Nanodevices for THz Applications

Tomás González University of Salamanca, Spain

Research Group on Devices THz Nanodevices at USAL

 Research Group on Semiconductor Devices - Modeling of nanodevices for THz applications - Design of optimized structures (feedback to technology)

 THz Laboratory - Detection and emission of THz radiation from plasma wave nanodevices - Time-domain and imaging in the THz range

T. González - Nanodevices for THz Applications December 12, 2012 Research Group on Semiconductor Devices

http://campus.usal.es/~gelec/ CONTACT: Prof. Tomás González ([email protected]) Staff: 8 permanent researchers, 3 post-doc, 2 students Collaborations with several EU (IEMN, Chalmers, Manchester, Montpellier, etc.) and USA Labs. (Rochester)

Monte Carlo simulation of high-frequency nanodevices InGaAs/InAlAs, InAs/AlSb and GaN/AlGaN HEMTs

RESEARCH LINES

(FP6 project METAMOS) InGaAs based THz ballistic nanodevices (FP5 project NANOTERA ) Advanced Si MOSFETs

100nm TBJs YBJs MUX/DEMUX SSDs

Coordinator of the FP7 STREP Project ROOTHz (FP7-243845) Characterization Laboratory (DC-GHz) Semiconductor Nanodevices for Room Temperature THz Emission and Detection - http://www.roothz.eu/

GaN diodes InGaAs/InAlAs diode Research Group on Semiconductor Devices EQUIPMENT Computer Clusters Probe station (Cascade M150)

Keithley 4200: DC and pulsed VNA Agilent PNA-X: measurements (Keithley 4225) RF measurements up to 43.5 GHz THz Laboratory

Contact: Dr. Yahya Meziani ([email protected])

Plasma-wave nanodevices

A glimpse of the considered structures:

Doubly interdigitated grating Strained Si/SiGe n-MODFET gates in III-V HEMT

THz detectors based on transistors THz Laboratory

Si/SiGe MODFETs used as sensors in THz signals detection

Si/SiGe MODFETs used as sensors in THz imaging THz Laboratory

Facilities

Terahertz Spectroscopy System Probestation

THz-Time Domain Spectroscopy System: EKSPLA Cascade Summit 11000B manual probestation with

Spectrometer+Ti:Sapphire Laser (Spectra-Physics) FemtoGuard® and PurelineTM technologies (200mm-chuck)

THz imaging: Gunn Diode at 0.2TH + frequency tripler + Agilent B1500 (4 SMUs, 1 multifreq CMU and 1 WG/FMU

OutlineOutline

 Introduction. Importance of THz

 ROOTHz Project

 Self Switching Diodes (SSDs)

 Conclusions / Perspectives

T. González - Nanodevices for THz Applications December 12, 2012 The THz Band

1 THz = 1012 Hz THz range (100 GHz to 10 THz) (300 GHz to 3 THz, 1 - 0.1 mm)

T. González - Nanodevices for THz Applications December 12, 2012 Potential applications

THz radiation can penetrate poor weather, dust and smoke far better than or visible systems.

Aeronautics: guidance and landing Satellite Telemetry

Image of sea surface temperature (European Space Agency)

T. González - Nanodevices for THz Applications December 12, 2012 Potential applications: medical diagnosis

THz radiation can penetrate organic materials without ionizing

Readily absorbed by water: distinguish between materials with varying water content

Medical imaging

Skin Cancer Detection

Courtesy of Teraview Courtesy of Teraview

T. González - Nanodevices for THz Applications December 12, 2012 Potential applications: security

THz radiation can penetrate dielectrics such as windows, paper, clothing and in certain instances even walls

T. González - Nanodevices for THz Applications December 12, 2012 Potential applications: testing

THz radiation can penetrate dielectrics such as windows, paper, clothing and in certain instances even walls

Non-destructive testing: package inspection

Courtesy of Teraview

T. González - Nanodevices for THz Applications December 12, 2012 Potential applications: security

THz radiation can penetrate dielectrics such as windows, paper, clothing and in certain instances even walls

THz radiation can penetrate organic materials without ionizing

Weapon or Explosive Detection (metallic or non metallic)

Courtesy of Qinetiq Courtesy of Qinetiq Courtesy of Thruvision

T. González - Nanodevices for THz Applications December 12, 2012 Potential applications: security

THz radiation can penetrate dielectrics such as windows, paper, clothing and in certain instances even walls

Full-body security screening, body scanners

Passive Detection - no THz source is needed

T. González - Nanodevices for THz Applications December 12, 2012 Potential applications: spectroscopy

THz radiation can be used to identify spectral fingerprints of explosives, narcotics, or active pharmaceutical ingredients THz Spectroscopy

Active Detection - THz sources are needed (narrow or broadband)

Driving force of THz technology so far: spectroscopy, imaging, sensing

T. González - Nanodevices for THz Applications December 12, 2012 Potential applications: communications

T. González - Nanodevices for THz Applications December 12, 2012 Evolving THz market

T. González - Nanodevices for THz Applications December 12, 2012 The THz gap

PHOTONICS THz Gap ELECTRONICS

All-optical sources All-electronic sources • Mixing lasers with close frequencies • Gunn diodes + frequency multipliers (Schottky diodes) • Excitation of or superconductors with fs laser pulses • Quantum cascade lasers Very low power in the THz range

Bulky and expensive equipment Backward wave oscillators - BWOs Useful for spectroscopy and sensing, but (vacuum electronic device) not for communications

T. González - Nanodevices for THz Applications December 12, 2012 The THz gap

Signal generation at THz frequencies

500 GHz – 5 THz

Quantum cascade lasers (QCL) QCL at cryogenic T Frequency multipliers _ Other electronic devices: amplifiers, RTDs, IMPATT and Gunn diodes

SemiconductorPROBLEM Nanodevices for RoomLack Temperature of a compact, THz room-temperature, The THz Gap Emissionhigh-power, and semiconductor Detection (ROOTHztunable source Project) Source: T. H. Crowe, W. L. Bishop, D. W. Porterfield, J. L. Hesler, and R. M. Weikle “Opening the Terahertz Window with Integrated Diode Circuits” IEEE J. Solid-State Circuits 40, 2104 (2005)

T. González - Nanodevices for THz Applications December 12, 2012 OutlineOutline

 Introduction. Importance of THz

 ROOTHz Project

 Self Switching Diodes (SSDs)

 Conclusions / Perspectives

T. González - Nanodevices for THz Applications December 12, 2012 The Project

Semiconductor Nanodevices for Room Temperature THz Emission and Detection (ROOTHz Project)

• Funded under: 7th FWP (Seventh Framework Programme) • Area: FET Open (ICT-2007.8.0) • Project Reference: 243845 • Total cost: 2.1 M€ • EU contribution: 1.57 M€ • Execution: from 1st January 2010 to 30th June 2013 • Duration: 42 months • Website: www.roothz.eu

T. González - Nanodevices for THz Applications December 12, 2012 Partners

J. Grahn Chalmers University of Technology Gothenburg, Sweden A.M. Song The University of Manchester Manchester, UK

C. Gaquiere Coordinator: J. Mateos Institut d’Electronique Microélectronique University of Salamanca et de Nanotechnologie, Lille, France Salamanca, Spain

T. González - Nanodevices for THz Applications December 12, 2012 Semiconductor nanodevices in ROOTHz

Final objective: fabrication of THz detectors and emitters with the same technology

Self Switching Diodes (SSDs)

Ohmic Ohmic

Contact Contact Contact Contact Insulating Trenches Current

Cap Layer Top View Barrier Channel Narrow Bandgap Buffer Wide Bandgap Semiconductors (NBG): Semiconductors (WBG): InGaAs/AlInAs GaN/AlGaN InAs/AlSbSlot Diodes (Ungated HEMTs)

T. González - Nanodevices for THz Applications December 12, 2012 OutlineOutline

 Introduction. Importance of THz

ROOTHz Project

 Self Switching Diodes (SSDs)

 Conclusions / Perspectives

T. González - Nanodevices for THz Applications December 12, 2012 Self-Switching Diodes (SSDs)

1 µm 3.0 2.5 W approx. 60 nm 2.0 A) W approx. 70 nm

 1.5 1.0

Current ( 0.5 0.0 -0.5 -3 -2 -1 0 1 2 3 V (V)

– – – – – nanochannel d doping + + + + + InP – + InP – – – – – + + + + + InGaAs

V<0, channel closed V>0, channel open InP - substrate InGaAs channel

T. González - Nanodevices for THz Applications December 12, 2012 Self-Switching Diodes (SSDs)

Simple technological Tuneable threshold voltage process: etching of insulating from almost zero to more than trenches on a semiconductor ten volts by adjusting the surface channel width

Easy downscaling and parallelization: THz Adequate geometry operation can be for the onset of Gunn obtained oscillations

T. González - Nanodevices for THz Applications December 12, 2012 Self-Switching Diodes (SSDs)

• THz Detection: non-linear I-V characteristics  Use of NBG materials (Room Temperature ballistic transport) for increased sensitivity and broadband

• THz Emission: Gunn Effect in InGaAs, and GaN !!  Use of WBG materials for increased power and frequency

• Planar geometry (and antennas) allow for a better coupling

• Parallelization for enhanced performances (and correct thermal management)

T. González - Nanodevices for THz Applications December 12, 2012 OutlineOutline

 Introduction. Importance of THz

 ROOTHz Project

 Self Switching Diodes (SSDs)  SSDs as THz detectors  Conclusions / Persp.  SSDs as THz emitters

T. González - Nanodevices for THz Applications December 12, 2012 SSDs as THz detectors: experiments

B 20 V 16

12 A)  8 2DEG 4

Current( 0 4 diodes in 3 m -4 parallel -1.0 -0.5 0.0 0.5 1.0 Voltage (V) 0 1 mm -5 RoomResponsivity temperature 1330THz V/W detection @ 12 K -10 -15 150 mV/mW Free Electron

Laser at 1.5 THz -20 -25 -30 300 mV/mW T = 300 K Output DC Voltage (mV) Voltage DC Output -35 0.0 0.2 0.4 0.6 0.8 C. Balocco et al., Appl. Phys. Lett. 98, 223501 (2011) Bias Current (A)

T. González - Nanodevices for THz Applications December 12, 2012 SSDs as THz detectors: experiments

V

2DEG THz imaging using black body radiation

4 diodes in 3 m parallel

T. González - Nanodevices for THz Applications December 12, 2012 SSDs as THz detectors: experiments

Interdigital InGaAs mesa with 2000 etched SSDs

600nm

106 ) 5 1/2 10 1/f noise • Corner frequency below 100 kHz 104 even at relatively high biases 103 200 nA 2 1/2 10 300 nA • NEP @ 110 GHz ~ 65 pW/Hz comparable to SBD 500 nA 101 1 A 2 A

Voltage noise (nV/Hz no bias 100 100m 1 10 100 1k 10k Noise can be reduced by increasing Frequency (Hz) the number of SSDs in parallel

T. González - Nanodevices for THz Applications December 12, 2012 SSDs as THz detectors: Monte Carlo simulations

• THz Detection: non-linear I-V characteristics  Use of NBG materials (Room Temperature ballistic transport) for increased sensitivity and broadband.  Possibility for RESONANT DETECTION

2.0 AC to DC 1.4 THz W =20 nm 1.5 rectification V In0.53Ga0.47As T=300 K Vo=0.25 V

1.0

WC=50 nm

0.5

Rectified DC current(A/m) V=V sen(2pf) WH=5 nm o I 0.0

175 nm LC=250 nm 175 nm 0.1 1 Frequency (THz)

Enhanced rectification in the THz range (tunable by geometry)

T. González - Nanodevices for THz Applications December 12, 2012 THz dynamics in SSDs: pump-probe experiments

Schematics of electro-optic Sampling beam (EO) sampling 800 nm

EO crystal fs laser excitation beam 400 nm

Experiments done at Univ. of Rochester Bias by Jie Zhang and Roman Sobolewski

T. González - Nanodevices for THz Applications December 12, 2012 SSDs as THz detectors: pump-probe experiments

3000 8

6

2000 Experimental 4

2 1000 0

Current (A/m) Current V=1.0 V -2

0 u.) (a. Experimental V=0.0 V -4 V=-1.0 V -1000 -6 15 17 19 21 23 Time (ps)

MC simulations predict a much sharper peak THz oscillations may be emitted from the (1/3 FWHM), but the shape is similar excitation of the SSDs with fs-lasers

T. González - Nanodevices for THz Applications December 12, 2012 SSDs as THz detectors: InAs technology

 Progress in InAs SSDs technological process

higher mobility  improved responsivity and fc

29 nm

38 nm

650 nm

T. González - Nanodevices for THz Applications December 12, 2012 OutlineOutline

 Introduction. Importance of THz

 ROOTHz Project

 Self Switching Diodes (SSDs)  SSDs as THz detectors  Conclusions / Persp.  SSDs as THz emitters

T. González - Nanodevices for THz Applications December 12, 2012 SSDs as THz emitters: Gunn oscillations

(a)

• Suitable geometry: vertical trench  focuses n+ n- n n+ the electric field at the cathode side of the channel, and anode voltage increases electron

concentration  onset of domains and propagation along the channel (b) Cointegration with detectors

• Material: GaN channels

 High saturation velocity, low energy relaxation time  high frequency  High threshold field  high power  Planar design  SSDs in parallel  facilitates heat dissipation

T. González - Nanodevices for THz Applications December 12, 2012 SSDs as THz emitters: Monte Carlo simulations

Monte Carlo Simulations 2.0 60 V (a) WV=100 nm GaN T=300 1.6 K Gunn WC=75 nm 1.2 50 V Oscillations

W =50 nm I (mA) H in GaN 0.8 40 V SSDs 150 nm LC=900 nm 500 nm 30 V 0.4 10 15 20 25 30 35 40 45 50 Time (ps) 1.0 450 (b) 0.8

0.6 400 0.4

I (mA) 0.2 350

0.0 (GHz) Frequency 300 -0.2 -40 -20 0 20 40 60 25 30 35 40 45 50 55 60 65 V (V) V (V) Oscillation frequencies above 400 GHz (voltage controlled and tunable by geometry)

T. González - Nanodevices for THz Applications December 12, 2012 Experimental results: Run 1 of GaN SSDs

16 parallel GaN SSDs

 Unexpectedly high surface charge  too low electron concentration in the channel  no Gunn oscillation observed (on probe electrical measurements)  Monte Carlo constant surface charge model fails  new model (self-consistent model) in order to fit the experimental results

T. González - Nanodevices for THz Applications December 12, 2012 Experimental results: Run 2 of GaN SSDs

New strategies in the design

Wider square SSDs V-Shape SSDs

(a) 100 nm (b)

100 nm 4 00 nm

W=500 nm, 750 nm Win=350 nm 50nm 4 =

out 50 nm 400 nm 50 nm W V-shape GaN SSDs

200 nm L= 500 nm 450 nm 200 nm L=500 nm 450 nm

1.5 1.5 L= 500 nm L= 500 nm L= 500 nm

1.0 W=500 nm W=750 nm Win=350 nm 1.0 W =450 nm 0.5 out 0.5

0.0 (a) (b) (c) 0.0 -0.5 -0.5

Current (mA) Current Experimental Experimental Experimental (mA) Current -1.0 MC MC MC -1.0 -1.5 -1.5 -10 -5 0 5 10 15 20 -10 -5 0 5 10 15 20 -10 -5 0 5 10 15 20 Bias (V) Bias (V) Bias (V) New Monte Carlo Self-consistent surface charge model GOOD AGREEMENT T. González - Nanodevices for THz Applications December 12, 2012 Experimental results: Run 2 of GaN SSDs

New strategies in the design

Wider square SSDs V-Shape SSDs

(a) 100 nm (b)

100 nm 4 00 nm

W=500 nm, 750 nm Win=350 nm 50nm 4 =

out 50 nm 400 nm 50 nm W V-shape GaN SSDs

200 nm L= 500 nm 450 nm 200 nm L=500 nm 450 nm

 Square SSDs: W ≥ 500 nm to provide Gunn oscillations (much wider that initially expected!!)  VERY STRONG HEATING

 V-shaped SSDs facilitate the onset of oscillations: Heating is much o Lower threshold voltage (30V instead of 50V in square SSDs) reduced with o Narrower channels are needed (W ≥ 200 nm) the V-shape geometry

T. González - Nanodevices for THz Applications December 12, 2012 Experimental results: Run 2 of GaN SSDs

Free space measurements (devices with antenna mounted on PCB and Si lens)

Pulsed-mode measurements developed In spite of large effort in characterization of emission in RF and THz no evidence of oscillations were found in Run 2

T. González - Nanodevices for THz Applications December 12, 2012 Experimental results: Run 3 of GaN SSDs

Run 3 fabricated

T. González - Nanodevices for THz Applications December 12, 2012 Experimental results: Run 3 of GaN SSDs

Bow-tie Emission not perpendicular Z ~ 75 Ω

720 µm 4 µm

Integration with adequately Equiangular spiral designed Emission perpendicular Z ~ 120 Ω broadband antennas 1.8 mm

T. González - Nanodevices for THz Applications December 12, 2012 Experimental results: Run 3 of GaN SSDs

Good control of the technology

T. González - Nanodevices for THz Applications December 12, 2012 Experimental results: Run 3 of GaN SSDs

Free-space characterization Structures designed for optimized heating

Higher bias can be applied (above the threshold for the onset of oscillations)

No emission observed yet Guided-wave characterization under probes

T. González - Nanodevices for THz Applications December 12, 2012 Desynchronization of the oscillations: MC simulations

Single SSD

2-SSDs

4-SSDs

More SSDs in parallel, more An external resonator is pronounced desynchronization needed for synchronization

T. González - Nanodevices for THz Applications December 12, 2012 Resonant circuit modeling

• Series and parallel RLC circuits already implemented

• Circuit equations (solved in the time domain) coupled to the MC current

 The voltage between terminals is fixed by the RLC circuit

T. González - Nanodevices for THz Applications December 12, 2012 Resonant circuit modeling

Resonant frequency f0=1/(2pLC) 0.20 Constant quality factor Q=117.8 300K 0.15 500K

C (fF) L (nH) R (MW) f0 0.10 Heating is not 0.073 33.0 2.5 102.3 blocking the

0.061 27.5 2.5 122.7 (%) Efficiency 0.05 oscillations 0.050 22.5 2.5 150.1 0.00 0.042 19.0 2.5 177.7 100 200 300 400 500 600 0.039 17.5 2.5 192.9 f0 (GHz) 0.031 14.0 2.5 241.1 0.022 10.0 2.5 337.6 Crosstalk capacitance 0.020 9.0 2.5 375.1 New design iteration of about 5 fF can kill with integrated 0.017 7.5 2.5 450.2 the oscillations resonant circuit 0.010 4.5 2.5 750.3 needed For N parallel diodes  C×N, L/N and R/N Very small Around 100 SSDs in parallel capacitances needed to avoid its effect

T. González - Nanodevices for THz Applications December 12, 2012 OutlineOutline

 Introduction. Importance of THz

 ROOTHz Project

 Self Switching Diodes (SSDs)

 Conclusions / Perspectives

T. González - Nanodevices for THz Applications December 12, 2012 Future work

 THz detection:

• Fabrication, THz characterization and optimization of InAs SSDs as detectors

• Spectral characterization of the responsivity of the SSDs (InGaAs, GaN and InAs) Identification of plasma resonances

• GaN SSDs as THz detectors (two patents filed): - Mixing of THz signals (heterodyne detection) - Direct demodulation of THz signals (ultra-high bandwidth detection)

• Graphene SSDs

 THz emission (main focus):

• High frequency (>900 GHz) FTIR cryogenic detection

• Design and fabrication of optimized structures with resonant circuits

T. González - Nanodevices for THz Applications December 12, 2012 Acknowledgements

ROOTHz: Semiconductor Nanodevices for Room Temperature THz Emission and Detection www.roothz.eu

J. Mateos A. M. Song C. Gaquiere J. Grahn S. Pérez A. Rezazadeh G. Ducournau P. A. Nilsson B. G. Vasallo M. Hallsall P. Sangaré H. Rodilla I. Íñiguez-de la-Torre C. Balocco A. Westlund J. Millithaler L. Zhang H. Zhao A. Íñiguez-de la-Torre Y. Alimi S. García

J. Torres L. Varani Jie Zhang P. Nouvel Roman Sobolewski A. Penot Institut d’Électronique du Sud Université Montpellier II

T. González - Nanodevices for THz Applications December 12, 2012 Thanks for the attention !

T. González - Nanodevices for THz Applications December 12, 2012 T. González - Nanodevices for THz Applications December 12, 2012