Instrumental Chemistry

Total Page:16

File Type:pdf, Size:1020Kb

Instrumental Chemistry Instrumental Chemistry Prof. Zvi C. Koren Topics Spectrometric Techniques: UV/Vis (ultraviolet/visible) Spectrometry – electronic transitions FTIR (Fourier Transform Infrared) Spectrometry – molecular vibrations NMR (Nuclear Magnetic resonance) Spectrometry – nuclear spins MS (Mass Spectrometry) AA (Atomic Absorption) Spectrometry Chromatographic Methods: GC-MS (Gas Chromatography – Mass Spectrometry) HPLC-PDA (High-Performance Liquid Chromatography – Photodiode Array detection) GPC (Gel Permeation Chromatography) Thermal Analysis: DSC (Differential Scanning Calorimetry) DMTA (Dynamic Mechanical Thermal Analysis) Others: TOC (Total Organic Carbon) Analyzer Spectroscopy = Spectrometry = Spectrophotometry The study of the interaction between light and matter UV/Vis Spectroscopy: Absorption of light leads to a transition of an electron from one level to the next. Wave Theory of Light l A The Electromagnetic Spectrum Spectral Regions and Molecular Transitions Region Wavelengths () Transitions X-ray 10–2 – 10 nm K and L electrons Far UV 10 – 200 nm Mid-shell e’s Near UV 200 – 400 nm Valence e’s Visible 400 – 800 nm Valence e’s Near Infrared, NIR 0.8 – 2.5 m Molecular vibrations IR 2.5 – 50 m Molecular vibrations Far IR 50 – 300 m Molecular rotations Microwave 0.3 mm – 0.5 m Molecular rotations Radiowave 0.5 – 300 m NMR, Nuclear Magnetic Resonance Visible Light R O Y G. B I V Violet: 400 - 420 nm Indigo: 420 - 440 nm Blue: 440 - 490 nm Green: 490 - 570 nm Yellow: 570 - 585 nm Orange:585 - 620 nm Red: 620 - 780 nm Color Wheel: Complementary Colors Absorbed and Reflected Colors: “What you see is NOT what you got.” Complementary colors are diametrically opposite each other: color absorbed vs. Color observed Note: Green is unique in that it can be created by absorption close to 400 nm as well as absorption near 800 nm. UV/Vis Spectrometer: Dual Beam (multiple l‘s) (prism) mono- chromatic single l Transmittance vs. Absorbance Transmittance: T = I/Io < 1 (sometimes expressed as a percent, %, and not as a fraction) Absorbance: A = log10(Io/I) = –log10T If no absorption of light has occurred: A = 0 T = 1 Beer’s Law (or Beer-Lambert Law) Absorbance: A = a·b·c (but often written as A = bc) a or = molar absorptivity (or extinction coefficient), l-dependent units of M–1cm–1 b = light path through the cell (cuvet), typically 1 cm c = concentration of the solute in the solution A = f(l), and of the material of course A is linear with c, ideally For strongly absorbing compounds: > 10,000. For weakly absorbing compounds: = 10 – 100. Typical UV/Vis Spectrum Note the Experimental Conditions: c = 0.142 M (in 95 % ethanol), Homework Assignment 1: b = 1.0 cm (Email the answers to me) 1. What is the color of the solution? Explain. 2. What are the values of 395 and 255? Use the appropriate units. Show the calculation. Do the numbers make sense? 3. What is the name of the compound? (Use the naming tool from the ChemSketch program from the free site www.acdlabs.com.) Why Are Some Organic Molecules Colored? extensively conjugated pi-electrons.
Recommended publications
  • General Information Academic Subject Analytical and Instrumental
    General Information Academic subject Analytical and instrumental chemistry with laboratory Degree course Bachelor programme: Food Science and Technology ECTS credits 6 ECTS Compulsory attendance No Teaching language Italian Subject teacher Name Surname Mail address SSD Elisabetta [email protected] AGR/13 Loffredo ECTS credits details Basic teaching activities 4 ECTS Lectures 2 ECTS Laboratory classes Class schedule Period II semester Course year Second Type of class Lecture- workshops-laboratory-didactic visits Time management Hours 150 In-class study hours 60 Out-of-class study hours 90 Academic calendar Class begins February 24th, 2020 Class ends June 12th, 2020 Syllabus Prerequisites/requirements Prerequisites: “Chemistry” Knowledge of general, inorganic and organic chemistry Expected learning outcomes Knowledge and understanding o Knowledge and understanding for the choice and use of the most appropriate techniques to solve specific problems concerning food processes Applying knowledge and understanding o Ability to select and use appropriate analytical techniques to evaluate food quality o Ability to perform correctly the general or specific sequence of phases of a chemical analysis o Ability to follow safety rules in the chemistry laboratory Making informed judgements and choices o Ability to select appropriate procedures to evaluate important properties of food or other matrices influencing food quality o Ability to improve and implement analytical procedures that are appropriate to determine important chemical characteristics
    [Show full text]
  • Department of Chemistry
    188 Department of Chemistry Department of Chemistry Chairperson: Ghaddar, Tarek H. Al-Ghoul, Mazen H.; Bouhadir, Kamal H.; Ghaddar, Tarek H.; Ghauch, Antoine R.; Haddadin, Makhlouf J.; Professors: Halaoui, Lara I.; Hasanayn, Faraj A.; Kaafarani, Bilal R.; Patra, Digambara J.; Saliba, Najat I.; Sultan, Rabih F. Associate Professors: Karam, Pierre M.; El-Rassy, Houssam T. Assistant Professor: Hmadeh, Mohamad A. Instructors: Abi Rafii, Randa A.; Deeb, Hana H.; Sadek, Samar A. BS in Chemistry Mission Statement The Chemistry Department provides liberal arts and professional education in chemistry. The undergraduate program at the department is dedicated to teaching, scholarship, research and creative endeavors. Through this program, the department delivers a strong theoretical course of study and practical training in the chemical sciences to assure the success of its students in graduate schools, professional schools and employment. Undergraduate students are able to explain the essential facts, principles and theories across the four major areas of chemistry, i.e. analytical, organic, inorganic and physical. In addition, they are strongly encouraged to be engaged in research in these aforementioned areas. The program also plays a central role in the education of students of other majors, including students of Medicine, Health Sciences, Engineering, and Agriculture. Students accepted as chemistry majors must maintain an average of 2.2 (or 70) or above in their first three terms in major courses in order to remain in the program. Students must complete the following minimum requirements: CHEM 201, CHEM 201L, CHEM 211, CHEM 212, CHEM 215, CHEM 216, CHEM 217, CHEM 218, CHEM 220, CHEM 225, CHEM 228, CHEM 229, and CHEM 230, at least two elective courses of the following five courses: CHEM 231, CHEM 232, CHEM 233, CHEM 234 and BIOL 220, in addition to MATH 201, MATH 202, and CMPS 209 or CMPS 200, PHYS 211 and PHYS 211L, 6 credits in the Social Sciences, and 12 credits in the Humanities.
    [Show full text]
  • Analytical Platforms at Swiss Universities of Applied Sciences
    618 CHIMIA 2020, 74, No. 7/8 Columns doi:10.2533/chimia.2020.618 Chimia 74 (2020) 618–628 © Swiss Chemical Society FH Universities of Applied Sciences HES Fachhochschulen – Hautes Ecoles Spécialisées Analytical Platforms at Swiss Universities of Applied ments (e.g. HPLC, MS, NMR) to follow reactions and perform Sciences quality control. Sometimes such platforms are partially orga- nized as open-access facilities, where a dedicated team maintains Christian Berchtolda, Jean-Pascal Bourgeoisb, Verena instruments and each scientist uses these open-access systems on Christena, Michal Dabrosb, Caspar Demuthd, Anika a need basis. Hoffmannc, Franka Kalmanc, Susanne Kernd, Nadia Finally, there are independent multidisciplinary analytical Marconc, Olivier Nicoletb, Marc E. Pfeiferc, Umberto platforms that run their own instruments, perform their own Piantinic, Denis Primc, Cyril Portmannb, Samuel Rothb, projects for method and instrument development and support Jean-Manuel Segurac, Olivier Vorletb, Chahan Yeretziand, other teams inside and outside the institution with analytical Mathieu Zollingerc, and Götz Schlotterbeck*a expertise and instrumentation. The techniques used in all these fields where analytical platforms play a key role, as well as *Correspondence: Prof. Dr. G. Schlotterbecka, E-mail: [email protected] aFHNW Fachhochschule Nordwestschweiz, Hochschule für Life Sciences, how they are organized within the different institutions, is as Institut für Chemie und Bioanalytik, Hofackerstrasse 30, CH-4132 Muttenz; diverse as the different research and education models. This bHES-SO Haute école spécialisée de Suisse occidentale, Haute école d’ingénierie article provides an overview of analytical platforms, projects et d’architecture Fribourg, Institute of Chemical Technologies, Boulevard de Pérolles 80, CH-1700 Fribourg; infrastructure and focus of the Universities of Applied Science cHES-SO Haute école spécialisée de Suisse occidentale, HES-SO Valais-Wallis, across Switzerland.
    [Show full text]
  • About Continuity and Rupture in the History of Chemistry: the Fourth Chemical Revolution (1945–1966)
    About continuity and rupture in the history of chemistry: the fourth chemical revolution (1945–1966) José A. Chamizo Foundations of Chemistry Philosophical, Historical, Educational and Interdisciplinary Studies of Chemistry ISSN 1386-4238 Found Chem DOI 10.1007/s10698-018-9308-9 1 23 Your article is protected by copyright and all rights are held exclusively by Springer Science+Business Media B.V., part of Springer Nature. This e-offprint is for personal use only and shall not be self-archived in electronic repositories. If you wish to self-archive your article, please use the accepted manuscript version for posting on your own website. You may further deposit the accepted manuscript version in any repository, provided it is only made publicly available 12 months after official publication or later and provided acknowledgement is given to the original source of publication and a link is inserted to the published article on Springer's website. The link must be accompanied by the following text: "The final publication is available at link.springer.com”. 1 23 Author's personal copy Found Chem https://doi.org/10.1007/s10698-018-9308-9 About continuity and rupture in the history of chemistry: the fourth chemical revolution (1945–1966) José A. Chamizo1 © Springer Science+Business Media B.V., part of Springer Nature 2018 Abstract A layered interpretation of the history of chemistry is discussed through chemical revolutions. A chemical revolution (or rupture, discontinuity, transition) mainly by emplacement, instead of replacement, procedures were identifed by: a radical reinter- pretation of existing thought recognized by contemporaries themselves, which means the appearance of new concepts and the arrival of new theories; the use of new instruments changed the way in which its practitioners looked and worked in the world and through exemplars, new entities were discovered or incorporated; the opening of new subdisci- plines, which produced, separated scientifc communities.
    [Show full text]
  • Department of Chemistry 187
    Department of Chemistry 187 Department of Chemistry Chairperson: Ghaddar, Tarek H. Al-Ghoul, Mazen H.; Bouhadir, Kamal H.; Ghaddar, Tarek H.; Haddadin, Makhlouf J.; Halaoui, Lara I.; Professors: Hasanayn, Faraj A.; Kaafarani, Bilal R.; Saliba, Najat I.; Sultan, Rabih F. El-Rassy, Houssam T.; Ghauch, Antoine R.; Patra, Associate Professors: Digambara J. Assistant Professors: Hmadeh, Mohamad A.; Karam, Pierre M. Instructors: Abi Rafi, Randa A.; Deeb, Hana H.; Sadek, Samar A. BS in Chemistry Mission Statement The Chemistry Department provides liberal arts and professional education in chemistry. The undergraduate program at the department is dedicated to teaching, scholarship, research and creative endeavors. Through this program, the department delivers a strong theoretical course of study and practical training in the chemical sciences to assure the success of its students in graduate schools, professional schools and employment. Undergraduate students are able to explain the essential facts, principles and theories across the four major areas of chemistry, i.e. analytical, organic, inorganic and physical. In addition, they are strongly encouraged to be engaged in research in these aforementioned areas. The program also plays a central role in the education of students of other majors, including students of Medicine, Health Sciences, Engineering, and Agriculture. Students accepted as chemistry majors must maintain an average of 2.2 (or 70) or above in their first three terms in major courses in order to remain in the program. Students must complete the following minimum requirements: CHEM 201, CHEM 201L, CHEM 211, CHEM 212, CHEM 215, CHEM 216, CHEM 217, CHEM 218, CHEM 220, CHEM 225, CHEM 228, CHEM 229, and CHEM 230, at least two elective courses of the following five courses: CHEM 231, CHEM 232, CHEM 233, CHEM 234 and BIOL 220, in addition to MATH 201, MATH 202, and CMPS 209 or CMPS 200, PHYS 211 and PHYS 211L, 6 credits in the Social Sciences, and 12 credits in the Humanities.
    [Show full text]
  • General Information Academic Subject Analytical and Instrumental
    General Information Academic subject Analytical and instrumental chemistry with laboratory Degree course Bachelor programme: Food Science and Technology ECTS credits 6 ECTS Compulsory attendance No Teaching language Italian Subject teacher Name Surname Mail address SSD Elisabetta [email protected] AGR/13 Loffredo ECTS credits details Basic teaching activities 4 ECTS Lectures 2 ECTS Laboratory classes Class schedule Period II semester Course year Second Type of class Lecture- workshops-laboratory-didactic visits Time management Hours 150 In-class study hours 60 Out-of-class study hours 90 Academic calendar Class begins March 5th, 2018 Class ends June 22th, 2018 Syllabus Prerequisites/requirements Prerequisites: “Chemistry” Knowledge of general, inorganic and organic chemistry Expected learning outcomes Knowledge and understanding o Knowledge and understanding for the choice and use of the most appropriate techniques to solve specific problems concerning food processes Applying knowledge and understanding o Ability to select and use appropriate analytical techniques to evaluate food quality o Ability to perform correctly the general or specific sequence of phases of a chemical analysis o Ability to follow safety rules in the chemistry laboratory Making informed judgements and choices o Ability to select appropriate procedures to evaluate important properties of food or other matrices influencing food quality o Ability to improve and implement analytical procedures that are appropriate to determine important chemical characteristics
    [Show full text]
  • Mass Spectrometry-Based Investigations to Characterize Specific Cell Types Within the Brain
    MASS SPECTROMETRY-BASED INVESTIGATIONS TO CHARACTERIZE SPECIFIC CELL TYPES WITHIN THE BRAIN BY ANN M. KNOLHOFF DISSERTATION Submitted in partial fulfillment of the requirements for the degree of Doctor of Philosophy in Chemistry in the Graduate College of the University of Illinois at Urbana-Champaign, 2011 Urbana, Illinois Doctoral Committee: Professor Jonathan V. Sweedler, Chair Assistant Professor Ryan C. Bailey Professor Martha U. Gillette Professor Alexander Scheeline ABSTRACT Investigations of the chemical content of the brain and its many constitutive cell types yield information regarding normal and abnormal brain function. Frequently, proteomics, peptidomics, and metabolomics experiments survey brain regions and attribute detected species to neurons. However, many other cell types are present, including astrocytes, oligodendrocytes, and microglia. It is also known that different cell types can vary greatly in their analyte content and concentration; therefore, to obtain an adequate representation of brain function, specific cell types require further characterization. Cell types of particular interest are astrocytes, which are involved in neuronal communication, and mast cells, which are involved in allergic response. Moreover, morphologically similar cells can exhibit chemical heterogeneity; to characterize these differences, single-cell analyses are necessary. In this case, single cells from the model organism, Aplysia californica, are isolated for analysis. Mass spectrometry (MS) is well-suited for such applications because it has limits of detection in the attomole range for both small molecule metabolites and peptides, has a wide dynamic concentration range, and can detect and identify molecules of interest without a priori knowledge of sample content. To characterize metabolite profiles in single cells and tissue homogenates, a laboratory-built capillary electrophoresis (CE) system coupled to electrospray ionization (ESI) MS is implemented.
    [Show full text]
  • Publikationen 2005
    _______ Westfälische Wilhelms-Universität Münster Publikationen 2005 Institut für Medizinische Physik und Biophysik Universitätsklinikum Münster Westfälische Wilhelms-Universität Münster Zeitschriftenartikel, Buchbeiträge, Bücher Fachge- biet(e)* Balen, B., Zamfir, A., Vakhrushev, S., Krsnik-Rasol, M., Peter- ESI Kataliniş, J. Determination of Mammalaria gracillis N-glycan Patterns by ESI QTOF Mass Spectrometry Croatica Chim. Acta 78 (2005) 463-477 Berezhna S., Schaefer S,. Heintzmann R., Jahnz M., Boese G., BP, ZB Deniz A., Schwille P. New effects in polynucleotide release from cationic lipid carriers revealed by confocal imaging, fluorescence cross-correlation spectroscopy and single particle tracking. Biochim. Biophys. Acta 1669 (2005) 193-207 Bindila, L., Peter-Kataliniş, J., Zamfir, A. ESI Sheathless revers polartiy capillary electrophoresis-electrospray mass spectrometry for analysis of underivatized glycoconjugates. Electrophoresis 26 (2005) 1488-1499 Böse, G. and Peters, R. BP, ZB Nanoporen als künstliche molekulare Maschinen. Bioforum 7/8 (2005) 42-44 Bulau, P., Okuno, A., Thome, E., Schmitz, T., Peter-Kataliniş, J., BC, ESI Keller, R. Characterization of a molt-inhibiting hormone (MIH) of the crayfish, Orconectus limosus, by cDNA cloning and mass spectrometric analysis. Peptides (2005), in press Cederkvist, H., Zamfir, A., Bahrke, S., Eijsink, V.G.H., Sorle, M., ESI, BC Peter-Kataliniş, J., Peter, M.G. Analysis of non-covalent complexes of chitinase B and chitooligosaccharides by (+) NanoESI QTOF mass spectrometry. Angew. Chemie (2005), in press Dreisewerd, K., Müthing, J., Pohlentz, G., Rohlfing, A., Meisen, I., LM Vukelic, Z., Kölbl, S., Peter-Kataliniş, J., Hillenkamp, F., Berkenkamp, S. Analysis of Oligosaccharides and Gangliosides Directly from HPTLC Plates by IR-MAALDI-o-TOF Mass Spectrometry with a Glycerol Matrix.
    [Show full text]
  • Graduation Requirements for Chemistry
    Chemistry (Teacher Certification), B.S. 43 courses of three or more credits, 3 one-credit Field Experiences, 3 one-credit PE courses GENERAL EDUCATION CORE MAJOR BASIC REQUIREMENTS (2 courses and 3 one- CH 101: Chemical Principles credit PE courses) CH 102: General Chemistry Composition and Rhetoric CH 231: Organic Chemistry I EN 103 Composition and Rhetoric I CH 232: Organic Chemistry II EN 104 Composition and Rhetoric II Physical Education Courses CH 304: Inorganic Chemistry PE 100 CH 351: Physical Chemistry I PE ____ CH 352: Physical Chemistry II PE ____ CH 361: Analytical Chemistry CH 362: Instrumental Anal. Chemistry MODES OF THINKING (5 courses) CH 435: Biochemistry I Literature (Select one) CH 455: Research Seminar (Must be Brit or Am Lit for STEP) CH 461: Research or CH 396-399: EN 110, EN 112, EN 115 Internship Mathematics (Satisfied by major) MA 121: Calculus Natural Science (Satisfied by major) MA 122: Calculus II Philosophy PH 201: Gen Phys. I: Mechanics and PL 109 Heat Social Sciences PH 202: Gen. Phys. II: Wave ED 209 Phenomena and Electromagnetism (Required by STEP) STEP Controlled Requirements CULTURAL LITERACY (4 courses) CH 1053 (1 credit) Humanities I and II. Preferably select a set (e.g., HI201/202). STEP students must take two math courses. MA 107 and Hum. I: HI201, PO201, HI213 MA 108 are recommended. Hum. II: HI 202, PO202, HI214 Humanities III: Great Works of Art & Music EDUCATION (13 courses & three 1-credit field courses) (See Master Schedule of Day Classes) ED 109 ____ ED 3801* ____
    [Show full text]
  • Department of Chemistry
    Chemistry Department Texas A&M University-Commerce P.O. Box 3011 Commerce, TX, 75429 (903) 886-15391 [email protected] Laurence A. Angel Qualifications Doctor of Philosophy, Chemistry, 2000. Bachelor of Science (Honors), Environmental Science with North American Studies (minor), 1996. Professional Experience June 2013 – Present, Associate Professor, Texas A&M University-Commerce. Aug 2007 – May 2013, Assistant Professor, Texas A&M University-Commerce. July 2003 – Aug 2007, Assistant Research Professor, University of Nevada, Reno. Sept.1999 – July 2003, Postdoctoral Research, Professor K.M. Ervin, University of Nevada, Reno. Education Sept.1996 – Sept.1999, Doctor of Philosophy, Professor A.J. Stace, University of Sussex, U.K. Oct.1992 – June 1996, BSc (Hons), Environmental Science with North American Studies, University of Sussex. Awards Texas A&M University – Commerce 2011 Provost Award: Research and Creative Activity. Teaching Quantitative and Instrumental Analysis, Advanced Analytical Chemistry, Instrumental Chemistry, Advanced Instrumental Analysis I, Advanced Instrumental Analysis II, Physical Chemistry II, Advanced Research Techniques and Design I, Advanced Research Techniques and Design II, General and Quantitative Chemistry I, General and Quantitative Chemistry II, General Chemistry Tutorial I, General Chemistry Tutorial II, Undergraduate Research, Graduate Thesis, Chemical Science and Profession, Graduate Seminar. Research Developing ion mobility - mass spectrometry techniques for protein and nanocluster research. External Research Funding Acquired PI, National Science Foundation – Major Research Instrumentation Grant. CBET-0821247, Acquisition of a IM- Q-TOF Mass Spectrometer, Laurence Angel, Ph.D., (PI), Nenad Kostic, Ph.D., (Co-PI), Frank Miskevich, Ph.D., (Co-PI), Stephen Starnes, Ph.D., (Co-PI), William Whaley, Ph.D., (Co-PI), Serge P.
    [Show full text]
  • Major in Chemistry Course Descriptions
    Department of Natural Sciences Professors: Stuart I. Cromarty, Edward J. Dix (Chairperson), Brian K. Niece, Owen D.V. Sholes, Steven J. Theroux; Associate Professors: Elizabeth A. Colby Davie, David Crowley, Aisling S. Dugan, Georgi Y. Georgiev, James F. Hauri, Michele L. Lemons, Kimberly A. Schandel; Assistant Professors: Karolina Fucikova, Benjamin J. Knurr, Laura Marcotte, Jessica A. McCready; Visiting Instructors: Elissa Kraus, Anthony Sacino; Lecturers: Soraya Betancourt-Calle, Arthur LaPlante, Mary Lou Lombardi-Butler, Sandra Nedelescu, Hubert G. Meunier (Professor Emeritus). MISSION STATEMENT The Department of Natural Sciences is dedicated to preparing students to live and work in a changing world by ensuring competency in the natural sciences and scientific inquiry. The department strives to provide a basic understanding of classical and contemporary scientific concepts in these areas. While developing an understanding of the scientific process and its application, the following critical skills are stressed: observation, inquiry, data collection, analysis, communication, and correlation of scientific concepts. The department prepares students for careers and professional opportunities in the sciences as well as for life-long learning in the context of a liberal arts curriculum in the Catholic tradition. PROGRAMS OF STUDY AND CAREER OPTIONS The Department of Natural Sciences offers majors in Biology, Biology with a Concentration in Neuroscience and Behavior, Biotechnology and Molecular Biology, Neuroscience, Chemistry, Environmental Science, and Environmental Science with a Concentration in Environmental Policy. The Department also offers minors in Biology, Environmental Science, Chemistry, and Physics, and it co-sponsors a concentration in Physical and Occupational Therapy with the Department of Human Services and Rehabilitation Studies. Research opportunities are available at the College and at nearby institutions (e.g., University of Massachusetts Medical School and the Biotechnology Park).
    [Show full text]
  • CHEM 300 – Spring 2012
    CHEM 300 – Spring 2012 Instrumental Chemistry and Analytical Methods Lectures: Monday, Wednesday, Friday 11 – 11:50 AM, Beaven 118 Instructor: Professor Amber Hupp Office: Haberlin 335 Telephone: 508-793-2502 Email: [email protected] Office Hours: Tuesday 1 – 3 PM, Wednesday 1 – 2 PM, Thursday 2 – 3 PM, Friday 2 – 3 PM, or by appointment Laboratory: Monday 1 – 5 PM OR Tuesday 8 AM – 12 PM, Haberlin 319 Lab Supervisor: Antonet DeSouza-Goding Office: Haberlin 312 Email: [email protected] Office Hours: Monday 9:30 – 10:30 AM, Thursday 1 – 2 PM Required Course Material: Principles of Instrumental Analysis, 6th Ed., by Skoog, Holler, & Crouch Chemistry 300 Laboratory Manual (available on Moodle) Bound laboratory notebook (carbon-less are okay) USB flash drive (for lab data) Scientific Calculator (graphing type are okay) Moodle is accessible from: http://www.holycross.edu/login/ Course goals: This course will focus on key concepts of quantitative and instrumental methods of analysis. Students will learn about molecular and atomic spectroscopy, electrochemistry, separation science, and mass spectrometry. Lecture and laboratory work will emphasize major analytical methods of analysis, instrumental design, and some method development. Students will learn how and why instruments are designed to operate according to specific criteria and should be able to make intelligent choices among several possible ways of solving an analytical problem. Prerequisites: Chemistry 231, Physics 111 or Physics 115 with laboratory (may be co-requisite) 1 Quizzes and Examinations: There will be two quizzes, three hourly examinations, and one final cumulative examination. See attached schedule for dates. Quizzes and exams will focus on lecture material, however, due to the integrated nature of the course, concepts and content from the laboratory portion will be included.
    [Show full text]