P.O. Box 200, NL-3200 lab code: AE Spijkenisse the Netherlands ing R.J. Starink Tel.: +31 181 694541 Fax: +31 181 694543 E-mail: [email protected]
INTERLABORATORY STUDY IIS15P03 Phthalates in Plastics 2015
REPORT FORM A Report before May 29, 2015
Test results on sample #15065: Phthalate CAS no. unit Preferred no. results in %M/M #15065(**) of digits 28553-12-0 & 68515-48- DINP %M/M #.### 0 DBP 84-74-2 %M/M #.### BBP 85-68-7 %M/M #.### 26761-40-0 & 68515-49- DIDP %M/M #.### 1 DNOP 117-84-0 %M/M #.### DEHP 117-81-7 %M/M #.### DiBP 84-69-5 %M/M #.### DHP 84-75-3 %M/M #.### Other Phthalate(s) %M/M #.###
Test results on sample #15066: Phthalate CAS no. unit Preferred no. results in %M/M #15066(**) of digits 28553-12-0 & 68515-48- DINP %M/M #.### 0 DBP 84-74-2 %M/M #.### BBP 85-68-7 %M/M #.### 26761-40-0 & 68515-49- DIDP %M/M #.### 1 DNOP 117-84-0 %M/M #.### DEHP 117-81-7 %M/M #.### DiBP 84-69-5 %M/M #.### DHP 84-75-3 %M/M #.### Other Phthalate(s) %M/M #.### (**) See letter of instructions Please give the actual test method used (for example EN14372) :
Name of laboratory: Date of sample receipt:
City Country:
Name of contact person: Date of report:
NB Electronic version of the report form is available on our internet site www.iisnl.com P.O. Box 200, NL-3200 lab code: AE Spijkenisse the Netherlands ing R.J. Starink Tel.: +31 181 694541 Fax: +31 181 694543 E-mail: [email protected]
INTERLABORATORY STUDY IIS15P03 Phthalates in Plastics 2015
REPORT FORM B Report before May 29, 2015
Additional details for sample #15065:
What was the type of plastic? (for example PE, PP, PVC, ..)
How was the type of plastic identified?
Was the sample grinded or cut before analysis?
What was the final particle size before use?
Which technique was used to release/extract the phthalate? eg. Soxhlet, Ultrasonic or other.
Which extraction solvent was used? E.g. THF, DEE or other.
Additional details for sample #15066:
What was the type of plastic? (for example PE, PP, PVC, ..)
How was the type plastic identified?
Was the sample grinded or cut before analysis?
What was the final particle size before use?
Which technique was used to release/extract the phthalate? eg. Soxhlet, Ultrasonic or other.
Which extraction solvent was used? E.g. THF, DEE or other.
Name of laboratory: Date of sample receipt:
City: Country:
Name of contact person: Date of report:
NB Electronic version of the report form is available on our internet site www.iisnl.com P.O. Box 200, NL-3200 AE Spijkenisse, the Netherlands ing R.J. Starink Tel.: +31 181 694541 Fax: +31 181 694543 E-mail: [email protected]
INTERLABORATORY STUDY IIS15P03 Phthalates in Plastics 2015
INSTRUCTIONS TO PARTICIPANTS
Please confirm sample receipt as soon as you have received and checked the contents of this package, preferably using the fax form that you receive together with this package. Please complete the form and send it to iis (email [email protected] or fax no. + 31 181 69 4543).
This interlaboratory study concerns 2 different samples, you receive for each sample (#15065 and #15066) approx. 3 grams for determination of number of individual phthalates. Please treat each sample as if it is a routine sample.
DINP = Diisononylphthalate (CAS nos. 28553-12-0 & 68515-48-0) DBP = Dibutylphthalate (CAS no. 84-74-2) BBP = Benzylbutylphthalate (CAS no. 85-68-7) DIDP = Diisodecylphthalate (CAS nos. 26761-40-0 & 68515-49-1) DNOP = Dioctylphthalate (CAS no. 117-84-0) DEHP = Bis 2-ethylhexylphthalate (CAS no. 117-81-7) DiBP = Diisobutylphthalate (CAS no. 84-69-5) DHP = Dihexylphthalate (CAS no. 84-75-3)
Each laboratory is requested to analyse the samples in the way it would normally do in day-to-day circumstances.
Please report your analytical test results using the indicated units on the report form and the requested minimum number of significant digits. Preferably unrounded results are used for the statistical evaluation. Please do not report ‘less than’-results which are above your detection limit. Results reported as ‘less than’ cannot be used for meaningful statistical calculations.
Please complete the report forms A & B with the requested details of the analysis performed.
In order to avoid mix-up of test results we have added a box for your laboratory code. Please understand that it is not mandatory to use, but it will facilitate identification of your test results.
Please return the completed report form to iis preferably one week after sample receipt, but in any case before the indicated closing date: MAY 29, 2015 (preferably by email).
If you have any remarks/questions please contact: ing R.J. Starink, Institute for Interlaboratory Studies P.O. box 200, NL-3200 AE Spijkenisse, the Netherlands tel.no. + 31 181 69 4541, fax.no. + 31 181 69 4543 e-mail: [email protected]
NB Electronic version of the report form is available on our internet site www.iisnl.com