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Inorganic Syntheses
INORGANIC SYNTHESES Volume 27 .................... ................ Board of Directors JOHN P. FACKLER, JR. Texas A&M University BODlE E. DOUGLAS University of Pittsburgh SMITH L. HOLT, JR. Oklahoma State Uniuersity JAY H. WORRELL University of South Florida RUSSELL N. GRIMES University of Virginia ROBERT J. ANGELIC1 Iowa State University Future Volumes 28 ROBERT J. ANGELIC1 Iowa State University 29 RUSSELL N. GRIMES University of Virginia 30 LEONARD V. INTERRANTE Rensselaer Polytechnic Institute 31 ALLEN H. COWLEY University of Texas, Austin 32 MARCETTA Y. DARENSBOURG Texas A&M University International Associates MARTIN A. BENNETT Australian National University, Canberra FAUSTO CALDERAZZO University of Pisa E. 0. FISCHER Technical University. Munich JACK LEWIS Cambridge University LAMBERTO MALATESTA University of Milan RENE POILBLANC University of Toulouse HERBERT W. ROESKY University of Gottingen F. G. A. STONE University of Bristol GEOFFREY WILKINSON Imperial College of Science and Technology. London AKlO YAMAMOTO Tokyo Institute 01 Technology. Yokohama Editor-in-Chief ALVIN P. GINSBERG INORGANIC SYNTHESES Volume 27 A Wiley-Interscience Publication JOHN WILEY & SONS New York Chichester Brisbane Toronto Singapore A NOTE TO THE READER This book has been electronically reproduced from digital idormation stored at John Wiley h Sons, Inc. We are phased that the use of this new technology will enable us to keep works of enduring scholarly value in print as long as there is a reasonable demand for them. The content of this book is identical to previous printings. Published by John Wiley & Sons, Inc. Copyright $? 1990 Inorganic Syntheses, Inc. All rights reserved. Published simultaneously in Canada. Reproduction or translation of any part of this work beyond that permitted by Section 107 or 108 of the 1976 United States Copyright Act without the permission of the copyright owner is unlawful. -
INORGANIC SYNTHESES Volume 23 Board of Directors
INORGANIC SYNTHESES Volume 23 Board of Directors DUWARD F. SHRIVER Norrhwesrern University HENRY F. HOLZCLAW, JR. University of Nebraska BODIE E. DOUGLAS University of Pirrsburgh JAY H. WORRELL University of Sourh Florida JOHN P. FACKLER, JR. Texas A&M University SMITH L. HOLT, JR. Oklahoma State University Future Volumes 24 JEAN’NE SHREEVE University of Idaho 25 HERBERT D. KAESZ University of California, Los Angeles 26 HARRY R. ALLCOCK Pennsylvania State University 27 STEVEN D. ITTEL E. I. du Ponr de Nemours and Co. 28 ALVIN P. GINSBERG Bell Laboratories 29 ROBERT J. ANGELIC1 Iowa Srare University International Associates MARTIN A. BENNETT Australian National University FAUSTO CALDEWO University of Pisa E. 0. FISCHER Technische Universirar Miinchen SACK LEWIS Cambridge University LAMBERTO MALATESTA University of Milan RENE POILBLANC University of Toulouse HERBERT ROESKY University of Goningen F. G. A. STONE University of Brisrol GEOFFREY WILKINSON Imperial College of Science and Technology AKIO YAMAMOTO Tokyo Kogyo Daigaku (TokyoInstirure of Technology) Editor-in-Chief STANLEY KIRSCHNER Deportment of Chemistry Wayne State Universily Detroit, Michigan INORGANIC SYNTHESES Volume 23 A Wiley-Interscience Publication JOHN WILEY tk SONS New York Chichester Briskne Toronto Singapore Published by John Wiley & Sons, Inc. Copyright 0 1985 by Inorganic Syntheses, Inc. All rights reserved. Published simultaneously in Canada. Reproduction or translation of any part of this work beyond that permitted by Section 107 or 108 of the 1976 United States Copyright Act without the permission of the copyright owner is unlawful. Requests for permission or further information should be addressed to the Permissions Department, John Wiley & Sons, Inc. Library of Congress Caralog Number: 39-23015 ISBN 0-471-81873-9 Printed in the United States of America 10 9 8 7 6 5 4 3 2 I HARRYR. -
INORGANIC SYNTHESES Volume 32
INORGANIC SYNTHESES Volume 32 ....... Board of Directors BODIE E. DOUGLAS University of Pittsburgh HERBERT D. KAESZ University of California, Los Angeles DARY LE H. BUSCH University of Kansas JAY H. WORRELL University of South Florida RUSSELL N. GRIMES University of Virginia ROBERT J. ANGELIC1 lowa State University DONALD W. MURPHY AT&T Bell Laboratories LEONARD V. INTERRANTE Rensselaer Polytechnic Institute ALAN H. COWLEY University of Texas, Austin Future Volumes 33 DIMITRI COUCOUVANIS University of Michigan 34 JOHN R. SHAPLEY University of Illinois, Urbana 35 TOBIN MARKS Northwestern University 36 RICHARD J. LAGOW University of Texas, Austin International Associates MARTIN A. BENNETT Australian National University, Canberra FAUSTO CALDERAZZO University of Pisa E. 0. FISCHER Technical University, Munich M. L. H. GREEN Oxford University JACK LEWIS Cambridge University LAMBERTO MALATESTA University of Milan RENE POILBLANC University of Toulouse HERBERT W. ROESKY University of Gottingen F. G. A. STONE Baylor University H. VAHRENKAMP University of Freiburg AKIO YAMAMOTO Tokyo Institute of Technology Editor-in-Chief MARCETTA YORK DARENSBOURG ....................Texas A&M University .......... INORGANIC SYNTHESES Volume 32 A Wiley-Interscience Publication JOHN WILEY & SONS, INC. New York Chichester Weinheim Brisbane Singapore Toronto This book is printed on acid-fee paper. @ Copyright 0 1998 by John Wiley & Sons, Inc. All rights reserved. Published simultaneously in Canada. No part of this publication may be reproduced, stored in a retrieval system or transmitted in any form or by any means, electronic, mechanical, photocopying, recording, scanning or otherwise, except as permitted under Sections 107 or 108 of the 1976 United States Copyright Act, without either the prior written permission of the Publisher, or authorization through payment of the appropriate per-copy fee to the Copyright Clearance Center, 222 Rosewood Drive, Danvers, MA 01923, (508) 750-8400, fax (508) 750-4744. -
INORGANIC SYNTHESES Volume 25 Board of Directors
INORGANIC SYNTHESES Volume 25 Board of Directors J,OHN P. FACKLER, JR. Texas A&M University BODIE E. DOUGLAS University of Pittsburgh SMITH L. HOLT, JR. Oklahoma State University JAY H. WORRELL University of South Florida STANLEY KIRSCHNER Wayne State University JEAN'NE M. SHREEVE, University of Idaho Future Volumes 26 HERBERT D. KAESZ University of California, Los Angela 27 ALVIN P. GINSBURG AT&T Bell Laboratories 28 ROBERT J. ANGELIC1 Iowa State University 29 RUSSELL N. GRIMES University of Virginia 30 LEONARD V. INTERRANTE Rensselaer Polytechnic Institute International Associates MARTIN A. BENNETT Australian National University, Canberra FAUSTO CALDERAZZO University of Pisa E. 0. FISCHER Technicnl University, Munich JACK LEWIS Cambridge University LAMBERTO MALATESTA University of Milan RENE POILBLANC University of Toulouse HERBERT W. ROESKY University of Gottingen F. G. A. STONE University of Bristol GEOFFREY WILKINSON Imperial College of Science and Technology, London AKIO YAMAMOTO Tokyo Institute of Technology, Yokohama Editor-in-Chief HARRY R. ALLCOCK Department of Chemistry Pennsylvania State University INORGANIC SYNTHESES Volume 25 A Wiley-Interscience Publication JOHN WILEY & SONS New York Chichester Brisbane Toronto Singapore Published by John Wiley & Sons, Inc. Copyright 0 1989 Inorganic Syntheses, Inc. All rights reserved. Published simultaneously in Canada. Reproduction or translation of any part of this work beyond that permitted by Section 107 or 108 of the 1976 United States Copyright Act without the permission of the copyright owner is unlawful. Requests for permission or further information should be addressed to the Permissions Department, John Wiley & Sons, Inc. Libnuy of Congnss Catalog Nunk:39-23015 ISBN 0-471-61874-8 Printed in the United States of America 10 9 8 7 6 5 4 3 2 1 This volume is dedicated to W. -
Inorganic Syntheses, Volume 33
Inorganic Syntheses, Volume 33. Edited by Dimitri Coucouvanis Copyright # 2002 John Wiley & Sons, Inc. ISBNs: 0-471-20825-6 (Hardback); 0-471-22450-2 (Electronic) INORGANIC SYNTHESES Volume 33 Board of Directors BODIE E. DOUGLAS University of Pittsburgh HERBERT D. KAESZ University of California, Los Angeles DARYLE H. BUSCH University of Kansas JAY H. WORRELL University of South Florida RUSSELL N. GRIMES University of Virginia ROBERT J. ANGELICI Iowa State University DONALD W. MURPHY AT&T Bell Laboratories LEONARD V. INTERRANTE Rensselaer Polytechnic Institute ALAN H. COWLEY University of Texas, Austin Future Volumes 34 JOHN R. SHAPLEY University of Illinois, Urbana 35 ALFRED SATTELBERGER Los Alamos National Lab 36 TOM RAUCHFUSS University of Illinois 37 TOBIN MARKS Northwestern University 38 LOU PIGNOLET University of Minnesota International Associates MARTIN A. BENNETT Australian National University, Canberra FAUSTO CALDERAZZO University of Pisa E. O. FISCHER Technical University, Munich M. L. H. GREEN Oxford University JACK LEWIS Cambridge University LAMBERTO MALATESTA University of Milan RENE POILBLANC University of Toulouse HERBERT W. ROESKY University of Go¨ttingen WARREN R. ROPER University of Auckland F. G. A. STONE Baylor University JAN REEDIJK Leiden University H. VAHRENKAMP University of Freiburg AKIO YAMAMOTO Tokyo Institute of Technology Editor-in-Chief DIMITRI COUCOUVANIS University of Michigan INORGANIC SYNTHESES Volume 33 A Wiley-Interscience Publication JOHN WILEY & SONS, INC. Designations used by companies to distinguish their products are often claimed as trademarks. In all instances where John Wiley & Sons, Inc., is aware of a claim, the product names appear in initial capital or ALL CAPITAL LETTERS. Readers, however, should contact the appropriate companies for more complete information regarding trademarks and registration. -
Inorganic-Synthesis19.Pdf
INORGANIC SYNTHESES Volume XIX Board of Directors W. CONARD FERNELIUS Kent Srate University WILLIAM L. JOLLY University of California HENRY F. HOLTZCLAW University ofNebraska JAY H. WORRELL University of South Florida FRED BASOLO Northwestern University ALAN G. MACDIARMID University ofPennsylvania BODIE E. DOUGLAS University of P irtsburgh Future Volumes XX DaryleH.Busch XXI John P. Fackler, Jr. XXII Smith L. Holt International Associates E. 0. FISCHER Technische Universitut (Munich) JACK LEWIS Cambridge University LAMBERTO MALATESTA University of Mifan F. G. A. STONE Brisrof University GEOFFREY WILKINSON Imperial College ofScience and Technology (London) AKIO YAMMOTO Tokyo lnstirute of Technology (Yokahama) Editor-in Chief DUWARD F. SHRIVER Department of Chemistry Northwestern University Evanston,.................... Illinois 60201 ..~................ INORGANIC SYNTHESES Volume XIX A Wiley-Interscience Publication JOHN WILEY & SONS New York Chichester Brisbane Toronto Published by John Wiley & Sons, Inc. Copyright @ 1979 Inorganic Syntheses, Inc All rights reserved. Published simultaneously in Canada. Repmduction or translation of any part of this work beyond that permitted by Sections 107 or 108 of the 1976 United States Copyright Act without the permission of the copyright owner is unlawful. Requests for permission or further information should be addressed to the Permissions Department, John Wiley & Sons, Inc. Library of Congress Cotalog Number: 39-23OI5 ISBN 0471-04542-X Printed in the United States of America I0987654321 PREFACE The wide range of synthetic techniques and compounds described here reflects the diversity of current inorganic chemistry. For example, the recent enthusiasm among inorganic chemists and solid-state physicists for studying anisotropic electronic conductors and fast-ion conductors is represented by a collection of syntheses for linear-chain conductors, layered tantalum sulfide intercalation compounds, and derivatives of the ionic conductor 0-alumina. -
INORGANIC SYNTHESES Volume XXI
INORGANIC SYNTHESES Volume XXI .................... .*..................... Board of Directors HENRY F. HOLTZCLAW University of Nebrusku JAY H. WORRELL University of South Florida BODlE E. DOUGLAS University of Pittsbuurgh DUWARD F. SHRIVER Northwestern University DARYLE H. BUSCH Ohio Stute University Future Volumes XXII SMITH L. HOLT Oklahoma State University XXIII STANLEY KIRSCHNER WuyneStute University XXIV JEAN'NE M. SHREEVE University of Iduho XXV HERBERT D. KAESZ University of Culiforniu,Los Angeles International Associates E. 0. FISCHER Technische Universitat Munich JACK LEWIS Cambridge University LAMBERTO MALATESTA University of Milun F. G. A. STONE Universftyof Bristol GEOFFREY WILKINSON Imperiul College of Science und Technology London AKIO YAMAMOTO TokyoInstitute of Technology Yokohamu MARTIN A. BENNETT Austruliun Nutionul University R. POILBLANC Nation01 Center for Scientifc Research Toulouse H. W. ROESKY University Gottingen Editor-inChief JOHN P. FACKLER, JR. Department of Chemistry ....................Case Western Reserve....................... University INORGANIC SYNTHESES Volume XXI A Wiley-Interscience Publication JOHN WILEY & SONS New York Chichester Brisbane Toronto Singapore Published by John Wiley & Sons, Inc. Copyright 0 1982 Inorganic Syntheses, Inc. All rights reserved. Published simultaneously in Canada. Reproduction or translation of any part of this work beyond that permitted by Section 107 or 108 of the 1976 United States Copyright Act without the permission of the copyright owner is unlawful. Requests for permission or further information should be addressed to the Permissions Department, John Wiley & Sons, Inc. Library of Congress Catalog Number: 39-23015 ISBN 0-471 -86520-6 Printed in the United States of America 10 9 8 7 6 5 4 3 2 1 PREFACE Inorganic Syntheses continues to fulfill a vital role for inorganic chemists and other users of inorganic and organometallic materials.