inorganic compounds Acta Crystallographica Section E Experimental Structure Reports Crystal data Online ˚ 3 Mn2AsO4(OH) V = 469.33 (15) A ISSN 1600-5368 Mr = 265.81 Z =4 Orthorhombic, Pnnm Mo K radiation a = 8.5478 (16) A˚ = 12.29 mmÀ1 Redetermination of eveite, b = 8.7207 (16) A˚ T = 293 K c = 6.2961 (12) A˚ 0.05 Â 0.05 Â 0.04 mm Mn2AsO4(OH), based on single-crystal X-ray diffraction data Data collection Bruker APEXII CCD area-detector 3315 measured reflections diffractometer 911 independent reflections a b c Yongbo W. Yang, * Ryan A. Stevenson, Alesha M. Siegel Absorption correction: multi-scan 849 reflections with I >2(I) and Gordon W. Downsd (SADABS; Sheldrick, 2005) Rint = 0.015 Tmin = 0.579, Tmax = 0.639 aDepartment of Chemistry and Biochemistry, University of Arizona, 1306 Refinement E. University Blvd, Tucson, Arizona 85721-0041, USA, bDepartment of 2 2 Geosciences, University of Arizona, 1040 E. 4th Street, Tucson, Arizona R[F >2(F )] = 0.021 49 parameters 2 85721-0077, USA, cDepartment of Molecular and Cellular Biology, University of wR(F ) = 0.055 All H-atom parameters refined ˚ À3 Arizona, 1007 E. Lowell Street, Tucson, Arizona 85721-0106, USA, and dUniversity S = 1.09 Ámax = 1.28 e A 911 reflections Á = À1.15 e A˚ À3 High School, 421 N. Arcadia Avenue, Tucson, Arizona 85711-3032, USA min Correspondence e-mail:
[email protected] Received 16 October 2011; accepted 24 October 2011 Table 1 Hydrogen-bond geometry (A˚ , ). Key indicators: single-crystal X-ray study; T = 293 K; mean (As–O) = 0.002 A˚; R factor = 0.021; wR factor = 0.055; data-to-parameter ratio = 18.6.