United States Patent (19) (11) 3,872,165 Schenk Et Al
United States Patent (19) (11) 3,872,165 Schenk et al. (45) Mar. 18, 1975 54) MANUFACTURE OF WINYL SULFONATES AND WINYLSULFONIC ACID FROM 58 Field of Search................................. 260/513 R CARBYL SULFATE (56) References Cited (75) Inventors: Walter Schenk, Bad Duerkheim; UNITED STATES PATENTS Roland Dahlinger, Neckargemuend; 3,255,240 6/1966 Wolfram et al................. 260/513 R Dieter Stockburger, Gruenstadt, all of Germany OTHER PUBLICATIONS 73) Assignee: Badische Anilin- & Soda-Fabrik Breslow et al., V. Am. Chem. Soc. 79, 5000-5002 Aktiengesellschaft, (1957). Ludwigshafen Rhine, Germany Primary Examiner-Leon Zitver (22) Filed: Nov. 30, 1971 Assistant Examiner-Nicky Chan Attorney, Agent, or Firm-Johnston, Keil, Thompson 21 Appl. No. 203,453 & Shurtleff (30) Foreign Application Priority Data (57) ABSTRACT Nov. 30, 1970 Germany............................ 2058776 Manufacture of vinyl sulfonates and vinylsulfonic acid by saponifying carbyl sulfate under alkaline condi (52) U.S. Cl.............................................. 260/513 R tions. (51) Int. Cl. .......................................... C07c 143/16 3 Claims, No Drawings 3,872,165 1 2 MANUFACTURE OF VINYL SULFONATES AND nates is obtained in a substantially pure form without WNYLSULFONCACID FROM CARBYL SULFATE the formation of a plurality of by-products. This object is achieved in a process for the manufac This invention relates to a process for the manufac ture of vinyl sulfonates and vinylsulfonic acid by treat ture of vinyl sulfonates and vinylsulfonic acid by
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