PITTCON Conference and Expo 2010
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PITTCON Conference and Expo 2010 Abstracts Orlando, Florida, USA 28 February - 5 March 2010 Index ISBN: 978-1-63439-018-7 4/4 Printed from e-media with permission by: Curran Associates, Inc. 57 Morehouse Lane Red Hook, NY 12571 Some format issues inherent in the e-media version may also appear in this print version. Copyright© (2010) by the Pittsburgh Conference All rights reserved. Printed by Curran Associates, Inc. (2014) For permission requests, please contact the Pittsburgh Conference at the address below. Pittsburgh Conference 300 Penn Center Boulevard Suite 332 Pittsburgh, PA 15235-5503 USA Phone: (412) 825-3220 (800) 825-3221 Fax: (412) 825-3224 [email protected] Additional copies of this publication are available from: Curran Associates, Inc. 57 Morehouse Lane Red Hook, NY 12571 USA Phone: 845-758-0400 Fax: 845-758-2634 Email: [email protected] Web: www.proceedings.com Technical Program SUNDAY, FEBRUARY 28, 2010 AFTERNOON AWARD Session 10 Pittcon Heritage Award and Plenary Speaker Sunday Afternoon, Room W320, Chapin Theater 4:30 Presentation of the 2010 Pittcon Heritage Award to Walter G Jennings, University of California at Davis, by Annette S Wilson, 2010 Pittcon President Immediately followed by Plenary Lecture - Alan G Marshall, Florida State University - The Role of High-End Instrumentation SYMPOSIUM Session 20 ACS Division of Analytical Chemistry New Frontiers in Mass Spectrometric Analysis of Proteins - arranged by Heather Desaire, Kansas University Sunday Afternoon, Room 300 Heather Desaire, Kansas University, Presiding 1:00 Introductory Remarks - Heather Desaire 1:05 (20-1) Structural Characterization of Pre-Amyloid Protein Oligomers Using Covalent Labeling and Mass Spectrometry RICHARD W VACHET, University of Massachusetts, Amherst, Vanessa L Mendoza, Shaynah Browne 1:40 (20-2) Developing Mass Spectrometry-based Tools for Biomarker Discovery in Neurodegenerative Diseases LINGJUN LI, University of Wisconsin, Xin Wei, Robert Cunningham, Paige Jany, Feng Xiang, Allen Herbst, Albee Messing, Judd Aiken 2:15 (20-3) High-Throughput Pipeline for Discovery-to-Targeted Analysis of Topology and Function in Integral Membrane Proteins CHRISTINE C WU, University of Colorado School of Medicine 2:50 (20-4) Understanding and Controlling Gas-phase Ion Chemistry to Improve the Analytical Capabilities of Biological Mass Spectrometry for Phosphoproteome Analysis GAVIN E REID, Michigan State University 3:25 (20-5) Emerging Strategies for Facilitating Glycoprotein Analysis HEATHER DESAIRE, University of Kansas SYMPOSIUM Session 30 Advances in Hand-portable Ion Mobility and Ion Trap Chemical Analyzers - arranged by Milton L Lee, Brigham Young University and Herbert H Hill, Washington State University Sunday Afternoon, Room 311A Milton L Lee, Brigham Young University, Presiding 1:00 Introductory Remarks - Milton L Lee 1:05 (30-1) Microfabricated Planar Electrode Ion Traps: Combining Accuracy with Simplicity for Miniaturization DANIEL E AUSTIN, Brigham Young University 1:40 (30-2) Ion Preparation before Differential Mobility Spectrometry (DMS) Including DMS/DMS Analyzers GARY ALAN EICEMAN, New Mexico State University 2:15 (30-3) Quantitative Detection in the Field Using Hand-portable GC-MS EDGAR D LEE, Torion Technologies Inc., Milton L Lee, Douglas W Later, Joseph L Oliphant, Carmela R Jackson LePage, Philip A Smith, Charles S Sadowski, Tiffany C Wirth 2:50 (30-4) Portable Mass Spectrometers vs. Portable Mass Spectrometry Analysis Laboratories ZHENG OUYANG, Purdue University, R Graham Cooks, He Wang, Jiangjiang Liu, Nicolas E Manicke, Guangming Huang 3:25 (30-5) Multidimensional Ion Mobility Spectrometer for High Fidelity Chemical Identification HERBERT H HILL, Washington State University SYMPOSIUM Session 40 Analytical Chemistry for the Study of Nanotoxicity - arranged by Wenwan Zhong, University of California, Riverside Sunday Afternoon, Room 206A Wenwan Zhong, University of California, Riverside, Presiding 1:00 Introductory Remarks - Wenwan Zhong 1:05 (40-1) A Role for Particle Surface Effects in TiO2 and Quartz-related Nanoparticle Pulmonary Toxicity DAVID B WARHEIT, DuPont Haskell Global Centers 1:40 (40-2) Systems-Level Approaches to Understanding Nanoparticle Biocompatibility BRIAN D THRALL, Pacific Northwest National Laboratory 2:15 (40-3) Nanoparticle-plasma Interactions: A Basis for Nanosafety Assessment KENNETH ADRIAN DAWSON, University College Dublin 2:50 (40-4) The Study of Protein-nanomaterial Interaction with Free-solution Separation Techniques WENWAN ZHONG, University of California, Riverside, Ni Li, Lei Ren 3:25 (40-5) Gold Nanorod Uptake by Cultured Cells and the Mechanisms of Cytotoxicity at High Doses CATHERINE J MURPHY, University of Illinois SYMPOSIUM Session 50 Emerging Materials in Separation Science - arranged by Matthew R Linford, Brigham Young University and Abdul Malik, University of South Florida Sunday Afternoon, Room 311B Matthew R Linford, Brigham Young University, Presiding 1:00 Introductory Remarks - Matthew R Linford 1:05 (50-1) Hyper-crosslinked Silica Phases: Emerging Materials in Separation Science PETER W CARR, University of Minnesota, Yu Zhang, Lianjia Ma, Hao Luo 1:40 (50-2) Titania- and Germania-based Hybrid Organic-Inorganic Sol-Gel Coatings and Monolithic Beds for Ultrahigh Stability in Separation Science ABDUL MALIK, University of South Florida, Scott S Segro, Erica B Turner, Minhphuong Tran, Chemgliang Jiang, Abdullah Alhendal 2:15 (50-3) Porous Graphitic Carbon: A Solution for Difficult LC Separations HARALD RITCHIE, Thermo Fisher Scientific 2:50 (50-4) Functionalized Diamond as a Stationary Phase in Chromatography MATTHEW R LINFORD, Brigham Young University, Li Yang, Gaurav Saini, Wiest Landon, David S Jensen, Andrew Dadson, Michael A Vail 3:25 (50-5) Micro and Nanofabrication of Chromatography Media ROBERT C DAVIS, Brigham Young University, Vanfleet R Richard , Matthew R Linford SYMPOSIUM Session 60 Sol-Gel Materials for Chemical Analysis - arranged by Maryanne M Collinson, Virginia Commonwealth University Sunday Afternoon, Room 205B Maryanne M Collinson, Virginia Commonwealth University, Presiding 1:00 Introductory Remarks - Maryanne M Collinson 1:05 (60-1) High Surface Area Materials for Chemical Analysis MARYANNE M COLLINSON, Virginia Commonwealth University 1:40 (60-2) Sol-Gel-Derived Mesoporous Silica Materials in Electroanalysis ALAIN WALCARIUS, LCPME-CNRS 2:15 (60-3) Sol-Gel Derived Thin Films for Spectroelectrochemical Sensors WILLIAM R HEINEMAN, University of Cincinnati, Carol J Seliskar, John A Lynch, Ronnee N Andrews 2:50 (60-4) Nanocrystallite-xerogel Hybrids for Optical Sensing FRANK V BRIGHT, University at Buffalo, SUNY 3:25 (60-5) Sepsis Monitoring via Sol-Gel Derived Chemical Sensors MARK H SCHOENFISCH, University of North Carolina, Chapel Hill, Benjamin J Privett SYMPOSIUM Session 70 Ultrasmall and Ultrasensitive Chemical Imaging of Cells and Cell Networks "WEBCAST"- arranged by Andrew G Ewing, Penn State University Sunday Afternoon, Room 205C Andrew G Ewing, Penn State University, Presiding 1:00 Introductory Remarks - Andrew G Ewing 1:05 (70-1) Probing Transport of Catecholamines in the Adrenal Gland with Microelectrodes MARK WIGHTMAN, University of North Carolina, Chapel Hill 1:40 (70-2) Nanopore-based Artificial Ion-Channel Sensors for Monitoring Cell Secretion BO ZHANG, University of Washington, Jin Chen 2:15 (70-3) Optodes: A New Approach to Imaging Chemicals at Single Cells in a Network ANDREW G EWING, Penn State University/University of Gothenburg, Niklas Strömberg, Maja Puchades 2:50 (70-4) Tip-Enhanced Raman Spectroscopy Bio-spectroscopy Below 20-Nanometer Resolution VOLKER DECKERT, IPHT 3:25 (70-5) Mass Spectrometric Profiling and Imaging Approaches for Understanding the Neuronal Metabolome JONATHAN V SWEEDLER, University of Illinois WORKSHOP Session 80 Analytical Challenges Facing the U.S. Department of Energy Office of Environmental Management- arranged by Jacob Venzie, Savannah River National Laboratory Sunday Afternoon, Room 311D Jacob Venzie, Savannah River National Laboratory, Presiding 1:00 Introductory Remarks - Jacob Venzie 1:05 (80-1) An Overview of DOE-EM Technology and Engineering SHARON MARRA, Savannah River National Laboratory 1:40 (80-2) Analytical Methods for Monitoring Vitrification of Hanford Radioactive Waste ARUNA V ARAKALI, URS-Washington Division, Kenneth R Wells, Thomas A Lane, Jinesh C Jain, Douglas M Perkins 2:15 Recess 2:30 (80-3) Analytical Challenges in the Department of Energy (DOE) Deactivation and Decommissioning Program JOHN GLADDEN, Savannah River National Laboratory, Andrew Szilagyi 3:05 (80-4) Unique Requirements for Analytical Tools in the EM Complex JACOB VENZIE, Savannah River National Laboratory 3:40 Discussion/Wrap Up ORGANIZED CONTRIBUTED SESSION Session 90 SEAC Organized Session - Electrochemistry and Materials - arranged by Richard A Durst, Cornell University Sunday Afternoon, Room 311C Anna Brajter-Toth, University of Florida, Presiding 1:00 (90-1) Treating Carbon Nanotube Arrays to Increase the Oxygen Species for Further Functionalization AMOS DOEPKE, University of Cincinnati, Changseok Han, William R Heineman 1:20 (90-2) Scanning Electrochemical Microscopy of Individual Single-Walled Carbon Nanotubes JIYEON KIM, University of Pittsburgh, Shigeru Amemiya 1:40 (90-3) Fourier Transform Voltammetry at Microelectrodes: Principles and Applications ANNA BRAJTER-TOTH, University of Florida, Alan M Bond, Darrell Elton, Chong-Yong Lee 2:00 (90-4) Investigating Surface Transformations Induced by Electrochemical