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CSIR-Institute of Minerals & Materials Technology CSIR-Institute of Minerals & Materials Technology Volume 1, January 2020 From Director… cated publication is a step forward in the direction of I am glad to know that CSIR-IMMT, promoting all round activities of the institute, which Bhubaneswar is starting e-Newsletter are carried during the period of last six months. I “MinMat” from the year 2020. This is extend my sincere gratitude to the editorial board the perfect platform to share the activ- members who are part of this successful venture and ities of IMMT, which forms an integral good wishes to all the students, scientists, staffs for part of the institute’s emerging socio- their contribution regularly. economic scenario. This e-Newsletter will widen the horizon of the readers and will flash Wish you all a very happy & prosperous new year the R & D efforts, Innovations, Societal work under- 2020 taken by the institute. This e-Newsletter, our dedi- Prof. Sudhasatwa Basu CSIR-IMMT : Vision & Mission CSIR-Institute of Minerals and Materials Technology how and consultancy services for commercial exploi- (IMMT) is a constituent R&D laboratory under the tation of natural resources through the public-private aegis of the Council of Scientific and Industrial Re- -partnership (PPP) approach. Today, CSIR-IMMT is search (CSIR), New Delhi. The main thrust of R&D the first choice for many mineral based industries. It at CSIR-IMMT has been to empower Indian indus- is also carving out a niche in processing of advanced tries to meet the challenges of globalization by materials for greater value addition and working on providing advanced and zero waste process know- resource use efficiency of critical raw materials . VISION MISSION A center of world-class “Knowledge & Innova- To develop globally competitive, scientific & in- tion” for sustainable development of mineral & novative knowledge that helps realize maximum material resources societal and economic value from our mineral and material resources 2 Highlighted Research @ CSIR-IMMT Newly designed 1,2,3-triazole functionalized cova- combination with facile modular synthesis via rationally lent triazine frameworks with exceptionally high up- designed building blocks, high thermal and chemical stabil- ity, and excellent CO2, H2 and CH4 uptake and separation take capacity for both CO2 and H2 capabilities make them promising task-specific adsorbents A numerous research activities are going-on in the domain for various potential applications. of functional porous materials to avoid global warming via stabilizing the atmospheric CO2 level. The search for effi- (Corresponding author: [email protected]) cient and high performing physisorbents for CO2 capture and separation from point sources as well as storage of cleaner gaseous fuels, such as H2 and/or CH4, is consid- ered to be a major challenge. In this study (Soumya Mukherjee et. al. Journal of Materials Chemistry A, 7 (3), 2019: 1055-1068), a set of novel 1,2,3-triazole func- tionalized covalent triazine frameworks (TzCTFs) was syn- thesized under typical ionothermal conditions utilizing two rationally designed C3-symmetric triazole-substituted aro- matic trinitrile building block analogues, namely Tz-FCN and Tz-HCN, with fluorinated and non-fluorinated phenyl core, respectively. The obtained novel TzCTF materials in Ultrasonic-assisted flotation for enhancing the re- enhancing the flotability of flaky graphite from low-grade covery of flaky graphite from low-grade graphite ore graphite ore was investigated in this present study (Santosh Deb Barma et. al. Ultrasonics Sonochemis- Graphite is known to ex- try, 56, 2019; 386-396). The flotation experiments were hibits the properties of conducted in three stages viz., rougher, cleaner, re-cleaner both metal and non-metal stage during both convention and ultrasonic-assisted flota- and hence responsible for tion. It was found that the efficiency of ultrasonic-assisted its profound applications in flotation was significantly higher than conventional flota- various industries. In order tion. The yield, fixed carbon content and percentage recov- to separate natural graph- ery of the flotation concentrate products increased signifi- ite from the associated cantly under ultrasonic-assisted flotation. Furthermore, the impurities, flotation tech- ultrasonic mechanism and its effect responsible for the nique is commonly em- breakage of graphite-impurities locked particles and parti- ployed at an industrial cle size reduction were also discussed comprehensively. scale. The feasibility of low- (Corresponding author: [email protected]) frequency ultrasound in Flaky graphite in flotation concentration Hydrogen Photosynthesis through Schottky Junction RGO and NiPO surface which efficiently interferes with of RGO-NiPO and the Perspective of the Mechanism the charge carrier losses during the water reduction reac- tion in the presence of light. Furthermore, this phenomena The synthesis of an eco- was evidenced from the time-resolved photoluminescence nomical and efficient photo- spectra, where the decay components were calculated to catalyst for the fabrication have a shorter decay time (1.40 ns) in the case of 12RGO- of clean H-2 from water NiPO than that of NiPO (5.3 ns), implying efficient e(-) splitting is significant for the transfer across the NiPO-RGO interface. The NiPO nanos- actual application. In this trings were face-to-face assembled on the surface of the study (Alka Samal et.al. graphene sheet, which makes the intimate contact between ACS Sustainable Chemis- the nanostrings and graphene feasible. Such noble-metal- try & Engineering, 7(11), free photocatalyst may provide an approach for the design 2019; 10052-10063), the of very efficient water-splitting catalysts, which are predict- researchers have reported ed to be applied to the actual photocatalytic water-splitting the low-cost synthesis of industry. Owing to the synergetic effect of the distinguisha- reduced graphene oxide ble structural and compositional privileges, the RGO-NiPO embedded nickel phosphate nanostrings showed admirable activity with a H-2 rate of (RGO-NiPO) photocatalyst by low-temperature hydro- 9000 mu mol/h/g and high photocatalytic water-splitting thermal reaction system. The composite showed great stability without the use of any other cocatalysts. potential in the photoreduction reaction of water under visible spectrum irradiation. The morphological analysis of (Corresponding author: [email protected]) RGO-NiPO explains an amazing interaction between the 3 News & Events 14th Ore & Minerals Analysis (OMA) Workshop, strations. The hands-on exposure was most beneficial to CSIR-IMMT Bhubaneswar (13th - 14th June 2019) ~20 research scholars who attended the workshop. Ore & Minerals Analysis (OMA) Workshop is an annual event which is hosted periodically by M/s Malvern Panalyti- cal in different countries. The 14th OMA Workshop was jointly organized by M/s Malvern Panalytical and CSIR- IMMT, Bhubaneswar during 13th-14th June 2019 and for the first time, the workshop was held in Asia. The theme of the workshop was “Latest developments in X-ray tech- niques for minerals, metals, and materials”. A total of 74 participants from industry, academia, and R&D attended the workshop. Overseas experts from The Netherlands, Australia, Indian faculties from CSIR-IMMT, Institute of Physics, ICT-Mumbai and from the Malvern Panalytical provided both theoretical insights and practical demon- Intellectual Property Rights (IPR) A workshop on Intellectual Property Rights (IPR) Aware- ness was organized on 25th April 2019 (14:00 – 17:30) by the Department of Business Development of CSIR-IMMT. The resource persons were Dr. S.K. Kar and Dr. P. Karthigeyan of Intellectual Property Facilitation Centre (IPFC), Central Tool Room & Training Centre (CTTC). Head of Business Development Shri Santosh Mishra, Chief Scientist welcomed the gathering and explained the objec- tives of the program. A brief introduction on IPFC activities and IPR was presented by Dr. Kar, Head of IPFC. Subse- quently Dr. Karthigeyan explained in detail about different IPR concepts such as Patent, Industrial Design, Trademark, GI, Copy Rights. Later he presented on prior art Search, Patent drafting, Filing procedure and Fees (a case study), PCT filing, Technology Licensing, FTO analysis. The pro- gram winded up with a vote of thanks by Dr. A K Sahoo, Chief Scientist. Utkal Diwas Every financial year in CSIR-IMMT starts with a vibrant atmosphere due to “Utkal Diwas”, the Odisha state for- mation day on 1st April. Like earlier years, IMMT-Staff Club celebrated the Utkal Diwas of 2019 with great enthusiasm. Shri Trilochan Kanungo, an eminent educationist, econo- mist and ex-member of parliament from Odisha was the Chief guest on this occasion. The event was started in the traditional way by the lightening of the lamp and recitation of Odisha state song, “Bande Utkala Janani”. The director of the institute, Prof. S. Basu welcomed all the staffs & guests present in the function and narrated the history of the first instance of formation of provinces (Orissa and Sindh) based on language before independence. Shri San- in Odisha since its formation. The program got over with tosh K. Mishra, Chief Scientist introduced the chief guest the distribution of prizes to the winners of Rangoli & Jhoti to the audience and informed the contributions of Shri competitions which were conducted on the eve of Utkal Kanungo as a social worker and parliamentarian. Shri Diwas. Kanungo highlighted the economic growth & social changes 4 News
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