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Product Catalog January 2020 Table of Contents PRODUCT CATALOG JANUARY 2020 TABLE OF CONTENTS SINGLE WALL CARBON NANOTUBES 4 TUBALL™ PRODUCTS FOR ENERGY STORAGE 14 TUBALL™ BATT TUBALL™ FOIL PRODUCTS FOR ELASTOMERS 40 TUBALL™ MATRIX 603 TUBALL™ MATRIX 601 / 602 / 605 TUBALL™ LATEX PRODUCTS FOR THERMOSET COATINGS & COMPOSITES 60 TUBALL™ MATRIX 200/300s TUBALL™ COAT_E TUBALL™ INK SAFETY INFORMATION 78 TUBALL™ CENTER 80 3 SINGLE WALL CARBON NANOTUBES 4 5 SINGLE WALL CARBON NANOTUBES TUBALL™ SINGLE WALL CARBON NANOTUBES Human existence is shaped by the materials we use. More than 70% of all basic materials can be improved by introducing a universal additive – single wall Diameter carbon nanotubes. These tiny tubes provide us with a rare opportunity to create nanoaugmented materials that have extraordinary properties. 1.6±0.4 nm Length >5 μm Amount in 1 g 1017 nanotubes Single wall carbon nanotubes (SWCNTs) can also be called graphene nanotubes as they are essentially an extremely thin rolled up sheet of graphene. The prе-eminence of these nanotubes is related to their exceptional properties, such as superior conductivity, high temperature resistance, ultra-low weight, record strength and high flexibility. 6 7 SINGLE WALL CARBON NANOTUBES SINGLE WALL CARBON NANOTUBES TUBALL™ HOW IT WORKS While the huge potential of SWCNTs has been recognised for many TUBALL™ provides significant improvements in material properties years, until recently their wide application in industry was not possible upon the addition of ultra-low loadings – starting from only 0.01%. because of the absence of technology for their mass production, their high price and the lack of methods for introducing them into materials. TUBALL™ nanotubes are the first SWCNTs to be available for commercial applications in a wide range of industries. OCSiAl’s breakthrough yet low-cost mass-production technology has made the widespread use of nanotubes economically viable while still preserving their high quality. FEATURES • High quality of SWCNT (G/D ratio >90); Microparticles Nanofibers SWCNTs • Best price-to-performance ratio compared with analogues; • Gains traction starting from extremely low concentrations; • Adds uniform electrical conductivity; Unlike conventional additives such as multi wall carbon nanotubes, carbon fibers • Enhances mechanical properties of materials; and most types of carbon black that unequally disperse in material’s matrix, • Maintains colour, elasticity and other key properties; SWCNTs create a 3D uniform reinforced and conductive network.* • Versatile for an extremely wide range of applications. The same concentration of particles (~0.1%) in the same volume. * Ma, P. C., Siddiqui, N. A., Marom, G., & Kim, J. K. (2010). Dispersion and functionalization of carbon nanotubes for polymer-based nanocomposites: a review. Composites Part A: Applied Science and Manufacturing, 41 (10), 1345-1367. 8 9 SINGLE WALL CARBON NANOTUBES SINGLE WALL CARBON NANOTUBES NANOTUBES: THE ULTIMATE CARBON ADDITIVE THERMOSETS WITH TUBALL™ SHOW A SIGNIFICANT INCREASE IN CONDUCTIVITY Conductive carbon black TUBALL™ single wall carbon nanotubes 109 Аnti-static compounds 108 107 106 ESD compounds and electrostatic paintings 105 104 500 μm 500 μm 103 Volume resistivity, Ω•cm 102 Conductive compounds 101 0% 2% 4% 6% 8% 10% 12% 14% Conductive filler, wt.% TUBALL™ single wall CNT Multi wall CNT Premium carbon black Conductive carbon black 10 μm 10 μm Results for unfilled polyester resin. ASTM D257. 10 11 SINGLE WALL CARBON NANOTUBES SINGLE WALL CARBON NANOTUBES APPLICATIONS PROCESSING GUIDELINES Transistors Composites To easily and properly incorporate TUBALL™ into materials, OCSiAl has developed Transparent and integrated conductors and successfully launched on the market a line of pre-dispersed concentrates, circuits Lightning strike protection masterbatches and suspensions that are compatible with various industry- Field standard formulations. Memory devices emission Anti-icing Aircraſt coatings EMI braking Optical shielding system switches coatings coatings Spintronics Flame-retardant materials Lead–acid battery Electronics Lithium-ion Polymer batteries Aerospace composites & aviation Supercapacitors ESD, EMI and RFI paints Energy EMI shielding coatings Photovoltaics Wear-resistant Fuel cells Automotive coatings Thermal barrier Gas Sensors coatings separation & filtration Chemical Composites and gas sensors Wind turbine Biomedicine blade composites Radiation Polystyrene sensors composites Desalination membranes Polymers Sensor with EMI or RFI materials shielding capabilities Biosensors for improving IR detection Conductive Drug Gene composites delivery delivery Wound For more information on TUBALL™ application in a specific healing Medical device MRI contrast matrix, refer to the product listed in the catalogue or contact coatings agents FRET biosensors the nearest OCSiAl office for assistance in selecting the right solution. 12 13 PRODUCTS FOR ENERGY STORAGE 14 15 PRODUCTS FOR ENERGY STORAGE PRODUCTS FOR ENERGY STORAGE TUBALL™ BATT TUBALL™ BATT is a ready-to-use dispersion designed to easily incorporate TUBALL™ into electrode formulations during the battery manufacturing process. TUBALL™ BATT provides a complete or partial substitute for carbon black in battery electrodes and can replace several percent of carbon black with 0.03–0.1% of TUBALL™. TUBALL™ forms conductive 3D networks between active material particles at very low concentrations. The nanotubes reinforce the electrode structure and improve its mechanical stability during cycling. TUBALL™ improves adhesion by establishing strong ties between the particles, reducing the amount of binder required. 16 17 PRODUCTS FOR ENERGY STORAGE PRODUCTS FOR ENERGY STORAGE GREAT CHALLENGE: E-NABLE ENERGY BEST TECHNOLOGY WINS In order for electric vehicles to have а range and cost that is competitive with cars powered by internal combustion engines, the energy density of LIBs needs to be dramatically improved. The 2020 energy density goal, which is shared by the majority of LIB manufacturers, is 300 Wh/kg. This is a major technological challenge, and solving it will require the most advanced materials and technologies to 300 be implemented in the design of LIBs. Wh/kg TUBALL™ SWCNTs for high-energy lithium-ion batteries 18 19 PRODUCTS FOR ENERGY STORAGE PRODUCTS FOR ENERGY STORAGE IN ORDER TO ACHIEVE THE HIGH ENERGY DENSITY GOALS SET BY THE AUTOMOTIVE INDUSTRY, >240 Wh/kg: addition of SiO or Si/C to anodes is a necessity ANODES MUST CONTAIN SILICON INSIDE 300 Wh/kg: >20% SiO should be used inside the anodes Based on the PHEV2 format 300/800 240/600 220/530 Energy, Wh/kg, (Wh/L) 180/430 170/400 2016 2017 2018 2019 2020+ 20 21 PRODUCTS FOR ENERGY STORAGE PRODUCTS FOR ENERGY STORAGE THE PULVERISATION However, the more Si in the anode, the worse the swelling OF Si ANODES and pulverisation problem Si nanoparticles Lithiation Delithiation Cycles Cracking Pulverisation Pulverisation Li4SiO4 inactive SiO₂ Li4SiO4 LixSiO Si Si Si Li Si Li* insertion x Li* extraction Si Li Si x a-Si SiO₂ SiO₂ Li SiO Li4SiO4 Li SiO 4 4 Li SiO Si 4 4 4 4 a-Si LixSi 22 23 PRODUCTS FOR ENERGY STORAGE PRODUCTS FOR ENERGY STORAGE SOLVING THE SWELLING PROBLEM OF SI/C ANODES E–NABLING THE INDUSTRIAL ADOPTION BY REINFORCING THEM WITH TUBALL™ SWCNTs OF Si/C ANODES IN HIGH-ENERGY4.1―3 LIBs.0V/±0.5C 100 4.1–3.0V/±0.5C TUBALL™ Unmatched conductivity 1000 cycles 80% retention possible Flexibility 95 Strength 90 Relative Capacity, % Relative capacity, % 85 NCM 523, 18650 80 0 100 200 300 400 500 600 700 800 CycleCycles Times TUBALL™ vs MWCNT vs carbon MWCNT 1%MWCNT VGCF TUBALL™VGCF 0.06% black performanceTUBALL in ™Si/C 0.06% anodes. OCSiAl has developed the first ready-to-use TUBALL™ nanotube-based solution, SP 1% SP 1% SP 1% NCM 523 18650 cells. TUBALL™ BATT H₂O, that efficiently solves the key problem of Si/C anodes – poor cycle life. TUBALL™ e-nables the opportunity for LIB manufacturers to use high-energy Si/С anodes in their commercial LIB recipes for the EV market, while having The ultra-fine and stable TUBALL™ SWCNTs dispersion in TUBALL™ BATT H₂O, good cycle life which can meet the industry standards. when introduced into Si/C anodes at the stage of slurry manufacturing (just mix it in), fully covers and electrically connects Si/C anode particles during the charge– >240 Wh/kg – THE BENEFITS START discharge process of LIBs, even during the most harsh cycling conditions required The more that high-energy-density anodes are used, the more essential is the by EV manufacturers. application of TUBALL™ SWCNTs. 24 25 PRODUCTS FOR ENERGY STORAGE TUBALL™ BATT H₂O ULTRA-FINE TUBALL™ DISPERSION IN H₂O FOR HIGH-ENERGY Si/C ANODES FEATURES: • 0.4% TUBALL™, CMC/PVP or other binders available • Compatible with the majority of state-of-the-art Si/C recipes • Ready and easy to use IMPROVES THE CYCLE LIFE OF Si/C ANODES E-nabling their industrial use in high-energy cells. 26 27 PRODUCTS FOR ENERGY STORAGE PRODUCTS FOR ENERGY STORAGE MAXIMISING THE ENERGY DENSITY The ultra-low loading level of TUBALL™ SWCNTs allows LIB manufacturers to maximise the energy density of the cathodes by using a higher amount OF CATHODES BY UTILISING THE UNMATCHED of active material: up to 99% in modern high-energy NCM and other CONDUCTIVITY OF TUBALL™ SWCNTs cathode materials. 1000 3–4 kg of conductive carbon black in EV batteries can be replaced with just SWCNTs MWCNTs 100 g of TUBALL™. Carbon black 100 10 Resistivity, Ω 1 0.1 0.01 0.10 1.00 10.00 Conductive additive content, % The exceptional conductive properties of TUBALL™ SWCNTs allow them to offer the required conductivity, adhesion, safety, rate and cycle performance in cathodes starting from a loading of just 0.06%. This is a best-in-class result — the typical effective concentration required of Electrode sample with 0.06% of TUBALL™ shows good coverage industrially used MWCNTs or conductive carbon black is 10–50 times higher! of the particle’s surface. 28 29 PRODUCTS FOR ENERGY STORAGE BOOSTING C-RATE, REDUCING DCR BY UTILISING THE UNMATCHED CONDUCTIVITY OF TUBALL™ SWCNTs 16 Ah, NCM 523 cells.
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