Trace Metal Analysis by Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry and X-Ray K-Edge Densitometry
Total Page:16
File Type:pdf, Size:1020Kb
Load more
Recommended publications
-
Discussion of the Surface Science of Quasicrystals Patricia Thiel
Discussion of the Surface Science of Quasicrystals Patricia Thiel To cite this version: Patricia Thiel. Discussion of the Surface Science of Quasicrystals. Philosophical Magazine, Taylor & Francis, 2008, 88 (13-15), pp.2123-2129. 10.1080/14786430802186973. hal-00513904 HAL Id: hal-00513904 https://hal.archives-ouvertes.fr/hal-00513904 Submitted on 1 Sep 2010 HAL is a multi-disciplinary open access L’archive ouverte pluridisciplinaire HAL, est archive for the deposit and dissemination of sci- destinée au dépôt et à la diffusion de documents entific research documents, whether they are pub- scientifiques de niveau recherche, publiés ou non, lished or not. The documents may come from émanant des établissements d’enseignement et de teaching and research institutions in France or recherche français ou étrangers, des laboratoires abroad, or from public or private research centers. publics ou privés. Philosophical Magazine & Philosophical Magazine Letters For Peer Review Only Discussion of the Surface Science of Quasicrystals Journal: Philosophical Magazine & Philosophical Magazine Letters Manuscript ID: TPHM-08-Mar-0086.R1 Journal Selection: Philosophical Magazine Date Submitted by the 30-Apr-2008 Author: Complete List of Authors: Thiel, Patricia; Iowa State University, Department of Chemistry Keywords: quasicrystals, surface physics Keywords (user supplied): quasicrystals, surface physics http://mc.manuscriptcentral.com/pm-pml Page 1 of 15 Philosophical Magazine & Philosophical Magazine Letters 1 2 3 Discussion of the Surface Science of Quasicrystals 4 5 6 7 8 Patricia A. Thiel 9 10 11 Ames Laboratory and Department of Chemistry, Iowa State University 12 13 Ames, IA 50011 USA 14 For Peer Review Only 15 16 17 18 19 20 Abstract. -
FY20 National Laser Users' Facility Program
FY20 NATIONAL LASER USERS’ FACILITY PROGRAM FY20 National Laser Users’ Facility Program M. S. Wei Laboratory for Laser Energetics, University of Rochester During FY19, the National Nuclear Security Administration (NNSA) and Office of Science jointly completed a funding opportu- nity announcement (FOA), review, and selection process for National Laser Users’ Facility (NLUF) experiments to be conducted at the Omega Facility during FY20 and FY21. After peer review by an independent proposal review committee for scientific and technical merit and the feasibility review by the Omega Facility team, NNSA selected 11 proposals for funding and Omega shot allocation with a total of 22.5 and 23.5 shot days for experiments in FY20 and FY21, respectively. During the first half of the FY20, LLE completed a one-time solicitation, review, and selection process for Academic and Industrial Basic Science (AIBS) experiments to utilize the remaining NLUF shot allocation in FY20–FY21. Ten new projects were selected for AIBS shot alloca- tion (a total of 11 and 10 shot days) for experiments staring in Q3FY20 and throughout FY21. FY20 was the first of a two-year period of performance for these 21 NLUF including AIBS projects (Table I). Fifteen NLUF and AIBS projects obtained a total of 232 target shots during FY20, which are summarized in this section. A critical part of the NNSA-supported NLUF program and the DOE Office of Fusion Energy Sciences (FES)-supported Laser- NetUS program is the education and training of graduate students in high-energy-density (HED) physics. In addition, graduate students can also access the Omega Laser Facility to conduct their theses research through collaborations with national labora- tories and LLE. -
The Avs 67Th International Symposium & Exhibition
THE AVS 67TH INTERNATIONAL SYMPOSIUM & EXHIBITION On behalf of the AVS, we invite you to submit an abstract to the AVS 67th International Symposium and Exhibition, which will be held October 24 – 29, 2021 in Charlotte, North Carolina. The AVS Symposium is the premier forum for the presentation and discussion of the science and technology of materials, interfaces, and processing. This year, the Symposium’s theme is “Advances in Interfacial Science for Energy and The Environment.” The challenges facing the development and implementation of new energy sources and solutions to outstanding environmental problems have never been more important. The AVS 67th Annual Symposium will highlight the emergent science and technology of materials and techniques for environmental applications and energy transformation. AVS 67 will be an ideal forum for presentation and discussion of your latest results and will provide many opportunities to connect with other engineers and scientists. A sampling of sessions that encompass this theme include: • Electronic and Photonic Devices for Energy Conversion and Storage • Bioenergy and Biomass Conversion • 2D Materials for Electrochemical, Energy, and Environmental Applications • Structural Characterization of Energy Materials • Analysis of Surfaces and Interfaces Related to Energy and the Environment • Astrochemistry and Surfaces for Space and Extreme Environments • Vacuum Technology for Fusion Research • Hybrid Nanomaterials Based on Biologically-Inspired Approaches • Advances in Heterogeneous Electrocatalysis • Atomic Layer Processing: Integration of Deposition and Etching for Advanced Material Processing • Environmental Interfaces • Catalysis at the Metal Oxide Interface • Pushing the Boundaries of Energy Transfer in Materials • MEMS Technology for Energy and Environment • Energy Efficient Nanoelectronics • Plasma-Engineered Materials and Interfaces for the Environment • Electronic Interfaces and Contacts In addition, we will feature programming on innovative topical areas. -
MRS Materials Connections
RESEARCH/RESEARCHERS ness of the TeSW-prepared p-Si is very thin ing orientation. Some recent studies have such efforts for PZN-PT. In the August and the rms roughness is only 1.6 nm. reported frictional differences, or aniso- issue of the Journal of the American Ceramic The researchers also performed a con- tropy, less than a factor of 3 for incom- Society (p. 2310; DOI: 10.111/j.1551- trolled experiment of p-Si formation using mensurate crystal surfaces when there 2916.2005.00391.x), G. Deng and col- NaOH etchant at various pH levels, but were periodicity differences. leagues from the Shanghai Institute of they observed no efficient PL emission To measure the frictional effects due to Ceramics, China, have reported their suc- from any of the NaOH-prepared samples. periodicity alone and not to other factors cess in synthesizing pure perovskite The researchers pointed out that the such as chemical differences, the re- ceramics of PZN-PZT, as an alternative to reproducibility appeared to be a problem searchers worked with decagonal quasi- PZN-PT, near their MPB. The researchers for the photoetched p-Si synthesis tech- crystals of an aluminum-nickel-cobalt (Al- have observed much higher piezoelectric nique. They point out that others have Ni-Co) alloy. Stacked planes of Al-Ni-Co and electromechanical coupling coeffi- suggested that the preexisting state of the crystals exhibit both tenfold and twofold cients for their newly synthesized mate- Si surface plays a decisive role in deter- rotational symmetry. By cutting a single rial than those reported earlier. -
A Programmable Mode-Locked Fiber Laser Using Phase-Only Pulse Shaping and the Genetic Algorithm
hv photonics Article A Programmable Mode-Locked Fiber Laser Using Phase-Only Pulse Shaping and the Genetic Algorithm Abdullah S. Karar 1,* , Raymond Ghandour 1 , Ibrahim Mahariq 1 , Shadi A. Alboon 1,2, Issam Maaz 1, Bilel Neji 1 and Julien Moussa H. Barakat 1 1 College of Engineering and Technology, American University of the Middle East, Kuwait; [email protected] (R.G.); [email protected] (I.M.); [email protected] (S.A.A.); [email protected] (I.M.); [email protected] (B.N.); [email protected] (J.M.H.B.) 2 Electronics Engineering Department, Hijjawi Faculty for Engineering Technology, Yarmouk University, Irbid 21163, Jordan * Correspondence: [email protected] Received: 24 July 2020; Accepted: 2 September 2020; Published: 4 September 2020 Abstract: A novel, programmable, mode-locked fiber laser design is presented and numerically demonstrated. The laser programmability is enabled by an intracavity optical phase-only pulse shaper, which utilizes the same linearly chirped fiber Bragg grating (LC-FBG) from its two opposite ends to perform real-time optical Fourier transformation. A binary bit-pattern generator (BPG) operating at 20-Gb/s and producing a periodic sequence of 32 bits every 1.6 ns, is subsequently used to drive an optical phase modulator inside the laser cavity. Simulation results indicate stable programmable intensity profiles for each optimized user defined 32 code words. The laser operated in the self-similar mode-locking regime, enabling wave-breaking free operation. The programmable 32 bit code word targeting a specific intensity profile was determined using 100 generations of the genetic algorithm. -
Minutes for the Basic Energy Sciences Advisory Committee Meeting July 29-30, 1998, Gaithersburg Hilton Hotel, Gaithersburg, Maryland
Minutes for the Basic Energy Sciences Advisory Committee Meeting July 29-30, 1998, Gaithersburg Hilton Hotel, Gaithersburg, Maryland BESAC members present: Boris Batterman Thomas Russell Jack Crow Zhi-Xun Shen Marye Anne Fox (Vice Chair) Sunil Sinha Jan Herbst Richard Smalley Linda Horton David Tirrell Franklin Orr Patricia Thiel Geraldine Richmond (Chair) BESAC members absent: Barbara Garrison Carolyn Meyers Robert Horsch Edel Wasserman Stephen Leone Conrad Williams Marsha Lester Also present: Jim Decker, Deputy Director, ER (Wednesday only) Patricia Dehmer, Associate Director, ER, OBES Martha Krebs, Director, ER (Wednesday afternoon only) Iran Thomas, Deputy Associate Director, ER, OBES and Director, Division of Materials Sciences, OBES July 29, 1998 Chair Geraldine Richmond opened the meeting at 8:30 a.m. She had each committee member introduce himself or herself. She then introduced Patricia Dehmer to provide an overview of the Department of Energy (DOE) and of the Office of Basic Energy Sciences (BES). In her preliminary remarks, Dehmer welcomed the members to the meeting and stressed the importance of this advisory committee, BESAC, pointing out that it produced outcomes as well as outputs. One outcome has been the Birgeneau Report that reviewed the major light-source initiatives; it will be the force in determining funding for those sources, and it has already become part of the vernacular on Capitol Hill. An output has been the analysis of the shutdown of the High-Flux Beam Reactor (HFBR). She pointed out that BESAC already has three charges for this year: to review the High Flux Isotope Reactor (HFIR), to conduct a workshop on fourth-generation light sources, and to conduct a workshop on complex systems. -
MRI-Guided Laser Ablation Surgery of Hypothalamic Hamartomas
NEUROSURGERY MRI-Guided Laser Ablation Surgery of Hypothalamic Hamartomas HOW DOES THE TEAM DECIDE IF A PATIENT IS A CANDIDATE FOR MRI-GUIDED LASER ABLATION? A careful review of each patient’s medical records is the first step, including MR imaging of the brain and any applicable neurology or neurosurgery records. Patients with Hypothalamic Hamartomas (HH) typically have gelastic seizures, which are characterized by emotionless laughing, although variations including abnormal movements or staring spells are also common. Every patient’s case is handled individually, and it may be necessary for a patient to come to Texas Children’s Hospital for further testing to determine if they are a candidate for MRI-guided laser ablation surgery. WHAT HAPPENS DURING MRI-GUIDED LASER ABLATION SURGERY? After being placed under general anesthesia, a head frame, or a set of markers, is fitted to the patient’s skull. A CT scan is completed to orient the brain to the frame in 3 dimensions. With the help of computer software, a safe pathway that goes through the brain to the HH is calculated for the laser. The neurosurgeon then makes a small incision and drills a small hole through the skull (3.2 mm wide). The laser applicator, a small tube about the width of a strand of spaghetti, is inserted and guided through the brain into the HH. Once the laser applicator is inserted into the brain, the head frame is removed, and the patient is transported to the MRI scanner. After confirming proper placement of the laser applicator and setting safety markers, the surgeon performs a small test firing using the laser. -
Congratulations to the New 25 Year Club Members of 2010
CONGRATULATIONS TO THE NEW 25 YEAR CLUB MEMBERS OF 2010 TWENTY-FIVE YEAR HONOREES The following persons completed 25 years of employment at ISU during the calendar year of 2008. New members being welcomed to this honored organization are: DIVISION OF THE PRESIDENT Cindy Van Loon Human Resource Services DIVISION OF ACADEMIC AFFAIRS COLLEGE OF AGRICULTURE & LIFE SCIENCES Dennis Garvey Animal Science Catherine Good Ag Exp Stn Administration Martha Jeffrey Animal Science Danny Johnson Animal Science Randy Killorn Agronomy Susan Lamont Animal Science Robert Martin Ag Education Sally Medford IA State Research Farms Pamela Mundt Agronomy Donna Nelson Animal Science Jonathan Sandor Agronomy Ann Shuey Animal Science Jeffrey Thorson Animal Science Helene Uhlenhopp Agronomy COLLEGE OF BUSINESS Ronald Ackerman Business Graduate Program Farhad Choobineh Log Operation & Mis Mark Power Finance Jenison Stoehr Log Operations and MIS COLLEGE OF DESIGN Clare Cardinal-Pett Architecture COLLEGE OF ENGINEERING Robert Abendroth Civ/Con/ Env Engineering Linda Edson Chemical & Bio Engineering Jeffrey Eichorn Ind/ Manufacturing Systems Engineering Scott Schlorholtz Materials Science and Engineering Martha Selby Materials Science and Engineering Terry Wipf Civ/Con/Env Eng COLLEGE OF HUMAN SCIENCES Marcia Rosenbusch Curriculum/ Instruction COLLEGE OF LIBERAL ARTS & SCIENCES Barbara Blakely English Michael Duffy Economics Sally Gleason Chemistry Kristy Goodale Mathematics Margaret Graham English J Arne Hallam Economics Paul Hollander Chemistry Margaret Holmgren Philosophy/ -
With Short Pulse • About 7% Coupling Significantly Less Than the Osaka Experiment
Electron/proton generation from solid targets and applications Farhat Beg University of California, San Diego This work was performed under the auspices of the U.S. DOE under contracts No.DE-FG02-05ER54834, DE-FC0204ER54789 and DE-AC52-07NA27344. We greatly acknowledge support of Institute for Laser Science Applications, LLNL. Committee on Atomic, Molecular and Optical Sciences Meeting The National Academy of Sciences Washington DC, April 5, 2011 1 Summary ü Short pulse high intensity laser solid interactions create matter under extreme conditions and generate a variety of energetic particles. ü There are a number of applications from fusion to low energy nuclear reactions. 10 ns ü Fast Ignition Inertial Confinement Fusion is one application that promises high gain fusion. ü Experiments have been encouraging but point towards complex issues than previously anticipated. ü Recent, short pulse high intensity laser matter experiments show that low coupling could be due to: - prepulse - electron source divergence. ü Experiments on fast ignition show proton focusing spot is adequate for FI. However, conversion efficiency has to be increased. 2 Outline § Short Pulse High Intensity Laser Solid Interaction - New Frontiers § Extreme conditions with a short pulse laser § Applications § Fast Ignition - Progress - Current status § Summary Progress in laser technology 10 9 2000 Relativistic ions 8 Nonlinearity of 10 Vacuum ) Multi-GeV elecs. V 7 1990 Fast Ignition e 10 ( e +e- Production y 6 Weapons Physics g 10 Nuclear reactions r e 5 Relativistic -
Chapter 20 SOFT LASER DESORPTION IONIZATION - MALDI, DIOS and NANOSTRUCTURES
Chapter 20 SOFT LASER DESORPTION IONIZATION - MALDI, DIOS AND NANOSTRUCTURES Akos Veites Department of Chemistry, Institute for Proteomics Technology and Applications, The George Washington University, Washington DC 20052 1. INTRODUCTION In 1948, Ame Tiselius won the Nobel Prize in chemistry for the discovery of electrophoresis and its application to analyze large molecules, specifically complex serum proteins. During the following decades, gel electrophoresis and its derivative techniques became a central method for molecular biology. They allowed for the identification of molecular mass with an accuracy of ~1 kDa, i.e., a thousand atomic mass units. Although this method enabled the separation of thousands of proteins from biological samples, the determination of the actual molecular weight, and with it finding the true identity of many substances, remained unachievable. When it came to accurate mass determination of small molecules, mass spectrometry was the method of choice. However, for the accurate mass analysis of large molecules, their low volatility presented a fundamental obstacle. Typically, the larger the molecule, the harder it is to transfer it into the gas phase without degradation. Depositing the energy necessary for volatilization initiates other competing processes that elevate the internal energy of the adsorbate and results in its fragmentation. This competition between evaporation (or desorption) and fragmentation was recognized early on and the method of rapid heating was proposed to minimize the latter (Beuhler, et al., 1974). Lasers with submicrosecond pulse length were appealing tools for rapid heating but the initial results indicated limitations with respect to the ultimate size of the biomolecules (m/z < 1,500) that could 506 Laser Ablation and its Applications be successfully analyzed (Posthumus ,et al., 1978). -
Laser Ablationablation
LaserLaser AblationAblation FundamentalsFundamentals && ApplicationsApplications Samuel S. Mao Department of Mechanical Engineering Advanced Energy Technology Department University of California at Berkeley Lawrence Berkeley National Laboratory March 10, 2005 University of California at Berkeley Q Lawrence Berkeley National Laboratory LaserLaser AblationAblation What is “Laser Ablation”? Mass removal by coupling laser energy to a target material University of California at Berkeley Q Lawrence Berkeley National Laboratory ion lat ab er IsIs itit important?important? las ) Film deposition substrate * oxide/superconductor films material * nanocrystals/nanotubes plume target mass spectrometer ) Materials characterization * semiconductor doping profiling plasma lens * solid state chemical analysis target optical spectrometer ) Micro structuring * direct wave guide writing * 3D micro fabrication microstructure target transparent solid University of California at Berkeley Q Lawrence Berkeley National Laboratory ion lat ab er IsIs itit important?important? las ) Film deposition * oxide/superconductor films * nanocrystals/nanotubes ) Materials characterization * semiconductor doping profiling * solid state chemical analysis 100 µm ) Micro structuring * direct wave guide writing * 3D micro fabrication University of California at Berkeley Q Lawrence Berkeley National Laboratory ion lat ab er DoDo wewe reallyreally understand?understand? las laser beam “Laser ablation … is still largely unexplored at the plasma fundamental level.” J. C. Miller & -
MRI-Guided Laser Ablation Surgery for Epilepsy
MRI-Guided Laser Ablation Surgery for Epilepsy In August 2010, Texas Children’s Hospital became the first hospital in the world to use real-time MRI-guided thermal imaging and laser technology to destroy epilepsy-causing lesions in the brain that are too deep inside the brain to safely access with usual neurosurgical methods. To date, our team has performed more than 100 of these procedures on patients who have traveled to Houston and Texas Children’s from around the globe. This technology has become a standard of care and is now being used in many adult and pediatric centers across the United States. The advantages of the MRI-guided laser surgery procedure include: • A safer, significantly less-invasive alternative to open brain surgery with a craniotomy, which is the traditional technique used for the surgical treatment of epilepsy. • No hair is removed from the patient’s head. • Only a 3 mm opening is needed for the laser. It is closed with a single suture resulting in less scarring and pain for the patient. • A reduced risk of complications and a faster recovery time for the patient. Most patients are discharged the day after surgery. MRI-guided laser surgery is changing the face of epilepsy treatment and provides a life-altering option for many epilepsy surgery candidates. The benefits of this new approach in reducing risk and invasiveness may open the door for more epilepsy patients to see surgery as a viable treatment option. Epilepsy today • Approximately 1 in 10 people will have at least one seizure during their lifetime.