Proposed Scope of Accreditation

Certificate # L1116-1 Scope of Accreditation For Liquor Control Board of Ontario

Quality Assurance Department Laboratory Carol Drummond 55 LakeShore Blvd. E. Toronto, Ontario, M5E 1A4, Canada 416-864-6726

In recognition of a successful assessment to ISO/IEC 17025:2005, accreditation is granted to Liquor Control Board of Ontario to perform the following tests:

Accreditation granted through: July 13, 2010

Testing Range, Methods Technology when Product Types Remarks necessary Determination of Sorbic Acid in Beverage Spectroscopy >20 mg/L A10 Alcohol Excluding Spirits and Liquors by Skalar, Colorimetry Segmented Continuous Flow Analysis Determination of Volatile Acidity in Beverage Spectroscopy >0.1 g/L A11 Alcohol Excluding Spirits and Liquors by Skalar, Colorimetry Segmented Continuous Flow Analysis Determination of Total Reducing Sugar in Spectroscopy >0.1 g/L A12 Beverage Alcohol by Segmented Continuous Skalar, Colorimetry Flow Analysis Determination of Cyanide Expressed as Potassium Ferrocyanide in Beverage Alcohol Spectroscopy >20 µg/L A13 Skalar, Colorimetry Excluding Spirits and Non-Pitted Fruit Liquors by Segmented Continuous Flow Analysis Determination of Free SO2 in Beverage Alcohol Spectroscopy >6 mg/L A14 Excluding Spirits and Liquors by Segmented Skalar, Colorimetry Continuous Flow Analysis Determination of Total SO2 in Beverage Alcohol Spectroscopy >12 mg/L A15 Excluding Spirits and Liquors by Segmented Skalar, Colorimetry Continuous Flow Analysis Determination of Ethanol in Beverage Alcohol Spectroscopy >0.5% v/v A16 Excluding Spirits and Liquors by Segmented Skalar, Colorimetry Continuous Flow Analysis Determination of Ethanol in Beverage Alcohol Chromatography >0.5% v/v A18 below 21% alc./vol. by Gas Chromatography- GC-FID Flame Ionization Detection Determination of Ethanol in Liquors and Spirits Chromatography 12-80% v/v A43 by Gas Chromatography-Flame Ionization GC-FID Detection Chromatography >240 mg/L A19 Determination of Methanol in Liquors and Spirits GC-FID by Gas Chromatography-Flame Ionization Form 28.6—Revision 5 05/23/06 Page 1 of 3 Certificate # L1116-1 Range, Methods Technology when Product Types Remarks necessary Detection Determination of Methanol in Wine by Gas Chromatography >40 mg/L A35 GC-FID Chromatography-Flame Ionization Detection Determination of Methyl Anthranilate in Wines by Chromatography >10µg/L A21 GC-MSD Gas Chromatography-Mass Selective Detection Determination of Ethyl Carbamate in Beverage Chromatography >5µg/L A20 Alcohol by Gas Chromatography-Mass Selective GC-MSD Detection Determination of Pesticide Residues in Wines Chromatography >30µg/L A22 and Beer by Gas Chromatography-Mass GC-MSD Selective Detection Determination of 2,4,6 Trichloroanisole and 2,4,6 Chromatography >0.5µg/L A24 Trichlorophenol in Corks, Wines and Spirits by GC-MSD Gas Chromatography-Mass Selective Detection Determination of Coumarin in Beverage Alcohol Chromatography >10µg/L A53 by Gas Chromatography-Mass Selective GC-MSD Detection Determination of Thujone in Beverage Alcohol Chromatography >30µg/L A54 by Gas Chromatography-Mass Selective GC-MSD Detection Determination of Pesticide Residues in Wine by Chromatography >50µg/L A23 HPLC-PDA HPLC-PDA Determination of Synthetic Dyes in Alcoholic Chromatography >1 mg/L A27 HPLC-PDA Beverages by HPLC-PDA Detection of Ochratoxin A in Wine and Beer by Chromatography >0.5 µg/L A51 HPLC-FD HPLC-Fluorescence Detector Determination of Ochratoxin A in Wine and Beer Chromatography >0.3 µg/L A52 by HPLC-Fluorescence Detector with HPLC-FD Immunoaffinity Column Clean-up Determination of Real Alcoholic Strength of Physical >0.5% v/v A17 Beverage Alcohol using Distillation and Densiometer Property Electronic Densimetry Physical Determination of Apparent Density and Specific A32 Densiometer Property Gravity at 20˚C by Density Meter Physical Measurement of Apparent Alcoholic Strength by >0.95% v/v A49 Densiometer Property Volume Using Electronic Densimetry Physical Determination of Turbidity in Beverage Alcohol 0.1-200NTU A33 Turbidimeter Property by Nephelometry Physical Determinationi of pH in Alcoholic Beverages by 1-14 A34 pH Meter Property pH Meter Physical Determination of Total Acidity in Wines by >0.075 g/L A26 pH Meter - Volumetric Property Titration to pH 8.2 Determination of Volatile Acidity in Alcoholic Wet Chemistry >130mg/L A36 Beverages Excluding Spirits and Liqueurs by Volumetric Cash Still Determination of Free and Total SO2 in Wine by Wet Chemistry >9 mg/L A41 Volumetric Titration (Ripper Method)

>2 µg/L Cd, Co, Sb >10 µg/L As Determination of Metals in Beverage Alcohol by ICP-MS A45 ICP-MS >20 µg/L Pb, ICP-MS Cu >40 µg/L Al, Zn ICP-MS >2 µg/L Cd A46 Determination of Lead and Cadmium Leached ICP-MS >20 µg/L Pb from Storage and Drinking Vessels by ICP-MS Form 28.6—Revision 5 05/23/06 Page 2 of 3 Certificate # L1116-1 Range, Methods Technology when Product Types Remarks necessary

>2 µg/L Cd, Co Determination of Metals (As, Cd, Co, Pb) in ICP-MS >10 µg/L As A47 Beverage Alcohol Requiring Acid Digestion by ICP-MS >20 µg/L Pb ICP-MS Determination of Sodium Chloride in Cooking ICP-MS >0.1% NaCl A48 ICP-MS Wines and Spirits by ICP-MS

Notes:

1) This laboratory offers commercial testing service.

Approved by: ______Date: __January 20, 2010______

Re-Issued: 10/3/07 Revised: 4/3/09 Revised: 1/20/10

Form 28.6—Revision 5 05/23/06 Page 3 of 3