, . VJU|FCI J U « ENVIRONMENTAL LABORATORIES, INC. ^Jf'­ I^ S flnaivtieaianalytica l testintestinag ananddenvironmentaenvironmentallsciencesciencess liKfcAK 142 Twipto SSMt Nmv Haven CT 06510 (203) 789-1260 OTHER: J^jg}{^ EPA«C7-02t Com. Cen. #PH.04SC /' ' NAME/ADDRESS: Mr. Robert F. Moody Raymark Industries, Inc. SDMS DocID 464969 . 75 East Main Street Stratford, CT 06497 E U PROJECT NUMBER: 91-545-18 EU SAMPLE NUMBER(S): 93-0090 ­ 93-0092 COIXECTED BY: EU/JP DATE COU£CTED: 1-24-94 DATE RECEIVED: 1-25-94 COMPLETION DATE: 1-31-94 Reviewed and Approved by: Date: yj^/y y^oben Schock, Laboratory Division Manager Tltis icpon b 'PROPRIETARY AND CONFIDENTIAL* and delivered to, and intended for the exclusive uie of tbe above named clieol only. Environmenul Labotaioriea, Inc. aiaimea no ieq>ooiibility or liability for the reliance hereon or uae hereof by anyone other than the above named client. 94FEBWK1J A SUBSIDIARY OF ENVIRONMENTAL AND INFRASTRUCTURE CONSULTANTS. INC. (EICON) BRIDGEPORT . NEW HAVEN • HARTFORD RESULTS OF ANALYSIS; SAMPLE DESCRIPnON: SB-68 02-04 SB-7 04-06 SB-68 06-08 EU SAMPLE NUMBER: 93-0090 93-0091 93-0092 FARAMETER UNITS TotalLead: Wet Weight 2,593 mg/Kg 1.56 % W/W 1.44 % W/W Diy Weight 2,998. mg/Kg 2.44 * W/W 2.01 % W/W Total PCB's: Wet Weight 45.9^ 177.» 76.8' mg/Kg Dry Weight 53.1' 277.' 107.' mg/Kg Percent Solid 86.5 63.9 71.7 % ' Matrix spike sample for lead analysis out of laboratory control limits (of 75 - 125 %) for this batch. Probably due to a dilution of the sample because elevated analyte levels. All other QA/QC are within laboratory control limits. ' Aroclor 1268 ND • Nooe Detected BDL - Below Dctrctioa Limit ENVIh /lENTAL LABORATORIES. INC. Chain Custody 142 Tompio Street /V». Haiieh, Cl ' Oi anal/ticai tatting and environmerttsl sciences Conn. C««t. #PM-0450 EPA IC Project Name: Raymark Phase UB ANALYSIS REQUIRED Project Location: Stratford, Conaectictit ITIM NUr^lBER: 10 III I U U 14 Project Number: 91-545-11 Tn LABORATORY: EU AQUATEC EEG TLI B««tlc Siic/Code: LAB No. »r B«ttl(s: ID pTBerre: ANALVnCAL TESTING D c C METHODS A o a STA. T M M A SAMnt iDooincATiot* FVMC lOltl No. C C r NUMSU A^a /roo t / cxm 4^ nnt> rvff-.7-. if li^ i \nof/ gg" r/^/W /^ ^ • OQit _L Sowct CODES: W - WEUL O - OUTTALL T - TANK SG « SLUDOC S - SOIL PnaEnvATivE CODES: A - ASCORBIC AOD N - Nmuc Aao (HNOJ S - SOOIUM - POTTLE CooB; L - LAOOON TR - TREATED X - OTKEK • - DEFINE HYDROXIDE (NAOH) H - HYDROcmjORJC Aao (HCL) I - ICED F - FILTCR£D E - A»«ER EPA VIAL BomjSTZt: 1 - 40 cc 2 - I25CC 3 - 230cc 4 - 500 cc J - JOOOcc T - SODIUM THiosiaFAtE f - SULFURIC AaixH,SO,) Z - ZINC ACETATE A - AMBOI C • CLEAI SAMPLER'S SIGNATURE AfTILIATION Time TRNSF ITEM .TRANSFERS NO. NO. CINQI ACCEPTED BV DATE TIME ± ^^l^^-j^j^ fgj^ ^ /loO^ RCMAIU'ftM^-U . / J I ll ArlUikL fy^' ill-/ (fille^rtl S^f/«:)«.^.1 ' n ENVIRONMENTAL LABORATORIES, INC. i^ B 5 analytical testing ani d environmental sciences 142 Tample SsMt Naw Haven CT 06510 (203) 789-1260 EPA «CT-0. Conn. Can #PH.04 NAME/ADDRESS: Mr. Robert F. Moody Raymark Industries, Inc. 75 East Main Street Stratford, CT 06497 FTI PROJECT NUMBER: 91-545-17 FT ,1 SAMPLE NUMBER(S): 94-0050 COLLECTED BY: EU/JP DATE COLLECTED: 1-18-94 DATE RECEIVED: 1-18-94 COMPLETION DATE: 1-24-94 Reviewed and yy/yi- ^ y^^ / n / ^^/^/ Anprovcd bv: .^'P^^ J^^^^JY Date: / ' X / " / 7 " Robert'Schock, I iiboratory Division Manager TUi fcpon U 'PROPRIETARY AND CONI-IDENTIAL' UKI deiivet«d to, and mteoded for the exclutive ueeofthe above named clieiu only. Eaviromneaial Labofatoriea, Inc. anumea no reqmnnbUity or liability for tbe reliance bereao or uae beieof by anyone other than tbe above named ciieal. 94iANWK4.24 I A SUBSIDiARV o r ENVIRONMENTAL AND INFRASTTtUCTunE CONSULTANTS. INC. (EICON) BRIDGEPORT • NEW HAVEN . HARTFORD }fY^}^Jfi OF ANALYSIS: SAMPLE TOTAL TCLP SLP DESCRIPTION LEAD LEAD LEAD EU SAMPLE mg/Kg mg/L mg/L NUMBER: 94^50 SBIO 18-48" 37. 0.34 ND < 0.20 Percent SoUds = 95.7 ND - None Detected BDL > Below Detectioo Limit RK5UT.TS OF ANALYSE! METOOD 8080 PC35 SAMPLE DESCRIPTION: SBIO 18-48" KI J SAMPLE NUMBER: 94-0050 TOTAL TCLP SIJ» (ms/Kg) (mg/L) (mg/L) PCB-1016 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1221 ND < 2.0 ND < 0.020 ND < 0.020 PCB-1232 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1242 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1248 ND < 0.2 ND < 0.002 ND < o.m PCB-1254 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1260 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1262 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1268 7.1 ND < 0.001 ND < 0.001 ND - None Delected BDL - Below Detection Liniit i-ivviH i tvlAL LABORATUmES . INC . Chain "ustody 142 r«rti,»(cj Street /V«» ven. c r 0 6 ''""'vJical I ,j find environmental ,scJencas Conn. Cert. #PH O450 CPAdCT ^V.^ject Name: Rayiii-rk Phase IIH f*rojecl Locafioii: Siirtirord, Conjietiii ui • VViijt;; Ntimber; 91 .'^45-17 SuuacECopf.^; w := wiji. o ­ otHFAij. r ­ 'IH K SO ­ Smxit <; ­ SOIL PHI-AljivAnVtCOPei: A = A'» OK BIC ACID N ­ NiTKU: ALIO (HNOJ S ­ S'HillAt­ L ­ LAOOON TR ­ I«I:>IT-U X ­ OTMM • pimsc llM)Ri)>.l|lF. (NAOH ) H " IbliKiKTHIORICACID fHCl.) I ­ IcCD F " Fll1t«>X) E ­ AMRIJI EPA VIAL BomjStZ^: I . 40.f . ^ |2JoC J ­ 2VI.. 4 . SOO CC S ­ l<t<ifi .; r ­ SiiliKIMDttOSULfAlK V ' Stlll-imiC AOtHHjSO.t Z ­ ZlMC ACtTATF. A ­ AMBUl C ­ CLEAK bAMPLER'^ SVjfiA niHI; A»Mi I ^ | u REMABU: Oc/'^Cy<J L W ENVIRONMENTAL LABORATORIES, INC. I- 5 analytical testing and environmental sciences M2 Tenvte StiMi NMT HMon CT 06510 (203) 789-1260 EPA«CT< Com. Ccn «PH.O­ NAME/ADDRESS: Mr. Robert F. Moody Raymaik Industries, Inc. 75 East Main Street Stratford, CT 06497 FT .1 PROJECT NUMBER: 91-545-17 E U SAMPLE NUMBERCS): 94-0050 COLLECTED BY: EU/JP DATE COLLECTED: 1-18-94 DATE RECEIVED: 1-18-94 COMPLETION DATE: 1-24-94 Reviewed and /^yP\- ^ / ^ / yi>/ ^^/^Z Aooroved bv: ^ ^ Jy<^^j7^ Date: /'P/r-/ y Robert'Schock, 1.ahoratory Division Manager Thu fcpoft it 'PROPRIETARY AND CONFIDENTIAL' and deliverad lo, end intended for the excluiive the relience beraoo or lue hereof by anyone other than tbe above named cbent. 94JANWK4J4 1 A SUBSIDIARV (3F ENVIRONMENTAI. AND INFRASTRUCTURE CONSULTANTS. INC. (EICON) BRIDGEPORT . NEW HAVEN . HARTFORD SAMPLE TOTAL TCLP SLP DESCRIPTION LEAD LEAD LEAD F U SAMPLE mg/Kg mg/L mg/L NUMBER: 94-0050 SBIO 18-48" 37. 0.34 ND < 0.: Percent Solids = 95.7 ND - None Detected BDL - Below Detection Limit FRSTTT.T? Of ANAl-YSJS: MKTHQP g08Q ECBs SAMPLE DESCRIPTION: SBIO 18-48' E U SAMPLE NUMBER: 94-0050 TOTAL TCLP SLP (mg/Kg) (mg/L) (mg/L) PCB-1016 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1221 ND < 2.0 ND < 0.020 ND < 0.020 PCB-1232 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1242 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1248 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1254 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1260 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1262 ND < 0.2 ND < 0.002 ND < 0.002 PCB-1268 7.1 ND < 0.001 ND < 0.001 ND - None Detected BDL • Below Detection Limit i-WviHL fcMAL LABORAIUMIES, INC. Cham Custody 142 refrr.,^16 Street fit /avan. CT Oi inniytlcal ^ttni hnd environmental science! Conn. Cert. *PM O4S0 EPA fC yr»]tti Nttnit: Rayin-rk Phase IIB ANALYSIS REQlrtRI'n Projec* LocalHiiv: Siiatfoid, Coimctii>ui l*riije.} Ntimber: 91 .'45-17 •rrrst si -.frcR: II U I; 13 14 LAM)h>.":.)KV: • Ell '-Ul.ATEC EEC Tl.l V-M S:..> ud«: O L LAD Ne. of B- ti<rs: ID fx^terte: s ANAl.^":^<:M, • I TEST INC D c c ^u:TMllll^ A o a nd d ('•.«t«.iiti T A I ?» S o ( ti! ^ l^^l--iIilki\cy*.'L • X fn-fi tf'Hf^ t / TYCO.!. V ± StiiiBCECopf4| w •= wijj o - OuTFAij r • '»NK so ­ siiixit ^ ­ suit |'»ni>VAnv|-Copet: A = AN.-iSBic ACIO N - Nir«ii: ACID (HNOJ S •S'iiiiu»4­ L - LAUOON TR - lRi>iH) X - Omi^ji • MiiivE llMXiiMiiF. (NAOH) 11 « ihincK.-HiflwcAaDfllCi.) I - IccD F - Fiin»u) E - AMDia EPA VIAL BuULtlEt 1-40.1 . - iJJcc 3 - jvi.. 4 J ^oooc 5 - i'l"! •; r - SiiiiKiM TXlOSUIjAtl-. V "^ SdltllKIC Aai><H,S(l.t Z - TIMC AtWAlF. A - AMBUI C - CLEA )N ^^••p^\i^^ 7?I7l ft X REI4ABK*: W ENVIRONMENTAL LABORATORIES. INC. I- " analytical testing and environmental sciences M2 TenwM SiiMl Nr» Havwi CT 06510 (203) 789-1260 EPA «CTO Com Cen «PH.Od NAME/ADDRESS: Mr. Robert F. Moody Raymaik Industries, Inc. 75 East Main Street Stratford, CT 06497 E U PROJECT NUMBER: 91-545-17 FU SAMPLE NUMBER(S): 94-0050 COLLECTED BY: EU/JP DATE COLLECTED: 1-18-94 DATE RECEIVED: 1-18-94 COMPLETION DATE: 1-24-94 Reviewed and /yfy)- ^ ^y* / yi// ^ y / ADDTOvedbv: y^<> J^.^£y/r Date: /'P/X'/ z - ' Robert Schock, Laboratory Division Manager Tliii repon b -PROPRIETARY AND CONFIDENTLa* and deliverad lo.