitions. (1) “Act” means the medical marihuana facilities licensing act, 2016 PA 281, MCL 333.27101 to 333.27801. (2) “Batch” means all the plants of the same variety of medical marihuana that have been grown, harvested, and processed together and exposed to substantially similar conditions throughout cultivation and processing. (3) “Building” means a combination of materials forming a structure affording a facility or shelter for use or occupancy by individuals or property. Building includes a part or parts of the building and all equipment in the building. A building shall not be construed to mean a building incidental to the use for agricultural purposes of the land on which the building is located. (4) “Bureau” means the department of licensing and regulatory affairs’ bureau of medical marihuana regulation. (5) “Bureau of fire safety” or “BFS” means the department of licensing and regulatory affairs’ bureau of fire safety. (6) “Department” means the department of licensing and regulatory affairs. (7) “Director” means the director of the department of licensing and regulatory affairs or his or her designee. (8) "Employee" means a person performing work or service for compensation. (9) “Harvest batch” means marihuana that has been harvested. (10) "Immature plant” means a nonflowering marihuana plant that is no taller than 8 inches and no wider than 8 inches produced from a cutting, clipping, tissue culture, or seedling that is in a growing/cultivating medium or in a growing/cultivating container that is no larger than 2 inches wide and no more than 2 inches tall that is sealed on the sides and bottom. (11) “Limited access area” means a building, room, or other contiguous area of a marihuana facility where marihuana is grown, cultivated, stored, weighed, packaged, sold, or processed for sale, under control of the licensee. (12) “Marihuana facility” means a location at which a licensee is licensed to operate under the act and these rules. (13) “Marihuana product” means marihuana or marihuana-infused product, or both, as those terms are defined in the act unless otherwise provided for in these rules. (14) “Marihuana tracking act” means the marihuana tracking act, 2016 PA 282, MCL 333.27901 to 333.27904. (15) “Michigan medical marihuana act” means the Michigan medical marihuana act, 2008 IL 1, MCL 333.26421 to 333.26430.

411 2017 MR 22 – December 15, 2017 (16) “Package tag” means an RFID tag supplied through the statewide monitoring system for the purpose of identifying a package containing marihuana product. (17) “Plant tag” means an RFID tag supplied through the statewide monitoring system for the purpose of identifying an individual marihuana plant. (18) “Proposed marihuana facility” means a location at which an applicant plans to operate under the act and these rules if the applicant is issued a state operating license. (19) “Restricted access area” means a designated and secure area at a marihuana facility where marihuana products are sold, possessed for sale, and displayed for sale. (20) “Same location” means separate state operating licenses that are issued to multiple marihuana facilities that are authorized to operate at a single property but with separate business addresses. (21) “Stacked license” means more than 1 state operating license issued to a single licensee to operate as a grower of class C-1,500 marihuana plants as specified in each license at a marihuana facility. (22) “Tag” or “RFID tag” means the unique identification number or Radio Frequency Identification (RFID) issued to a licensee by the department for tracking, identifying and verifying marihuana plants, marihuana products, and packages in the statewide monitoring system.

Rule 2. Terms; meanings. Terms defined in the act have the same meanings when used in these rules unless otherwise indicated.

Rule 3. Adoption by reference. (1) National fire protection association (NFPA) standard 1, 2018 edition, entitled “Fire Code” is adopted by reference as part of these rules. Copies of the adopted provisions are available for inspection and distribution from the National Fire Protection Association, 1 Batterymarch Park, P.O. Box 9101, Quincy, Massachusetts, 02169, telephone number 1-800-344-3555, for the price of $99.50. (2) Cannabis Inflorescence: Standards of Identity, Analysis, and Quality Control monograph published by the American Herbal Pharmacopoeia. A copy of that publication may be obtained from the American Herbal Pharmacopoeia, P.O. Box 66809, Scotts Valley, California 95067, or at the Internet address http://www.herbal- ahp.org/, for the price of $44.95. (3) Safe Quality Food (SQF), 7.2 edition available at http://www.sqfi.com/wp-content/uploads/SQF-Code_Ed-7.2- July.pdf. (4) The International Organization for Standardization (ISO), ISO 22000 / ISO/TS 22002-1 - food safety bundle, available for purchase at: https://webstore.ansi.org/RecordDetail.aspx?sku=ISO+22000+%2f+ISO%2fTS+22002- 1+-+Food+Safety+Bundle, for the price of $275.00. (5) International Organization for Standardization (ISO), ISO/IEC 17025:2005, general requirements for the competence of testing and calibration laboratories available at: https://webstore.ansi.org/RecordDetail.aspx?sku=ISO%2fIEC+17025%3a2005, for the price of $162.00.

Rule 4. Application procedure; requirements. (1) A person may apply for a state operating license on the form created by the department accompanied by the application fee as prescribed in these rules. Each question on the application must be answered in its entirety and all information requested and required by the act and these rules must be submitted in the application. Failure to comply with these rules and the application requirements in the act is grounds for denial of the application. (2) A person may submit a partial application under Rule 5 on the condition that it is to prequalify to complete the remaining application requirements. This is a pending status until all application requirements in Rule 6 are completed. The department shall not issue a license at this stage of the application. (3) The department may delay an application while additional information is requested including, but not limited to, requests for additional disclosures and documentation to be furnished to the department. (4) For purposes of this rule and Rules 5 and 6 the term “applicant” includes the officers, directors, and managerial employees of the applicant and any persons who hold any direct or indirect ownership interest in the applicant.

Rule 5. Application requirements; financial and criminal background.

412 2017 MR 22 – December 15, 2017 (1) The first part of the application is a financial background and full criminal history background check of the applicant. For purposes of this rule an applicant includes the officers, directors, and managerial employees of the applicant and any persons who hold any direct or indirect ownership interest in the applicant. (2) An applicant shall disclose the identity of every person having any ownership interest in the applicant with respect to which the license is sought including, but not limited to, date of birth, government issued identification, or any other documents required by the act. (3) An applicant and any persons who have a direct or indirect interest in the applicant, as well as any officers, directors, and managerial employees of the applicant shall disclose all the financial information required in the act and these rules in a format created by the department including, but not limited to, the following: (a) Financial statements, pecuniary interest, any deposit of value of the applicant or made directly or indirectly to the applicant, or both, and financial account information including but not limited to, funds, savings, checking, or other accounts including any or all financial institutions information, such as names, account type, amounts of the foregoing, and a list of all loans, amounts, securities, or lender information. (b) Property ownership information, deeds, leases, rent, real estate trusts, purchase agreements or institutional investors. (c) Tax information, W-2 and 1099 forms, and any other information required by the department. (d) For in-state and out-state applicants, the applicant’s business organizational documents filed with this state, local county, or foreign entity, if applicable, including proof of registration to do business in this state and certificate of good standing from this state or foreign entity, if applicable. (e) Disclosure by the applicant of the identity of any other person who meets either of the following: (i) Controls, directly or indirectly, the applicant. (ii) Is controlled, directly or indirectly, by the applicant or by a person who controls, directly or indirectly, the applicant. (f) Written consent by the applicant to a financial background investigation as authorized under the act and these rules. (g) Disclosure by the applicant of any true parties of interest as required in section 404 of the act. (h) Disclosure by the applicant of the stockholders or other persons having a 1% or greater beneficial interest in the proposed marihuana facility as required in section 303 of the act. (i) The sources and total amount of the applicant's capitalization to operate and maintain the proposed marihuana facility in compliance with Rule 11. (j) A CPA-attested financial statement including foreign attested CPA statement, or its equivalent, if applicable, on capitalization pursuant to Rule 11. (k) Information on the financial ability of the applicant to purchase and maintain adequate liability and casualty insurance in compliance with Rule 10. (l) Any other documents, disclosures, or attestations created or requested by the department that are not inconsistent with the act or these rules. (4) An applicant and each person having any ownership interest in the proposed marihuana facility and each person who is an officer, director, or managerial employee of the applicant shall disclose criminal history background information and regulatory compliance as provided under the act and these rules in a format created by the department, including, but not limited to, all the following: (a) Attestation, in writing, that the person consents to inspections, examinations, searches, and seizures that are permitted under the act and these rules. (b) Written consent to a criminal history check, submission of a passport quality photograph to the department and 1 set of fingerprints to the department of state police in accordance with section 402 of the act and these rules for the applicant, each person having any ownership interest in the proposed marihuana facility, and each person who is an officer, director, or managerial employee of the applicant. (c) Submission of a handwriting exemplar, fingerprints, photographs, and information authorized by the act and by these rules. (d) Attestation affirming a continuing duty to provide information requested by the department and to cooperate in any investigation, inquiry, or hearing.

413 2017 MR 22 – December 15, 2017 (e) Attestation acknowledging that sanctions may be imposed for violations on a licensee while licensed or after the license has expired as provided in the act and these rules. (f) Disclosure of any noncompliance with any regulatory requirements in this state or any other jurisdiction. (g) Disclosure of an application or issuance of any commercial license or certificate issued in this state or any other jurisdiction and the requirements under section 401(1)(e) of the act. (h) Any other documents, disclosures, or attestations created or requested by the department that are not inconsistent with the act or these rules. (5) An applicant shall submit in the application any information requested and required by the act and these rules.

Rule 6. Application requirements; complete application. (1) A complete application for a state operating license must include all the information in Rule 5 and all the following: (a) A description of the type of marihuana facility, anticipated or actual number of employees, projected or actual gross receipts, a business plan, proposed marihuana facility location, and security plan as required under the act and these rules. (b) A copy of the proposed marihuana facility plan under Rule 8. (c) An applicant shall pass the pre-licensure inspection as provided in Rule 9. (d) An applicant shall submit confirmation of compliance with the municipal ordinance as required in section 205 of the act and these rules. For purposes of these rules, confirmation of compliance must be on an attestation form prepared by the department that contains all of the following information: (i) Written affirmation that the municipality has adopted an ordinance under section 205 of the act, including, if applicable, the disclosure of any limitations on the number of each type of marihuana facility. (ii) Description of any zoning regulations that apply to the proposed marihuana facility within the municipality. (iii) The signature of the clerk of the municipality or his or her designee attesting that the information stated in the document is correct. (e) The disclosure of the true party of interest as required in section 404 of the act and these rules. (f) The disclosure of the beneficial interest as required in section 303(1)(g) of the act. (g) Additional information and documents requested by the department not inconsistent with the act and these rules. (h) Any other documents, disclosures, or attestations created or requested by the department that are not inconsistent with the act and these rules.

Rule 7. Application; fees; assessment. (1) An application for a state operating license must be accompanied by the nonrefundable application fee of $6,000.00 upon initial application under Rule 5. (2) If the costs of the investigation and processing the application exceed the application fee, the applicant shall pay the additional amount. (3) The regulatory assessment must be paid on or before the date a licensee begins operating and annually thereafter pursuant to section 603 of the act and these rules. (4) A license will not be issued until a complete application is submitted, the fees required under these rules are paid, and it is determined that the applicant is qualified to receive a license under the act and these rules.

Rule 8. Marihuana facility plan. (1) To ensure the safety, security, and integrity of marihuana facility operations, an applicant shall submit a marihuana facility plan for the proposed marihuana facility as required in Rule 6 and thereafter upon request by the department. Upon the request of the department an applicant or licensee may be required to submit a revised marihuana facility plan. (2) The marihuana facility plan shall include, but not be limited to, the following: (a) The type of proposed marihuana facility, location, description of the municipality, and any of the following if applicable: (i) Operation at the same location under Rule 24. (ii) Proof of common ownership interest under Rule 24.

414 2017 MR 22 – December 15, 2017 (iii) Stacked license under Rule 22. (iv) Temporary operation under Rule 19. (b) Diagram of the marihuana facility including, but not limited to, its size and dimensions; specifications; physical address; location of common entryways, doorways, or passageways; means of public entry or exit; limited-access areas within the marihuana facility; and indication of the distinct areas or structures at a same location as provided for in Rule 24. (c) Floor plan and layout, including dimensions, maximum storage capabilities, number of rooms, dividing structures, fire walls, and entrances and exits. (d) Means of egress, including, but not limited to, delivery and transfer points. (e) Construction details for structures and fire-rated construction for required walls. (f) Building structure information, including but not limited to, new, pre-existing, free-standing, or fixed. Building type information, including but not limited to, commercial, warehouse, industrial, retail, converted property, house, building, mercantile building, pole barn, greenhouse, laboratory, or center. (g) Zoning classification and zoning information. (h) If the proposed marihuana facility is in a location that contains multiple tenants and any applicable occupancy restrictions. (i) A proposed security plan that demonstrates the proposed marihuana facility must meet the security requirements under Rule 27. (j) Any other information required by the department as long as it is not inconsistent with the act and these rules. (3) Any changes or modifications to the marihuana facility plan under this rule must be reported to the department and may require preapproval by the department. (4) The department may provide a copy of the marihuana facility plan to the state fire official, local fire department, and local law enforcement for use in pre-incident review and planning. (5) The department may reinspect the marihuana facility to verify the plan at any time and may require that the plan is resubmitted upon renewal.

Rule 9. Pre-licensure investigation and proposed marihuana facility inspection. (1) An applicant for a state operating license shall submit to a pre-licensure physical inspection to ensure the safety, security, and integrity of the operation of a proposed marihuana facility. (2) The department shall establish an inspection process to confirm that the applicants and proposed marihuana facilities meet the requirements of the act and these rules. (3) The department shall investigate applicants in accordance with the act and these rules. (4) The department, through its investigators, agents, auditors, or the state police, shall conduct inspections and examinations of applicants and proposed marihuana facilities in accordance with the act and these rules. (5) An applicant shall submit proof to the department of the following: (a) A certificate of use and occupancy as required pursuant to section 13 of 1972 PA 230, MCL 125.1513 and these rules. (b) A final inspection completed by the department notwithstanding any local ordinance or building permit inspection. (c) Proof of a fire safety inspection as provided for in Rule 26.

Rule 10. Proof of financial responsibility; insurance. (1) Before a license is issued or renewed, the licensee or renewal applicant shall file a proof of financial responsibility for liability for bodily injury on the form prescribed in section 408 of the act for an amount not less than $100,000.00. If the proof under this subrule is a bond, the bond must be in a format acceptable to the department. (2) A renewal applicant or licensee shall carry premise liability and casualty insurance for an amount not less than $100,000.00. An applicant shall provide proof of premises liability insurance to the department no later than 60 days after a state operating license is issued or renewed.

415 2017 MR 22 – December 15, 2017 (3) A secure transporter shall show proof of auto insurance, vehicle registration, and registration as a commercial motor vehicle as applicable for any transporting vehicles used to transport marihuana product as required by the act and these rules.

Rule 11. Capitalization requirements. (1) An applicant shall disclose the sources and total amount of capitalization to operate and maintain a proposed marihuana facility. (2) The total amounts of capitalization based on the type of marihuana facility specified in the application for a state operating license are as follows: (a) Grower: Class A - $150,000.00. (b) Grower: Class B - $300,000.00. (c) Grower: Class C - $500,000.00. (d) Processor: $300,000.00. (e) Provisioning Center: $300,000.00. (f) Secure Transporter: $200,000.00. (g) Safety Compliance Facility: $200,000.00. (3) An applicant shall provide proof to the department of the capitalization amounts in subrule (2) of this rule from sources as follows: (a) Not less than 25% is in liquid assets to cover the initial expenses of operating and maintaining the proposed marihuana facility as specified in the application. For purposes of this subdivision liquid assets include assets easily convertible to cash, including, but not limited to, cash, CDs, 401(k), stocks and bonds, and marihuana inventory that meet the all the following conditions: (i) The marihuana inventory is possessed by an applicant who is a registered qualifying patient or registered primary caregiver or by an applicant who applies for a state operating license and possesses marihuana inventory in compliance with the Michigan medical marihuana act. (ii) No more than 15 ounces of usable marihuana or 72 marihuana plants may be utilized as marihuana inventory in this subdivision or utilized towards the capitalization requirement under this subrule. (b) Proof of the remaining capitalization to cover the initial expenses of operating and maintaining the proposed marihuana facility may include but is not limited to additional liquid assets as described in subdivision (a) of this subrule or equity in real property, supplies, equipment, fixtures or any other nonliquid asset. (4) The applicant shall provide proof that there is no lien or encumbrance on the asset provided as a source of capitalization. (5) The capitalization amounts and sources must be validated by CPA-attested financial statements. The applicant shall disclose any of the capitalization sources that are foreign and a foreign CPA or its equivalent shall attest to the validation and a domestic CPA shall attest that foreign validation.

Rule 12. Denial of the issuance of a license; additional reasons. (1) If an applicant fails to comply with the act or these rules, a license may be denied as provided under the act and these rules. (2) In addition to the reasons for denial in the act, a license may be denied as provided in the act and these rules for the following reasons: (a) The applicant’s marihuana facility plan does not fully comply with the act or these rules. (b) The applicant’s proposed marihuana facility or marihuana facility is substantially different from the marihuana facility plan pursuant to Rule 8 and these rules. (c) The department is unable to access the proposed marihuana facility for pre-licensure physical inspection or the applicant denied the department access to the proposed marihuana facility. (d) The applicant made a material misrepresentation on the application. (e) The applicant failed to correct any deficiencies within the application in accordance with section 403 of the act and these rules. (f) The applicant has failed to satisfy the confirmation of compliance by a municipality in accordance with section 205 of the act and these rules.

416 2017 MR 22 – December 15, 2017 (g) The applicant is operating a proposed marihuana facility or a marihuana facility without a license after December 15, 2017, except for as provided in Rule 19, that would otherwise require an application for a state operating license as required under the act and these rules.

Rule 13. Renewal of license. (1) A license is issued for a 1-year period and is renewable annually. A licensee may apply to renew a license on a form established by the department. (2) Failure to comply with any of the provisions in the act and these rules may result in the nonrenewal of a license. (3) The licensee shall meet the requirements of the act and any other renewal requirements set forth in these rules or laws to be promulgated or enacted.

Rule 14. Notification and reporting. (1) Applicants and licensees have a continuing duty to provide the department with up-to-date contact information and shall notify the department in writing of any changes to its mailing address, phone numbers, electronic mail address, and other contact information it provides the department. (2) Applicants and licensees shall report any material and nonmaterial changes to the department. (3) Applicants and licensees shall report nonmaterial changes to the department within 7 business days. (4) Applicants and licensees shall report material changes to the department prior to the change, within 1 business day, and may need prior authorization by the department. Material changes, include, but are not limited to, the following: (a) Change in owners, officers, members, or managers. (b) Change of location. A change of location of a marihuana facility may trigger a new license and new inspection. (c) The addition or removal of named people. (d) Change in entity name. (e) Any attempted transfer, sale, or other conveyance of an interest in a license. (5) An applicant or licensee shall notify the department within 1 business day of all the following: (a) Adverse reactions to marihuana product sold or transferred by any licensee. (b) Criminal convictions, charges, or civil judgements in this state or any other state. (c) Regulatory disciplinary action taken or determined against an applicant or licensee by this state or any other states, including any pending action. (6) Failure to report material changes pursuant to subrule (4) of this rule or notifications under subrule (5) of this rule may result in sanctions or fines, or both.

Rule 15. Notifications of diversion, theft, loss, or criminal activity pertaining to any marihuana product. (1) Licensees and applicants shall notify the department, state police, and local law enforcement authorities within 24 hours of theft or loss of any marihuana product or criminal activity. (2) Failure to notify or report under subrule (1) of this rule may result in sanctions or fines, or both.

Rule 16. Inspection; investigation. (1) The department shall do all of the following with respect to inspections and investigations of applicants, licensees, proposed marihuana facilities, and marihuana facility operations: (a) Oversee and conduct inspections through its investigators, agents, auditors, or the state police of proposed marihuana facilities and marihuana facilities as provided in section 303 of the act to ensure compliance with the act and these rules. (b) Investigate individuals employed by marihuana facilities. (c) Inspect and examine marihuana facilities and proposed marihuana facilities. (d) Inspect, examine, and audit records of the licensee. (2) The department may at any time, through its investigators, agents, auditors, or the state police, without a warrant and without notice to the licensee, enter the proposed marihuana facility or marihuana facility, offices, or other places of business of a licensee, if evidence of compliance or noncompliance is likely to be found in accordance with the act and these rules.

417 2017 MR 22 – December 15, 2017 (3) To ensure the safety, security, and integrity of marihuana facility operations, the department, through its investigators, agents, auditors, or the state police may place an administrative hold on marihuana product and order that no sales or transfers occur during an investigation for an alleged violation or violation of the act or these rules. (4) The department, through its investigators, agents, auditors, or the state police may inspect, examine, and audit relevant records of the licensee. If a licensee fails to cooperate with an investigation, the department through its investigators, agents, auditors, or the state police may impound, seize, assume physical control of, or summarily remove records from a proposed marihuana facility or marihuana facility. (5) The department through its investigators, agents, auditors or the state police may eject, or exclude or authorize the ejection or exclusion of, an individual from a proposed marihuana facility or marihuana facility if that individual violates the act, a final order, or these rules. (6) The department through its investigators, agents, auditors, or the state police may take any reasonable or appropriate action to enforce the act and rules. (7) This rule does not limit the application of any other remedies or sanctions that are available through local, state, and federal laws, the act, and these rules. (8) For purposes of this rule, the term “record” means books, ledgers, documents, writings, photocopies, correspondence, electronic records, videotapes, surveillance footage, electronic storage mediums, electronically stored records, money receptacles, equipment in which records are stored, including data or information in the statewide monitoring system, or any other document that is used for recording information.

Rule 17. Persons subject to penalty; violations. (1) If the department through its investigators, agents, auditors, or the state police during the physical site inspection determine violations of the act or these rules exist, the department shall notify the person, applicant, or licensee of the violation during the physical site inspection or thereafter and the person, applicant or licensee may be responsible for sanctions or fines, or both. (2) The department may issue a notice of a violation or fine, or both, for any violations of the act and applicable rules, including those observed by the department through its investigators, agents, auditors, or the state police while in the performance of their duties. (3) Where the department through its investigators, agents, auditors, or the state police determine a violation of the act or these rules exists, such violations must be cited in a format established by the department. After a notice of violation or fine or both is issued to a person, applicant, or licensee, the department may hold a compliance conference or a hearing if applicable as prescribed in the act and these rules. (4) The department may forward information regarding violations of the act or these rules or any other state or federal law to the state police, department of attorney general, and the prosecutor for the jurisdiction in which the alleged violation of the act or rules has occurred. (5) The department may take action for failure to pay any fine within the time written on the violation notice pursuant to the act or these rules.

Rule 18. Sanctions; fines. (1) A person, applicant, or licensee found in violation of these rules or the act may be subject to sanctions, including, but not limited to, license denial, limitation, fines, revocation, suspension, nonrenewal, administrative holds, and orders to cease operations. (2) A violation of these rules, the act, the marihuana tracking act, or any ordinance adopted under section 205 of the act may result in 1 or more of the following: (a) A license may be denied, limited, revoked, or restricted. (b) A licensee or an employee of a licensee may be removed. (c) Civil fines of up to $5,000.00 may be imposed against an individual. (d) Civil fines up to $10,000.00 or an amount equal to the daily gross receipts, whichever is greater, against a licensee for each violation of the act, these rules, or an order. (e) Civil fines may be assessed for each day the licensee is not in compliance with the act or these rules. Assessment of a civil fine is not a bar to the investigation, arrest, charging, or prosecution of an individual for any other violation of the act or these rules.

418 2017 MR 22 – December 15, 2017 (3) A license may be suspended without notice or hearing upon a determination that the safety or health of patrons or employees is jeopardized by continuing a marihuana facility's operation as provided in the act or these rules. (4) The attempted transfer, sale, or other conveyance of an interest in a license without prior approval is grounds for suspension or revocation of the license or for other sanction as provided in sections 406 and 409 of the act or these rules. (5) The department may impose any other remedies, sanctions, or penalties not inconsistent with the act or these rules.

Rule 19. Temporary operation; limited circumstances; conditional. (1) An applicant for a state operating license may temporarily operate a proposed marihuana facility that would otherwise require a state operating license if either of the following applies: (a) The applicant’s proposed marihuana facility is within a municipality that adopted an ordinance before December 15, 2017 but is pending the adoption of an ordinance pursuant to section 205 of the act. The applicant shall submit an attestation on a form established by the department that includes the signature of the clerk of the municipality or his or her designee attesting to all of the following: (i) The municipality has adopted an ordinance before December 15, 2017. (ii) The municipality authorizes the temporary operation of the applicant. (b) The applicant’s proposed marihuana facility is within a municipality that has adopted an ordinance pursuant to section 205 of the act before December 15, 2017. The applicant shall submit an attestation on a form established by the department that includes the signature of the clerk of the municipality or his or her designee attesting to all the following: (i) The municipality has adopted an ordinance pursuant to section 205 of the act, including, if applicable, the disclosure of any limitations on the number or type of marihuana facilities, or both. (ii) The municipality authorizes the temporary operation of the applicant. A resolution may be adopted by a municipality that authorizes the clerk of the municipality or his or her designee to sign the attestation form in subdivision (b) of this subrule. (2) A person that does not comply with this rule shall cease and desist operation of a proposed marihuana facility and may be subject to all the penalties, sanctions, and remedies under state and federal law, the act, or these rules. (3) An applicant that is temporarily operating under this rule is not guaranteed a state operating license. (4) For purposes of this rule only, an applicant shall apply for a state operating license as prescribed by the act and these rules no later than February 15, 2018. If the applicant does not apply for a state operating license as prescribed by the act and these rules no later than Feb 15, 2018 then the temporary operation may be used as a reason for denial of a license as prescribed in Rule 12. (5) The department shall issue or deny a state operating license on or before June 15, 2018. A municipality with an authorizing ordinance under subrule (1)(a) of this rule shall have adopted a new or amended ordinance pursuant to section 205 of the act and these rules no later than June 15, 2018. (6) An applicant under this rule that has been denied licensure, or has not been issued a license by June 15, 2018, is operating without a license and shall cease any operation. Any temporary operation after June 15, 2018 is considered unlicensed activity. Unlicensed activity may result in a referral to law enforcement for unlicensed activity. The department may notify the state police and department of attorney general of any unlicensed activity. (7) Notwithstanding the provisions of this rule, if a state operating license is issued, an applicant is no longer operating temporarily and shall comply with all the provisions of the act and these rules.

Rule 20. Transition period. (1) To ensure the safety, security, and integrity of the operation of marihuana facilities, there is a transition period consisting of 30 calendar days during which marihuana product can be entered into the statewide monitoring system to ensure statewide tracking beginning on the day a state operating license is issued to a licensee for the first time except for additional licenses issued to the same license holder for a stacked license after a first license is issued. (2) Within the 30-calendar-day period, a licensee shall do all of the following: (a) Record all marihuana product in the statewide monitoring system during this 30-calendar-day period as prescribed by the act and these rules.

419 2017 MR 22 – December 15, 2017 (b)Tag or package all inventory that has been identified in the statewide monitoring system as prescribed by the act and these rules. (c) Comply with all testing requirements as prescribed by the act and these rules. (3) After the 30-calendar-day period, any marihuana product that has not been identified in the statewide monitoring system under these rules and the act is prohibited from being onsite at a marihuana facility. (4) A violation of this rule may result in sanctions or fines, or both. (5) At any time during this 30-calendar-day period and thereafter, a marihuana facility is subject to an inspection under Rule 16.

Rule 21. State operating licenses; licensees; operations; general. (1) A state operating license and a stacked license as described in Rule 22 are limited to the scope of the state operating license issued for that type of marihuana facility that is located within the municipal boundaries connected with the license. (2) In order to ensure the safety, security, and integrity of the operation of marihuana facilities, a licensee shall comply with all of the following: (a) Marihuana facilities shall be partitioned from any other marihuana facility, activity, business, or dwelling. (b) Access to the marihuana facility is restricted to the licensee, employees of the licensee, and registered qualifying patients and registered primary caregivers with valid registry cards, if applicable, and the department, through its investigators, agents, auditors, or the state police. A separate waiting area may be created for visitors not authorized to enter the marihuana facility. The licensee shall maintain a log tracking all visitors to a marihuana facility. The visitor log must be available at all times for inspection by the department, through its investigators, agents, auditors, or the state police to determine compliance with the act and these rules. (c) Licensee records must be maintained and made available to the department upon request. (d) The marihuana facility must be at a fixed location. Mobile marihuana facilities and drive through operations are prohibited. Any sales or transfers of marihuana product by internet or mail order, consignment, or at wholesale are prohibited. (e) A state operating license issued under the act must be framed under a transparent material and prominently displayed in the marihuana facility. (f) Any other operational measures requested by the department that are not inconsistent with the act and these rules.

Rule 22. Stacked license. A grower that has already been issued a state operating license specified as a class C-1,500 marihuana plants may apply to stack a license at a marihuana facility specified in the state operating license subject to payment of a separate regulatory assessment for each state operating license stacked and may be subject to any additional fees under Rule 7 and is subject to all requirements of the act and these rules.

Rule 23. Changes to licensed marihuana facility. (1) Any change or modification to the marihuana facility after licensure is governed by the standards and procedures set forth in the act and these rules and any regulations adopted pursuant thereto, and requires the approval of the department before any changes or modification. (2) Any change of a location of a marihuana facility after licensure requires a new license application under Rules 5 and 6 and may include, but is not limited to, regulatory assessment or application fees or both. A licensee shall produce written documentation from the municipality approving the proposed new marihuana facility location as indicated on the application provided to the department and be in compliance with section 205 of the act.

Rule 24. Operation at a same location—grower, processor, and provisioning center. (1) Any combination of the following types of state operating licenses may operate as separate marihuana facilities at the same location: (a) A grower. (b) A processor. (c) A provisioning center.

420 2017 MR 22 – December 15, 2017 (2) To operate at a same location subject to subrule (1) of this rule all the following apply: (a) The department has authorized the proposed operation at the same location. (b) The operation at a same location shall not be in violation of any local ordinances or regulations. (c) The municipality shall not limit the type or number of marihuana facilities under section 205 of the act or prohibit the operation at the same location by local ordinance or zoning regulations. (d) Each marihuana facility subject to subrule (1) of this rule shall do all the following: (i) Apply for and be granted separate state operating licenses and pay a separate regulatory assessment for each state operating license. (ii) Have distinct and identifiable areas with designated structures that are contiguous and specific to the state operating license. (iii) Have separate entrances and exits, inventory, record keeping, and point of sale operations, if applicable. (iv) Post the state operating license on the wall in its distinct area and as provided in these rules. (e) Additional inspections and permits may be required for local or state building inspection, fire safety, and public health standards. (3) Operation of a state operating license at the same location that includes a licensed provisioning center shall have the entrance and exit to the licensed provisioning center marihuana facility and entire inventory physically separated from any of the other licensed marihuana facility or facilities so that persons can clearly identify the retail entrance and exit. (4) For purposes of this rule, a marihuana facility operating at a same location under this rule with multiple state operating licenses may transfer marihuana product or money between marihuana facilities authorized to operate at a same location under the following circumstances: (a) Each state operating license operating at a same location has common ownership. (b) An employee is designated by each licensee of a marihuana facility to monitor the transfer and execute the transfer or a licensed secure transporter executes the transfer in accordance with the act and these rules. (c) A manifest in the statewide monitoring system is created documenting the transfer as provided in the act and these rules. (d) Receipt of the transfer is recorded in the statewide monitoring system as provided in these rules.

Rule 25. Marihuana facilities; requirements. (1) To ensure the safety, security, and integrity of the operation of marihuana facilities a grower shall operate at a marihuana facility under either of the following conditions: (a) The marihuana facility operations are within a building that meets the security requirements and passes the inspections in these rules and has a building permit pursuant to Rule 26 and these rules. (b) The marihuana facility operations are within a building except for cultivation may occur in an outdoor area that must meet all the following conditions: (i) The outdoor area containing the cultivation of marihuana plants is contiguous with the building, fully enclosed by fences or barriers that block outside visibility of the marihuana plants from the public view, with no marihuana plants growing above the fence or barrier that is visible to the public eye and the fences are secured and comply with the applicable security measures in these rules, including but not limited to, locked entries only accessible to authorized persons or emergency personnel. (ii) After the marihuana is harvested, all drying, trimming, curing, or packaging of marihuana occur inside the building meeting all the requirements under these rules. (iii) The building meets the security requirements and passes the inspections in these rules and has a building permit pursuant to Rule 26 and these rules. (2) To ensure the safety, security, and integrity of the operation of marihuana facilities, a secure transporter shall have a primary place of business as its marihuana facility that is operating in a municipality that has adopted an ordinance that meets the requirements of section 205 of the act and these rules and its marihuana facility must comply with the requirements prescribed by the act and these rules. A secure transporter may travel through any municipality to transport marihuana product. All the following apply: (a) The secure transporter may take physical custody of the marihuana or money but legal custody belongs to the transferor or transferee.

421 2017 MR 22 – December 15, 2017 (b) A secure transporter is prohibited from selling or purchasing marihuana products. (c) A secure transporter must transport any marihuana product in a locked, secured, sealed container that is not accessible while in transit. If the licensee transports money associated with the purchase or sale of marihuana product between facilities, the licensee shall lock the money in a sealed container kept separate from the marihuana product and only accessible to the licensee and its employees. (d) All transactions including, but not limited to, current inventory must be entered in the statewide monitoring system. These records must be maintained and made available to the department upon request. (e) All handling of money associated with the purchase or sale of marihuana between facilities must be logged and tracked. These records must be maintained and made available to the department upon request. (f) A secure transporter shall have a route plan and manifest available for inspection by the department, through its investigators, agents, auditors, or the state police to determine compliance with the act and these rules. A copy of the route plan and manifest must be carried with the secure transporter during transport between marihuana facilities. A secure transporter is subject to administrative inspection by a law enforcement officer at any point during the transportation of marihuana product pursuant to the act or these rules. A copy of a route plan and manifest must be carried in the transporting vehicle and presented to a law enforcement officer upon request. (g) A secure transporter shall follow the manifest. In cases of emergencies the secure transporter shall notify the transferor and transferee, update the statewide monitoring system and revise the manifest to reflect the unexpected change to the original manifest. (h) The reasonable timeframe for the secure transporter to maintain custody of the marihuana is not more than 48 hours or by permission of the department on a case-by-case basis. (i) A secure transporter shall identify and record all vehicles with the department and have the required registration with the secretary of state as required under state law. Secure transporter vehicles may be subject to inspection at any time by the department, through its investigators, agents, auditors, or the state police to determine compliance with act or these rules. (3) To ensure the safety, security, and integrity of the operation of marihuana facilities, a provisioning center shall have a separate room that is dedicated as the point of sale area for the transfer or sale of marihuana product as provided in the act and these rules. The provisioning center shall keep marihuana products behind a counter or other barrier to ensure a registered qualifying patient or registered primary caregiver does not have direct access to the marihuana products.

Rule 26. Building and fire safety. (1) An applicant’s proposed marihuana facility or a licensee’s marihuana facility may be subject to inspection by a state building code official, state fire official, or code enforcement official to confirm that no health or safety concerns are present. (2) The department or its authorized agents, state building code official, or his or her authorized designee may conduct pre-licensure and post-licensure inspections to ensure that applicants and licensees comply with the Stille- DeRossett-Hale single state construction code act, 1972 PA 230, MCL 125.1501 to 125.1531. (3) An applicant or licensee shall not operate a marihuana facility unless a permanent certificate of occupancy has been issued by the appropriate enforcing agency. Prior to a certificate of occupancy being issued work must be completed in accordance with the Stille-DeRossett-Hale single state construction code act, 1972 PA 230, MCL 125.1501 to 125.1531. All of the following apply: (a) An applicant or licensee shall obtain a building permit for any building utilized as a proposed marihuana facility or marihuana facility as provided in the act and these rules. The issuance, enforcement, and inspection of building permits under this act may remain with the governmental entity having jurisdiction under 1972 PA 230, MCL 125.1501 to 125.1531. (b) An applicant or licensee shall obtain a building permit for a change of occupancy for an existing building to be utilized as a proposed marihuana facility or marihuana facility as provided in the act and these rules. (4) An applicant or licensee shall not operate a marihuana facility unless the proposed marihuana facility or marihuana facility has passed prelicensure fire safety inspection by the Bureau of Fire Services (BFS). The department or its authorized agents, or state fire marshal or his or her authorized designee, may conduct pre-

422 2017 MR 22 – December 15, 2017 licensure and post-licensure inspections of a marihuana facility. An applicant or licensee shall comply with the following: (a) A BFS inspection may be conducted at any reasonable time to ensure fire safety compliance as provided in this rule and subrule (5) of this rule. A BFS inspection may be annual or biannual and result in the required installation of fire suppression devices or other means necessary for adequate fire safety pursuant to state standards. (b) BFS may require marihuana facilities to obtain operational permits, including but not limited to, carbon dioxide systems used in beverage dispensing applications, amended for cultivation use and extraction, compressed gases, combustible fibers, flammable and combustible liquids, fumigation and insecticidal fogging, hazardous materials, high piled storage (high rack system cultivation), and liquefied petroleum (LP) gas. (c) For specific installation or systems, BFS may require facilities to obtain construction permits, including but not limited to, building construction, electrical, mechanical, compressed gases, flammable and combustible liquids, hazardous materials, LP gas, automatic fire extinguishing/suppression systems, fire alarm and detections systems, and related equipment found during fire safety inspections. (5) The department or its authorized agents, or state fire marshal or his or her authorized designee, may conduct a BFS fire safety inspection of marihuana facility, at any reasonable time to ensure compliance with the national fire protection association (NFPA) standard 1, 2018 edition, entitled “fire code,” which is adopted by reference as part of these rules. A licensee shall comply with the NFPA 1, 2018 fire code as adopted and the following additional requirements: (a) Ductwork must be installed with accordance with the manufacturer and NFPA 90A. (b) Suppression systems outlined in NFPA 12, NFPA 13, NFPA 17, NFPA 2001 may be required to meet the suppression needs within a marihuana facility. (c) Processors, growers, and safety compliance facilities shall implement appropriate exhaust ventilation systems to mitigate noxious gasses or other fumes used or created as part of any production process or operations. Exhaust ventilation equipment must be appropriate for the hazard involved and must comply with local fire code and Michigan mechanical codes. (6) In addition to meeting all the requirements in subrules (1) to (4) of this rule, growers and processors shall also comply with the following: (a) The department or its authorized agents, or state fire marshal or his or her authorized designee, may enter and inspect a grower and processor marihuana facility at any reasonable time. (b) In addition to any inspections required under the act and these rules, fire safety inspections are required if any of the following occur: (i) Modifications to the grow areas, rooms and storage, extraction equipment and process rooms, or marihuana- infused product processing equipment within a marihuana facility. (ii) Changes in occupancy. (iii) Material changes to a new or existing grower or processor facility including changes made pre-licensure and post-licensure. (iv) Changes in extraction methods and processing or grow areas and building structures may trigger a new inspection. (c) For extractions using compressed gases of varying materials including, but not limited to, butane, propane, and carbon dioxide that are used in multiple processes in cultivation or extraction the following must be met: (i) Flammable gases of varying materials may be used in multiple processes in cultivation or extraction and must meet the requirements in NFPA 90 A, NFPA 58, Appendix B of NFPA 58, NFPA 70 and the applicable parts of the international fuel gas code. (ii) Processes that extract oil from marihuana plants and marihuana products using flammable gas or flammable liquid must have leak and/or gas detection measures. All equipment used in the detection of flammable and/or toxic gases must be approved by the BFS and may require construction and mechanical permits. (iii) Marihuana facilities that have exhaust systems are regulated by NFPA 45, NFPA 91 and the applicable parts of the Michigan mechanical code.

Rule 27. Security measures; required plan; video surveillance system.

423 2017 MR 22 – December 15, 2017 (1) An applicant for a license to operate a proposed marihuana facility shall submit a security plan that demonstrates, at a minimum, the ability to meet the requirements of this rule. (2) Licensees shall ensure that any person at the marihuana facility, except for employees of the licensee, are escorted at all times by the licensee or at least 1 employee of the licensee when in the limited-access areas at the marihuana facility. (3) A licensee shall securely lock the marihuana facility, including all interior rooms, windows, and points of entry and exits with commercial-grade, nonresidential door locks. (4) A licensee shall maintain an alarm system at the marihuana facility. Upon request, a licensee shall make available to the department all information related to the alarm system, monitoring, and alarm activity. (5) A licensee shall have a video surveillance system that, at a minimum, consists of digital or network video recorders, cameras capable of meeting the recording requirements in this rule, video monitors, digital archiving devices, and a color printer capable of delivering still photos. (6) The licensee shall ensure the video surveillance system does all the following: (a) Records at a minimum the following areas: (i) Any areas where marihuana products are weighed, packed, stored, loaded, and unloaded for transportation, prepared, or moved within the marihuana facility. (ii) Limited-access areas and security rooms. Transfers between rooms must be recorded. (iii) Areas storing a surveillance system storage device with at least 1 camera recording the access points to the secured surveillance recording area. (iv) The entrances and exists to the building must be recorded from both indoor and outdoor vantage points. The areas of entrance and exit between marihuana facilities at the same location if applicable, including any transfers between marihuana facilities. (v) Point of sale areas where marihuana products are sold and displayed for sale. (b) Records at all times images effectively and efficiently of the area under surveillance with sufficient resolution. (7) A licensee shall install each camera so that it is permanently mounted and in a fixed location. Each camera must be placed in a location that allows the camera to clearly record activity occurring within 20 feet of all points of entry and exit on the marihuana facility, and allows for the clear and certain identification of any person, including facial features, and activities, including sales or transfers, in all areas required to be recorded under these rules. (8) A licensee shall have cameras that record continuously 24 hours per day and recorded images must clearly and accurately display the time and date. (9) A licensee must secure the physical media or storage device on which surveillance recordings are stored in a manner to protect the recording from tampering or theft. (10) A licensee shall keep surveillance recordings for a minimum of 14 days, except for in instances of investigation or inspection by the department, through its investigators, agents, auditors, or the state police, in which case the licensee shall retain the recordings until such time as the department notifies the licensee that the recordings may be destroyed. (11) Surveillance recordings of the licensee are subject to inspection by the department, through its investigators, agents, auditors, or the state police, and must be kept in a manner that allows the department to view and obtain copies of the recordings at the marihuana facility immediately upon request. The licensee shall also send or otherwise provide copies of the recordings to the department upon request within the time specified by the department. (12) A licensee shall maintain a video surveillance system equipped with a failure notification system that provides notification to the licensee of any interruption or failure of the video surveillance system or video surveillance system storage device. (13) A licensee shall maintain a log of the recordings, which includes all of the following: (a) The identities of the employee or employees responsible for monitoring the video surveillance system. (b) The identity of the employee who removed the recording from the video surveillance system storage device and the time and date removed. (c) The identity of the employee who destroyed any recording.

Rule 28. Prohibitions.

424 2017 MR 22 – December 15, 2017 (1) Marihuana products not identified and recorded in the statewide monitoring system pursuant to the act, the marihuana tracking act, or these rules are prohibited from being on or at a marihuana facility. A licensee is prohibited from transferring or selling marihuana product that is not identified in the statewide monitoring system pursuant to the act or these rules. (2) Any marihuana product without a batch number or identification tag or label pursuant to these rules is prohibited from being on or at a marihuana facility. Marihuana product must be immediately tagged or identified into the statewide monitoring system or recorded as part of a batch as defined in these rules. (3) A violation of these rules may result in sanctions or fines, or both, in accordance with the act or these rules.

Rule 29. Plant batches, testing procedures. (1) A grower shall uniquely identify each immature plant batch in the statewide monitoring system. Each immature plant batch must not consist of more than 100 immature plants. (2) A grower shall tag each plant that is greater than 8 inches in height or more than 8 inches in width with an individual plant tag and record the identification information in the statewide monitoring system. (3) A grower shall delineate or separate the plants as the plants go through different growth stages and ensure that the plant tag is always identified with the plant throughout the growth span so that all plants can be easily identified and inspected pursuant to the act and these rules. A grower shall ensure that identification information is recorded in the statewide monitoring system in accordance with the act, the marihuana tracking act, and these rules. (4) After a tagged plant is harvested, it is part of a harvest batch so that a sample of the harvest batch can be tested by a safety compliance facility. A grower shall isolate a harvest batch from other plants or batches that has test results pending. A harvest batch must be easily distinguishable from other harvest batches until the batch is broken down into packages. (5) Before the marihuana product can leave the grower facility, a sample of the harvest batch must be tested by a licensed safety compliance facility as provided in Rule 32, and test results must indicate a passed test result in the statewide monitoring system before the marihuana can be packaged. Marihuana product from harvest batches must not be transferred or sold until tested, packaged, and tagged as required under subrule (4) of this rule. (6) After test results show a passed test, the grower shall destroy the individual plant tags and the harvest batch is packaged. Each package must have a package tag attached. A grower shall ensure this information is placed in the statewide monitoring system in accordance with the act, the marihuana tracking act, and these rules. (7) A grower shall not transfer or sell any marihuana product that has not been packaged with a package tag attached and recorded in the statewide monitoring system in accordance with the act, the marihuana tracking act, and these rules. (8) After a processor receives or purchases a package in the statewide monitoring system, and the processor proceeds to process the marihuana product in accordance with the scope of a processor license, the act, and these rules, the processor must give the marihuana product a new package tag anytime it changes state or is incorporated into something else. (9) Once a package is created by a processor of the marihuana product in its final state, the processor shall have the sample tested pursuant to Rule 32. The processor shall not transfer or sell a final package until after test results indicate a passed test. (10) After a provisioning center receives or purchases marihuana product in the statewide monitoring system, a licensee may sell or transfer marihuana product only to a registered qualifying patient or registered primary caregiver under all of the following conditions: (a) The marihuana product has received passing test results in the statewide monitoring system. If the information cannot be confirmed, the marihuana product must be tested by a safety compliance facility and receive passing test results prior to sale or transfer. (b) The marihuana product bears the label required for retail sale under the act and these rules.

Rule 30. Retesting. (1) A safety compliance facility may test or retest a sample to validate the results of a failed quality assurance test except as indicated under subrule (2) of this rule. The marihuana facility that provided the sample is responsible for all costs involved in a retest.

425 2017 MR 22 – December 15, 2017 (2) A failed test sample must pass 2 separate retests consecutively in order to be eligible to proceed to sale or transfer. If both retests pass, then the batch is out of quarantine and eligible for sale or transfer. If 1 or both retests fail, then the marihuana product must be destroyed as provided in these rules. (3) Marihuana product is prohibited from being retested in all the following: (a) The marihuana product is in a final package. (b) An original test for pesticides failed pursuant to these rules. If the amount of pesticides is not permissible by the department, the marihuana product is ineligible for retesting and the product must be destroyed. (c) An original failed test for microbials on marihuana-infused product is ineligible for retesting and the product must be destroyed.

Rule 31. Testing; safety compliance facility. (1) A safety compliance facility shall use analytical testing methodologies for the required quality assurance tests in subrule (2) of this rule that are validated and may be monitored on an ongoing basis by the department or a third party which shall include either of the following: (a) Following the most current version of the Cannabis Inflorescence: Standards of Identity, Analysis, and Quality Control monograph published by the American Herbal Pharmacopoeia. (b) Following the alternative testing methodology approved by the department and validated by an independent third party that the methodology followed by the laboratory produces scientifically accurate results as quality assurance for each test it conducts. (2) A safety compliance facility shall conduct the required quality assurance tests that include all of the following: (a) Moisture content. (b) Potency analysis. (c) Tetrahydrocannabinol level. (d) Tetrahydrocannabinol acid level. (e) Cannabidiol and cannabidiol acid levels. (f) Foreign matter inspection. (g) Microbial and mycotoxin screening. (h) Pesticides. (i) Chemical residue. (j) Fungicides. (k) Insecticides. (l) Metals screening. (m) Residual solvents levels. (n) Terpene analysis. (o) Water activity content. (3) Except as otherwise provided, if a sample collected pursuant to Rule 32 or provided to a safety compliance facility pursuant to these rules does not pass the microbial, mycotoxin, heavy metal, pesticide chemical residue, or residual solvents levels test based on these rules, the marihuana facility that provided the sample shall dispose of the entire batch from which the sample was taken and document the disposal of the sample using the statewide monitoring system pursuant to the act, marihuana tracking act, and these rules. (4) For the purposes of the microbial test, a sample provided to a safety compliance facility pursuant to this rule is deemed to have passed if it satisfies the standards set forth in Table 9 of the Cannabis Inflorescence: Standards of Identity, Analysis, and Quality Control monograph adopted by reference pursuant to these rules. (5) For the purposes of the mycotoxin test, a sample provided to a safety compliance facility pursuant to this rule is deemed to have passed if it meets the following standards:

Test Specification The total of aflatoxin B1, aflatoxin B2, aflatoxin G1 and aflatoxin G2...... <20 uG/KG of Substance Ochratoxin A...... <20 uG/KG of Substance

426 2017 MR 22 – December 15, 2017 (6) For the purposes of the heavy metal test, a sample of marihuana is deemed to have passed if it meets the following standards:

Metal Natural Health Products Acceptable Limits uG/KG Arsenic...... <0.14 Cadmium...... <0.09 Lead...... <0.29 Mercury...... <0.29

(7) A safety compliance facility shall do the following: (a) Become fully accredited by the International Organization for Standardization (ISO), ISO/IEC 17025:2005, or by an entity approved by the department within 1 year after the date the license is issued and agree to have the inspections and reports of the International Organization for Standardization made available to the department. (b) Become provisionally accredited under subdivision (a) of this subrule within 6 months from the issuance of a license. A safety compliance facility may be ordered to cease operations if provisional accreditation is not received within 6 months. (c) Maintain internal standard operating procedures. (d) Maintain a quality control and quality assurance program. (8) The department shall establish a proficiency testing program and designate safety compliance facility participation. A safety compliance facility shall analyze proficiency test samples using the same procedures with the same number of replicate analyses, standards, testing analysts and equipment as used for marihuana product testing. (9) The department shall publish a list of approved pesticides for use in the cultivation and production of marihuana plants and marihuana products to be sold or transferred in accordance with the act or these rules. For the purposes of the pesticide chemical residue test, a sample provided to a safety compliance facility pursuant to this rule is deemed to have passed as to that chemical if the sample satisfies the most stringent acceptable standard for an approved pesticide chemical residue as set forth in Subpart C of 40 C.F.R. Part 180. 40 C.F.R., § 180, et seq. or FIFRA section 25(b), whichever is more stringent. (10) If a sample provided to a safety compliance facility pursuant to this rule and Rule 32 passes the tests required under subrule (2) of this rule, the safety compliance facility shall enter the information in the statewide monitoring system of passed test results. Passed test results must be in the statewide monitoring system for a batch to be released for immediate processing, packaging, and labeling for transfer or sale in accordance with the act and these rules. (11) A safety compliance facility shall enter the results into the statewide monitoring system and file with the department an electronic copy of each safety compliance facility test result for any batch that does not pass the required tests while it transmits those results to the facility that provided the sample. In addition, a safety compliance facility shall maintain the test results and make them available to the department upon request. (12) The department shall take immediate disciplinary action against any safety compliance facility that fails to comply with the provisions of this rule or falsifies records related to this rule, including any sanctions or fine, or both. (13) A safety compliance facility is prohibited from doing the following: (a) Desiccating samples. (b) Dry labeling samples. (c) Pre-testing samples. (14) A safety compliance facility shall comply with random quality assurance compliance checks upon the request of the department. The department or its authorized agents may collect a random sample of marihuana product from a safety compliance facility or designate another safety compliance facility to collect a random sample of marihuana product in a secure manner to test that sample for quality assurance compliance pursuant to this rule.

Rule 32. Sampling.

427 2017 MR 22 – December 15, 2017 (1) A safety compliance facility shall test samples as provided in the act, the Michigan medical marihuana act, and these rules. (2) To ensure the safety, security, and integrity of the operation of marihuana facilities, a safety compliance facility shall collect the samples of marihuana product from another marihuana facility as follows: (a) The safety compliance facility shall physically collect samples of marihuana product from another marihuana facility to be tested at the safety compliance facility. The safety compliance facility shall ensure the samples of marihuana product are placed in secured, sealed containers that bear the labeling information as required under these rules. (b) The safety compliance facility shall enter in the statewide monitoring system the marihuana product sample that was collected from a grower, processor, or provisioning center, including the date and time the marihuana product is collected, transferred, tested, and returned. (c) When a testing sample is collected from a marihuana facility for testing in the statewide monitoring system, that marihuana facility must quarantine the marihuana product that is undergoing the testing from any other marihuana product at the marihuana facility. The marihuana facility shall indicate the sample being tested in the statewide monitoring system. The quarantined marihuana product must not be transferred or sold until testing results pass as provided under these rules. (d) Any marihuana product that a safety compliance facility collects for testing from a licensee under this rule must not be transferred or sold to any other marihuana facility other than the licensee from whom the sample was collected. (e) A safety compliance facility may request additional sample material from the same licensee where the sample was collected from for the purposes of completing the required quality assurance tests as long as the requirements of this rule are met. (f) A safety compliance facility or its authorized employee shall be physically present when collecting the samples of marihuana product for testing.

Rule 33. Requirements and restrictions on marihuana-infused products; edible marijuana product. (1) A processor shall prepackage and properly label marihuana-infused products before sale or transfer. (2) A processor of marihuana-infused products shall list and record the THC level of marihuana-infused products, as provided in Rule 34, in the statewide monitoring system and indicate the THC level on the label along with the tag identification as required under these rules. Items that are part of a product recall issued in the statewide monitoring system, the department, or other state agency if applicable must be immediately pulled from production and not sold or transferred. (3) Marihuana-infused products must be stored and secured as prescribed under these rules. (4) At a minimum, a processor shall label any marihuana-infused product it produces or packages with all the following: (a) The name and address of the marihuana facility that processes or packages the marihuana-infused product. (b) The name of the marihuana-infused product. (c) The ingredients of the marihuana-infused product, in descending order of predominance by weight. (d) The net weight or net volume of the product. (e) For an edible marihuana product, the processor shall comply with subdivisions (a) to (d) of this subrule and all of the following: (i) Allergen labeling as specified by federal labeling requirements. (ii) If any nutritional claim is made, appropriate labeling as specified by federal labeling requirements and these rules. (iii) A statement printed in at least the equivalent of 11-point font size in a color that provides a clear contrast to the background: "Made in a marihuana facility.” (5) A processor of edible marihuana product shall comply with all the following to ensure safe preparation: (a) 21 CFR part 110, except that refrigerated potentially hazardous marihuana product must be stored at 4.4 degrees Celsius (40 degrees Fahrenheit) or below. (b) The licensee shall provide employee training on safe food handling by providing any of the following: (i) Proof of ServSafe certification.

428 2017 MR 22 – December 15, 2017 (ii) Documentation of employee training on food handling, including, but not limited to, allergens and proper sanitation and safe food handling techniques. (c) A licensee, to ensure the safe preparation standards under this subrule, shall comply with 1 or more of the following: (i) FDA Food Safety Modernization Act (FSMA), 21 U.S.C. section 2201 et seq. (ii) Safe Quality Food (SQF), 7.2 edition. (iii)The International Organization for Standardization (ISO), ISO 22000/ISO/TS 22002-1. (d) The department may request in writing documentation to verify certifications and compliance with these rules. (6) A processor edible marihuana product must comply with all the following: (a) No edible marihuana product can be in a shape, color, package, or labeled in a manner that it would appeal to minors aged 17 years or younger. No edible marihuana product can be associated with or have cartoons, caricatures, toys, colors, designs, shapes, labels, or package that would appeal to minors. (b) No edible marihuana product can be easily confused with commercially sold candy. The use of the word candy or candies on the packaging or labeling is prohibited. (c) An edible marihuana product must be in child resistant packages or containers. (7) A processor is prohibited from producing an edible marihuana product that requires time or temperature control for safety. The end-product must be a stable shelf-life edible marihuana product. (8) For purposes of this rule, the term “edible marihuana product” means any marihuana-infused product containing marihuana that is intended for human consumption in a manner other than smoke inhalation. (9) This rule does not affect the application of any applicable local, state, or federal laws or regulations.

Rule 34. Maximum THC levels for marihuana-infused products. Marihuana-infused products processed, sold, or transferred through provisioning centers must not exceed the maximum THC levels as shown in table 1 as follows:

TABLE 1 Maximum THC Levels for Marihuana-Infused Products

*All MEDICAL MARIHUANA THC CONCENTRATION AND SERVING SIZE limits allow for a LIMITS variance of + or Type of Marihuana-Infused Maximum Maximum – 10%. Product Concentration or Concentration or Rule 35. Amount of THC Per Amount of THC in Storage of marihuana Serving* Container* product. (1) All Topical formulation N/A 6% by volume inventory of marihuana (examples – lotions, balms, rubs, etc.) products must be Tincture N/A 1,000mg stored at a marihuana Beverage 50mg 500mg facility in a secured Edible Substance 50mg 500mg limited (examples – candy bars, cookies, access area popcorn, honey, gummies, butter, etc.) or restricted access area, Other similar high-potency N/A 1,000mg and identified infused product and tracked consistently (examples – capsules, suppositories, with the statewide transdermal patches, etc.) monitoring system under the act, the marihuana tracking act, or these rules. (2) All containers used to store marihuana products for transfer or sale between marihuana facilities must be clearly marked, labeled, or tagged, if applicable, and enclosed on all sides in secured containers. The secured containers must be latched or locked in a manner to keep all contents secured within. Each secured container must be identified and tracked in accordance with the act, the marihuana tracking act, and these rules.

429 2017 MR 22 – December 15, 2017 (3) All chemicals or solvents must be stored separately from marihuana products and kept in locked storage areas. (4) Marihuana-infused products or materials used in direct contact with such products must have separate storage areas from toxic or flammable materials. (5) A provisioning center shall store all marihuana products for transfer or sale behind a counter or other barrier separated from stock rooms. (6) A safety compliance facility shall establish an adequate chain of custody and instructions for sample and storage requirements. (7) A licensee shall ensure that any stock or storage room meets the security requirements of these rules and any other applicable requirements in the act and these rules.

Rule 36. Marihuana product destruction and waste management. (1) Marihuana product that is to be destroyed or is considered waste must be rendered into an unusable and unrecognizable form and recorded in the statewide monitoring system. (2) A licensee shall not sell marihuana waste or marihuana products that are to be destroyed, or that the department orders destroyed. (3) A licensee shall manage all waste that is hazardous waste pursuant to part 111 of 1994 PA 451, MCL 324.11101 to 324.90106. (4) A licensee shall dispose of marihuana product waste in a secured waste receptacle using 1 or more of the following: (a) A manned and permitted solid waste landfill. (b) A manned compostable materials operation or facility. (c) An in-vessel digester. (d) In a manner in compliance with applicable state and local laws and regulations. (5) Wastewater generated during the cultivation of marihuana and processing of marihuana products shall be disposed of in compliance with applicable state and local laws and regulations.

Rule 37. Tracking identification; labeling requirements; general. (1) All marihuana product sold or transferred between marihuana facilities must have the tracking identification number that is assigned by the statewide monitoring system affixed, tagged, or labeled and recorded, and any other information required by the department, the act, and these rules. (2) To ensure access to safe sources of marihuana product the department if alerted in the statewide monitoring system may recall any marihuana products, issue safety warnings, and require a marihuana facility to provide information material or notifications to a registered qualifying patient or registered primary caregiver at the point of sale.

Rule 38. Marihuana plant; tracking requirements. Prior to a marihuana plant being sold or transferred, a package tag must be affixed to the plant or plant container and enclosed with a tamper proof seal that has the following information: (a) Business or trade name, licensee number, and RFID package tag assigned by the statewide monitoring system that is visible. (b) Name of the strain. (c) Date of harvest if applicable. (d) Seed strain if applicable. (e) Universal symbol if applicable.

Rule 39. Marihuana product sale or transfer; labeling requirements. Prior to marihuana product being sold or transferred to or by a provisioning center, the container, bag, or product holding the marihuana product must have a label and be sealed with all the following information: (a) The name of the licensee and license number that is the producer, including business or trade name, and tag or source number as assigned by the statewide monitoring system.

430 2017 MR 22 – December 15, 2017 (b) The name of the licensee and license number including business or trade name of licensee that packaged the product, if different from the processor of the marihuana product. (c) The unique identification number for the package or the harvest if applicable. (d) Date of harvest. (e) Name of strain. (f) Net weight in United States customary and metric units. (g) Concentration of THC or CBD. (h) Activation time expressed in words or through a pictogram. (i) Name of the safety compliance facility that performed any test, any associated test batch number, and any test analysis date. (j) Universal symbol published by the department. (k) A warning that states all the following: (i) "For use by registered qualifying patients only. Keep out of reach of children." (ii) "It is illegal to drive a motor vehicle while under the influence of marihuana."

Rule 40. Sale or transfer; provisioning centers. (1) A provisioning center may sell or transfer marihuana product to a registered qualifying patient or a registered primary caregiver if the following are met: (a) The licensee verifies with the statewide monitoring system that the registered qualifying patient or a registered primary caregiver holds a valid, current, unexpired, and unrevoked registry identification card. (b) The licensee confirms that the registered qualifying patient or the registered primary caregiver presented his or her valid driver license or government-issued identification card that bears a photographic image of the qualifying patient or primary caregiver. (c) The licensee determines, if completed, any transfer or sale will not exceed the daily purchasing limit prescribed in Rule 41. (d) Any marihuana product that is sold or transferred under this rule has been tested and bears the label required for sale or transfer in accordance with Rule 39. (2) A provisioning center may sell or transfer marihuana product to a visiting qualifying patient if all the following are met: (a) The licensee verifies that the visiting qualifying patient has a valid unexpired medical marihuana registry card or its equivalent issued in another state, district, territory, commonwealth, or insular possession of the United States that allows the medical use of marihuana. (b) The licensee confirms that the visiting qualifying patient presented his or her valid driver license or government- issued identification card that bears a photographic image of the visiting qualifying patient. (c) The licensee determines, if completed, any transfer or sale will not exceed the daily purchasing limit prescribed in Rule 41. (d) Any marihuana product that is sold or transferred under this rule has been tested and bears the label required for sale or transfer in accordance with Rule 39. (e) For purposes of this subrule, the term “visiting qualifying patient” means that term as defined in section 3 of the Michigan medical marihuana act. (3) The provisioning center shall enter all transactions, current inventory, and other information required by these rules in the statewide monitoring system in compliance with the act, marihuana tracking act, and these rules. The provisioning center shall maintain appropriate records of all sales or transfers under the act and these rules and make them available to the department through its investigators, agents, auditors, or the state police upon request.

Rule 41. Daily purchasing limits; provisioning center. The licensee shall verify in the statewide monitoring system before a sale or transfer of marihuana product to a registered qualifying patient or registered primary caregiver that the sale or transfer will not exceed the daily purchasing limit as follows: (a) For a registered qualifying patient, an amount of marihuana product that does not, in total, exceed 2.5 ounces per day.

431 2017 MR 22 – December 15, 2017 (b) For a registered primary caregiver, an amount of marihuana product that does not, in total, exceed 2.5 ounces per day for each registered qualifying patient with whom he or she is connected through the department’s registration process.

Rule 42. Marketing and advertising restrictions. (1) Marihuana facilities shall comply with all municipal ordinances, state law, and these rules regulating signs and advertising. (2) A licensee shall not advertise marihuana product where the advertisement is visible to members of the public from any street, sidewalk, park, or other public place. (3) Marihuana products must be marketed or advertised as “medical marihuana” for use only by registered qualifying patients or registered primary caregivers. (4) Marihuana products must not be marketed or advertised to minors aged 17 years or younger. Sponsorships targeted to members aged 17 years or younger are prohibited.

Rule 43. Employees; requirements. (1) A licensee shall conduct a criminal history background check on any prospective employee prior to hiring that individual pursuant to section 405 of the act. The licensee shall keep records of the results of the criminal history background checks. A licensee shall record confirmation of criminal history background checks and make the confirmation of criminal history background checks available for inspection upon request by the department or authorized persons. (2) To ensure the safety, security, and integrity of marihuana facility operations, a licensee shall comply with all of the following: (a) A licensee shall have a policy in place that requires employees to report any new or pending charges or convictions. If an employee is charged or convicted for a controlled substance-related felony or any other felony, the licensee shall report it immediately to the department. (b) A licensee shall enter any employee of the licensee at the time of hire in the statewide monitoring system for an identification number that will be assigned by the department in the statewide monitoring system. The licensee shall immediately update in the statewide monitoring system employee information and status. (c) If an employee is no longer employed by a licensee, the licensee shall remove access and permissions to the marihuana facility and the statewide monitoring system. (d) A licensee shall train employees and have an employee training manual that includes, but is not limited to, employee safety procedures, employee guidelines, security protocol, and educational training, including, but not limited to, marihuana product information, dosage and daily limits, or educational materials. (e) A licensee shall establish point of sale or transfer procedures for employees at provisioning centers performing any transfers or sales to registered qualifying patients and registered primary caregivers. The qualifications and restrictions must include, but are not limited to, training in dosage, marihuana product information, health or educational materials, point of sale training, daily purchasing limits, CBD and THC information, serving size, and consumption information including any warnings. (f) A licensee shall screen prospective employees against a list of excluded employees based on a report or investigation maintained by the department in the statewide monitoring system. (g) At the time a registered primary caregiver is hired as an employee of a grower, processor, or secure transporter, the licensee or the individual shall withdraw registration as a registered primary caregiver in a manner established by the department. (h) If an individual is present at a marihuana facility or in a secure transporter vehicle who is not identified as a licensee or an employee of the licensee in the statewide monitoring system or is in violation of the act or these rules, the department, through its investigators, agents, auditors, or the state police may take any action permitted under the act and these rules. (3) Employee records are subject to inspection or examination by the department, through its investigators, agents, auditors, or the state police to determine compliance with the act or these rules. (4) For purposes of this rule “employee” includes, but is not limited to, hourly employees, contract employees, trainees, or any other person given any type of employee credentials or authorized access to the marihuana facility.

432 2017 MR 22 – December 15, 2017

Rule 44. Definitions. These rules use terms as defined in Rule 1, sections 101 to 102 of the act, and sections 1 to 3 of the APA. In addition, as used in this these rules: (a) “Agency” means the department, bureau, board, authority, or officer created by the constitution, statute, or agency action. (b) “APA” means the administrative procedures act of 1969, 1969 PA 306, MCL 24.201 to 24.328. (c) “Contested case hearing” means an administrative hearing conducted by an administrative law judge within MAHS on behalf of the agency in accordance with MCL 333.27407(4) and 333.27302(i). (d) “MAHS” means the Michigan administrative hearing system within the Michigan department of licensing and regulatory affairs. (e) “MAHS general hearing rules” means the administrative hearing rules promulgated by the Michigan administrative hearing system set forth in R 792.10101 to R 792.10137 of the Michigan administrative code. (f) “Public investigative hearing” means a proceeding before the medical marihuana licensing agency to provide an applicant an opportunity to present testimony and evidence to establish suitability for a license, in accordance with MCL 333.27407(3).

Rule 45. Hearing procedures; scope and construction of rules. (1) These rules apply to hearings under the jurisdiction of the agency involving the denial of a license or other licensing action pursuant to section 407 of the act, marihuana tracking act, or involving complaints brought by licensees pursuant to section 302 of the act. (2) These rules are construed to secure a fair, efficient, and impartial determination of the issues presented in a manner consistent with due process. (3) If the rules do not address a specific procedure, the MAHS general hearing rules, the currently effective Michigan court rules, and the contested case provisions of sections 71 to 87 of the APA apply.

Rule 46. Hearing on license denial. (1) An applicant denied a license by the agency may request a public investigative hearing in writing within 21 days of service of notice of the denial. (2) After the agency receives notice of an applicant’s request for a public investigative hearing, the agency shall provide an opportunity for such hearing at which the applicant may present testimony and evidence to establish suitability for a license. (3) The agency shall provide the applicant with not less than 2 weeks written notice of the public investigative hearing. The notice must include all of the following information: (a) A statement of the date, hour, place, and nature of the hearing. (b) A statement of the legal authority and jurisdiction under which the hearing is to be held. (c) A short and plain statement of the issues involved, and reference to the pertinent sections of the act and rules involved. (d) A short description of the order and manner of presentation for the hearing. (4) Not less than 2 weeks before the hearing, the agency shall post notice of the public investigative hearing at its business office in a prominent place that is open and visible to the public. (5) The agency, or 1 or more administrative law judges designated and authorized by the agency, may conduct and preside over the public investigative hearing and may do all of the following: (a) Administer oaths or affirmations to witnesses called to testify at the hearing. (b) Receive evidence in the form of testimony and exhibits. (c) Establish and regulate the order of presentation and course of the public investigative hearing; set the time and place for continued hearings; and fix the time for filing written arguments, legal briefs, and other legal documents. (d) Accept and consider relevant written and oral stipulations of fact and law that are made part of the hearing record. (6) Upon timely request of the applicant or the agency in accordance with the Michigan court rules currently in effect, the agency or the agency’s designated administrative law judge may issue subpoenas duces tecum for the

433 2017 MR 22 – December 15, 2017 production of books, ledgers, records, memoranda, electronically retrievable data, and other pertinent documents and administer oaths and affirmations to witnesses as appropriate to exercise and discharge the powers and duties under the act. (7) During the public investigative hearing, the applicant and the agency must be given a full opportunity to present witnesses and questions or cross-examine the opposing party’s witnesses, and to present all relevant information to the agency regarding the applicant’s eligibility and suitability for licensure. (8) The applicant shall at all times have the burden of establishing, by clear and convincing evidence, its eligibility and suitability for licensure under the act and these rules. (9) The agency shall record the public investigative hearing at its direction, stenographically or by other means, to adequately ensure preservation of an accurate record of the hearing. (10) Following the public investigative hearing, the matter must be considered by a quorum of the agency at a regular or emergency meeting properly noticed, at which the agency shall decide whether to affirm, reverse, or modify in whole or in part the denial of license. (11) The agency’s decision to affirm, reverse, or modify in whole or in part the denial of license must be based on the whole record before the agency and not be limited to testimony and evidence submitted at the public investigative hearing, in accordance with section 407(3) of the act. (12) The agency’s decision to affirm, reverse, or modify in whole or in part the denial of license must be reduced to writing and served upon the applicant and agency within a reasonable time.

Rule 47. Review of licensing action. (1) A licensee notified of a license violation, or of the agency’s intent to suspend, revoke, restrict, or refuse to renew a license or impose a fine, may be given an opportunity to show compliance with the requirements before the agency taking action as prescribed by the act or these rules. (2) A licensee aggrieved by an action of the agency to suspend, revoke, restrict, or refuse to renew a license, or to impose a fine, may request a contested case hearing in writing within 21 days of service of notice of the intended action. (3) Upon receipt of a timely request, the agency shall provide the licensee an opportunity for a contested case hearing in accordance with sections 71 to 87 of the APA and the MAHS general hearing rules. (4) The contested case hearing must be conducted by an administrative law judge or judges within the MAHS. (5) Upon timely request of the licensee or the agency in accordance with the Michigan court rules currently in effect, an assigned administrative law judge may issue subpoenas duces tecum for the production of books, ledgers, records, memoranda, electronically retrievable data, and other pertinent documents, and administer oaths and affirmations to witnesses as appropriate to exercise and discharge the powers and duties under the act. (6) A written request for admission may be served upon a designated party in a contested case pursuant to the Michigan court rules. Each of the matters for which an admission has been requested must be deemed admitted, unless the designated party responds to the request in the manner set forth in the currently effective Michigan court rules. (7) The agency has the burden of proving, by a preponderance of the evidence, that sufficient grounds exist for the intended action to suspend, revoke, restrict, or refuse to renew a license, or to impose a fine, or for the summary suspension of a license.

Rule 48. Summary suspension. (1) If the agency summarily suspends a license under section 407(2) of the act without notice or hearing upon a determination that the safety or health of patrons or employees is jeopardized by continuing a marihuana facility’s operation, a post-suspension hearing must be held promptly to determine if the suspension should remain in effect, in accordance with section 92 of the APA and the MAHS general hearing rules. (2) At the post-suspension hearing, the agency has the burden of proving by a preponderance of the evidence that the summary suspension should remain in effect because the safety or health of patrons or employees is jeopardized by continuing a marihuana facility’s operation. (3) Immediately after the post-suspension hearing, the administrative law judge assigned to hear the matter shall issue a written order granting or denying dissolution of the summary suspension.

434 2017 MR 22 – December 15, 2017 (4) If the licensee fails to appear at the post-suspension hearing, the administrative law judge shall find that the safety or health of patrons or employees is jeopardized by continuing a marihuana facility’s operation, and continue the order of summary suspension. (5) The record created at the post-suspension hearing becomes a part of the record at any subsequent hearing in the contested case.

Rule 49. Complaint by licensee. (1) A licensee may file a written complaint with the agency regarding any investigative procedures of this state that are believed to be unnecessarily disruptive of marihuana facility operations, as provided in MCL 333.27302(i). (2) The agency may delegate to a subcommittee of the agency the authority to hear, review, or rule on a licensee complaint. (3) The agency or its subcommittee may delegate authority to an administrative law judge to hear a licensee complaint as a contested case in accordance with sections 71 to 79 of the APA and the MAHS general hearing rules. (4) As the complaining party, a licensee has the burden of proving by a preponderance of the evidence that the investigative procedures of this state unreasonably disrupted its marihuana facility operations.

Rule 50. Proposal for decision, exceptions, and replies. Following an opportunity for contested case hearing and closure of the record after submission of briefs, if any, the administrative law judge shall prepare and serve upon the parties a proposal for decision containing proposed findings of fact and conclusions of law, in accordance with section 81 of the APA.

Rule 51. Final order. (1) The agency shall consider the entire contested case record and may affirm, reverse, or modify all or part of the proposal for decision. (2) The agency’s decision must be reduced to writing and served upon the licensee within a reasonable time. (3) The review decision or order of the agency following an opportunity for hearing is deemed to be the final agency decision or order for purposes of judicial review under sections 101 to 106 of the APA.

MICHIGAN DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS

______Shelly Edgerton, Director Department of Licensing and Regulatory Affairs

Pursuant to Section 48(1) of 1969 PA 306, as amended, MCL 24.248(1), I hereby concur in the finding of the Department of Licensing and Regulatory Affairs that the circumstances creating an emergency have occurred and the promulgation of the above rules is required for the preservation of the public health, safety, and welfare.

______Rick Snyder, Governor Date

435 2017 MR 22 – December 15, 2017

EXECUTIVE ORDERS AND EXECUTIVE REORGANIZATION ORDERS

MCL 24.208 states in part:

“Sec. 8. (1) The Office of Regulatory Reform shall publish the Michigan register at least once each month. The Michigan register shall contain all of the following:

(a) Executive orders and executive reorganization orders.”

436 2017 MR 22 – December 15, 2017

EXECUTIVE ORDERS

EXECUTIVE ORDER No. 2017 - 10

CREATION OF THE PUBLIC HEALTH ADVISORY COUNCIL

DEPARTMENT OF HEALTH AND HUMAN SERVICES

WHEREAS, Section 1 of Article V of the Michigan Constitution of 1963 vests the executive power of the state of Michigan in the Governor; and

WHEREAS, Section 8 of Article V of the Michigan Constitution of 1963 provides that each principal department shall be under the supervision of the Governor unless otherwise provided by the constitution; and

WHEREAS, the Public Health Advisory Commission was created as a temporary commission under Section 4 of Article V of the Michigan Constitution by Executive Order 2016-19 to make recommendations for improvements to Michigan’s public health delivery system; and

WHEREAS, the Public Health Advisory Commission successfully completed its duties by issuing a final report in April of 2017 (“the Report”); and

WHEREAS, in the Report, the Public Health Advisory Commission recommended that a permanent public health advisory council be created to provide advice in implementing the recommendations of the Public Health Advisory Commission, to serve as a forum to address emerging state and local public health threats, and to provide state officials and external public health stakeholders the opportunity to collaborate on public health responses; and

WHEREAS, it is necessary to create a permanent advisory council to ensure the successful implementation of the recommendations set forth in the Report; and

WHEREAS, addressing emerging state and local public health threats requires the collaboration of state officials and external public health stakeholders;

NOW, THEREFORE, I, Richard D. Snyder, Governor of the state of Michigan by virtue of the powers and authority vested in the Governor by the Michigan Constitution of 1963 and Michigan law, order the following:

437 2017 MR 22 – December 15, 2017

I. CREATION OF THE PUBLIC HEALTH ADVISORY COUNCIL

A. The Public Health Advisory Council (“the Council”) is established in the Department of Health and Human Services (“the Department”).

B. The Council shall be composed of twenty-six (26) members appointed as follows:

1. The Chief Medical Executive, head of the Office of Chief Medical Executive established by Executive Order 2016-19, shall be a voting member and shall serve as the chairperson of the Council.

2. The Governor shall appoint twenty (20) voting members to the Council serving at the pleasure of the Governor.

3. The following five (5) department heads or their designees from within their respective departments who shall serve as non-voting, ex officio members:

 The Department of Agriculture and Rural Development  The Department of Environmental Quality  The Department of Health and Human Services  The Department of Licensing and Regulatory Affairs  The Department of State Police, or a designee from the Division of Emergency Management and Homeland Security, within the Department of State Police.

C. Of the initial appointments made by the Governor, seven (7) shall be for 1-year terms, six (6) shall be for 3-year terms, and seven (7) shall be for 4-year terms. Thereafter, all members shall be appointed to 4-year terms. Members of the Council may be reappointed to successive terms.

D. A vacancy on the Council shall be filled in the same manner as the original appointment.

E. The Governor shall, to the extent practicable, appoint members from all regions of Michigan to achieve geographic diversity.

F. The nineteen voting members of the Council appointed by the Governor shall include at least one member representing each of the following categories:

 A physician  A registered nurse  A licensed pharmacist  A veterinarian  A representative of a nationally-accredited medical school  A representative of a school of public health from an institution of higher education in the state  A local public health official  A person with experience in hospital administration  A local director of public works  An epidemiologist  A toxicologist  A food safety expert  An expert in environmental health; and

438 2017 MR 22 – December 15, 2017  A representative of a non-profit health or environmental organization.

II. CHARGE TO THE COUNCIL

A. The Council shall act in an advisory capacity to the Governor and the Director of the Department, and shall do all the following:

1. Provide guidance and advice about emerging issues in public health, or other public health matters, as deemed appropriate, or as requested by the Governor or the Director of the Department.

2. Develop and propose an action plan for implementing the recommendations set forth in the Report.

3. Monitor the effectiveness of Michigan’s public health response system, particularly in circumstances in which multiple government agencies are required to work in collaboration in response to a public health threat.

4. Review multiagency efforts that support a One-Health approach (human health/animal health interface) to reduce duplication of effort by involved agencies and to form a unified communications strategy when addressing public health concerns.

B. The Council shall issue an annual report to the Governor outlining the status of its progress addressing the charges set forth in this section and providing recommendations of further actions necessary to improve Michigan’s public health delivery system.

III. OPERATIONS OF THE COUNCIL

A. The Council shall be assisted by personnel from the Department.

B. The Council may select from among its members a Vice Chairperson.

C. The Council shall meet at the call of the Chairperson, at least twice per year, and as otherwise may be provided in procedures adopted by the Council, to review multi-agency Emerging Public Health Issue Notifications for the relevant period and provide guidance and advice for enhanced future responses.

D. The Council may establish workgroups or committees assigning Council members to and inviting public participation on these workgroups or committees as the Council deems necessary. The Council may adopt, reject, or modify recommendations made by the workgroups or committees.

E. A majority of the voting members of the Council serving constitutes a quorum for the transaction of the Council's business, notwithstanding the existence of one or more vacancies. The Council shall act by majority vote of its present and voting members.

F. The Council shall adopt procedures consistent with Michigan law and this Order governing its organization and operations.

G. The Council may, as appropriate, make inquiries, studies, investigations, hold hearings, and receive comments from the public. Subject to the approval of the Director of the Department, the Council may consult with outside experts to perform its duties, including, but not limited to, experts in the private sector, government agencies, institutions of higher education, and the nonprofit sector.

H. To gather information, as appropriate, the Council may hold public hearings. 439 2017 MR 22 – December 15, 2017

I. Members of the Council shall serve without compensation. Subject to the approval of the Director of the Department and available funding, members of the Council may receive reimbursement for necessary travel and expenses according to relevant statutes and the rules and procedures of the Department.

J. The Council may accept grants of funds, donations of funds, property, labor, services, or other things of value from any public or private agency or person. Any donations shall be expended in accordance with applicable laws, rules, and procedures.

K. A member of the Council shall not use for personal gain information obtained by the member while performing business of the Council, nor shall a member of the Council disclose confidential information obtained by the member while conducting Council business, except as necessary to perform Council business.

L. Members of the Council, staff, or contractors shall refer all legal, legislative, and media contact relating to Council actions or activities to the Department.

440 2017 MR 22 – December 15, 2017

IV. MISCELLANEOUS

A. The Public Health Advisory Commission created by Executive Order 2016-19 is abolished, its task having been completed.

B. Nothing in this Order is intended to modify the important roles played by the Michigan Association for Local Public Health (MALPH) or the Michigan Association of Local Environmental Health Administrators (MALEHA). State public health leaders should continue to meet and actively engage with MALPH and MALEHA on a regular basis, as appropriate.

C. Any suit, action, or other proceeding lawfully commenced prior to the effective date of this Order shall not abate by reason of the taking effect of this Order. Any lawfully commenced suit, action, or other proceeding may be maintained by, against, or before the appropriate successor of any entity affected by this Order.

D. The invalidity of any portion of this Order shall not affect the validity of the remainder of the Order, which may be given effect without any invalid portion. Any portion of this Order found invalid by a court or other entity with proper jurisdiction shall be severable from the remaining portions of this Order.

This Order shall become effective upon filing.

Given under my hand and the Great Seal of the state of Michigan this ______day of November, in the Year of our Lord Two Thousand and Seventeen.

______RICHARD D. SNYDER GOVERNOR

BY THE GOVERNOR:

______SECRETARY OF STATE

441 2017 MR 22 – December 15, 2017

EXECUTIVE ORDERS

EXECUTIVE ORDER No. 2017 - 11

CLEANUP OF OBSOLETE AND OUTDATED BOARDS, COMMISSIONS, AND COUNCILS

RESCISSION OF EXECUTIVE ORDERS 1993-16, 1993-18, 1993-23, 1995-20, 2000-6, 2004-1, 2007-42, 2007-50, 2007-51, 2007-52, 2008-18, 2009-1, 2009-19, 2009-35, 2009-46, 2010-5, 2010-19, 2011-10, 2011-12, 2012-3, 2016-5, 2016-6, 2016-14, and 2016-16

DEPARTMENT OF CIVIL RIGHTS DEPARTMENT OF ENVIRONMENTAL QUALITY DEPARTMENT OF HEALTH AND HUMAN SERVICES DEPARTMENT OF LICENSING AND REGULATORY AFFAIRS DEPARTMENT OF NATURAL RESOURCES MICHIGAN STATE HOUSING DEVELOMENT AUTHORITY OFFICE OF PERFORMANCE AND TRANSFORMATION STATE BUDGET OFFICE

WHEREAS, Section 1 of Article V of the Michigan Constitution of 1963 vests the executive power of the state of Michigan in the Governor; and

WHEREAS, Section 8 of Article V of the Michigan Constitution of 1963 provides that each principal department shall be under the supervision of the Governor unless otherwise provided by the Constitution; and

WHEREAS, governors of this state have created, by executive order and other means, numerous boards, commissions, councils, and other similar executive bodies to address specific concerns or fill specific purposes that no longer exist or that no longer require ongoing attention; and

WHEREAS, many prior executive orders have established timelines that have since passed or have established goals that have since been met; and

WHEREAS, abolishing outdated or obsolete boards, commissions, councils, and other similar executive bodies, and rescinding outdated and obsolete executive orders, will help to avoid possible confusion about the ongoing nature of functions and entities that no longer exist or no longer serve their intended purposes; and

WHEREAS, the Office of Performance and Transformation, which includes the Office of Regulatory Reinvention, was established by Executive Order 2016-4 to undertake a continuous and systematic review of the state’s regulatory, business, and customer service environments and processes; and

WHEREAS, as part of its mission to optimize government services, the Office of Performance and Transformation has identified certain outdated or obsolete bodies, functions, and orders that should be abolished or rescinded to simplify state government.

NOW, THEREFORE, I, Richard D. Snyder, Governor of the state of Michigan, by virtue of the powers and authority vested in the Governor by the Michigan Constitution of 1963 and Michigan law, order the following: I. RESCISSION OF OUTDATED OR OBSOLETE EXECUTIVE ORDERS 442 2017 MR 22 – December 15, 2017 A. Executive Order 1993-16, which established the K I Sawyer Air Force Base Conversion Authority within the Executive Office is rescinded. B. Executive Order 1993-18, which created the Michigan Justice Statistics Center in the Executive Office, and Executive Order 1995-20, which re-created the Michigan Justice Statistics Center within the Executive Office, are rescinded. C. Executive Order 1993-23, which transferred the Michigan Martin Luther King, Jr. Holiday Commission to the Department of Civil Rights, is rescinded, and the Michigan Martin Luther King, Jr. Holiday Commission is abolished. D. Executive Order 2000-6, which established the e-Michigan Office and the e-Michigan Advisory Council within the Executive Office, is rescinded. E. Executive Order 2004-1, which established the Medicaid Long-Term Care Task Force within the Department of Community Health (now the Department of Health and Human Services), is rescinded. F. Executive Order 2007-42, which created the Michigan Climate Action Council within the Department of Environmental Quality, is rescinded. G. Executive Order 2007-50, which created the Idlewild Centennial Commission within the Department of History, Arts, and Libraries (and later transferred to the Michigan State Housing Development Authority by Executive Order 2009-36), is rescinded. H. Executive Order 2007-51, which created the Michigan Commission on the Commemoration of the Bicentennial of the within the Department of History, Arts, and Libraries (and later transferred to the Department of Natural Resources by Executive Order 2009-36), is rescinded. I. Executive Order 2007-52, which ordered that the Michigan Historical Commission shall constitute an advisory body within the Department of History, Arts, and Libraries (later transferred to the Department of Natural Resources by Executive Order 2009-36) to recognize the sesquicentennial of the Civil War, is rescinded. J. Executive Order 2008-18, which created the Michigan Prisoner Reentry Advisory Council within the Department of Corrections, is rescinded. K. Executive Order 2009-1, which created the Great Lakes Wind Council within the Department of Energy, Labor, and Economic Growth (now the Department of Licensing and Regulatory Affairs), and Executive Orders 2009-19 and 2009-46, which amended Executive Order 2009-1, are rescinded. L. Executive Order 2009-35, which created the Michigan Economic Recovery Office and the Michigan Economic Oversight Board within the Executive Office, and Executive Order 2010-19, which transferred the Michigan Economic Recovery Office to the State Budget Office, are rescinded. M. Executive Order 2010-5, which extended the date for the Michigan Center for Innovation and Reinvention Board to complete its work to July 1, 2010, is rescinded and the Michigan Center for Innovation and Reinvention Board, created within the Department of Natural Resources by Executive Order 2009-36, is abolished. N. Executive Order 2011-10, which established the Michigan State Parks and Outdoor Recreation Blue Ribbon Panel, is rescinded. O. Executive Order 2011-12, which established the Indigent Defense Advisory Commission, is rescinded. P. Executive Order 2016-5, which created the 21st Century Infrastructure Commission within the Executive Office, is rescinded. 443 2017 MR 22 – December 15, 2017 Q. Executive Order 2016-6, which created the 21st Century Education Commission within the Executive Office, and Executive Order 2016-16, which amended Executive Order 2016-6, are rescinded R. Executive Order 2016-14, which created the Building the 21st Century Economy Commission within the Executive Office, is rescinded. II. ABOLISHMENT OF OTHER EXECUTIVE BODIES THAT HAVE COMPLETED THEIR TASKS A. The Air Quality Division Workgroup created within the Department of Environmental Quality is abolished, its work having been completed. B. The Better Off Working Workgroup created with the Department of Human Services (now the Department of Health and Human Services) is abolished, its work having been completed. C. The DNR-Managed Public Land Strategy Advisory Committee created within the Department of Natural Resources is abolished, its work having been completed. D. The independent Flint Water Advisory Task Force is abolished, its work having been completed. E. The Michigan Prescription Drug and Opioid Abuse Task Force created within the Executive Office is abolished, its work having been completed. F. The Michigan Special Election Reform Task Force created within the Executive Office is abolished, its work having been completed. G. The Third-Grade Reading Workgroup created within the Executive Office is abolished, its work having been completed. H. The Water Use Advisory Council created within the Department of Environmental Quality is abolished, its work having been completed. III MISCELLANEOUS A. Any remaining records possessed by any executive body subject to this Order shall be maintained and disposed of by the department within which the executive body was housed according to the department’s applicable record retention rules. B. Any rules, orders, contracts, and agreements relating to the assigned functions lawfully adopted prior to the effective date of this Order shall continue to be effective until revised, amended, or rescinded. C. Any suit, action, or other proceeding lawfully commenced by, against, or before any entity affected by this Order shall not abate by reason of the taking effect of this Order. Any suit, action, or other proceeding may be maintained by, against, or before the appropriate successor of any entity affected by this Order. D. The invalidity of any portion of this Order shall not affect the validity of the remainder of the Order, which may be given effect without any invalid portion. Any portion of this Order found invalid by a court or other entity with proper jurisdiction shall be severable from the remaining portions of this Order. This Order shall become effective upon filing. Given under my hand and the Great Seal of the state of Michigan this ______day of ______, in the Year of our Lord Two Thousand Seventeen.

444 2017 MR 22 – December 15, 2017 ______RICHARD D. SNYDER GOVERNOR

BY THE GOVERNOR:

______SECRETARY OF STATE

445 2017 MR 22 – December 15, 2017

MICHIGAN ADMINISTRATIVE CODE TABLE (2017 SESSION)

MCL 24.208 states in part:

“Sec. 8. (1) The Office of Regulatory Reform shall publish the Michigan register at least once each month. The Michigan register shall contain all of the following:

* * *

“(2) The office of regulatory reform shall publish a cumulative index for the Michigan register.”

The following table cites administrative rules promulgated during the year 2017, and indicates the effect of these rules on the Michigan Administrative Code (1979 ed.).

446 2017 MR 22 – December 15, 2017 MICHIGAN ADMINISTRATIVE CODE TABLE (2017 RULE FILINGS)

2017 2017 2017 MR MR MR R Number Action Issue R Number Action Issue R Number Action Issue 11.101 R 4 257.123 R 2 281.770.1 R 19 11.102 R 4 257.124 R 2 281.770.3 R 19 11.103 R 4 257.124a R 2 285.203.1 R 1 11.104 R 4 257.124b R 2 285.547.1 R 12 11.105 R 4 257.125 R 2 299.44 * 20 11.106 R 4 257.126 R 2 299.49 * 20 11.107 R 4 257.131 R 2 299.9102 * 6 11.108 R 4 257.132 R 2 299.9103 * 6 11.109 R 4 257.133 R 2 299.9104 * 6 11.110 R 4 257.134 R 2 299.9105 * 6 11.111 R 4 257.135 R 2 299.9107 * 6 11.112 R 4 257.136 R 2 299.9108 * 6 11.113 R 4 257.137 R 2 299.9109 * 6 11.114 R 4 257.141 R 2 299.9202 * 6 11.115 R 4 257.142 R 2 299.9203 * 6 11.116 R 4 257.143 R 2 299.9204 * 6 29.1701 * 6 257.144 R 2 299.9205 * 6 29.1702 * 6 257.145 R 2 299.9206 * 6 29.1703 * 6 257.151 R 2 299.9217 * 6 29.1704 * 6 257.152 R 2 299.9220 * 6 29.1705 * 6 257.153 R 2 299.9224 * 6 29.1706 * 6 257.154 R 2 299.9225 * 6 29.1707 * 6 257.155 R 2 299.9226 * 6 29.1708 * 6 257.156 R 2 299.9227 * 6 29.1710 * 6 257.157 R 2 299.9231 * 6 29.1721 * 6 257.161 R 2 299.9304 * 6 29.1723 * 6 257.162 R 2 299.9307 * 6 29.1731 * 6 257.163 R 2 299.9409 * 6 29.1733 * 6 257.164 R 2 299.9502 * 6 29.1722 R 6 257.165 R 2 299.9519 * 6 29.1732 R 6 257.166 R 2 299.9525 * 6 257.101 R 2 257.166a R 2 299.9607 * 6 257.102 R 2 257.167 R 2 299.9608 * 6 257.103 R 2 257.168 R 2 299.9612 * 6 257.104 R 2 257.169 R 2 299.9621 * 6 257.111 R 2 257.17 R 2 299.9629 * 6 257.112 R 2 257.171 R 2 299.9801 * 6 257.121 R 2 257.172 R 2 299.9808 * 6 257.122 R 2 257.173 R 2 299.9822 * 6 (* Amendment to Rule, A Added Rule, N New Rule, R Rescinded Rule)

447 2017 MR 22 – December 15, 2017

2017 2017 2017 MR MR MR R Number Action Issue R Number Action Issue R Number Action Issue 299.11001 * 6 325.13105 * 18 325.13309 A 18 299.11002 * 6 325.13106 * 18 325.13110 R 18 299.11003 * 6 325.13107 * 18 325.13202 R 18 299.11004 * 6 325.13108 * 18 325.13210 R 18 299.11005 * 6 325.13109 * 18 325.13212 R 18 299.11006 * 6 325.13111 * 18 325.13543 R 18 299.9232 A 6 325.13201 * 18 325.21105 * 5 299.9233 A 6 325.13203 * 18 325.51101 * 4 299.9234 A 6 325.13204 * 18 325.51101a * 4 299.9230 R 6 325.13205 * 18 325.51102 * 4 318.111 * 21 325.13207 * 18 325.51103 * 4 318.145c * 21 325.13208 * 18 325.51104 * 4 318.146 * 21 325.13211 * 18 325.59001 A 4 323.1701 * 12 325.13213 * 18 325.59005 A 4 323.1714 * 12 325.13301 * 18 325.59010 A 4 324.20402 * 5 325.13302 * 18 325.59012 A 4 324.20506 * 5 325.13303 * 18 325.59015 A 4 324.20602 * 5 325.13304 * 18 325.60151 * 4 324.21102 * 5 325.13305 * 18 325.60151a * 4 325.125 * 10 325.13306 * 18 325.60152 * 4 325.126 * 10 325.13307 * 18 325.60155 * 4 325.127 * 10 325.13501 * 18 325.60156 * 4 325.128 * 10 325.13503 * 18 325.60157 * 4 325.129 * 10 325.13505 * 18 325.60158 * 4 325.130 * 10 325.13507 * 18 325.60159 * 4 325.131 * 10 325.13509 * 18 325.60160 * 4 325.132 * 10 325.13511 * 18 325.60161 * 4 325.133 * 10 325.13513 * 18 325.63001 * 4 325.134 * 10 325.13515 * 18 325.63002 * 4 325.135 * 10 325.13517 * 18 325.63049 R 4 325.136 * 10 325.13519 * 18 325.69001 A 4 325.137 * 10 325.13521 * 18 325.69005 A 4 325.138 * 10 325.13523 * 18 325.69010 A 4 325.1922 * 10 325.13525 * 18 325.69012 A 4 325.1923 * 10 325.13527 * 18 325.69015 A 4 325.1944 * 10 325.13529 * 18 336.1610 * 6 325.13101 * 18 325.13541 * 18 336.1611 * 6 325.13102 * 18 325.13112 A 18 336.1612 * 6 325.13104 * 18 325.13308 A 18 336.1613 * 6 (* Amendment to Rule, A Added Rule, N New Rule, R Rescinded Rule)

448 2017 MR 22 – December 15, 2017 2017 2017 2017 MR MR MR R Number Action Issue R Number Action Issue R Number Action Issue 336.1614 * 6 338.1236 * 20 340.237 R 2 336.1618 * 6 338.1237 * 20 340.238 R 2 336.1619 * 6 338.1215 A 20 340.1101 R 2 336.1622 * 6 338.1251 A 20 340.1102 R 2 336.1625 * 6 338.1252 A 20 340.1103 R 2 336.1627 * 6 338.1238 R 20 340.1104 R 2 336.1628 * 6 338.1378 A 18 340.1105 R 2 336.1629 * 6 338.1301 * 18 340.1106 R 2 336.1632 * 6 338.1309 * 18 340.1107 R 2 336.1651 * 6 338.1317 * 18 340.1301 R 2 336.1660 * 6 338.1321 * 18 340.1302 R 2 336.1661 * 6 338.1325 * 18 340.1303 R 2 338.471b A 21 338.1337 * 18 340.1304 R 2 338.701 * 5 338.1341 * 18 340.1305 R 2 338.705 * 5 338.1345 * 18 338.7001 * 4 338.709 * 5 338.1349 * 18 338.7001a * 4 338.711 * 5 338.1357 * 18 338.7002 * 4 338.713 * 5 338.1369 * 18 338.7003 * 4 338.715 * 5 338.1305 R 18 338.7126 A 1 338.717 * 5 338.1313 R 18 338.8102 A 1 338.719 * 5 338.1329 R 18 338.8103 * 21 338.723 * 5 338.1333 R 18 338.8108 R 21 338.727 * 5 338.1353 R 18 338.8109 * 21 338.704 A 4 338.1365 R 18 338.8110 * 21 338.731 A 5 338.1373 R 18 338.8111 * 21 338.733 A 5 338.1377 R 18 338.8113 * 21 338.703 R 5 338.2101 * 6 338.8114 R 21 338.721 R 5 338.2179 * 6 338.8126 * 21 338.725 R 5 340.71 R 2 338.8127 * 21 338.1223 * 20 340.72 R 2 338.8128 * 21 338.1223a * 20 340.73 R 2 338.8129 R 21 338.1224 * 20 340.74 R 2 338.8130 R 21 338.1226 * 20 340.75 R 2 338.8110 * 1 338.1227 * 20 340.231 R 2 338.8111 * 1 338.1229 * 20 340.232 R 2 338.8127 * 1 338.1233 * 20 340.233 R 2 338.8131 R 1 338.1233a * 20 340.234 R 2 338.8132 R 1 338.1234 * 20 340.235 R 2 338.8133 R 1 338.1235 * 20 340.236 R 2 338.8134 R 1 (* Amendment to Rule, A Added Rule, N New Rule, R Rescinded Rule)

449 2017 MR 22 – December 15, 2017

2017 2017 2017 MR MR MR R Number Action Issue R Number Action Issue R Number Action Issue 338.8135 R 1 338.10401 * 1 339.22205 R 6 338.8136 R 1 338.10401a A 1 339.22207 R 6 338.5101 * 1 338.10401b A 1 339.22211 R 6 338.5102 * 1 338.10403 * 1 339.22215 R 6 338.5115 * 1 338.10404 * 1 339.22301 R 6 338.5405 * 1 338.10404a A 1 339.22309 R 6 338.10101 * 1 338.10405 * 1 339.22310 R 6 338.10102 R 1 338.10405a A 1 339.22311 R 6 338.10103 R 1 338.10405b A 1 339.22317 R 6 338.10105 A 1 338.10601 * 1 339.22319 R 6 338.10201 R 1 338.10602 * 1 339.22323 R 6 338.10203 * 1 338.10603 R 1 339.22325 R 6 338.10204 * 1 338.10701 * 1 339.22327 R 6 338.10206 * 1 338.10702 * 1 339.22329 R 6 338.10207 A 1 338.10703 * 1 339.22339 R 6 338.10208 A 1 338.10704 * 1 339.22401 R 6 338.10209 A 1 338.11123 A 1 339.22405 R 6 338.1021 A 1 338.11202 * 1 340.1121 * 5 338.10211 A 1 338.11301 * 1 340.1122 * 5 338.10212 A 1 338.11303 * 1 408.11402 A 4 338.10213 A 1 338.11307 * 1 408.11407 * 4 338.10301 * 1 338.11501 * 1 408.11412 * 4 338.10302 R 1 338.11503 R 1 408.11421 * 4 338.10303 * 1 338.11505 * 1 408.11422 * 4 338.10303a A 1 338.11507 R 1 408.11425 * 4 338.10303b A 1 338.11509 R 1 408.11433 * 4 338.10303c A 1 338.11511 R 1 408.11445 * 4 338.10305 * 1 338.11515 * 1 408.15102 * 4 338.10305a A 1 338.11519 * 1 408.15111 * 4 338.10305b A 1 338.11523 * 1 408.15114 * 4 338.10305c A 1 338.11601 * 1 408.15117 * 4 338.10306 * 1 338.11602 * 1 408.15120 * 4 338.10307 * 1 338.11603 * 1 408.15125 * 4 338.10308 * 1 338.11605 * 1 408.15127 * 4 338.10309 * 1 338.11701 * 1 408.15130 * 4 338.1031 * 1 338.11704 * 1 408.15131 * 4 338.10310a A 1 338.11704b * 1 408.15144 * 4 338.10311 * 1 338.11704c * 1 408.15146 * 4 338.10312 * 1 338.11705 * 1 408.15148 * 4 (* Amendment to Rule, A Added Rule, N New Rule, R Rescinded Rule)

450 2017 MR 22 – December 15, 2017 2017 2017 2017 MR MR MR R Number Action Issue R Number Action Issue R Number Action Issue 408.15150 * 4 418.10909 * 1 460.2403 R 4 408.15165 * 4 418.10915 * 1 460.2404 R 4 408.15166 * 4 418.10922 * 1 460.2405 R 4 408.15117a A 4 418.10925 * 1 460.2406 R 4 408.15117b A 4 418.101002 * 1 460.2407 R 4 408.15146a A 4 418.101003a * 1 460.2408 R 4 408.15146b A 4 418.101004 * 1 460.2409 R 4 408.19001 * 4 418.101005 * 1 460.2410 R 4 408.19002 * 4 418.101007 * 1 460.2411 R 4 408.19101 * 4 418.101008a * 1 460.2412 R 4 408.19102 * 4 418.101023 * 1 460.2413 R 4 408.19103 * 4 418.101101 * 1 460.2414 R 4 408.30401 * 20 418.101304 * 1 490.111 R 20 408.30757 * 12 418.101503 * 1 490.112 R 20 408.31087 * 10 436.1117 R 9 490.115 R 20 408.31087a * 10 436.1601 * 5 490.116 R 20 408.31088 * 10 436.1609 * 5 567.1 A 5 408.31090 * 10 436.1611 * 5 567.2 A 5 408.31089 R 10 436.1613 * 5 567.3 A 5 408.31087b A 10 436.1617 * 5 567.4 A 5 408.31088a A 10 436.1621 * 5 567.5 A 5 408.31091 A 10 436.1631 * 5 567.6 A 5 408.31092 A 10 436.1641 * 5 567.7 A 5 408.31092a A 10 436.1605 R 5 567.8 A 5 408.31093 A 10 436.1607 R 5 567.9 A 5 408.31098b A 10 436.1615 R 5 567.10 A 5 408.31098c A 10 436.1705 * 5 567.11 A 5 418.10106 * 1 436.1708 * 5 567.12 A 5 418.10107 * 1 436.1719 * 5 567.13 A 5 418.10108 * 1 436.1720 * 5 567.14 A 5 418.10109 * 1 436.1725 * 5 567.15 A 5 418.10111 * 1 436.1735 * 5 418.10119 R 1 436.1701 A 5 418.10202 * 1 436.1704 A 5 418.10209 * 1 436.1702 R 5 418.10505 * 1 436.1703 R 5 418.10901 * 1 436.1712 R 5 418.10904 * 1 460.2401 R 4 418.10907 R 1 460.2402 R 4 (* Amendment to Rule, A Added Rule, N New Rule, R Rescinded Rule)

451 2017 MR 22 – December 15, 2017

CUMULATIVE INDEX A ARGICULTURE AND RURAL DEVELOPMENT, DEPARTMENT OF Repeal Repeal PA 257 of 2016 Regulation 203 Animal remedies (2017-1) Repeal PA 210 of 2015 Regulation No. 547. Hazardous Substances (2017-11)

Regulation No. 202 Fresh Fruits and Vegetables Containing Poisonous Spray Residue (2017-14)

ATTORNEY GENERAL, DEPARTMENT OF Opinions Aquaculture not permitted in the Michigan waters of the Great Lakes AG Opinion No. 7293 (2017-1)

Validity of local ordinance raising the age of person able to purchase tobacco products to the age of 21 AG Opinion No. 7294 (2017-3)

Compatibility of Offices of Village President and Village Manager AG Opinion No. 7295 (2017-5)

Reduction of state school aid for use of certain mascots or logos AG Opinion No. 7296 (2017-13)

County commissioner and member of board of review AG Opinion No. 7297 (2017-16)

Duplicate certificates of marriage as proof of marriage AG Opinion No. 7298 (2017-19)

Appropriations and expenditures from Michigan Natural Resources Trust Fund AG Opinion No. 7299 (2017-20)

E 452 2017 MR 22 – December 15, 2017 EDUCATION, DEPARTMENT OF Certification and Licensure of School Counselors (2017-21) Education of Pregnant and Parenting Students (2017-5) Eye Protection Devices (2017-2) Personality Test (2017-2) Release of Children for Attending Religious Instruction Classes (2017-2) School Administrator Certification Code (2017-21) School Administrator Continuing Education(2017-21) School Psychologist Certification Code (2017-21) Teacher Certification Code (2017-21) Teacher and School Administrator Evaluation Tools (2017-6) Use of School Bus for Transportation of Senior Citizens (2017-2)

E ENVIRONMENTAL QUALITY, DEPARTMENT OF EMERGENCY RULE Establishment of Cleanup Criteria for 1, 4-Dioxane (2017-8)

Environmental Contamination Response Activity (2017-20) Environmental Contamination Response Activity (2017-22*) Hazardous Waste Management (2017-6) Part 6. Emission Limitations and Prohibitions Existing Sources of Volatile Organic Compound Emissions (2017-6) Part 17. Soil Erosion and Sedimentation Control (2017-12)

EXECUTIVE OFFICE PROCLAMATION Request for Extension of Declaration of Emergency (2017-2)

Executive Order No. 1 -2017 (2017-5) No. 2 -2017 (2017-5) No. 3 -2017 (2017-7) No. 4 -2017 (2017-11) No. 5 -2017 (2017-12) No. 6 -2017 (2017-16) No. 7 -2017 (2017-19) No. 8 -2017 (2017-20) No. 9 -2017 (2017-20) No. 10 -2017 (2017-22) No. 11 -2017 (2017-22)

H HEALTH AND HUMAN SERVICES, DEPARTMENT OF Certificate of Need Nursing Home and Hospital Long Term Care Unit Beds (2017-18) Surgical Services (2017-22)

Birth Defect Reporting (2017-16*) Crime Victims Services – General Rules (2017-19*) Statewide Trauma System (2017-10) 453 2017 MR 22 – December 15, 2017

I INSURANCE AND FINANCIAL SERVICES, DEPARTMENT OF Certificates of No-Fault Self-Insurance (2017-14*) Credit Union Rules (2017-20) Replacement of Life Insurance Policies (2017-12)

L LICENSING AND REGULATORY AFFAIRS, DEPARTMENT OF CORRECTIONS Administrative Standard Part 11 Recording and Reporting of Occupational Injury and Illnesses (2017-6) Construction Safety Standard Part 8 Handling and Storage of Materials (2017-5) Construction Safety Standard Part 12. Scaffolds and Scaffold Platforms (2017-9) General Industry Safety Standard Part 14 Conveyors (2017-6) General Industry Safety Standard Part 21 Powered Industrial Trucks (2017-6) General Industry Safety Standard Part 24 Mechanical Power Presses (2017-5) Occupational Health Standard Part 590 Silica in General Industry (2017-9)

EMERGENCY RULE Standing Order for Dispensing Opioid Antagonist (2017-10) Extension of Emergency Rule Standing Order for Dispensing Opioid Antagonist (20147-22) Construction Code – Part 4. Building Code (2017-11) Medical Marihuana Facilities Licensing Act (20174-22)

REPEAL Repeal – Real Estate Broker Rules (2017-6) Repeal - Residential Conservation Program Standards (2017-5)

A Standing Order for Dispensing Opioid Antagonist (2017-18*) Architects – General Rules (2017-14*) Athletic Training – General Rules (2017-1 Beer – General Rules (2017-5) Billing Practices Applicable to Non-Residential Electric and Gas Customers (2017-22) Board of Athletic Trainers (2017-18) Board of Physical Therapy General Rules (2017-1) Board of Psychology – General Rules (2017-6) Board of Nursing - General Rules (2017-1) (2017-16*) Consumer Standards and Billing Practices for Electric And Gas Residential Service (2017-22) Cosmetology (2017-6) Dentistry - General Rules (2017-1) Electrical Supply and Communication Lines and Associated Equipment (2017-22) Employment Relations Commission – General Rules (2017-14) General Rules Public Health Code (2017-4) Homes for the Aged (2017-10) Hospice and Hospice Residences (2017-18) Licensing Qualifications -Retail license; Participating agreement (2017-9) Licensing Qualifications - - SDD License; prohibited issuance or transfer (2017-15*) Massage Therapy – General Rules (2017-5) Nursing Homes and Nursing Care Facilities (2017-5) 454 2017 MR 22 – December 15, 2017 Occupational Therapy (2017-20) Part 1. General Provisions (2017-17*) Part 2. Walking Working Surfaces (2017-17*) Part 3. Fixed Ladders (2017-17*) Part 4 Portable Ladders (2017-17*) Part 4. Building Code (2017-13*) (2017-20) Part 5. Powered Platforms for Building Maintenance (2017-21*) Part 7. Plumbing Code (2017-12) Part 10a Michigan Energy Code (2017-10) Part 14 – Conveyors GI (2017-4) Part 18. Overhead and Gantry Cranes (2017-17*) Part 21. Powered Industrial Trucks (2017-17*) Part 25. Manlifts (2017-17*) Part 27. Woodworking Machinery – GI (2017-20*) Part 30 – Telecommunications for Construction (2017-2) Part 33. Personal Protective Equipment (2017-17*) Part 50 – Telecommunications for General Industry (2017-2) Part 50. Telecommunications (2017-17*) Part 51 – Logging GI (2017-4) Part 52. Sawmills – GI (2017-20*) Part 58. Aerial Work Platforms – GI (2017-20*) Part 63. Pulp, Paper, and Paperboard Mills (2017-22*) Part 86. Electric Power Generation, Transmission, and Distribution (2017-21*) Part 90 – Permit Required Confined Spaces GI (2017-4) Part 91 – Process Safety Management of Highly Hazardous Chemicals GI (2017-4) Part 94 Textiles (2017-22*) Part 301 – Air Contaminants for GI (2017-4) Part 340 Beryllium (2017-17*) Part 490 – Permit Required Confined Spaces OH (2017-4) Part 590 – Silica in GI (2017-4) Part 601 – Air Contaminants for Construction OH (2017-4) Part 690 – Silica in Construction OH (2017-4) Penal Facilities Fire Safety Rules (2017-6) Pharmacy - General Rules (2017-21) Podiatric Medicine and Surgery - General Rules (2017-21) Public Health Code – General Rules (2107-16*) Real Estate Brokers and Salesperson – General Rules (2017-18*) Responsibilities of Providers of Basic Local Exchange Service that Cease to Provide the Service (2017-12*) Veterinary Medicine – General Rules (2017-16*) Veterinary Technician Licensure (2017-16*) Wine – General Rules (2017-5) Workers’ Compensation Health Care Services (2017-19*)

N NATURAL RESOURCES, DEPARTMENT OF Mackinac Island State Park Commission – General Rules (2017-21) Pure Michigan Trail, Water Trail, and Trail Town Designation (2017-22) Special Local Watercraft Controls (2017-19*) S STATE, DEPARTMENT OF Assigned Claims Plan (2017-4) 455 2017 MR 22 – December 15, 2017 Automotive Regulations (2017-2)

STATE, DEPARTMENT OF Repeal Michigan Uniform Traffic Code Test for Breath Alcohol Repeal PA 61 of 2017 (2017-15)

Alcohol and Drug Testing of Biological and Nonbiological Specimens (2017-21) Test for Breath Alcohol (2017-15*) T TRANSPORTATION, DEPARTMENT OF Automotive Regulation – General Rules (2017-3)

TREASURY, DEPARTMENT OF Audit Standards for Examinations under the Uniform Unclaimed Property Act (2017-5) Charitable Gaming (2017-20*) Lottery Rules (2017-20*) Taxpayer Bill of Rights (2017-21*)

456 2017 MR 22 – December 15, 2017

ADMINISTRATIVE RULES ENROLLED SENATE AND HOUSE BILLS SIGNED INTO LAW OR VETOED (2017 SESSION)

Mich. Const. Art. IV, §33 provides: “Every bill passed by the legislature shall be presented to the governor before it becomes law, and the governor shall have 14 days measured in hours and minutes from the time of presentation in which to consider it. If he approves, he shall within that time sign and file it with the secretary of state and it shall become law . . . If he does not approve, and the legislature has within that time finally adjourned the session at which the bill was passed, it shall not become law. If he disapproves . . . he shall return it within such 14-day period with his objections, to the house in which it originated.”

Mich. Const. Art. IV, §27, further provides: “No act shall take effect until the expiration of 90 days from the end of the session at which it was passed, but the legislature may give immediate effect to acts by a two-thirds vote of the members elected to and serving in each house.”

MCL 24.208 states in part:

“Sec. 8. (1) The Office of Regulatory Reform shall publish the Michigan register at least once each month. The Michigan register shall contain all of the following:

* * *

(b) On a cumulative basis, the numbers and subject matter of the enrolled senate and house bills signed into law by the governor during the calendar year and the corresponding public act numbers.

(c) On a cumulative basis, the numbers and subject matter of the enrolled senate and house bills vetoed by the governor during the calendar year.”

457 2017 Michigan Public Acts Table

Legislative Service Bureau December 12, 2017 Legal Division, Statutory Compiling and Law Publications Unit 124 W. Allegan, Lansing, MI 48909 Through Act 193 of 2017

ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 1 0016 Yes 3/30 3/31 6/29/17 Corrections; parole; parole sanctions certainty act; create. (Sen. J. Proos)

2 0005 Yes 3/30 3/31 6/29/17 Criminal procedure; other; certain definitions and requirements for the manner in which data regarding recidivism are collected; provide for in the code of criminal procedure. (Sen. J. Proos)

3 0006 Yes 3/30 3/31 6/29/17 Corrections; alternatives; certain definitions and requirements for the manner in which data regarding recidivism are collected; provide for in the community corrections act. (Sen. T. Schuitmaker)

4 0007 Yes 3/30 3/31 6/29/17 Corrections; other; definitions of certain terms and the manner in which data regarding recidivism are collected; provide for in the code of corrections. (Sen. M. Knollenberg)

5 0008 Yes 3/30 3/31 6/29/17 Corrections; parole; use of evidence-based supervision practices; require. (Sen. P. MacGregor)

6 0009 Yes 3/30 3/31 6/29/17 Corrections; other; reentry services provided to prisoners housed in correctional institutions by certain organizations; require the department to develop screening and registration policies and procedures for those organizations. (Sen. J. Proos) 7 0010 Yes 3/30 3/31 6/29/17 Corrections; parole; department to provide quarterly report providing reasons inmates beyond their earliest release date have not been paroled; require. (Sen. M. O'Brien)

8 0012 Yes 3/30 3/31 6/29/17 Corrections; parole; commutation hearings and procedures; expedite review and hearing process for certain commutations if requested by governor. (Sen. R. Jones)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 1 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 9 0013 Yes 3/30 3/31 6/29/17 Criminal procedure; probation; penalties for probationers who commit technical probation violations; modify. (Sen. J. Proos)

10 0015 Yes 3/30 3/31 6/29/17 Criminal procedure; probation; reduction of term of probation; allow in certain cases. (Sen. R. Jones)

11 0017 Yes 3/30 3/31 6/29/17 # Corrections; parole; supervising region incentive program; create. (Sen. M. Shirkey)

12 0018 Yes 3/30 3/31 6/29/17 # Corrections; parole; department of corrections to report parole absconders to department of health and human services; require. (Sen. K. Horn)

13 0019 Yes 3/30 3/31 6/29/17 # Human services; services or financial assistance; services or financial assistance provided to individual who absconds from parole; require to be discontinued. (Sen. D. Zorn)

14 0020 Yes 3/30 3/31 6/29/17 Corrections; other; reference to general education development (GED); revise to high school equivalency. (Sen. D. Robertson)

15 0021 Yes 3/30 3/31 6/29/17 Crime victims; other; crime victims fund; ensure funds may be provided to minor victims of crime and require certain reporting. (Sen. R. Warren)

16 0022 Yes 3/30 3/31 6/29/17 Corrections; prisoners; department to provide rehabilitation programming for 18-to 22-year-old inmates that specifically takes the prisoners' age into consideration and to report certain information; require. (Sen. B. Johnson) 17 0023 Yes 3/30 3/31 6/29/17 Criminal procedure; other; swift and sure probation sanctions; modify, and create the swift and sure probation supervision fund. (Sen. J. Proos)

18 0024 Yes 3/30 3/31 6/29/17 Courts; other; swift and sure sanctions court; create. (Sen. J. Proos)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 2 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 19 0034 Yes 3/30 3/31 6/29/17 Highways; name; portion of US-23; designate as the "Sergeant Joe Johnson Memorial Highway". (Sen. J. Ananich)

20 0039 Yes 3/30 3/31 3/31/17 Probate; other; exceptions to definition of surviving spouse in relation to a funeral representative; revise. (Sen. R. Jones)

21 0069 Yes 3/30 3/31 3/31/17 State financing and management; other; disclosure of certain information in procurement process; modify. (Sen. R. Jones)

22 0213 Yes 3/30 3/31 3/31/17 Health; other; prescribing drugs, including controlled substances, via telehealth; provide for under certain circumstances and allow Michigan board of nursing to promulgate certain rules for clinical nurse specialists. (Sen. P. MacGregor)

23 4080 Yes 4/27 4/27 4/27/17 State financing and management; other; certain forms of energy improvement financing for certain school districts; provide for. (Rep. B. Griffin)

24 4137 Yes 5/4 5/4 8/2/17 Law enforcement; records; fingerprinting and photographing of child or youth with special health care needs taken and submitted to the automated fingerprint identification system (AFIS) and the statewide network of agency photos upon request of parent or guardian; allow. (Rep. B. Frederick) 25 0038 Yes 5/4 5/4 8/2/17 Law enforcement; records; procedure for fingerprinting and photographing of individual with special health care needs taken and submitted to the automated fingerprint identification system (AFIS) and the statewide network of agency photos upon request of parent or guardian; allow and establish. (Sen. R. Jones) 26 0119 Yes 5/4 5/4 5/4/17 Property; conveyances; transfer of certain state- owned property in Marquette County; provide for. (Sen. T. Casperson)

27 4136 Yes 5/4 5/4 5/4/17 Property tax; delinquent taxes; administration of delinquent tax revolving funds; clarify. (Rep. J. Tedder)

28 4057 Yes 5/9 5/9 8/7/17 Highways; name; portion of US-12 in the city of Jonesville; designate as the "James Bondsteel Memorial Highway". (Rep. E. Leutheuser)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 3 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 29 4063 Yes 5/8 5/9 8/7/17 # Crimes; other; aiming a beam of directed energy from a directed energy device at or into path of aircraft or moving train; prohibit and provide penalty. (Rep. L. Cox)

30 4064 Yes 5/8 5/9 8/7/17 # Criminal procedure; sentencing guidelines; sentencing guidelines for crime of aiming beam of directed energy from a directed energy device at aircraft or into path of aircraft or path of moving train; enact. (Rep. T. Barrett) 31 4203 Yes 5/8 5/9 8/7/17 State; identification cards; secretary of state sharing of photographs taken for official state personal identification card with the department of state police; allow. (Rep. B. LaFave)

32 4204 Yes 5/8 5/9 8/7/17 Traffic control; driver license; access to driver license photograph of concealed weapons license holders; allow by department of state police. (Rep. T. Cole)

33 4329 Yes 5/8 5/9 5/9/17 Appropriations; zero budget; supplemental appropriations; provide for fiscal year 2016-2017. (Rep. J. Yaroch)

34 4219 Yes 5/23 5/23 8/21/17 Criminal procedure; sentencing; deferral and dismissal eligibility for victims of human trafficking; expand. (Rep. B. Kahle)

35 4167 Yes 5/23 5/23 8/21/17 Vehicles; trucks; length limit; increase truck and trailer combinations transporting agricultural drainage tubing to 75 feet. (Rep. B. Frederick)

36 4288 Yes 5/23 5/23 5/23/17 Family law; other; jurisdiction to establish a support order in certain circumstances under uniform interstate family support act (UIFSA); modify. (Rep. K. Kesto)

37 0046 Yes 5/23 5/23 8/21/17 Traffic control; traffic regulation; requirement that emergency lights be mounted on the roof of an authorized emergency vehicle; eliminate. (Sen. D. Zorn)

38 0102 Yes 5/23 5/23 8/21/17 Property; other; Michigan community foundation act; create. (Sen. W. Schmidt)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 4 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 39 0118 Yes 5/23 5/23 8/21/17 Recreation; trails; National Trails System; allow department of natural resources to become a trail sponsor, and provide limited liability for personal injuries. (Sen. G. Hansen)

40 0129 Yes 5/23 5/23 8/21/17 Natural resources; mining; small native copper mining operations; establish separate regulatory program for. (Sen. T. Casperson)

41 0202 Yes 5/23 5/23 5/23/17 Crimes; gambling; social media internet game providing certain awards to players; allow. (Sen. J. Brandenburg)

42 0359 Yes 5/25 5/25 5/25/17 Property tax; exemptions; delivery of combined document for personal property exemption; modify deadline date. (Sen. D. Hildenbrand)

43 4131 Yes 6/7 6/7 9/5/17 Retirement; other; forfeiture of employer contributions to a defined contribution plan if public employee is convicted of certain felonies; provide for. (Rep. J. Runestad)

44 4058 Yes 6/7 6/7 6/7/17 Economic development; neighborhood enterprise zones; requirement to send report of assessed values and ad valorem taxes to the Michigan enterprise zone authority; eliminate. (Rep. E. Leutheuser)

45 0176 Yes 6/7 6/7 9/5/17 Highways; signs; tourist-oriented directional sign; revise requirements for eligible attractions. (Sen. T. Casperson)

46 0111 Yes 6/8 6/9 7/24/17 Economic development; brownfield redevelopment authority; transformational brownfield plans; provide for. (Sen. K. Horn)

47 0112 Yes 6/8 6/9 7/24/17 Individual income tax; collections; certain revenues attributable to transformational brownfield plans; capture and earmark. (Sen. J. Brandenburg)

48 0113 Yes 6/8 6/9 7/24/17 Sales tax; collections; certain revenue attributable to transformational brownfield plans; capture and earmark. (Sen. T. Casperson)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 5 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 49 0114 Yes 6/8 6/9 7/24/17 Use tax; collections; certain revenue attributable to transformational brownfield plans; capture and earmark. (Sen. P. MacGregor)

50 0115 Yes 6/8 6/9 7/24/17 Economic development; renaissance zones; exemption of certain taxes; modify. (Sen. S. Bieda)

51 4209 Yes 6/15 6/15 9/13/17 Courts; juries; juror compensation; increase. (Rep. P. Lucido)

52 4210 Yes 6/15 6/15 9/13/17 # Courts; juries; increase in juror compensation; provide for. (Rep. P. Lucido)

53 4211 Yes 6/15 6/15 9/13/17 Criminal procedure; evidence; testimony of expert witnesses regarding behavior pattern of human trafficking victims; allow under certain circumstances. (Rep. P. Lucido)

54 4532 Yes 6/15 6/15 6/15/17 Property; recording; marital status in instruments conveying or mortgaging real estate; modify. (Rep. M. Whiteford)

55 0043 Yes 6/15 6/15 9/13/17 Public employees and officers; compensation and benefits; public employee health benefits act; allow alternative cash reserves option for pooled plans. (Sen. G. Hansen)

56 0126 Yes 6/15 6/15 9/13/17 Occupations; real estate; continuing education hours for real estate brokers and salespersons; revise requirements. (Sen. M. Kowall)

57 0158 Yes 6/15 6/15 9/13/17 Occupations; business licensing and registration; licensure of used motor vehicle parts dealers; exclude certain businesses regulated under the natural resources and environmental protection act. (Sen. R. Jones)

58 0168 Yes 6/15 6/15 6/15/17 Insurance; no-fault; auto theft prevention authority assessment; expand to commercial vehicles. (Sen. R. Jones)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 6 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 59 4013 Yes 6/28 6/28 9/26/17 Vehicles; registration; paperless registration; allow. (Rep. P. Lucido)

60 4082 Yes 6/28 6/28 9/26/17 Natural resources; other; DNR prescribed burns; require notification to township supervisor and 9-1-1 service. (Rep. M. Whiteford)

61 4215 Yes 6/28 6/28 9/26/17 Traffic control; violations; unattended running vehicles; allow under certain circumstances. (Rep. H. Hughes)

62 4286 Yes 6/28 6/28 6/28/17 Drains; districts; addition of county to or removal of county from drainage district; provide for. (Rep. R. Victory)

63 0239 Yes 6/28 6/28 9/26/17 Highways; other; transfer of abandoned highway; clarify. (Sen. T. Casperson)

64 4612 Yes 6/29 6/30 6/30/17 Criminal procedure; sentencing; certain permissible costs; extend sunset. (Rep. R. VerHeulen)

65 4613 Yes 6/29 6/30 9/28/17 Courts; other; trial court funding commission; create, and prescribe powers and duties. (Rep. R. VerHeulen)

66 4169 Yes 6/29 6/30 6/30/17 Liquor; licenses; prohibition on issuing license within 500 feet of church or school; extend exemption to licenses issued or renewed before certain date. (Rep. T. Brann)

67 4325 Yes 6/29 6/30 6/30/17 Insurance; producers; continuing education credit carryover system for insurance producers; provide for, and revise valuation standards for certain individual annuity and pure endowment contracts. (Rep. T. Barrett)

68 4636 Yes 7/11 7/11 10/9/17 Crimes; other; procedures of clitoridectomy, infibulation, or other female genital mutilation; prohibit, and provide penalties. (Rep. M. Hoitenga)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 7 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 69 4637 Yes 7/11 7/11 10/9/17 Crimes; other; transporting person for purpose of performing genital mutilation; prohibit. (Rep. D. Farrington)

70 0337 Yes 7/11 7/11 10/9/17 Crimes; other; procedures of clitoridectomy, infibulation, or other female genital mutilation; prohibit, and provide penalties. (Sen. M. O'Brien)

71 0368 Yes 7/11 7/11 10/9/17 Crimes; other; penalties for transporting for the purpose of female genital mutilation; provide for. (Sen. T. Schuitmaker)

72 0338 Yes 7/11 7/11 10/9/17 # Criminal procedure; sentencing guidelines; crime of performing clitoridectomy, infibulation, or other female genital mutilation; provide sentencing guidelines for. (Sen. R. Jones)

73 0369 Yes 7/11 7/11 10/9/17 # Criminal procedure; sentencing guidelines; sentencing guidelines for crimes of transporting female for purpose of female genital mutilation; provide for. (Sen. J. Emmons)

74 4638 Yes 7/11 7/11 10/9/17 # Criminal procedure; sentencing guidelines; crimes of performing female genital mutilation and of transporting a person for purpose of genital mutilation; provide sentencing guidelines for. (Rep. D. Rendon)

75 4639 Yes 7/11 7/11 10/9/17 # Health occupations; health professionals; permanent revocation of occupational license or registration if convicted of female genital mutilation or transporting person for purpose of performing female genital mutilation under state law; provide for. (Rep. K. Kesto) 76 4641 Yes 7/11 7/11 10/9/17 # Civil procedure; statute of limitations; female genital mutilation; extend statute of limitations for minor victims. (Rep. S. Chang)

77 4642 Yes 7/11 7/11 10/9/17 Health; education; education and outreach program related to female genital mutilation; provide for. (Rep. P. Faris)

78 4661 Yes 7/11 7/11 10/9/17 # Civil procedure; civil actions; victims of clitoridectomy, infibulation, or other female genital mutilation; provide for cause of action. (Rep. B. Griffin)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 8 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 79 4690 Yes 7/11 7/11 10/9/17 # Criminal procedure; statute of limitations; statute of limitations on female genital mutilation violations; extend. (Rep. B. Kahle)

80 0159 Yes 7/11 7/11 10/9/17 Traffic control; traffic regulation; gross vehicle weight limits; provide exemption for certain natural gas vehicles. (Sen. T. Casperson)

81 0410 Yes 7/11 7/11 10/9/17 # Health occupations; health professionals; permanent revocation of occupational license or registration if convicted of female genital mutilation or transporting person for purpose of performing female genital mutilation under state law; provide for. (Sen. P. Colbeck) 82 4575 Yes 7/12 7/12 10/10/17 Civil procedure; costs and fees; fee for publication of legal notice; extend sunset for annual increases for inflation. (Rep. B. LaFave)

83 4558 Yes 7/12 7/12 10/10/17 Liquor; advertising; regulation of displays; provide for. (Rep. J. Moss)

84 4186 Yes 7/12 7/12 7/12/17 Animals; animal shelters; certain definition of animal; revise. (Rep. J. Alexander)

85 4427 Yes 7/12 7/12 1/8/18 Law enforcement; other; release of recording taken by law enforcement officers with a body-worn camera; prohibit in certain circumstances. (Rep. J. Runestad)

86 4556 Yes 7/12 7/12 10/10/17 # Criminal procedure; sentencing guidelines; sentencing guidelines for unauthorized sale, delivery, or importation of beer or wine; enact. (Rep. J. Bellino)

87 4557 Yes 7/12 7/12 10/10/17 Liquor; retail sales; penalties for selling, delivering or importing beer or wine in violation of act; increase. (Rep. J. Bellino)

88 4559 Yes 7/12 7/12 7/12/17 Liquor; authorized distribution agents; wholesaler employees sampling beer or wine for educational purposes on the wholesaler's licensed premises; allow. (Rep. T. Barrett)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 9 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 89 4213 Yes 7/12 7/12 10/10/17 Liquor; drinking age; obtaining court order before nonconsensual preliminary chemical breath testing of a minor; require. (Rep. P. Lucido)

90 4540 Yes 7/12 7/12 7/12/17 Environmental protection; funding; sunsets on fees for wastewater and drinking water certifications and waste program facility and user charges; extend. (Rep. M. Whiteford)

91 4541 Yes 7/12 7/12 7/12/17 Water; quality; safe drinking water act; extend sunset on fees for training programs for certified operators. (Rep. M. Whiteford)

92 0401 Yes 7/13 7/13 7/13/17 Retirement; public school employees; default defined contribution only for employees hired after certain date; require, and provide for other general amendments. (Sen. P. Pavlov)

93 0076 Yes 7/13 7/13 7/13/17 Appropriations; supplemental; Michigan natural resources trust fund; provide appropriations for fiscal year 2016-2017. (Sen. D. Booher)

94 0160 Yes 7/13 7/13 10/11/17 Vehicles; motorcycles; definitions of implement of husbandry, autocycle, and motorcycle; modify. (Sen. T. Casperson)

95 0219 Yes 7/13 7/13 10/11/17 Weapons; licensing; application process for licensing; modify. (Sen. M. Green)

96 0245 Yes 7/13 7/13 10/11/17 Weapons; other; spring-assisted knife; allow. (Sen. R. Jones)

97 0248 Yes 7/13 7/13 7/13/17 Veterans; other; World War I centennial commission; create. (Sen. R. Warren)

98 0249 Yes 7/13 7/13 7/13/17 Local government; other; educational instruction access act; create. (Sen. M. Shirkey)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 10 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 99 0260 Yes 7/13 7/13 7/13/17 Higher education; education programs; authorization and distance education reciprocal exchange act; extend sunset. (Sen. D. Hildenbrand)

100 0267 Yes 7/13 7/13 7/13/17 Law enforcement; other; student safety act; repeal sunset. (Sen. J. Emmons)

101 0333 Yes 7/13 7/13 10/11/17 Courts; business court; types of cases heard by the business court; revise. (Sen. R. Jones)

102 0380 Yes 7/13 7/13 7/13/17 Property tax; local community stabilization share; distribution of local community stabilization share; modify dates. (Sen. D. Hildenbrand)

103 0383 Yes 7/13 7/13 8/2/17 Law enforcement; records; procedure for fingerprinting and photographing of child or youth with special health care needs taken and submitted to the automated fingerprint identification system (AFIS) and the statewide network of agency photos upon request of parent or guardian; modify. (Sen. R. Jones) 104 0394 Yes 7/13 7/13 10/11/17 Human services; county services; sunset on certain administrative rate changes to foster care services; change and revise the amount of the administrative rate paid by the department. (Sen. P. MacGregor)

105 0433 Yes 7/13 7/13 7/13/17 Marihuana; facilities; background check requirements for prospective licensees; modify. (Sen. R. Jones)

106 4759 Yes 7/13 7/13 7/13/17 Property; conveyances; transfer of certain state- owned property in Ingham County; provide for. (Rep. A. Schor)

107 4323 Yes 7/14 7/14 7/14/17 + Appropriations; omnibus; appropriations for fiscal year 2017-2018; provide. (Rep. L. Cox)

108 4313 Yes 7/14 7/14 7/14/17 + Appropriations; zero budget; fiscal year 2017-2018 omnibus appropriations for school aid, higher education, and community colleges; provide for. (Rep. T. Kelly)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 11 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 109 0242 Yes 7/26 7/26 8/25/17 Economic development; Michigan strategic fund; good jobs for Michigan program; create. (Sen. J. Stamas)

110 0243 Yes 7/25 7/26 8/25/17 Individual income tax; collections; certain revenues attributable to the good jobs for Michigan program; capture and earmark. (Sen. W. Schmidt)

111 0244 Yes 7/25 7/26 8/25/17 Taxation; administration; disclosure of certain information under the Michigan strategic fund act; allow. (Sen. S. Bieda)

112 4160 Yes 7/27 7/27 7/27/17 Traffic control; traffic regulation; solicitation of contributions in public roadways by certain nonprofit organizations; allow under certain circumstances. (Rep. S. Hernandez)

113 4177 Yes 7/27 7/27 10/25/17 Elections; ballots; requirement of political party vignettes being printed on election ballots; remove. (Rep. H. Vaupel)

114 4178 Yes 7/27 7/27 10/25/17 # Campaign finance; other; reference to party vignette in the Michigan campaign finance act; remove. (Rep. E. Canfield)

115 4306 Yes 7/27 7/27 10/25/17 Vehicles; motorcycles; motorcycle endorsement fee; increase and increase earmark of motorcycle registration fees into motorcycle safety fund. (Rep. J. Tedder)

116 0332 Yes 7/27 7/27 10/25/17 Traffic control; driver license; requirement of examination regarding existence of certain medical conditions affecting applicant's ability to operate vehicle safely; modify. (Sen. T. Casperson)

117 0474 Yes 7/27 7/27 7/27/17 Land use; land division; conflict between certain plats; resolve. (Sen. M. O'Brien)

118 4892 Yes 9/18 9/18 9/18/17 Elections; election officials; modifying the nominating petition filing deadline for candidates for city offices; authorize under certain circumstances, add certain election accountability provisions, and provide for civil fines. (Rep. L. Chatfield)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 12 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 119 0335 Yes 9/20 9/20 9/20/17 Campaign finance; independent expenditures; general amendments to the Michigan campaign finance act; provide for. (Sen. D. Robertson)

120 0336 Yes 9/20 9/20 9/20/17 # Criminal procedure; sentencing guidelines; independent expenditure committee contribution violations; provide for in sentencing guidelines. (Sen. D. Robertson)

121 4335 Yes 10/5 10/5 10/5/17 # Property tax; principal residence exemption; claiming a principal residence exemption in this state while claiming a substantially similar exemption on property in another state; clarify procedures for rescinding the latter. (Rep. D. Pagel) 122 4336 Yes 10/5 10/5 10/5/17 # Property tax; principal residence exemption; obtaining or attempting to obtain a principal residence exemption on property in this state while claiming a substantially similar exemption on property in another state; prohibit. (Rep. K. LaSata) 123 4939 Yes 10/5 10/5 10/5/17 Liquor; drinking age; effective date of certain provisions; amend. (Rep. P. Lucido)

124 4424 Yes 10/12 10/12 1/10/18 Natural resources; hunting; penalties for possession of certain cervid parts killed in another state; increase. (Rep. J. Kivela)

125 4654 Yes 10/17 10/17 1/15/18 Occupations; alarm systems; installation of certain business monitoring systems without electrician's permit; authorize for registered or licensed security alarm providers. (Rep. M. Hoitenga)

126 4655 Yes 10/17 10/17 1/15/18 Construction; permits; installation, maintenance, replacement, or servicing of a business monitoring system; exempt from construction code permit requirements. (Rep. B. Griffin)

127 4580 Yes 10/17 10/17 1/15/18 Housing; housing development authority; refinancing option; allow. (Rep. D. Farrington)

128 0223 Yes 10/17 10/17 1/15/18 Law enforcement; records; maintain record for separation of employment; require, and establish that agency is immune from civil liability. (Sen. R. Jones)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 13 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 129 0356 Yes 10/17 10/17 4/15/18 Occupations; other; salesperson license; establish. (Sen. J. Hune)

130 0357 Yes 10/17 10/17 1/15/18 Liquor; distribution; wholesalers and manufacturers refunding or replacing beer or wine under certain circumstances; allow. (Sen. R. Warren)

131 0358 Yes 10/17 10/17 1/15/18 Liquor; advertising; providing signs that promote brands and prices of alcoholic liquor to retailers; allow. (Sen. R. Jones)

132 4508 Yes 10/26 10/26 1/24/18 State agencies (existing); technology, management, and budget; Michigan cyber civilian corps act; create. (Rep. B. Iden)

133 4457 Yes 10/26 10/26 1/24/18 State financing and management; other; certain forms of energy improvement financing for community colleges; provide for. (Rep. B. Iden)

134 4583 Yes 10/26 10/26 1/24/18 Environmental protection; underground storage tanks; funding at certain cleanups; provide for. (Rep. M. Whiteford)

135 4999 Yes 10/26 10/26 10/26/ Taxation; other; local unit of government implementing an excise tax on the manufacture, distribution, or sale of food; prohibit. (Rep. R. VerHeulen)

136 0049 Yes 10/26 10/26 1/24/18 Probate; guardians and conservators; provision related to compensation for professional guardian or professional conservator; modify. (Sen. D. Booher)

137 0352 Yes 10/26 10/26 1/24/18 Health; education; training program and written clearance form regarding concussions in youth athletes and their return to athletic activity; specify frequency of training and modify definition of youth athlete. (Sen. J. Proos) 138 4781 Yes 10/29 10/30 1/28/18 Vehicles; bicycles; operation of electric bicycles on certain trails; allow. (Rep. H. Hughes)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 14 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 139 4782 Yes 10/29 10/30 1/28/18 Vehicles; bicycles; definition and regulation of electric bicycles; provide for. (Rep. H. Hughes)

140 4783 Yes 10/29 10/30 10/30/17 # Insurance; no-fault; electric-assist bicycles; exempt from no-fault insurance requirements. (Rep. K. Kesto)

141 4305 Yes 10/29 10/30 10/30/17 Trade; securities; exemption from registration of certain securities issued by Michigan companies; revise. (Rep. B. Kahle)

142 4311 Yes 10/29 10/30 1/28/18 Health; vital records; reporting a live birth; amend to protect the confidentiality of parents who surrender a newborn under the safe delivery of newborns law. (Rep. H. Vaupel)

143 0133 Yes 11/2 11/2 11/2/17 Appropriations; school aid; multisection school aid supplemental; provide for. (Sen. D. Hildenbrand)

144 0264 Yes 11/2 11/2 1/31/18 Law enforcement; fire personnel; firefighters training council act; modify. (Sen. J. Stamas)

145 0265 Yes 11/2 11/2 1/31/18 # Fireworks; other; administration of Michigan fireworks safety fund; modify. (Sen. J. Stamas)

146 0370 Yes 11/2 11/2 1/31/18 Occupations; athletics; Michigan unarmed combat regulatory act; revise fines and make other general revisions. (Sen. D. Robertson)

147 0402 Yes 11/2 11/2 11/2/17 Environmental protection; sewage; maximum total grant for municipalities; increase. (Sen. P. Pavlov)

148 0450 Yes 11/2 11/2 11/2/17 Businesses; nonprofit corporations; authorization to restructure municipal health facilities corporations; revise requirements. (Sen. M. Shirkey)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 15 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 149 4396 No 11/2 11/2 ** Individual income tax; deductions; certain pension income for certain individuals; modify. (Rep. J. Bellino)

150 0098 Yes 11/6 11/6 11/6/17 Higher education; financial aid; number of governing bodies authorized to establish promise zones; increase. (Sen. J. Ananich)

151 4181 Yes 11/8 11/8 2/6/18 Education; counseling; requirements for employment as a school counselor; revise. (Rep. B. Roberts)

152 4547 Yes 11/8 11/8 2/6/18 # Criminal procedure; sentencing guidelines; blood alcohol level requirement for certain alcohol-related offenses; eliminate sunset for .08 limit. (Rep. K. Kesto)

153 4548 Yes 11/8 11/8 2/6/18 # Crimes; intoxication or impairment; blood alcohol level requirement for certain alcohol-related driving violations; eliminate sunset for .08 limit. (Rep. P. Green)

154 4170 Yes 11/8 11/8 2/6/18 # Health; other; physician orders for scope of treatment forms; allow. (Rep. J. Tedder)

155 4171 Yes 11/8 11/8 2/6/18 # Probate; guardians and conservators; physician orders for scope of treatment form; authorize a guardian to sign. (Rep. L. Cox)

156 4173 Yes 11/8 11/8 2/6/18 # Human services; adult foster care; physician orders for scope of treatment form; establish procedure if adult foster care facility is unwilling to comply with the form. (Rep. H. Vaupel)

157 4174 Yes 11/8 11/8 2/6/18 # Health; emergency response; procedure for complying with a do-not-resuscitate order; revise to reflect physician orders for scope of treatment forms and provide for other general amendments. (Rep. L. Love)

158 0253 Yes 11/8 11/9 11/9/17 Appropriations; zero budget; supplemental appropriations; provide for fiscal years 2016-2017 and 2017-2018. (Sen. D. Hildenbrand)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 16 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 159 4166 Yes 11/8 11/9 2/7/18 Education; employees; provisions providing employment preferences for certain personnel in special education programs and services; repeal. (Rep. M. Whiteford)

160 4756 Yes 11/8 11/9 1/1/18 Crimes; intoxication or impairment; abstract of court record for certain violations of the minor in possession of alcohol statute; revise. (Rep. P. Lucido)

161 0435 Yes 11/9 11/13 2/11/18 # Courts; drug court; certification of drug treatment courts by the state court administrative office; require and provide certain definitions and for transferring jurisdiction of certain cases. (Sen. T. Schuitmaker)

162 0436 Yes 11/9 11/13 2/11/18 # Courts; drug court; certification of DWI/sobriety court by the state court administrative office; amend the vehicle code to reflect. (Sen. T. Schuitmaker)

163 0437 Yes 11/9 11/13 2/11/18 # Courts; other; certification of mental health courts by the state court administrative office; require. (Sen. T. Schuitmaker)

164 0438 Yes 11/9 11/13 2/11/18 # Courts; other; certification of veterans courts by the state court administrative office; require. (Sen. T. Schuitmaker)

165 0360 Yes 11/9 11/13 2/11/18 Health occupations; pharmacists; dispensing additional quantities of a prescription drug within the limits of the prescription; allow under certain circumstances. (Sen. M. O'Brien)

166 0372 Yes 11/9 11/13 2/11/18 Liquor; retail sales; requirement to tag certain beer kegs; eliminate. (Sen. G. Hansen)

167 0378 Yes 11/9 11/13 2/11/18 Senior citizens; housing; home for the aged; amend definition and create an exemption from licensing. (Sen. M. Knollenberg)

168 0415 Yes 11/20 11/21 2/19/18 Agriculture; other; security measures to combat credit card skimmers; require on retail motor fuel pumps with scanning devices. (Sen. W. Schmidt)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 17 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 169 0107 Yes 11/20 11/21 2/19/18 Housing; inspection; inspection procedures and regulations; modify. (Sen. R. Jones)

170 0120 Yes 11/20 11/21 2/19/18 Traffic control; traffic regulation; maximum length of stinger-steered combination and tow-away trailer transporter; revise. (Sen. T. Casperson)

171 0238 Yes 11/20 11/21 2/19/18 Consumer credit; lending practices; authority to pay referral fees under regulatory loan act; clarify. (Sen. D. Booher)

172 0286 Yes 11/20 11/21 2/19/18 Health facilities; other; nurse aide training and registration program; establish. (Sen. H. Hopgood)

173 0278 Yes 11/20 11/21 11/21/17 Libraries; state; interstate library compact; create. (Sen. J. Proos)

174 0381 Yes 11/20 11/21 2/19/18 Criminal procedure; bail; service of notices to surety bonds; modify. (Sen. R. Jones)

175 0520 Yes 11/20 11/21 11/21/17 Commercial code; secured transactions; bulk sales of records by filing offices; revise requirements. (Sen. D. Booher)

176 0553 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in the property tax act; update. (Sen. G. Hansen)

177 0554 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in the business corporation act; update. (Sen. G. Hansen)

178 0555 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in the nonprofit corporation act; update. (Sen. G. Hansen)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 18 2017 Michigan Public Acts Table ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 179 0556 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in the revised judicature act; update. (Sen. G. Hansen)

180 0557 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in 1964 PA 105; update. (Sen. G. Hansen)

181 0558 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in 1957 PA 29; update. (Sen. W. Schmidt)

182 0559 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in the Michigan penal code; update. (Sen. W. Schmidt)

183 0560 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in the legal defense fund act; update. (Sen. W. Schmidt)

184 0561 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; references to the Michigan history center act in the Michigan campaign finance act; update. (Sen. W. Schmidt)

185 0562 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; issuance of historical markers; modify. (Sen. M. Green)

186 0563 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; natural resources and environmental protection act; update references to the Governor John B. Swainson Michigan historical markers act. (Sen. M. Green)

187 0564 Yes 11/20 11/21 2/19/18 # History and arts; historic sites; Michigan historical center; rename to the Michigan history center and provide for expenditures from the Michigan history center operations fund. (Sen. M. Green)

188 0565 Yes 11/20 11/21 2/19/18 # History and arts; other; Michigan historical center; update references to the Michigan history center. (Sen. M. Green)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 19 ENROLLED

PA I.E.* Governor Filed No. HB SB Yes/No Approved Date Effective Date SUBJECT 189 4285 Yes 11/20 11/21 11/21/17 Property tax; payment and collection; personal liability for unpaid property taxes; clarify. (Rep. P. Lucido)

190 0509 Yes 12/5 12/5 3/5/18 Highways; name; portion of M-52; designate as the "Deputy Grant Whitaker Memorial Highway". (Sen. C. Hertel)

191 4065 Yes 12/7 12/7 3/7/18 Corrections; other; prohibition against the department of corrections hiring a formerly convicted felon; modify. (Rep. D. Pagel)

192 4208 Yes 12/7 12/7 3/7/18 Legislature; legislators; term of removal or resignation from the office of state senator or representative; provide for. (Rep. A. Miller)

193 4716 Yes 12/7 12/7 3/7/18 Children; parental rights; termination of parental rights for subjecting child to undergo female genital mutilation; require. (Rep. P. Lucido)

Veto 0011 No 3/30/17 Legislature; other; program for the management and collection of data related to criminal justice statistics; create. (Sen. P. Colbeck)

Veto 0050 No 3/30/17 Corrections; other; county jail bed savings program; establish. (Sen. D. Booher)

Veto 0094 No 7/25/17 Sales tax; collections; sales tax on the difference; accelerate phase-in. (Sen. D. Hildenbrand)

Veto 0095 No 7/25/17 Use tax; collections; use tax on the difference; accelerate phase-in. (Sen. D. Robertson)

Veto 0163 No 6/30/17 Vehicles; fund-raising registration plates; fund-raising registration plate for Choose Life Michigan Fund; create. (Sen. P. Colbeck)

* - I.E. means Legislature voted to give the Act immediate effect. ** - Act takes effect on the 91st day after sine die adjournment of the Legislature. *** - See Act for applicable effective date. + - Line item veto. ++ - Pocket veto. # - Tie bar. © 2016 by Legislative Council, State of Michigan. All rights reserved Page 20