ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC. VOLATILE ORGANIC ANALYSIS CUSTOMER NAME: OBG LABORATORIES, INC. • MR. MIKE PETTERELLI SAMPLE SOURCE: Blosenskl Landfill_________________ WORK ORDER NO.: N/A________ PROJECT NO.: 12319 DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-16-90 SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 0.50 ANALYST: J. Tobler DILUTION FACTOR: 1.00 CUSTOMER SAMPLE NO.: AS-l-60 EHRT SAMPLE NO.: 29460 NOTEBOOK NO.: 162, Pg. 9_______ METHOD NO.: EPA6Q1&602 RESULT COMPOUNDS UQ/L 1. Bromodlchloromethane < 5.00 2. Bromoform < 5.00 3. Bromomethane < 5.00 4. Carton Tetrachloride < 5.00 5. Chlorobenzene 22.10 6. Chloroethane < 5.00 7. 2-CWoroethyMnyl Ether < 5.00 8. Chloroform 96.60 9. Chloromethane < 5.00 10. DlbromocMoromethane < 5.00 11. 1,2-DlcWorobenzene < 5.00 12. 1,3-DfchIorobenzene < 5.00 13. 1,4-DIchfoFobenzene < 5.00 14. DlcWorodffluofomethane < 5.00 15. 1,1-Dlchloroethane 34.10 ia 1,2-Dtchloroethane < 5.00 17. 1,1 -Dlchloroethene < 5.00 18. trans-1,2-Dlchloroethene 103.70 19. 1^-DIch(oropropane < 5.00 20. c!s-1,3-D!chloropropene < 5.00 21. trans-1,3-DichJoropropene < 5.00 22. Methylene Chloride < 10.00 AR002I 13 CUSTOMER SAMPLE NO.: AS-l-60 EHRT SAMPLE NO.: 29460 23. 1,1,2,2-Tetrachloroethane < 5.00 24. Tetrachloroethene < 5.00 25. 1,1,1-Trichloroethane 135.90 26. 1,1,2-Trichloroethane < 5.00 27. Trichloroethene 68.60 28. Trichlorofluoromethane < 5.00 29. Vinyl Chloride < 5.00 30. Benzene 1286.70 31. Ethylbenzene < 5.00 32. Toluene < 5.00 SURROGATE STANDARDS - % RECOVERIES 1,2-Dichloroethane-d4 - ____110.00% Toluene-d8 - 81.00% Bromofluorobenzene - 98.00% COMPUTER SEARCH Acetone - Approx. 111.60 ug/L 4R002I \k ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC. VOLATILE ORGANIC ANALYSIS CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELU SAMPLE SOURCE: Blosenski Landfill______________ WORK ORDER NO.: N/A__________ PROJECT NO.: 12319 DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-14-90 SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00 ANALYST: J.Tobler DILUTION FACTOR: 1.00 CUSTOMER SAMPLE NO.: AS-E-60 ___ EHRT SAMPLE NO.: 29461 LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA 601 & 602 RESULT COMPOUNDS____ ug/L 1. Bromodichloromethane < 0.50 2. Bromoform < 0.50 3. Bromomethane < 0.50 4. Carbon Tetrachloride < 0.50 5. Chlorobenzene 2.94 6. Chloroethane < 0.50 7. 2-Chloroethylvinyl Ether < 0.50 8. Chloroform 17.05 9. Chloromethane < 0.50 10. Dibromochloromethane < 0.50 11. 1,2-Dichlorobenzene < 0.50 12. 1,3-Dichlorobenzene < 0.50 13. 1,4-Dichlorobenzene < 0.50 14. Dichlorodifluoromethane < 0.50 15. 1,1-Dichloroethane 5.04 16. 1,2-Dichloroethane < 0.50 17. 1,1-Dichloroethene < 0.50 18. trans-1,2-Dichloroethene 18.00 19. 1,2-Dichloropropane < 0.50 20. cis-1,3-Dichloropropene < 0.50 21. trans-1,3-Dichloropropene < 0.50 22. Methyiene Chloride < 1.00 CUSTOMER SAMPLE NO.: AS-E-60________ EHRT SAMPLE NO.: 29461 23. 1,1,2,2-Tetrachloroethane < 0.50 24. Tetrachloroethene < o.SO 25. 1,1,1-Trichloroethane . 7.15 26. 1,1,2-Trichloroethane < 0.50 27. Trichloroethene 4.40 28. Trichlorofluoromethane < 0.50 29. Vinyl Chloride < 0.50 30. Benzene 122.61 31. Ethylbenzene < 0.50 32. Toluene < 0.50 SURROGATE STANDARDS - % RECOVERIES 1,2-Dichloroethane-d4 - ____98.00% Toluene-d8 - 93.00% Bromofluorobenzene - 100.00% Page2 SR002I I 6 SOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY j Name: ENVIRONMENTAL HEALTH RESEARCH AND TESTING. INC.______ " stomerName: OBG LABORATORIES. INC. - MR. PETTERELU_______________ Method No.: EPA 601 & 602______ Project No.: 12319 stomer Sample No.: AS-E-60_________ EHRTNo.: 29461 AMOUNT ADDED SAMPLE CONC. MS CONC. MS% QC LIMITS COMPOUND (ng) (ug/L) (ug/L) REC# REC. -Dichloroethene 250 0 56.22 112 59-172 jhloroethene 250 4.4 62.2 116 62-137 Benzene 250 123 190.8 136 66-142 uene 250 0 56.1 112 59-139 'orobenzene 250 2.9 57.6 109 60-133 MSD CONC. MSD% MS% % QCLI tflTS MPOUND (ug/L) REC# REC# RPD# RPD REC. , , . -Dichloroethene 57.5 115 112 3 22 59-172 Trichloroethene 64.8 121 116 4 24 62-137 izene 178.6 111 136 20 21 66-142 . -,uene 58 116 112 4 21 59-139 Chlorobenzene 58 110 109 0.01 21 60-133 # Column to be used to flag recovery and RPD values with an asterick . aiues outside of QC limits RPD: _____0____ out of 5 outside limits Spike Recovery:_____0____ out of 10 outside limits 'MMENTS: Page1 3RQQ2II7 ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC. VOLATILE ORGANIC ANALYSIS CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI SAMPLE SOURCE: Blosenski Landfill ____ ____ . WORK ORDER NO.: N/A___________ PROJECT NO.: 12319 DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-15-90 SAMPLE TYPE: Water Sample_____ SAMPLE VOLUME: 0.50 ANALYST: J.Tobler DILUTION FACTOR: 1.00 CUSTOMER SAMPLE NO.: AS-l-50 EHRT SAMPLE NO.: 29462 LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA601&602 RESULT COMPOUNDS_____ ug/L 1. Bromodlchloromethane < 5.00 2. Bromoform < 5.00 3. Bromomethane < 5.00 4. Carbon Tetrachloride < 5.00 5. Chlorobenzene 17.30 6. Chloroethane < 5.00 7. 2-Chloroethylvinyl Ether < 5.00 8. Chloroform 85.40 9. Chloromethane < 5.00 10. Dibromochloromethane < 5.00 11. 1,2-Dichlorobenzene < 5.00 12. 1,3-Dichlorobenzene < 5.00 13. 1,4-Dichlorobenzene < 5.00 14. Dichlorodifluoromethane < 5.00 15. 1,1-Dichloroethane 30.00 16. 1,2-Dichloroethane < 5.00 17. i,1-Dichloroethene < 5.00 18. trans-1,2-Dichloroethene 91.50 19. -1,2-Dichloropropane < 5.00 20. cis-1,3-Dichloropropene < 5.00 21. trans-1,3-Dichloropropene < 5.00 22. Methylene Chloride < 10.00 Page 1 CUSTOMER SAMPLE NO.: AS-l-50 _____ EHRT SAMPLE NO.: 29462 23. 1,1,2,2-Tetrachloroethane < 5.00 24. Tetrachloroethene < 5.00 25. 1,1,1 -Trichloroethane 117.70 26. 1,1,2-Trichloroethane < 5.00 27. Trichloroethene 37.10 28. Trichlorofluoromethane < 5.00 29. Vinyl Chloride < 5.00 30. Benzene 1210.70 31. Ethylbenzene < 5.00 32. Toluene < 5.00 SURROGATE STANDARDS - % RECOVERIES 1,2-Dichloroethane-d4 - ____106.00% Toluene-d8 - 78.00% Bromofluorobenzene - 112.00% Page2 flR002l 19 ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC. VOLATILE ORGANIC ANALYSIS CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELU SAMPLE SOURCE: Blosenski Landfill WORK ORDER NO.: N/A_____________ PROJECT NO.: 12319 DATE EXTRACTED: N/A__________ DATE ANALYZED: 1M4-90 SAMPLE TYPE: Water Sample_____ SAMPLE VOLUME: 5.00 ANALYST: J. Tobler_______ DILUTION FACTOR: 1.00 CUSTOMER SAMPLE NO.: AS-E-50 ____ EHRT SAMPLE NO.: 29463 LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA 601 & 602 RESULT COMPOUNDS____ ug/L 1. Bromodichloromethane < 0.50 2. Bromoform < 0.50 3. Bromomethane < 0.50 4. Carbon Tetrachloride < 0.50 5. Chlorobenzene 1.98 6. Chloroethane < 0.50 7. 2-Chloroethylvinyl Ether < 0.50 8. Chloroform 10.92 9. Chloromethane < 0.50 10. Dibromochloromethane < 0.50 11. 1,2-Dichlorobenzene < 0.50 12. 1,3-Dichlorobenzene . < 0.50 13. 1,4-Dichlorobenzene < 0.50 14. Dichlorodifluoromethane < 0.50 15. 1,1-Dlchloroethane 3.23 16. 1,2-Dlchloroethane < 0.50 17. 1,1-Dichloroethene < 0.50 18. trans-1,2-Dichloroethene 11.61 19. 1,2-Dichloropropane < 0.50 20. cis-1,3-Dichloropropene < 0.50 21. trans-1,3-Dichloropropene < 0.50 22. Methylene Chloride < 1.00 Page1 3RQG2I20 CUSTOMER SAMPLE NO.: AS-E-50________ EHRT SAMPLE NO.: 29463 23. 1,1,2,2-Tetrachloroethane < 0.50 24. Tetrachloroethene < 0.50 25. 1,1,1-Trichloroethane 4.44 26. 1,1,2-Trichloroethane < 0.50 27. Trichloroethene < 0.50 28. Trichlorofluoromethane < 0.50 29. Vinyl Chloride < 0.50 30. Benzene 81.19 31. Ethylbenzene < 0.50 32. Toluene < 0.50 SURROGATE STANDARDS - % RECOVERIES 1,2-Dichloroethane-d4 - ____97.00% Toluene-d8 . - 98.00% Bromofluorobenzene - 103.00% Page2 ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC. VOLATILE ORGANIC ANALYSIS CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELU SAMPLE SOURCE: Blosenski Landfill_________________ WORK ORDER NO.: N/A__________ PROJECT NO.: 12319 DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-09-90 SAMPLE TYPE: Water Blank A SAMPLE VOLUME: 5.00 ANALYST: J.Tobler DILUTION FACTOR: 1.00 CUSTOMER SAMPLE NO.: N/A__________ EHRT SAMPLE NO.: N/A LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA601&602 RESULT COMPOUNDS____ ug/L 1. Bromodichloromethane < 0.50 2. Bromoform < 0.50 3. Bromomethane < 0.50 4. Carbon Tetrachloride < 0.50 5. Chlorobenzene < 0.50 6. Chloroethane < 0.50 7. 2-Chloroethylvinyl Ether < 0.50 8. Chloroform < 0.50 9. Chloromethane < 0.50 10. Dibromochloromethane < 0.50 11. 1,2-Dichlorobenzene < 0.50 12. 1,3-Dichlorobenzene < 0.50 13. 1,4-Dichlorobenzene < 0.50 14. Dlchlorodifluoromethane < 0.50 15. 1,1-Dichloroethane < 0.50 16. 1,2-Dichloroethane < 0.50 17. 1,1-Dichloroethene < 0.50 18. trans-1,2-Dichloroethene < 0.50 19. 1,2-Dichloropropane < 0.50 20. cis-1,3-Dichloropropene < 0.50 21. trans-1,3-Dichloropropene < 0.50 22. Methylene Chloride < • 1.00 AR002I22 CUSTOMER SAMPLE NO.: N/A__________ EHRT SAMPLE NO.: N/A 23. 1,1,2,2-Tetrachloroethane < 0.50 24. Tetrachloroethene < 0.50 25. 1,1,1-Trichloroethane < 0.50 26. 1,1,2-Trichloroethane < 0.50 27. Trichloroethene < 0.50 28. Trichlorofluoromethane < 0.50 29. Vinyl Chloride < 0.50 30. Benzene < 0.50 31. Ethylbenzene < 0.50 32. Toluene 0.76 SURROGATE STANDARDS - % RECOVERIES 1,2-Dichloroethane-d4 - ____96.00% Toluene-d8 - 100.00% Bromofluorobenzene - 98.00% Page2 3R002123 ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC. VOLATILE ORGANIC ANALYSIS CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELU SAMPLE SOURCE: Blosenski Landfill WORK ORDER NO.: N/A__________ PROJECT NO.: 12319 DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-14-90 SAMPLE TYPE: Water Blank B SAMPLE VOLUME: 5.00 ANALYST: J.Tobler DILUTION FACTOR: 1.00 CUSTOMER SAMPLE NO.: N/A__________ EHRT SAMPLE NO.: N/A LAB NOTEBOOK NO.: 162.