K/EM-534 K-25
OAK RIDGE
K-25 SITE COMPREHENSIVE ENVIRONMENTAL RESPONSE, COMPENSATION, AND LIABILITY ACT SECTION 120(h) ASSESSMENT FOR COLONIE INTERIM STORAGE SITE (CISS), COLONIE, NEW YORK
LOCKHEED HI A K rTWV^
JULY 1997
MANAGED BY LOCKHEED MARTIN ENERGY SYSTEMS, INC. FOR THE UNITED STATES DEPARTMENT OF ENERGY 200. le Colonie 01.06 0014 UCN-13671 {16 fr«5) Illilllllllllll DISCLAIMER
This report was prepared as an account of work sponsored by an agency of the United States Government. Neither the United States Government nor any agency thereof, nor any of their employees, makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness, or use-fulness of any information, apparatus, product, or process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific commercial product, process, or service by trade name, trademark, manu-facturer, or otherwise, does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United States Government or any agency thereof. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Government or any agency thereof. K/EM-534
COMPREHENSIVE ENVIRONMENTAL RESPONSE, COMPENSATION, AND LIABILITY ACT SECTION 120 (h) ASSESSMENT FOR COLONIE INTERIM STORAGE SITE (CISS), COLONIE, NEW YORK
July 1997
Prepared by the Environmental Compliance Organization East Tennessee Technology Park Oak Ridge, Tennessee 37831-7236 managed by LOCKHEED MARTIN ENERGY SYSTEMS, INC for the This document has bem approved for nloai» U.S. DEPARTMENT OF ENERGY thejxiblk by: <^HAX^^A_^^' under contract DE-AC05-84OR21400 7/30/97 T«**ic*l Information Ori&«r_^/3v Date K-25 Site TABLE OF CONTENTS
Page
EXECUTIVE SUMMARY iii
1. PROPERTY IDENTIFICATION 1
2. TITLE SEARCH 4
3. FEDERAL, STATE, AND LOCAL RECORDS SEARCH 6
4. PAST AND PRESENT ACTIVITIES 8
4.1 PAST ACTIVITIES FOR THE COLONIE INTERIM STORAGE SITE (CISS) UNDER COMMERCIAL OWNERSHIP 8 4.2 PAST AND PRESENT ACTIVITIES AT THE COLONIE INTERIM STORAGE SITE (CISS) UNDER DOE OWNERSHIP 9 4.3 PAST AND PRESENT ACTIVITIES FOR THE ADJACENT PROPERTY 13
5. RESULTS OF VISUAL AND PHYSICAL INSPECTIONS 15
5.1 VISUAL AND PHYSICAL INSPECTIONS OF THE CISS 15 5.2 VISUAL AND PHYSICAL INSPECTION OF ADJACENT PROPERTY 16
6. RESULTS OF SAMPLING CONDUCTED IN CONJUNCTION WITH THE PROPOSED EASEMENT 17
REFERENCES 18
APPENDIX A
APPENDIX B
APPENDIX C 1 EXECUTIVE SUMMARY The Colonie Interim Storage Site (CISS) is located at 1130 Central Avenue, Colonie, New York and is owned by the Department of Energy (DOE). The site is undergoing remediation under DOE's Formerly 1 Utilized Sites Remedial Action Program (FUSRAP). The Department of Energy is proposing to grant an easement right-of-way over a portion of the CISS to the Niagara Mohawk Power Corporation to accommodate DOE's needs for relocating an existing transmission line and associated tower structures to I the new right-of-way. This action will enable DOE to accomplish remediation and stabilization of soil having radiological and chemical contamination within the existing right-of-way. Although DOE will grant a permanent easement, there will be no change in ownership of the property. The area in the immediate 1 vicinity of the tower structures in the new right-of-way will be remediated prior to their installation. The remediation of the remaining area of the new easement right-of-way is scheduled as part of the remaining 1 remedial actions to be completed at the CISS. A review of government records and an inspection of the property was performed in accordance with Section 120(h) of the Comprehensive Environmental Response, Compensation, and Liability Act to identify 1 any areas on the property where hazardous substances and petroleum products were stored for one year or more, known to have been released, or disposed of. Section 120(h) also requires that DOE include in any contract for the sale or transfer of real property, which is owned by the United States, a notice of the i time at which storage, release, or disposal of hazardous substances or petroleum products have taken place.
The following is a summary of the results of the CERCLA 120(h) evaluation performed:
• There is documentation that hazardous substances and other hazardous chemicals were stored at the CISS for one year or more during the period of commercial operation by the property's previous owners in quantities meeting or exceeding the 1000 kg reporting threshold of 40 CFR 373, the implementing regulations for CERCLA 120(h). Chemical inventories were also present on site when DOE assumed ownership of the property and remained on-site pending off-site disposal.
• There is evidence that a release or disposal of hazardous substances or petroleum products in excess of the substance's reportable quantity (RQ) occurred at the CISS during its operation by National Lead Industries.
• There is radiological contamination at the CISS in excess of the release limits specified in DOE Order 5400.5 and 10 CFR 835. Additionally, surveys found radiological contamination at 56 vicinity properties. Fifty-three of these properties have been remediated. This radiological contamination occurred during the period of ownership by National Lead Industries as a result of airborne stack emissions from the plant.
• The CISS is not on the Environmental Protection Agency's National Priorities List (NPL) of Superfund sites under CERCLA.
• There is surface and subsurface radiological, chemical, and metals contamination in, and adjacent to, the footprint of the proposed easement.
in I I 1. PROPERTY IDENTIFICATION The Colonie Interim Storage Site (OSS) is located at 1130 Central Avenue in the Town of Colonie, Albany County, New York and consists of approximately 11.2 acres in area. The location of this property is depicted 1 in Figure 1 and Figure 2'. The U.S. Department of Energy (DOE) is planning to grant an easement to Niagara Mohawk Power Company for the installation of overhead electrical transmission lines and associated tower structures at the C1SS. The new easement will replace an existing easement over the property. The general I area of the proposed easement is shown on the site drawing in Appendix A, page A-2. The exact location of the easement is subject to minor changes before the final real estate documents are prepared between DOE and I the Niagara Mohawk Power Company. 1 I 1 I I I 1 I I I
I 1 The main building and small storage sheds to the southwest depicted on Figure 2 have been demolished. The figure also shows the relation to the site of the former Patroons Lake which was partially I filled by National Lead. The remaining portion of the lake was drained. I I 1 I I 1 1 I I I I I I I 1 I
I 0 12 3 4 Kilometers I 1 Figure 1. Geographical Location of the Colonie Interim Storage Site I Figure 2. Colonie Interim Storage Site Map (Showing Sit i Structures) FUS/COLONIE EE/CAM25M I I 2. TITLE SEARCH On June 30, 1997, the Albany County (New York) Clerk's Office was visited and a review was conducted I of the recorded deeds documenting previous ownership of the land that comprises the present CISS property. These deed records document that on April 28, 1923, the Embossing Company purchased two parcels of land (single purchase) from Redacted - Privacy Act . These two parcels comprise most of the present-day CISS. A review of deeds documenting ownership of the parcels before their sale by the Fords to the I Embossing Company produced no evidence that they had been utilized for the storage or disposal of hazardous substances and/or petroleum products.
I On January 17, 1927, the Magnus Company, Inc. purchased the above-mentioned parcels from the Embossing Company. Magnus Company, Inc. expanded the size of the site with the purchase of two additional small parcels of land on March 25,1927. Separate transactions consummated the purchase of these I parcels, one parcel being conveyed by George Ford, and the other being conveyed by Lillian Ford. A review of deeds documenting previous ownership of these latter two parcels before their sale to Magnus Company, Inc. produced no evidence that they had been utilized for the storage or disposal of hazardous substances 1 and/or petroleum products.
On October 31, 1936, the National Lead Company purchased the property from Magnus Metal Corporation I (formerly known as Magnus Company, Inc.). Following this initial purchase, National Lead Company purchased an adjacent land parcel on August 25, 1937, from Redacted - Privacy Act (Executor and Trustee of the estate of Redacted - Privacy Act ). Recorded as part of the deed of conveyance is an Albany County Clerk's I Subdivision Map No. 592, which contains a March 12, 1936, boundary survey of the parcel that was made by Sham brook and Browne. Facilities and other features shown on the map indicate that this parcel was 1 previously utilized for recreational purposes only. On January 15, 1940, National Lead Company conveyed a parcel of land containing approximately 2.48 acres of land to the New York Power and Light Corporation. This parcel accommodated the needs of the New I York Power and Light Corporation for a right-of-way for an electrical transmission line system and construction of a substation near Central Avenue. I On May 21, 1956, the Niagara Mohawk Power Company, the successor company of New York Power and Light Corporation, purchased an additional parcel of land for its electrical transmission line right-of-way from Redacted - Privacy Act containing approximately 0.86 acres of land.
1 On March 6, 1959, National Lead Company acquired an adjacent parcel of land (designated as Parcel No. 2) from Redacted - Privacy Act , and in exchange and as part of the consideration, conveyed part of its site (designated as Parcel No. 1) to Redacted - Privacy ActAn Albany County Clerk's Office Subdivision Map that contains I the boundary survey of these two parcels was made a part of the deed of conveyance and is maintained on file in the Albany County Clerk's Office. This survey, dated October 24, 1948, was made by Conrad Hammam.
1 A review of deeds documenting the prior ownership of the above-mentioned parcels conveyed by Redacted - Privacy Act produced no evidence that they had been utilized for the storage or disposal I of hazardous substances and/or petroleum products. I I I On February 28, 1984, DOE acquired the land belonging to National Lead Industries. The land was conveyed to DOE for a sum of $10.00. In exchange for the land, DOE would undertake remediation of the I property.
On August 28, 1984, DOE, with the exception of the land comprising Niagara Mohawk's substation, I acquired all of the land comprising two parcels of Niagara Mohawk's existing electrical transmission right-of- way with Parcel No. 1 containing approximately 0.445 acres and Parcel No. 2 containing approximately 1.69 acres of land. This land became a part of the current CISS, which with the land acquired from National Lead I Industries totals approximately 11.2 acres.
Currently, DOE is in the process of acquiring an additional small parcel of land totaling approximately .023 I acres adjacent to the CISS and the Consolidated Rail Corporation (Conrail) main railroad line to West Albany. This small parcel of land is being acquired so that radioactive contamination resulting from previous industrial operations on the land that now comprises the CISS can be addressed. This land was initially purchased by I the New York Central Rail Road Company ( a predecessor company of Conrail) on December 27, 1858 from the Albany and Schnectady Turnpike Company. A review of this 1858 conveyance deed produced no evidence that the land had been utilized for the storage or disposal of hazardous substances or petroleum products. I However, with the subsequent use of the railroad by coal and diesel locomotives and the use creosoted railroad ties, there is the potential that inadvertent releases of hazardous substances or petroleum products may have I occurred.
5 I I 3. FEDERAL, STATE, AND LOCAL RECORDS SEARCH In addition to the research of the files at the Albany County Clerk's Office, the offices of the DOE Former I Sites Restoration Division (FSRD) and Bechtel National, Inc.(BNI) were visited in Oak Ridge, Tennessee to obtain information and records from cognizant officials on prior and current activities at the site comprising the CISS. The BNI Oak Ridge office maintains a microfilm copy of the site administrative file and other documents (reports, correspondence, etc.) pertaining to the site and dating back to the 1984 time frame. A list I of the files pertaining to the CISS was provided by BNI and documents which appeared to be pertinent were reviewed.
I On June 30, 1997 and July 1, 1997, a visit was made to the CISS to inspect the site. During this visit, on- site records and photographs were reviewed. A reference to 4 drawings prepared by Science Applications International Corporation (SAIC) depicting on-site soil contamination was also identified while on-site. A I request for a copy of these drawings was made to the SAIC Oak Ridge office and these drawings were provided.
I During the review, the following aerial photographs and maps reflecting prior uses of the land were examined. A copy of these photographs and maps is maintained on file in the Lockheed Martin Energy Systems, Inc. Real Estate Office. They are also reasonably obtainable through other federal, state, and local I governmental agencies, and private sector sources. Selected photographs and maps are included in Appendix A of this report.
I Aerial Photographs Source Mid-1980's Aerial Photograph (Appendix A, page A-3 ) BNI I 1995 Aerial Photograph (Appendix A, page A-4) BNI 1996 Aerial Photograph (Appendix A, page A-5) BNI I Topographic Maps Source
Section 1 of 2 of U. S. Geological Survey (USGS) USGS Reston, Va. I Topographic Map (1898 Edition, Reprinted in 1911) (Appendix A, page A-6)
I Section 1 of 2 of U. S. Geological Survey (USGS) USGS Reston, Va. Topographic Map (1927 Edition, Reprinted in 1930) I (Appendix A, page A-7 I Real Estate Maps Source Albany County (NY) Clerk's Subdivision Map 592 Albany County Clerk's office I dated March 12, 1936 (Appendix A, page A-8) I I I
Survey Map dated December 28, 1939, titled, "New Albany County Clerk's office I York Power & Light Corporation - Central Ave. Substation - Property Magnus Metal Corp. - Purchase" • (Copy available on file) Albany County Subdivision Map dated October 24, 1948 Albany County Clerk's office • made by Conrad Hammam (Copy available on file) 1 1 1 1 1 I I I I I I I I I I I I 4. PAST AND PRESENT ACTIVITIES 4.1 PAST ACTIVITIES FOR THE COLONIE INTERIM STORAGE SITE (CISS) UNDER I COMMERCIAL OWNERSHD? Industrial activities at the CISS date back to April 28, 1923, when the Embossing Company purchased a portion of the present-day CISS to construct a facility for manufacturing wood products and toys. Two parcels of land were purchased from Redacted - Privacy Act . A review of deeds documenting 1 ownership of the parcels before their sale by the Fords to the Embossing Company produced no evidence that they had been utilized for the storage or disposal of hazardous substances or petroleum products.
1 On January 17, 1927, Magnus Metal Company, Inc., purchased the property and converted the facility into a brass foundry that manufactured railroad components and brass bearing housings. The manufacturing process used babbit metal, an alloy of lead, copper, and antimony. Bearings were degreased by immersion in 1 acid baths. Two additional small parcels of land were separately purchased by Magnus Metal from Redacted - Privacy Act . A review of deeds documenting ownership of these additional parcels before their sale by the Redacted - Privacy to Act Magnus Metal produced no evidence that they had been utilized for the storage or I disposal of hazardous substances or petroleum products.
On October 31, 1936, National Lead Company purchased the facility from Magnus Metal Corporation 1 (formerly Magnus Metal Company, Inc.) and continued the foundry operations begun by Magnus Metal. An adjacent parcel of property on the west side of the existing facility was also purchased. This parcel included Patroons Lake2. A May 1936 drawing (Appendix A, page A-8) depicts a bath house and concession stand 1 located on the south side of the lake and a road labeled, "road to beach" leading to the lake from Central Avenue. This would imply that the lake area was used for recreational purposes prior to its purchase by National Lead. On January 15, 1940, a portion of this parcel consisting of approximately 2.48 acres and I containing a portion of Patroons Lake was sold to New York Power and Light Company, the predecessor company to Niagara Mohawk. This transfer accommodated the needs of New York Power and Light Corporation for a right-of-way for an electrical transmission line and the construction of an electrical substation I near Central Avenue. Around this time, National Lead began filling in Patroons Lake using among other items used casting sand as fill material. Disposal of these materials also took place on property that belonged to New York Power and Light.
I After World War II, National Lead began casting of aluminum mainframes for the aircraft industry. Brass foundry operations continued until 1960, but by this time, National Lead was engaged in other manufacturing activities involving radioactive materials, primarily depleted uranium but also with some I smaller amounts of thorium and enriched uranium. In 1958, the nuclear division of National Lead began producing items manufactured from uranium and thorium under a license from the Atomic Energy Commission (AEC). Enriched uranium was handled at the facility from approximately 1960-1972 during I which time National Lead received several contracts to manufacture enriched uranium fuel elements for experimental nuclear reactors and to process unirradiated, enriched uranium scrap. The plant also reduced depleted uranium tetrafluoride to depleted uranium metal. Beginning in the 1970's, AEC work declined and I work increased for the Department of Defense in production of deleted uranium munitions, and for commercial business in production of depleted uranium counterweights for aircraft and other ballast weights. In 1980, I 2 Patroons Lake and the associated Patroons Creek are alternatively referred to in many documents I as "Patroon Lake" and "Patroon Creek." I I the Army contract was canceled. Other processes at the plant involved the electroplating of uranium with I nickel and cadmium. In February 1980, the New York Supreme Court issued a temporary restraining order to National Lead barring further operations because of radiological contamination of nearby properties from airborne emissions from the plant's stacks. On May 12, 1980, the temporary restraining order was amended to allow limited operations. With the exception of a small amount of aircraft counterweight production, most 1 of the facility operations were discontinued in 1981. In September of 1983, National Lead indicated to DOE that they intended to discontinue operations at the plant and negotiations began between the two parties for I remediating the site. In the Energy and Water Development Act of 1984, Congress authorized DOE to undertake a decontamination research and development project at the Colonie site. On February 28, 1984, National Lead I entered into an agreement with DOE to transfer ownership of the property for a sum of $ 10.00 and in exchange for DOE assuming the responsibility of remediating the site. Plant operations ceased and DOE placed the site 1 in the Formerly Utilized Sites Remedial Action Program (FUSRAP). On August 28, 1984, DOE, with the exception of the land comprising Niagara Mohawk's substation acquired all of the land comprising the two parcels of Niagara Mohawk's existing electrical transmission right- 1 of-way. This acquired area was included in the CISS. From a review of records, it appears that the transfer of property from Niagara Mohawk to DOE was made to facilitate remediation of the property belonging to New York Power and Light Company, and later Niagara Mohawk, on which National Lead had disposed of I waste materials. Acquiring the property also concluded legal actions that Niagara Mohawk had initiated against National Lead for contaminating this property. I During its years of operation, first by Magnus Metal and later by National Lead, a wide variety of metals and chemicals were used at the facility. The foundry operations used a number of metals including lead, copper, and antimony as constituents in the products and acids in the intermediate production process. The I introduction of uranium operations at the plant by National Lead and the processes used in those operations increased the types of chemicals used on site. Chemicals used in the uranjum plating operation included nickel sulfamate, sodium cyanide, ferric chloride, nitric acid, silicate phosphate, iridite, cadmium metal, nickel metal, boric acid, and perchloroehtylene. Other items in use included carbon tetrachloride, polychlorinated biphenyls I (PCB's), benzene, various acids, and degreasers. Additionally, at least some of the fluorescent light fixtures had ballasts which contained PCBs. A more complete inventory of known hazardous substances, other chemicals, and petroleum products that have been present at the facility is contained in the tables in Appendix B.
4.2 PAST AND PRESENT ACTIVITIES AT THE COLONIE INTERIM STORAGE SITE (CISS) UNDER DOE OWNERSHD?
Since 1984, activities at the CISS have been associated with remediation of the site and nearby properties which radiological surveys indicated were contaminated from past operations at the site. Environmental legacy issues which accompanied the transfer of the property from National Lead to DOE included:
- Radiological contamination of a number of nearby residential and commercial vicinity properties;
- Radiological contamination of the site property;
- Radiological and chemical surface and subsurface soil contamination;
9 - Possibility of groundwater contamination;
- Radiological and chemical contamination of the inside of site buildings; and
- A large amount of radioactive, mixed, and hazardous wastes and hazardous chemicals left on site by National Lead.
When DOE assumed ownership of the property, National Lead's main building dominated the site (see Figure 2 for a site drawing and the aerial photograph in Appendix A, page A-3). The main building covered approximately 3 acres of the site. The building was one story and approximately 20 feet high except for the high bay area and in the northwest corner where there was an upstairs office area. The building sat on a concrete slab. The manufacturing area of the building consisted of four large bays and several smaller rooms around the bay areas. The low bay areas were constructed with unreinforced masonry-bearing walls with steel beams. Some of the roof areas were of sheet metal decking on steel cross beams; other sections were constructed of reinforced concrete. In the high bay area, the building was steel frame with masonry walls. The walls in the high bay area were tied together by structural trusses which supported the roof. In the high bay area, the roof was made of wooden planks on rectangular wood purlins resting on steel trusses. Interior walls were clay tile, brick, or masonry in the bay areas and wood paneling or plaster board in the office area. The roof of the building contained a large number of sloped windows which facilitated interior lighting. Inside the southeast corner of the building, three 10,000 gallon oil tanks supplied fuel to the building's boiler. These tanks can be seen in the lower right corner of the aerial photograph in Appendix C, page C-3. A 1991 radiological characterization of the building showed that virtually all interior surfaces were radiologically contaminated at levels exceeding DOE release guidelines. The contamination was generally in the form of uranium oxide. Concrete floors in the process areas were oily and highly contaminated. Horizontal surfaces and ceilings were also contaminated.
Two reinforced concrete storage buildings were located west of the main building and adjacent to the railroad spur entering the site on the southern side of the site. Together, these two buildings were about 170 feet long, 20 feet wide, and 12 feet high and were divided up into a number of storage bays.
In addressing the environmental legacies associated with the site, DOE actions since 1984 can be generally categorized to:
- Characterize and remediate vicinity properties for radiological contamination;
- Establish an environmental monitoring program;
- Prevent any further off-site contamination;
- Characterize the contamination;
- Characterize wastes and hazardous substances remaining in the building; identify treatment and disposal options and methods, and dispose of these materials;
- Demolish the main building and ancillary structures; and to
- Remediate the soil contamination remaining on site and in those vicinity properties which were not previously addressed.
10 In 1984, 1985, and 1988, 53 of 56 nearby properties having elevated levels of radioactive contamination were remediated by removal of contaminated surface soils and the removal of small amounts of contaminated roofing materials. This material was temporarily stored in the main building and later shipped off-site for disposal. Three vicinity properties; i.e., the Town of Colonie property to the west, the Niagara Mohawk electrical substation, and the Conrail property to the south will be remediated (for radiological contamination only) as part of the remaining response actions.
A large quantity of packaged hazardous chemicals and waste materials were left in the main building by National Lead when the company vacated the premises. These included various acids, bases, and degreasing agents; carbon tetrachloride, benzene, polychlorinated biphenyls (PCBs), cyanide, heavy metals, asbestos, and laboratory and photographic chemicals. A substantial portion of these materials were radioactively contaminated. An inventory of the chemicals left at the site upon National Lead's departure is shown in Appendix B, Table 5. This inventory was included as an appendix in the "Closure Plan for the Colonie Interim Storage Site" prepared by Bechtel National, Inc. in November 1986 and appears to be a complete listing of the materials on site when DOE assumed ownership of the property.
DOE's actions relating to chemical and waste inventories included sampling, analysis, characterization, and consolidation of chemicals; draining, sampling, analysis, and containerization of machine oils; and consolidation of oils containing PCBs. Other actions included stabilization of electroplating liquids, neutralization and solidification of acidic liquids, and solidification of electroplating residues. On December 3, 1984, DOE submitted a Resource Conservation and Recovery Act (RCRA) Part A application to the State of New York Department of Environmental Conservation to obtain a permit for the on-site storage of hazardous waste at the CISS. The majority of the RCRA wastes at the CISS were used oils drained from processing equipment during initial cleanup activities, unused chemical reagents, and other used processed liquids. Some of the RCRA wastes were also radiologically contaminated. Several of the wastes contained heavy metals, cresols, trichloroethylene, and perchloroethylene at concentrations exceeding toxicity characteristic leaching procedures (TCLP) regulatory levels. Wastes were classified as RCRA listed, RCRA characteristic, and radioactive-hazardous mixed wastes. Several of the RCRA wastes required treatment to meet the requirements for off-site disposal at permitted facilities. After bench-scale testing of treatment methods, treatment was performed in the containers in which the waste was stored or in similar containers into which the wastes was transferred. Additional secondary wastes were generated during RCRA closure. These included items such as used personal protective equipment (PPE), spent filters, dirty rags, gloves, etc. Off-site shipments of RCRA wastes subject to the permit commenced in the mid-1980's and continued until 1995 by which time all of the wastes and hazardous chemicals left by National Lead had been removed from the site. In September 1995, DOE submitted a RCRA closure report to the State of New York and on October 17, 1995, the state confirmed receipt of the closure report and terminated DOE's authority to operate as a Treatment, Storage, and Disposal Facility.
In June 1993, DOE issued an "Engineering Evaluation/Cost Analysis (EE/CA) for the Colonie Interim Storage Site (CISS) Buildings." In this report, DOE set forth the alternatives for management and disposition of the main building and the smaller outbuilding located on the property. The alternative selected was to decontaminate the building and then demolish it. Preparatory actions to building demolition included removal of wastes being stored in the building, removal of asbestos containing materials (i.e., insulation, tiles, transite siding), removal of process equipment, and decontamination. Demolition of the building was completed in September 1995. Brick, masonry, and wood used in the building's structure were ground up and presently remain stored on the building's footprint. Some of this material is awaiting shipment for off-site disposal while some of the material will be used as fill in the Patroons Lake area after contaminated soil from that area has
11 been removed. Building demolition activities are depicted in the photographs in Appendix C, pages C-2 and C-3. The site drawing in Appendix C, page C-4 shows the location of the rubble stockpiles from the building and slab demolition and indicates the contents of each rubble pile. The photograph in Appendix C, page C-5 shows a lump of suspected uranium oxide that was removed in soil excavation around the building's east bay area in 1996.
Production processes during the plant's history also generated various waste products. Information regarding how and where the disposal of these waste products occurred is lacking but it is known that some materials were disposed of on-site such as the used casting sand disposed of by National Lead in Patroons Lake between 1940 and 1975. There is also information that National Lead buried approximately 55 cubic yards of graphite, slag, refractory, uranium oxide, insoluble oil, metal scrap, and burnable trash in the Patroons Lake area in 1961. Radioactive materials have been found as deep as 21 feet within the perimeter of Patroons Lake. Modeling diagrams depicting uranium and thorium contamination are shown in Appendix C, pages C-6, C-7, and C-8. Other on-site soil contaminants include lead, copper, thallium, and cadmium. Metals in the soil are mainly beneath the southwest corner of the main building and in the Patroons Lake area with other lesser amounts around the north, south, and east sides of the building. The primary chemicals that exceed proposed soil cleanup goals include copper and lead. The modeling diagram depicting lead contamination in on-site soils is shown in Appendix C, page C-9. The lead model shows soil contamination impinging and possibly even slightly crossing the site boundary adjacent to the entrance to the plant at the 500 mg/kg level and in two areas along the southern site boundary at the same 500 mg/kg level. However, it is important to note that the modeling diagrams included in Appendix C are interpretations of available data and serve as an indicator of where contamination may exist. The models are not meant to portray the location of contamination in an absolute sense.
No significant soil contamination by volatile organic compounds (VOCs) has been identified but low concentrations of various VOCs do exist. The principle VOC in the soil is perchloroethylene (PCE) which has been found in areas of the former Patroons Lake and on the east side of the main building. Trichloroethylene (TCE) and vinyl chloride, which are known as breakdown products of PCE, have been found in lower concentrations just west of the main building. TCE has also been identified in soils just east of the building.
A number of groundwater investigations have been conducted at the site since 1984 to better understand the groundwater flow and the extent of any groundwater contamination. Groundwater flows south across the site and is strongly influenced by the backfilled former stream channel associated with the now-filled-in Patroons Lake. Groundwater is not used for public drinking water supplies in the vicinity of the CISS. Groundwater contamination by radioactive constituents, metals, and volatile organic compounds does exist on-site. Trace contaminations of chlorinated organic compounds and lead have been intermittently detected in off-site down gradient wells. Concentrations of these contaminants in off-site wells are at or below regulatory levels with the exception of dissolved lead which occasionally slightly exceeds drinking water goals. Other metals and radionuclides are present in the off-site down gradient wells at background levels comparable to those reported in the up gradient wells used for background comparison. In 1996, all analytical results for radioactive constituents (i.e., thorium-232, thorium-230, thorium 228, and uranium) in both the upper and lower groundwater zones were well below the limits set forth in DOE Order 5400.5. The 1996 results for metals showed that drinking water limits for arsenic, lead, and zinc were exceeded in some on-site monitoring wells. The presence of metals is generally confined to the area of known subsurface contamination just east of the main building and in wells near the backfilled channel associated with Patroons Lake. In 1996, on-site groundwater in three distinct areas contained tetrachloroethene and/or its degradation products (trichloroethene, 1,2,-dichloroethene, and vinyl chloride) at concentrations in excess of the federal drinking
12 water standards or the state water quality standards. No off-site groundwater contamination of tetrachloroethene or its degradation products has been observed.
In September 1995, DOE issued an "Engineering Evaluation and Cost Analysis (EE/CA) for the Colonie Site" to evaluate the cleanup options for the CISS and the three remaining adjacent vicinity properties. The selected option is to conduct "moderate excavation and cap and cover." All U-238 above 100 pCi/g and Th- 232 above 15 pCi/g will be excavated and transported for disposal at a licensed disposal facility. The remaining soils with U-238 concentrations between 35 pCi/g and 100 pCi/g will be consolidated in the former Patroons Lake burial area and covered with an 18 inch gravel and earthen cap. The portion of the site that is not covered by the cap will be covered with 6 inches of clean soil, and will be available for commercial, industrial, or recreational development.
The CISS has been evaluated by the U. S. Environmental Protection Agency (EPA) for inclusion on the National Priorities List (NPL) of Superfund sites under Section 120 of CERCLA. In a February 12, 1992, letter to DOE, EPA Region II assigned the site a "No Further Action Planned" status meaning that the site did not qualify for inclusion on the NPL.
4.3 PAST AND PRESENT ACTIVITIES FOR THE ADJACENT PROPERTY
The CISS is located at 1130 Central Avenue in the Town of Colonie, New York approximately 4 miles northwest of Albany, New York. The setting is in an urban environment with adjacent and nearby land being a mixture of residential and commercial properties. The CISS is bounded to the west-northwest by a wooded lot. Conrail tracks are immediately adjacent to the southern boundary of the site with Interstate 90 being just a few hundred yards south of the railroad. A small residential community is located south of the CISS in between the Conrail tracks and Interstate 90. Central Avenue fronts the northern boundary of the site with properties on this street being primarily commercial with some residences interspersed among the business establishments. Properties to the north of Central Avenue are primarily residential. A Niagara Mohawk electrical substation is located on the northwest corner of the site.
The majority of the residences in the immediate vicinity of the property appear to date back several decades indicating that the present usage of the area around the CISS has not changed much in recent decades. A U.S. Geological Service (USGS) topographic map of 1898 (Appendix A, page A-6) indicates that the site area was basically a rural, sparsely populated area at that time frame with only one dwelling being on, or near, the current site. The use of the land at that time was most likely agriculture with large areas of forest growth. A later 1927 USGS topographic map (Appendix A, page A-7) shows more numerous structures in the vicinity of the site including one which is likely the building constructed by the Embossing Company. Both topographic maps show the New York Central and Hudson River Railroad, which is presently owned by Conrail along the southern boundary of the site. The 1927 map also shows the man-made Patroons Lake to the west of the site. This lake was constructed in the early 1900's by construction of a dam just to the west of where the main building was later constructed by Magnus Metal and added on to by National Lead.
A March 12, 1936, map (Appendix A, page A-8) shows a "grill" very near, or at the same location of the present-day restaurant which is adjacent to the present site entrance. The 1936 map also depicts the railroad tracks along the south side of the site and the portion of Patroons Lake to the west.
The Niagara Mohawk electrical substation dates back to the 1940's as it is on property conveyed by National Lead Company to New York Power and Light Corporation on January 15, 1940.
13 Radiological surveys conducted in the early 1980's indicated that 56 vicinity properties were contaminated from past site operations by National Lead. In 1984, 1985, and 1988, DOE remediated 53 of the properties by removing and replacing surface-contaminated soil and some small amounts of roofing. This contaminated soil was temporarily stored inside the building on the CISS and was later shipped off-site for disposal.
Three remaining parcels (i.e., the Conrail tracks, the Town of Colonie property to the west, and the Niagara Mohawk substation) will be remediated (for radiological contamination only) as part of the future remedial activities at the CISS.
14 5. RESULTS OF VISUAL AND PHYSICAL INSPECTIONS
5.1 VISUAL AND PHYSICAL INSPECTIONS OF THE CISS
An on-site inspection of the CISS was conducted on June 30, 1997 and July 1, 1997, as part of the CERCLA 120(h) assessment. The site visit included discussions with DOE contractor personnel assigned to the site, a review of selected documents and photographs kept on site, and a walk over of the site.
The site is enclosed by a chain link fence and is accessible through a gate from Central Avenue. All permanent structures/buildings which were part of the National Lead operations have been demolished. The northern half of the building's concrete slab has also been removed, crushed into smaller pieces and is being stockpiled on the building's footprint along with several other piles of crushed building rubble and contaminated soil. On the southeast side of the building footprint, the three 10,000 gallon fuel oil tanks used in the original building remain on site. These tanks are reported to be empty although there may be some small amounts of sediment remaining in the tank bottoms. The footprint of the building is roped off and designated as a radiological contamination area.
The eastern portion of the facility (north and east of the original main building) is asphalt paved. A storage area is being maintained on the eastern side of the facility for mixed wastes in boxes and drums awaiting shipment off-site for disposal (see photograph in Appendix C, page C-10). It was reported that some of the drums failed tests for dioxin and will have to be treated before disposal. This storage area is roped off and is designated as a radiological contamination area. No evidence of any spills or leaks was observed emanating from the stored wastes (See Appendix B, Table 3 for an inventory of the wastes being maintained in this area). A storm drain was observed southwest of this storage area and east of the demolished building. This storm drain leads to the city sanitary sewer system. No evidence of any spills or discharges were observed in the vicinity of this drain.
DOE contractor personnel are located in a cluster of 5 trailers in the northwest corner of the plant adjacent to the Niagara Mohawk electrical substation. These trailers have been connected to the city sanitary sewer system.
Just to the west of the contractor's trailers is a small electrical substation which serves the CISS. This substation is on CISS property and is very near the Niagara Mohawk substation. It is possible that transformer oils used in the past in this substation contained PCBs. However, there is no evidence of any past discharges or releases of PCBs from this area.
Three additional temporary structures used to support remedial activities are located near the trailers. A tent-type chemical maintenance building is located on the north side of the original building. It's dimensions are approximately 70' by 40'. The structure still contains some equipment and materials which has been used in remedial activities at the site. Approximately 10 drums of radioactive wastes were observed in the building during the site inspection. To the south of the office trailers is the warehouse building. It is being used to store various pieces of equipment and materials used at the site. Items observed included personal protective equipment, safety signs, sampling jars and other laboratory items, drums, pipe, paint, etc. Two storage cabinets were also in the building; one containing small quantities of acids and the other containing flammable materials. The majority of the chemical inventory now on site and shown in Appendix B, Table 2 is being stored in this building and consists largely as constituents of paints, adhesives and lab supplies. To the south of the warehouse is a plastic covered decontamination pad and decontamination fluid tank. Decontamination
15 fluids are disposed of off-site. Adjacent to the pad is one of two 500 gallon diesel fuel tanks used in remedial activities on-site. The other fuel tank is to the southeast nearer the demolished main building.
Just to the west of the former main building a drain was observed which leads to the unnamed tributary to Patroons Creek. This tributary flows south underneath the site from the northwest corner of the property and enters Patroons Creek south of the Conrail tracks.
The west side of the CISS in the area of the filled in Patroons Lake and the area south of the lake is roped off as a radiological contamination area. The area is covered with vegetation. Near the southern boundary of property in the vicinity of the old storage sheds used by National Lead is a pile of building rubble from the demolition of those sheds. There is also a large pile of used, empty drums between the rubble pile and the original building (see photograph in Appendix C, page C-l 1). The building rubble stockpile and the empty drum area are roped off and designated as radiological contamination areas.
5.2 VISUAL AND PHYSICAL INSPECTION OF ADJACENT PROPERTY
The majority of adjacent and nearby properties are typical of those which one would encounter in any urban, mixed commercial and residential area. A drive through of the adjacent residential areas gave the impression of an older, well established, and neat neighborhood. With the possible exception of the Niagara Mohawk electrical substation adjacent to the northwest corner of the CISS, there did not appear to be any adjacent property which could contribute to the contamination of the CISS.
The electrical substation has been present since the early 1940's. It is likely that the transformer oils used on the substation at some point in the past contained PCB's. It is unknown if any spills of oil or any other discharges have occurred from the electrical substation. From the CISS property and looking through the fence at the substation, no evidence of spills was readily apparent and the grounds appeared to be clean and well- maintained.
The Conrail tracks parallel the southern site boundary. The CISS gradually slopes down toward the railroad and it is unlikely that any surface spill would significantly impact the CISS. Additionally, the groundwater flow is generally to the south from the CISS.
16 6. RESULTS OF SAMPLING CONDUCTED IN CONJUNCTION WITH THE PROPOSED EASEMENT
There was no additional sampling or characterization conducted solely for the preparation of this CERCLA 120(h) report.
17 7. REFERENCES
1. Bechtel National, Inc., Closure Plan for the Colonie Interim Storage Site, November 1986, DOE/OR/20722-74 Rev. 2, Oak Ridge, Tennessee.
2. Bechtel National, Inc., Engineering Evaluation of Disposal Alternatives for Radioactive Waste from Remedial Actions In and Around Colonie, New York, March 1986, DOE/OR/20722-78, Oak Ridge, Tennessee.
4. Bechtel National, Inc., Colonie Interim Storage Site -1996 Environmental Surveillance Information, May 29, 1997, Oak Ridge, Tennessee.
5. Bechtel National, Inc., Work Plan for Cyanide Destruction Colonie, NY, May 27, 1986.
6. Bechtel National, Inc., Work Plan for Nitric Acid Neutralization Colonie, New York, June 3, 1986.
7. DOE, June 1993, Engineering Evaluation/Cost Analysis (EE/CA) for the Colonie Interim Storage Site (CISS) Buildings, DOE/OR/21950-888, Oak Ridge, Tennessee
8. DOE and Science Applications International Corporation, September 1995, Engineering Evaluation and Cost Analysis (EE/CA) for the Colonie Site, DOE/OR/21950-1008, Oak Ridge, Tennessee.
9. DOE Memorandum dated February 14, 1997, Colonie Site- Action Memorandum for Removal Action.
10. Heritage Environmental Services, Inc., RCRA Closure Certification Report, Colonie Interim Storage Site, Colonie, New York, September 20, 1995
11. Marley J.L., Oak Ridge National Laboratory, Martin Marietta Energy Systems, Inc., Results of the Radiological Survey of a Municipal Property, Town of Colonie, Colonie, New York (AL064), March 1987, Oak Ridge, Tennessee
12. Science Applications International Corporation, January 1997, Responsiveness Summary: Engineering Evaluation/Cost Analysis (EE/CA) for the Colonie Site, DOE/OR/21950-1022, Oak Ridge, Tennessee.
18 APPENDIX A Appendix A
Table of Contents
BNI Drawing No. 139-DD602-C01 A-2
Mid-1980's Site Aerial Photograph A-3
1995 Site Aerial Photograph A-4
1996 Site Aerial Photograph A-5
Section 1 of 2, U. S. Geological Survey Topographic Map (1898 Edition, Reprinted in 1911) A-6
Section 1 of 2, U. S. Geological Survey Topographic Map (1927 Edition, Reprinted in 1930) A-7
Albany County (NY) Clerk's Subdivision Map 592 dated March 12, 1936 A-8 1* -40* A A A A A ISSUED FOR BIO BY CW'H CnC' POLE AND titUt DtiCftlPHOt 11081 BJR1NG SCALt J' . 40'
V EXCAVATION LIMIT AND U.S. DEPARTMENT OF ENERGY rup-s^^ \ DEMARCATION SHEET INC FORMERLY UTILIZED SITES REMEDIAL ACTION PROGRAM BECHTEL NATIONAL INC. ^^^M^ OAK RIDGE, TENNESSEE COLONIE INTERIM STORAGE SITE REMEDIATION FOR POWER LINE RELOCATION SITE, VICINITY PLAN, SECTION, AND DETAIL PfitPJSa) POLE BtCHTEL JOB NO. DOE CONTRACT NO. 14501 DE-Acr BNI Drawing No. 139-DD602-C01 d£& 13 A-2
? JM'£
1. ALL Wfi( SHALL BE OiRECIEO Br THE BECHtEL SHE iLIPERIITENDENT.
\ 2. JHIS SECTION IS 70 BE UStU ONLT OH NCIN-ASnou.1 AREAS IN THE \ ACCESS ROUTE. H —nr J. MATERIALS USED FOR DEMARCATION SHEETING M»V INCLUDE POLYETHYLENE, 5CRAP HW/U.ON. CORRUGATED FIBERGLASS SHEETING OR OTHER MATEfilALS (4IICH SHALL NOT HOST, 6I0DEGRADE NOR DISINTEGRATE OVER TIME, IS APPROVED BY THE SHE SUPERINTENDENT.
N) 900 4. silOfllNC. HEE7ING THE REQUIREMENTS Of 29 Cffl PART 1326, SUBPART ?. SHALL BE INSTILLED IN ALL EXCAVAHOtlS AT OR r-B^oO DEEPER THAN 4 FEET. -r s /
NlbOO U
F Nieoo
REFERENCE DRAWINGS
DESCRIPTION DRAWING NO.
NHOO
LEGEND
APPRO* DEPTH Of RAO CONTAMINATION 6 INCHES HI 300 APPROX DEPTH OF RAD CONTAMINATION 3 FEET
APPROX DEPTH OF RAD CONTAMINATION G FEET
APPROX DEPTH DF RAD CONTAMINATION 9 FEET D
APPROX DEPTH RAD CONTAMINATION > 9 FEET
PROPEHTT BOUNDARY
EXCAVATION LIMIT
ACCESS nam N1200 RAILROAD
FENCE
0€- EXISTING OVERHEAD POWER LIMES
— uc— - EXISTING UNDERGROUND POWER LINES
H EXISTING POWER POLE
PROPOSED POWER LINE t RIGHT-LiF-WAY Ni 100 HYPALON 60 NIL PROPOSED POWER POLE OR EOUAL —, -GRAVEL c GUY WIRE EXISTING
• ? Wi-VA TYPICAL SECTIOH THROUGH ACCESS BOM 40 120 SEE NOTE 2 i' •«• SECTION /T Ml 000 [••V A A A isstto tt» bib i pm •-•.,«• PILE ANO iiv* •iirmP'iiJh CM-• t~.-« EXaOfiA'ORI BJRINC Uiu T • U" NSOO U.S. DEPARTMENT OF ENERGY FORMERLY UTILIZED SITES REMEDIAL ACTION PROGRAM BECHTEL NATIONAL INC. OAK RIDtt, TENNESSEE IO; Dfl Iff >^ . X >0 *^&» ?\.._J^ 1995 Aerial Photograph Colonic Interim Storage Site A-4 1996 Aerial Photograph Colonie Interim Storage Site A-5 • • AX.BA1 - S.J,.;., '.../. Section 1 of 2 USGS Topographic Map (1898 Edition, Reprinted in 1911) A-6 . • y I S h—tti ••',!•/1 > —s - 8M V; •• * • ^1 V. 375'' •V- •^ I 1? & SS . ,X>- A K,,n,.-,- v,«| ;v t J ma* • £k \ /^ a Land Area That Comprises the Current CISS ' V' fcv £* 1/ - W v . « \AI,IIA.\V /Tfffn »'- ^ -T • r"—\ "• - 1 S- Section 1 of 2 ; USGS Topographic Map 1 : (1927 Edition, Reprinted in 1930) H*-J " . A-7 '-" • VXJ Redacted - Privacy Act Albany County (NY) Clerk's Subdivision Map 592 dated March 12,1936 A-8 APPENDIX B I Appendix B Table of Contents Table 1. Hazardous Chemicals Which Were Present at the Colonie Interim Storage Site (CISS) in Amounts Over 1000 Kilograms (kg) During Commercial Operations and/or After DOE Assumed Ownership Table 2. Radioactive Materials Used by National Lead at the Colonie Interim Storage Site Table 3. Colonie Interim Storage Site Waste Inventory (as of May 19, 1997) Table 4. Colonie Interim Storage Site Chemical Inventory as of July 1, 1997 Table 5. Hazardous Chemical Inventory at the Colonie Interim Storage Site Left by National Lead (and later transported by DOE for off-site disposal) Table 1. Hazardous Chemicals Which Were Present at the Colonie Interim Storage Site (CISS) in Amounts over 1000 Kilograms (kg) During Commercial Operations and/or After DOE Assumed Ownership Chemical CASRN 40 CFR 302.4 40 CFR 261.30 Quantity Stored Regulatory RCRAHazardous (in Kilograms (kg)) Synonyms Waste Number Acetic acid 64-19-7 U002 > 1000 kg Aluminum (metal) 7429-90-5 > 1000 kg Aluminum oxide 7429-90-5 > 1000 kg Antimony 7440-36-0 —_ > 1000 kg Asbestos 1332-21-4 > 1000 kg Barium 7440-39-3 — > 1000 kg Benzene . 71-43-2 U109 > 1000 kg Boric acid 10043-35-3 > 1000 kg Cadmium 7440-43-9 > 1000 kg Carbon tetrachloride 56-23-5 methane, tetrachloro- U211 > 1000 kg Chromium 7440-47-3 > 1000 kg Copper 7440-50-8 > 1000 kg Ethyl alcohol 64-17-5 > 1000 kg Ferric chloride 7705-08-0 _— > 1000 kg Ferrous sulfate 7720-78-7 > 1000 kg Fuel oil (diesel) 68334-30-5 > 1000 kg HYHrnr.hlnrir. arid 7647-01-0 Hvrlrnpen chloride > lonnicp Table 1. Hazardous Chemicals Which Were Present at the Colonie Interim Storage Site (CISS) in Amounts over 1000 Kilograms (kg) During Commercial Operations and/or After DOE Assumed Ownership Chemical CASRN 40 CFR 302.4 40 CFR 261.30 Quantity Stored Regulatory RCRA Hazardous (in Kilograms (kg)) Synonyms Waste Number Iridite NA -— > 1000 kg Lead 7439-92-1 > 1000 kg Nickel 7440-02-0 ... > 1000 kg Nickel sulfamate 13770-89-3 — > 1000 kg Nitric acid 7697-37-2 -— > 1000 kg Potassium hydroxide 1310-58-3 _. > 1000 kg Sodium cyanide 143-33-9 Sodium cyanide NA > 1000 kg (1,130 gallons (CN) left on site by NL Industries) Sodium hydroxide 1310-73-2 > 1000 kg Sulfuric acid 7664-93-9 —- > 1000 kg Tetrachloroethylene 127-18-4 ethene, tetrachloro-, — > 1000 kg perchloroethylene, tetrachloroethene Zinc 7440-66-6 ... > 1000 kg 2 of 2 Table 2. Radioactive Materials Used by National Lead at the Colonie Interim Storage Site Chemical CASRN 40 CFR 302.4 Regulatory Quantity Stored Synonyms Uranium 7440-61-1 — >1000 kg Uranium tetrafluoride 10049-14-6 — >1000 kg Uranium oxide 1334-59-8 — >1000 kg Thorium 7440-29-1 — <1000kg 1 of 1 Table 3 - Colonie Interim Storage Site Waste (as of May 19,1997) Drum No. Waste Type Contents Status Matrix Weight (lbs.)/ Location Volume 5S-GAL Drums 4093 BROKEN GLASS SOLID UNKNOWN SOLID UNKNOWN CHEM. MGMT. BLDG. 4094 BROKEN GLASS SOLID UNKNOWN SOLID UNKNOWN CHEM. MGMT. BLDG. 4100 HOT SPOT SOIL SOIL UNKNOWN SOLID 925 EAST PARKING LOT 4085 HOT SPOT SOIL SOIL UNKNOWN SOLID 950 EAST PARKING LOT 4099 HOT SPOT SOIL SOIL UNKNOWN SOLID 925 EAST PARKING LOT 4087 HOT SPOT SOIL SOIL UNKNOWN SOLID 920 EAST PARKING LOT 4110 HOT SPOT SOIL SOIL UNKNOWN SOLID 945 EAST PARKING LOT 4123 HOT SPOT SOIL SOIL UNKNOWN SOLID 765 EAST PARKING LOT 4109 HOT SPOT SOIL SOIL UNKNOWN SOLID 865 EAST PARKING LOT 4085 HOT SPOT SOIL SOIL UNKNOWN SOLID 935 EAST PARKING LOT 4089 HOT SPOT SOIL SOIL UNKNOWN SOLID 875 EAST PARKING LOT 4108 HOT SPOT SOIL SOIL UNKNOWN SOLID 970 EAST PARKING LOT 4106 HOT SPOT SOIL SOIL UNKNOWN SOLID 960 EAST PARKING LOT EAST PARKING LOT 4105 HOT SPOT SOIL SOIL UNKNOWN SOLID 900 EAST PARKING LOT 4107 HOT SPOT SOIL SOIL UNKNOWN SOLID 860 EAST PARKING LOT 4098 HOT SPOT SOIL SOIL UNKNOWN SOLID 950 EAST PARKING LOT 4104 HOT SPOT SOIL SOIL UNKNOWN SOLID 935 EAST PARKING LOT 4102 HOT SPOT SOIL SOIL UNKNOWN SOLID 940 EAST PARKING LOT 4101 HOT SPOT SOIL SOIL UNKNOWN SOLID 920 CHEM. MGMT. BLDG. 4096 LIQUID WASTE OIL FROM EQUIPMENT NON-RCRA LIQUID UNKNOWN EAST PARKING LOT 4062 MISC. SOLIDIFICATION SOLIDIFIED MATERIAL NON-RCRA SOLID UNKNOWN CHEM. MGMT. BLDG. 4126 OIL FILTERS SOLID MATERIAL NON-RCRA SOLID UNKNOWN EAST PARKING LOT 4072 SOLIDIFIED MATERIAL NON-RCRA SALT BATH BRICK SOLID 690 EAST PARKING LOT 4071 SOLIDIFIED MATERIAL NON-RCRA SOLID SALT BATH BRICK 692 EAST PARKING LOT SOLIDIFIED MATERIAL NON-RCRA SOLID 4078 SALT BATH BRICK 880 EAST PARKING LOT 4063 SOLIDFIED Mg CHIPS SOLIDIFIED MATERIAL NON-RCRA SOLID UNKNOWN EAST PARKING LOT 4070 SOLIDIFED CHELATING AGENTS SOLID MATERIAL NON-RCRA SOLID 855 EAST PARKING LOT 4075 U-RAFF SOLIDIFIED OIL RCRA - F002 SOLID 870 EAST PARKING LOT 4073 U-RAFF SOLIDIFIED OIL RCRA-F002 SOLID 610 EAST PARKING LOT 4079 U-RAFF SOLIDIFIED OIL RCRA-F002 SOLID 810 EAST PARKING LOT 4064 U-RAFF SOLIDIFIED OIL RCRA-F002 SOLID 775 EAST PARKING LOT 4066 U-RAFF SOLIDIFIED OIL RCRA-F0Q2. SOLID 765 EAST PARKING LOT 4081 U-RAFF SOLIDIFIED OIL RCRA-F002 SOLID' 725 EAST PARKING LOT 4091 U-RAFF SOLIDIFIED OIL RCRA-F002 SOLID 700 EAST PARKING LOT 4090 U-RAFF SOLIDIFIED OIL RCRA- F002 SOLIt> 705 EAST PARKING LOT 4065 U-RAFF SOLIDIFIED OIL RCRA - F002 SOLID 825 1 of 3 5/19/97 Table 3 - Colonie Interim Storage Site Waste Inventory (as of May 19,1997) 4067 U-RAFF SOLIDIFIED OIL RCRA-F002 SOLID 745 EAST PARKING LOT 4077 U-RAFF SOLIDIFIED MATERIAL RCRA-F002 SOLID 745 EAST PARKING LOT 4076 U-RAFF SOLIDIFIED MATERIAL RCRA-F002 SOLID 775 EAST PARKING LOT 4124 WATER DRUM SEDIMENT SOLIDIFIED MATERIAL UNKNOWN SOLID 810 EAST PARKING LOT 3621 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F00B SOLID 835 EAST PARKING LOT 3622 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 870 EAST PARKING LOT 3623 WS*6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 300 EAST PARKING LOT 3953 WS06013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 850 EAST PARKING LOT 3954 WSH6013-01 SOLIDIFIED MATERIAL RCRA -F002.F008 SOLID 745 EAST PARKING LOT 3955 WS#6013-01 SOLIDIFIED MATERIAL RCRA -F002.F008 SOLID 860 EAST PARKING LOT 3956 WS*B013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 830 EAST PARKING LOT 3957 WSS6013-01 SOLIDIFIED MATERIAL RCRA-F002. F008 SOLID 885 EAST PARKING LOT 3958 WSA6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 775 EAST PARKING LOT 3959 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLIC 865 EAST PARKING LOT 3960 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 870 EAST PARKING LOT 3961 WSA6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 880 EAST PARKING LOT 3962 WSA6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 880 EAST PARKING LOT 3963 WS06013-O1 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 900 EAST PARKING LOT 3964 WS*6013-01 SOLIDIFIED MATERIAL RCRA-F002.FO08 SOLID 880 EAST PARKING LOT 3965 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 860 EAST PARKING LOT 3968 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 875 EAST PARKING LOT 3967 WS#6013-01 SOLIDIFIED MATERIAL RCRA • F002, F008 SOLID 850 EAST PARKING LOT 3968 WS*6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 870 EAST PARKING LOT 3969 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 880 EAST PARKING LOT 4074 WS*6013-01 SOLIDIFIED MATERIAL RCRA-F002, F008 SOLID 845 EAST PARKING LOT 3970 WS#6013-O1 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 860 EAST PARKING LOT 3971 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 790 EAST PARKING LOT 3972 WS»6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 860 EAST PARKING LOT 3973 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002, F008 SOLID 845 EAST PARKING LOT 3974 WS#6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 845 EAST PARKING LOT 3975 WS96013-01 SOLIDIFIED MATERIAL RCRA-F002. F008 SOLID 865 EAST PARKING LOT 3976 WS»6013-01 SOLIDIFIED MATERIAL RCRA-F002.F008 SOLID 805 EAST PARKING LOT LSA BOX B0777 FIBERGLASS SOLID MATERIAL NON-RCRA SOLID UNKNOWN EAST PARKING LOT B0778 FIBERGLASS SOLID MATERIAL NON-RCRA SOLID UNKNOWN EAST PARKING LOT B0B08 FIBERGLASS SOLID MATERIAL NON-RCRA SOLID UNKNOWN EAST PARKING LOT B0414 HEPA FILTERS SOLID MATERIAL NON-RCRA SOLID 9910 EAST PARKING LOT B0371 PPE SOLID MATERIAL NON-RCRA SOLID 1315 EAST PARKING LOT 5/19/97 . 2 of 3 Table 3 - Colonie Interim Storage Site Waste Inventory (as of May 19,1997) B0716 PPE SOLID MATERIAL NON-RCRA SOLID 1130 EAST PARKING LOT B0788 PPE SOLID MATERIAL NON-RCRA SOLID 935 EAST PARKING LOT B0507 PPE SOLID MATERIAL NON-RCRA SOLID UNKNOWN EAST PARKING LOT B0517 PPE SOLID MATERIAL NON-RCRA SOLID 1105 EAST PARKING LOT UNK PPE SOLID MATERIAL NON-RCRA SOLID 1050 EAST PARKING LOT B0642 PPE SOLID MATERIAL NON-RCRA SOLID 1080 EAST PARKING LOT UNK PPE SOLID MATERIAL NON-RCRA SOLID 1145 EAST PARKING LOT B0165 PPE SOLID MATERIAL NON-RCRA SOLID 1150 . EAST PARKING LOT UNK PPE SOLID MATERIAL NON-RCRA SOLID 1140 EAST PARKING LOT B0644 PPE SOLID MATERIAL NON-RCRA SOLID UNKNOWN NEAR OFFICE TRAILERS B0573 PRE-FILTERS SOLID MATERIAL NON-RCRA SOLID 2306 EAST PARKING LOT B0782 PRE-FILTERS SOLID MATERIAL NON-RCRA SOLID UNKNOWN NEAR OFFICE TRAILERS B0107 RESPIRATOR CARTRIDGES SOLID MATERIAL NON-RCRA SOLID 2206 EAST PARKING LOT B0130 RESPIRATOR CARTRIDGES SOLID MATERIAL NON-RCRA SOLID 1918 EAST PARKING LOT B0312 RESPIRATOR CARTRIDGES SOLID MATERIAL NON-RCRA SOLID 1998 EAST PARKING LOT B0368 RESPIRATOR CARTRIDGES SOLID MATERIAL NON-RCRA SOLID 2120 EAST PARKING LOT B0409 RESPIRATOR CARTRIDGES SOLID MATERIAL NON-RCRA SOLID 1870 EAST PARKING LOT B0767 RESPIRATOR CARTRIDGES SOLID MATERIAL NON-RCRA SOLID 2560 EAST PARKING LOT B0839 RESPIRATOR FILTERS SOLID MATERIAL NON-RCRA SOLID UNKNOWN NEAR OFFICE TRAILERS B0B42 RESPIRATOR FILTERS SOLID MATERIAL UNKNOWN SOLID 1165 EAST PARKING LOT B0772 SOIL SAMPLE RETURNS SOIL NON-RCRA SOLID UNKNOWN EAST PARKING LOT UNK UNKNOWN UNKNOWN UNKNOWN UNK UNKNOWN NEAR OFFICE TRAILERS B0840 UNKNOWN - ASBESTOS STICKER UNKNOWN UNKNOWN UNK UNKNOWN EAST PARKING LOT PILES 1 BUILDING RUBBLE CONCRETE NON-RCRA SOLID 1500 CY NW CORNER OF SITE 2 WOOD CHIPS SHREDDED WOOD RCRA-EXEMPT SOLID 1500 CY NW ALONG WEST LOADING DOCK 3 BUILDING RUBBLE CRUSHED CONCRETE NON-RCRA SOLID 400 CY WEST END OF EXISTING SLAB 4 BUILDING RUBBLE CRUSHED CONCRETE NON-RCRA SOLID 4000 CY CENTER OF EXISTING SLAB 5 SOIUDEBRIS REMOVED FROM ZONE 19B SOIUDEBRIS NON-RCRA SOLID 80 CY SOUTH END OF FORMER BLDG. SLAB 6 SOIUDEBRIS REMOVED FROM ZONE 19B SOIUDEBRIS RCRA - D008 SOLID 600 CY SE END OF FORMER BLDG. SLAB 7 RR BALLAST MATERIAL SOIL NON-RCRA SOLID 150CY EAST END OF FORMER BLDG. SLAB 8 SOIL > 100,000 CPM SOIL NON-RCRA SOLID 40 CY EAST END OF FORMER BLDG. SLAB 9 SOIL 30,000 < 100,000 CPM SOIL NON-RCRA SOLID 80 CY EAST END OF FORMER BLDG. SLAB 10 BUILDING RUBBLE CRUSHED BRICK NON-RCRA SOLID 3600 CY SOUTH END OF EXISTING SLAB 5/19/97 3 of 3 Table 4. Colonie Interim Storage Site Chemical Inventory as of July 1,1997 40 CFR 261.30 40 CFR 302.4 RCRA Hazardous Chemical CASRN Regulatory Synonyms Waste Number Quantity Stored Acetic acid 64-19-7 U002 < 1kg Acetone (in cement) 67-64-1 2-propanone < 1kg Adhesive (various brands) Methyl alcohol 67-56-1 < 10 kg Toluene 108-88-3 benzene, methyl- U220 < 10 kg Zinc oxide 1314-13-2 < 10 kg 1-Hexane 110-54-3 < 1kg Batteries Lead 7439-92-1 27 kg Antimony 7440-36-0 — — < 5 kg Arsenic 7440-38-2 <5kg Calcium chloride 10043-52-4 < 1kg Chlorodifluoromethane 75-45-6 < 1kg Chlorine (calibration gas) 7782-50-5 <10kg Cyclohexanone 108-94-1 Benzene, hexahydro- U056 < 1kg Diesel fuel 68334-30-5 350 kg Ethyl oxide (in starting fluid) 60-29-7 < 1kg Ethylene glycol 107-21-1 <5kg Ferrous sulfate 7720-78-7 1590 kg Formic acid 64-18-6 — U123 < Ike 1 of 3 Table 4. Colonie Interim Storage Site Chemical Inventory as of July 1,1997 40 CFR 261.30 40 CFR 302.4 RCRA Hazardous Chemical CASRN Regulatory Synonyms Waste Number Quantity Stored Gasoline 67-56-1 < 15 kg Hydrochloric acid 7647-01-0 Hydrogen chloride < 1kg Hydrogen sulfide 7783-06-4 Hydrogen sulfide H2S U135 < 5 kg Isopropanol (rubber cement) 67-63-0 500 kg Kerosene 8008-20-6 -— < 15 kg Liquid paper correction fluid Trichloroethylene 79-01-6 Ethene, trichloro, U228 < 1kg 1,1,1- Trichloroethane 71-55-6 Ethane, 1,1,1- U226 < 1kg trichloro, methyl alcohol Methanol (in buffer solutions) 67-56-1 Methyl alcohol U154 < 1kg Methyl ethyl ketone (in cement) 78-93-3 2-butanone U159 < 1kg Methyl isobutyl ketone (in cleaner) 108-10-1 4-methyl-2-pentanone U161 <5kg Motor oil (lubricating oil) —- < 5 kg Nitric acid 7697-37-2 200 kg Nitrogen dioxide 10102-44-0 Nitrogen oxide N02 P078 <5kg Phosphoric acid (in cleaner) 7664-38-2 < 1kg Potassium hydroxide 1310-58-3 < 1kg Potassium permanganate 7722-64-7 — < 1kg 2 of 3 Table 4. Colonie Interim Storage Site Chemical Inventory as of July 1,1997 40 CFR 261.30 40 CFR 302.4 RCRA Hazardous Chemical CASRN Regulatory Synonyms Waste Number Quantity Stored Propane 74-98-6 -_- -— < 200 kg Propoxur (in wasp killer) 114-26-1 — < 1kg Silver (in solder) 7440-22-4 < 1kg Sodium carbonate 497-19-8 12 kg Sodium silicate (solution) -— <5kg Sodium hydroxide 1310-73-2 < 5 kg Sodium phosphate (in cyanide test 10101-89-0 — < 1kg kit) Styrene monomer 100-42-5 < 1kg Sulfuric acid 7664-93-9 < 60 kg Threadlock Saccharin 81-07-2 — < 1kg Cumene hydroperoxide 80-15-9 — < 1kg Methyl alcohol 67-56-1 < 1kg Zinc (in wheel bearing grease) 7440-66-6 — — < 1kg 3 of 3 Table 5. Hazardous Chemical Inventory at CISS Left by National Lead (and later transported by DOE for off-site disposal) ROOM CODES ER Electroplating OR Oil room MP Metals plant PS Paint storage CR- Chemical room SB Spray booth Bl Bay 1 B2 Bay 2 B4 Bay 4 OB Outside bin OA Office area TR Tool room SBA Salt bath area BR2 Boiler room 2 LD Loading dock FS Fuel storage 058471 I MAIN LABORATORY I AREA A Liquid Ammonia Plus (Ammonium Hydroxide) (2) 110 fl. oz. bottle - I 220 fl. oz. (1) 24° (1) 26° I ASP 2 (Allied-Kelite (1) 1 pint bottle (est) #1 Acetone (which appears to have uranium chips in bottle) • (1) est - 1 pt. • #2 Acetone (Same as above) (1) 10% Ammonium Holybdate (liquid with settled out white powder 1 on bottom (1) est - 1/4 pt. 50% Ammonium Citrate - Just liquid (1) - est less than 1/4 Pt. I Aluminum 1,000 ppm (1) 1 pt. I 1% Barium Dipilenyl Amine Sulfonate in 60% HAC(l) less than 1/4 pt. -' . '••-• I Barium hydroxide - (1) est - 1/4 pt. Bg (DiPheuce)? Sulfate (1) est - less than 1/4 pt. I Buffer pH 7.00 € 25°C (1) est - 1/2 pt. Buffer solution pH 4.00 (2) 1.1 pt container (plastic) - 2.2 pt. • " pH 7.00 (2) 1.1 pt container - 2.2 pt. pH 10.00 (2) 1.1 pt container - 2.2 pt. 8 pH 8.00 (1) 1 qt. plastic bottle - est - 3/4 pt. Std. Cd. Stock Solution 0.0001 gm/ml DiL Ho(l) 1 pt. plastic bottle - est 1 pt. Collodion U.S.P. (1) 1 pt. bottle - est - 1/2 pt. copper Cyanide Strike (date of 6-5-72) (1) 1 gal plastic bottle - est 1 gal. 2.6% Dimethyl Glyoxime (1) 1 plastic bottle - est -less than 1/4 pt. A-l 058471 •Chips Doloraro X-9016-50 (2) est 5 lb. can - est - 9 lbs. Did not •Solid open. " Doloram X-11462 (2) est 5 lb. can - est - 9 lbs. Did not open. Liquid 5% Elvanol Water Polyvinyl Alcohol (1) 1 pt. plastic bottle dated 10/73 - est - 3/4 pt. Hg(N03)2 - 5.43 mg/ml - 25 g/1 (1) 2 pt. plastic bottle - est - 2 pt. HNO3 Plating Tank No. 2 (1) 1/2 pt. plastic bottle - 1/4 pt. HSO3 ^2 1«5 M (1) est 1/2 pt. bottle - est - less than 1/4 pt. 10% HA^HCL (1) est 1/2 pt. bottle - less than 1/4 pt. (2 or 3 drops) H2SO4 1 M (1) est 1 pt. bottle - est - 1 pt. 5% 8-Hydroxy quinoline 1N2N HAC (1) 1/4 pt. plastic bottle - est - l/4_j>t. HNO3 Plating Tank (3) 1/2 pt. plastic bottles - est - 1-1/2 pt. Fe 100 ppm - (1) 100 nil containers - est - 50 ml Fe 200 ppm - (1) 100 ml containers - est - 50 ml Fe 1 ppm - (1) 200 ml containers - est - 100 ml Fe 3 ppm - (1) 200 ml containers - est - 150 ml Fe 5 ppm - (1) 200ml container..- 100 ml Fe STK (1) 1. pt container - est - 1 pt. FeSC-4 1M dated 07/02/81 (1) 1 pt. bottle - est - 1/4 pt. Chips Ferrous chloride (1) 1/4 lb. Liquid Genesolv DTA (196-8090 (1) 10 lb. bottle - est - 8.0 lb Genesolv Dl AZEOTROPE Code 8802 (1) 10 lb. bottle 7.5 lb. est. KMn04 (1) est 1/2 pint bottle - est - 1/4 pt. K4Fl(CN)6 (1) est. 4 02. plastic .bottle - est - 4 02. A-2 05647 I Liquid 0.002 ti KI (1) est. 4 oz. plastic bottle - est - 3.5 oz. 10% KCN est. 3/4 pt. bottle - est - 1/4 pt. I 1% KMn04 1 pt. bottle - 3/8 pt. >> I KCl Solution (Beckman 3502 saturated) (1) 150 ml plastic bottle - est - 60 ml 1 Luster - FOS (2100) (1) est - 1 1/2 pt. plastic bottle - est « - less, than 1/4 pt. £ Luster - FOS Sealer -900 (1) «- 1 pt. bottle - 1 pt. Luster - FOS (2100) (1) est. 10 lb. plastic bottle - est - 8.5 lbs.. I Powder Mannitol D-Mannitol (1) 500 g bottle - est - 20g I Liquid Stdstu,. Magnesiu naynes> j.um 1 x mg/m jug/wol. (1v •*•) Ies «»t w *• - pt fc>t plasti pxaaticw bottl uui.tj.te s - —es eatt . - - *m 2/5 pt. J Manganese (standard solution 1,000 ppm) (1) 1.1 pt. plastic bottle - 1.1 pt. I Methyl cellosove (H20) (1) est - 1 1/2 pt. est - 1/2 pt. 4 molar KCl saturated with Ag (Beckman) (1) est - 1 pt. plastic bottle - est - 3/4 pt. I Mogul - Products'Co. with label reading Acid - est - 1 pt. • plastic bottle - est 1/2 pt. * Chromate - est - 1/2 pt plastic bottle - est - 1/2 pt. • • • pH Indicator - est - 1/2 pt plastic bottle - est - 1/2 pt. I • • ' • Silver - est - 1/2 pt plastic bottle - est:- 1/2 pt. • • » • Soap - est - 1/2 pt plastic bottle - est - 1/4 pt. Molybdenum (reference solution 1,000 ppm (1) 1.1 pt. plastic bottle - est - 3/4 pt. Mo (1,000) 7/19/78 (1) est - 1 pt. bottle - est - 1 pt. Mo (300) (1) 200 ml bottle - est - 25 ml Mo (Az) (1) 200 ml bottle - est - 25 ml Mo (10) (1) 100 ml bottle - est - 25 ml Mo (100) (1) 200 ml bottle - est - less than 10 ml Mo (30) (1) 100 ml bottle - 25 ml A-3 058471 Liquid Neocuproine in ethyl ale. For Cu (1) est. 1/2 pt. plastic bottle - est - less than 1/8 pt. " ' (NH4) MO 2.4 Sol (1) est* 1 pt.- bottle - est - 1/2 pt. " • NaF 313 g/1 (1) 1 pt. plastic bottle and cardboard container - est - 3/4 pt. " " NOC2O1 in H2SO7 (glass cleaner (1) est. 1 pt. bottle - est •- 1 pt. Flakes NaOH (1) 10 lb est - bottle - est - 8 lbs. Liquid (NO2CO2O4 in Kiss)? (1) est 1 pt. bottle - est - less than 1/8 pt. • • Nickel - alkaline (electroless) P4 86 Metal Finish 1967 (1) est pt. plastic bottle est - 1 pt. • " 4% NaF (1) est 4 oz. plastic bottle - est - less than 1 oz. • 10% NaOH (1) est 4 oz. plastic bottle -* est - less than 2 oz. " 2% NaOH (1) est 4 oz. plastic bottle - est - less than 1-1/2 oz. " " 10% NH4OH (1) est 4 oz. plastic bottle - est - less than 2 oz. " ' 1% Nacu (1) est 4 oz. plastic bottle - est - less than 1 oz. • "1% NaN02 (1) est 4 oz. plastic bottle - est - less than 2 oz. • • OPCARB (1) est 2 oz. bottle - est - 1 oz. Crystal- lized Oakite (1) est pt. plastic bottle - est - 1/8 pt. Liquid 2R 1.0 ug/ml (1) est 1 pt bottle - est - 1 pt. • ' Std Mo 0.1 mg/ml tl) est - 2 pt. bottle - est - 11/2 pt. • • Th 20 gm/lL (1) est 1 pt. bottle - est - 3/4 pt. • " Potassium Sodium Tartrate (1) est - 4 oz. plastic bottle - est - 3 oz. • c Phenolphthalein 0.02% (pH rage 8.2-10.0) (1) est 4 oz. bottle - est - 2 oz " " Phosphate Carbonate for cu (1) est - 1 pt bottle - est - 1 pt. A-4 058471 I Liquid Nickel - Lume (H-VW-M) MAR 1972 (1) 2 L plastic bottle - I 4 lbs. Nickel sulfamate as rec'd 8-29-73 (1) est 1 qt. plastic bottle - est - 1/2 qt. I Silicon (reference solution 1,000 ppm (1) 1.1 pt. plastic bottle - est - 3/4 pt. I Nickel Sulfamate Plating Soln. (1) est. 10 lb. plastic bottle - 4 lbs. I Pellets Sodium Hydroxide - pellets (electrolytic) liquid and pellets » in bottle (1) 500 gm bottle .- est - 100 gm • Liquid Sodium Trate for Cu(l) est 4 oz. plastic bottle - est - 2 oz. SOD Meta .Silicate (1) est 1/2 pt. - est 1/4 pt. 10% Tartaric Acid (1) est 4 oz plastic bottle - est - less than 1 oz. I Ti (150) (!)• est 1 qt. bottle - est - 1 qt. Ti (200) (1) 200 ML bottle - est - 75 ML I Ti (150) (1) est. 1 pt plastic bottle - est - 1 pt. Titanium (reference solution 1,000 ppm) (1) 1 pt. plastic I bottle - est - 1/3 pt. Thorium Stock Sol. (1,000 g Th/L) 2.36 gm Thorium Nitrate (1) est 2 pt. bottle - est - 1 1/2 pt. 1 Cry- stals Tri Sod Phosphate (1) est 1/2 pt bottle - est - 1/4 pt. „ I Liquid VOSO (1) est 1/2 pt bottle _- .est - less than -1/8 pt. r I Wetting.agenwetting, agentt useuseds iinn ultrsoniuj.crsonic.canc tankK (1 {.!)) es estc 2 -i ozoz.. plastipiascicc « bottle - est - 3/4 oz. | Working solution (Si Mn Pe Al) (1) 500 ML bottle - est - 250 ML -.:*.'<•-•.•.• ;" Working solution (Fe Si Mn) (1) 500 ML bottle - est - 250 ML I 2 Trays of Unknown Chemicals, Mostly Liquid, Kith (1) Bottle of Large Chunks I Std U (.0168 gm U/ML (1) est 1 pt. bottle - est - 1/8 pt. I 500 ng/1 (U) (1) est 1 qt. bottle - est - 1/2 qt. Std U 1 mg/ml DjOa in dil. HNO3 (1) est 1 1/2 qt. bottle - est - 1 1/2 qt. I A-5 I 058^71 0.02 gm/ml (U) (1) est 2 qt. bottle - est - 2 gt. 0.2 mg U/ml (1) est 1 pt. plastic bottle - est - 1/2 pt. 6 Si 6 Fe 1.5 Al 1.5 Mn unalloyed (l)-est 1 pt. plastic bottle - est - 1/8 pt. ; *** 4 Fe 4 Si 1. Al 1 Mn unalloyed (1) est 1 pt. plastic bottle - est - 1/8 pt. 2 Si 2 Fe .5 Al ..5 Mn unalloyed (1) est 1 pt. plastic bottle - est - 1/8 pt. Std u .20 g/L (1) est 1 pt bottle - est - 1 pt. Std U 0.01 Mg/1 (1) est 1 pt bottle - est - 1 pt. Std U .05 g/L (1) est 1 pt bottle - est ^ 1/2 pt. Std U SO4 0.01 mg/ml est 1 pt bottle - est - 1 pt. Std U 3.84 mg/ml est 1 pt bottle - est - 3/4 pt. Std U .10 g/L est 1 pt bottle - est - 1 pt. Std .U .50 g/L est 1 pt bottle - est - 1/2 pt. Std U 50 mg/ml (1) est 8 oz. plastic bottle - est- 1 1/2 oz. Depleted uranium std (1) est 8 oz. plastic bottle - est - less than 1 oz. Std U 20 mg/ml (1) est 8 oz. plastic bottle - est - less than 1 oz. 0 50 ug/ml (1) est 8 oz. plastic bottle - est - 4 oz. U 3.0 ug/ml (1) est 8 oz. plastic bottle - est - 4 oz. U 1.0 ug/ml (1) est 8 oz. plastic bottle - est - 4 oz. 0 4.0 ug/ml (1) est 8 oz. plastic bottle - est - 5 oz. O3O8 1 g/10 ml (1) est 8 oz. plastic bottle - est - 3 02. O3O8 3 g/10 ml (1) est 8 oz. plastic bottle - est - 3 oz. 0 0.5 ugm/ml (1) est 8 oz. plastic bottle - est -4 oz, 0 7 ugm/ml (1) est 8 oz. plastic bottle - est - 5 oz. Depleted uranium std (1) est. 8 oz. plastic bottle - est -• 3.5 oz. A-6 058471 Liquid Normal 0 10 ugm/ml (1) est. 8 02. plastic bottle - est - 4 oz. ' • Normal .0 25 ugm/ml (1) est. 8 oz. plastic bottle - est - 5 02. AREA B - Bottom Shelf Liquid AgN03.(l) 500 ml bottle - est - 300 ml • ' 10% ammonium carbonate (1) est - 2 pt. bottle - est -4 pt. • • Buffer pH 6.86 (1) est - 1 pt. plastic bottle - est - 1/2 pt. " " Buffer pH 9 (1) est - 1 pt. plastic bottle - est -1/2 pt. • " 10% Bacl2 (1) est 1/2 pt. bottle - est - 1/4 pt. " " (CAS) eerie Ammonium Sulfate (1) est - 2 pt. bottle - est - 1 1/2 pt. .. . , „ . • " Std Cu. (Rocheltex) (1) est 2 pt. bottle - est - 1 1/2 pt. " " EDTA 0.1M (1) est 1 1/2 pt. plastic bottle - est - 1/4 pt. • " EDTA 0.01M (1) est 1 1/2 pt. plastic bottle - est - 1 1/2 pt. • " Ferrous Ammonium sulfate 0.40 N (1) 2 pt. bottle - est. - 1 pt. " " 1-Hexanol (CH3 (CI^JsOH (1) 3 kg bottle « est - 2 kg " " HNO3 1.4N Max OR 10% Max (1) 2 L bottle - 2 L " " 2% NaOH (1) est 1 1/2 pt. plastic bottle - est - 3/4 pt. " "2 N H2SO4 2.027 N 56'ml/1 (1) est 1 1/2 pt plastic boTtle- est -.172 pt. z.-.s • • 10% NaScN for Fe in Ni plating (1) est 1 pt. bottle - est - 1/2 pt. • • 0.15 M Na2C204 for HNO3 N (1) est 2 pt. bottle - est - l/2""pt. ~ • " Sat. K4Fe (CN)g . 3H2Q for boric acid (1) est X 1/2 pt bottle - est - 3/4 pt. • • 2% Sodium Chromate (1) est 1 pt. bottle - est - less than 1/8 pt. • " Sodium Oxalate (1)1 lb. plastic bottle - est - less than 1/4 lb. A-7 058471 AREA B - Top Shelf Liquid AgN03 0.0192 N for CN plating waste (1) est. 1 1/2 pt. plastic bottle - est - 3/4 pt. .101 AgN03 (1) est 4 oz. bottle - est - less than 1/2 oz. Alizarin Red S (1) est 8 oz. plastic bottle - est - 1 1/2 oz. Bromocresol purple 59% (ethesol)? (1) est - 4 oz. plastic bottle 1- est - 1 oz. Bromocresol purple 0.04% pH 5-2-6.8 (1) 500 cc plastic bottle - est - 100 cc. Bromocresol purple plus bromocresol blue on label (1) est 2 oz. bottle - est - 1/4 oz. Bromthymol blue Bromocresol purple (1) est. pt. bottle - est - 1/2 pt. Bry-CAD #53 (1) est 1/2 pt. bottle - est - 3/5 pt. Std cu 1.2482 gm/1 -(1) est 1 1/2 pt. bottle - 1 1/2 pt. Erichrome BT 0.5% w/v (1) est 1 pt bottle - est - 1/4 pt. 50% HCl (1) est 2 plastic bottle - est - 2 oz. K2Cr2°l 5% d) est 4 oz. plastic bottle - est - 2 oz.' KMn04 1.038 x 10"2N (1) est 1 1/2 pt. plastic bottle - est - 1/4 pt. PAN 0.1% (1) est 4 oz. plastic bottle - est - 1 1/4 oz. Methyl Red .2% w/v (1) est 2 oz. bottle - est - less than 1/4 oz. NACN 3% -(1) est 4 oz. plastic bottle - est - 11/2 oz. NA2CO3 20% (1) est. 8 02. plastic bottle - est - 1 1/2 02. _-,-..-' Mogul Products Co. (Phenolphthalen) O-Phenanthroline Ferrous Sulfate Complex (I) 4 fl. 02. - est - 3 fl. 02. 1,10-Phenanthroline Ferrous Sulfate Complex (1) 4 fl. oz. - est - 3 fl. 02. Phenol - phthalen (1) est'2 02. plastic bottle - est - less than 1/8 02. 4% Rocheltex (1) est. 4 oz. plastic bottle - est - 3 1/2 oz,. A-8 058471 Liquid 2% Sodium chromate (1) est. 1 pt. bottle - est - less than 1/8 pt. " " Sodium diphenylamine sulfonate (1) est - 4 oz. plastic bottle - est 3 oz. V> " • 1% starch (1) est 8 oz. bottle - est - 3 oz. Crys- 10% starch (1) est 2 oz. bottle - est less than 1/8 oz. talized (min.) Liquid Tyopaeolen (1) est 2 oz. bottle - est 1 oz. • • 15% Tartaric Acid (.1) est 1 pt. bottle - est - 1/3 pt. " ' 1% Thymolthalfin (alcohol sol) (1) est 1 pt. bottle - est - 1/2 pt. " " .1% (Tropalolin)? 0 Water Base (for NAOH in Cd baths) (1) est 4 oz. plastic bottle - est - 2 1/2 oz. " ' 1/2% (Tropaeclin)? for NAOH Cd. Tank (1) est 4 oz. plastic bottle - est - 2 oz. - AREA C Liquid Amyl Alcohol (1) est 1 pt. bottle - est - 7/8 pt. AcH Hydro (cannot identify) (1) est 1 pt. plastic bottle - est 4 1/4 pt. Ammonium Sulfide (1) 1 pt. bottle - est - 3/4 pt. Beryllium nitrate (Be(N03}2.3H2Q) (1) est 200 gm bottle - est - 75 gm Butyl Acetate (1) 1. pt. bottle - est - 3/8 pt. Collodion U.S.P. (Alcohol 24%) C 407 (1) 1 qt. bottle - est ~ 3/4 qt. Diacetyl"(CH3COCOH3) (1) 4 fl. oz. bottle - est - 3 fl. oz. Dodecyl Alcohol (1) 4 fl. oz. bottle - est - 2 1/2 fl. oz. Dowex 1-X8 (used) (1) - est. 500 gm bottle - est - less than 100 gm Ethyl Acetate (1) est 1 pt. bottle - est - 1/4 pt. Formaldehyde Solution 37% w/w (1) pt. bottle - est - 1 pt. • • (1) 1 pt. bottle - est - 1/2 pt. A-9 058471 Liquid Formic Acid (1) 1 qt. bottle - 1 qt* Glycerine (1) 1 pt. bottle - 1. pt. Hexyl Alcohol (CH3(CH2)50H (1) est - 500 gm bottle - est - 300 gm Hydrochloric Acid (1) 2.72 Kg 6 lbs. - est - 5 1/2 lb. (Area D) Lactic Acid Merck U.S.P. - 85% (2) 1 lb. bottle - est - 5/8 lb. Lime Water U.S.P. - (1) est 1 qt. bottle - est - 1 qt. NW Kleer Aid #35 dated 02-22-79 (1) est - 1 qt. plastic bottle - est - 1 qt. • #5-A " " " (1) est - 1 qt. plastic bottle - 1 qt. • #2-X " " " (1) est - 1 qt. plastic ', bottle - 1 qt. Nitric Acid (A.C.S.) (1) 7 lb. bottle - est i lb. (Area D) 2,2,2-Nitrilo - Triethanol (1) 250 gm bottle - est - 125 gm Nitrobenzene (1) 1 pt bottle - est - 1 pt. Acid Oleic, U.S.P. (1) 1 qt. bottle - 1 qt. Potassium Hydroxide Solution (1) est 1 pt. plastic bottle - est - 3/4 pt. Acid Perchloric 70-72% (1) 1 lb. bottle - est - 3/4 lb. Pyridine (1) 1 pt. bottle -est 3/4 pt. 10% Sulfuric Acid (1) 9 lb. bottle - est - 11/2 lbs. Sulfuric Acid (2) 40 ml plastic bottles - est - 30 ML (Area D) Acid Sulfuric, Fuming (Oleum 65%) (1) est 1 pt. bottle - est - 1/2 pt. Toluene - 3,4 - dithiol (CH3CgH3(SH)2 MW 156.27 (1) 5 gm bottle - est - 2 gra. Triisooctyl Amine, Tech. (2) 100 gr - 125 gr Titanium Trichloride 20% solution (1) 1 kg bottle - est. 1/2' *9. A-10 055471 Liquid Thioglycollic Acid (1) double container est 2 oz. "' • Tri-N-Butyl Phospha(Label Torn) (1) 1 pt. bottle - est - 1/2 pt. " • Hydrogen Peroxide (4) 1 pt. bottles' - est - 4 pt. • • Hydrofluoric Acid (6) 1 lb. plastic bottles - est - 3 lbs. AREA D Liquid Acetone (used) (1) 1 qt. bottle - est - 1 pt. Ammonium Hydroxide (1) 4 lb bottle -est - 2 lbs. ^Benzene (1) 1 gal. bottle - est about 1 qt. (Brobine?) water (1) est. 1/2 gal. bottle - est - 1 1/2 qt. f Carbon Tetrachloride (1) 1 gal. bottle est >- 1/8 gal. Chloroform fl) 1 gal bottle - est - 1/8 gal. Ethyl Alcohol (1) 1 gal bottle - est - 1 gal.- Hexane (1) 1 gal. bottle - est - 1/8 gal. Methanol (1) 1 gal. bottle - est- 3/8/ gal. Methyl Isobutyl Ketone (2) 1 gal. bottles - est - 1 gal. AREA E Liquid Ba(N03)2 10% w/? dated 9/23/81 (1) est 1 qt bottle - est */4 qt- ...•••- • • . Bromo Cresol purple (1) est 1 pt. bottle - est - 3/4 pt'. " " Bromophene Blue (1) est 2 plastic bottle - est - 1/2 oz. " " Bromothynol Blue (in wa'ter) (1) est - 4 oz. plastic bottle - est - 3/4 oz. • • It Diphenolamine indicator in acetic acid (1) est - 2 oz. plastic bottle - est - 3/4 , • • oz. • " 1% Diphenolamine indicator in B2SO4 (1) est - 2% plastic bottle - est - 3/4 oz. • • E.D.T.A. - Di Sod. 21.500 gl/liter dated 09/13/83 (1) est 1 qt bottle - est - 3/8 qt. - powder Eriochrome (Cd) Black T ind (1) est - 1 pt. bottle - less than 1/8 pt. (Mim.) A-ll 055471 Liquid 8% Formaldehydez (1) est 1 pt. bottle - est - 1/4 pt. " ' 25% H2SO4 (1) est 1 pt. plastic bottle - est - 1/4 pt. " " HgCl2 saturated (1) est* 1 pt. bottle*- est - 1/2 pt. " " H3PO4 Cone. 0.85% (1) est. 1 qt. plastic-'ibottle - est - 3/4 qt. • ' 10% KI - (1) est - lqt. bottle - est - 1/4 qt. • " Methyl Orange (1) est. 1 pt. bottle - est - 1/4 pt. Powder (Murexide or Marexide) (1) est 1 pt. bottle - est - less than 1/8 pt (Mim.) Liquid 0.1 IJ AgN03 (1) est - 1 gt. bottle - est - less than 1/6 qt. TMim.) " ' 01N K3Cr307 (1) est - 1 qt bottle - est - less than 1/8 qt. " " Phenolthalein pH 9.0 2 drops/100 ml 1 gram/0.1L Ethanol 50 L dated 05/28/80 (1) est. 4 oz. plastic bottle - est - less than 1/8 oz. " " 9.9 g/lL 9.9% NLX Sol. U in AcL + BNO3 dated 12/01/80 (1) est 1 qt. bottle - est -1/2 qt. " " HSO3NK2 1.5 M (1) est 1 qt bottle - est - 1 qt. • " Na2S203.5H20 for Cn03 and iridite F«2.243 (1) est - 1 qt. bottle " • SNR dated 11/13/80 (1) 4 oz. plastic bottle - est - 2 oz. Crystal Stannous Chloride (1) 1/4 lb. bottle -est - less than 1/8 lb. Liquid Sulfo Orange pH 11.0 - 12.6 (1) est 1 pt. bottle - est - 3/4 lb. .•••"•'.'•••'•'.''.:. • * 5% SrCl in HC1 Sol (1) est - 1 pt. plastic bottle - est - 1/2 pt. Powder Thyodene (indicator for IODIM (IODIMETRY) (1)4 oz. bottle - .est - 2 ozs. Liquid 15% v/v H204 15% v/v H3PO4 15% (1) est - 1 qt. bottle - est - 1/4 qt. A-12 058*71 | AREA F I Liquid Acetic Acid (Glacial) (2) 5 lb. bottles - est - 6 lbs. • " Hydrochloric Acid (written across bottle is contaminated) I for cleaning -(1)5 lb. bottle- est - 1 1/4.lbs Hydrochloric Acid (1) 5 lb. bottle - est - 4 3/4 lbs. I Hydrochloric Acid (10% written on label - (1) 5 lb. bottle - est -^ 1/2 lbs. I Hydrochloric Acid (52%) (2) 1 lb. plastic bottles - est - {I 1 1/4 lbs. • 8N HN03 (1) est 5 lb. bottle - est - 4 3/4 lbs. • 12N HNO3 (1) est 5 lb. bottle - est- 3 lbs. Nitric" Acid (1) 7 lb. bottle - est - 3 4/4 lbs. | Phosphoric Acid 85% (2) 1 gal bottle - est - 1 1/2 gals. Sulfuric Acid (3) 9 lb bottle - est - 4.5 lbs. Ammonium Hydroxide (NH4OH) (1) est pt bottle - est - 1 3/8 pt. •.:•...-•;• -.-.:;.•.••': ~ I HNO3 Cone (1) est 1 pt. plastic bottle - est - less than m 1/8 pt. I HNO3 1:1 (1) est. 1 gal bottle - est 1/4 gal NAOH Sol to Neutralize HNO3 (1) est - 1 gal bottle'- est • - 5/8 gal. Cone Acid Sulphuric (H2SO4) (1) est - 1 pt bottle - est - less than 1/4 pt. Misc. (6) Unknown contents (4) in open containers (powder form) Chips (2) in est 1 pt plastic bottles Liquid (1) Magnesium chips in sealed bottles - est - less than . 1/4 lb.\ • • Sulfuric chromic Cleaning Sol. (1) est - 1 gal bottle - est - 1/2 gal A-13 058471 AREA G Liquid 0-Tolidine dated 09/30/69 (1) Est. 1 pt bottle - Est - 3/4 pt. ' " 0-0.5 M Vanadyl Sulfate (1) Est. 1 pt bottle - Est - 3/4 pt (liquid has film on top and bottom) • " Kerosene (odorless) (1) 1 gal. bottle - Est - 3/4 gal. Note: Probably not kerosene. • " AgN03 0.25% (1) est 1 pt. bottle - est - 3/8 pt., " " Alizarin Red S (1) est 1 pt. bottle - est - 3/4 pt. • * Alkali - Iodine Azide (1) est - 1 pt plastic bottle (liquid with crystals on top and bottom) - est -__3/4 pt.. • • 1% Ammonium Molybdate (1) est - 1 pt plastic bottle - est - 3/8 pt • • Al Ammonium Behzoate (1) est - 1 pt bottle - est - 5/8 pt " " Arsenazo (1) est 1 pt bottle i- est - 5/8 pt • " Diphenylamine Sulfonate; Barium (1) est 1 pt bottle - est - I Pt • • 0.1% Ditzo (1) 100 ml bottle - est 50 ml " " Erichrome BT (1) est 2 oz. bottle - est - 3/8 of 2 oz. " " 1M Ferrous Sulfate (1) est 1 pt. bottle - est - 1/2 pt. • " Manganese Sulfate (1) est 1 pt. bottle ^ est - 5/8 pt. • " Al 8-quinollinol in d.L HAC (1) est 1 pt bottle - est - 3/4 pt. .:'-•:.••••-' " " 0.025N Sodium Thiosulfate (1) est 1 qt. bottle - est - 3/4 • " 10% SnCl2 (1) est 1 pt bottle - est - 1/4 pt. • '•• Nitric Sulfamic'- Molybdate (1) est - 1 qt. bottle - 1/3 qt. . • " Si Reducing Sol. (1) 1 pt. plastic bottle - est - 1 pt " * 0.01H - 0.27% Sodium Diphenylamine Sulfonate (1) est 1/2 pt. bottle - est - 1/4 pt. • " Sodium Arsenite 5 g/1 (1) est 1 qt bottle - est - 7/8 qt. • " 1.5M Sulfamic Acid 150 g/1 (1) est 1 qt. bottle - est - 3/8 qt. A-14 058471 AREA H Kodak Glass Plates — unopened (2) boxes - 36 plates 4" x 10" - Total 72 Spectrum Analysis Plates #1 Kodak Spectroscopic Plates (2) opened boxes - 12 plates 4° x 10" - Total 24 Dylon Graphite Cement (1) opened 1 gal can - est - 1 gal Dylon Super Refractory Cement (1) opened qt can - est - 1 qt Liquid 2% Benzoinoxime in ethyl alcohol (1) est 1 qt bottle - est - 1/2 qt Buffer Solution Concentrate (1) pt bottle - est *- 3/4 pt 4% Ferrous Ammonium Sulfate (1) est qt plastic bottle - est - 3/4 qt Frinchrome cyanine R (1) est qt bottle - est*- 3/4 qt 5% HF(1) est 1 pt plastic bottle - est - 3/4 pt Methylene Blue 0.001M (1) est 1 pt plastic bottle - est - 5/8 pt Methylene Blue-stock Sol. 3.676 g/l (1) 'l 1/2 plastic bottle - est - 1 1/2 pt 0.5M TTA/Xylene (1) est 2 oz. bottle - est - 1 oz. 20% NH4SCN (1) est 1 pt bottle - est - 1/4 pt 20% NH4SCN (1) est 1-pt bottle - est - 3/4 pt 0.1M KMn04 (1) est 2 oz. plastic bottle - est - 1 oz. H20 Distilled (2) est 1 gal bottle - est — 3/4 gal (Dump it unless rad) 1% 0 - Phenanthroline/ethylalchol (1) est 4 oz. bottle - est - less than 1 oz. 0.5% Ortho Phenanthroline (1) est 1 pt plastic bottle - est - 1/2.pt 35% SnCl2 (1) est 1 qt. bottle - est - less than 1/4 pt. 0.1% Thoron (1) est 1 pt.. bottle.- est - 3/4 pt. Titanium Reference solution 1,000 ppm (4) 1 pt. plastic bottls - est - 3 3/4 pt. A-15 058471 Liquid Triethanolamine buffer dated 3-2-73 (1) est 1 pt. plastic bottle - est - 1/2 pt. " " Ethyl Acetone (1) 4 liter can -est - 4 liters Unknown Liquids Liquid (4) 1 qt plastic bottles (D-19 on label dated 10/24/79 - est - 4 qt Crystal (1) dried and crystal formed - (1) qt. bottle Liquid (1) Est pt. bottle - est - less than 1/4 pt. Liquid (1) Est 4 oz. bottle - est - 3 oz. LABORATORY STORAGE ROOM INVENTORY - UNOPENED Sulfuric Acid (2) 9 LB. (4 KG) Bottles - ' ' ' • Hydrochloric Acid (16) 6 Lbs. (2.72 KG) Bottles Hydrogen Peroxide (36) 1 Pint Plastic Bottles Acetic Acid Glacial (6) 3 Lbs. (2.26 KG) Bottles Sodium cloride - 25 Lb. Box Sulfamic Acid (1) 500 g (1.1 Lbs.) A 295 Sodium Phosphate (1) 453 g (1 Lb.) S 373 Sodium Oxalate <1) 453 g (1 Lb.) S 356 (78722) Sodium Hydroxide (3) 500 g (1.1 Lb.) S 318 Vanadyl Sulfate (1) 100 g (3.5 oz.) V8 Stannous Chloride (4) 113 g (1/4 Lb.) T 142 (78998) Silver Nitrate (1) 100 g (3.5 oz.) S 181 Barium Diphenylamine Sulfonate 5 g (0.18 oz.) B 38 Zinc Metal (1) 453 g (1 Lb.) 2-12 (80126) Carminic Acid (4) 5 g (785550) Congo Red (1) 453 g (1 Lb.) A-795 Mannitol D-Mannitol (1) 500 gm (1.1 Lbs.) H-120 Ferrous Sulfate (3) 453 gm (1 Lb.) 2070 A-16 058*71 Magnesium Perchlorate (1) (size unknown) Magnesium Acetate (1) 453 gm (1 Lb.) M-13 Citric Acid (canhydrous) (1) 2.26 KG (5 Lbs.) A-106 Kodak (Liquid) X-ray Fixer and Replenisher (2) 5 gallons Kodak (P-122) Color Print Processing Kit (1) (1 gallon of 6 solutions) Kodak Hardener Stop Bath Process p-111 (1) to make (3-1/2 gal) Kodak First Hardener - Fixer (1) to make 3-1/2 gallons Kodak Rapid Fixer with Hardener (1) to make 1 gallon of film and plate fixer and 2 gallons of paper fixer Kodak Bleach and Replenisher (1) can to make 3-1/2 gallons of | solution (13.2 Liters) process P-111 Type R Kodak Developer D-19 (1) can to make 1 gallon (3.8 Liters) Kodak Developer C-22 (1) can to make 3.5 gallons (13.2 Liters) ; Kodak color Developer Process P-111 (1) can to make 3.5 gallons of solution (13.2 Liters) DARK ROOM - OPENED Liquid Kodak - Versatol Developer (2) 1 gal. Bottle - Est. 1 gal. Stop Bath - (1) 4 Lb. Bottle - Est. 3 Lbs. • Kodak - Photo- Flo concentrate (1) 1 gal. Bottle - Est. 1/2 gallon • Foto Flow 1:600 (1) 1 gal. Bottle - Est. - 1/2 gal. • Kodak - DEKTOL 2* (1) 1 gal. Bottle - Est. - 3/4 gal. Microdol 476 (1) 1 gal. Bottle - Est. - 3/4 gal. • Kodak - indicator Stop Bath (1) 1 Pt. elastic container - est - 1/2 pt. Fixer (1) 1 gal. Bottle - Est. - 3/4 gal. • Kodak Hardener (contains sulfuric acid) Est. 8 fl. oz. (1) plastic bottle - Est. 8 fl. oz. •• Kodak - Print Flattening Solution (1) 8 fl. oz. Bottle - est - 1 fl oz. A-17 058471 Kodak - Photo- Flo 200 Solution (1) A fl oz bottle - est - 2 fl 02. • Kodak - Print Flattening Solution (1)1 gal bottle - est - 1/2 gal. .Stop Bath - (1) gal.bottle - est 1 pt. ** • Versatol for Paper (1) 1 gal bottle - est - 3/4 gal. Kodak - Print Flattening Solution (1) 1 gal bottle - 1/2 gal • (1) Bottle of Liquid - Unknown contents - 3/4 gal (in acid bottle - Red Cap) DARKROOM - UNOPENED Kodak First Developer Replenisher (1) Can Process 111 Type R to make 5 gallons of solution (19 liters) Kodak First Developer Process P-lll Type R (1) Can to make 3.5 gallons of solution (13.2 liters) Kodak Suffer P-122 (1) Can to make 3.5 gallons (13.2 liters) of solution or 2.25 gallons of replenisher (8.5 liters) Kodak Direct Positive Film Developing Outfit (1) Box Kodak Developer P-122 (1 Box) to make 3.5 gallons (13.2 liters) Kodak Processing Kit for Processes E-2 and E-3 (1) Box 1/2 gallon size (1.9 liters) Kodak color Print Processing Kit P-122 (1) Box Net Wt. 3.25 lbs. (1.2 kilos) 1 gallon size (3.8 liters) A-18 058471 SODIUM COMPOUNDS - UNOPENED Powder or Sodium Acetate (1) Bottle 5 lb. bottle - est. - 2.5 lbs Crystals Sodium Ammon. Phosphate C.P. (2) Bottle - est no. wgt. Sodium Arsenite (META) (1) 1 lb. Bottle - Es* - 3/4 Lb. Sodium Azide (1) 1 oz. Bottle - Est - 1/4 oz. Sodium Bicarbonate (1) 5 lb. bottle - est - 1-1/2 lbs. Sodium Bisulfate C.P. (1) 1 lb. bottle - est - 1/4 lb. Sodium Bisulfite (META) (1) 1 lb. bottle —est - 1/2 lb Sodium Borate (1) 1 lb. bottle -r est - 1/2 lb Sodium Carbonated) 5 lb. bottle - est. - 2 lbs Sodium Chloride (1) 1 lb bottle - est - 1/16 lbs Sodium Chromate (1) 1 lb bottle - est - 7/8 lbs Sodium cobaltinitrite (1) 1/4 lb bottle - est - 1/4 lbs Sodium Dichromate (technical) (2) 1.1 lb bottle - 1.1 lbs *•-.-•• Sodium Fluoride (Acs Reagent) (2) 1 lb bottle - 1.3 lbs Sodium Kypophosphite (1) 1 lb bottle - est - 3/4 lbs Pellets Sodium Hydroxide (1) 1.1 lb bottle - est - 2/3 lbs Powder or Sodium Nitrate (2) 1 lb bottle - est - 1 lb Crystals sodium Oxalate (1) 1 lb bottle - est - 2/3 lbs Sodium Perborate (1) no weight on bottle - est - 3/4 lbs Sodium Phosphate (1) 1 lb bottle - est - 3/4 lbs Sodium Potass. Tatrate, c.P. (1) 1 lb bottle'1/4 lb Sodium Pyrophosphate (1) 1 lb bottle - est - 1/4 lb Sodium Silicate (1) 1 lb bottle .- est - 1/2 lb Sodium Silicofluride (1) 1 lb bottle - «st - 3/4 lb Sodium Sulfate, N.F. VII (1) 1 lb bottle - est - 1/16 lb A-19 i 058471 Powder Sodium sulfate (Anhydrous) (1) 5 lb bottle•- est r 2\lbs Crystals Fused Flakes Sodium Sulfide 60% (1) 5.5 lb bottle - est - 4 lbs i Sodium Sulfite <1) 5 lb bottle - est - 3 lbs Sodium Thiocyanate (1) 1 lb bottle - est - 1/2 lb Sodium Thioglycolate (1) 100 gm bottle - est - 50 gm Sodium Thiosulfate (1) 1 lb bottle - est - 1/2 lb Sodium Diphenylamine Sulfonate (1) 10 gm bottle - est - 3 gms Powder Sodium piphenyi-Benzidine Sulfonate (1) 5 gm bottle - 1.5 gm Sodium Rhodizonate (1) 1/10 gm bottle - est - min. amount- . Magnesium Uranyl Acetate.(1) est 1 02 bottle - est 3/4 oz Granular-Sodium Chloride (3) 5 lb containers - est - 13 lb SODIUM COMPOUNDS - OPENED Powder Potassium Bicarbonate (1) 1 lb bottle - est - 1/2 lb Potassium Binoxalate, C.P. (1) 1 lb bottle - est - 3/4 lb Potassium Bisulfate (3) 1 lb bottles - est - 2 lbs potassium carbonate (1) 1 lb bottle - est - 3/4 lbs Potassium Bromate (1) 4 oz bottle - est - 4 oz Potassium Chlorate (1) 1 lb bottle - est - 3/4 lbs Potassium Chloride (1) 5 lb bottle P-217 - est - 3.5 lbs Potassium Cyanide (2) 1 lb bottles - est - 1 lb Potassium Dichromate (1) 5 lb bottle - est -2.5 lbs Potassium Dichromate (2) 1 lb bottles - est - 1.5 lbs Potassium Ferricyanide (2) 1 lb bottles - est - 1 lb Potassium Ferricyanide (1) 4 oz bottle - est - 2 ozs Potassium Iodate (1) 4 oz bottle - est - 3 ozs A-20 056471 I Powder Potassium. Iodide (2) 1 lb bottles - est - 1/2 lb I • Potassium' Fluoride.(1) 5 lb bottle - est - 2.5 lbs Pellets potassium Hydroxide (1) 1 lb bottle - est - 1/4 lb I Flakes . Potassium Hydroxide (1) 1 lb bottle - est - 3.5 lbs I Powder potassium Nitrated) 1 lb bottle - est - 1/4 lb' potassium Oxalate (1) 5 lb bottle - est - 2 lbs I . potassium Permanganate (2) 1 lb bottles - est - 3/4 lbs potassium Periodate (1) 4 oz bottle - est - 2 oz I . Potassium Phosphate (3) (Dibasic) 1 lb bottles - est - 2 lbs I Potassium Phosphate (1) (Monobasic) 1 lb bottle - est - 3/4 lb I potassium Phthalate (1) 4 oz bottle - 1/2 oz Potassium Pyrosulfate (1) 5 lb bottle - est - 3 lbs I Potassium Sodium Tartrate (1) 1 lb bottle - est - 3/4 lb Potassium Thiocyanate (1) 4 oz bottle - est - 1/4 oz I Potassium* Xanthogenate (1) 1 lb bottle - est - 3/4 lbs I crystal Potassium Hydrogen Phthalate (1) 4 oz bottle - est - 1.5 ozs I Liquid Potassium Chloride Solution (1) 4 fl oz (maybe not used?) ...... OPENED - A's I Powder Alizarin (1) 25 gm bottle - est - 1 gm I Alizarine Sodium Monosulfonate (1) est - 1/2 oz Alizarin Red S (1) 25 gm bottle - est - 25 gms I Alizarol cyanine P.c (I) 10 gm bottle - est - 6 gms Aluminon (2) 25 gm bottles 7 est- 15 gms I Wire Aluminun Metal (1) 1 lb box .... I Powder 1-Amino 2-Naphthol-4 Sulfonic Acid (1) 25 gm bottle - 12.5 gm I A-21 I 056*71 Powder Aroinopyrene (1) 5 gm bottle- est - 2.5 gms • 4-Aminoantipyrine (1) 25 gm bottle - est - 12.5 gms Lump Antimony (1) 1 lb container - est - 1/2 lb Powder Antimony Metal (1) 1 lb bottle - est -3/4 lb l-(0-Arsonophenylazo)-2-Naphthol-3,6-disulfonic Acid Disodium Salt (1) unknown weight bottle - est - 1/2 oz 3-(2-Arsenophenylazo)-4,5-Dihydroxy-2,7 - est - Naphthalene Disulfonic Acid (1) 10 gm bottle - est - 5 gm Crystal Solid Arsenic Metal (1) 4 oz botle - est - 3 oz Crystals Aerosol OT (1) est 5 lb bottle ^ est - 3/4 lb Fiber Asbestos (1) large bottle - est - 2 lbs Powder Aluminum Green CZ (1)1 lb metal container - est - 1/4 lb Alundum (Norton) 'KRm (1) 5 lb bottle - est - 2 lbs Alumina, Adsorption (1) 1 lb bottle - est - 3/4 lb Crystal Aluminum potassium Sulfate (1) 1 lb bottle - est - 3/4 lb Powder Aluminu (caustic) (1) plastic container - est - 1/4 lb Amberlite CG 400 (1) 1 lb bottle - est - 3/4 lb Amberlite CG 50 (1) 1 lb bottle - est - 3/4 lb Crystal Ammonium Acetate (1) 5 lb bottle - est.- 2.5 lbs powder Ammonium Bifluoride (1) plastic container - est - min., amount Ammonium Borate C.P. (1) 4 oz bottle - est - 3 oz Crystal Ammonium Bisulfate (1) 1 lb bottle - est - 1/2 lb Lumps Ammonium Carbonate (1) 5 lb bottle - est - 1 lb Powder Ammonium Chloride (1) 5 lb bottle - est - 1-1/2 lb • Ammonium Citrate (1) 1 lb bottle - est - 2 oz Crystal Ammonium Fluoride (2) 1 lb botrtles - est - 1.5 lb A-22 G56i71 I Crystal Ammonium Formate (1) 1 lb bottle - est - 1/2 lb Ammonium Oxalate (1) 1 lb bottle - est - 1/2 lb I Ammonium Nitrate (1) 5 lb bottle - est .- 3.5 lbs I Ammonium Nitrate (1) 1 lb bottle - est - less than -1/4 lb - Aluminum Nitrate (1) 5 lb bottle - est - 3 lbs I Ammonium Molydate (1) 4 oz bottle - est - less than l'oz I Ammonium Molydate (1) 1.1 lb bottle - est - 1/2 lb Ammonium Perchlorate (1) 1 lb bottle - est - 3/4 lb I Ammonium Phosphate, Dibasic (1) 1 lb bottle - est - 1/2 lb • I Ammonium Sulfate (1) 1 lb bottle - est - 3/4 lb I Ammonium Sulfate (2) 4 oz bottles - est - 6 oz • Ammonium Tartrate (2) 1 lb bottles - est - 1-1/2 lbs Ammonium Thiocyanate (4) 1 lb bottles - est - 2-3/4 lbs Anhydrome (1) 1 lb bottle - est - 3/4 lb Powder Atomized Aluminum - 325 (1) can - est ?• 1 lb • Atomex - Immersion Gold Solution (1) bottle - est - less, than 1 oz Liquid Atomex (Cyanide) Immersion Gold Solution (1) 1 gal bottle - 1 gal powder Alodine 1200 (paint-bonding) (1) 1 q-t can - est - 1 pt OPENED - B's Powder Barium Carbonate C.P. (1) 1 lb bottle - est - 3/4 lb Barium carbonate (1) 1 lb bottle - est - 1/2 lb Barium Chloranilate (1) 10 gm bottle - est - 3 gni Barium Chloride (1) 1 lb bottle - est - 3/4 lbs Barium Fluride (1) 1 lb bottle - est - 3/4 lb Barium Hydroxide (1) 1 lb bottle - est - 3/4 lb A-23 056471 Powder Barium Nitrate (1) 1 lb bottle - est - 1/4 lb Benzenearsonic Acid (1) 100 gm bottle - est - 60 gm Benzidine Base (1) 25 gm bottle - est - 16 gm Benzohydroxamic Acid Potassium Salted) 25 gm bottle - est - 10 gm Benzoic Acid Ammonium Salt (1) 250 gm bottle - est - 200 gm , Benzoin Oxime (cupron) (1) 100 gm bottle - est - 75 gm Benzoyl Peroxide,cP. (1) 4 oz bottle - est - 3 oz 2,2'-Bipyridine (1) 5 gm bottle - est ^ 1 gm Granular Bismuth Metal (1) unknown weight bottle - est - 1 lb Powder Bromcresol,Green (3) 5 gm bottles -est - 5 gm .Bromcresol purple (2) 10 gm bottles -est - 4 gm Bromothymol Blue (2),10_gm bottles - est - 4 gm Bromophenol Blue (1) 5 gm bottle - est - 1.5 gm Liquid Brom Phenol Blue indicator (1) small bottle - 1 oz Powder Boric Acid (1) 1 lb bottle —est - 3/4 lb Boric Acid (1) 5 lb bottle - est - 1.5 lb barium piphenylamine Sulfonate (2)-(l) 5 gm bottle-(l), 10 gm bottle - 7-1/2 gm OPENED - C's Sticks Cadiurn Metal (1) 1 lb container - est - 3/4 lb Turnings Calcium (1) 1/4 lb bottle - est - 1/4 lb powder Calcium Acetate (1) 1 lb bottle -est - 3/4 lbs Calcium Carbonate (1) 4 oz bottle - est - 2 02 Granular Calcium Chloride (1) 1 lb bottles - est - 3/4 lb Crystals Calcium Chloride -<1) 1 lb bottle - est - 1/2 lb 20 Mesh Calcium Chloride (!) 5 lb bottle - est - 2.5 lb 4 Mesh Calcium Chloride (1) 5 lb bottle - est - 3.5 lb A-24 053471 I Powder Calcium Hydroide (2) 1 lb bottles - est - 1.25 lb I Granular Calcium Oxide, N.F. (1) 5 lb bottle - est - 2.5 lb Powder Carminic Acid (1) 5 gm bottle - est - 1 gin I " Ceric Ammonium Sulfate (1) 1 lb bottle - est - 1/2 lb I Cerium (ic) Sulfate (1) 4 oz bottle - est - 3 02 • Ceric Sulfate (1) 4 oz bottle - est - 2 02 I Granular Chromium (1) 1 lb bottle - est - 1/3 lb Powder Chromium (2) 1 lb bottles - est - 10 ozs I Chrome powder Grade #1 (1) 1.1 02 jar «*• est - 1.1 02 Chromium Oxalate (1) 1 lb bottle - est - 1/2 lbs I Cinchonine (2) 140 gm bottles - est - 110 gms I Citric Acid. (Anhydrous) (1) 1 lb bottle - est - 1/4 lb Cobalt(ous) Chloride, c.P. (2) 02 bottles - est - 6 02s I Clayton Yellow (2) 100 gm bottles - est - 70 gms Cobalt Metal (1) 4 02 bottle - est - 2 oz I Granular cobalt Metal (1) 1.1 02 bottle -' less than 1/4 bottle Powder Columbium Metal (1) 4 gm bottle - less than 1 gm I Chips combax Accelerator (1) 5 lb bottle - est - 2 lbs • Copper (1) est 2 02 bottle - est - less than 1 02 Powder Copper Oxide (1) 1 02 bottle - est - 1/2 o: • , ; copper(ous) Chloride C.?. (1) 1 lb bottle - est - 1/2 lb Granular Cr03 (1) 1 lb bottle - est - 1 lb Powder Cupferron (1) 100 gm bottle - est - 25 gm Cupferron (1) 100 gm bottle - est - 25 gm Cuprous cyanide (1) 1 lb bottle - est - 1/2 lb Cupric Fluoride (1) 1 lb bottle - est - 3/4 lbs Cupric Oxide (1) 1 lb bottle - est - 1 lb Cupric sulfate (1) 1 lb bottle - est - 1/2 lb A-25 .058471 Powder Cupric Sulfate (1) 5 lb bottle - est - 3.5 lbs • Curcuroin (1) 10 gm bottle - est - 8 gms Resins Carboset 525 (1) 5 lb plastic bottle - est - 3/4 lb Liquid carboset 514 H (1) 5 lb bottle - est - 1/2 pint AREAS D AND E - OPENED Powder- Dimethyl Glyoxime (1) 4 02. bottle - est - 3.5 oz 5-(p-Dimethylamina)-Benzylidene Rhodanine (1) 10 gm bottle - est- 8.5 gms 2,9-Dimethyl-l 10-Phenanthrolihe (1) 1 gm bottle *• est - 1/2 gm 1,3-Dipenylguanidine (1) 100 gm - est - 90 gms P-Dipenylaminesulfonic Acid Sodium Salt (1) 5 gm bottle - est - less than 1 gm 1,5-Diphenylcarbohydrazide(1) 10 gm bottle - est - 1.5 gm Diphenyl Carbazone (1) 5 gm bottle - est - 1.5 gm Diphenylthiocarbazone (2) 10 gm bottles - est - 9 gms 5-Diphenylcarbazide (1) 25 gm bottle —est - 15 gms .. Dithizone (1) 10 gm"bottle- est - 2 gms Spheres Dowex 50W-X8 (2) 1 lb bottles - est - 3/4 lb' :; Si 5 50-100 MESH ~ Spheres Dowex 50W-X8 (1) 5 lb bottle - est - 2.5 lbs 50-100 MESH , v.. ; Spheres Dowex 1-XlO (1) 1 lb bottle - est - 3/4 lb 200-400 MESH Spheres Dowex 1-X8 (1) 1 lb bottle - est - 1/4 lb 100-200 MESH Crystal Dextrose/Anhydrous-D-Glucose (1) 1 lb bottle - est - 3/4 lb Granular Devarda's alloy (1) 1 lb bottle - est - 1/3 lb A-26 058471 Powder Dextrin (Bacteriological) (1) 4 oz bottle - est - 2 oz Disodium Ethylenediaminetetraacetate (1) 1 lb bottle - 1/2 lb Eriochrome Black T (1) 10 gm bottle - est - 2 oV.s Erythrosine Red (1) 1 oz bottle - est - 1/2 oz Ethylenedinitrilotetraacetic Acid (3) 1 lb bottles, est •-* 1-1/2 lbs Crystal prierite (CaS04) (1) 5 lb bottle - est - 1 lb AREAS F AND G - OPENED Granular Ferrous Ammonium Sulfate (2) 1 lb bottles - est Purified - 3/4 lb Lump Granular Ferric Sulfate (1) 1 lb bottle - est - 1/2 lb Powder Ferric Sulfate (1) 1 lb bottle - est - 1/4 lb Fuchsin (Basic) (1) 10 gm bottle - est - 8 gms Flouescein (2) est 10 gm bottle - est - 10 gms Powder Graphite Powder (2) 1 lb bottles - est - 1 lb Powder Graphite Powder (2) 8 oz bottles - est - 3/4 lb 325 MESH Powder L-(+)-GlUtaraic Acid - (1) 100 gm - est - 90 gms AREAS H AND I - OPENED Granular Hexamethyl-Enamine (1) 1 lb bottle - est - 3/4 lb Hydrazine Sulfate (2) 100 gm bottles - est - 120 gms Hydroxylamine Hydrochloride (2) :100 gm bottles - est - 50 gms Hydroxylamine Hydrochloride (2) 500 gm bottles - est - 350 gms Hydroxylamine Sulfate C.P. (1). (1.) 100 gm bottle - 50 gms Powder Iodine, USP (1) est 100 gm bottle - est - 90 gms A-27 058471 Powder Iron metal (1) 1 lb.bottle - est - 3/4 lb Iron metal (reduced by Hydrogen)/ (1) 1 lb. bottle - 3/4 lb Iron, N.F. (1) 1 lb bottle - est - 3/4 lb Granular Indicarb 6-10 Mesh (1) 1 lb bottle - est - Foil Indium Foil from Film Badges - 3 pes in a bottle Chips/ Flakes Iron Chip (1) unlabeled plastic bottle - est - 1/2 lb AREAS L AND M - OPENED Powder Lanthanum Chloranilate (1) 25 gm bottle - est - 10 gms Shot 20-260 Lead Metal (1) 1 lb container - est - 3/4 lb ••- Granular Lead (4) 1 lb bottles - est -,2-3/4 lbs Crystal Lead Acetate (1) 4 oz bottle - est - 2 ozs Lead Acetate (2) 1 lb bottle r est - 1-1/2 lbs Powder Lead chromate (1) 1 lb bottle - est - 1/2 lb " Lead Carbonate (1) 1 lb bottle - est - 1 lb • Lithium Chloride (1) 4 oz bottle - est - 3.5 oz Lithium Chloride (1) 1 lb bottle - est - 1/2 lb Powder Macro Bronze ^ 4 (1) 1 lb plastic bottle - est - 3/4 lb • ' -:- Mg (1) 1 gal tin cans - est -' 4 lbs " 2-Methyl-8-Quinolino (2) 5 gm bottle - est - 2 gms • Magnesium sulfate (1) 1 lb bottle - est - 1 lb Crystal Magnesium Nitrate (1) 1 lb bottle - est - 1/2 lb Powder Magnesium Perchlorate (1) est 1 lb bottle - est - 1/4 lb • Manganous Sulfate, Monohydrate (1) 5 lb bottle - est - 3-1/2 lbs • Manganous sulfate Monohydrate (1) 1 lb bottle - est - • 1/2 lb A-28 058471 Powder Manganese Dioxide Special (1) 25 gm bottle - est - 25 gms Magnesium Ribbon (2) 12" pc in bottle - est - 24" Mercuric Chloride (2) 4 02 bottles - est - less than 1 02 Crystal Mercuric Chloride (1) 4 02 bottle - est - less than 1 02 Powder Mercuric Iodide (1) Red 1 02 bottle - 1 02 Crystal Mercuric Nitrate (1) 1 lb bottle - 1/2 lb Powder Mercury (ic) Chloride (2) 1 lb bottle - est - 1-1/4 lb Mercuric Thiocyanate (1) 1 lb bottle - est - 3/4 lb Methyl Oxalate (1) 100 gm bottle - est - 100 gms j Crystals Methylene Blue (1) 25 gm bottle - est - 12.5 gms Methyl Red (1) 1 02 bottle - est - less than 1/2 02 Methyl Red (2) 4 02 bottles"- est - 4 02 Methyl Orange 4 02 bottle - est 3 oz Molybdic Anhydride (1) 4 02 bottle * est - 2 02 Powder Murexide (1)1 gm bottle - est - less than 1/2 gm AREAS N AND 0 - OPENED Powder 1-Naphthylamine (1) ,100 gm bottle - est - 60 gm , r 1-Naphthylamine Hydrochloride (1) 100 gm bottle - 70 gm Nickel Ammonium Sulfate (1) 1 lb bottle - 3/4 lb Nickel Formate (1) est. 4 oz bottle - est - 3.5 02 Nickel Ketal in Powder Form (1) est 4 02 bottle - est - 2 OZ - Nickel Metal (1) 1 lb bottle - est - 1/2 lb Crystal -Nickel Nitrate (1) 1 lb bottle - est - 3/4 lb powder Niobium Pentoxide (1) est. 4 02 bottle - est - 1 oz Nitrilotriacetic Acid (1) 500 gm bottle - est - 250 gm Nitrilotriacetic Acid (2) 100 gm bottle - est - 125 gm A-29 35847! Powder P-Nitrodiazoamino-Azobenzene (1) 2 gm bottle - est - less than 1 gm Nitron (1) 25 gm bottle - est - 12.5 gm Nitro Phenol (1) 10 gm bottle - ess - 10 gm Crystal NiS04 (1) est. 100 gm bottle - est - 100 gm • NiSp4 (1)' 1 lb bottle- est - less than 1/4 lb Powder Nickel Sulfamate (SNAP) Anti Pit (1) 1 lb box - est - 1/4 lb Liquid Nickel Sulfamate (Concent) (1) 1 gal bottle - est.- 2 pints Crystals Osmic Acid (2) 1/4 gm bottle - est - 1/2 gm Powder Oxalic Acid (2) 1 lb bottles - est - 1-1/2 lbs Granular Oxalic.Acid (1) 1 lb bottle - est - 3/4 lb Oxalic Acid (1) 5 lb bottle - est - 1-1/2 lb AREA P - OPENED Palladium Chlo(Missing) (1) 1/4 oz est. bottle -.est - less than 1/4 oz Powder Pan (1) 1 gm bottle - est - less than 1/4 gm Pan Indicator (1) 1 gm bottle - est - 1/4 gm O-Phenanthr.oline (1) 10 gm bottle - est - 1-1/2 gm Liquid Phenanthroline Ferrous sulfate complex (1) 1 fl oz - est—less than 1/4 fl oz Crystals Phenol (1) 1/4 lb bottle - est - 1/8 lb Powder Phenol Red (1)1 gm bottle - est - less than 1/4 gm Phenolphthaleih (1) 1/4 lb bottle - 1/8 lb Phenolphthalein (1) 1 lb bottle•- 3/4 lb N-Phenylanthranilic Acid (1) 10 gm bottle - est - 10 gm est •-„•.: ! • Phenylmercuric Acetate (Pract.) (1) 100 gm bottle - est. - 75 gm A-30 058471 Powder Phthalic Acid Monopotassium' Salt (1) est 1/4 lb.bottle • - est - 1/8 lb • Phosphorous (1) 1.1b bottle - est - 3/4.lb Crystals plantanex 111 L.S. (1) 12 gm bottle - est - 9 gm • Platinum Diammino Nitrate (1) est 4 oz bottle - est 1 02 Powder Phosphorous Pentoxide (1) 1 lb bottle - est - 1/2 lb. (powder appears to have gotten wet just on top.) • Primuline Yellow (1) 10 gm bottle - est - 6 gm Pumice Stone N.F. (1) 1 lb bottle - est - 2/3 lb. " Pyrocatechol violet (1) 5 gm bottle - est - 1 gm AREAS Q AND R - OPENED Powder Quinalizarin (1) 5 gm bottle -.est - 1 gm • 8-Quinolinol 8-Hydroxyquinoline (1) 1/4 lb bottle - est - 1/4 lb " 8-Quinolinol 8-Kydroxyquinline (2) 1 lb bottles - est - 1 lb Powder Rexyn *RG50 (H) (1) 1 'lb bottle - est - 1/2 lb Rexyn *101 (H) (1) 5 lb bottle - est - - Crystal Rhodamine B (1)10 gm bottle - est - 8 gm AREA S - OPENED " Crystals Salicylic Acid (1) 1 lb bottle - est - 3/4 lb Powder Silicic Acid (1) 1 lb bottle - est - 1/4 lb BBS or Pellets Silver Chloride. (3) 20 gm plastic bottles - est - 10 gm Crystals Silver Nitrate (2) 1 lb bottles - est - 1/4 .lb Silver Nitrate (1) 4 oz bottle - est - 1-1/2 oz Powder Silver sulfate (2) 1 oz bottles - est -1/4 oz Crystals Stannous Chloride (1) 1/4 lb bottle - est - 1/8 lb. (Crystals appear to have gotten wet on top.) powder Starch (1) 1 lb bottle - est - 3/4 lb A-31 058471 Crystals Succinic Acid (1) 1 lb bottle - est - 3/4 lb " Sulfamic Acid (1) 500 gm bottle - est - 250 gm ' Sulfamic Acid (1) 1 kg - est - 1/2 kg Sulfanilic Acid (1) 1 lb bottle - est - 3/4 lb • Sublimed Sulfur, N.F. (1) 1 lb bottle - est - 2/3 lb Crystals Silica Gel - Air Dryer (5) metal discs 1/2' x 3" - est - 5 oz Liquid Sel-Rex Temperex HD Gold Solution (1)1 qt plastic bottle - 1 qt AREA T - OPENED Powder Tannic Acid (1) 4 oz bottle - est - 2-1/4 Tannic'Acid Merck (1) est 25 gm bottle - est 20 gm • " Tantalum Pentoxide .(1) est 5 gm bottle - est - less than 1 gm • Tantalum (1) est 5 gm bottle - est less than 1 gm :-..- Crystals Tartaric Acid (1) 5 lb bottle - est - 2 lbs • Tetramethylanunonium Hydrotriborate (1) est 4 oz bottle - est 1 oz " Thenoyltrifluoroacetone (1) 25 gm bottle - est - 5 gm " Thioacetamide (1) 4 oz bottle -est 1 oz • , Thiourea (1) 500 gm bottle -est - 400 gm • Thorium Nitrate (2) 4 oz^bottle •'- est - 3.5 oz Powder Thorium Oxide (1) est 1 lb bottle - est - 1/3 lb Chunks Thorium Oxalate (1) est 1 lb bottle - est - 3/4 lb powder TBQ Indicator (1) est 4 oz bottle - est - 3 oz • Thymolphthalein C.P. (1) 10 gm bottle - est - 5 gm. ,r • Thymolphthalein (1) 4 oz bottle - est - 2 oz • Tin Metal 30 Mesh (2)1 lb bottles - est - 1 lb • Tin Metal (1) 1/4 lb bottle - est - 1/8 lb A-32 353471 Crystals Trichloroacetic Acid (1) 1 lb bottle - est - 1/2 lb " Tri-Sodium Phosphate (1) est 25 02 bottle - est - 5 oz Titaniiim(ic) Oxide (1) 1 lb bottle - est - 3/4 lb • O-Tolidine Dihydrochloride (1) 100 gm - est - 1^0 gm Powder Trioctylphosphine Oxide (1) 25 gm bottle - est - 12.5 gr Tropaeolin 0, Dry Indicator (1) 25 gm bottle - est - 20 gms Tungsten 30 Mesh (1) 4 oz plastic bottle - est - less .than 1 oz • Tungsten Oxide (1) 4 oz bottle - est - less than 1 oz AREAS U, V, AND Z - OPENED _ • Crystals Uranium Acetate (1) 1 oz bottle - est - less than 1/4 oz • Uranyl Acetate (1) 1 oz bottle - est - less than 1/4 oz Uranyl Acetate (1) 1/4 lb bottle - est - 1/8 lb Urea (1) 1 lb bottle - est 7/8 lb Powder Vanadium Pentoxide (1) 4 oz bottle - est - 3-1/2 oz Crystals Vanadyl Su.lfate (lj 1/4 lb bottle --est - 3-1/2 oz Crystals Zinc Acetate (1) 4 oz bottle - est.- 3-1/2 oz Zinc Chloride .(1) 1 lb bottle - est - 1/2 lb Dust Zinc Metal (1) 1 lb bottle - est - 3/4 lb Granular Zinc Metal 30 Mesh (1) 1- lb bottle - est - 5/8. lb Zinc Metal 30 Mesh (1) 1 lb bottle - est - 1/4 lb Zinc Metal (8 to 30 Mesh Combined) (1) 1 lb bottle - est - 1/4 lb • ~ Zinc Metal40 Mesh (1) 5 lb bottle - est - 2-1/2 lb Chips . Zircaloy 2 (1) est 1 lb bottle - est - 1/4 lb Powder zirconium Chloride (1) 1 lb bottle - est - 1/2 lb • zirconium Chloride (1) 4 oz bottle - 1.25 oz • zirconium Oxide (1) 1 lb bottle - est - 3/4 lb A-33 055471 Powder Zirconium Sulfate (1) 4 oz bottle - est - 3 oz ' Zirconyl Nitrate (1) 1 lb bottle - est - 3/4 lb . ' Zinc Oxide (1) 5 lb bottle"- est - less than 1 lb. A-34 G5347. SPECTROGRAPH* ROOM Spectrographically standardized Substance (1) Ammonium Metavanadate 1 g Three sealed wooden boxes. NH4VO3 - Ammonium Cannot determine actual •weights. Weight listed on Aquochlororuthenium wooden boxes. (NH4).2Ru.(H20) Cl5 (2) Ammonium Molybdate 20 g Three sealed wooden boxes. (NH4)6 M07 024 4 H20 (1) Antimony Tetxaoxide (Sb204> 1 g (1) Ammonium Titanyloxalate 10 g Three sealed wooden boxes, (NE4) Ti0(C204)2 H20 (1) Barium carbonate (BaC03) 10 g : i (1) Bismuth Oxide (Bi203) 10 g (1) Crado Oxide 10 g (1) Cadmium Oxide (CdO) 5 g (1) cobalt Oxide (C03O4) 10 g (1) Cupric Oxide (CuO) 10 g (1) Dysprosium Oxide (Dy203) 1 g (1) Europium Oxide (EU2O3) 1 g (1) Hafnium Oxide (Hf02) 1 g (1) Iron Oxide (FE2O3) 5 g (1) Lanthanum Oxide (1^203} 1 g (1) Lead Oxide (PbO) 5 g (1) Manganese Oxide (Mr^O^j) 10 g I (2) Molybdenum Trioxide (M0O3) 20 g (1) Nickel Oxide (NiO) 10 g I (1) Silver Oxide (Ag20) 5 g (1) Sodium Nitrate (NaN03) 5 g I (1) Tantalum Pentoxide (Ta20s) 1 g I A-35 I 058*71 (1) Tin Oxide (Sn02) 5 g (1) Thorium Oxide (Th02) 5 g (1) Tungsten Trioxide (WO3) 5 g (1) Vanadium Pentoxide (V2O5) . 5 g (1) Zirconium Oxide (Zr02> 10 g (2) Aluminum Oxide (AI2O3) 20 g Unopened; est (1) Boric Acid (H3BO3) 10 g Unopened; est (1) Beryllium Oxide (BeO) 5 g Unopened; (1) Calcium Carbonate (CaC03) 10 g opened est. 7 gm (1) Chromium Sesquioxide (C^Cji INCOMPLETE SPECTROGRAPH ROOM - LABORATORY Standards - Spectrographically standardized substances "Matthey Specpure' Johnson Matthey and Limited London Container sizes are 1 to 10 grams. Magnesium Oxide Cobalt Oxide - Yttrium Oxide Dysprosium Oxide Silicon Dioxide Cadmium Oxide Zinc Oxide Sodium Nitrate Lithium Carbonate . Silver Oxide Lithium Nitrate Molybdenum Oxide Chromium Sesquioxide Barium carbonate Calcium Carbonate Bismuth Oxide Beryllium Oxide Ammonium Titanyloxalate Boric Acid Antimony Tetraoxide Aluminum Oxide Molybdenum Trioxide Nickel Oxide Molybdenum Trioxide Potassium Perrhenate Ammonium Molybdate Thorium Oxide Lead Oxide Tantalum Pentoxide Zirconium Oxide Cupric Oxide Vanadium Pentoxide Tin Oxide Hafnium Oxide Europium Oxide Iron Oxide Gadolinium Oxide Ammonium Metavanadate . Ammonium Aquochlororuthenite A-36 053471 Standards - Spex Industries, Inc. . Container sizes are 2 to 20 grams Titanium Dioxide (6) Thulium Oxide Lanthanum Oxide Niobium pentachloride Neodymium Oxide Germanium Oxide Ammonium Phosphate Gallium Oxide/Graphite "Al" Copper Flouride Strontium Flouride Gallium Oxide Spex Mix Sodium Chloride Standards - New Brunswick Labs U308 Analyzed Samples.for Spectrographic Use (30) 25 g each Th02 for Spectrographic Analysis (6). Miscellaneous Standards and Samples Cresilver (75% Pure Ag) Thorium (9) Misc. Lab Standards (21) Magnesium MgCs (20 5) Lacquer samples U3O8 Samples (4) Yellow liquid (4) 100 ml Vollmetric Three pint-size boxes of miscellaneous standards, including nickel, uranium, molybdenum iron, chromium. Each sample contained in small vials of 1-g capacity. v Standards.- Miscellaneous Five 1-quart cans of miscellaneous standards and samples, primarily U3O8. Samples are contained in 1-g vials. A-37 05S^7i Powder Normal Uranium Oxide (1) bottle - est - 1/4 lb .— " NBL Std Uranium Oxide (1) bottle - est - less than 1/4 lb • Depleted Uranium Oxide (1) bottle •- est - less than 1 oz Chips Unalloyed Depleted Uranium (1) bottle - est - brittle reads 699 g Powder 9.3% Enriched Uranium (1) bottle - 32 gms • 4,9% Enriched Uranium (1) bottle - est - 32 gms Pellet Ag (1) bottle - (1) pellet - est - less than 1 02 Thick Fused H3B03 (1) bottle - est - less than 1 02 Flakes Powder Ignited Si02 (1) bottle - est - 1/4 lb Powder Nb2n5 (1) bottle - est - less than 1 oz Liquid Mixed Indicator Methyl-Red-8r Methylene Blue (1) - est - 4 c bottle - est - 2 oz (6) bottles of unknown contents A-39 055*71 UNOPENED STANDARDS . .— U.S. Department of commerce NBS Silicon Steel 131 c (1) U308 950 b (1) U-900 (1) U-850 (1) U-800 (2) •• UO3 Analyzed Sample # 18 (4) OPENED-STANDARDS Powder U-005 (2) Pew Partials U-010 (1) Few Partials U-015 (1) Few Partials U-020 (1) Few Partials (Less than 1/2 lb total) U-030 (2) (1) Few partials U-050 (2) (1) Few Partials U-850 (2) (1) Few partials U-900 (2) (1) Few partials Crystals Th Metal Chips f 20 (1) less than 3/4 lb Th Metal Chips I 19 (1) est - less than 1/4 lb Wire Iron metal (1) 4 02 container - est - 3 02 Solid Cadmium, R (1) container reads 20 gr " Zr 1 (1) container reads 57.0 g " Zr 4 (1) container reads 56.5 g " • Z* 2 (1) container reads 59.5 g Powder Synthetic Salt Std. (1) 4 02 bottle - est - 3 02 Large Chips Unknown Metal Punchings for Carbon - est - 1 02 Small Chips Unknown Metal Turnings for Carbon - est - less than 1 02 Shot Unknown Metal Shot for Carbon - est - less than 1 oz 100 Mesh Stainless Steel (1) est - 3/4 lb Powder Chips Unknown Metal (3) bottles read just 1,2,3 - est - 4 oz Solid Depleted Unalloyed Uranium (2) bottles - est - 5 lbs Peilets^ Normal Uranium (1) bottle - est - 1/4 lb . A-38 MATERIALS INVENTORY Item Type and No. Estimated NO. Item of Containers Quantity Comments ELECTROPLATING ROOM ER-1 SNAP (1) 10-gal 7 gal Allied-Kellite. Non-hazardous and Non toxic. container ER-2 SNAC (1) 10 gal 3 gal Allied-Kellite * • ER-3 isobrite 541 (1) 5-gal Carboy 2 gal Allied-Kellite. Cadimtim Plating Brlghtner ; - Non-hazardous and non-toxic. ER-4 Iridite 8P (1) 1-gal can 1 gal Allied Kcllite. Cadmium or Zinc Blue Bright. Contains chromic acid. ER-5 SNR 24 (1) 55-gal drum 20 gal Allied-Kellite. ER-6 Caustic Soda (2) 400-lb 400 lb Crystal drums ER-8 Muriatic Acid (1) 55-gal,plastic Hydrochloric Acid. drum . .. ER-9 caustic-Soda (1) 55-gal drum 20 gal (Solid) ' ER-11 Boric Acid (1) 30-gal druin 5 gal Drum marked for Magnesium Chips. » ER-12 Hater conditioner 20 gal Tower contains white "rock salt" like Packed Tower material. '< ER-13 Unknown <. i (1) 10 Gal 8 gal ER-14 Unknown (1) 5-gal 2 gal container .y, ER-15 Unknown (1) 5-gal 1 gal Contains white crystalline substance. drum MATERIALS INVENTORY Item Type and Ho. Estimated Ho. Item of Containers Quantity .__ Comments OIL ROOM OR-1 Misc. Oil ft 5 gal Grease Cans t • \ OR-2 DTE Heavy Oil (1) 55-gal 40 gal Mobil Corp. drum i >' METALS PLANTS MP-1 Carbon ft Graphite , (1) fiberboard 10 lb Union Carbide Corp. Causes Irritation. Powder . container MP-2 Carbon ft Graphite , (1) 1-qt can 1 qt Same as above Bonding Liquid MP-3 Enamel Paint (1) 1-gal can 0.55 ga g l Protective Coatings. MP-4 Reducer (2) 1-gal cans . 1 gal Michigan Chrome and Chemical Co. Plammable MP-5 Pep Epoxy (1) 1-gal can 1 gal Protective Coatings. Toxic, combustible. • Activator Component B MP-6 Pep 1 Epoxy (1) 1-gal can 1 gal Same as above. Enamel Component A MP-7 Aerosol cans Paint (5) 15-oz cans en Plammable oo Cleaners, (13) 15-oz cans Plammable Lubricants, and •• i Penetrating Oil MP-8 Tap Zol Tapping (2) lpt cans 2 Pt Rust Lick Corp. non-Combustible. Contains . Fluid 1,1,1 Trchloroethane, Inhibited E.P ami . Patty oils. MATERIALS INVENTORY Item Type and No. Estimated No. Item of containers Quantity Comments MP-9 Red Gauge Oil (1) Plastic Tube 0.75 Oz. Dwyer Industries MP-10 Silver Plating (1) Lb can 1 Lb The Cool Amp. Co. Powder (Cool-Amp) • 1-- : \ MP-11 PR-1 Polyester (1) Qt can 1 Qt Townsend Inc. Flammable Liquid, contains Resin Styrene • MP-12 Hi-Temp Anti- (1) 4 oz Can 2 Oz Pel-Pro fnc. Lubricant and sealer Seize compound MP-13 DAP 33 Glazing (1) 1 Qt Can 24 Oz Dap Inc. Glazing compound $ MP-14 High Vaccum (I) Plastic 50 Oz Dow corning Silicone Lubricant Grease Container (II) Tubes - r •• : - ;; 10 (6) 100 Lb 600 Lbs Dresser industries. Harbison Walker MP-15 Flint Mill bags Refractory ( MP-16 Unibond P/19 (1) 55 Gal 25 Gal Unicast Development Corp. Flammable Liquid Drum HP-17 Terra Paint (3) 100 Lb 225 Lbs Poseco. Foundry Products Division. Irritant. cans Liquid Ceramic Facing * HP-18 Silicon Spray (1) 60 Lb 60 Lb IMS Co.~ * canister MP-19 Dolemlte (5) 55 Gal 200 Gal J. E. Baker Co. (Pueller's Drums o Earth) OJ MP-20 zirconia Powder (1) 5. Lb 1 Lb > Container . MP-21 Yttrium oxide (2) 25 Lb bags 30 Lbs Research'chemicals Division of NUCOR MATERIALS INVENTORY Item Type and Ho. Estimated No. Item of Containers Quantity Comments MP-22 capacitors General Electric (1) Cat I 19P622 No. M376264 Pyranol Capacitor. Contains PCBs. Red Label (2) Cat I 19L622H SN N512359. 0.78 Gal of Combustible Liquid. Green Label (3) Cat I 19L522 No. HO92002 Pyranol Capacitor. Red Label (4) Cat I 19L582NH No. H514339. Blue Label MP-23 Reactor 1 Hunteroon Transformer Co. Fleming, NJ Spec. I A-1851-16 315 AMP. NP-2< Hardener (7) 0.5 oz 3.5 OZ 60% Methyl Ethyl Ketone Peroxide • tubes MP-25 Quick Setting (1) Gal Can 1 Gal Sauereisen Cement Co. I Cement (Binder) MP-26 Molybdenum U> 45 Kg 34 Kg GTE Sylvanla-Precision Metals Group Metal Powder Container HP-27 Tasll 301 Cement (1) 100 Lb 25 Lbs Chas. Taylor Sons Co. Contents solidified. Container I MP-28 Preon 113 (1) Gal 1 Gal B. I. DUPont Sottle Trichlorotrifluoroethane MP-29 Lampblack, . . (11) 100 Lb 1100 Lbs R. T. Vanderbllt co. Medium Thermal Carbon (The unak Powder bags , N991) MP-30 Taycor 414 PH (14) 100 Lb 1500 Lbs Taylotylor Refractories Hydrocast (1) 30 Gal Drum Refractory j- • . (Aluminum Oxide) MP-31 Stab-fused (6) 100 Lb 500 Lb . Refractory 2R02- 61.163 (Lustergrip) MATERIALS INVENTORY Item Type and No. Estimated No. Item of Containers Quantity Comments MP-32 X-12263B (42) 100 Lb Cans 4200 Lbs Refractory MP-3 3 Carbase Sodium (2) 30 Gal 500 Lbs BASF Wyanndote. Sodium carboymethylcellylose CMC (5) 100 Lb bags MP-3 4 Dura-Pak (4) 100 Lb bags 400 Lbs Refractory Powder MP-35 Acid Proof (4) 100 Lb bags 400 Lbs Sauereisen Cement Co. Cement 131 Filler MP-3 6 Zircon Plaste (2) 300-lb 400 lb No other markings barrels MP-37 Aery1 60 CD 2-qt l qt Thoro system products contains acrylic resin MP-38 . Celvacene Medium (3) 1-lb 1.5 lb Consolidated Vacuum Corp. Vacuum Crease containers MP-39 Moroline White (1) 16-oz Ragh Inc., Memphis, TN Petroleum Jelly container PAINT STORAGE PS-1 Latex Paint (26) gal cans 20 gal Brand names: Dutch Boy, Protective Coatings. Typical composition-pigment including titanium dioxide, CaCOj, BaSOj, Silicates. Vehicle including acrylic latex, non-volatile acrylic latex, water o PS-2 Enamel paint (53) gal cans 40 gal ' Brand Names: butch Boy, Protective Coatings. Epoxy cu and marine enamels. Typical composition-pigment including metal (iron, titanium) oxides, CaCOj, silicates. Vehicle-Alkyd resins, solvents PS-4 Multi-Purpose (1) gal can 0.5 gal Roberts consolidated Ind. Latex base adhesive Floor Adhesive containing small amount of toluene MATERIALS INVENTORY Item Type and Ho.. Estimated No. Item of Containers Quantity Comments PS-4 Kencove (2) qt cans 2 qt Combustible Mixture Adhesive PS-5 Parks Sealer (1) Gal Can 0.3 Gal Park8 Corporation Primer PS-6 . Catalyst (T-916 (11) Gal Cans 8 Gal Koppers. (Brolite) Pi re hazard. May contain T-917, mild for (2) Gal Plaotic lead or chromium oxide Epoxy) Primers Containers PS-7 T-120 Hash (2) Gal Cans 1 Gal Koppers (Brolite) Thinner PS-8 P-908 Bpoxy (2) Gal Cans 1 Gal Koppers (Brolite) Component (skyspar Epoxy) PS-9 Topcoat Thinner 1) Gal Can 0.5 Gal Sterling Lacquer Co. Paint flammable liquid PS-10 Topcoat Gl08s 1) Gal can 0.5 Gal The Marblette Co. PS-11 • Poiyurethane- 3) Qt Cans 2 Qts Sterling. Flammable Aliphatic PS-12 . Epoxy hardner 1) Qt Can 0.5 Qts Buehler Ltjd. PS-13 Epoxy resin 1) Gal can 0.5 Gal Duehler Ltd. PS-14 Epoxy primer 1) Gal Can 0.5 Gal Koppers (Brolite) a PS-15 Polyurethane 2) Gal Cans 1 Gal Sterling Lacquer. Flammable Coating ' PS-15 Resin-acid Metal 6) Gal Cans 5 Cal Koppers Company, Inc. contains phosphoric Pretreatment acid and alcohol solvents Compound PS-17 . Primer Coating 3) Gal Cans 2 Gal Koppers MATERIALS INVENTORY Item Type and No. Estimated No. Item of Containers Quantity Comments PS-18 A932 Bpoxy Coat (2) Gal Cans 1 Gal Koppers. May contain lead or 1716 Aluminlzed Chromium oxide PC-19 Primer Coating (2) Gal cans 1 Gal Koppers. Spec. No. Mll-P-7962 PS-20 Laminar X-500 1 Pt Can 1 Pt Manufacturer: Dexter-Midland, Fast Production/ Plammable Solvent Reducer PS-21 Unknown 1 qt can 1 qt PS-22 Primer Coating 4 Gal cans 2 Gal Deft. Flammable Phosphate, Ester Resistant, Catalyst Component PS-23 Component 2 (3) Gal Cans 2 Gal Bostick. Flammable. Flash pt, a* Polyamide 28#F. MFR Code CA-15B Converter PS-24 Epoxy Topcoat (3) Gal Cans 1 Gal Bostick. Flammable • Gloss PS-25 Corrosion (5) Gal Cans 4 Gal Bostick. Flammable inhibiting Primer PS-26 Fluid Resistant (2) Gal Cans 1 Gal Bostick. Flammable Flash pt. 23*F Code catalyst CM 16. Spec DMS 1786 0 DPM 2232 PS-27 Resin Acid Metal (6) Qt Cans 4 QtS Koppers Co. Inc., Broilte Div. MFR Code I P- Pretreatment 204 D. Expired shelf Life Coating PS-28 U1344 catalyst (3) Gal Cans 2 Gal Sterling Lacquer Co. Plammable. Contains Aliphatic Polylsocyanates, Ester and Petroleum Distillate'Solvents. Lung Irritant. PS-29 .Paint Thinner (1) Gal Can Negligible Combustible MATERIALS INVENTORY , Item type and No. Estimated Ho. Item of Containers Quantity ; Comments PS-30 Polane catalyst (1) Gal can V66 V27 500-1318 0.5 Gal Sherwin Williams. Combustible. Lung Irritant PS-31 Polane. (Polyure- (1) Gal Can thane Coating) 0.5 Gal Sherwin Williams. Plammable P 63 W13 PS-32 Crystalloid (1) Gal Can 0.5 Gal Dutch Boy. Combustible PS-33 Pluid Resistant (8) Gal cans 6 Gal USH Corp.'Bostlck Chemical Group, code CA-116 Catalyst Spec. DHS, 1786C PS-34 Catalyst Solution (15) Ot Cans 15 Qts Bostlck. Code X-304, X-306 PS-35 Pluid Resistant (5) Gal Cans 3 Gal Dostick. Plammable. Code 463-12-8, Spec DHS 1789C Primer PS-3 6 Primer Rpoxy (5) Gal Cans 5 Gal Bostlck. Plammable. Plash Pt. 2B*P. HPR polyamide Code 463-7-10. Expired Shelf Life Component 1-epoxy Resin Compound PS-37 Corrosion (1) Gal Can 0.5 Gal Essex Chemical Corp. Plammable. Contains' Inhibitive Sealant Toluene. Expired shelf life. PS-38 Accelerator (1) Pt can 1 Pt Essex. Contains Hanganese Dioxide PS-39 Rust-Oleum (1) Pt Can 1 Pt Rust-Oleum, combustible PS-40 Sprft-Tool (IS) 13 oz 195 oz Crown Industrial Products. Spray cans blchlorodifluoromethane Propellant. PS-41 Green-tine (15) 13 oz 195 oz Plammablel Primer Spray Cans PS-42 Netal Working (9) 31 kg 279 kg. Van Straaten ehemlcal Co. QC 14808 Pluid Plastic .951 (Samples) Containers MATERIALS INVENTORY Item Type and No. Estimated No. Item of Containers Quantity Comments PS-44 Primer coating (1) 1-gal cont. 0.25 gal Deft, cod<»,| 02-GN-28; Lockheed Spec LCM-37-1035A. ester resistant base coponent PS-45 PEP 10 epoxy (10) 1-gal cans 9 gal The Passano Corporation, Watervliet, NY. enamel clear component A PS-46 PEP epoxy, (1) 1-gal can 1 gal The Passano Corporation, Watervliet, NY. activator com- ponent B PS-47 T-916 catalyst, (1) 2-gal can 2 gal Drollte - Andrew Brown Co., Marietta, GA. for A-932 17170 aluminized >.i\ ••••" '<•"• > PS-48 . Catalyst for (1) 2-gal can 2 gal Drollte - {toppers Company Inc., Spec No. N11P23377 I 4* epoxy primer 09 PS-49 T-916 catalyst (1) 1-gal plastic 1 gal Broilte identification number 53409250 for A-932 epoxy container • coating . u?'? ••".;-1 - PS-50 PEP-1 epoxy : (1) 1-gal can 1 gal The Passano Corporation, Watervliet, NY. enamel white component A . PS-51 Grey enamel 1750 (1) 1-gal can 1 gal The Marblette Company PS-52 U114C catalyst (1) 1-qt can 1 qt sterling Lacquer Nfg Co., Sunbrlte Subsidiary, '; batch No. 5083 CHEMICAL ROOM CR-1 Nlcklad Electro- (4) 5 Gal 15 Gal The Richardson company. Allied-Kellte Div. less, Nickel con- Fiberboard con- Corrosive. centrate, 794, tainers 794B MATERIALS INVENTORY Item Type and No. Estimated !JO. Item of Containers Quantity Comments CR-2 Solar Salt Dealer (3) 80 Lb bags 240 Lbs International salt Company (Sea Salt) CR-J Iridite 8P (1) Gal Can 1 Gal Allled-Kelite. Oxidzer cadmitia or Zinc Dlue Dright CR-4 Snac Barrett (2) 50 Lb 75 Lbs Allled-Kellite suiramate Nickel Piberboard Acid Compound Containers CR-5 Hetao Granular (1) 55 Gal 30 Gal The PQ Corporation. Sodium Silicate Detergent Drum Detergent. Contained In drum Libeled for Magnesium chips. CR-6 Soda Ash (Dense) (1) 100 Lb Bag 100 Lb Allied Chemical CR-7 Chronic Acid (1) 100 Lb Can 100 Lb Allied Chemical. 991 CrOj Technical Plake. Strond Oxidant. PosIon CR-8 Air Dry Rock (3) Gal Cans 3 Gal Michigan Chrome and Chemical Co. Flammable coating Liquid CR-9 CI452 Primer (1) 5 Gal Metal 2 Gal Michigan Chrome and Chemical Co. Container CR-10 c-12 Activator (1) 5 Gal Metal 3 Gal Container CR-11 Nickel Carbonate (1) 5 Gal Metal 5 Gal No other marking or lablea. 'Container CR-12 Aluminum Cleaner (1) 55 Gal Drum 10 Gal Gaklte Products, inc. Mlldy alkaline with with biodegradable surfactants. CR-13 Lacolene Petro- (1) 55 Gal 15 Gal Ashland chemicals... Flammable leum Naptha drum Liquid ' CR-14 Deslcclte 25 (11) 5 Gal *« r.i OIU..I —I -• • MATERIALS INVENTORY Item Type and No. Estimated No. Item of Containers Quantity Comments CR-15 cadmium Oxide (1) 5 Gal 2 Gal Amax zinc Co. Amax Lead and Zinc Div. Toxic Container by inhalation and Ingestion. CR-16 Sodium Sulfide (1) 55 Gal 38 Lbs PPG Industries. Corrosive solid Drum CR-17 Trisodium (1) 100 Lb Bag 100 Lbs Monsanto Co. Technical TSP Crystalline. Phosphate CR-18 Boric Acid (1) 100 Lb Bag 100 Lbs Stauffer Chemical Co. Granular Technical Grade. CR-19 Sodium Cyanide (2) 200 Lb 350 Lbs Phi Hipp Brother Chemicals, Inc. Poslon. Drums • 99% NaCN CR-20 Nickel Chloride (1) 20 cal 5 Gal Drum labeled for flake caustic. Metal Container CR-21 ZE-3 Emulsifier (1) 5 cal Metal 3 Gal Nagnaflux Corporation. Zyglo-Pentrex Containers Emulsifier. Contains petroleum products and surface active agents. Combustible mixture. Plash Pt exceeds 200°P. CR-22 ZL-30A Penetrant (1) 5 Gal 2 Gal Nagnaflux Corp. Spotcheck Penetrant Formula Container A. Type SKL-w. contains petroleum distillates and surface active agents. Combustible Mixture. Plash Point exceedo 190«P. CR-23 Metso Penta Bead (1) 100 Lb Bag 100 Lbs The.PQ Corp. Pentahydrate Sodium Metasllicate. * * , • '••' ^ - CR-24 Unknown (1) 20 Gal Drum 20 Gal No markings or labels CR-25 Unknown (1) 55 Gal Drum 50 Gal The Mogul Corp. Irritant Marking - AG470 CR-26 Dearborn 157 (1) 55 Cal 30 Gal Dearborn Chemical Co. Corrosive Liquid Drum MATERIALS I NVENTORY Item Type and No. Estimated No. Item of Containers Quantity ^Comments CR-27 8083 Energized (1) 15 cal 10 Gal Crown Industrial Products. Poison. Contains Rust Remover brum Acid. CR-28 Waste Oil S D3bria (1) 20 Gal 5 Gal No Marking or Labels Drum CR-29 Hheelmate High (1) S Gal Netal 3 Gal Norton Company. Grinding Wheel Division Performance Container Metal working Fluid Nitrite Free 674 cn-30 Rust Inhibitor (1) Gal Metal . 1 Gal No Markings or Labels container CR-31 Unknown (1) 40 Gal Drum 30 Gal Amltron chemical Industries, No other > markings or labels. I CR-32 Rins A Mink Plus (1) 5 Gal 3 Gal i ' Amltron Chemical Industries, Inc. Mild Container Alkaline (pro 8-8.5) cleaner. Non-flammable Non-Toxic, Biodegradable. CR-33, Netal Working (1) 5 Gal 4 Gal Daystar Co rip. Non-flammable. Non-Toxic Fluid Concentrate Container CR-34 Nighty Strip (1) 55 Gal 10 Gal Environmental chemical and Equipment Co. (Ammonlated, . - Drum Contains sodium Meta Silicate. Butylized Detergent) CR-35 Sentry Dry Chlori- Oxidizing Agent. Calcium Hypochlorite. nating Chemical •• I- CR-36 Unlbond P/19 (1) 55 Gal 30 Gal Unicast Development Corporation. ..«. Drum Flammable Liquid CR-37 PetIsol 202 (2) 4 Gal 3 Gal Silo Incorporated. Flammable Liquid. Contains Carburetor Containers Orthodichlqrobenzene and Xylol. .r.nd Metal Cleaner MATERIALS INVENTORY Item Type and No. Estimated No. Item of Containers Quantity Comments CR-38 . Microseal Impreg- (1) Gal can 0.5 Gal Themicro Seal nant CR-39 Hydro Seal (1) 55 Gal 20 Gal Radiator specialty company. Contains Drum Chlorinated Hydrocarbons and Cresyllc Compounds. CR-40 Unknown (1) 55-gal Tank contains "bricks.* ; Possibly for Porcelain Tank neutralization. CR-41 Unknown (1) 5.gal 3 gal Container is unmarked and not labeled. metal container CR-42 Potassium (16) 100 lb 1500 lb Majority of bags are opened and spilled Carbonate Bags onto floor. > i • CR-43 Microsol heat- (1) 5-gal 4 gal Michigan Chrome ( Chemical u» hi cured rack coat- container ing E1003 CR-44 Unknown (1) 55-gal drum 50 gal The Mogul Corp. drum markings 64560, EG5345 CR-45 (1) 55-gal drum 50 gal The Mogul Corp., AG470 irrintant. CR-46 Buehler Metadl (1) 1 qt plastic 1 qt Buehler Ltd.; extender for diamond pastes. fluid container CR-47 Microtex micro- (1) 1-gal can 0.5 gal Michigan Chrome.fc chemical - CR-48 Pormula A (1) 5-gal can 4 gal Magna Plux Corp. type SRL-N water washable penetrant combustible .mixture. Plash point exceeds 190P. f » » :> '.• '•- ? CR-49 Unknown' (1) 30-gai 30 gal Amltron Chemical Industries, 9143520660 container s> SPRAY BOOTH SB-1 Unknown (1) Gal Bottle 0.3 Gal Yellow viscous llauld MATERIALS INVENTORY Item Type and No. Estimated NO. Item of Containers Quantity Comments SB-2 Paint Thinner (1) 5 Gal 2 Gal Protective Coatings. Petroleum Oistlllateo. Container SB-3 Laminar X-500. (19) 1 Gal Cans 19 Gal The Dexter Corp. Midland Dlv. Contains Organic solvent. Expired shelf life. Batch lll-MT-48 Spec I BMS-10-86A. Flammable SB-4 X-500 Lt. Stable (22) 1 Ot Cans 5 Gal Dexter Corp. Pi. Pt 108°F Flammable Hardener . Batch S N H44 10-C-81N. Expired shelf life. SB-5 Dope i Lacquer (6) 1 Gal cans 6 Gal Koppers Company-Broilte Dlv. Batch 12-119 Thinner Spec-TT~T-266C SB-6 Acrylic Lacquer (4) 1 Gal cans 4 Gal The Koppers Company. Spec! Mll-t-19544 Thinner A-5 3 SB-7 . Lacquer Acrylic (4) 1 Gal Cans 3 Gal Koppers Spec! M11-L-19537C tlltrocellulose 17178 Aluminum SO-fl Epoxy Polyamlde (3) Gal Can 1.5 Gal Bostick Corp. Spec I Mll-P-23377 D Type 1. Primer Batch 20677. Expired shelf life. SB-9 Primer Epoxy (1) Gal Can 1 Gal Bostick Component 1. Pigmented epoxy resin Polyamlde compound, ij'lash Pt. 28°. Expired shelf life Spec II MU-P-23377C Class 2 Batch 112090. ' SB-10 Epoxy Polyamlde (3) Gal cans 2 Gal Bostick. code X-369. Expired shelf life. Catalyst Spec I Mll-P-23377 D Type 1 Batch 20199. SB-11 Component Mo. 2 (5) Gal Cans 4 Gal Bostick. Flash Pt. 28*F Expired shelf life Polyamlde Converter Spec f1il-P-23377C Class 2 Batch 11380 SB-12 18CA28T322 (1) Qt. Can 1 Qt Technical Research* Highly Flammable Flash Tere'cb Compound B Pt. 20*F. Contains hydrocarbon and oxygenated solvents. Expired shelf life. 175 M Liquid NOS. MATERIALS I Item Type and No. Estimated No. Item of Containers Quantity Comments SB-12 General Purpose (1) Qtcan 1 Ot Broilte. Spec. Lac 37 722 Type I. Batch Costing Primer 44001. SD-14 Aluminum Paste (1) Qt Can •1 Qt Brolite. Batch 12026. 1 SB-15 Catalyst Solution (1) Qt can 0.25 Qt Bostick Corp. Flammable. SB-16 Netyl ethyl (1) S Gal Can 3 Gal Ashland Chemicals. Flammable Liquid Ketone SB-17 Reducer for Rule €€ (1) Gal 1 Gal Deft Chemical Coatings. Flammable Liquid Epoxy Polyamide Primer Spec! nil-T-19588 Hod. Batch 20564. SB-18 03-GT-202 (2) Gal Can 2 Gal Deft Chemical. Flammable. Aliphatic, catalyst Isocyanate Reactant Coating. Polyurethane Component II Aliphatic. Spec Mil-C-83286 B SB-19 OZ-Y-19 Catalyst (2) Gal Can 2 Gal Deft Chemical. Flammable Spec. N11-P-23377C Componlent XX Poly- Class 2 Epoxy Polyamide. Chemical and solvent Amide Converter ' ' ...:,; o> resistant Primer SB-20 Methyl Alcohol (1) 5 Gal can 4 Gal Hallinckrodt. Reagent Grade. •-, • • ' • • . . ^ SB-21 Component I (1) Gal Can 1 Gal Deft Chemical. Polyurethane, Aliphatic Spec' Pigmented Resin M11-C-J3286E -. " Base coating SB-22 A 315 General (1) Gal Can 0.5 Gal purpose coating .. ' ' ,- .-,-.•.; i r i I f '•••'-• SB-23 Topcoat (1) Gal Can 0.75 Gal Pinch Paint * Chemical. Spec. Bms 10-11 II Type Gloss Paint B-24 Epoxy Enamel (1) Gal Can 1 Gal Zynolyte Products Co. Flammable. . Paint MATERIALS INVENTORY Item Type and No. Eotlmated No. Item of Containers Quantity Comments cn-26 Urethane Abrasion ' (1) Gal can 0.75 Gal Desoto Inc. Contains Ester and Ketone Resistant Enamel Solvents. Flammable. SD-27 Blue Label Sll (1) Lb Jar 0.75 Lbs United Hire and Supply Corp. Contains Flux Plourides and Boric Acid. SB-28 Unknown (1) Gal can 0.5 Gal No other markings or labels. SB-29 Whlel Beering (1) 5 Lb 2 Lbs Vavollne Grease Container SB-30 Dykem Steel (4) 8 Ox 16 Oz Dykem Co. blue Layout Fluid I SB-31 Dykem Layout ' (2) 8 Oz Cans 12 Oz Dykem Co. Flammable White {DXK-327) > i SB-32 Unknown (1) Pt Jar 4 oz / White solid; no other markings or labels m SB-33 Dutch Boy Hhlte f) 15 Oz can 8 Oz Dutch Boy. 891 Carbonate White Lead, Lead SB-34 PC 7 Epoxy (1) 16 02 Can 8 Oz SB-35 Component X pig- (1) 1-gal can 1 gal Deft Chemical Coatings Mfr. code Ho. 02-Y-19 mented epoxy resin compound, class 2 SB-36 Acetone (1) 5-gal can 1 gal Ashland Chemical SB-37 Master Quik-Blld (1) 1-gal can 0.5 gal The Kindt-Collins Co. o SB-38 K-lens-H-lens (1) 1-gal plastic 0.5 gal The Wilklni 1 Co. cleaner container SB-39 Permatex thread (1) 16-oz can empty * Permatex Company Inc. sealant with .teflon MATERIALS INVENTORY Item Type and No. Estimated No. Item of Containers .Quantity Comments DAY 1 . 7 ' ' <~ ' '. J t* > '•'> V ' J *' * Bl-1 plly Sludge (8) 55 Cal Drums 400 Gal Oily sludge from machinery catch pans Bl-2 Tool-Mate (1) 5 Gal 2 Gal Container Dl-3 Unknown ,... (1) 55 Gal Drum 30 cal Drum marked "For Lab" Bl-4 Chemtrol 307 ... (1) 100 Lb 100 Lb Precision Finishing, Inc. Highly alkaline Container Bl-5 Finishing Stones (1) 30 Gal Drum and finishing Hill Bl-6 Aerosolcans (21) Spray paint (31) Spray Lubricant (24) Spray cleaner (3) Spray Adhesive r •'• f '• ' (1) Insecticide CI Penetrant $ r- i 'v Bl-7 Phillips Vapor Contains t'hllsol Solvent (Perchloroethylene) Degtcaoer ji J : '• '-•• 01-8 Sump Contains oily water i "' i f^ • „'.*'•' BAT 2 02-1. Alcaid Oil, (1)555 Gal 50 Gal No markings' or labels. Drum D2-3 Rex 13 Ltibe (1) Gal Can 1 Gal Magnaflux Corp. contains inert mineral powders. - t(' -V i ' • • B2-4 Spotcheck (2) 25 Lb 35 Lb Magnaflux Corp. Contains petroleum products Developer SRD-H Containers and surface active agents. Flash pt. exceeds (wet type) i5n.Op MATERIALS INVENTORY Item Type and No. • Estimated MO. Item of containers Quantity Comments B2-5 Zyglo Zl-lC (1) Gal container 1 Gale Magnaflux Corp. Penetrant B2-6 Spotcheck SKL-HP (1) Qt Containers 24 Oz 3M Company. Flammable mixture. . Penetrant B2-7 Thermofax Belt (1) 8 oz Can 8 Oz Crown Industrial Products. Plammablc Cleaner. B2-8 Toolmaker's (3) 8 oz 16 Oz Acco Wilson Ink B2-9 Eel skid (1) 8 Oz Can V: 3 Oz Dykem Lubricating Oil B2-10 Dykem Cteel (2) 8 Oz Can 8 Oz Dykem > I .Blue Ul ••'•' • '-< '•••>•'• B2-11 Dykem layout (1) 8 oz can 4 oz Dykem wltlte DXX-327 B2-12 Liquid Wrench (1) 8 Oz Can 8 Oz B2-13 LACO Sllc-Tite (1) 16 Oz Can Lake Chemical Co. Non Toxic. Paste B2-14 zyglo developer (1) 5 Lb, Bag 5 Lbs ZP-4A Dry Type B2-15 Tam Zirconium (1) 36 Lb 36 Lbs Scrap Container o CO B2-16 Unknown (1) 5 Gal Can Residual No markings or labels. Container B2-17 Niobium Metal (1) 50 Lb SO Lbs ; Kaweckl Chemical Corp. KCl 26C 30/700 powder Container B2-18 Crystalline (1) 50 Lb 50 Lbs HAH Chattel mm. MATERIALS INVENTORY Item Type and no. Estimated No. Item of Containers Quantity Comments In} D2-19 Pelpro Anti-8iew (lV 16 Oz can 8 oz Cmp. B2-20 Pilo Bond (1) Qt Can industrial 10 Oz Goodyear. Plammable mixture. Adhesive . B2-21 cove Base (1) Ot Can 24 Oz Adhesive WW Henry Co. Combustible mixture. Contains Methyl Alcohol. B2-22 Angle Cyclinders (24) SO Lb 1200 Lbs 1 Ceramic Tumbling BOKCO Med Is .r , :<-fi BAY 4 ' •> •: •• 5 M Unisbrb v-1 Hon- (3) 48 Lb Bags shrink Grout 120 Lba Unisorbi Machinery Installation Systems B4-2 Embeco 636 Grout (7) 55 Lb 385 Lbs Master Builders Bags.^jtv;,.., i i .''? 5 \u B4-3 Insblock 19- 2 Boxes Refractory A. P. Green Refractors B4-4 * MC-25 Refractory <13V 45*kg Bags 585 Kg A. P. Green 5 B4-5 Castolite ' (11)100 Lb 800 Lbs A. P. Green Insulation Castable ; B4-6 * Unknown' (1) 5 Gal can 5 Gal Supplier: • Sager-Spock Supply, Albany B4-7 Safety-Kleen (1) 30Gai c 10 Gal ;•- Safety Klcen Drum B4-8 Magnesium (1) 30 Gal . chips Drum H Gal. Reade Manufacturing. Plammable solid. B4-9 e Jebco (1) 180 Lb. 180 Lb J. E. Baker Co* Spilled onto floor contents. MATERIALS INVENTORY Item Type and No. Estimated No. Item of containera Quantity Comments B4-10 Jebco (1) 25 Lb Bag 10 Lba J. E. Baker B4-11 Sunicut flD 406 (1) Gal Can 1 Gal Sun Oil (Sample 3927) 84-12 Lbreaco TWPB (1) 200 Lb ISO Lba Loresco DWI Backfill Container B4-13 Multifax 2 (1) 120 Lb 90 Lb8 Texaco Crease Container B4-14 Used Oil (1) 5 Gal 2 Gal B4-16 Acid Proof (1) Gal can 1 Gal . sauereisen Cement Co. cement > I B4-17 , Carbon and 10 Lba Union Carbide. Causes Irritation in Graphite Povder «o OUTSIDE BIN OB-1 No. 900 Neutral (35) 400 Lb 7 tone Park Chemical Co. Poiaon. Contains Barium Salt Containera Chloride. OB-2 San Heat 900 (8) 400 Lb 3,200 Lba Henry B. Sanaon k Sons, Inc. Containera OB-3 R-17 Neutral Salt (4) 400 Lb 1,600 Lbs Park Chemical Co. Poiaon. Acid Soluble Salt Containera of Barium OB-4 Nu-SAl Neutral Salt (4) 400 Lb 1,600 Lbs Park Chemical Co. Containers OFFICE AREA OA-1 . Calcium Sulfate 5 Lbs in various containera including volumetric (Desaicant) flasks, jars, baking pan MATERIALS INVENTORY Item Type and No. Estimated NO. I ten of Containers Quantity Comments OA-2 Sodium Chloride 5 Lb Jar 5 Lbs Majlinckrodt USP. Grade (Granular) OA-3 Kleen-Peel 1 Qt Jar 16 ox Beck Chemicals OA-4 Viaolite Filter Dag (1) Gal can 1 Gal Baghous* Accessories, Inc. Tracer Compound OA-5 Unknown 1 Qt jar 1 Qt Pale yellow liquid OA-6 Brake Fluid (1) 5 Gal can 2 Gal Scholle Co. TOOL ROOM TR-1 Permatex (1) 11 Oz Tube 11 Ox Permatex Co. Combustible Mixture. Form a Gasket I o TR-2 Master Quick (1) Gal Can 0.5 Gal The Kindt-Collins Co. Contents Solidified Bild Plastic Filler TR-3 K-Lens-M (3) 1 Gal 2.5 Gal The Wllkins Co. Non Flammable Lena cleaner,. Dottles TR-4 yellow 77 Wire (2) 1 Gal Cans 0.3 Gal Ideal Industries Pulling Lubricant TR-5 Contact Cement (1) Gal can 0.3 Gal Roberts Consolidated Industries TR-6 ffheel Bearing (1) 5 Lb 2 Lbs Vavolini; Greaae Container o Go TR-7 Unkne'.tn (1) Qt can 0.25 Qt •fc- -J TR-8 Bar ft chain (1) Qt Can 1 Qt Sabre Townsend saw chain Co. Lubricant TR-9 Vibron A-43 (5) Qt Cans 3.5 Qts Burgess and Associates Drive Lube MATERIALS INVENTORY Item Type and Mo. Estimated No. Item of containers Quan 11 ty Comments TR-10 GRP-orange (1) 4 ox can 4 Oz Shellac TR-11 Vaspar I 70 (1) Qt Can 5 Oz The Valspar Co. combustible contains petroleum ' Danish Oil Distillate TR-12 Sunoco (1) Gal Can 1 Gal TR-13 Kinseal Vacuum (2) Qt cans 2 Qts Kinney Vaccum Co. Sealer TR-14 Unknown (1) Qt Can Qt Harry Miller Corp. TR-15 Gram Traction . (1) Qt can 1 Qt Graham Transmissions Lube TR-16 . Paint (2) 1 Qt can lot TR-17 Lapping and (4) 1 Lb cans 3 Lbs Clover Mfg. Co. Grinding (1) 0.25 Lb Can Compound (Grease Kix) TR-18 Dykem Layout (9) 0 Oz Cans 50 Oz Dykem Co. Flammable White DXX-327 TR-19 Dykem Steel (7) 8 OS Cans 24 Oz Dykem Co.| Blue TR-20 Parker Lube (1) 4 Oz Tube 4 oz. Parker seal Co. Barium Base TR-21 Special Purpose (1) 0 Oz Can 8 oz seeburg Corp. Oil TR-22 Sanding Disc <1) 8 Oz 4 Oz Sear8 fc Roebuck Co. Cement Container TR-23 . Quick Drying (26) 1 Oz 26 Oz Honeywell ink for Strip Containers Chart Records MATERIALS INVENTORY Item Type and No. Estimated No. Item of Containers . Quantity Comments TR-24 York's 3 in 1 (3) 1 Lb cans 2.5 Lbs York Engineering Co. • l<• Special Plux 77 Tft-25 General Purpose (2) 16 02 32 Oz. HG Welding Products. Corrosive, contains zinc Soldering plux Dottles - Chloride • TR-26 Sure Poot (8) 1 Gal Cans 8Cal Hemisphere Chemical Corp. Non-skid Safety (component A) ;< Surface :- \ J •. (7)1 Qi cans 7 Qts (Component D). TR-27 Perrp Plux . (1) 16 Oz Can 12 Oz Union Carbide. Contains Soda Ash. TR-28 Nokorode (1) 1 Lb can 8 Oz The M.W. Dunton Co. Contains Zinc Chloride •Soldering Paste TR-29 Snopake (1) Pt can 4 oz Litho Art: Products. Plammable. Contents Solidified. TR-30 Solvent and (1) Pt can 4 Oz Union Rubber and Asbestos Co. extremely plammable. Thinner ; TR-31 • Kleerite Rubber (1) Qt Can 16 OZ American Writing Ink co. Cement Type I TR-32 2 Cycle Oil (1) Pt Can 1 Pt Homelite , TR-33 Rld-a-Blrd 4 Rods Rid-A-Blrd Inc. Poison .-, Rods „• TR-34 Haste Oil (2) Pt Jars 8 Oz TR-35 Unknown (1) 16 oz bottle 16 oz Clear liguld in Pepsi bottle. TR-36 Sil Plux (3) 16 Oz ' 32 Oz Soldering Containers TR-37 Kestcr soldering 11) 1 Lb Can 12 oz Litton Systems, contains zinc Chloride. Paste MATERIALS INVENTORY Item Type and No. Estimated No. Item of Containers Quantity Comments TR-38 Pipe Joint (1) 16 Oz can 12 oz Hercules Chemical - Compound TR-39 Metal Marker (6) 8 Oz Tubes 48 oz John P. iNlssen Jr. Co. TR-40 Taagon Penetrat- (1) 3 Oz Can 1.5 Oz Samuel Cabot, Inc. ' ing Rust Solvent TR-41 Liquid Mrench (1) 8 Oz Can 8 Oz Radiator Specialty Co. Combustible Mixture TR-42 Hi-Temp C5-A (1) 10 Oz Can 10 oz Pel Pro, Inc. Anti-sieze Lubricant TR-43 Kodak Rapid CD 4 Oz. Tube 4 Oz Kodak Mounting Cement >I TR-44 Motor Oil (28) 1 Qt. Cans 28 Qts Mobile u TR-45 silicon Rubber (2) 8 Oz. Tubes 10 oz Molykote 111 Compound Dow corning. GE (1) 2.8 Oz. Tubes TR-46 Pen Rust Paint (1) Gal can 1 Gal Passonno Paints. Combustible. TR-47 Do* Hag/ 1 at. can 1 pt Reade Manf. Co. Metal Power Division TR-48 Unknown (2) Pt Bottles 20 Oz Contents unknown. Silver metal appearance (1) 4 Oz Dottle TR-49 High Vacuum (1) 8 Oz 8 Oz Grease Container TR-50 Air Motor (1) 4 oz 4 Oz Lubrication Oil Container TR-51 ink (6) Bottles 10 Oz TR-52 . Rector Seal PVC (1) 16 oz Can 8 Oz The Rector Seal Corp. Extremely Flammable Cement '•>—»•• •;**»• • MATERIALS INVENTORY Item Type and No. Estimated No. Its* of Containers _ Quantity Comments TR-53 Tap zol (3) Pt cans 24 Oz Tapping Fluid TR-56 No. 630 Hultt (1) 14.5 ox 14.5 Oz Purpose Graaaa Tube TR-37 Aluminum paint (1) 1-qt can 0.3 qt All-purpose aluminum paint* other marking! ,1 ! '••'-'. obscured by paint. TR-58 Allan aoldaring (1) 2-oz can paata 1 oz L.o; Allen Co. Inc. w-sr Heavy duty (1) 5-gal can break fluid 2 gal Scholle: combustible mixture • _ SALT BATH AR8A > J SBA-1 Spotcheck af» (1) 55 Gal pormiia Drun 25 Gal Hagna Plux Corp. Combustible mixture. 8BA-2 OHR (1) 55 Gal 25 Gal • DrUM • „' / 8BA-3 Ryaol Surface (2) Gal cana 2 Gal Coat (TC8-6328) The Dexter Corp. Hysol Division. SP14 \ ; 4 * Classification. Hay cause skin sensitization. 8BA-4 Ryaol Tooling (4) Gal Cans 3 Gal Same as above. Compound (TC8- <329,TC8-<328) 8BA-S Hardener (3) Qt Cans TN-3201 2 Qts Same as above. 8BA-6 Hold Release (2) 1 Gal Cane AC4 43«8 1.5 cal Ryaol. Extremely flammable. SPI Classificati SPI 2 on SBA-7 Perrlc Chloride (1) 220 Lb 100 Lbn Manufacturer: Hallinckrodt. corrost Container ve MATERIALS INVENTORY Item Type and Ho. Estimated No. Item Of Containers ~0uantUr Comment-., 8BA-8 Press Bump Contains approx. 18" of oil and debris. . 8DA-9 Acetone (1) 5 Gal can 2 Gal Ashland Chemical. Flammable Liquid. BOILER ROOM 2 BR2-1 Salrset Bonding (1) 50 Lb can Mortar 25 Lb A.P. Green Refractories BR2-2 Hast* Oil (1) 5 Gal Can 1 Gal Appears to be heavy gear oil. BR2-3 Boiler Boiler is Insulated. Appears to be fiberglass. LOADING DOCK LD-r Unknown (23) 55 Gal 80 Gal Drums may contain waste oil. FUEL STORAGB P8-1 Fuel Storage (3) 11,000 Gal Tanks probably contain "bottoms" P8-2 Unknown (1) 5 Gal can May be fuel oil. APPENDIX C Appendix C Table of Contents BNI Photograph No. 139-129-22, dated August 28, 1995, Building Demolition C-2 BNI Photograph No. 139-134-02, dated September 28, 1995, Building Demolition, Wood Processing C-3 BNI Site Drawing No. 139-DD564-F01 C-4 BNI Photograph No. 139-143-05, dated April 25, 1996, Suspected Uranium Oxide from Zone 19B1 C-5 SAIC Modeling Diagram of July 1997, CISS U238 > 35 pCi/g Isoshells C-6 SAIC Modeling Diagram of July 1997, CISS U238 > 100 pCi/g Isoshells C-7 SAIC Modeling Diagram of July 1997, CISS Th232 > 15 pCi/g C-8 SAIC Modeling Diagram of July 1997, CISS Pb > 500 mg/kg Isoshells C-9 Photograph dated July 1, 1997, Waste Storage Area East Parking Lot C-10 Photograph dated July 1, 1997, Empty Used Drums Along Southern Site Boundary C-l 1 JBNI Photograph No. 139-129-22 dated August 28, 1995 Building Demolition C-2 • • ^; BNI Photograph No. 139-134-02 dated September 28, 1995, Building Demolition, Wood Processing C-3 E900 ass Gnu £1000 El 200 0 60 120 180 l'*60* s A A A A REVISED « NOrtO AND RE-ISSUED FOR BID A ISttK DESCOIPTIOW B SCilE |" =50' U.S. DEPARTMENT OF ENERGY FORMERLY UTILIZED SITES REMEDIAL ACTION PROGRAM BECHTEL NATIONAL INC. OAK RIDGE, TENNESSEE COLONIE INTERIM STORAGE SITE SITE REMEDIATION BECHTEL JOB NO.SIT E ANDOED CONTRACVICINITT NOY. PLAN 1450' A JITION BNI Drawing No. 139-DD564-F01 C-4 2 SIZI-. L" + NOTES . REMEDIATION WORK SHALL BE PERFORMED IN ACCORDANCE WITH SC 564. 2. ALL QUANTITIES ARE ESTIMATED AND SHALL BE VERIFIED BY THE SUBCONTRACTOR AS HECESSARY. 3. EMERGENCY ACCESS AND EGRESS ARE SHOWN ON DRAWING I39-DO0KK07. THIS DRAWING IS POS7E0 ON SITE. SUB- CONTRACTOR SHALL NOT BLOCK THESE ROADWAYS AT ANY TIME. i. FLOOR SLAB DETAILS SHOWN ON DRAWING 133-OO000 C42 ARE ASSUMED. THE SUBCONTRACTOR SHALL VERIFY THE ACTUAL CONFIGURATION OF SLAB AND FOUNDATIONS AS NECESSARY. 5. GROUNDWATER MONITORING WELLS SHALL BE PROTECTED PRIOR TO START OF EXCAVATION. 6. INSTALL AND MAINTAIN SILT FENCE AND CATCH BASIN INLET PROTECTION IN ACCORDANCE WITH DRAWING 1J9DDW0-Ct2. THE SUBCONTRACTOR MAY SUBMIT ALTERNATE DETAILS TO BECHTEL FOR REVIEW AMD APPROVAL. 7. POST SIGNS 6.12, AND 22. ON THE SECURITY FENCE AND SIGNS 1,2, 3, AND 4 ON THE GATE NOTED, IN ACCORDAHCE WITH DRAWING I9I-DOOOO-C06. REFERENCE DRAWINGS EMERGENCY EOUIPMENT LOCATION PLAN I39-00000-C0T gUILolNA 61SHANILMHT. I39000IKJ-CI2 • niljUHPUI WQ.KIilLS_—. Mi REMEDIAUOH. FLOOR SLAB AND 133DD000-C42 LOADING DOCK REMOVAL, OVERHEAD CABLE ROUIt I39-0D0O0EDI ELECTRICAL LAYOUT, SINGLE LINE ANO OIACRAMS I39-DO000-E02 EXAMPLE SIGNS FOR FUSRAP SITES I91-DD00JC06 LEGEND — 1 1 ' 1 RAILROAD ^^™^*^^™ • W PROPERTY BOUNDARY • EXISTING FENCE ——— PROPOSED SECURITY FEKCE AREA DESIGNATED FOR PLACEMENT OF MATERIALS CONTAINING URANIUM BET«EN 35 AND 100 pCi/g MIS NOT IN SCOPE SV SEA-VAN ASPHALT CONCRETE A STOCKPILE JIA GHAS5 OR OTHER GROUND VEGETATION » EXISTING POWER POLE • PROPOSED POWER POLE -an- EXISTING OVERHEAD POWER LINE • OH PROPOSED OVERHEAD POWER LINE 0 60 120 ISO I'-SO" ftEY|^FI> »S Nl!(n AH& RF r.CIKO F nn PIP l jiiIFo FOB nin JFM Art rau wsi run U.S. DEPARTMENT OF ENERGY FORMERLY UTILIZED SITES REMEDIAL ACTION PROGRAM BECHTEL NATIONAL INC. M RiDCE, TENNESSEE COLONIE INTERIM STORAGE SITE SITE REMEDIATION SITE AND VICINITY PLAN BECHTEL JOB NO. ME CONTRACT HO. FILENAME 14501 DE-AC05-9I0R2I949 D564FQ1.DGN DRt»INC HO. I39-DD564-F01 BNl Photograph No. 139-143-05 dated April 25,1996 Suspected Uranium Oxide, Zone 19B1 C-5 CISS Th232 > 15 pCi/g (north at bottom of figure) •~-/ ^_ ^~ Z exaggeration: 10.0 \ \ <> • * -»" • * t / • • ' • + • ".-" m § 1 m 0 m * m 1 • m m • \ £b •' s D n n CISS Pb >500 mg/kg Isoshells (north at bottom of figure) "> I Waste Storage Area East Parking Lot dated July 1,1997 C-10 Empty Used Drums Along Southern Site Boundary dated July 1,1997 C-ll