This is to attest that

TUV SUD SOUTH ASIA PVT. LTD. A1, INDUSTRIAL ESTATE OPPOSITE TO NIRMAN PARK KANCHARAPALEM MAIN ROAD, VISAKHAPATNAM ANDHRA PRADESH 530007 INDIA

Testing Laboratory TL-703 has met the requirements of the IAS Accreditation Criteria for Testing Laboratories (AC89), has demonstrated compliance with ISO/IEC Standard 17025:2005, General requirements for the competence of testing and calibration laboratories, and has been accredited, commencing May 30, 2016, for the test methods listed in the approved scope of accreditation. This certificate expires June 1, 2017.

(See laboratory’s scope of accreditation for fields of testing and accredited test methods.)

This accreditation certificate supersedes any IAS accreditation bearing an earlier effective date. The certificate becomes invalid upon suspension, cancellation or revocation of accreditation. See http://iasonline.org/More/search.html for current C.P. Ramani, P.E., C.B.O accreditation information, or contact IAS at 562-364-8201. President

IAS Accreditation Number TL-703 Accredited Entity TUV SUD South Asia PVT. LTD. Address A1, Industrial Estate Opposite to Nirman Park Kancharapalem Main Road, Visakhapatnam Andhra Pradesh 530007 India Contact Name Dr. Shaik Ali Telephone +91 0891-6567000 Effective Date of Scope May 30, 2016 Accreditation Standard ISO/IEC Standard 17025:2005

FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Fish and Marine Aerobic Plate Count Chapter 3, US FDA - BAM Products IS 5402 ISO 4833 – 1 ISO 4833 – 2 Escherichia coli Chapter 4, US FDA - BAM IS 5887 (P 1) ISO 16649 – 2 ISO 16649 – 3 Enumeration of Fecal Coliforms Chapter 4, US FDA – BAM Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) ISO 4832 ISO 4831 Shigella spp Chapter 6, US FDA - BAM IS 5887 (P 7) Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) IS 5887 (P 2) ISO 6888 (P 1) Salmonella spp IS 5887 (P 3) Chapter 5, US FDA - BAM ISO 6579 2013.01, AOAC Yeast and Mold Count Chapter 18, US US FDA - BAM IS 5403 Bacillus cereus Chapter 14, US FDA – BAM IS 5887 (P 6) ISO 7932 Listeria monocytogenes Chapter 10, US FDA - BAM IS 14988 (P 1) ISO 11290 - 1 ISO 11290 - 2 2004.02, AOAC Enterobacteriaceae ISO 21528 - 2 Enterococci Chapter 10, APHA 5th Edition

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Fish and Marine Clostridium perfringens Chapter 16, US FDA - BAM Products IS 5887 (P 4) ISO 7937 Vibrio cholerae Chapter 9, US FDA - BAM IS 5887 (P 5) ISO 21872 - 1 Vibrio parahaemolyticus Chapter 9, US FDA - BAM IS 5887 (P 5) ISO 21872 - 1 Vibrio vulnificus Chapter 9, US FDA - BAM ISO 21872 - 2 Sulfite reducing bacteria / ISO 15213 Sulphide spoilage spore formers Meat & Meat Products Aerobic plate count Chapter 3, US FDA - BAM IS 5402 ISO 4833 - 1 & 2 Escherichia coli Chapter 4, US FDA - BAM IS 5887 (P 1) Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) IS 5887 (P 2) Salmonella spp IS 5887 (P 3) Chapter 5, US FDA - BAM 2013.01, AOAC Yeast and Mold count Chapter 18, US FDA - BAM IS 5403 Listeria monocytogenes Chapter 10, US FDA - BAM IS 14988 (P 1) 2004.02, Chapter 17, AOAC Clostridium perfringens ISO 7937 IS 5887 (P 4) Shigella spp IS 5887 (P 7) Poultry & Poultry Aerobic plate count Chapter 3, US FDA - BAM Products IS 5402 / ISO 4833 - 1 & 2 Escherichia coli Chapter 4, US FDA - BAM IS 5887 (P 1) Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) IS 5887 (P 2) Salmonella IS 5887 (P 3) Chapter 5, US FDA - BAM 2013.01, Chapter 17, AOAC

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Poultry & Poultry Yeast and Mold count Chapter 18, US FDA - BAM Products IS 5403 Listeria monocytogenes Chapter 10, US FDA - BAM IS 14988 (P 1) 2004.02, Chapter 17, AOAC Clostridium perfringens ISO 7937 IS 5887 (P 4) Shigella spp IS 5887 (P 7) Vegetables & Aerobic plate count Chapter 3, US FDA - BAM Vegetables Products IS 5402 ISO 4833 – 1 & 2 Escherichia Coli Chapter 4, US FDA - BAM IS 5887 (P 1) ISO 16649 - 2 Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) Shigella spp IS 5887 (P 7) Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) IS 5887 (P 2) Salmonella spp IS 5887 (P 3) Chapter 5, US FDA - BAM 2013.01, Chapter 17, AOAC Vibrio cholerae Chapter 9, US FDA - BAM IS 5887 (P 5) Listeria monocytogenes Chapter 10, US FDA - BAM IS 14988 (P 1) 2004.02, Chapter 17, AOAC Bacillus cereus Chapter 14, US FDA - BAM IS 5887 (P 6) Yeast and Mold count Chapter 18, US FDA - BAM IS 5403 Clostridium perfringens Chapter 16, US FDA - BAM IS 5887 (P 4) Lactic acid bacteria ISO 15214 Flat sour spore formers Clause 25.6, Chapter 25, APHA 5th Edition Other Specified Food Aerobic plate count Chapter 3, US FDA - BAM Items - Raw, Cooked IS 5402 Foods and Ready to ISO 4833 – 1 & 2 Eat Foods Escherichia coli Chapter 4, US FDA - BAM IS 5887 (P 1) Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) Shigella spp IS 5887 (P 7) Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Other Specified Food Salmonella spp IS 5887 (P 3) Items - Raw, Cooked Chapter 5, US FDA - BAM Foods and Ready to 2013.01, Chapter 17, AOAC Eat Foods Yeast and Mold count Chapter 18, US FDA - BAM IS 5403 Bacillus cereus Chapter 14, US FDA - BAM IS 5887 (P 6) Listeria monocytogenes Chapter 10, US FDA - BAM IS 14988 (P 1) 2004.02, Chapter 17, AOAC Clostridium perfringens Chapter 16, US FDA - BAM IS 5887 (P 4) Vibrio cholerae Chapter 9, US FDA – BAM IS 5887 (P 5) ISO 21872-1 Enterobacteriaceae ISO 21528 – 2 Drinking Water - Coliforms 9221 B, 9221 C, 9221 E, APHA Piped and Bore Well IS 1622 Escherichia coli 9221 B, 9221 E, APHA IS 1622 Escherichia coli and coliforms IS 15185 by membrane filtration ISO 9308 - 1 technique Enterococci IS 15186 ISO 7899 - 2 Pseudomonas aeruginosa ISO 16266 Clostridium perfringens Annex 3, EU 98/83/EC Colony count @ 220C ISO 6222 Colony count @ 370C ISO 6222 Packaged Natural Escherichia coli IS 5887 (P 1) Mineral Water and IS 15185 Packaged Drinking ISO 9308 - 1 Water Coliform IS 5401 (P 1) IS 15185 ISO 9308 - 1 Fecal Streptococci IS 5887 (P 2) IS 15186 ISO 7899 - 2 Staphylococcus aureus IS 5887 (P 2) Sulphite reducing anaerobes IS 13428 Pseudomonas aeruginosa IS 13428 Yeast and Mold Count IS 5403 Aerobic Microbial Count IS 5402 @ 22 deg C & 37 Deg C Salmonella IS 5887 (P 3) IS 15187 Shigella IS 5887 (P 7) Vibrio choleraee IS 5887 (P 5)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Packaged Natural Vibrio parahemolyticus IS 5887 (P 5) Mineral Water and Packaged Drinking Water Water for Processed Standard Plate Count IS 1622 Food Industry Coliform IS 1622 Proteolytic & Lipolytic count Appendix A, IS 4251 Beverages - (Alcoholic Aerobic Plate Count Chapter 3, US FDA - BAM /Non - Alcoholic) IS 5402 ISO 4833 - 1 Escherichia coli Chapter 4, US FDA - BAM ISO 16649 - 2 Yeast and Mold Count Chapter 18, US FDA - BAM IS 5403 ISO 21527 - 1 Salmonella spp IS 5887 (P 3) ISO 6579 2013.01, Chapter 17, AOAC Shigella spp IS 5887 (P 7) Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) ISO 6888 - 1 Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) IS 5401 (P 2) ISO 4831 ISO 4832 Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Vibrio cholerae IS 5887 (P 5) Flat Sour Spore Organism Clause 25.6, Chapter 25, APHA 5th Edition Cereal, Pulses and Staphylococcus aureus Chapter 12, US FDA - BAM Cereal Products IS 5887 (P 2) IS 5887 (P 8 / Sec 1) Salmonella spp IS 5887 (P 3) Chapter 5, US FDA - BAM 2013.01, Chapter 17, AOAC Yeast and Mold count Chapter 18, US FDA - BAM IS 5403 Bacillus cereus ISO 7932 Chapter 14, US FDA – BAM Faecal Streptococci IS 5887 (P 2) Microbiology Cereal, Pulses and Aerobic Plate Count Chapter 3, US FDA - BAM Cereal Products IS 5402 ISO 4833 – 1 & 2 Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) IS 5401 (P 2) ISO 4832

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Coffee and Cocoa Escherichia coli Chapter 4, US FDA - BAM Products Cereal, Pulses and Cereal ISO 16649 - 2 Products IS 5887 (P 1) Aerobic Plate Count Chapter 3, US FDA - BAM IS 5402 ISO 4833 – 1 & 2 Escherichia coli Chapter 4, US FDA - BAM IS 5887 (P 1) Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) Salmonella spp Chapter 5, US FDA - BAM IS 5887 (P 3) 2013.01, Chapter 17, AOAC Yeast and Mold Count Chapter 18, US FDA - BAM IS 5403 Bacillus cereus Chapter 14, US FDA - BAM ISO 7932 Clostridium perfringens ISO 7937 Chapter 16, US FDA – BAM Fruit and Fruit Total Plate Count Chapter 3, US FDA - BAM Products IS 5402 ISO 4833 – 1 & 2 Coliform Count Chapter 4, US FDA - BAM IS 5401 (P 1) IS 5401 (P 2) ISO 4832 ISO 4831 Escherichia coli Chapter 4, US FDA - BAM ISO 16649 - 2 IS 5887 (P 1) Shigella spp IS 5887 (P 7) Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) IS 5887 (P 2) Salmonella spp IS 5887 (P 3) Chapter 5, US FDA - BAM 2013.01, Chapter 17, AOAC Vibrio cholerae IS 5887 (P 5) Chapter 9, US FDA - BAM Listeria monocytogenes Chapter 10, US FDA - BAM IS 14988 (P 1) 2004.02, Chapter 17, AOAC Bacillus cereus Chapter 14, US FDA - BAM IS 5887 (P 6) Yeast and Mold Count Chapter 18, US FDA - BAM IS 5403

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Fruit and Fruit Clostridium perfringens Chapter 16, US FDA - BAM Products ISO 7937 IS 5887 (P 4) Lactic acid bacteria ISO 15214 Incubation test @ 37 deg for 10 IS 2860 days & 55 deg for 7 days Flat sour spore formers Clause 25.6, Chapter 25, APHA 5th Edition Herbs, Spices and Aerobic Plate Count Chapter 3, US FDA - BAM Condiments IS 5402 ISO 4833 - 1 Escherichia coli Chapter 4, US FDA - BAM ISO 16649 - 2 IS 5887 (P 1) Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) ISO 4832 Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Salmonella spp Chapter 5, US FDA - BAM IS 5887 (P 3) 2013.01, Chapter 17, AOAC ISO 6579 Yeast and Mold Count Chapter 18, US FDA - BAM IS 5403 ISO 21527 - 2 Bacillus cereus Chapter 14, US FDA - BAM IS 5887 (P 6) ISO 7932 Clostridium perfringens Chapter 16, US FDA - BAM ISO 7937 IS 5887 (P 4) Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) ISO 6888 - 1 Shigella spp IS 5887 (P 7) Sulfite reducing bacteria ISO 15213 Milk and Dairy Aerobic Plate Count Chapter 3, US FDA - BAM Products IS 5402 ISO 4833 - 1 Escherichia coli Chapter 4, US FDA - BAM ISO 16649 - 2 IS 5887 (P 1) Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) ISO 4832 Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Shigella spp IS 5887 (P 7)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Milk and Dairy Staphylococcus aureus Chapter 12, US FDA - BAM Products IS 5887 (P 8 / Sec 1) IS 5887 (P 2) ISO 6888 - 1 Salmonella spp Chapter 5, US FDA - BAM IS 5887 (P 3) 2013.01, Chapter 17, AOAC ISO 6579 Yeast and Mold Count Chapter 18, US FDA - BAM IS 5403 ISO 21527 – 1 Bacillus cereus Chapter 14, US FDA - BAM IS 5887 (P 6) ISO 7932 Listeria monocytogenes Chapter 10, US FDA - BAM IS 14988 (P 1) 2004.02, Chapter 17, AOAC ISO 11290 - 1 Clostridium perfringens Chapter 16, US FDA - BAM ISO 7937 IS 5887 (P 4) Enterobacteriaceae ISO 21528 – 2 Tea Aerobic Plate Count Chapter 3, US FDA - BAM IS 5402 ISO 4833 - 1 Escherichia coli Chapter 4, US FDA - BAM ISO 16649 - 2 IS 5887 (P 1) Enumeration of Coliforms Chapter 4, US FDA - BAM IS 5401 (P 1) ISO 4832 Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM Staphylococcus aureus Chapter 12, US FDA - BAM IS 5887 (P 8 / Sec 1) ISO 6888 - 1 Salmonella spp Chapter 5, US FDA - BAM IS 5887 (P 3) 2013.01, Chapter 17, AOAC ISO 6579 Yeast and Mold Count Chapter 18, US FDA - BAM IS 5403 ISO 21527 - 1 ISO 21527 - 2 Bacillus cereus Chapter 14, US FDA - BAM ISO 7932 Listeria monocytogenes Chapter 10, US FDA - BAM 2004.02, Chapter 17, AOAC ISO 11290 – 1

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Tea Clostridium perfringens Chapter 16, US FDA - BAM ISO 7937 IS 5887 (P 4) Enterobacteriaceae ISO 21528 – 2 Wet Chemical Fish and Marine Total Solids / Moisture 952.08, Chapter 35, AOAC Products FSSAI Lab Manual 6 (Clause 2.2) Total Fat 948.15, Chapter 35, AOAC Total Nitrogen 940.25, Chapter 35, AOAC Total Ash 938.08, Chapter 35, AOAC Sodium Chloride 937.09, Chapter 35, AOAC FSSAI Lab Manual 6 (Clause 2.3) Total Volatile Base Nitrogen LAB_P_SOP_129 FSSAI Lab Manual 6 (Clause 1.2) Acid Insoluble Ash IS 14950 Annex F FSSAI Lab Manual 6 (Clause 2.4) Polyphosphates IS 5960 (P 13) Clause 8 ISO 5553 FSSAI Lab Manual 6 (Clause 3.5) Lead, Cadmium, Mercury & Lab_P_SOP_36 / AAS Arsenic Meat And Poultry Moisture 950.46, Chapter 39, AOAC Products Crude fat 960.39, Chapter 39, AOACFSSAI Lab Manual 6 (Clause 2.1) Salt 935.47, Chapter 39, AOAC FSSAI Lab Manual 6 (Clause 2.3) Total ash 920.153, Chapter 39, AOACFSSAI Lab Manual 6 (Clause 2.4) Nitrogen 928.08, Chapter 39, AOACFSSAI Lab Manual 6 (Clause 2.2) Copper, Zinc, Tin, Mercury, LAB_P_SOP_50 Arsenic, Lead, Cadmium & AAS Selenium Drinking Water / Colour IS 3025 (P 4) Clause 2 Packaged Drinking 2120 B of APHA Water / Mineral Total dissolved solids IS 3025 (P 16) Water / Process 2540 C of APHA Water (Council Odour IS 3025 (P 5) Directive 98/83/EC) 2150 B of APHA Turbidity IS 3025 (P 10) 2130 B of APHA Taste IS 3025 (P 8) 2160 C of APHA Aluminium IS 3025 (P 55) Lab_P_SOP_37 / AAS Boron IS 3025 (P 57) Lab_P_SOP_37 / AAS Residual free chlorine IS 3025 (P 26) Clause 3 4500 Cl-B of APHA

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Drinking Water / Hexavalent chromium IS 3025 (P 52) Clause 6 Packaged Drinking 3500 Cr B of APHA Water / Mineral Nitrites IS 3025 (P 34) Clause 4 Water / Process 4500 NO2 B of APHA Water (Council pH value IS 3025 (P 11) Clause 2 Directive 98/83/EC) 4500 H+ B of APHA

Total hardness (as CaCO3) IS 3025 (P 21) Clause 5 2340 C of APHA Copper (as Cu) IS 3025 (P 42) Lab_P_SOP_37 / AAS Iron (as Fe) IS 3025 (P 53) Lab_P_SOP_37 / AAS Manganese (as Mn) IS 3025 (P 35) Lab_P_SOP_37 / AAS

Nitrate (as NO3) IS 3025 (P 34) Clause 3 4500 NO3 B of APHA Flouride (as F) IS 3025 (P 60) Clause 5 4500 F- D of APHA Zinc (as Zn) IS 3025 (P 49) Lab_P_SOP_37 / AAS Nickel (as Ni) Annexure F of IS 13428 Lab_P_SOP_37 / AAS Chloride (as Cl) IS 3025 (P 32) Clause 2 3114 C of APHA Selenium (as Se) IS 3025 (P 56) Lab_P_SOP_37 / AAS

Sulphate (as SO4) IS 3025 (P 24) Clause 4 4500 SO4 E of APHA Alkalinity (as CaCO3) IS 3025 (P 23) 2320 B of APHA Total Solids IS 3025 (P 15) Calcium (as Ca) IS 3025 (P 40) Clause 5 3500 Ca B of APHA

Phenolic compounds (as C6H5OH) IS 3025 (P 43) 5530 D of APHA Mercury (as Hg) IS 3025 (P 48) Lab_P_SOP_37 / AAS Cadmium (as Cd) IS 3025 (P 41) Lab_P_SOP_37 / AAS Arsenic (as As) IS 3025 (P 37) Lab_P_SOP_37 / AAS Lead (as Pb) IS 3025 (P 47) Lab_P_SOP_37 / AAS Chromium (as Cr) Annexure J of IS 13428 Lab_P_SOP_37 / AAS Barium (as Ba) Annexure F of IS 13428 Lab_P_SOP_37 / AAS Magnesium (as Mg) IS 3025 (P 46) 3500 Mg B of APHA

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Drinking Water/ Sodium (as Na) IS 3025 (P 45) Packaged Drinking Lab_P_SOP_37 / AAS Water/Mineral Silver (as Ag) Annex J IS 13428 Water/Process Lab_P_SOP_37 / AAS Water (Council Molybdenum (as Mo) IS 3025 (P 2) Directive 98/83/EC) Lab_P_SOP_37 / AAS Mineral Oil IS 3025 (P 39) 5520 C of APHA Anionic Surface Active Agents as Annex K of IS 13428 MBAS 5540 C of APHA

Sulphide as H2S IS 3025 (P 29) Clause 3 4500 S2- F of APHA Antimony (as Sb) Annex G IS 13428 Lab_P_SOP_37 / AAS Cyanide (as CN) IS 3025 (P 27) Clause 2 4500 CN- E of APHA Borates (as B) Annex H of IS 13428

Chloramines as Cl2 4500 Cl -G APHA Ammonia IS 3025 (P 34) Clause 2 – (as Total Ammonia –N) 4500 NH3 C of APHA Oxidisability IS 3025 (P 58) Dissolved oxygen IS 3025 (P 38) Clause 4 Total Organic Carbon (TOC) In-house method Specific conductance IS 3025 (P 14) 2510 B of APHA Milk (Raw and Total Milk Solids & Total Solids IS 1166 Append B Pasteurized)/Curd/ IS 1479 Clause 4 Lassi/Condensed IS 11622 Milk/Sweetened IS 12333 Clause 8 UHT Treated 990.20, Chapter 33, AOAC Condensed Milk FSSAI Lab Manual 1 (Clause 1.3.3) Titratable Acidity as Lactic Acid IS 1166 Append D IS 11766 Clause 8 IS 1479 (P 1) Clause 14 947.05, Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 9.5) pH IS 4238 Append C

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Milk (Raw and Total Fat IS 13688 Clause 5B Pasteurized)/Curd/ IS 1479 (P 2) Lassi/Condensed IS 11762 Milk/Sweetened IS 1166 UHT Treated FSSAI Lab Manual 1 (Clause Condensed Milk 1.3.4) Total Ash IS 1479 (P 2) Clause 16 945.46, Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 10.7) Lactose IS 1479 (P 2) Clause 13 Sucrose IS 1166 Append C FSSAI Lab Manual 1 (Clause 9.4) Crude Protein IS 1479 (P 2) Clause 8 IS 7219 FSSAI Lab Manual 1 (Clause 19.0) Total Nitrogen IS 1479 (P 2) Clause 8 991.20,Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 19.0) Solids-Not-Fat (SNF) 990.21,Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 15.2) Titratable Acidity (as Acetic Acid) IS 12176 Append D FSSAI Lab Manual 1 (Clause 9.5) Total Antibiotics as Beta Lactum Lab_P_SOP_238(Detection of Antibiotic Residue in Milk and Milk Power) / Delvo Kit Dry Milk Powder Moisture IS 11623 (Milk Powder, Skim IS 14433 Milk Powder, Partly IS 16072 Skimmed Milk FSSAI Lab Manual 1 (Clause Powder, Infant Milk 10.2) Substitute) Total Solids IS 1165 IS 13334 (P 1) IS 13334 (P 2) IS 14542 FSSAI Lab Manual 1 (Clause 10.2) Sucrose IS 4079 Append C FSSAI Lab Manual 1 (Clause 9.4) Fat IS 11721 IS 14433 FSSAI Lab Manual 1 (Clause 10.3) Total Ash IS 1165 Append A 930.30, Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 10.7)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Dry Milk Powder Titratable Acidity as Lactic Acid IS 1165 Append B (Milk Powder, Skim IS 11766 Milk Powder, Partly FSSAI Lab Manual 1 (Clause Skimmed Milk 10.4) Powder, Infant Milk Protein / Milk Protein in MSNF IS 7219 Substitute) 930.29, Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 10.6) Total Antibiotics as Beta Lactum Lab_P_SOP_238 (Detection of Antibiotic Residue in Milk and Milk Power)/ Delvo Kit Cheese (Includes Moisture IS 2785 Append A Natural & Processed IS 10484 Append A Cheese) & Paneer 926.08, Chapter 33, AOAC Milk Fat IS 10484 Append B

Salt IS 2785 Append C

Titratable Acidity as Lactic Acid IS 10484 Append C 920.124, Chapter 33, AOAC19th Edition Ash 935.42, Chapter 33, AOAC Total Nitrogen 2001.14, Chapter 33, AOAC pH 943.02, Chapter 33, AOAC Dairy Products Copper, Zinc, Tin, Mercury, Lab_P_SOP_36 / AAS Arsenic, Lead, Cadmium & Selenium Milk and Milk Aflatoxin M1 LAB_P_SOP_235 Products LC-MS/MS Animal Feed / Pet Moisture IS 7874 (P 1) Foods 934.01, Chapter 4, AOAC Clause 4 Crude Fat IS 7874 (P 1) 920.39, Chapter 4, AOAC Clause 7 Protien IS 7874 (P 1) 984.13, Chapter 4, AOAC Clause 5 Ash IS 7874 (P 1) 942.05, Chapter 4, AOAC Clause 9 Sugars 974.06, Chapter 4, AOAC Crude Fibre IS 7874 (P 1) Clause 8 Animal Feeds Lead, Cadmium, Arsenic & Lab_P_SOP_36 / AAS Mercury Wheat Atta Moisture IS 1155 Append A FSSAI Lab Manual 3 (Clause 8.2) Total Ash IS 1155 Append B FSSAI Lab Manual 3 (Clause 8.3)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Wheat Atta Gluten IS 1155 Append D FSSAI Lab Manual 3 (Clause 8.5) Acid Insoluble Ash IS 1155 Append C FSSAI Lab Manual 3 (Clause 8.4) Alcoholic Acidity IS 1155 Append F FSSAI Lab Manual 3 (Clause 8.6) Crude Fiber IS 1155 Append E FSSAI Lab Manual 3 (Clause 8.9) Maida Gluten IS 1009 Append D FSSAI Lab Manual 3 (Clause 8.5) Moisture IS 1009 Append A FSSAI Lab Manual 3 (Clause 8.2) Ash IS 1009 Append B FSSAI Lab Manual 3 (Clause 8.3) Acid insoluble ash IS 1009 Append C FSSAI Lab Manual 3 (Clause 8.4) Alcoholic Acidity IS 1009 Append E FSSAI Lab Manual 3 (Clause 8.6) Cereals, Pulses and Copper, Zinc, Tin, Mercury, Lab_P_SOP_36 / AAS By Products Arsenic, Lead & Cadmium Spices and Moisture IS 1797 Clause 9 Condiments Pepper FSSAI Lab Manual 10 (Clause - Black, Kalimirchi 3.0) / IS 1798 White (Whole, Total ash IS 1797 Clause 6 Powder) FSSAI Lab Manual 10 (Clause 4.0) / IS 1798 Non-volatile ether extract IS 1797 Clause 14 FSSAI Lab Manual 10 (Clause 9.0) / IS 1798 Volatile oil IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0) / IS 1798 Extraneous matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 2.0) / IS 1798 Light Berries IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 13.2) / IS 1798 Pinheads or broken berries IS 1798 Clause 4 Bulk density Lab_P_SOP_16 (Determination of Bulk Density) FSSAI Lab Manual 10 (Clause 13.1) Piperine 987. 07, Chapter 43, AOAC FSSAI Lab Manual 10 (Clause 13.3) Turmeric – Haldi Moisture IS 1797 Clause 9 (Whole, Powder) FSSAI Lab Manual 10 (Clause 3.0)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Turmeric - Haldi Total Ash IS 1797 Clause 9 (Whole, Powder) FSSAI Lab Manual 10 (Clause 4.0) Acid Insoluble Ash IS 1797 Clause 9 FSSAI Lab Manual 10 (Clause 5.0) Colouring power expressed as IS 3576 / IS 10925 Append B curcuminoid content FSSAI Lab Manual 10 (Clause 15.4) Total Starch IS 4706 Clause 9 FSSAI Lab Manual 10 (Clause 15.5) Test for Lead Chromate IS 3576 Annex A FSSAI Lab Manual 10 (Clause 15.6) Extraneous Matter IS 3576 Clause 4.3 FSSAI Lab Manual 10 (Clause 2.0) Defective rhizomes IS 3576 Clause 4.4 Cumin- Safed Zeera Moisture IS 1797 Clause 9 (Whole, Powder) FSSAI Lab Manual 10 (Clause 3.0) Total Ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0) Acid Insoluble Ash IS 1797 Clause 8 FSSAI Lab Manual 10 (Clause 5.0) Volatile oil Content IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0) Non Volatile Ether Extract IS 1797 Clause 14 FSSAI Lab Manual 10 (Clause 9.0) Extraneous Matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 2.0) Broken Fruits (Dam Discoloured IS 2447 Clause 4 and Immature Seeds) Cumin Black – Moisture IS 1797 Clause 9 Kalonji (Whole, FSSAI Lab Manual 10 (Clause Powder) 3.0) Total Ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0) Cumin Black – Acid Insoluble Ash IS 1797 Clause 8 Kalonji (Whole, FSSAI Lab Manual 10 (Clause Powder) 5.0)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Cumin Black – Volatile Oil Content IS 1797 Clause 15 Kalonji (Whole, FSSAI Lab Manual 10 (Clause Powder) 10.0) Non Volatile Ether Extract IS 1797 Clause 14 FSSAI Lab Manual 10 (Clause 9.0) Extraneous Matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 2.0) Broken Fruits (Damaged, IS 1797 Clause 4 Shrivelled, Discoloured and Immature Seeds) Edible seeds other than Cumin IS 2447 Clause 4 Black Cardamom - Choti Moisture IS 1797 Clause 9 Elachi , Large FSSAI Lab Manual 10 (Clause Cardamom - Badi 3.0) Elachi (Whole, Total Ash IS 1797 Clause 6 Seeds, Powder) FSSAI Lab Manual 10 (Clause 4.0) Volatile Oil Content IS 1797 Clause 16 FSSAI Lab Manual 10 (Clause 10.0) Extraneous Matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 2.0) Chillies and Moisture IS 1797 Clause 9 Capsicum (Whole, FSSAI Lab Manual 10 (Clause Powder) 3.0) Total ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0) Acid insoluble ash IS 1797 Clause 8 FSSAI Lab Manual 10 (Clause 5.0) Volatile oil content IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0) Extraneous matter IS 2322 Clause 5.4 FSSAI Lab Manual 10 (Clause 2.0) Unripe and marked fruits IS 2322 Clause 5.5 Broken fruits, seed & fragments IS 2322 Clause 5.5 Crude fiber IS 1797 Clause 13 FSSAI Lab Manual 10 (Clause 11.0) Non-volatile ether extract IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 9.0)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Chillies and Colour 971.26, Chapter 43, AOAC / Capsicum (Whole, ASTA Colour Powder) Cinnamon – Moisture IS 1797 Clause 9 Dalchini (Whole, FSSAI Lab Manual 10 (Clause Powder) 3.0) Total Ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0) Acid Insoluble Ash IS 1797 Clause 18 FSSAI Lab Manual 10 (Clause 5.0) Volatile Oil Content IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0) Extraneous Matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 2.0) Cloves – Laung Moisture IS 1797 Clause 9 (Whole, Powder) FSSAI Lab Manual 10 (Clause 3.0) Total ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0) Acid insoluble ash IS 1797 Clause 18 FSSAI Lab Manual 10 (Clause 5.0) Volatile oil IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0) Crude fiber IS 1797 Clause 13 FSSAI Lab Manual 10 (Clause 11.0) Extraneous matter IS 4404 FSSAI Lab Manual 10 (Clause 2.0) Tendrils, Mother cloves IS 4404 Khokar cloves IS 4404 Headless cloves IS 4404 Coriander – Dhania Moisture IS 1797 Clause 9 (Whole, Powder) FSSAI Lab Manual 10 (Clause 3.0) Total ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0) Acid insoluble ash IS 1797 Clause 18 FSSAI Lab Manual 10 (Clause 5.0)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Coriander – Dhania (Whole, Powder) Volatile oil content IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0) Extraneous matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 2.0) Split fruits IS 1797 Clause 4 Damaged / discolored fruits IS 1797 Clause 4.1 Spices and Moisture IS:1797- 1985 Condiments FSSAI Lab Manual 10 (Clause 3.0) Total ash IS:1797- 1985 FSSAI Lab Manual 10 (Clause 4.0) Acid insoluble ash IS:1797- 1985 Non-volatile ether extract IS:1797- 1985 FSSAI Lab Manual 10 (Clause 9.0) Volatile oil IS:1797- 1985 FSSAI Lab Manual 10 (Clause 10.0) Extraneous matter IS:1797- 1985 FSSAI Lab Manual 10 (Clause 2.0) Copper, Zinc, Tin, Mercury, Lab_P_SOP_36 / AAS Arsenic, Lead & Cadmium Fruit and Vegetable Total soluble solids IS 13815 Products (Canned 920.151, Chapter 37, AOAC Fruits and FSSAI Lab Manual 5 (Clause 1.6) Vegetables) pH IS 2860 Clause 8 / IS 3881 Annex D FSSAI Lab Manual 5 (Clause 2.3) Protein IS 7219 920.152, Chapter 37, AOAC Salt IS 2860 Clause 11/ IS 1797 Clause 16 Reducing Sugars IS 6287 Clause 8 FSSAI Lab Manual 5 (Clause 2.6) Sucrose IS 6287 Clause 9 FSSAI Lab Manual 5 (Clause 2.6) Titratable Acidity IS 2860 Clause 10 942.15, Chapter 37, AOAC Drained weight / net weight IS 2860 Clause 7 Vitamin C 967.21 Chapter 45, AOAC Wet Chemical Fruit and Vegetable pH IS 2860 Clause 8 / IS 3881 Products (Pickles) Annex D Protein IS 7219 920.152, Chapter 37, AOAC

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Fruit and Vegetable Salt IS 2860 / IS 1797 Clause 16 Products (Pickles) Reducing Sugars IS 6287 Clause 8 Sucrose IS 6287 Clause 9 Titratable Acidity IS 2860 942.15, Chapter 37, AOAC FSSAI Lab Manual 5 (Clause 2.4) Drained weight / Net weight IS 2860 FSSAI Lab Manual 5 (Clause 1.4) Vitamin C 967.21, Chapter 45, AOAC Sulphur di oxide 990.28, Chapter 47, AOAC Fruit and Vegetable Total soluble solids IS 13815 Products (Jam, 920.151, Chapter 37, AOAC Jellies, Marmalades) FSSAI Lab Manual 5 (Clause 17.3) pH IS 2860 Clause 8 / IS 3881 Annex D Protein IS 7219 920.152, Chapter 37, AOAC Reducing Sugars IS 6287 Clause 8 Sucrose IS 6287 Clause 9 Titratable Acidity IS 2860 942.15, Chapter 37, AOAC FSSAI Lab Manual 5 (Clause 2.4) Vitamin C 967.21, Chapter 45, AOAC Sulphur di oxide 990.28, Chapter 47, AOAC Water Insoluble solids 922.10, Chapter 37, AOAC Soluble solids 932.12, Chapter 37, AOAC Total Ash 940.26, Chapter 37, AOAC Fruit and Vegetable pH IS 2860 Clause 8 / IS 3881 Products Annex D (Dehydrated and FSSAI Lab Manual 5 (Clause Frozen Fruits and 17.3) Vegetables) Protein IS 7219 920.152, Chapter 37, AOAC Salt IS 2860 / IS 1797 Reducing Sugars IS 6287 Clause 8 Sucrose IS 6287 Clause 9 Titratable Acidity IS 2860 942.15, Chapter 37, AOAC Vitamin C 967.21, Chapter 45, AOAC Water Insoluble solids 922.10, Chapter 37, AOAC Soluble solids 932.12, Chapter 37, AOAC Total Ash 940.26, Chapter 37, AOAC Moisture Lab_P_SOP_247 FSSAI Lab Manual 5 (Clause 4.1) Acid Insoluble Ash Lab_P_SOP_248 FSSAI Lab Manual 5 (Clause 17.4)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Fruit and Vegetable Starch IS 4706 (P 2) Clause 9 Products Sulphur di oxide 990.28, Chapter 47, AOAC (Dehydrated and Frozen Fruits and Vegetables) Fruit and Vegetable Total soluble solids IS 13815 Products (Ketchup, 920.151, Chapter 37, AOAC Sauces, Culinary FSSAI Lab Manual 5 (Clause 1.6) Paste) pH IS 2860 / IS 3881 Annex D Protein IS 7219 920.152, Chapter 37, AOAC Salt IS 2860 / IS 1797 Clause 16 Reducing Sugars IS 6287 Clause 8 Sucrose IS 6287 Clause 9 Titratable Acidity IS 2860 942.15, Chapter 37, AOAC FSSAI Lab Manual 5 (Clause 2.4) Vitamin C 967.21, Chapter 45, AOAC Fill of container Lab_P_SOP_250 (Determination of percentage fill of container in fruit and vegetable products)

Acid Insoluble Ash Lab_P_SOP_248 Determination of Ash Insoluble in Ash in Fruits and Vegetable product Fruit and Vegetable Total soluble solids IS 13815 Products (Fruit Juice 920.151, Chapter 37, AOAC / Beverages, FSSAI Lab Manual 5 (Clause 1.6) Squash, Cordial, Fruit content Lab_P_SOP_244 Crush, Carbonated FSSAI Lab Manual 5 (Clause Juices) 2.11) pH IS 2860 / IS 3881 Annex D FSSAI Lab Manual 5 (Clause 2.3) Reducing Sugars IS 6287 Clause 8 FSSAI Lab Manual 5 (Clause 2.6) Sucrose IS 6287 Clause 9 FSSAI Lab Manual 5 (Clause 2.6) Titratable Acidity 942.15, Chapter 37, AOAC / FSSAI Lab Manual 5 (Clause 2.4) Sulphur di oxide 990.28, Chapter 47, AOAC Alcoholic and Non - Copper, Zinc, Tin, Mercury, Lab_P_SOP_36 / AAS Alcoholic Beverages Arsenic, Lead & Cadmium (including Carbonated Beverages)

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Wet Chemical Coffee (Roasted Total ash IS 3077 Coffee/R&G 920.93, Chapter 30, AOAC Coffee/Soluble Annex F Coffee Powder, FSSAI Lab Manual 4 (Clause 1.3) Soluble Coffee - Acid insoluble ash IS 3077 Annex G Chicory Powder, FSSAI Lab Manual 4 (Clause 1.5) Roasted Coffee - Water soluble ash IS 3077 Annex H Chicory Powder, FSSAI Lab Manual 4 (Clause 1.4) Instant Coffee - Alkalinity of ash IS 3077 Annex J Chicory Mixture) FSSAI Lab Manual 4 (Clause 1.6) Ether Extract IS 3077 Annex M 920.97 Chapter 30, AOAC Aqueous extract IS 3077 Annex K FSSAI Lab Manual 4 (Clause 1.7) Moisture IS 3077 Annex E 979.12, Chapter 30, AOAC FSSAI Lab Manual 4 (Clause 1.2) Acidity 920.92, Chapter 30, AOAC Crude fiber 920.98, Chapter 30, AOAC Total ash IS 612 FSSAI Lab Manual 4 (Clause 1.3) Tea (Black Tea, Total ash IS 13854 / IS 13860 Green Tea, Instant FSSAI Lab Manual 4 (Clause 1.3) Tea) Acid insoluble ash IS 13857 FSSAI Lab Manual 4 (Clause 1.5) Water soluble ash IS 13855 FSSAI Lab Manual 4 (Clause 1.4) Alkalinity of ash IS 13856 FSSAI Lab Manual 4 (Clause 1.6) Moisture IS 13853 FSSAI Lab Manual 4 (Clause 1.2) Water soluble Extract IS 13862 FSSAI Lab Manual 4 (Clause 1.7) Total polyphenols as Gallic Acid ISO 14502 Crude fiber IS 10226 (P 1) FSSAI Lab Manual 4 (Clause 5.8) Total ash 920.100, Chapter 30, AOAC FSSAI Lab Manual 4 (Clause 1.3) Acid insoluble ash IS 3633 Alkalinity of ash IS 3633 Coffee, Tea, Cocoa Copper, Zinc, Tin, Mercury, Lab_P_SOP_36 / AAS and By Products Arsenic, Lead, Cadmium, Selenium, Manganese, Chromium, Iron & Nickel

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Chemical (Analytical) Food & Agricultural Pesticide Residues: AOAC 20th Edition 2015 Commodities 4-Bromo-2-Chlorophenol, EN 15662 : 2009 Alachlor, , Allethrins, LAB_P_SOP_50-Fish & Fish , , Products , Butachlor, , LAB_P_SOP_97-Dairy & Dairy Captafol, Captan, -cis & Products trans, Chlorfenopyr, LAB_P_SOP_137- Beverages , Chlorobenzilate, LAB_P_SOP_202- Cereals, Pulses Chlorothalonil, - & their Products methyl, ethyl, - LAB_P_SOP_207-Spices I,II,III,IV, - I, II, Condiments & their products III, IV, , , LAB_P_SOP_260 – Fruits & , , α-, β- Vegetables Endosulfan, Endosulfan - LAB_P_SOP_287 – Simulant Sulphate, , , Foods Ethofenprox, By GC-MS/MS Lab_P_SOP_198 – Etrimfos,, Fish & Fish Products , -I,II, GCMSMS , Fluvalinate-I,II, Fluchloralin, , HCB, , Heptachlor epoxide, Imazethapyr,Iprodione, Isodrin, , Metolachlor, , o,p', p,p' – DDD, o,p', p,p' - DDE, o,p', p,p' – DDT, Oxyfluorfen, -ethyl, methyl, Pendimethalin, -I,II, , Pretilachlor, Propanil, Propetamphos, Pyrene, , Tau-Fluvalinate, Tetraconazole, Tetrahydrophthalimide, , Trifluralin, Vinconazolin, α-BHC, β-BHC, ϒ- BHC, δ-BHC, λ-

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Chemical (Analytical) Food & Agricultural Pesticide Residues: AOAC 20th Edition 2015 Commodities 2,4 - D, 3,4-Dichloroaniline, 3- EN 15662 : 2009 Hydroxy , , LAB_P_SOP_50-Fish & Fish , , Aldicarb Products sulfone, Aldicarb Sulfoxide, LAB_P_SOP_97-Dairy & Dairy Anilophos, Atrazine, Benfuracarb, Products Benomyl, Bitertanol, , LAB_P_SOP_137- Beverages Carbaryl, Carbendazim, LAB_P_SOP_202- Cereals, Pulses Carbofuran, , & their Products Carpropamid, LAB_P_SOP_207-Spices Cartaphydrochloride, Condiments & their products Chlorimuron-ethyl, LAB_P_SOP_260 – Fruits & Chlormequatchloride, Clomazone, Vegetables Clodinafop-propargyl, Cyhalofop- LAB_P_SOP_287 – Simulant butyl, Cymoxanil, , Foods Diclofop-methyl, Difenoconazole, By GC-MS/MS Lab_P_SOP_198 – , , Fish & Fish Products Dimethomorph, Dithianon, LCMSMS Diuron, Dodine, Edifenphos, Ethephon, Ethion, Ethoxyquin, Ethoxysulfuron, Fenamidone, Fenarimol, Fenazaquin, , Fenoxy-prop-p-ethyl, , Fenthion sulfone, Fenthion sulfoxide, Formothion, Flonicamid, Flufenacet, Fosetyl-Al, Glufosinate-ammonium, Glyphosphate, Hexaconazole, , Indoxacarb, Iprodione, Isoprothiolane, Isoproturon, Kitazin (Iprobenphos), Linuron, Lufenuron, , , Malic Hydrazide, Metalaxyl, Metalaxyl-M, Metasulfuron- methyl, Methabenzthiazuron, , , Methyl Chloro-phenoxy-acetic Acid (M.C.P.A.), Metribuzin, , Myclobutanil, Novaluron, O-methoate, Oxadiargyl, Oxadiazon, Oxydemeton methyl, Paclobutrazole, , Paraoxon-methyl, Paraquat, Penconazole, , Phorate sulfone, Phorate sulfoxide, , , Pirimiphos-methyl, ,

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Chemical (Analytical) Food & Agricultural Propargite, Propiconazole, Commodities Pyrazosulfuron ethyl, Quinolphos, Quizalofop-ethyl, Simazine, Spinosad-A, D, Sulfosulfuron, Tebuconazole, , Thiochlorprid, Thiodicarb, Thiometon, Thiophenatemethyl, TNFA, TNFG, Triadimefon, Triadimenol, Triallate, Triazophos, Trichlorfon, Tricyclazole, Tridemorph, α-Naphthyl acetic acid Food and Pesticide Residues: LAB_P_SOP_210 GC-MS Agricultural Dithiocarbamates as CS2, Commodities Mancozeb, Metiram, & Propineb Food and Aflatoxins B1, B2, G1 & G2 Lab_P_SOP_225 Agricultural LC-MS/MS Products, Animal Feeds Food and Copper Oxychloride By AAS Agricultural Commodities Nut and Nut Aflatoxin B1, B2, G1 & G2 Lab_P_SOP_225 Products, Cereals & LC-MS/MS Grains, Coffee Fish And Marine Chloramphenicol LAB_P_SOP_43 Products LC-MS/MS Sulfonamides: LAB_P_SOP_48 Sulfamethoxazole, Sulfadoxine, LC-MS/MS Sulfamerazine, Sulfadiazine, Sulfadimethoxine, Sulfapyridine, Sulfamethazine, Sulfachloropyridazine, Sulfamethoxypyridazine, Sulfamethizole, Sulfathiazole Nitrofuran Metabolties: LAB_P_SOP_44 AHD, AMOZ, AOZ, SEM LC-MS/MS Nitrofurans: LAB_P_SOP_96 Furaltadone, Furazolidone, LC-MS/MS Nitrofurantoin, Nitrofurazone Dyes: LAB_P_SOP_148 Crystal violet, Leuco Crystal LC-MS/MS Violet, Malachite green, Leuco Malachite Green Tetracyclines & Epimers: LAB_P_SOP_49 Chlorotetracycline, 4-epi- LC-MS/MS Chlortetracycline, Oxyteracycline, 4-epi-Oxytetracycline, Tetracycline, 4-epi-Tetracycline

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Chemical (Analytical) Fish And Marine Fluoroquinolones: LAB_P_SOP_111 Products Ciprofloxacin, Danofloxacin, LC-MS/MS Difloxacin, Enrofloxacin, Flumequine, Oxolinic Acid, Sarafloxacin, Norfloxacin, Nalidixic acid Antihelmintics : Emamectin LAB_P_SOP_315 benzoate, Ivermectin LC-MS/MS Pesticide Residues: LAB_P_SOP_50 Aldrin, Carbaryl, Chlordane, GC-MS/MS Chlordane, Dieldrin, Endosulfan- α, Endosulfan-β, Endosulfa- sulfate, Endrin, , Heptachlor, Heptachlorepoxide, Hexachlorobenzene, , Methoxychlor, o,p’, p,p’-DDD, o,p’, p,p’-DDE, o,p’, p,p’--DDT Pendimethalin, Quinolphos, Trifluralin, α HCH, β HCH, γ-HCH, δ- HCH Polychlorobiphenyls: LAB_P_SOP_50 PCB28, PCB52, PCB101, PCB138, GC-MS/MS PCB153, PCB180 Ethoxyquin LAB_P_SOP_198 LCMSMS Water (IS Pesticide Residues: LAB_P_SOP_46 14543:2004, IS Alachor, Aldrin, , Butachlor, GC-MS/MS 10500:1994, IS Methyl parathion, Chlordane, 13428:2005) Chlorpyrifos-methyl, Diledrin, o, p’,p,p’--DDT, o,p’,p,p’--DDE, o,p’, p,p’-DDD, Endosulfan-α, Endosulfan-β, Endosulfan sulfate, Ethion, Endrin, Heptachlor, Heptachlor epoxide, α-HCH, β- HCH, γ-HCH, δ-HCH, Hexachlorobenzene , Parathion- methyl, ethyl, Phorate 2,4 – D, Atrazine, Carbaryl, LAB_P_SOP_46 Ethion, Isoproturon, Malaoxon, LC-MS/MS Malathion, Methyl paraoxon, Monocrotophos, Pendimethalin, Phorate Sulfone, Phorate Sulfoxide, Quinolphos, Trifluralin & Simazine Polychlorobiphenyls (PCBs): LAB_P_SOP_46 PCB28, PCB52, PCB101, PCB138, GC-MS/MS PCB153, PCB180

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FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Chemical (Analytical) Water (IS Polyaromatic Hydrocarbons LAB_P_SOP_46 14543:2004, IS (PAHs) GC-MS/MS 10500:1994, IS Acenaphthalene, Acenaphthene, 13428:2005) Anthracene, Benz(a)anthracene, (Council Directive Benzo(a)pyrene, 98/83/EC) Benzo(b)fluoranthene, Benzo(g,h,i)perylene, Benzo(k)fluoranthene, Chrysene, Di-benz(a,h)anthracene, Fluoranthrene, Fluorene, Indeno 1,2,3(c,d)pyrene, Naphthalene, Phenanthrene & Pyrene Water (Council Volatile Organic Compounds LAB_P_SOP_45 Directive 98/83/EC) (VOCs): 1,2-dichloroethane, GC-MS/MS (IS 14543:2004, IS Acrylamide, Benzene, LC-MS/MS 10500:1994, IS Trihalomethanes 13428:2005) (Bromodichloromethane, Bromoform, Chloroform, Dibromochloromethane), Epichlorohydrin, Tetrachloroethene, Trichloroethene & Vinyl Chloride

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