the Standards Have Been Withdrawn (Implemented by the Laboratory for a Transitional Period)

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the Standards Have Been Withdrawn (Implemented by the Laboratory for a Transitional Period)

Hellenic Accreditation System

Annex F1/15 to the Certificate No 46-4 SCOPE of ACCREDITATION of the Testing Laboratory of the “CHΕMICOTECHNIKI”, Lagouvardou - Spantidaki Co.

Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

Chemical tests

In House Method ΝΧ_14 1. Water 1. Nephelometric determination of Turbidity based on APHA* 2130 B, 22th Ed., 2012  Potable  Surface and 2. Determination of pH ΕΛΟΤ 658:1983 Groundwater for human 3. Determination of Conductivity Μ 2510, APHA*, 22th Ed., 2012 consumption or not 4. Determination of Total Hardness ISO 6059:1984 ΕΛΟΤ EN ISO 9963-1:1996 (Water quality – Determination 5. Determination of Total and Composite Alkalinity of alkalinity-Part 1 : Determination of total and composite alkalinity) 6. Determination of Calcium ΕΛΟΤ 169:1978 APHA*3500-Μg B, 7. Determination of Magnesium 22th Ed., 2012 8. Determination of Potassium In House Method NΧ_20 with spectrophotometry ICP-OES 9. Determination of Sodium Calculated parameter (Αccording 10. Calculation of Sodium Absorption Ratio, SAR to U.S. Dept.of Agriculture, Handbook No 60, 1954) 11. Determination of Chlorides ΕΛΟΤ 666:1983 (Argentometric method)

Page 1 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products In House Method ΝΧ_17 based 1. Water 2- 12. Determination of Sulfates on APHA* 4500-SO4 E, 22th  Potable Ed., 2012 M 4500-NO -Β, APHA*, 22th  Surface and 13. Determination of Nitrates 3 Groundwater for Ed., 2012 (Screening method) human M 4500-ΝΟ -B APHA*, consumption or not 14. Determination of Nitrites 2 22th Ed., 2012 In House method ΝΧ_05 15. Determination of Ammonium (Spectrophotometric method using Nesslerization) In House method ΝΧ_07 (Colorimetric method using 16. Determination of free Chloride and total Chloride N,N-diethyl-1,4- phenylenediamine for routine control purposes) 17. Determination of Total Suspended Solids, TSS APHA 2540 D, 22th Ed., 2012 (103 – 105 οC) In House Method ΛΜΧ_04 18. Determination of Chemical Oxygen Demand, COD based on ISO 15705 , APHA* 5220D, EPA 410.4 In House Method ΛΜΧ_14 19. Determination of Biochemical Oxygen Demand, based on APHA 5210 D, BOD 5 22th Edition 2012 In House Method ΝΧ_12 20. Determination of Phosphates based on ISO 6878, APHA* 4500-Ρ, EPA 365.2+3 In House Method ΝΧ_18 21. Determination of Total Nitrogen based on EN ISO 11905-1 In House Method ΝΧ_13 22. Determination of Ammonium Nitrogen based on ISO 7150/1 ,

APHA* 4500-ΝΗ3, EPA 350.1 In House Method ΝΧ_16 23. Determination of Fluoride based on APHA* 4500-F E, 22th Ed., 2012 2. Potable Water and 1. Determination of Chromium(VI) ISO 18412:2005 Groundwater In House Method ΛΜΧ_06 3. Sea water 1. Determination of Total Phosphorus based on ISO 6878, APHA* 4500-Ρ, EPA 365.2+3 In House Method ΛΜΧ_09 2. Determination of Ammonium Nitrogen based on ISO 7150/1,

APHA* 4500-ΝΗ3, EPA 350.1

4. Waste water 1. Determination of pH ΕΛΟΤ 658:1983 2. Determination of Conductivity Μ 2510, APHA*, 22th Ed., 2012 3. Nephelometric determination of Turbidity In House Method ΛΜΧ_10 based on APHA* 2130 B,

Page 2 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

22th Ed., 2012

M 4500-ΝΟ -B APHA*, 4. Determination of Nitrites 2 22th Ed., 2012

5. Determination of Total Hardness In House Method ΛΜΧ_19 based on ISO 6059:1984 6. Determination of Calcium In House Method ΛΜΧ_16 based on ΕΛΟΤ 169:1978 In House Method ΛΜΧ_17 7. Determination of Magnesium based on 3500-Μg B ΑΡΗΑ 22th edition 2012

8. Determination of Chlorides- In House Method ΛΜΧ_18 based on ΕΛΟΤ 666:1983 1. Determination of Total Suspended Solids, TSS 5. Waste water & APHA 2540 D, 22th Ed., 2012 (103 – 105 οC) Wastes 2. Determination of Chemical Oxygen Demand, In House Method ΛΜΧ_04 COD based on ISO 15705, APHA* 5220D, EPA 410.4 3. Determination of Biochemical Oxygen Demand, In House Method ΛΜΧ_14 BOD based on APHA 5210 D, 5 22th Edition 2012 ΕΛΟΤ EN ISO 9963.01:1996 (Water quality – Determination 4. Determination of Total and Composite Alkalinity of alkalinity-Part 1 : Determination of total and composite alkalinity) In House Method ΛΜΧ_06 5. Determination of Total Phosphorus based on ISO 6878, APHA* 4500-Ρ, EPA 365.2+3 In House Method ΛΜΧ_07 6. Determination of Phosphates based on ISO 6878, APHA* 4500-Ρ, EPA 365.2+3

7. Determination of Total Nitrogen In House Method ΛΜΧ_12 based on EN ISO 11905-1

8. Determination of Nitrogen Nitrate, ΝΟ3-Ν In House Method ΛΜΧ_15 In House Method ΛΜΧ_09 9. Determination of Ammonium Nitrogen based on ISO 7150/1,

APHA* 4500-ΝΗ3, EPA 350.1 In House Method ΛΜΧ_11 10. Determination of Fluoride based on APHA* 4500-F E, 22th Ed., 2012 In House Method ΛΜΧ_13 5. Waste water & (Photometric determination using Wastes 11. Determination of Free and Total Chlorine N, N-diethyl-1,4- (cont.) phenylenediamine for routine control purposes) 1. Determination of Aluminium, Al

Page 3 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

6. Water, 2. Determination of Arsenic, As Waste water, 3. Determination of Boron, B Reuse water 4. Determination of Barium, Ba (of low organic load without digestion) 5. Determination of Beryllium, Be 6. Determination of Cadmium, Cd

7. Determination of Cobalt, Co

8. Determination of Chromium, Cr

9. Determination of Copper, Cu

10. Determination of Iron, Fe In House Method NΧ_19 with 11. Determination of Lithium, Li spectrophotometry ICP-OES 12. Determination of Manganese, Mn

13. Determination of Molybdenum, Mo

14. Determination of Nickel, Ni

15. Determination of Lead, Pb

16. Determination of Antimony, Sb

17. Determination of Selenium, Se

18. Determination of Strontium, Sr

19. Determination of Vanadium, V

20. Determination of Zinc, Zn

21. Determination of Potassium In House Method ΛΜΧ_20 with spectrophotometry ICP-OES 22. Determination of Sodium Calculated parameter (Αccording 23. Calculation of Sodium Absorption Ratio, SAR to U.S. Dept.of Agriculture, Handbook No 60, 1954)

7. Sludge - Sediments, 1. Determination of Total Solids (103 οC– 105 οC) APHA 2540 G, 22th Ed., 2012 Solid wastes 2. Determination of Volatile Solids (550 οC)

Page 4 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products 8. Water 1. Residue-determination of agricultural drugs:  Potable Acetamiprid, Acibenzolar-S-methyl, Alachlor, Alanycarb,  Surface and Aldicarb-sulfone (Aldoxycarb), Ametryn, Atrazine, Azaconazole, Azamethiphos, Azoxystrobin, Benalaxyl, Groundwater for Benthiavalicarb-isopropyl, Bifenox, Bitertanol, Boscalid, human Bromacil, Bromoxynil, Bromuconazole, Bupirimate, Buprofezin, consumption or Butralin, Buturon, Carbaryl (NAC), Carbendazim, Carbofuran, not Carbofuran-3-hydroxy (3-Hydroxycarbofuran), Carbophenothion Carpropamid, Chlorfenvinphos, Chlorpyrifos, Chlorpyrifos- methyl, Climbazole, Clodinafop-propargyl, Clomazone, Cloquintocet-mexyl, Clothianidin, Coumaphos, Cyazofamid, Cymoxanil, Cyproconazole, Cyprodinil, Deet, Desmetryn, Diazinon, Diclobutrazol, Diclosulam, Dicrotophos, Diethofencarb, Difenoconazole, Diflubenzuron, Dimethoate, Dimethomorph, Dimoxystrobin, Diniconazole, Dinocap, Diuron (DCMU), DMST, Epoxiconazole, Ethiofencarb-sulfoxide, Ethion, Etrimfos, Fenamidone, Fenamiphos-sulfoxide, Fenarimol, Fenbuconazole, Fenoxycarb, Fenthion-oxon-sulfone, Fenthion-sulfone, Fludioxonil, Flufenacet, Fluquinconazole, In House multi-residue method Flusilazole, Flutolanil, Fosthiazate, Furathiocarb, Hexaconazole, NXO_02 employing Liquid Hexaflumuron, Hexythiazox, Imazalil, Imidacloprid, Indoxacarb, Chromatography-Mass Isoprothiolane, Isoxathion, Kresoxim-methyl, Linuron, Spectrometry LC-MS/MS Malaoxon, Malathion, Mefenacet, Mepanipyrim, Mephosfolan, Mepronil, Metalaxyl, Metalaxyl-M, Metconazole, Methidathion, Methoxyfenozide, Metolachlor, Metoxuron, Monocrotophos, Monolinuron, Myclobutanil, Nuarimol, Oxadixyl, Oxycarboxin, Oxydemeton-methyl, Paclobutrazol, Paraoxon-ethyl, Paraoxon- methyl, Penconazole, Pencycuron, Pendimethalin, Phenthoate, Phorate-sulfone, Phorate-sulfoxide, Phosalone, Phosmet, Phosphamidon, Picolinafen, Picoxystrobin, Piperonyl-butoxide, Pirimicarb, Pirimicarb-desmethyl, Pirimiphos-methyl, Prochloraz, Profenofos, Prometryn, Propachlor, Propanil, Propargite, Propiconazole, Propoxur, Propyzamide, Pyraclostrobin, Pyrazophos, Pyridaphenthion, Pyrifenox, Pyrimethanil, Pyriproxyfen, Quinalphos, Quinoxyfen, Quizalofop-ethyl, Quizalofop-methyl, Quizalofop-P-ethyl, Rotenone, Simazine, Tebuconazole, Teflubenzuron, Terbuthylazine, Terbutryn, Tetraconazole, Thiacloprid, Thionazin, Tolclofos-methyl, Triadimefon, Triadimenol, Triasulfuron, Triazamate, Triazophos, Trifloxystrobin, Triflumizole, Triflumuron 2. Residue-determination of agricultural drugs: 3-Hydroxycarbofuran, Acetamiprid, Acetochlor, Acibenzolar-S- methyl, Alachlor, alpha-BHC, Ametryn, Amitraz, Atrazine, Azaconazole, Azinphos-ethyl, Azinphos-methyl, Azoxystrobin, Benalaxyl, Bendiocarb, Benfuracarb, beta-BHC, beta- In House multi-residue method Endosulfan, Bifenazate, Bifenox, Bifenthrin, Bitertanol, NXO_02 employing Gas Boscalid, Bromacil, Bromophos, Bromophos-ethyl, Chromatography-Mass Bromopropylate, Bromuconazole, Bupirimate, Buprofezin, Spectrometry GC-MS/MS Carbofuran, Carbophenothion, Carbosulfan, Carfentrazone-ethyl, Chlorfenson, Chlorpropham, Chlorpyrifos, Chlorfenvinphos, Clomazone, Clothianidin, Coumaphos, Cyfluthrin beta, Cyproconazole, Cyprodinil, delta-BHC, Desmedipham deg., Dicloran, Diclobutrazol, Diclofop-methyl, Diclorvos, Dicofol 8. Water deg. (4,4'-Dichlorobenzophenone), Dicrotophos, Dieldrin,  Potable Diethofencarb, Difenoconazole, Dimethoate, Dimethomorph, Diniconazole, Endosulfan-alpha, Endosulfan sulfate,  Surface and Epoxiconazole, Ethion, Etofenprox, Etrimfos, Fenarimol, Groundwater for Fenitrothion, Fenvalerate, Fludioxonil, Flusilazole, Flutolanil, Page 5 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

human Fluvalinate, Heptachlor-exo-epoxide, Iprodione, lambda- consumption or Cyhalothrin, Leptophos, Linuron, Malathion, Metalaxyl, not Methidathion, Methoxychlor, Metolachlor, Myclobutanil, o,p'- DDD, o,p'-DDT, Oxyfluorfen, p,p'-DDD, p,p'-DDE, p,p'-DDT, (cont.) Paclobutrazol, Parathion, Parathion-methyl, Penconazole, In House multi-residue method Pendimethalin, Permethrin, Phenthoate, Phosalone, Phosmet, NXO_02 employing Gas Piperonyl butoxide, Pirimicarb, Pirimiphos-methyl, Chromatography-Mass Procymidone, Profenofos, Propachlor, Propanil, Propyzamide, Spectrometry GC-MS/MS Pyrazophos, Pyridafenthion, Pyrimethanil, Quinalphos, Tebuconazole, Tebufenpyrad, Tolclofos-methyl, trans- Chlordane, Triadimefon, Triadimenol, Triazophos, Tricyclazole, Triflumizol, Vinclozolin 3. Determination of trihalomethanes and halogenated volatile organic compounds in water.  Trihalomethanes Τribromomethane (Bromoform), In House Method with Gas Chromatography GC/ECD, Trichloromethane(Chloroform), based on Bromodichloromethane, Dibromochloromethane APHA 6232B, 22th Edition 2012  1,2 Dichloroethane  Trichloroethylene  Tetrachloroethylene 1. Residue-determination of agricultural drugs: 9. Waste water Acetamiprid, Acibenzolar-S-methyl, Alanycarb, Aldicarb- sulfone (Aldoxycarb), Ametryn, Atrazine, Azaconazole, Azamethiphos, Azinphos-methyl, Azoxystrobin, Benalaxyl, Benthiavalicarb-isopropyl, Bifenthrin, Bitertanol, Boscalid, Bromacil, Bromuconazole, Bupirimate, Buprofezin, Butralin, Buturon, Carbaryl (NAC), Carbendazim, Carbofuran, Carbofuran-3-hydroxy (3-Hydroxycarbofuran), Carbophenothion, Carpropamid, Chlorfenvinphos, Chlorpyrifos, Chlorpyrifos-methyl, Climbazole, Clodinafop-propargyl, Clofentezine, Clomazone, Cloquintocet-mexyl, Cloransulam- In House multi-residue method methyl, Clothianidin, Coumaphos, Cyazofamid, Cymoxanil, NXO_02 employing Liquid Cypermethrin, Cyproconazole, Cyprodinil, Deet, Deltamethrin, Demeton-S-methyl-sulfone, Desmetryn, Diazinon, Chromatography-Mass Diclobutrazol, Diclosulam, Dicrotophos, Diethofencarb, Spectrometry LC-MS/MS Difenoconazole, Diflubenzuron, Dimethoate, Dimethomorph, Dimoxystrobin, Diniconazole, Diuron (DCMU), DMST, Epoxiconazole, Ethion, Etofenprox, Etrimfos, Famoxadone, Fenamidone, (E)-Fenpyroximate, Fenarimol, Fenbuconazole, Fenoxycarb, Fenthion-oxon-sulfone, Fludioxonil, Flufenacet, Flufenoxuron, Fluquinconazole, Flusilazole, Flutolanil, Fosthiazate, Furathiocarb, Hexaconazole, Hexaflumuron, Hexythiazox, Indoxacarb, Iprovalicarb, Isoprothiolane, Isoxathion, Kresoxim-methyl, Lambda-Cyhalothrin, Linuron, Malaoxon, Malathion, Mefenacet, Mepanipyrim, Mephosfolan, Mepronil, Metalaxyl, Metalaxyl-M, Metconazole, Methidathion, Methiocarb-sulfoxide, Methomyl, Methoxyfenozide, 9. Waste water Metolachlor, Metoxuron, Monocrotophos, Monolinuron, Myclobutanil, Nuarimol, Oxadixyl, Oxamyl, Oxycarboxin, (cont.) Paclobutrazol, Paraoxon-ethyl, Paraoxon-methyl, Penconazole, Pencycuron, Permethrin, Phenthoate, Phorate-sulfone, Phorate- sulfoxide, Phosalone, Phosmet, Phosphamidon, Picolinafen, Picoxystrobin, Piperonyl-butoxide, Pirimicarb, Pirimicarb- In House multi-residue method

Page 6 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

desmethyl, Pirimiphos-methyl, Prochloraz, Profenofos, Prometryn, Propanil, Propargite, Propiconazole, Propoxur, Propyzamide, Pyraclostrobin, Pyrazophos, Pyridaphenthion, Pyrifenox, Pyrimethanil, Pyriproxyfen, Quinalphos, Quinoxyfen, NXO_02 employing Liquid Quizalofop-ethyl, Quizalofop-methyl, Quizalofop-P-ethyl, Chromatography-Mass Rotenone, Tau-Fluvalinate, Tebuconazole, Tebufenozide, Spectrometry LC-MS/MS Teflubenzuron, Terbuthylazine, Terbutryn, Tetraconazole, Thiabendazole, Thiacloprid, Thiamethoxam, Thidiazuron, Triadimefon, Triadimenol, Triasulfuron, Triazamate, Triazophos, Trifloxystrobin, Triflumizole, Triflumuron

Commission Regulation (EEC) 10. Olive Oil – Olive 2568/91 (Annex ΙΙ) 1. Determination of Acidity Pomace oils & COI/T.20/Doc. No 34 as in force

Commission Regulation (EEC) 2. Absorption coefficient K for λ=232 nm and 268 nm and 2568/91 (Annex ΙX) Absorption coefficient difference (ΔΚ) & COI/T.20/Doc. No 19 as in force

Commission Regulation (EEC) 2568/91 (Annex XX) 3. Determination of Waxes - Alkylesters & COI/T.20/Doc. No 28 as in force

Commission Regulation (EEC) 4. Determination of the difference between actual and 2568/91 (Annex XVIII) theoretical content of triacylglycerols with ECN 42 & COI/T.20/Doc. No 20 as in force

Commission Regulation (EEC) 5. Determination of the composition of Sterols and 2568/91 (Annex V) triterpene Dialcohols & COI/T.20/Doc. No 30 as in force

Commission Regulation (EEC) 2568/91 (Annex IV) 6. Determination of the Aliphatic Alcohols & COI/T.20/Doc. No 26 as in force

Commission Regulation (EEC) 7. Determination of the percentage content of 2-glycerol- 2568/91 (Annex VΙΙ) monopalmitate & COI/T.20/Doc. No 23 as in force

10. Olive Oil – Olive 8. Determination of the composition of di- and tri- Pomace oils acylglycerol by capillary column gas chromatography in COI/T.20/Doc. 32 (cont.) vegetable oils

Commission Regulation (EEC) 1. Determination of Peroxide value 2568/91 (Annex III) as in force

Page 7 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

2. Determination of moisture content and volatile in animal ISO 662:2016 and vegetable fats and oils 3. Determination of content of insoluble substances in ISO 663:2007 4th edition animal and vegetable fats and oils Commission Regulation (EEC) 2568/91 (Annex X) 4. Determination of methyl esters of fatty acids & COI/T.20/Doc. No 33 as in force 5. Determination of phthalates and adipate esters (Plasticisers) In house multiresidue method, benzyl-butyl-phthalate (BBP), bis-(2-ethylhexyl)-adipate ΛΧ_06, with Gas (DEHA), bis-(2-ethylhexyl)-phthalate (DEHP), dibutyl- Chromatography-Mass adipate (DBA), dibutyl-phthalate (DBP), diethyl-phthalate Spectometry GC-MS/MS. (DEP), diisobutyl-phthalate (DiBP), dimethyl-phthalate (DMP), di-n-octyl-phthalate (DnOP)

12. Vegetable oils Commission Regulation (EEC) 1. Determination of stigmastadienes 2568/91 (Annex XVII) & COI/T.20/Doc. No 11 as in force 1. Residue-determination of agricultural drugs: 13. Vegetable products high in fat: Acephate, Acetamiprid, Acibenzolar-S-methyl, Acrinathrin, Alachlor, Alanycarb, Aldicarb, Aldicarb-sulfone (Aldoxycarb),  Olive oil, Ametryn, Atrazine, Azaconazole, Azamethiphos, Azinphos- vegetable fats and methyl, Azoxystrobin, Benalaxyl, Benthiavalicarb-isopropyl, oils Bifenox, Bifenthrin, Bitertanol, Boscalid, Bromacil, Bromuconazole, Bupirimate, Buprofezin, Butocarboxim-  Olives, Avocado sulfoxide, Butralin, Buturon, Cadusafos, Carbaryl (NAC), etc. Carbofuran, Carbofuran-3-hydroxy (3-Hydroxycarbofuran),  Oil seeds (sesame, Carbofuran-3-keto,Carbophenothion, Carboxin, Carpropamid, Chlorfenvinphos, Chlorpyrifos,Chlorpyrifos-methyl, Clodinafop- soybean etc.) In house multi-residue method, propargyl, Clofentezine, Clomazone, Cloquintocet-mexyl, ΛΧ_05 employing Liquid Clothianidin, Coumaphos, Cyazofamid, Cycloate, Cymoxanil, Chromatography-Mass (ESYD G- Cypermethrin, Cyprodinil, Deet, Deltamethrin, Demeton-S- FYTOPROST/01/02/20- Spectometry LC-MS/MS, based methyl, Demeton-S-methyl-sulfone, Desmedipham, Desmetryn, on SANTE doc. 11945/2015 10-2016- Diazinon, Dichlorvos, Diclobutrazol, Dicrotophos, PRODUCT Diethofencarb, Difenoconazole, Diflubenzuron, Dimethoate, CATEGORY 4.2-4) Dimethomorph, Dimoxystrobin, Diniconazole, Diuron (DCMU), DMST, Epoxiconazole, Ethiofencarb-sulfoxide, Ethion, Etofenprox, Etrimfos, Fenamidone, Fenamiphos, Fenarimol, Fenbuconazole, Fenoxycarb, Fenpyroximate, Fenthion, Fenthion-oxon, Fenthion-oxon-sulfone, Fenthion-oxon- sulfoxide, Fenthion-sulfoxide, Fludioxonil, Flufenacet, Flufenoxuron, Fluquinconazole, Flusilazole, Flutolanil, Fosthiazate, Hexaconazole, Hexaflumuron, Hexythiazox, 13. Vegetable Imidacloprid, Indoxacarb, Iprovalicarb, Isoprothiolane, Isoxaflutole, Isoxathion, Kresoxim-methyl, Linuron, Malathion, products high in fat: Mefenacet, Mepanipyrim, Mephosfolan, Mepronil, Metalaxyl,  Olive oil, Metalaxyl-M, Metconazole, Methidathion, Methiocarb, vegetable fats and Methiocarb-sulfone, Methiocarb-sulfoxide, Methomyl, oils Methoxyfenozide, Metolachlor, Monocrotophos, Monolinuron, Myclobutanil, Nuarimol, Omethoate, Oxadixyl, Oxamyl,  Olives, Avocado Oxycarboxin, Paclobutrazol, Paraoxon-ethyl, Paraoxon-methyl, etc. Penconazole, Pencycuron, Pendimethalin, Phenmedipham, Phenthoate, Phorate, Phorate-sulfone, Phorate-sulfoxide, In house multi-residue method,

Page 8 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

 Oil seeds (sesame, Phosalone, Phosmet, Phosphamidon, Picolinafen, Picoxystrobin, soybean etc.) Piperonyl-butoxide, Pirimicarb, Pirimicarb-desmethyl, Pirimiphos-methyl, Prochloraz, Profenofos, Prometryn, (ESYD G- Propachlor, Propanil, Propargite, Propiconazole, Propyzamide, Pyraclostrobin, Pyrazophos, Pyridaphenthion, Pyrifenox, FYTOPROST/01/02/20- ΛΧ_05 employing Liquid 10-2016- Pyrimethanil, Pyriproxyfen, Quinalphos, Quinoxyfen, Quizalofop-ethyl, Quizalofop-methyl, Quizalofop-P-ethyl, Chromatography-Mass PRODUCT Spectometry LC-MS/MS, based CATEGORY 4.2-4) Rotenone, Simazine, Spirodiclofen, Spiromesifen, Spinosyn A, Spinosyn D, Sulfotep, Tau-Fluvalinate, Tebuconazole, on SANTE doc. 11945/2015 (cont.) Tebufenozide, Teflubenzuron, Terbuthylazine, Terbutryn, Tetraconazole, Thiacloprid, Thiamethoxam, Thiofanox-sulfone, Thionazin, Tolclofos-methyl, Triadimefon, Triadimenol, Triazamate, Triazophos, Trifloxystrobin, Triflumizole, Triflumuron 2. Residue-determination of agricultural drugs: Acephate, Acetochlor, Acibenzolar-S-methyl, Acrinathrin, Alachlor, Aldrin, Ametryn, Amitraz, Atrazine, Azaconazole, Azamethiphos, Azinphos ethyl, Azinphos-methyl, Benalaxyl, Bendiocarb, Benfluralin, Bifenazate, Bifenthrin, Biphenyl, Bitertanol, Boscalid, Bromacil, Bromophos ethyl, Bromophos methyl, Bromopropylate, Bromuconazole, Bupirimate, Buprofezin, Butralin, Cadusafos, Carbofuran, Carbophenothion, Carbosulfan, Carboxin, Carfentrazone-ethyl, Chlordane-cis, Chlordane-trans, Chlorfenson, Chlorfenvinphos, Chloroneb, Chlorpropham, Chlorpyrifos ethyl, Chlorpyrifos methyl, Clomazone, Clothianidin, Coumaphos, Cyfluthrin-beta, Cyhalothrin-lamda, Cypermethrin, Cypermethrin-alpha, Cyproconazole, Cyprodinil, DDD-o,p', DDD-p,p', DDE-p,p', DDT-pp’, Deltamethrin, Diazinon, Dichlobenil, Dichloran, Dichlorvos, Diclobutrazol, Diclofop-methyl, Dicloran, Dicofol (deg. DCBP), Dicofol deg. (4,4'-Dichlorobenzophenone), Dieldrin, Diethofencarb, Difenoconazole, Dimethoate, In house multi-residue method, Dimethomorph, Diniconazole, Endosulfan – alpha, Endosulfan – ΛΧ_05 employing Gas beta, Endosulfan sulfate, Endrin-ketone, Epoxiconazole, Ethion, Chromatography-Mass Ethoprophos, Etofenprox, Etrimfos, Fenamiphos, Fenarimol, Spectometry GC-MS/MS, based Fenitrothion, Fenoxycarb, Fenthion, Fenthion Oxon, Fenthion on SANTE doc. 11945/2015 Oxon sulfone, Fenthion sulfone, Fenthion sulfoxide, Fenvalerate, Fludioxonil, Flusilazole, Flutolanil, Fluvalinate, HCH-alpha, HCH-beta, HCH-delta, HCH-gamma (lindane), Heptachlor, Heptachlor endo epoxide, Heptachlor exo epoxide, Iprodione, Kresoxim methyl, Leptophos, Malathion, Metalaxyl, Methamidophos, Methidathion, Methoxychlor, Metolachlor, Monocrotophos, Myclobutanil, Nitrofen, Omethoate, Oxyfluorfen, Paclobutrazol, Parathion, Parathion ethyl, Parathion methyl, Parathion-methyl, Penconazole, Pendimethalin, Permethrin, Phenthoate, Phorate, Phosalone, Phosmet, Phosphamidon, Piperonyl-butoxide, Pirimicarb, Pirimiphos methyl, Procymidone, Profenofos, Propachlor, Propanil, Propargite, Propyzamide, Pyrazophos, Pyridafenthion, Pyrimethanil, Pyriproxyfen, Quinalphos, Quintozene, Simazine, Tebuconazole, Tebufenpyrad, Tefluthrin, Terbuthylazine, Tetradifon, Tetramethrin, Tolclofos-methyl, Triadimefon, Triadimenol, Triazophos, Trifloxystrobin, Triflumizole, Trifluralin, Vinclozolin 12. Flour , Cereals & 1. Determination of Moisture Modified based on 925.09, 935.36 th Bakery Products (AOAC 17 Ed. 2003)

Page 9 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

Modified based on 923.03 2. Determination of Ash (AOAC 17th Ed. 2003)

Modified based on 991.20 3. Determination of Proteins (AOAC 17th Ed. 2003) & ISO 1871:2009

13. Milk & Dairy Modified based on 926.08 1. Determination of Moisture Products (AOAC 17th Ed. 2003)

Modified based on 935.42 (AOAC 17th Ed. 2003) cheese, 2. Determination of Ash 945.46 (AOAC 17th Ed. 2003) milk Modified based on 991.20 3. Determination of Proteins (AOAC 17th Ed. 2003) & ISO 1871:2009

Modified based on 950.46 14. Meat & Meat 1. Determination of Moisture (AOAC 17th Ed. 2003) Products

Modified based on 920.153 2. Determination of Ash (AOAC 17th Ed. 2003)

Modified based on 991.20 3. Determination of Proteins (AOAC 17th Ed. 2003) & ISO 1871:2009

15. Honey Modified based on 969.38 1. Determination of Moisture (AOAC 17th Ed. 2003)

Modified based on 920.181 2. Determination of Ash (AOAC 17th Ed. 2003)

Harmonised Methods of the 3. Determination of Diastase Activity International Honey Commission (2009), method 5.2

EU Regulation 2568/91 as 4. Determination of Hydroxymethylfurfural (HMF) amended and in force

In house multi-residue method, 16. Products with high Προσδιορισμός υπολειμμάτων γεωργικών φαρμάκων: TX_05, employing Gas sugar content: honey, Acephate, Acrinathrin, Alachlor, Aldrin, Amitraz, Chromatography-Mass jams etc. Atrazine, Azinphos ethyl, Azinphos methyl, Bromophos ethyl, Bromophos methyl, Bromopropylate, Cadusafos, Spectometry GC-MS/MS.  Honey Chlordane – cis, Chlordane – trans, Chlorfenvinphos,  Raisins Chlorpyrifos ethyl, Chlorpyrifos methyl, Coumaphos, Cyfluthrin-beta ,Cyhalothrin-lamda, Cypermethrin – alpha,  Jam DDD-pp’, DDE-pp’, DDT-pp’, Deltamethrin, Diazinon, Dichlorvos, Dicloran, Dicofol deg. (DCBP), Dieldrin,  Figs, molasses etc. Dimethoate, Endosulfan – alpha, Endosulfan – beta, (ESYD G- Endosulfan sulfate, Endrin ketone, Ethion, Ethoprophos, FYTOPROST/01/02/20- Fenarimol, Fenitrothion, Fenoxycarb, Fenthion, Fenthion 10-2016- sulfone, Fenthion sulfoxide, Fenvalerate , Fluvalinate,

Page 10 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products PRODUCT HCH-alpha, HCH-beta, HCH-gamma, HCH-delta, CATEGORY 4.2-3) Heptachlor, Heptachlor endo epoxide, Heptachlor exo epoxide, Iprodione, Kresoxim methyl, Malathion, Methidathion, Methoxychlor, Metolachlor, Monocrotophos, Nitrofen, Omethoate, Oxyfluorfen, Parathion ethyl, Parathion methyl, Pendimethalin, Permethrin, Phorate, Phosalone, Phosphamidon, Pirimicarb, Pirimiphos methyl, Procymidone, Propachlor, Propanil, Propyzamide, Pyrazophos, Pyriproxyfen, Quintozene, Simazine, Terbuthylazine, Triadimefon, Trifluralin, Vinclozolin

Modified based on 925.40 1. Determination of Moisture 17. Nuts & Nuts (AOAC 17th Ed. 2003) Products Modified based on 950.49 2. Determination of Ash (AOAC 17th Ed. 2003)

Modified based on 991.20 3. Determination of Proteins (AOAC 17th Ed. 2003) & ISO 1871:2009 Modified based on 925.45 1. Determination of Moisture 18. Sugar & Sugar (AOAC 17th Ed. 2003) Products Modified based on 900.02 2. Determination of Ash (AOAC 17th Ed. 2003)

Modified based on 991.20 3. Determination of Proteins (AOAC 17th Ed. 2003) & ISO 1871:2009 Modified based on 934.01 1. Determination of Moisture 19. Animal Feed (AOAC 17th Ed. 2003)

Modified based on 942.05 2. Determination of Ash (AOAC 17th Ed. 2003)

Modified based on 2001.11 3. Determination of Proteins (AOAC 17th Ed. 2003) & ISO 1871:2009

Physical tests

Thermistor cryoscope routine 1. Raw Milk 1. Determination of freezing point method, ISO 5764 | IDF 108: 2009, Annex C

Biochemical tests

Diffusion method 1. Detection of microbial inhibitors 1. Raw Milk DELVOTEST penicillin, penethamate, ambicillin, amoxicillin, nafcillin, SP NT cloxacillin, dicloxacillin, oxacillin, cefacetrile, cephalexin, cephalonium, cefoperazone, ceftiofur, cephapirin,

Page 11 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products

cefazolin, cefuroxime, doxycycline, sulfadimidine, sulfadimethoxine, sulfamerazine, sulfathiazole, sulfadiazine, sulphamethazine, sulphadoxine, sulphamethοxazole, tylosin, tilmicosin, gentamιcin, neomycin, paranomycin, chloramphenicol, dapsone, rifamixin, pirlimycin, trimethoprim

Microbiological tests

1. Food – Animal 1. Enumeration of microorganisms - Colony Count ISO 4833-1:2013 Feeding Stuffs technique at 300C 2. Enumeration of coliforms - Colony Count technique at ISO 4832:2006 300C

3. Enumeration of β-glucuronidase – positive E.coli ISO 16649-2:2001

4. Enumeration of coagulase- positive staphylococci ISO 6888.02:1999/Αmd 1:2003 (Staphylococcus aureus and other species) at 370C

5. Detection and enumeration of Enterobacteriaceae ISO 21528-2:2004 #

6. Salmonella spp : Detection (presence / absence) ISO 6579:2002 #

7.Listeria monocytogenes : Detection ISO 11290-1:1996/Amd 1:2004#

8. Enumeration of Listeria monocytogenes ISO 11290-2:1998/Amd 1:2004#

2. Food – Animal Feeding Stuffs with 1. Enumeration of yeasts and moulds ISO 21527-1 :2008

aw > 0.95 3. Food – Animal Feeding Stuffs with 1. Enumeration of yeasts and moulds ISO 21527-2 :2008

aw < 0.95

1. Detection and enumeration of Enterococci ΕΛΟΤ ΕΝ ISO 7899-2:2000 4. Surface, Drinking and Swimming 2. Enumeration of the total aerobic micro-organisms at ΕΛΟΤ ΕΝ ISO 6222:1999 pool waters 220 C and 370 C

3. Enumeration of Total Coliforms and E. coli ΕΛΟΤ ΕΝ ISO 9308-1:2014

4. Detection of presumptive Salmonella spp. ISO 19250:2010

5. Detection and enumeration of Pseudomonas ISO 16266:2006 aeruginosa

6. Detection and enumeration of Clostridium perfringens ISO 14189:2013

Page 12 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products 5. Water – Environmental 1. Detection and enumeration of Legionella spp. ISO 11731:1998 # samples

6. Sea Water 1. Enumeration of Total Coliforms ΕΛΟΤ ISO 9308-1:2014

2. Enumeration of Ε.coli ΕΛΟΤ ISO 9308-1:2014

3. Detection and enumeration of Intestinal Enterococci ΕΛΟΤ ISO 7899-2:2000

4. Detection of presumptive Salmonella spp. ISO 19250:2010

7. Water for 1. Enumeration of total culturable microorganisms at 20°C ISO 13959: 2014 hemodialysis and ± 3°C relevant treatments 8. Wastewater & 1. Detection and enumeration of Total Coliforms APHA* 9222B:2012 Wastes, Surface (Membrane Filtration procedure) Water 2. Detection and enumeration of Fecal Coliforms APHA* 9222D:2012 (Membrane Filtration procedure)

3. Detection and enumeration of Ε.coli APHA* 9222G:2012

4. Detection and enumeration of Intestinal Enterococci ISO 7899-2:2000

5. Detection of presumptive Salmonella spp. ISO 19250:2010

9. Animal faeces and in environmental ISO 6579:2002/Amd1:2007, samples from the 1. Detection of Salmonella spp. primary production ANNEX D stage

Sampling

1. Sampling for chemical parameters ISO 5667-1:2006 1. Drinking water, ISO 5667-3:2012 groundwater- ISO 5667-5:2006 surface waters, ISO 5667-9:1992 swimming pools, ISO 5667-10:1992 seawater, marine ISO 5667-14:2014

Page 13 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018 Tested materials/ Types of tests / Parameters to be measured Applied standards/methods products ISO 19458:2006 waters and waste ISO 5667-1:2006 waters ISO 5667-3:2012 ISO 5667-5:2006 2. Sampling for microbiological parameters ISO 5667-9:1992 ISO 5667-10:1992 ISO 5667-14:2014 Directive 2006/7/EC

2. Milk 1. Sampling for chemical and microbiological parameters ISO 707:2008

# The standards have been withdrawn (implemented by the laboratory for a transitional period).

* American Public Health Association, American Water Works Association, Water Environment Federation, “Standard Methods for the Examination of Water and Wastewater”, 22st Edition , 2012

Site of assessment: Permanent laboratory premises : 1 Dikonymou Makri Str.Ag. Markos 74100, Rethymno, Greece

Approved signatory: Afroditi Lagouvardou , Maria Spantidaki, Emmanouil Fafoutakis

This scope of Accreditation replaces the previous one dated 21.12.2017 The Accreditation Certificate No 46-4 to ELOT EN ISO/IEC 17025:2005 is valid until 26.11.2021.

Athens, 06.03.2018

Konstantinos Voutsinas Managing Director of E.SY.D.

Page 14 of 14 Annex F1/15 to the Certificate ESYD No 46-4 15.03.2018

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