Third Supplement, FCC 11 Index / All-Trans-Lycopene / I-1
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Inositol Safety: Clinical Evidences
European Review for Medical and Pharmacological Sciences 2011; 15: 931-936 Inositol safety: clinical evidences G. CARLOMAGNO, V. UNFER AGUNCO Obstetrics & Gynecology Center, Rome (Italy) Abstract. – Myo-inositol is a six carbon ent required by the human cells for the growth cyclitol that contains five equatorial and one axi- and survival in the culture. In humans and other al hydroxyl groups. Myo-inositol has been classi- species, Myo-inositol can be converted to either fied as an insulin sensitizing agent and it is L- or D-chiro-inositol by epimerases. Early stud- commonly used in the treatment of the Polycys- tic Ovary Syndrome (PCOS). However, despite ies showed that inositol urinary clearance was al- its wide clinical use, there is still scarce informa- tered in type 2 diabetes patients, the next step tion on the myo-inositol safety and/or side ef- was to link impaired inositol clearance with in- fects. The aim of the present review was to sum- sulin resistance (for a review see1). Because of marize and discuss available data on the myo-in- these properties, inositol have been classified as ositol safety both in non-clinical and clinical set- “insulin sensitizing agent”2. tings. The main outcome was that only the highest In the recent years, inositol has found more dose of myo-inositol (12 g/day) induced mild and more space in the reproductive clinical prac- gastrointestinal side effects such as nausea, fla- tice3-6. Indeed, since the main therapy for Poly- tus and diarrhea. The severity of side effects did cystic Ovary Syndrome (PCOS) is the use of in- not increase with the dosage. -
Evaluation of Liquid Ammonium Polyphosphate As a Carrier of Iron and Zinc
EVALUATION OF LIQUID AMMONIUM POLYPHOSPHATE AS A CARRIER OF IRON AND ZINC by ; V<P RATMUNDO RALLAN GANIRON B. S. A., University of the Philippines, 1961 A MASTER'S THESIS submitted in partial fulfillment of the requirement for the degree MASTER OF SCIENCE Department of Agronomy KANSAS STATE UNIVERSITY Manhattan, Kansas 1966 Approved by: Jor Professor LP ZGGf it Tj( £/<?7 TABLE OF CONTENTS INTRODUCTION 1 REVIEW OF LITERATURE 3 Iron . 3 Zinc * MATERIALS AND METHODS 13 Fertiliser Materials 13 Field Experiments H Soil Sampling 20 Laaf Sampling 22 Chemical Analysis 22 (a) Zinc 22 (b) Iron 24 (c) Phosphorua 25 (d) Potassium •« 27 (a) Organic Matter 27 (f) pH 27 (g) Protain 27 RESULTS AND DISCUSSIONS 26 SUMMARY AND CONCLUSIONS 4$ ACKNOWLEDGMENT. 51 LITERATURE CITED 52 INTRODUCTION Increasing attention has baan focused to the need of fertilising with micronutrient elements to achieve maximum production and optimum quality of farm crops. The supply of these elements in the soil has become limited in some areas as a result of the introduction of high yielding varieties, better and more intensive cropping practices, and increased use of high analysis fertilisers. In some cases, the ob- served deficiencies of these micronutrients have been man- made due to addition of interfering elements for other pur- poses. For instance there is the copper induced iron chlorosis, copper being introduced as agricultural sprays and the phosphorus induced iron and zinc deficiencies, phos- phorus being introduced to meet the phosphorus requirement of farm crops. How to minimise such interactions and the problems of keeping these micronutrient elements available to the plants when applied to the soil have been the sub- ject of intensive researches. -
Alcohols Combined 1405
ALCOHOLS COMBINED 1405 Formulas: Table 1 MW: Table 1 CAS: Table 2 RTECS: Table 2 METHOD: 1405, Issue 1 EVALUATION: PARTIAL Issue 1: 15 March 2003 OSHA : Table 2 PROPERTIES: Table 1 NIOSH: Table 2 ACGIH: Table 2 COMPOUNDS: (1) n-butyl alcohol (4) n-propyl alcohol (7) cyclohexanol (2) sec-butyl alcohol (5) allyl alcohol (8) isoamyl alcohol (3) isobutyl alcohol (6) diacetone alcohol (9) methyl isobutyl carbinol SYNONYMS: See Table 3. SAMPLING MEASUREMENT SAMPLER: SOLID SORBENT TUBE TECHNIQUE: GAS CHROMATOGRAPHY, FID (Coconut shell charcoal, 100 mg/50 mg) ANALYTE: Compounds above FLOW RATE: 0.01 to 0.2 L/min DESORPTION: 1 mL 5% 2-propanol in CS2 Compounds: (1-3 ) (4-9) VOL-MIN: 2 L 1 L INJECTION -MAX: 10 L 10 L VOLUME: 1 µL SHIPMENT: Routine TEMPERATURE -INJECTION: 220 °C SAMPLE -DETECTOR: 250 - 300 °C STABILITY: See Evaluation of Method. -COLUMN: 35 °C (7 minutes), to 60 °C at 5 °C/minute, hold 5 minutes, up to BLANKS: 2 to 10 field blanks per set 120 °C at 10 °C /minute, hold 3 minutes. CARRIER GAS: He, 4 mL/min ACCURACY COLUMN: Capillary, fused silica, 30 m x 0.32-mm RANGE STUDIED: Not studied [1, 2]. ID; 0.5 µm film polyethylene glycol, DB- wax or equivalent BIAS: Not determined CALIBRATION: Solutions of analyte in eluent (internal OVERALL standard optional) PRECISION (Ö ): Not determined rT RANGE: See EVALUATION OF METHOD. ACCURACY: Not determined ESTIMATED LOD: 1 µg each analyte per sample PRECISION: See EVALUATION OF METHOD. APPLICABILITY: This method may be used to determine two or more of the specified analytes simultaneously. -
Revisions to USP 31–NF 26, Second Supplement
Revisions to USP 31–NF 26, Second Supplement (published May 2008) Published April 2008 General Chapters Monographs:A–C D–N O–S T–Z Monograph Title Section Head Scientific Liaison DANTROLENE SODIUM Dissolution <711> CAPSULES PF 33(4) Pg. 645 DEHYDROACETIC ACID PF 33(4) Title Pg. 703 DEHYDROACETIC ACID PF 33(4) Chemical Info Pg. 703 DEHYDROACETIC ACID PF 33(4) Definition Pg. 703 DEHYDROACETIC ACID PF 33(4) Packaging and storage Pg. 703 DEHYDROACETIC ACID PF 33(4) USP Reference standards <11> Pg. 703 DEHYDROACETIC ACID PF 33(4) Identification Pg. 703 DEHYDROACETIC ACID PF 33(4) Heavy Metals, Method II <231> Pg. 703 DEHYDROACETIC ACID PF 33(4) Loss on drying <731> Pg. 703 DEHYDROACETIC ACID PF 33(4) Melting range, Class I <741> Pg. 703 DEHYDROACETIC ACID PF 33(4) Residue on ignition <281> Pg. 703 DEHYDROACETIC ACID PF 33(4) Assay Pg. 703 DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. Title 784 DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. Definition 784 file:///C|/Documents%20and%20Settings/rwt/Desktop/revisions/usp31nf26secondSupplement03.html[4/26/2011 1:18:07 PM] DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. Packaging and storage 784 DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. Labeling 784 DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. USP Reference stadards 784 DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. Identification 784 DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. Uniformity of dosage units 784 DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. Loss on drying 784 DIDANOSINE TABLETS FOR ORAL SUSPENSION PF 32(3) Pg. -
Notice of Modification to the List of Permitted Food Enzymesto Enable
Notice of Modification to the List of Permitted Food Enzymes to Enable the Use of Lysophospholipase from Trichoderma reesei RF7206 in the Production of Sugars and Dextrins from Starch Notice of Modification – Lists of Permitted Food Additives Reference Number: NOM/ADM-0172 August 10, 2021 Summary Food additives are regulated in Canada under Marketing Authorizations (MAs) issued by the Minister of Health and the Food and Drug Regulations (Regulations). Approved food additives and their permitted conditions of use are set out in the Lists of Permitted Food Additives that are incorporated by reference in the MAs and published on the Canada.ca website. A petitioner can request that Health Canada approve a new additive or a new condition of use for an already approved food additive by filing a food additive submission with the Department's Food Directorate. Health Canada uses this premarket approval process to determine whether the scientific data support the safety of food additives when used under specified conditions in foods sold in Canada. Health Canada’s Food Directorate received a food additive submission seeking approval for the use of lysophospholipase from Trichoderma reesei RF7206 in starch used in the production of dextrins, dextrose, fructose syrups and solids, glucose (glucose syrup), glucose solids (dried glucose syrup), or maltose. The food enzyme is intended to be used at a level consistent with Good Manufacturing Practice1. Its purpose of use is to improve the efficiency of the starch processing. Lysophospholipase is a type of phospholipase. Phospholipase from other microbial sources is already permitted for use in Canada as a food enzyme in certain foods, but not in the production of sugars and dextrins from starch. -
Retention Indices for Frequently Reported Compounds of Plant Essential Oils
Retention Indices for Frequently Reported Compounds of Plant Essential Oils V. I. Babushok,a) P. J. Linstrom, and I. G. Zenkevichb) National Institute of Standards and Technology, Gaithersburg, Maryland 20899, USA (Received 1 August 2011; accepted 27 September 2011; published online 29 November 2011) Gas chromatographic retention indices were evaluated for 505 frequently reported plant essential oil components using a large retention index database. Retention data are presented for three types of commonly used stationary phases: dimethyl silicone (nonpolar), dimethyl sili- cone with 5% phenyl groups (slightly polar), and polyethylene glycol (polar) stationary phases. The evaluations are based on the treatment of multiple measurements with the number of data records ranging from about 5 to 800 per compound. Data analysis was limited to temperature programmed conditions. The data reported include the average and median values of retention index with standard deviations and confidence intervals. VC 2011 by the U.S. Secretary of Commerce on behalf of the United States. All rights reserved. [doi:10.1063/1.3653552] Key words: essential oils; gas chromatography; Kova´ts indices; linear indices; retention indices; identification; flavor; olfaction. CONTENTS 1. Introduction The practical applications of plant essential oils are very 1. Introduction................................ 1 diverse. They are used for the production of food, drugs, per- fumes, aromatherapy, and many other applications.1–4 The 2. Retention Indices ........................... 2 need for identification of essential oil components ranges 3. Retention Data Presentation and Discussion . 2 from product quality control to basic research. The identifi- 4. Summary.................................. 45 cation of unknown compounds remains a complex problem, in spite of great progress made in analytical techniques over 5. -
Visible-Light-Driven Photooxidation of Alcohols Using Surface-Doped Graphitic Carbon Nitride
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is © The Royal Society of Chemistry 2017 Visible-Light-Driven Photooxidation of alcohols using surface-doped graphitic carbon nitride Wuyuan Zhang, Anna Bariotaki, Ioulia Smonou, and Frank Hollmann* Material and Methods Materials Unless stated otherwise all chemicals were purchased from Sigma-Aldrich, Fluka, Acros or Alfa-Aesar with the highest purity available and used without further treatment. Synthesis of g-C3N4 and carbon nanodots doped (CD-C3N4) The g-C3N4 was synthesized via the simple calcination (Carbolite furnace; CWF 12/5, 2400 W) of urea (10.0 g) at 600 °C for 4 h (5 °C/min), a yellowish powder was obtained after the cooling to room temperature.1 The carbon nanodots were synthesized via the thermal decomposition of sucrose with slight modification.2 Briefly, 0.75 g of sucrose was dissolved in 30 mL of MilliQ water and stirred at room temperature for 0.5 h. The solution was transferred into a 45 mL Teflon-lined stainless steel autoclave reactor, and heated at 180 °C for 5 h (10 °C/min). After cooling the reactor to room temperature, a brown mixture was obtained. The mixture was centrifuged (8000 rpm for 20 min), and the pellet was washed with water (3×) and freeze-dried. 3 In order to deposit carbon nanodots to the surface of g-C3N4, Liu et al’s procedures were adopted. Firstly, a stock solution of carbon nanodots (1 mg in 25mL water) was prepared. 15.0 mL of this stock solution was mixed with 15.0 mL of NH4OH (28 %) and sealed in a 45 mL Teflon-lined autoclave reactor. -
Enlarging Knowledge on Lager Beer Volatile Metabolites Using Multidimensional Gas Chromatography
foods Article Enlarging Knowledge on Lager Beer Volatile Metabolites Using Multidimensional Gas Chromatography Cátia Martins 1 , Tiago Brandão 2, Adelaide Almeida 3 and Sílvia M. Rocha 1,* 1 Departamento de Química & LAQV-REQUIMTE, Universidade de Aveiro, Campus Universitário Santiago, 3810-193 Aveiro, Portugal; [email protected] 2 Super Bock Group, Rua do Mosteiro, 4465-703 Leça do Balio, Portugal; [email protected] 3 Departamento de Biologia & CESAM, Universidade de Aveiro, Campus Universitário Santiago, 3810-193 Aveiro, Portugal; [email protected] * Correspondence: [email protected]; Tel.: +351-234-401-524 Received: 30 July 2020; Accepted: 6 September 2020; Published: 11 September 2020 Abstract: Foodomics, emergent field of metabolomics, has been applied to study food system processes, and it may be useful to understand sensorial food properties, among others, through foods metabolites profiling. Thus, as beer volatile components represent the major contributors for beer overall and peculiar aroma properties, this work intends to perform an in-depth profiling of lager beer volatile metabolites and to generate new data that may contribute for molecules’ identification, by using multidimensional gas chromatography. A set of lager beers were used as case-study, and 329 volatile metabolites were determined, distributed over 8 chemical families: acids, alcohols, esters, monoterpenic compounds, norisoprenoids, sesquiterpenic compounds, sulfur compounds, and volatile phenols. From these, 96 compounds are reported for the first time in the lager beer volatile composition. Around half of them were common to all beers under study. Clustering analysis allowed a beer typing according to production system: macro- and microbrewer beers. Monoterpenic and sesquiterpenic compounds were the chemical families that showed wide range of chemical structures, which may contribute for the samples’ peculiar aroma characteristics. -
Hazardous Substance Fact Sheet
Right to Know Hazardous Substance Fact Sheet Common Name: DIOXOLANE Synonyms: 1,3-Dioxolan; Formal Glycol; Glycol Methylene Ether CAS Number: 646-06-0 Chemical Name: 1,3-Dioxolane RTK Substance Number: 0791 Date: February 1999 Revision: April 2008 DOT Number: UN 1166 Description and Use EMERGENCY RESPONDERS >>>> SEE BACK PAGE Dioxolane is a clear, colorless liquid with an Ether-like odor. It Hazard Summary is used in lithium batteries and as a solvent for oils, fats, waxes Hazard Rating NJDOH NFPA and dyes. HEALTH - 1 FLAMMABILITY - 3 REACTIVITY - 2 FLAMMABLE AND REACTIVE POISONOUS GASES ARE PRODUCED IN FIRE CONTAINERS MAY EXPLODE IN FIRE Hazard Rating Key: 0=minimal; 1=slight; 2=moderate; 3=serious; Reasons for Citation 4=severe f Dioxolane is on the Right to Know Hazardous Substance List because it is cited by ACGIH, DOT, and NFPA. f Dioxolane can affect you by ingestion and may be absorbed f This chemical is on the Special Health Hazard Substance through the skin. List. f Contact can irritate and burn the skin and eyes with possible eye damage. f Inhaling Dioxolane can irritate the nose and throat causing coughing and wheezing. f Exposure to Dioxolane may damage the nervous system. f Dioxolane may damage the kidneys. f Dioxolane is FLAMMABLE and REACTIVE and a SEE GLOSSARY ON PAGE 5. DANGEROUS FIRE and EXPLOSION HAZARD. FIRST AID Eye Contact f Immediately flush with large amounts of cool water for at Workplace Exposure Limits least 15 minutes, lifting upper and lower lids. Remove ACGIH: The threshold limit value (TLV) is 20 ppm averaged contact lenses, if worn, while flushing. -
Development and Optimization of Organic Based Monoliths for Use in Affinity Chromatography
University of Nebraska - Lincoln DigitalCommons@University of Nebraska - Lincoln Student Research Projects, Dissertations, and Theses - Chemistry Department Chemistry, Department of Winter 12-2-2011 Development and Optimization of Organic Based Monoliths for Use in Affinity Chromatography Erika L. Pfaunmiller University of Nebraska-Lincoln, [email protected] Follow this and additional works at: https://digitalcommons.unl.edu/chemistrydiss Part of the Analytical Chemistry Commons Pfaunmiller, Erika L., "Development and Optimization of Organic Based Monoliths for Use in Affinity Chromatography" (2011). Student Research Projects, Dissertations, and Theses - Chemistry Department. 28. https://digitalcommons.unl.edu/chemistrydiss/28 This Article is brought to you for free and open access by the Chemistry, Department of at DigitalCommons@University of Nebraska - Lincoln. It has been accepted for inclusion in Student Research Projects, Dissertations, and Theses - Chemistry Department by an authorized administrator of DigitalCommons@University of Nebraska - Lincoln. DEVELOPMENT AND OPTIMIZATION OF ORGANIC BASED MONOLITHS FOR USE IN AFFINITY CHROMATOGRAPHY by Erika L. Pfaunmiller A THESIS Presented to the Faculty of The Graduate College at the University of Nebraska In Partial Fulfilment of Requirements For the Degree of Master of Science Major: Chemistry Under the Supervision of Professor David S. Hage Lincoln, Nebraska December, 2011 DEVELOPMENT AND OPTIMIZATION OF ORGANIC BASED MONOLITHS FOR USE IN AFFINITY CHROMATOGRAPHY Erika L. Pfaunmiller, M.S. University of Nebraska, 2011 Adviser: David S. Hage Affinity chromatography is an important and useful tool for studying biological interactions, such as the binding of an antibody with an antigen. Monolithic supports offer many advantages over traditional packed bed supports in affinity chromatography, including their ease of preparation, low back pressures and good mass transfer properties. -
Product Information Sheet
September 17, 2015 productISOVACTIN information AA PLUS Nutrients 8.5 fl oz (250mL) per 100mL SKU 37002 Calories 186 74 Calories From Fat 57 23 NET WEIGHT 2 GAL (7.5 L) Protein Equivalent, g 20 8 Free Amino Acids, g 22 9 SERVING SIZE 8.5 fl oz (250mL) Carbohydrates, g 13 5 Sugar, g 5 2 SERVINGS PER PACKAGE 30 Sugar Alcohols, g 0 0 Dietary Fiber, g 2.8 1 Fat, g 6 2.4 24359-0702-03 REIMBURSEMENT CODE Saturated Fat, g 0.5 0.2 (for USA only) Trans Fat, g 0.0 0.0 DHA, mg 150.0 60.0 Cholesterol, mg 0.4 0 MEDICAL FOOD PRODUCT Vitamin A, IU 1100.0 440.0 For the dietary management of Isovaleric Acidemia. Dispensed by prescription. Vitamin C, mg 40.0 16.0 Isovactin AA Plus is a ready-to-drink metabolic formula product for Isovaleric Acidemia Vitamin D, IU 620.0 248.0 patients, over 1 year of age. Isovactin contains an advanced fortification blend. Product Vitamin E, IU 10.0 4.0 Vitamin K1, mcg 20.0 8.0 comes in a 250 mL carton. Vitamin K2 (MK-7), mcg 20.0 8.0 Thiamin (B1), mg 0.5 0.2 Riboflavin (B2), mg 0.5 0.2 Niacin (B3), mg 6.6 2.6 PRECAUTIONS For the dietary management of Isovaleric Acidemia (IVA) and Vitamin B6, mg 0.5 0.2 other disorders of leucine metabolism. Use as directed by physician. Must be Folic acid, mcg 186.0 74.4 administered under medical supervision only. -
Consolidated Version of the Sanpin 2.3.2.1078-01 on Food, Raw Material, and Foodstuff
Registered with the Ministry of Justice of the RF, March 22, 2002 No. 3326 MINISTRY OF HEALTH OF THE RUSSIAN FEDERATION CHIEF STATE SANITARY INSPECTOR OF THE RUSSIAN FEDERATION RESOLUTION No. 36 November 14, 2001 ON ENACTMENT OF SANITARY RULES (as amended by Amendments No.1, approved by Resolution No. 27 of Chief State Sanitary Inspector of the RF dated 20.08.2002, Amendments and Additions No. 2, approved by Resolution No. 41 of Chief State Sanitary Inspector of the RF dated15.04.2003, No. 5, approved by Resolution No. 42 of Chief State Sanitary Inspector of the RF dated 25.06.2007, No. 6, approved by Resolution No. 13 of Chief State Sanitary Inspector of the RF dated 18.02.2008, No. 7, approved by Resolution No. 17 of Chief State Sanitary Inspector of the RF dated 05.03.2008, No. 8, approved by Resolution No. 26 of Chief State Sanitary Inspector of the RF dated 21.04.2008, No. 9, approved by Resolution No. 30 of Chief State Sanitary Inspector of the RF dated 23.05.2008, No. 10, approved by Resolution No. 43 of Chief State Sanitary Inspector of the RF dated 16.07.2008, Amendments No.11, approved by Resolution No. 56 of Chief State Sanitary Inspector of the RF dated 01.10.2008, No. 12, approved by Resolution No. 58 of Chief State Sanitary Inspector of the RF dated 10.10.2008, Amendment No. 13, approved by Resolution No. 69 of Chief State Sanitary Inspector of the RF dated 11.12.2008, Amendments No.14, approved by Resolution No.