24 Madison Road - Fairfield, NJ 07004 Tel #: 973-439-1401 Fax #: 973-439-1402 [email protected] www.jeen.com Frizz Control and Moisturizer Shampoo

Code Application Body Parts Form Appearance Emulsion Type J18-99B Hair Care Hair Gel Opaque Oil in Water This shampoo formulation has a control frizz property and moisturizing effects. Trade Name

Phase INCI Name % Vendor Highlight Jeen Ingredients

A WATER 21.800 Jeen

B Polymer Jr-30m 0.7500 Amerchol Polyquaternium-10

C JEECOL® CS-20 2.8000 Jeen Ceteareth-20

D WATER 15.000 Jeen

E JEECHEM® CAH-60 2.5000 Jeen Peg-60 Hydrogenated Castor Oil

F JEECHEM® GMO 0.5000 Jeen Glyceryl Oleate

G JEECHEM® SHAMPOO CONC.#5CL 45.000 Jeen Sodium Laureth Sulfate,cocamide Dea,cocamidopropyl Betaine

HSodium Chloride 0.1000 Fisher Scientific Sodium Chloride

I JEESILC® 94 3.0000 Jeen Amodimethicone, Trideceth-12, Cetrimonium Chloride

J Fragance 0.0500 West Fragance Marine Type B

K JEECOL® LA-7 3.3000 Jeen Laureth-7

L JEECIDE® P 1.0000 Jeen Phenoxyethanol,methylparaben,ethylparaben,buty lparaben,propylparaben,isobutylparaben L PROPYLENE GLYCOL USP 1.5000 Jeen Propylene Glycol

M SALICYLIC ACID 0.2000 Jeen Salicylic Acid

N AVOCADO OIL 1.0000 Jeen Persea Gratissima (avocado) Oil N GRAPE SEED OIL 1.0000 Jeen Vitis Vinifera (grape) Seed Oil N Sodium Benzoate 0.5000 Fisher Scientific Sodium Benzoate

100.0000 % Procedure Product Specifications 1 Mix water and Polymer JR-30M until homogenous at 60C degrees Appearance Gel Shampoo 2 Add Jeecol CS-20 Stability @ RT/45C° / FT 11-10-2012 3 Add Water mix slowly Start Date 4 Add Jeechem CAH-60 mix until homogenous Stability @ RT/45C° / FT 02-10-2013 5 Add Jeechem GMO End Date 6 Add Jeechem Concentrate #5CL mix until homogeous, mix slowly to avoid Ph 5.3 bubbles Viscosity 6,739cps 7 Add sodium chloride mix until homogenous 8 Add Jesilc 94 and Fragance 9 Add Jeecol LA-7 and Jeecide P mix until homogenous 10 Add Propylene Glycol and Salicylic acid keep mixing until a good dispersion of the salycylic acid. 11 Continue adding oils mix well and Add Sodium Benzoate. 12 keep mixing until you see a good emulsion and the shampoo look opaque, reduce heat and pour it at 25C degrees You Can Count On Us! This information is furnished without warranty, expressed or implied, except that it is accurate to the best knowledge of JEEN International Corporation. The data on this sheet relates only to the specific material designated herein