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Zbornik Radova I Sažetaka Hrvatsko društvo kemijskih inženjera i tehnologa Prehrambeno-tehnološki fakultet Osijek XII. Ružičkini dani Vukovar18. i 19. rujna 2008. Znanost i nove tehnologije u razvoju gospodarstva ZBORNIK RADOVA I SAŽETAKA . Osijek, 2008. ZBORNIK RADOVA I SAŽETAKA XII. Ružičkini dani Znanost i nove tehnologije u razvoju gospodarstva Izdavači: Hrvatsko društvo kemijskih inženjera i tehnologa (HDKI) Prehrambeno-tehnološki fakultet u Osijeku Glavni urednik: Srećko Tomas Izvršni urednik: Damir Hasenay Tehničke urednice: Sanda Hasenay i Maja Blažević Tisak i uvez: TIPO Osijek ISBN 978-953-6894-35-2 (HDKI) ISBN 978-953-7005-17-7 (PTF) CIP zapis dostupan u računalnom katalogu Gradske i sveučilišne knjižnice Osijek pod brojem 120411075 Počasni odbor Zdenka Buljan, dipl. politolog prof. dr. sc. Ivan Butula Petar Čobanković, dipl. ing. Mirko Ćavara, dipl. oec. Božo Galić, dipl. ing. akademik Marin Hraste prof. dr. sc. Zvonimir Janović Vlado Jerbić, dipl. ing. prof. dr. sc. dr. h. c. Gordana Kralik mr.sc. Božidar Pankretić akademkinja Vlasta Piližota prof. dr. sc. Antun Pintarić Damir Polančec, dipl.ing. prof. dr. sc. Dragan Primorac dr. sc. Mladen Proštenik akademik Nenad Trinajstić Znanstveno-organizacijski odbor prof. dr. sc. Srećko Tomas - predsjednik dr. sc. Ante Jukić, docent - dopredsjednik mr. sc. Filip Kljajić - dopredsjednik dr. sc. Damir Hasenay, docent - tajnik (Osijek) mr. sc. Ivan Hubalek - tajnik (Vukovar) prof. dr. sc. Milena L. Mandić - član Ružica Marić, prof. - član Ana Mrgan, dipl. ing. - član prof. dr. sc. Milan Sak-Bosnar - član dr. sc. Danko Škare, viši znanstveni suradnik - član prof. dr. sc. Drago Šubarić - član Darko Vrbešić, dipl. ing. – član pokrovitelj: HAZU Razred za matematičke, fizičke i kemijske znanosti uz potporu: Ministarstvo znanosti, obrazovanja i športa Ministarstvo gospodarstva, rada i poduzetništva Ministarstvo poljoprivrede, ribarstva i ruralnog razvoja Ministarstvo regionalnog razvoja, šumarstva i vodnog gospodarstva Sveučilište J.J. Strossmayera u Osijeku Znanost i nove tehnologije u razvoju gospodarstva _________________________________________________ SADRŽAJ _______________________________________________________ XII. Ružičkini dani – Vukovar – 18. i 19. rujna 2008. Znanost i nove tehnologije u razvoju gospodarstva SADRŽAJ _________________________________________________ Srećko Tomas XII. RUŽIČKINI DANI: uvodna riječ……………………………………………... 1 Ivan Hubalek JEDANAEST ″RUŽIČKINIH DANA″………………………………………… 3 Filip Kljajić VLADIMIR PRELOG I RUŽIČKINI DANI…………………………………… 19 PLENARNA PREDAVANJA P - 1 Hartwig Höcker: Ciklički i makrociklički organski spojevi – pregledni rad posvećen Lavoslavu Ružički = Cyclics and macrocyclics – a personal review in honor of professor Leopold Ruzicka…..……..... 24 P – 2 Jasenka Piljac Žegarac, Sanja Martinez, Lidija Valek, Tamara Stipčević, Ana Belščak i Dunja Šamec: Ukupni sadržaj fenola i antioksidacijski kapacitet hrvatskih prehrambenih proizvoda = Total phenol content and antioxidant capacity of croatian food products – an overview………………………………………...……………………… 39 P – 3 Valery P. Kukhar: Biomasa – obnovljiva sirovina za organske kemikalije – ″bijela kemija″ = Biomass – renewable feedstock for organic chemicals – ″white chemistry″……………………………..…. 52 P – 4 Davor Kovačević: Nastajanje, svojstva i primjena polielektrolitnih višeslojeva = Formation, properties and application of polyelectrolyte multilayers ……………………………………………………….…….. 61 P – 5 Djuro Josic i Spomenka Kovač: Proteomika i genomika u biotehnologiji = Proteomics and genomics in biotechnology……...…... 65 P – 6 Srećko Tomas, Mate Bilić, Mirela Planinić, Ana Bucić-Kojić i Darko Velić: Održivost proizvodnje drvenog ugljena u klasičnim vodoravnim retortama = Sustainability of destructive distillation of wood in classic horizontal retorts……………………………………… 66 P – 7 Jasmin Hirschmann, Martina Marchetti, Hongjuan Dong, Wolfgang Winkler, Christian Kubicek i Günter Allmaier: Identifikacija gljivica vakuumskom maldi tof masenom spektrometrijom = Intact spore mass spectrometry for fungus identification by vacuum maldi time-of-flight mass spectrometry……..…. 78 XII. Ružičkini dani – Vukovar – 18. i 19. rujna 2008. Znanost i nove tehnologije u razvoju gospodarstva SADRŽAJ _________________________________________________ P – 8 Marko Rogošić: Razvoj polimernih nanokompozita na osnovi slojevitih hidroksida = Development of polymeric nanocomposites based on layered hydroxids……………………………………..……… 79 Sekcija 1: KEMIJSKA ANALIZA I SINTEZA S 1- 1 Marija Kaštelan-Macan, Vladimir Grdinić i Njegomir Radić: Hrvatsko nazivlje u analitičkoj kemiji = Croatian nomenclature in analytical chemistry …………………………………………..…… 84 S 1- 2 Irena Sović, Saša Kostel, Tihomir Pospišil i Grace Karminski- Zamola: Amidni derivati benzimidazola = Amide derivates of benzimidazole ………...………………………………..………….. 85 S 1- 3 Marijana Hranjec, Borka Lučić, Nataša Perin i Grace Karminski-Zamola: Ciklički derivati benzimidazola i imidazo[4,5- b]piridina = Cyclic derivates of venzimidazoles and imidazo[4,5- 86 b]pyridines…………………………………………………………. S 1- 4 Zorica Hodžić, Majda Srabović i Melita Joldić: Enzimska hidroliza škroba u procesu ekstrakcije smjese žitarica = Enzimic hydrolysis of starch in extraction process of grains mixtures……………………………………….......……………….. 87 S 1- 5 Maja Aleksić i Grace Karminski-Zamola: Novi imidazolinski derivati benzo[b]tieno[2,3-c]kinolona = Novel imidazolinyl derivates of benzo[b]thieno[2,3-c]quinolones……….……………. 88 S 1- 6 Pero Dabić, Petar Krolo, Juraj Šipušić i Neven Ukrainczyk: Ispitivanje žbuke hrama s arheološkog lokaliteta Narona-Vid = Examination of temples wall mortar from archaological site Narona Vid……………………………………………..…………………... 89 S 1- 7 Ranka Kubiček, Jozo Budimir, Mersiha Suljkanović i Jasmin Suljagić: Primjena nekih tenzida u spektrometrijskom određivanju CD (II)-ditizonata = Application some surfactants in spectrophotometric determination Cd (II)- dithizonate……………. 90 S 1- 8 Nikola Basarić, Margareta Horvat, Oliver Franković, Kata Mlinarić-Majerski, Marko Marjanović, Marijeta Kralj, Željka Mačak Šafranko i Zorka Mikloška: Sinteza i ispitivanje antitumorskog i antivirusnog djelovanja adamantanskih ftalimida = Synthesis, anticancer and antivirus investigation of adamantane phthalimides…………………………………..………………......... 91 XII. Ružičkini dani – Vukovar – 18. i 19. rujna 2008. Znanost i nove tehnologije u razvoju gospodarstva SADRŽAJ _________________________________________________ S 1- 9 Danijela Ašperger, Sandra Babić, Dijana Drljača, Marina Mrđa, Dragana Mutavdžić, Alka J. M. Horvat i Marija Kaštelan-Macan: Ultrazvučna ekstrakcija epikatehina i procijanidina B2 iz čokolade = Ultrasonic solvent exstraction of epicatechin and procyanidin B2 from chocholate……………….… 92 S1- 10 Maja Molnar, Milan Čačić, Mladen Trkovnik i Tatjana Jakšić: Sinteza novih čalkona na bazi 7-hidroksi-4-metil-2-okso-2H- kromena = Synthesis of novel chalcones of the basic 7-hydroxy-4- methyl-2-oxo-2H-chromen……………………………………….… 93 S1- 11 Milan Čačić, Maja Molnar, Mladen Trkovnik i Ivana Baračkov: Sinteza nekih 4-tiazolidinona na bazi 7-hidroksi-2-okso- 2H-kromena = Synthesis of some 4-thiazolidinones on the basis 7- hydroxy-2-oxo-2H-chromen…………………………………...…… 94 S1- 12 Bojan Šarkanj, Milan Čačić, Maja Molnar i Tomislav Klapec: Sinteza i dizajn novih tiadiazina s kumarinskom jezgrom = Synthesis and design of new thiadiazines with coumarin nucleus…………………………………………………….……….... 95 S1- 13 Iva Nižić, Ivan Radoš, Petra Burić, Marina Cvjetko i Jasna Vorkapić-Furač: Priprava supstituiranih imidazolijevih i Piridinijevih kvaternih soli, potencijalnih ionskih tekućina = Synthesis of subsittuted imidazolium and pyridinium Quaternary salts, potential ionic liquids…………………………….………….. 96 S1- 14 Vlasta Vojković i Astrid Gojmerac Ivšić: Ekstrakcija i spektrofotometrijsko proučavanje tantalova(v) tiocianatnog kompleksa = Extraction and spectrophotometric study of tantalum(v) thiocyanate complex………….………………………... 97 S1- 15 Midhat Jašić, Ružica Mertz i Predrag Kvolik: Značajke pH metara i utjecaj na mjernu nesigurnost = Design characteristic of pH meters and it's influence on measuring uncertainity…………........... 98 S1- 16 Štefica Podolski, Branka Špehar, Dunja Šeremešić i Roberta Gorup: Određivanje klora u nafti i naftnim proizvodima valno disperzivnom rendgenskom fluorescentnom spektrometrijom = Determination of chlorine content in petroleum and petroleum products - wavelength-disperzive x-ray fluorescence spectrometry... 99 XII. Ružičkini dani – Vukovar – 18. i 19. rujna 2008. Znanost i nove tehnologije u razvoju gospodarstva SADRŽAJ _________________________________________________ S1- 17 Dubravka Madunić-Čačić, Milan Sak-Bosnar, Mirela Samardžić i Zorana Grabarić: Potenciometrijsko određivanje anionskih tenzida u industrijskim efluentima koristeći 1,3-didecil-2- metil-imidazolijev-tetrafenilborat kao senzorski materijal = Potentiometric determination of anionic surfactants in industrial effluents using 1, 3-didecyl-2-methyl-imidazolium-tetraphenylborate as sensing material………………………………………………..……. 100 S1- 18 Milan Sak-Bosnar, Dubravka Madunić-Čačić, Nikola Sakač, Olivera Galović, Mirela Samardžić i Zorana Grabarić: Modeliranje potenciometrijske titracije pseudoionskog kompleksa tritona X-100 i barija s natrijevim tetrafenilboratom koristeći novi potenciometrijski senzor = Modelling of potentiometric titration of pseudoionic complex triton x-100 and barium with sodium tetraphenylborate using a new potentiometric sensor………………. 101 S1- 19 Natalija Velić, Mirela Samardžić, Olivera Galović,
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