Detailed Procedure for the Microwaves Reactor to Treat a Samples Odf Dioxane Water HCL
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Detailed procedure for the microwaves Reactor to treat a samples odf Dioxane water HCL at 80 degrees.
*Who will run the microwave needs to make four treatments:
*First you have to turn on the microwave, check the welcome message if there is any errors were happened, check the water cycle.
*second select if you want to run it manually or automatically, in this case automatic is better so u will control all conditions by using the three keys in the left .
*the first key will help you to choose the number of the flask form 1 to 16* the second key will help you to choose the treatment number from 1 to 16
*the third is to a make sequence changes in the microwave power and the time and the cooling or waiting time.
* And you will use the system key to choose which flask you will begin with.
*so if you will do one acidolysis process chooses one number( e. g. 1)
*after that press the first key choose number one
* press the 2nd choose the first treatment:
*press the third key: under this, u will make a sequence as shown:
P0=10 T0=3 P1= 1 T1=7
P2=5 T2=3 P3=1 T3=7
W= 7
*press the second key again chooses treatment number 2
*press the third one and do: P0=10 T0=3 P1=1 T1=8
P2=5 T2=3 P3=1 T3=8
W=7
*press the 2 nd key and choose the third treatment
*press the third and do so:
P0=10 T0=2 P1=1 T1=7
P2=5 T2=3 P3=1 T3=7
W= 8.3(500 sec)
*press the 2nd key and choose the forth treatment
*press the third and do so;
P0= 10 T0=3 P1=1 T1=7
P2=5 T2=3 P3=1 T3=7
W=00
*P= microwave power percent, T= time in minute, W= waiting time
1. The mixture composition that you are heating 2 g OD crude lignin, in 60mL aqueous doixane 2. The volume of the material you are heating and the size of the reaction flask , the big one of the device, 100 mL 3. A Scanned PDF version photocopy of the diagram of the keys (from the manual of the machine) indicating the location of the various keys you are referring to in this procedure.