*Manuscript Click here to view linked References 1 Ferrous metallurgy from the Bir Massouda metallurgical precinct at Phoenician and Punic 2 Carthage and the beginning of the North African Iron Age 3 4 Brett Kaufmana*, Roald Docterb, Christian Fischerc, Fethi Chelbid, Boutheina Maraoui Telminie 5 6 a) Joukowsky Institute for Archaeology and the Ancient World, Brown University, Rhode Island 7 Hall, Box 1837, Providence, RI, 02912, USA 8 b) Department of Archaeology, Ghent University, Ghent (BE), Sint-Pietersnieuwstraat 35, B- 9 9000 Ghent, Belgium 10 c) Department of Materials Science and Engineering, University of California, Los Angeles 11 (UCLA), 410 Westwood Plaza, Los Angeles, CA, 90095 1595, USA 12 d) Institut National du Patrimoine, 4 Place du château, TN-1008, Tunis, Tunisia 13 e) Faculté des Sciences Humaines et Sociales de Tunis, University of Tunis, Boulevard du 9 14 Avril 1938, Tunis, Tunisia 15 16 *Corresponding author, Tel: 312-505-0170; email:
[email protected] 17 18 Excavations of the Phoenician and Punic layers at the site of Bir Massouda in Carthage have 19 provided evidence for ferrous metallurgical activity spanning several centuries. 20 Archaeometallurgical analyses of slagged tuyères, slag, and alloys using optical microscopy, 21 portable x-ray fluorescence spectroscopy (pXRF), and variable pressure scanning electron 22 microscopy coupled with energy dispersive x-ray spectroscopy (VPSEM-EDS) show that 23 Carthaginian smiths were conducting primary smithing and forging of wrought iron and steel. 24 Although the majority of slag specimens are remnant from ferrous production, a few select finds 25 are from bronze recycling. The corpus represents the earliest known ferrous metallurgy in North 26 Africa.