Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

Effect of shot on strength of maraging steel

N. ~awa~oishi',T. ~a~ano~ & M. ~ori~arna~ I Faculty of Engineering, Kagoshima University,Kagoshima, Japan 2 Miyakonojyo National College of Technology, Miyakonojyo, Japan

Abstract

Rotating bendmg fatigue tests were carried out for a shot-peened maraging steel in order to investigate the effects of on the fatigue strength and the fracture mechanism focusing on the effect of surface roughness. Fatigue strength was markedly improved by shot peening because of hardening and generation of compressive residual in the surface layer. The origin of fatigue fracture changed from the specimen surface at high stress levels to an inclusion in the interior of specimen at low stress levels. And at the middle stress levels, both fracture modes were observed. Consequently, the shape of the S-N curve of shot- peened specimen was complex, corresponding to the change of fracture mode. In the region where surface fracture occurs, polishing the specimen surface and double shot peening using superhard fine particles were effective to improve the fatigue strength through the decrease in stress concentration due to smoothening the specimen surface.

Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

100 Surface Twatment V1

1. Introduction

Maraging steel is an ultra-high strength steel which has both high tensile strength and high ductility [1],[2]. However, fatigue strength is relatively low in

comparison with the hgh static strength [3]. Therefore, the study on the improvement of fatigue strength of maraging steel is important. Shot peening is one of effective methods for improving the fatigue strength [4]. However, the increase in surface roughness due to shot peening is very harmful to fatigue strength, because notch sensitivity of high strength steel is very high.

In the present study, rotating bending fatigue tests were carried out for shot- peened maraging steel in order to investigate the effects of shot peening on the fatigue strength and the fracture mechanism focusing on the effect of surface roughness.

2. Material and experimental procedures

The material used was an 18% Ni maraging steel whose chemical

Table 1. Mechanical properties.

Reversmn - I 1 Agw austen'te7vol.% ooc 1 UA 0116 cond~t~on MPa ' MPa I MPa I % / i I 753K-48ks ! 834 0 / 2073 2156 600 / BA

Table 2. Shot peening conditions.

Blastmy equlprnon! Air type

I I

Cemented a0 carblde

0 3 Ptessura ( MPa ] 0.3 0.3 0 3 I I

Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

Surface Treatment V1 10 1

Aging condition for fatigue test I 1 10 102 103 Aging time , ks

Figure 1:Agmg curve.

Figure 2: Shape and dimensions of specimen.

composition in weight was O.O05C, O.O5Si, O.O3Mn, 18.7Ni, 5.01M0,

8.94C0, 0.9.2Tq 0.12A1 and remainder Fe. The material was solution treated for 5.4 ks at 1123K in vacuum, followed by air cooling and age hardening in a salt bath. Figure 1shows the aging curve and the condition used for the fatigue test. As the aging condition for the fatigue test, the underaging condition of 753K-48ks was selected considering that the material had sufficiently @h and high fatigue strength, and that a marked effect of shot peering was confumed in the prelirmnary test.

Table 1shows the mechanical properties. Figure 2 shows the shape and dimensions of specimen. ARer machining, all the specimens were electro-polished by about 20 p m hmthe surface layer.

Table 2 shows the shot peening conditions. Distributions of hardness and were measured by using a micro Vickers hardness tester and an X ray diftjraction device, respectively

Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

102 Surface Deatment V1

Surface roughness was measured using a stylus-type profilometer and was the average value of five points of maximum roughness Ry. Fatigue tests were carried out using an Ono-type rotating bending fatigue testing machine with a capacity of 15 N m operating at about 50 Hz. Shot peened surface was observed using a scanning electron microscope.

3. Experimental results and discussion

Figure 3 is examples of SEM photographs of shot peened surfaces. Surface roughness was markedly improved by double shot peening.

Figures 4 and 5 show the distributions of hardness and residual stress, respectively. By shot peening, the surface layer was hardened and

Ry12 ,U m

Figure 3: Shot peened surface.

600 0 100 m 3W m0 500 Depth from the surface , ,xrn Figure 4: Hardness distribution.

Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

Surface Treatment V1 103 compressive residual stress was generated. The hardening was hgh in case of double shot peening, though the distribution of residual stress did not change, except for the one near the surface.

S-N curves of electro-polished specimens and specimens peened by 1.1 mm shot are shown in Q. 6, in which solid marks and open marks indicate an internal fracture and a surface fracture, respectively, and half solid marks as will indicate a combined fracture of internal and surface be described in detail hereinafter. Fame strength is strongly increased by shot peening and the shape of S-N curve of peened specimen is complex. l%gure 7 is an example of a crack initiated at peened surface at high stress level. Cracks initiated at the stress concentrated parts like a rugged or

0 1W 2a, XI0 400 500 Depth from the surface , urn

Figure 5: Distribution of residual stress.

Number of cycles N

Figure 6: S-N curves.

Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

104 Surface Deatment V1

Figure 7: Initiated crack at' shot peened surface ( 4 1.lmm).

@)oO= I 100m~~,X=%.7x10~cycfes (ch=750A%Ba, ~=5.4x10~cycles

8: Figure SEM photographs at several stress levels.

sunken part of peened surface.

Figure 8 is SEM photographs showing the fracture surfaces at several stress levels. Fracture occurred hmspecimen surface at high stress levels, while an internal fracture occurred at low stress levels. And at the middle stress levels, both hcture modes were observed. In general, hcture made is either the surface or the internal of specimen, consequently S-Ncurve showed a double- step wise in surface hardened steels [51,[61. In this case, however, combined hcture existed at middle stress levels. This may be the reason why S-N curve does not show dehite step. Moreover, ktigue strength for the surface fracture may be increased by improvement of surface roughness and

Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

Surface Treatment V1 105 distributions of hardness and residual stress. That is, it is effective to smmthen the surface and to maximize the peek of hardness and compressive residual stress near the surface.

Figure 9 shows S-N curves for specimens electropolished the peened surface by about 100,~m. In the figure, the results of double shot peened specimens using super hard heparticles are also shown. Fatigue strengths are markedly improved, in spite of the decrease in the depth of hardened ~ layer due to electropolishmg. Moreover, the similar effect is obtained by double shot peening. However, the influence of shot peening condition on the fatigue strength in long life region, where the internal fracture occurred, is very small. In the following, the improvement of fatigue strength in long life region will be investigated.

Figure 10 is SEM photographs magnified the crack initiation site and the boundary between the internal crack and the surface crack. A crack initiates hman inclusion and the surface is relatively flat around the inclusion, though a rough granular area is observed near the inclusion.

Moreover, many intergranular cracks are observed at the boundary between the internal crack and the surface crack. Murakami et al. [71 investigated the role of hydrogen brittleness in the early growth of fish eye cracks and indicated that a rough surface area can be observed in the vicinity of inclusions which caused internal hctures after a very hqgh fatigue cycles. The formation of rough surface around inclusions was recounted as a result of hydrogen brittleness assisted fatigue crack growth so that crack propagation in this area was extremely slow and discontinuous. On the other hand, authors indicated that the formation of reversion austenite was very

1600 - . .-....1 . . ...-.., . .-.....v ...... -.n

d DouMe '31 [email protected] P = 1m- 6 Ol.lmm-, €P. 1m-

e -3, a 1000- E, Single '31.1 D 800- e

" """I . ' . """ m0104 " 1 @ 106 I 07 108 Number of cydes N Figure 9: S-N curves of specimens eledro-polishedpeened surface.

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106 Surface Deatment V1

(a) Origin of crack initiation (b) Boundary between internal crack

and surface crack Figure 10: SEM photographs of internal crack (without reversion austenite).

Shot Size dO.6mm

. . Number of cycle N

Figure 11: S-Ncurves of steels with and without reversion austenite.

effective to improve the fatigue strength of maraging steel, especially at low stress levels [B]. Moreover, reversion austenite is insensitive to hydrogen brittleness. These results suggest that the fatigue strength in long life region can be improved by formation of reversion austenite.

Figure 11 is S-N curves showing the iduence ofthe reversion austenite. The results were obtained by using shot size of O.6mm. In this case, the steel

with the version austenite was prepared by aging the material at 783°C for 48 ks to obtain the similar static strength (o~=2043MPa, Hv=627) of the

steel without reversion austenite ( o ~=2065MPa, Hv=635). Fatigue strength was increased by the formation of reversion austenite in long life region,

though the one was decreased by the surface properties of hardness and

residual stress in short life region. Figure 12 shows a SEM photograph of fracture surface for steel with

Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

Surface Treatment V1 107

(dorigin of crack initiation (b) Boundary between internal crack and surface crack

Figure 12: SEM photographs of internal crack (with reversion austenite).

Effect of shot peening I

Fatigue strength &Fracture Mechanism Controlling factor I Increase of Nf by hardening and

compressive residual stress - Decrease of Nf by surface roughness

Increase of Nf by change in fracture S-N cuwe for unpeened I mechanism Number of cydes N

Figure 13: Schematic S-N curve showing influence of shot peening.

reversion austenite. A granular facet and intergranular cracks decrease compared with the results of steel without reversion austenite(Fig.10).

Results of Fyp. 11 and 12 suggest that the formation of reversion austenite may be effective to improve the fatigue strength through the suppression of hydrogen brittleness. Fgure 13 shows a schematic S-N curve showing the influence of shot peening and the fracture mechanism.

4. Conclusions

Rotatmg ben* fatigue tests were carried out for a shot-peened maraging steel in order to investigate the effects of shot peening on the fatigue strength

Transactions on Engineering Sciences vol 39, © 2003 WIT Press, www.witpress.com, ISSN 1743-3533

108 Surface Deatment V1

and the &acture mechanism focusing on the effect of surface roughness. Main

results were summarized as follows: (1) Fatzgue strength was markedly improved by shot peening because

of hardening and generation of compressive residual stress in the surface layer.

(2) Origin of fatigue fracture changed from the specimen surface at high stress levels to an inclusion in the interior of specimen at low stress

levels. And at the middle stress levels, both fracture modes were observed. Consequently, the shape of S-N cwe of shot-peened

specimen was complex corresponding to the change of hcture

mode. (3) In the region where surface hcture occurs,polishing the specimen

surface and double shot peening using super hard heparticles were effective to improve the fatigue strength through the decrease in

stress concentration due to smoothening the specimen surface. (4) In the region where internal hcture occurs, the formation of

reversion austenite was effective to improve the fatigue strength through the suppression of hydrogen brittleness.

References

[l] Kawabe, Y, B&. ofthe Jpn. hti'tute ofMetals. 14, pp.767-777,1975. Zackay, V.F., Parker, E.R. and Wood, W.E., hx.of the 9 Intex Cbd on

the Strength 0fMeta.k andays,No.25, pp.175-179,1975. 131 Murakami, Y, Abe, M. and Kiyota, T., h.J@n. k.M&. fig A. 53, pp.1482-1491,1987. L41 Moriyama, M., Nagano, T., Kawagoish~,N., Takaki, S. and Nagashima, E.,

JSMElntez Jour. A. 44, pp.301-308,2001. [51 Kawagoishi, N., Morino, K., Oka, T.,Tanaka, N. and Fukada, K., h,

Jpn. k.M&. Eng, A, 66, pp.2036-2043,2000. 161 Kawagoishi, Fukada, K., N., Morino, K., Chen, Q. and Kondo, E., %,

Jpn. k.Mmh. Eng, A, 67, pp.314-320,2001. L71 Murakami, Y, Nomoto, T. and Ueda, T., Fatigue & hctrrre of

Engineeni?gMaten*als& Structms, 22, pp.581-590,1999. [8] Moriyama, M., Takalu, S. and Kawagoishi, N., Jom ofk.Mat. Sir: Jpn,

49, pp.631-637,2000.