Book of Abstracts
Total Page:16
File Type:pdf, Size:1020Kb
International Symposium for HighPerformance ThinLayer Chromatography HPTLC 2011 Book of abstracts BASEL, 06th 08th July 2011 Some statistics 223 Abstract submissions 52 Lectures 165 Posters 333 Participants from 41 countries (16th June 2011) • 20 % from India • 15 % from Germany • 13 % from Switzerland • 11 % from France • 4 % from Poland and Russian Foederation each • 3 % from Brasil, Rumania and USA each • 2 % from China, Italy and Spain each • 18 % from residual 29 countries 41 % Academics 36 % Industry 22 % Students 60 % Women Edited and revised by Prof. Dr. Gertrud (Gerda) Morlock University of Hohenheim, Stuttgart and JustusLiebig-University Gießen Germany, June 2011 2 HPTLC 2011, Basel International Scientific Committee Chair: Prof. Dr. Colin Poole, USA and Prof. Dr. Gertrud Morlock, Germany Prof. Dr. Mario Vega, Chile Prof. Dr. Zheng Tao Wang, China Dr. Jacques Pothier, France Prof. Dr. Ilkka Ojanperä, Finland Prof. Dr. Lothar Kroh, Germany Prof. Dr. Imre Klebovich, Hungary Dr. J. Madhusudana Rao, India Prof. Dr. Teresa Kowalska, Poland Dr. Wanchai DeEknamkul, Thailand Dr. Irena Vovk, Slovenia Dr. Eike Reich, Switzerland Dr. Vicente Cebolla, Spain Prof. Dr. Joseph Sherma, USA 3 HPTLC 2011, Basel The series of international HPTLC Symposia 68 June 2011, Basel (21st) International Symposium for HighPerformance ThinLayer Chromatography, HPTLC 2011 1113 June 2008, Helsinki (20th) International Symposium for ThinLayer Chromatography, HPTLC 2008 911 October 2006, Berlin (19th) International Symposium for ThinLayer Chromatography, HPTLC 2006 2931 May 2005, Siofok (18th) Planar Chromatography 2005 2325 May 2004, Visegrad (17th) Planar Chromatography 2004 1518 October 2003, Lyon (16th) International Symposium for TLC 2123 June 2003, Budapest (15th) Planar Chromatography 2003 (in honor of Professor Thihak) 46 October 2002, Novo mesto (14th) Planar Chromatography Today 2002 1113 May 2002, Keszthely (13th) Planar Chromatography 2002 (in honor of Doctor Geiss) 2325 June 2001, Lillafüred (12th) Planar Chromatography 2001 1113 May 2000, Lillafüred (11th) Planar Chromatography 2000 (in honor of Professor Kaiser) 1619 May 1998, Visegrad 10th International Symposium on Instrumental Planar Chromatography (60 years TLC + 10 years JPC) 911 April 1997, Interlaken 9th International Symposium on Instrumental Planar Chromatography 57 April 1995, Interlaken 8th International Symposium on Instrumental Planar Chromatography 2326 March 1993, Brighton 7th International Symposium on Instrumental Planar Chromatography 2326 April 1991, Interlaken Sixth International Symposium on Instrumental Planar Chromatography 2124 February 1989, Brighton (Fifth) International Symposium on Instrumental High Performance ThinLayer Chromatography 22–25 September 1987, Selvino Fourth International Symposium on Instrumental High Performance ThinLayer Chromatography 17–19 April 1985, Würzburg Third International Symposium on Instrumental HighPerformance ThinLayer Chromatography 26 May 1982, Interlaken Second International Symposium on Instrumental HighPerformance ThinLayer Chromatography 1821 May 1980, Bad Dürkheim First International Symposium on Instrumentalized HighPerformance ThinLayer Chromatography 4 HPTLC 2011, Basel Scientific Honorary Board Dr. Friedrich Geiss, Italy Dr. Dieter Jänchen, Switzerland Dr. Helmut Traitler, Switzerland Dr. P.D. Sethi, India Dr. Fred Rabel, USA Prof. Dr. David Nurok, USA Prof. Dr. Edward Soczewinski, Poland Prof. Dr. Xie Peishan, China Prof. Dr. Victor Berezkin, Russian Federation Prof. Dr. Rudolf Kaiser, Germany Prof. Dr. Siegfried Ebel, Germany In memoriam Prof. Dr. Szabolcz Nyiredy The Scientific Community deeply recognizes the life work of the Honorary Board Members for planar chromatography! hl 5 HPTLC 2011, Basel Poster Award Committee Chair: Dr. Friedrich Geiss, Italy Dr. Wanchai DeEknamkul, Thailand Prof. Dr. Mario Aranda, Chile Dr. Jacques Pothier, France Dr. Irena Vovk, Slovenia Prof. Dr. Pulok Kumar Mukherjee, India Prof. Dr. Tadeusz Dzido, Poland Prof. Dr. Wolfgang Schwack, Germany Prof. Dr. Victor Berezkin, Russian Federation Thursday 7th July 2011, 14:45 15:15 Poster Award Committee Meeting for final decision on the awardees Thursday 7th July 2011, 19:20 19:40 Poster awards 6 HPTLC 2011, Basel Schedule of Oral Presentations Wednesday, 6th 8.00 Registration starts 9.00 Tutorial: Hyphenations in HPTLC with UV/Vis/FLD/MS/FTIR/NMR/bioassays Gertrud Morlock, Germany 9.00 Tutorial: HPTLC for the analysis of botanical materials and medicinal plants Eike Reich, Switzerland 10.00 Coffee break (30 min) 10.30 Opening ceremony starts with the traditional and famous "Basler Morgenstraich" 10.50 – 12.30 Session 1 – Fundamentals Chair: Dr. Friedrich Geiss Solvents and solvent selection for thinlayer chromatography Colin Poole, USA The latest achievements and prospects for pressurized planar electrochromatography Tadeusz Dzido, Poland The new variant of multidimensional planar chromatography Svetlana Khrebtova, Russia TLC for pharmaceutical analysis in resource limited countries Eliangiringa Kaale, Tanzania Influence of magnetic and electrostatic fields on amino acids’ and biogenic amines’ retention in TLC Irena Malinowska, Poland Fluorescence detection by intensity changes for AMDTLC separations of lipids Vincente Cebolla, Spain 12.30 Lunch (1h) 13.30 – 15.00 Session 2 Miniaturization and trends Chair: Prof. Dr. Mario Aranda, Chile Ultra Thin Layer Chromatography Using Electrospun Nanofibers Susan Olesik, USA Ultrathinlayer chromatography on nanoengineered films Steven Jim, Canada Fabrication and Chromatographic Separations on BinderFree, Carbon NanotubeFabricated Thin Layer Chromatography Plates Matthew Lindfort, USA Micro PLC to detect falsified fruit preservation Rudolf Kaiser, Germany 7 HPTLC 2011, Basel 15.40 – 17.30 Session 3 Planar chromatography as preferred tool Chair: Prof. Dr. Bernd Spangenberg and Dr. Kathrin Kabrodt, Germany Planar chromatography as analytical tool in synthetic biology Irena Vovk, Slovenia HPTLC as comprehensive tool for analytical determinations Mario Vega, Chile Pharmaceutical applications of HPTLC as a problem solving technique Clare McKinlay, UK Highthroughput planar solid phase extraction – a new cleanup concept in multiresidue analysis of pesticides Wolfgang Schwack, Germany Normalphase HPTLC separation of salicylic acid, lactic acid, retinoic acid, chlorogenic acid, caffeic acid and caffeine A. Jamshidi, Iran Assessing the quality of topical formulations of Calendula officinalis with HPTLC Snezana AgatonovicKustrin, Australia 19.30 Official symposium dinner 22.00 End Thursday, 7th 9.00 – 10.20 Session 4 Traditional Medicine Chair: Prof. Dr. Irmgard Merfort, Germany The TLC atlas of Chinese crude drugs ZhengTao Wang, China Marker Profiling – Evidence Based Approach for Quality Evaluation of Herbs in Indian System of Medicine Pulok K. Mukherjee, India Simple DensitometricTLC Analysis of NonChromophore Containing Wanchai DeEknamkul, Thailand Application of HPTLC for GI stability evaluation of Psoralen, Bakuchiol and Bakuchicin in simulated physiological fluids L Sathiyanarayanan, India 10.20 Poster session and coffee break (40 min) 11.00 – 12.20 Session 5 Food supplements and phytochemistry Chair: Prof. Dr. Olumuyiwa Ogegbo, England Utilization of HPTLC for authentication and identification of botanical specimens Troy Smillie, USA TLC with biodetection to screen plant extracts for the presence of potential drugs to be used in neurodegenerative diseases Monika WaksmundzkaHajnos, Poland 8 HPTLC 2011, Basel HPTLC: simple and effective tool to detect adulterated mixtures of Eurycoma longifolia root Joseph Goh Keng Sean, Malaysia Estimation of ursolic acid and luteolin in Phyla nodiflora (L.) Greene using HPTLC Sangita Shukla, India 12.20 Lunch (1h) 13.20 – 14.45 Session 6 Phytopharmaceutical industry Chair: Dr. Mieczyslaw Sajewicz, Poland The use of (HP)TLC in phytoindustrial R&D Clemens Erdelmeier, Germany Application of (HP)TLC as essential part of Phytoneering at Bionorica – is this analytical tool still able to compete with state of the art and novel high standard analytical tools? Gudrun Abel, Germany HPTLC and HPTLC/MS studies on some bioactive natural products J. Madhusudana Rao, India Use of HPTLC in quality control & standardisation of herbal medicinal plants & products Mohammad Kamil, United Arab Emirates 14.45 Poster session and coffee break (40 min) 15.25 – 17.00 Session 7 Validation and regulatory aspects Chair: Prof. Dr. Colin Poole, USA European regulatory framework and quality control of (traditional) herbal medicinal products Werner Knöss, Germany Validation of TLC procedures Bernd Renger, Germany Development of stability indicating chromatographic evaluation method for moxonidine in pharmaceutical formulations Rajendra B. Kakde, India Chemical profiling of exstesy recoverd from around Jakarta by HPTLCspectrophotodensitometry I M.A.Gelgel Wirasuta, Indonesia RPHPTLC estimation of benzhexol HCl and trifluperazine HCl in pharmaceutical dosage form M.S.Charde, India 17.00 Panel discussion with invited speakers (coffee available) Chair: Prof. Dr. Matthias Hamburger, Switzerland 17.45 – 19.20 Session 8 Manufacturers session Chair: Pierre BernardSavary, CCCM France Recent instrumentation developments at CAMAG Rolf Rolli, Switzerland 9 HPTLC 2011, Basel Future perspectives of TLC; The dominant marked leader steps ahead Mehmet Dogan, Germany HPTLCMALDITOFMS coupling for the MS and MS/MS analysis maintaining the chromatographic resolution Martin Schürenberg, Germany Phytochemical