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La Difusió D ADVERTIMENT . La consulta d’aquesta tesi queda condicionada a l’acceptació de les següents condicions d'ús: La difusió d’aquesta tesi per mitjà del servei TDX ( www.tesisenxarxa.net ) ha estat autoritzada pels titulars dels drets de propietat intel·lectual únicament per a usos privats emmarcats en activitats d’investigació i docència. No s’autoritza la seva reproducció amb finalitats de lucre ni la seva difusió i posada a disposició des d’un lloc aliè al servei TDX. No s’autoritza la presentació del seu contingut en una finestra o marc aliè a TDX (framing). Aquesta reserva de drets afecta tant al resum de presentació de la tesi com als seus continguts. En la utilització o cita de parts de la tesi és obligat indicar el nom de la persona autora. ADVERTENCIA . La consulta de esta tesis queda condicionada a la aceptación de las siguientes condiciones de uso: La difusión de esta tesis por medio del servicio TDR ( www.tesisenred.net ) ha sido autorizada por los titulares de los derechos de propiedad intelectual únicamente para usos privados enmarcados en actividades de investigación y docencia. No se autoriza su reproducción con finalidades de lucro ni su difusión y puesta a disposición desde un sitio ajeno al servicio TDR. No se autoriza la presentación de su contenido en una ventana o marco ajeno a TDR (framing). Esta reserva de derechos afecta tanto al resumen de presentación de la tesis como a sus contenidos. En la utilización o cita de partes de la tesis es obligado indicar el nombre de la persona autora. WARNING . On having consulted this thesis you’re accepting the following use conditions: Spreading this thesis by the TDX ( www.tesisenxarxa.net ) service has been authorized by the titular of the intellectual property rights only for private uses placed in investigation and teaching activities. Reproduction with lucrative aims is not authorized neither its spreading and availability from a site foreign to the TDX service. Introducing its content in a window or frame foreign to the TDX service is not authorized (framing). This rights affect to the presentation summary of the thesis as well as to its contents. In the using or citation of parts of the thesis it’s obliged to indicate the name of the author UNIVERSITAT POLITÈCNICA DE CATALUNYA Doctorat en Recursos Naturals i Medi ambient Technical and environmental viability of membrane technologies in water treatment NF in drinking water process and MBR for wastewater reuse PhD Thesis Gemma Ribera Simon March 2013 Supervised by: Xavier Martínez Lladó Frederic Clarens Blanco Miquel Rovira Boixaderas MIQUEL ROVIRA BOIXADERAS, director de l’Àrea de Tecnologia Ambiental de la Fundació CTM Centre Tecnològic, XAVIER MARTÍNEZ LLADÓ i FREDERIC CLARENS BLANCO, investigadors i responsables de les línees de tecnologia de l’aigua i d’ecologia industrial de la mateixa àrea, respectivament, juntament amb el XAVIER GAMISANS NOGUERA professor i investigador al Departament d’Enginyeria Minera i Recursos Naturals de la Universitat Politècnica de Catalunya (UPC) a Manresa (EPSEM) CERTIFIQUEM, Que el present treball, titulat “Technical and environmental viability of membrane technologies in water treatment: NF in drinking water process and MBR for wastewater reuse”, que presenta GEMMA RIBERA SIMON per a l’obtenció del Grau de Doctor per la Universitat Politècnica de Catalunya, ha estat realitzat sota la nostra direcció i tutoria. I per què així consti, signem el present document, Dr. Miquel Rovira Boixaderas Dr. Xavier Martínez Lladó Dr. Frederic Clarens Blanco Dr. Xavier Gamisans Noguera Manresa, Febrer 2013 AGRAÏMENTS - ACKNOWLEDGEMENTS Aquesta tesi és fruït del meu treball realitzat a la Fundació CTM Centre Tecnològic de Manresa, concretament a l’àrea de tecnologia ambiental (ATA). Trobo oportú agrair l’existència de fundacions, universitats i altres centres capaces de formar estudiants i desenvolupar les seves inquietuds personals. La resolució d’alguns problemes presents a la nostra societat no seria possible sense les tasques de recerca, innovació i ampliació de coneixements, aplicades a la tecnologia, en aquest cas. Per tant, gràcies al finançament per part del Ministerio de Ciencia y Technología (2008)/ Ministerio de Ciencia e Innovación (2009) en les convocatòries Plan de Centros, CENIT i CDTI pels projectes NANOAQUA, DEMETER i NAIGMA. El meu camí en el món de la tesi va començar al 2007 a la EPSEM de Manresa, quan el Xavier Gamisans va valorar el meu interès per realitzar el doctorat. Gràcies a ell, vaig poder entrar a formar part del grup de recerca sobre tractament de contaminacions gasoses i olors, on també vaig compartir les meves primeres inquietuds amb altres estudiants, doctors i professors, com la Montse Soler, l’Anna Bonsfills, la Conxita Lao, i també el Javier Lafuente i el David Gabriel, de la Universitat Autònoma. Del meu treball a la UPC també destacar al Toni Dorado, la Maria Tomas i el Ramon Navarro com a bons companys de feina i amics. Si en aquesta fase inicial ja vaig guanyar una bona experiència personal i acadèmica, la següent al CTM encara m’ha fet créixer molt més, per això vull donar les gràcies al Miquel Rovira, al Xavier Martínez i al Frederic Clarens, els meus directors de tesi, per deixar-me formar part del seu equip. Aquí, la tesi va prendre la direcció en el tractament de l’aigua mitjançat tecnologia de membranes, i agraeixo haver pogut seguir el fil del què, des d’un principi, els meus directors ja tenien en ment. És més, l’enfocament final ha permès que pogués mirar les membranes des d’un punt de vista ambiental, ecològic i sostenible, o un barreja de tots, com a mi m’agrada. Aquí, agraeixo especialment les dosis d’objectivitat per part del Frederic. En aquest punt, no em voldria quedar curta, el Xavier Martínez com a director de tesi s’hi ha esmerat, no he conegut mai ningú que estigui a tants llocs amb tantes ganes, aportant coses positives com: energia, idees, comentaris analitzats al detall per minimitzar possibles errors, i tantes altres experiències més que sense elles aquesta tesi no seria la mateixa, ni hauria pogut aprendre tant. A les companyes i companys de l’àrea els dono les gràcies per ser com són i per donar-me suport en més d’una ocasió, així com per col·laborar en l’obtenció dels resultats d’aquesta tesi: Cristina, Laura, Montse, Neus, Sandra, Irene, Isabel, David, I Ramon i Jose amb el teu sentit del humor, a més de sumar-hi els doctorands d’Amphos: la Eli, la Carolina, Christoph i ara últimament la Maria Rosa. En especial, Laia i Albert dir-vos que sou molt bons companys de despatx i de carrera, merci per la vostra ajuda. La complementarietat i bon treball d’aquest equip també és possible gràcies al Miquel Rovira, al Vicens Martí, al Joan De Pablo i al Jose Manuel Prado. Agrair al Josep Caixach i a la Núria Cortes del grup d’espectroscòpia de masses del CSIC la seva col·laboració proporcionant valuosos resultats i coneixements respecte la naturalesa orgànica de les aigües superficials. També donar les gràcies a les empreses on hem pogut realitzar els projectes que formen part d’aquesta tesi, per una part al Ricard, a la Montse, a l’Eva, la Marta, al Servitja i als operaris d’Aigües de Manresa que van col·laborar amb el bon funcionament de la planta pilot (NAIGMA). Parlant del pilotatge, agrair a TRAB S.L. que va fer front davant alguns imprevistos. Per altra banda, agrair a l’empresa Miguel Torres i Hera-Amasa la seva col·laboració al projecte DEMETER, sobretot al Ramon Nomen i del Toni Giménez per la seva ajuda tècnica i pràctica de les tecnologies estudiades pel tractament d’aigües residuals. In the last year of this career, I want to mention my stay in Netherlands, where I knew a country where cycling is always possible and where I met kind people. I am very pleased that Emile accepted to be my supervisor during my stay in KWR (Nieuwegein), together with my temporally partners Sara, Kerusha and Roberto. Thanks to Danny who helps me in my experiments planning and performance, and to Roberta as my officemate with a huge empathy. I am also glad to have shared funny moments with Helena, Bea, and with my Catalan compatriots, Elena and Joan. I was very pleased to live in Frank’s house, where I shared special moments during my stay. Gràcies als meus pares, Rosa i Ramon, que sempre m’han donat la llibertat per créixer i aprendre de la vida, a la meva germana Eva per ser un suport fonamental i per la seva visió clara de les coses. A la família més pròxima, Xiscu, cosins, tiets per saber que estan allà de manera incondicional quan els fets ho requereixen. Finalment, vull agrair a la meva gent el seu suport i els moments que m’aporten fora de la feina, tan important per mi com passar estones amb el meu nebot Arnau, o realitzant activitats diverses amb les meves amigues Aida, Annes, Elena, Ester, Glòria, Irene, Janine, Judit, Karina, Laures, Marta, Roser i Vanessa. També vull mencionar les bones relacions que he fet dins el món del vi de l’Abadal: Maria, Joan, Toni, Miki, i de l’aficionat: David i Pep. Gràcies a la resta de persones que sempre s’han mostrat interessades amb el què feia, motivant-me encara més a continuar en el meu trajecte. II TABLE OF CONTENTS AGRAÏMENTS/ ACKNOWLEDGEMENTS ...................................................................... I TABLE OF CONTENTS ................................................................................................. III INDEX OF FIGURES ...................................................................................................... V INDEX OF TABLES ....................................................................................................
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