Pesticide Analytical Manual Vol. I INDEX: METHODS Index to PAM I Methods, by Chemicals Tested for Recovery 1,1'-(2,2-dichloroethylidene)= 2,3-dihydro-3,3-methyl-2-oxo- 2-methoxy-3,5,6- 3-hydroxymethyl-4,5-dimethyl bis(2-methoxybenzene) 5-benzofuranyl methyl trichloropyridine phenyl methylcarbamate Sec. 303 C1-C2 R sulfonate Sec. 302 C5 P Sec. 401 DL1 C 1,2,3,5-tetrachlorobenzene Sec. 302 C5 NR Sec. 302 no C C 3-ketocarbofuran Sec. 302 E2/E3+C1 V Sec. 402 E1 NR Sec. 303 C1 P( Sec. 302 no C S Sec. 303 C1 P Sec. 402 E2 NR Sec. 303 C2 C Sec. 303 C1-C2 NR Sec. 303 C2 C 2,4,5-T Sec. 304 C1-C4 C Sec. 304 C1-C4 NR Sec. 304 E1-E5+C6 V Sec. 402 E1 P 3,4,5-trimethacarb Sec. 401 DL1 V 1,2,3-trichlorobenzene Sec. 402 E2 P Sec. 302 C3+DL1 C 3-methyl-4-nitrophenol Sec. 303 C1-C2 C 2,4,5-trichloro-alpha- Sec. 302 no C C Sec. 302 no C V Sec. 304 C1, C3 P methylbenzenemethanol Sec. 303 C2 NR Sec. 303 C1-C2 NR 1,2,4,5-tetrachloro-3- Sec. 302 no C R Sec. 304 C2, C4 NR Sec. 304 C1-C4 NR (methylthio)benzene Sec. 303 C1-C2 R Sec. 401 DL1 C 3-tert-butyl-5-chloro-6- Sec. 302 no C R 2,4-D 3,4-dichloroaniline hydroxymethyluracil Sec. 303 C1-C2 C Sec. 402 E1 P Sec. 302 no C V Sec. 303 C1-C2 NR Sec. 304 E1-E5+C6 C Sec. 402 E2 P Sec. 303 C1-C2 S Sec. 304 C1-C4 NR 1,2,4-triazole 2,4-DB 3,4-dichlorophenylurea 4'-hydroxy bifenthrin Sec. 302 no C V Sec. 402 E1 C Sec. 303 C1-C2 NR Sec. 302 no C C Sec. 303 C1-C2 NR Sec. 402 E2 C Sec. 304 C1-C4 NR 4-(dichloroacetyl)-1-oxa-4- Sec. 304 C1-C4 NR 2,4-dichloro-6- 3,5,6-trichloro-2-pyridinol azapiro[4.5]decane 1-hydroxychlordene nitrobenzenamine Sec. 402 NR Sec. 302 no C C Sec. 303 C1-C2 R Sec. 303 C1-C2 R 3,5-dibromo-4- Sec. 303 C1-C2 P 10,10-dihydromirex 2,6-dichlorobenzamide hydroxybenzoic acid 4-chloro-6-methoxyindole Sec. 303 C1-C2 C Sec. 302 C5 NR Sec. 402 S Sec. 303 C1 R 10-monohydromirex Sec. 302 no C C 3,5-dichloroaniline 4-chlorobenzoic acid Sec. 303 C1-C2 C Sec. 303 C1-C2 NR Sec. 302 no C S Sec. 402 E1 S 2,3,5,6-tetrachloroaniline Sec. 304 C1-C4 NR Sec. 303 C1-C2 S Sec. 402 E2 S Sec. 303 C1-C2 R 2,8-dihydromirex Sec. 304 C1-C4 S 4-chlorobenzylmethyl sulfone 2,3,5,6-tetrachloroanisidine Sec. 303 C1-C2 C 3-(3,4-dichlorophenyl)-1- Sec. 303 C1-C2 NR Sec. 303 C1-C2 C 2-chloroethyl caprate methoxyurea Sec. 304 C1-C4 NR Sec. 304 E1-E5+C6 V Sec. 303 C1-C2 C Sec. 302 no C R 4-chlorobenzylmethyl 2,3,5,6-tetrachloroanisole Sec. 304 C1-C4 C Sec. 303 C1-C2 NR sulfoxide Sec. 303 C1-C2 C 2-chloroethyl laurate Sec. 304 C1-C4 NR Sec. 303 C1-C2 NR Sec. 304 E1-E5+C6 C Sec. 303 C1-C2 C 3-carboxy-5-ethoxy-1,2,4- Sec. 304 C1-C4 NR 2,3,5,6-tetrachloronitro= Sec. 304 C1-C4 C thiadiazole 4-chlorophenoxyaniline anisole 2-chloroethyl linoleate Sec. 302 no C NR Sec. 302 no C S Sec. 303 C1-C2 C Sec. 303 C1-C2 V Sec. 402 NR 4-CPA Sec. 304 E1-E5+C6 V Sec. 304 C1-C4 P 3-chloro-5-methyl-4-nitro-1H- Sec. 402 E1 S 2,3,5,6-tetrachlorotere= Sec. 304 E1-E5+C6 V pyrazole Sec. 402 E2 C phthalic acid 2-chloroethyl myristate Sec. 302 no C C 4-hydroxymethyl-3,5-dimethyl Sec. 402 E1 NR Sec. 302 no C C 3-chlorosulfonamide acid phenyl methylcarbamate Sec. 402 E2 NR Sec. 303 C1-C2 V Sec. 402 NR Sec. 303 C1-C2 NR 2,3,5-triiodobenzoic acid Sec. 304 C1-C4 V 3-desmethyl sulfentrazone Sec. 304 C1-C4 NR Sec. 402 E1 V 2-chloroethyl palmitate Sec. 303 C1-C2 NR Sec. 401 DL1 C Sec. 402 E2 V Sec. 303 C1-C2 V Sec. 304 C1-C4 NR 6-chloro-2,3-dihydro-3,3,7- 2,3,5-trimethacarb Sec. 304 C1-C4 P 3-hydroxycarbofuran methyl-5H-oxazolo(3,2- Sec. 302 C3+DL1 C Sec. 304 E1-E5+C6 V Sec. 302 C3+DL1 C a)pyrimidin-5-one Sec. 302 no C C 2-hydroxy-2,3-dihydro-3,3- Sec. 302 E1/E4+C4 C Sec. 303 C1-C2 NR Sec. 303 C1 S methyl-5-benzofuranyl methyl Sec. 401 DL1 C Sec. 304 C1-C4 NR Sec. 303 C2 NR sulfonate 3-hydroxymethyl-2,5-dimethyl 6-chloro-2,3-dihydro-7- Sec. 304 C2, C4 NR Sec. 302 C5 NR phenyl methylcarbamate hydroxymethyl-3,3-methyl- Sec. 401 DL1 C Sec. 402 E1 NR Sec. 303 C1-C2 NR 5H-oxazolo(3,2-a)pyrimidin- 2,3,6-TBA Sec. 402 E2 NR Sec. 304 C1-C4 NR 5-one Sec. 402 E1 C Sec. 401 DL1 P Sec. 303 C1-C2 NR Sec. 402 E2 C Sec. 304 C1-C4 NR Codes: C: complete (recovery); P: partial; S: small; V: variable; R: recovered; NR: not recovered Transmittal No. 96-E1 (9/96) Form FDA 2905a (6/92) INDEX: METHODS–1 INDEX: METHODS Pesticide Analytical Manual Vol. I 6-chloronicotinic acid Sec. 304 C1, C3 C atrazine Sec. 303 C1-C2 C Sec. 303 C1-C2 NR Sec. 304 C2, C4 P Sec. 302 C5 C Sec. 304 C1-C4 C Sec. 304 C1-C4 NR allidochlor Sec. 302 no C C bifenox 6-chloropicolinic acid Sec. 302 no C C Sec. 303 C1 S Sec. 302 no C C Sec. 402 NR Sec. 303 C1-C2 NR Sec. 303 C2 NR Sec. 303 C1-C2 C 8-monohydromirex allophanate Sec. 304 C1-C4 NR Sec. 304 C1-C4 P Sec. 303 C1-C2 C Sec. 404 C azinphos-ethyl Sec. 402 E1 C AC 263,222 ammonium salt alloxydim-sodium Sec. 302 C5 C Sec. 402 E2 C Sec. 402 NR Sec. 402 E1 NR Sec. 302 no C C bifenthrin acephate Sec. 402 E2 NR Sec. 303 C1 P Sec. 302 C5 C Sec. 302 E1/E4+C2 C alpha-cypermethrin Sec. 304 C1, C3 S Sec. 302 no C V Sec. 302 no C C Sec. 302 E2/E3+C1 C azinphos-methyl Sec. 303 C1-C2 C acetochlor Sec. 302 no C C Sec. 302 no C C binapacryl Sec. 302 C5 C Sec. 303 C1-C2 C Sec. 303 C1-C2 NR Sec. 302 C5 C Sec. 302 no C C Sec. 304 E1-E5+C6 C Sec. 304 C1-C4 NR Sec. 302 no C C Sec. 303 C1 C ametryn azinphos-methyl oxygen Sec. 303 C1-C2 P Sec. 303 C2 P Sec. 302 no C C analog Sec. 304 C1-C4 P Sec. 304 C1-C4 P aminocarb Sec. 302 no C C bioresmethrin acifluorfen Sec. 302 C3+DL1 C benazolin Sec. 302 C5 NR Sec. 303 C1-C2 NR Sec. 302 no C C Sec. 402 E1 NR biphenyl Sec. 304 C1-C4 NR amitraz Sec. 402 E2 NR Sec. 302 C5 C Sec. 402 E1 P Sec. 302 no C S bendiocarb Sec. 302 no C C acrinathrin anilazine Sec. 302 no C C bis(2-ethylhexyl) phthalate Sec. 302 no C V( Sec. 302 no C V Sec. 401 DL1 C Sec. 303 C1-C2 C Sec. 303 C1 V( Sec. 303 C1-C2 S benfluralin Sec. 304 C1-C4 C Sec. 303 C2 V( Sec. 304 C1-C4 P Sec. 302 no C C bis(trichloromethyl)disulfide Sec. 304 C1, C3 NR Sec. 304 E1-E5+C6 S Sec. 303 C1-C2 C Sec. 303 C1-C2 R Sec. 304 C2, C4 V( aramite Sec. 304 C1-C4 C bitertanol alachlor Sec. 302 no C C benodanil Sec. 302 E1/E4+C4 C Sec. 302 C5 P Sec. 303 C1-C2 P Sec. 302 no C C Sec. 302 no C C Sec. 302 no C C Sec. 304 C1-C4 NR benomyl bromacil Sec. 303 C1 C Aroclor 1016 Sec. 302 no C+DL5 C Sec. 302 no C C Sec. 304 C1, C3 C Sec. 303 C1-C2 C Sec. 404 C Sec. 303 C1-C2 NR Sec. 304 C2, C4 S Sec. 304 C1-C4 C benoxacor Sec. 304 C1-C4 NR Sec. 304 E1-E5+C6 S Aroclor 1221 Sec. 302 no C C Sec. 402 E2 NR aldicarb Sec. 303 C1-C2 C Sec. 303 C1-C2 P bromofenoxim Sec. 302 C3+DL1 C Sec. 304 C1-C4 C Sec. 304 C1-C4 C Sec. 402 E1 P Sec. 302 E1/E4+C4 C Aroclor 1242 bensulide Sec. 402 E2 C Sec. 401 DL1 C Sec. 303 C1-C2 C Sec. 302 no C C bromophos aldicarb sulfoxide Sec. 304 C1-C4 C Sec. 303 C1 P Sec. 302 C5 C Sec. 302 C3+DL1 C Aroclor 1248 Sec. 304 C1, C3 C Sec.