COMMISSION OF THE EUROPEAN COMMUNITIES
Brussels, 8.2.2007 SEC(2007) 196
COMMISSION STAFF WORKING DOCUMENT
ON THE IMPLEMENTATION OF NATIONAL RESIDUE MONITORING PLANS IN THE MEMBER STATES IN 2005 (Council Directive 96/23/EC)
EN EN
COMMISSION STAFF WORKING DOCUMENT
ON THE IMPLEMENTATION OF NATIONAL RESIDUE MONITORING PLANS IN THE MEMBER STATES IN 2005 (Council Directive 96/23/EC)
The aim of this document is to summarise the actions taken in the Member States as a consequence of the non-compliant results found in food of animal origin through the implementation of Council Directive 96/23/EC on measures to monitor certain substances and residues thereof in live animals and animal products during 2005.
A summary report, including a compilation of the results obtained in the Member States in 2005, broken by food commodities (bovines, pigs, sheep and goats, horses, poultry, aquaculture, milk, eggs, rabbit meat, farmed game, wild game and honey) and groups of substances (hormones, corticosteroids, beta-agonists, prohibited substances, antibacterials, other veterinary medicinal products, “other” substances and contaminants) is attached to this document (“Report for 2005 on the results of residue monitoring in food of animal origin in the Member States”).
TABLE OF CONTENTS
1. INTRODUCTION ...... 1
2. ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS ...... 2
2.1. Sampling as suspect ...... 2
2.2. Modifications of the national plan for 2006 ...... 3
2.3. Other actions taken as a consequence of non-compliant results ...... 3
Annex I: Report for 2005 on the results of residue monitoring in food of animal origin in the Member States (SANCO/3635/2006) ...... 4
Annex II: Modifications of the national residue plan for 2006 and other actions taken as a consequence of non-compliant results...... 50
EN 2 EN
1. INTRODUCTION
Council Directive 96/23/EC1 on measures to monitor certain substances and residues thereof in live animals and animal products requires Member States to adopt and implement a national residue monitoring plan for specific groups of residues. Member States must assign the task of co-ordinating the implementation of the controls to a central public department or body. This department is responsible for drawing up the national plan, co-ordinating the activities of the central and regional departments responsible for monitoring the various residues, collecting the data and sending the results of the surveys undertaken to the Commission each year.
The Directive lays down specific sampling levels and frequencies, as well as the groups of substances to be monitored for each food commodity. Commission Decision 97/747/EC2 lays down additional rules for milk, eggs, honey, rabbits and game.
National monitoring plans should be targeted: samples should be taken with the aim of detecting illegal treatment or controlling compliance with the maximum residue limits (MRLs) for veterinary medicinal products set out in Annexes I and III of Council Regulation (EC) 2377/903, the maximum levels for pesticides set out in Annex II of Council Directive 86/363/EEC4 or the maximum levels laid down in relevant legislation on contaminants. This means that in the national plan the Member States target the groups of animals/gender/age combinations where the probability of finding residues is the highest. This approach is different from random sampling, where the objective is to gather statistically significant data, for instance to evaluate consumer exposure to a specific substance.
Member States must forward annually to the Commission the national monitoring plans, together with the results of their residue monitoring for the previous year, by 31 March at the latest. The Directive lays down a procedure by which the plans are approved on a yearly basis. This procedure involves the Member States.
As laid down in Article 8 of Directive 96/23/EC, the Commission has to report to the Member States, within the Standing Committee on the Food Chain and Animal Health, the outcome of the checks carried out, in particular on the implementation of the national plans and on the development of the situation in the various regions of the Community. To this end, the Commission has summarised the results of the national residue monitoring plans for the year 2006. Trends within the European Union are also indicated by comparison with the 2004 report.
1 OJ L 125, 29.4.1996, p. 10-24 2 OJ L 303, 6.11.1997, p. 12-15 3 OJ L 224, 18.8 1990, p. 1 4 OJ L 221, 7.8.1989, p. 43
EN 3 EN
This summary of results of the national monitoring plans, , was presented to the Member States within the Standing Committee on the Food Chain and Animal Health on 20 November 2006 (Summary report 2005 SANCO/3635/2005- Annex I)
2. ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS
In accordance with Article 8 of Directive 96/23/EC, the Member States were requested, as a follow-up, to provide information on actions taken at regional and national level. The objective is to provide an overview of actions taken as a consequence of non-compliant5 results for residues of non-authorised substances or when the maximum residue limits (MRLs) established in EU legislation are exceeded.
In order to collect information on actions taken as a consequence of non- compliant results, the Commission sent a questionnaire to the Member States. These actions could be divided into the following three groups:
2.1 Sampling as suspect
2.2 Modifications of the national plans for 2006
2.3 Other actions
2.1. Sampling as suspect
Suspect samples are defined as:
1) samples taken as a consequence of non-compliant results on samples taken in accordance with the monitoring plan (Article 5 of Directive 96/23/EC);
2) samples taken as a consequence of possession or presence of prohibited substances at any point during manufacture, storage, distribution or sale throughout the food and feed production chain (Article 11 of Directive 96/23/EC);
3) samples taken where the veterinarian suspects or has evidence of illegal treatment or non-compliance with the withdrawal period for an authorised veterinary medicinal product (Article 24 of Directive 96/23/EC).
In summary, this means that the term “suspect sample” applies to a sample taken as a consequence of: – non-compliant results and/or
– suspicion of an illegal treatment at any stage of the food chain and/or
5 Non-compliant results correspond to the presence of a prohibited substance or to the presence of an authorised substance above the maximum level allowed in the legislation.
EN 4 EN
– suspicion of non-compliance with the withdrawal period for an authorised veterinary medicinal product.
2.2. Modifications of the national plan for 2006
The national residue monitoring plan aims at detecting illegal treatment of food- producing animals, controlling compliance with the maximum residue limits for veterinary medicinal products, the maximum residue levels for pesticides and the maximum levels for contaminants. Non-compliant results for a specific substance/group of substances or a specific food commodity should result in intensified controls for this substance/group or food commodity in the plan for the following year.
2.3. Other actions taken as a consequence of non-compliant results
Article 16 and Articles 22-28 of Directive 96/23/EC prescribe a series of actions (other than modifications of the residue monitoring plan) to be taken in the case of non-compliant results or infringements: 1. To carry out investigations in the farm of origin, such us verification of records and additional sampling.
2. To hold animals in the farm as a consequence of positive findings.
3. To slaughter animals in case of confirmation of illegal treatment and to send them to a high risk processing plant.
4. To intensify the controls in the farms where non-compliant results were found.
5. To impound carcasses at the slaughterhouse when non-compliant results have been found.
6. To declare the carcasses or products of animal origin unfit for human consumption.
The changes introduced by some Member States for the 2006 plan together with the responses of the Member States in relation to this type of actions are summarised in Annex II to this document.
EN 5 EN
EUROPEAN COMMISSION HEALTH & CONSUMER PROTECTION DIRECTORATE-GENERAL
Directorate E Safety of the Food Chain E3 - Chemical contaminants and pesticides
ANNEX I SANCO/3635/2006
Report for 2005 on the results of residue monitoring in food of animal origin in the Member States
EN 6 EN
TABLE OF CONTENTS 1. LEGAL BASIS
2. COUNTRY CODES
3. MAIN FINDINGS
4. BOVINES, PIGS, SHEEP AND GOATS, HORSES AND POULTRY
4.1 Production and percentage of targeted samples for bovines, pigs, sheep and goats and horses.
4.2 Production and percentage of targeted samples for poultry.
4.3 Non-compliant results
4.3.1 Hormones
4.3.2 Corticosteroids
4.3.3 Beta-agonists
4.3.4 Prohibited substances (A6)
4.3.5 Antibacterials (B1)
4.3.6 Other Veterinary medicinal products (B2)
4.3.7 Other substances and environmental contaminants (B3)
4.3.8 Overall distribution of non-compliant results in the EU 5. ANIMAL PRODUCTS
5.1 Aquaculture
5.2 Milk
5.3 Eggs
5.4 Rabbit meat
5.5 Farmed game
5.6 Wild game
5.7 Honey
Annex 1: ANNEX I TO DIRECTIVE 96/23/EC
EN 7 EN
1. LEGAL BASIS
The aim of this report is to summarise the results of the national residue monitoring plans during the year 2005 in the Member States. This report includes for the second time the data obtained in the 10 new Member States after accession on 1 May 2004.
Council Directive 96/23/EC on measures to monitor certain substances and residues thereof in live animals and animal products states that Member States should draft a national residue monitoring plan for the groups of residues detailed in its Annex I6 in accordance with the sampling rules and levels referred to in Annex IV of the Directive. The Directive lays down sampling levels and frequency, as well as the groups of substances to be monitored for each food commodity. Decision 97/747/EC7 lays down additional rules for certain animal products: milk, eggs, honey, rabbits and game.
National plans should be targeted to take the following minimum criteria into account: sex, age, species, fattening system, all available background information and all evidence of misuse or abuse of substances. Member States should forward to the Commission the results of their residue monitoring by 31 March of each year at the latest.
Additionally, suspect samples may also be taken as part of residue control. Suspect sample applies to a sample taken as a consequence of:
– non-compliant results
– suspicion of illegal treatment
– suspicion of non-compliance with the withdrawal period for an authorised veterinary medicinal product
What does “non-compliant result” mean?
Commission Decision 2002/657/EC8 concerning the performance of analytical methods and the interpretation of the results lays down rules for the analytical methods to be used in the testing of official samples and specifies common criteria for the interpretation of analytical results.
Since the entry into force of Decision 2002/657/EC (1 September 2002), the correct term for those analytical results exceeding the permitted limits (in previous reports termed “positives”) is “non-compliant”. A non-compliant result means that the result has a sufficient statistical certainty and can be used for legal purposes9.
6 Annex I to Directive 96/23/EC lists the groups of substances to be covered by residue monitoring. It is presented in Annex 1 to this report for ease of reference. 7 OJ L 303, 6.11.1997, p. 12-15 8 OJ L 221, 17.8.2002, p. 8-36 9 As laid down in Article 6 of Decision 2002/657/EC, the result of an analysis shall be considered non-compliant if the decision limit of the confirmatory method for the analyte is exceeded. Decision limit is defined in Article 6(3) as the lowest concentration at which the method can confirm with a defined statistical certainty (99 % for substances for which no permitted limit has been established, and 95 % for all other substances) that the particular analyte is present.
EN 8 EN
Legal basis for permitted limits
For veterinary medicinal products, maximum residue limits (MRLs) are laid down in Council Regulation (EEC) No 2377/9010.
For pesticides, MRLs are laid down in Directive 86/363/EC11.
Maximum levels for lead, cadmium and mercury are laid down in Commission Regulation (EC) No 466/200112 and its amendments. For contaminants where no EU maximum levels had been fixed at the time of the collection of these samples, national tolerance levels were applied.
Minimum Required Performance Limits (MRPLs)
Annex to Commission Decision 2002/657/EC: means minimum content of an analyte in a sample, which at least has to be detected and confirmed. It is intended to harmonise the analytical performance of methods for substances for which no permitted limit has been established.
MRPLs for chloramphenicol, nitrofurans metabolites, medroxyprogesterone acetate13 and malachite and leucho malachite green14 have been established so far.
10 OJ L 224, 18.8.1990, p. 1 11 OJ L 221, 7.8.1986, p. 43-47 12 OJ L 37, 7.2.2002, p. 4-6 13 OJ L 71, 15.3.2003, p.17 14 OJ L 6, 10.1.2004, p.38
EN 9 EN
2. COUNTRY CODES
AT Austria BE Belgium CY Cyprus CZ Czech Republic DK Denmark EE Estonia FI Finland FR France DE Germany GR Greece HU Hungary IE Ireland IT Italy LV Latvia LT Lithuania LU Luxembourg MT Malta PL Poland PT Portugal SI Slovenia SK Slovak Republic ES Spain SE Sweden NL The Netherlands UK United Kingdom
EN 10 EN
3. MAIN FINDINGS IN 2005
This report includes for the second time the data obtained in the 10 new Member States after accession on 1 May 2004.
Altogether, around 707 163 targeted samples (456 163 samples for all groups+ 251 000 for inhibitor tests) and 73 000 suspect samples (70 505 samples for all groups + 2 350 for inhibitor tests) were taken in all Member States in 2005, i.e. 780 163 samples for residue control in all food commodities. 871 000 samples were taken in 2004.
For hormones (steroids and zeranol derivatives), 0.13 % of the samples taken in bovines were found to be non-compliant (0.12 % in 2004) and 0.44% in pigs (mainly due to the presence of nandrolone and contamination with the metabolite zearalenone), compared to 0.3% in 2004.
In 2005, 8 non-compliant were reported for thyrostatic agents in bovines. This is the first time since 2000 that non-compliant results for thyrostats have been detected in the EU. The finding was enabled by improving the performance of the analytical methods used for the analysis lowering the limit of detection form 50 to 1 ppb. However these results should be treated with caution as recent research have shown a possible background of natural occurrence of thyrostats in animals fed with cruciferous amounting up to 10 ppb.
The number of non-compliant results for corticosteroids in bovines increased from 42 targeted and 22 suspect in 2004 to 60 targeted and 126 suspect; dexamethasone was the most frequently found substance for corticosteroids.
For Beta-agonists, the incidence of non-compliant results increased from 0.06 % in 2004 to 0.08%. However in 2005 only 2 Member States have reported non-compliant results for beta- agonists compared to Six Member States in 2004.
For prohibited substances, the percentage of non-compliant results decreased from 0.11% in 2004 to 0.07% in 2005 in bovines. In pigs the percentage of non-compliant results for A6 was 0.05% (same as in 2004). Some non-compliant results were still found for chloramphenicol in different food commodities: bovines: 8 targeted and 6 suspect; pigs: 4 targeted and 2 suspect, poultry: 11 targeted and 39 suspect, aquaculture: 3 targeted and 8 suspect, milk: 2 targeted, rabbit: 3 targeted; for Nitrofurans, bovines: 1 targeted, 3 suspect, pigs: 5 targeted, sheep: 3 targeted, poultry: 6 targeted and 8 suspect, aquaculture: 1 targeted, eggs¨2 targeted, farmed game: 2 targeted and for nitroimidazoles: pigs: 1 targeted and 5 suspect; poultry: 2 targeted, 1 suspect; aquaculture: 1 targeted, 31 suspect;
The percentage of non-compliant results for antibacterials has decreased from 0.22 % to 0.20 % in 2005. Most of non-compliant results were found in pigs. In terms of number of non-compliant results antibacterials remains the main problem for meat (bovines, pigs, sheep, goats, poultry, and rabbits) and for milk, eggs and honey.
For veterinary medicinal products, in bovines most of the non-compliant results were for anti- inflammatory drugs such as dexamethasone, which has a MRL for meat, liver and milk but can also be used illegally as a growth-promoting agent. Additional investigations should be carried out when detecting residues in order to rule out that its presence is due to the illegal use as an anabolic substance. There were also some non-compliant results for non-steroid anti- inflammatory drugs (NSAIDs: phenylbutazone, flunixin meglumine and tolfenamic acid in bovines and sheep, diclofenac, metamizol and ramifenazon in pigs). However no residues for sedatives have been reported in pigs as in 2004.
EN 11 EN
Non-compliant results for anticoccidials were reported in bovines, pigs, poultry, eggs and rabbit meat; the most commonly found substances are nicarbazin, lasalocid, and diclazuril.
Antihelmintic residues were found in cattle, sheep and goats and aquaculture; the most commonly found substance was levamisole and avermectines.
Residues of malachite green in aquaculture products were found in eleven Member States. The number of non-compliant results continues to decrease from 58 targeted and 190 suspect in 2004 to 45 targeted and 49 suspect in 2005.
In milk, apart from antibiotics, most of the non-compliant results were for aflatoxin M1 and for organochlorine compounds (PCBs) and in eggs for anticoccidials, which are not authorised as feed additives for laying hens older than 16 weeks, but residues are often found in eggs, possibly due to cross-contamination of the feed in the feed mill.
There are no authorised antibacterial substances for treatment of bees in the EU; several non- compliant results for antibacterials were reported in honey as well as for heavy metals.
The results for the controls carried out on environmental contaminants are also included in this report:
Non-compliant results for heavy metals (cadmium, chromium, lead, mercury and arsenic) were reported for bovines, pigs, sheep and goats, horses, aquaculture, milk, rabbit meat, farmed game, wild game and honey.
Also residues of organochlorine compounds such as e.g. PCBs, HCH, PCDD, PCDF were reported in bovines, sheep and goats, aquaculture, milk, eggs, farmed game and wild game.
OVERALL CONCLUSION
Overall the picture shows a decrease of 10% in the number of samples taken for residue control together with a decrease in the global number of non-compliant results.
There is a continuing problem with residues of antimicrobial agents throughout the commodities tested. This highlights the importance of Member States utilising broad spectrum antimicrobial screening tests and taking appropriate corrective and preventive measures to decrease the prevalence of such residues. It is also important to further consider the differences in the strategies applied by the Member States for the screening of antimicrobials.
The issue of malachite green warrants highlighting even though the prevalence rate of residues detected in 2005 decreased relative to 2004. Again Member States are reminded to redouble their efforts to eliminate the use of this non-authorised substance in aquaculture.
Finally, residues of coccidiostats continue to represent a problem especially in eggs. The influence of cross contamination of animal feedingstuffs cannot be stressed enough both within feedmills and on farms. Efforts are required to minimised the possibility of such contamination occurring.
EN 12 EN
4. BOVINES, PIGS, SHEEP AND GOATS, HORSES AND POULTRY
4.1. PRODUCTION AND PERCENTAGE OF TARGETED SAMPLES: BOVINES, PIGS, SHEEP AND GOATS, HORSES
Directive 96/23/EC establishes the minimum number of samples that have to be analysed for each food commodity in relation to the production figures for the previous year. As an example, the number of bovine samples that have to be analysed in 2006 is 0.4% of the number of bovine animals slaughtered in 2005.
The number of animals slaughtered broken down by category is shown in Table 1. In all cases, the minimum number of samples is respected for the EU overall.
Table 1. Number of animals slaughtered and targeted samples
Bovines Production Targeted samples* % animals tested Minim. 96/23
2005 (EU 25) 27 900 727 139 152 0.49 0.4
2004 (EU 25) 28 093 383 139 000 0.49
Pigs
2005 (EU 25) 232 383 755 162 179 0.07 0.05
2004 (EU 25) 231 590 084 167 573 0.07
Sheep-goats
2005 (EU 25) 38 534 502 26 578 0.07 0.05
2004 (EU 25) 39 431 483 27 560 0.07
Horses
2005 (EU 25) 340 317 3 543 0.88 Not specified
2004 (EU 25) 338 640 4 140 1.18
*Figures corresponding to inhibitors testing programme in Germany have not been considered in this table -see chapter 4.3.5.
EN 13 EN
4.2. PRODUCTION AND PERCENTAGE OF TARGETED SAMPLES FOR POULTRY
According to Directive 96/23/EC, the minimum number of samples for each category of poultry must be one per 200 t of annual production, with a minimum of 100 samples for each group of substances where annual production in the category concerned is over 5 000 t. The graph below shows poultry production in ‘000 t in the Member States arranged by level of production and the number of targeted samples per 200 t of annual production. GR did not achieve the minimum number of samples.
Graph 1
Poultry: '000 t and targeted samples/200 t t samples/200 t 2000 14,90 16
1500 12
1000 6,98 8 5,23 3,96 500 4 2,16 1,89 1,49 1,43 1,42 1,021,031,211,221,191,03 1,32 1,181,311,03 1,16 1,201,271,23 0,57 0,00 0 0 FR UK ES DE IT PL NL HU BE PT CZ DK IE GR SE AT FI SK SI CY LT LV EE MT LU
For the EU as a whole, 62 853 targeted samples were taken in 2005, compared to 64 272 in 2004. The production remained around 10.3 million t in 2004 compared to 2003.
Table 2. Poultry: production t and number of targeted samples
Poultry (t) Production Targeted samples Samples tested/200t Minimum
2005 (EU 25) 10 358 202 62 853 1.21 1/200 t
2004 (EU 25) 10 327 818 64 272 1.24
EN 14 EN
4.3. NON-COMPLIANT RESULTS
4.3.1. HORMONES
Hormones include group A1 (stilbenes), A3 (steroids) and A4 (resorcylic acid lactones). There were no non-compliant results for group A1 (stilbenes and derivatives).
In 2005 FR reported 8 NC results for A2 (thyrostatic agents) out of 657 targeted samples. Since 2000 there were no NC results for thyrostats in the EU.
In terms of absolute results, 59 287 targeted samples were taking in 2005 for A1, A2, A3 and A4 and 8 non-compliant results were found for A2, 68 for A3 and 7 for A4 in bovine which means 0.13 % of non-compliant results for hormones in the EU, compared to 0.12 % in 2004.
In pigs, 71 targeted samples out of 11 229 were non-compliant for A3 and 48 for A4 out of 6 558 targeted samples and 0 out of 2 783 targeted samples for A2, (total 27 043 targeted samples) which means 0.44 % of non-compliant results for hormones in pigs in the EU (0.3 % in 2004).
Specific substances and figures are given in Tables 3, 4, 5, 6, 7 and 8 for both targeted and suspect sampling.
Table 3: stilbenes Stilbenes (A1) Targeted samples Suspect samples Bovine 13 216 1 474 Pigs 6 473 127 Sheep and goats 579 4 Horses 46 0 Poultry 3 077 42 Aquaculture 201 10 Rabbit 96 3 Game 35 0 Table 4: antithyroid agents Antithyroid agents (A2) Targeted samples Suspect samples Bovines 4 966 85 Pigs 2 783 62 Sheep and goats 493 6 Horses 85 1 Poultry 1 183 36 Aquaculture 6 0 Rabbit 69 1 Game 20 3
EN 15 EN
Table 4.b: antithyroid agents non-compliant results
BOVINES Group Substances MS NC
TARGET A2 Thiouracil FR(8) 8
TOTAL TARGET 8
Table 5: steroids Steroids (A3) Targeted samples Suspect samples Bovines 28 018 2 408 Pigs 11 229 440 Sheep and goats 1 161 21 Horses 157 6 Poultry 3 613 21 Aquaculture 364 31 Rabbit 93 4 Game 60 3 Table 6: steroids non-compliant results
Species Group Substances MS NC
Bovines A3 Boldenone-Alpha BE (1)1 1
Boldenone-Beta BE (1) 1
Dexamethasone IT (45) 45
Epinandrolone IT (4) 4
Nandrolone UK (4);IT(1) 5
Progesterone UK (10)* 10
Testosterone-17-Alpha BE (1) 1 1
Testosterone-17-Beta DE (1) 1 1
BOVINES TOTAL TARGET 68
PIGS Estradiol-17-Beta ES(19) 19
Nandrolone CZ (7);DE (1);ES(18);FR (16);IT (7);PL(3) 52
PIGS TOTAL TARGET 71
POULTRY Estradiol-17-Beta FR (1) 1
POULTRY TOTAL TARGET 1
SHEEP/GOATS Nandrolone UK(34)* 34
SHEEP/GOATS TOTAL TARGET 34
BOVINES Dexamethasone IT(9) 9
Estradiol-17-Alpha ES(8) 8
Testosterone-17-Beta ES (24) 24
BOVINES TOTAL SUSPECT 41
EN 16 EN
PIGS A3 Nandrolone CZ(7) 7 PIGS TOTAL SUSPECT 7
*UK: Natural occurring hormones. No evidence of misuse was proved after investigations BE1: the same sample contained the 3 substances
Table 7: resorcilic acid lactones Resorcilic acid lactones (A4) Targeted samples Suspect samples Bovines 13 087 512 Pigs 6 558 139 Sheep and goats 615 10 Horses 86 1 Poultry 3 207 0 Aquaculture 152 0 Rabbit 38 3 Game 69 3 Table 8: resorcilic acid lactones non-compliant results
BOVINES Group Substances MS NC
TARGET A4 Taleranol (Beta-Zearalanol) FR (1) 1
Zeranol (Alpha-Zearalanol) FR(1);UK(5) 6
TOTAL TARGET BOVINES 7
PIGS Zearalanone ES(48) 48
SHEEP/GOATS Zearalanone ES(1) 1
TOTAL TARGET BOVINES-PIGS-SHEEP/GOATS 56
EN 17 EN
4.3.2. CORTICOSTEROIDS
With regard to corticosteroids, some Member States include these in group A3 because they are steroids, whereas others allocate them to B2f (other pharmacologically active substances). Both approaches may be acceptable; dexamethasone is known to be used in cocktails with other growth promoters. The Member States that include them in group A argue that they then have more legal powers to respond.
In 2005 an increase can be observed in the number of non-compliant results for corticosteroids compared to 2004 (60 targeted and 126 suspect non-compliant results in 2005 compared to 42 targeted and 28 suspect in 2004). It is interesting that the same MS that found NC results for corticosteroids in 2004 have also found them in 2005, except FR that had no NC in 2004 and has 1 in 2005.
Information on substances found and whether they are considered as A3 or B2f is given in Table 9.
Table 9: corticosteroids non-compliant results
Species Group Substances MS NC BOVINES A3 Dexamethasone IT(45) 45 B2f Betamethasone ES(1) 1 Dexamethasone BE(2);DE(1);ES(5);FR(1);NL(1);PL(1) 11 Prednisolone BE(3) 3 TOTAL TARGET BOVINES 60 SHEEP/GOATS B2f Dexamethasone DE(1) 1 TOTAL TARGET SHEEP/GOATS 1 BOVINES A3 Dexamethasone IT(9) 9 B2f Dexamethasone BE(113);ES(3) 116 Prednisolone BE(1) 1 TOTAL SUSPECT BOVINES 126
EN 18 EN
4.3.3. BETA-AGONISTS
The percentage of non-compliant results for Beta-agonists is calculated by comparing the total number of samples in bovines tested for Beta-agonists with the non-compliant results found.
There was an increase in the percentage of non-compliant results for Beta-agonists in bovines from 0.06 % in 2004 to 0.08 % in 2005. In terms of absolute results, 17 targeted and 28 suspect non-compliant results were found in 2004 and 28 targeted and 4 suspects in bovines in 2005; in pigs 11 targeted non-compliant results in 2004 and 8 targeted in 2005. In addition, 4 targeted non-compliant results were found for sheep in P in 2004 and 3 in 2005. All NC results were for clenbuterol.
Table 10: beta-agonists Beta-agonists (A5) Targeted samples Suspect samples Bovines 31 260 2 510 Pigs 14 924 399 Sheep and goats 2 068 29 Horses 290 2 Poultry 6 261 58 Aquaculture 156 0 Rabbit 282 9 Game 113 9
Table 11: beta-agonists non-compliant results SPECIES Group Substances MS NC
BOVINES A5 Clenbuterol FR(1);IT(5);PT(22) 28
BOVINES TOTAL TARGETED 28
PIGS Clenbuterol PT(8) 8 PIGS TOTAL TARGET 8
SHEEP/GOATS Clenbuterol PT(3) 3 SHEEP/GOATS TOTAL TARGET 3
BOVINES Clenbuterol IT (1); PT(3) 4
BOVINES TOTAL SUSPECT 4
EN 19 EN
4.3.4. PROHIBITED SUBSTANCES (A6)
Group A6 lists compounds included in Annex IV to Council Regulation No 2377/90/EEC (prohibited substances), which are prohibited substances other than the ones covered by Directive 96/22/EC.
For bovines, the percentage of non-compliant targeted results in the EU decreased from 0.11 % in 2004 to 0.07% in 2005. AT, CZ, DE, FR and LV found non-compliant results for chloramphenicol in targeted sampling. Nitrofuran non-compliant results were found in IE 10 non-compliant results were found after suspect sampling in bovines (4 chloramphenicol and 4 nitrofurans) (see Table 13 for details).
For pigs, the percentage of non-compliant for targeted samples was 0.05 % same as in 2004. In absolute terms the number of non-compliant samples for A6 in pigs increased from 8 targeted in 2004 to 10 in 2005. Additionally 2 non-complaint results were found after suspect sampling for chloramphenicol and 5 for metronidazol.
For poultry, in 2005, 19 samples were found non-compliant for A6 for targeted samples and 48 suspect sample for A6 (see Table 13 for details).
1 non-compliant result was found in horses for nitrofurans targeted samples and 1 for suspect samples. For sheep and goats 8 non-compliant results for target samples and 9 for suspect samples, 3 of them for nitrofurans metabolites and 5 for chloramphenicol (see Table 13 for details).
Table 12: prohibited substances Prohibited substances (A6) Targeted samples Suspect samples Bovines 14 023 4 014 Pigs 15 910 759 Sheep and goats 1 846 71 Horses 148 19 Poultry 14 767 1 108 Aquaculture 1 717 263 Rabbit 860 47 Game 246 24
The list of substances found for targeted and suspect samples is shown in the following table.
EN 20 EN
Table 13: prohibited substances non-compliant results Species Group Substances MS NC BOVINES A6 AOZ ES (1) 1 Chloramphenicol AT(1); CZ (3);DE(2);FR(1);LV(1) 8 Furazolidone IE(2) 2 TOTAL TARGET BOVINES 11 HORSES AHD ES(1) 1 TOTAL TARGET HORSES 1 PIGS AHD ES(2) 2 AOZ GR(1);IT(1) 2 Chloramphenicol CZ (1); DE(1);NL(1);PL(1) 4 Metronidazol DE(1) 1 SEM (semicarbazide) ES(1) 1 TOTAL TARGET PIGS 10 POULTRY AHD ES(4) 4 AMOZ ES(1) 1 AOZ GR(1) 1 Chloramphenicol CZ(4);DE(3);ES(1);IT(1);SK(2) 11 Dimetridazol IT(1) 1 Metronidazol FR(1) 1 TOTAL TARGET POULTRY 19 SHEEP/GOATS AHD ES(1) 1 Chloramphenicol FR(5) 5 SEM (semicarbazide) ES(1); UK (1) 2 TOTAL TARGET SHEEP/GOATS 8 SUSPECT BOVINES Chloramphenicol AT(3);CZ(3) 6 Furazolidone IE(4) 4 TOTAL SUSPECT BOVINES 10 HORSES AHD ES (1) 1 TOTAL SUSPECT HORSES 1 PIGS Chloramphenicol AT(1);CZ(1) 2 Metronidazol DE (5) 5 TOTAL SUSPECT PIGS 7 POULTRY AHD ES(2) 2 AMOZ ES(5) 5 AOZ ES(1) 1 Chloramphenicol CZ(18);ES(21) 39 Dimetridazol IT(1) 1 TOTAL SUSPECT POULTRY 48 SHEEP/GOATS AHD ES(8) 8 AMOZ ES(1) 1 TOTAL SUSPECT SHEEP/GOATS 9
EN 21 EN
4.3.5. ANTIBACTERIALS
Antibacterials include all substances in group B1: sulfonamides, penicillins, quinolones, tetracyclines, etc. It should be pointed out that there are different ways of interpreting the results of the analysis for antimicrobials, depending on the analytical method used: Screening tests allow a high sample throughput and a high number of samples to be analysed in a relatively short time and they are designed to minimise the number of false negatives. When residues are found in a screening test, a confirmatory test shall be carried out, which normally involves a more sophisticated testing method, providing full or complementary information enabling the substance to be identified precisely and confirming that the MRL has been exceeding. These tests are intended to keep the number of false non-compliant results as low as possible.
In the case of antibacterials, some of the screening tests are based on microbiological tests, whereby the sample is cultivated in different bacterial media. If, after the incubation period, the sample has inhibited the growth of the bacteria, it is considered that an antibacterial is present, but the specific substance is not identified. Given that this is a qualitative analytical method, a misinterpretation of the results cannot be ruled out, and some false positives can occur. Physico-chemical analysis provides information on the specific substance present in the sample.
In some Member States and under specific control programmes (autocontrols), a positive result in a microbiological test is sufficient to reject the sample. This may mean that no confirmation by a physico-chemical method is carried out and there is thus no conclusive identification of the substance concerned. In other cases, a positive result in the screening test is confirmed by means of a physico-chemical test, and it is then possible to identify the substance and establish whether its concentration is above the MRL. Another possibility is to analyse directly with a physico-chemical test (i.e. sulfonamides analysis).
In Germany, for instance, there are two different strategies. One is to fulfil the requirements of Directive 96/23/EC and for which all results obtained by inhibitor tests are confirmed by physico-chemical methods to check compliance with MRLs. For the second strategy, all analyses are carried out by inhibitor tests (e.g. n-plate test) and food for which positive results are obtained is considered unfit for human consumption according to national law. 18 444 samples for bovines, 229 680 for pigs, 3 603 for sheep, 49 for horses, 47 for poultry, 37 for aquaculture, 79 for rabbits and 1 for game were analysed under this scheme, giving rise to 57 positive inhibitor tests for bovines, 223 for pigs and 9 for sheep.
With regard to suspect samples, NL had the highest absolute number of non-compliant results (480 out of 13 672 for bovines, and 517 out of 21 462 for pigs). In NL, in the event of positive results for inhibitor tests, investigations in the farm of origin are carried out to check whether the withdrawal period has been respected; also, carcasses are detained for 24 hours until the result is available. If it is positive for the inhibitor test, the sample is considered non-compliant, without the need for physico-chemical methods. This strategy explains the higher number of samples taken by the Netherlands compared to other Member States.
In Belgium, during meat inspections in the slaughterhouses, carcasses considered suspect by the veterinary inspector are subject to an inhibitor test. If the results are non-
EN 22 EN
compliant, the carcasses are considered unfit for human consumption. Belgium reported that 4 458 bovines, 658 pigs and 38 horses were subject to controls under this scheme giving rise to 58, 27 and 15 non-compliant results respectively.
In the EU as a whole, non-compliant results for antibacterials (bovines, pigs, sheep, goats, horses and poultry) decreased from 0.22% in 2003 and in 2004 to 0.20 % in 2005. The number of targeted samples in 2005 was 143 309 targeted samples + 251 823 inhibitor test in Germany, total 395 132 targeted samples compared to 422 621 targeted samples for bovines, pig, sheep and goats, horses and poultry in 2004.
The number of targeted non-compliant results decreased from 1 019 in 2004 to 786 in 2005.
59% of non-compliant targeted samples were found in pigs, 28% in bovines, 8% in sheep and goats, 4% in poultry and 1 % in horses. In the table below, the number of non-compliant results for antibacterials in bovines, pigs, sheep, goats, horses and poultry is listed, including the results obtained from suspect samples.
Table 14: antibacterials B1 No samples No samples Non- Non-compliant Targeted Suspect compliant suspect targeted Bovines 29 376+18 444* 25 043+ 1 391*[11 96+57* 649+4*[480**+58&] 690**+4 458&]
Pigs 80 950+229 680* 23 158+925* [26 249+223* 591+7*[517**+27&] [37 280**] 499**+658&]
Sheep 12 320+3 603* 5 52+9*
Horses 924+49* 95+1*[38&] 18+1* Poultry 19 739+47* 325+29* 35 4 [15&] *Inhibitors Germany/** Inhibitors the Netherlands/ & Inhibitors Belgium
Table 15: antibacterials non-compliant results
Number of Non Species Group Substances MS compliant
BOVINES B1 Amoxycillin FR (3) 3 TARGET Ampicillin DE (1); FR (2) 3 Antibacterials IE (7); PL (8) 15 Benzylpenicillin, Penicillin G DE (1); FR (1); SE(4) 6 Chlortetracyclin NL (1) 1 Danofloxacin FR (1) 1 Dihydrostreptomycin CZ (1); DE (3); FR (2); SK (1) 7 Doxycyclin ES (1); IT (1) 2
EN 23 EN
Enrofloxacin DE (1) 1 Gentamicin DE (3) 3 Inhibitors DE (57); MT (3) 60 Neomycin DE (4) 4 Oxytetracyclin BE (1); ES (4); UK (1) NL(8);SK (1) 15 Penicillin FR (1) 1 Spiramycin FR (2) 2 Sulfadiazine BE (1);CY (1);ES (1);UK (1);IT (2) 6 Sulfadimethoxin IT (1) 1 Sulfamerazin IT (1) 1 Sulfamethazine CY (2);ES (1);IT (4);PT(1) 8 Sulfamethoxypyridazin ES (1) 1 Sulphadimidine AT (1) 1 Tetracyclin DE (2);FR (2);SK (1) 5 Tetracyclines SK (1) 1 Tilmicosin CZ(1) 1 Tylosin BE (1);FR (1)IT (1);PT (1) 4 TOTAL TARGET: 153 BOVINES B1 Amoxycillin BE(1);ES(1) 2 SUSPECT Antibacterials BE(58);IE(27);NL(480) 565 Benzylpenicillin, Penicillin G BE(6);FI(1);IT(1) 8 Chlortetracyclin AT(1) 1 Dihydrostreptomycin CZ(1) 1 Erythromycin BE(2) 2 Inhibitors DE(4);ES(7);MT(2) 13 Neomycin DE(1) 1 Oxytetracyclin BE(5);DK(1);ES(3);UK(19);IE(1);IT(2) 31 Penicillin ES(1) 1 Streptomycin AT(4) 4 Sulfadiazine GB(1) 1 Sulfadimethoxin BE(2) 2 Sulfamethazine PT(1) 1 Sulfamethoxypyridazin ES(1) 1 Sulphadimidine AT(5) 5 Tetracyclin DE(1) 1 Tilmicosin BE(3);CZ(1) 4 Trimethoprim BE(3) 3 Tylosin BE(5);PT(1) 6 TOTAL SUSPECT: 653 BOVINES TOTAL TARGET+SUSPECT: 804 PIGS B1 Amoxycillin AT (2);BE (1);FR (1) 4 TARGET Antibacterials CY (21);IE (24); PL (7) 52 Benzylpenicillin, Penicillin G DE (1);DK (3);SE (1) 5 Chlortetracyclin ES (16); UK (3); GR (3) 22 Dihydrostreptomycin DE (2) 2
EN 24 EN
Doxycyclin BE (1);ES (13);NL (4) 18 Enrofloxacin ES (4) 4 Epi-Chlortetracycline UK (3)** 3 Gentamicin DE (4) 4 Inhibitors DE (223);FI(3);MT(1);SK (1) 228 Oxytetracyclin BE (2);DE (1);ES(31);FR(1);UK(1);NL(7) 43 Penicillin BE(1);FR(1) 2 Sulfadiazine BE(1);CY(4);DE(2);ES(19);UK(3);GR(6);PT(2) 37 Sulfadimethoxin FR(3);IT(5);PT(3) 11 Sulfadoxin DE(1) 1 Sulfamerazin DE(1) 1 Sulfamethazine DE(6);ES(3);IT(1);NL(1);PT(4) 15 Sulfamethoxypyridazin GR(1) 1 Sulphadimidine AT(1);BE(1);CY(2);GR(7) 11 Tetracyclin CZ(2); DE(2);ES(2);FR(1) 7 Tylosin ES(1) 1 TOTAL TARGET: 472 PIGS B1 Amoxycillin DK(1) 1 SUSPECT Antibacterials BE(27);IE(2);NL(517) 546 Benzylpenicillin, BE(1);DK(1) 2 Penicillin G Chlortetracyclin ES(4) 4 Danofloxacin AT(1) 1 Dihydrostreptomycin DE(2) 2 Doxycyclin CZ(2);ES(1) 3 Enrofloxacin FI(1) 1 Inhibitors DE(7);ES(5);MT(5) 17 Marbofloxacin DE(1) 1 Neomycin DE(1) 1 Oxytetracyclin BE(1);DK(2);ES(3);FI(1) 7 Sulfadiazine ES(3) 3 Sulfamethazine ES(8) 8 Tylosin AT(1) 1 TOTALSUSPECT: 598 PIGS TOTAL TARGET+SUSPECT: 1068 SHEEP/GOATS B1 Antibacterials FR(3);IE(5) 8 TARGET Chlortetracyclin ES(4);GR(1) 5 Ciprofloxacin ES(1) 1 Dihydrostreptomycin GR(1) 1 Doxycyclin ES(1) 1 Enrofloxacin ES(1) 1 Inhibitors DE(9);SK(2) 11 Oxytetracyclin ES(4);FR(1);UK(1) 6 Sulfadiazine ES(14);PT(5) 19 Sulfadimethoxin FR(4) 4
EN 25 EN
Sulfamethazine FR(1) 1 Sulphadimidine AT(1) 1 Tylosin ES(2) 2 TOTAL TARGET: 61 GRAND TOTAL TARGET: 729 SHEEP/GOATS B1 Antibacterials IE(1);NL(6) 7 SUSPECT Chlortetracyclin ES(4) 4 Inhibitors ES(1) 1 Sulfadiazine ES(13) 13 TOTAL SUSPECT: 25 SHEEP GOATS TOTAL TARGET+SUSPECT: 86 HORSES B1 Antibacterials BE(15) 15 SUSPECT Inhibitors DE(1);ES(3) 4 TOTAL SUSPECT: 19 HORSES TOTAL TARGET+SUSPECT: 19 POULTRY B1 Antibacterials PL(3) 3 TARGET Chlortetracyclin ES(2) 2 Doxycyclin ES(4);NL(2) 6 Enrofloxacin ES (4);IT(1);PT(2) 7 Flumequin IT(1) 1 Oxytetracyclin ES(10);PT(1) 11 Sulfadiazine ES(1);PT(1) 2 Sulfaquinoxaline PT(2) 2 Tylosin ES(1) 1 TOTALTARGET: 35 POULTRY B1 Doxycyclin NL(1) 1 SUSPECT Oxytetracyclin ES(2);PT(1) 3 TOTALSUSPECT: 4 POULTRY TOTAL TARGET+SUSPECT: 39 TARGET:717 B1 GRAND TOTAL SUSPECT:1299 Antibacterials* Include results obtained by microbiological screening tests. UK** 3 samples contained residues of chlortetracycline and epi-chlortetracycline
EN 26 EN
4.3.6. OTHER VETERINARY MEDICINAL PRODUCTS (B2)
The following table shows the non-compliant results found for group B2, which includes “other veterinary medicinal products” for both targeted and suspect sampling.
Table 16: other veterinary medicinal products B2 No samples No samples Non-compliant Non-compliant Targeted Suspect targeted suspect
Bovines 21 745 2 823 32 138
Pigs 25 648 777 10 0
Sheep/goats 5 609 55 8 0
Horses 676 13 3 0 Poultry 10 876 406 81 3
Table 17: other veterinary medicinal products non-compliant results
Species Group Substances MS NC BOVINES B2 Sulfadiazine IT(3) 3 TARGET B2b Anticoccidials TOTAL B2a: 3
Phenylbutazon AT(9);DE(2);FR(1);UK(1);IE(1) 14
B2e NSAIDs TOTAL B2e: 14
Betamethasone ES(1) 1
Dexamethasone BE(2);DE(1);ES(5);FR(1);NL(1);PL(1) 11
Prednisolone BE (3) 3
B2f Others TOTAL B2f: 15
BOVINES TOTAL B2 TARGET 32 BOVINES Levamisol BE(1) 1 SUSPECT B2a Anthelmintics TOTAL B2a: 1
Flunixin BE(6) 6
Phenylbutazon BE(1);DE(3) 4
Tolfenaminsacid BE(7) 7
B2e NSAIDs TOTAL B2e: 17
Dexamethasone BE(113);ES(3) 116
Prednisolone BE(1) 1
EN 27 EN
Procaine Be (3) 3
B2f Others TOTAL B2f: 120
TOTAL B2 SUSPECT 138
BOVINES TOTAL B2 TARGET+SUSPECT 170 PIGS Abamectin (Avermectin B1) AT(1) 1 TARGET Avermectin B1a-22-23-Dihydro FI(1) 1
Levamisol NL(3) 3
B2a Anthelmintics TOTAL B2a 5
Salinomycin UK(2) 2
B2b Anticoccidials TOTAL B2b 2
Diclofenac DE(1) 1 Metamizol, Dipyron Monohydrat AT(1) 1 (Prodrug) Ramifenazon, Isopyrin AT(1) 1
B2e NSAIDs TOTAL B2e: 3
PIGS TOTAL B2 TARGET+SUSPECT 10 HORSES Phenylbutazon AT(1);FR(1);UK(1) 3 TARGET B2e NSAIDs TOTAL B2e: 3
HORSES TOTAL B2 TARGET+SUSPECT 3 SHEEP/GOATS Fenbendazol UK(1)* 1 TARGET Ivermectin NL(1) 1
Oxfendazol UK(1) 1
Oxfendazol sulfon UK(1) 1
B2a Anthelmintics TOTAL B2a: 4
Flunixin AT(2) 2
Tolfenaminsacid AT(1) 1
B2e NSAIDs TOTAL: B2e 3
B2f Dexamethasone DE(1) 1
SHEEP/GOATS TOTAL B2 TARGET+SUSPECT 8 POULTRY B2b Amprolium SI(1) 1 TARGET Diclazuril BE(3);CY(8) 11
Lasalocid AT(2);PL(1);SI(2) 5
Lasalocid-Sodium CY(1) 1
Maduramicin CY(1) 1
Monensin UK(2);IE(1) 3
Nicarbazin AT(3);BE(1);CZ(2); CY(1);UK(27);IE(15);IT(2) 51
EN 28 EN
Salinomycin MT(2) 2
B2b Anticoccidials TOTAL B2b: 75
Flunixin AT(1);BE(1) 2
Sodiumsalicylate NL(2) 2
B2e NSAIDs TOTAL B2e 4
Olaquindox PT(2) 2
B2f Others TOTALB2f: 2
TOTAL B2 TARGET 81 POULTRY B2b Nicarbazin CZ(2) 2 SUSPECT Toltrazuril NL(1) 1
Anticoccidials TOTAL B2 SUSPECT: 3
POULTRY TOTAL B2 TARGET +SUSPECT 82 TARGET:132 B2 GRAND TOTAL SUSPECT:141 * UK 1 sample was NC for fenbendazol, oxfendazole and oxfendazole sulfone
EN 29 EN
4.3.7. OTHER SUBSTANCES AND ENVIRONMENTAL CONTAMINANTS (B3)
The following table shows the non-compliant results found for group B3, which includes “other substances and contaminants” for targeted and suspect sampling.
Table 18: other substances and environmental contaminants B3 No samples No samples Non-compliant Non-compliant Targeted Suspect targeted suspect
Bovines 8 312 575 112 16
Pigs 10 974 1 000 40 13
Sheep 3 023 33 33 0
Horses 1 227 14 123 17 Poultry 5 427 412 2 0
Table 19: other substances and environmental contaminants non-compliant results
Species Group Substances MS NC BOVINES B3a HCH-Beta IT(2) 2 TARGET PCB 138 DE (1) 1 PCB 153 DE (1) 1 PCB 180 DE (1) 1 PCB sum CZ(1) 1 B3a Organochlorine TOTAL B3a 6 AT(8);BE(16);CZ(8);DE(4);DK(1);ES(7);FR(5);HU(2);LT(2); Cadmium Cd 89 LV(1);NL(25)PL(5); SE(1);SI(2);SK(2) Chromium Cr IT (5) 5 Lead Pb AT(2);BE(1);UK(2);IT(6);LV(1) 12 B3c Heavy metals TOTAL B3c 106 TOTAL B3 TARGET 112 BOVINES HCH-Beta IT(6) 6 SUSPECT PCB sum CZ(1) 1 B3a Organochlorine TOTAL B3a 7 Cadmium Cd CZ(13) 13 B3c Heavy Metals TOTAL B3c 13 Aflatoxin B1 IT(1) 1 B3d Mycotoxins TOTAL B3d 1 TOTAL B3 SUSPECT 21 BOVINES TOTAL B3 TARGET+SUSPECT 137 PIGS Diazinon FR(1) 1 TARGET B3b Organophosphorous TOTAL B3b 1
EN 30 EN
Cadmium Cd AT(1);CZ(1); DE(2);ES(4);FR(3);HU(1);PL(6) 18 Chromium Cr IT(1) 1 Lead Pb AT(1);BE(1);ES(1);IT(4);NL(1);PL(6) 14 B3c Heavy Metals TOTAL B3c 35 Ochratoxin A CY(1);FI(1);PL(2) 4 B3d Mycotoxins TOTAL B3d 4 PIGS SUSPECT Cadmium Cd ES(2);UK(1);HU(1);PL(1);SI(1) 6 Lead Pb CY(1);FR(1);UK(1);GR(1);HU(1);PL(1) 6 B3c Heavy metals TOTAL B3c 12 PCB sum CZ(1) 1 B3a Organochlorine TOTAL B3a 1 PIGS TOTAL B3 TARGET +SUSPECT 53 SHEEP/GOATS DDT: Sum DDT, DDE, ES (2) 2 TARGET DDD HCH-Alpha ES (2);FR(1) 3 HCH-Beta ES(2);FR(1) 3 HCH-Gamma (lindane) ES(1) 1 B3a Organochlorine TOTAL B3a 9 Cadmium Cd AT(5);BE(1);FR(7);UK(4);GR(2) 19 Lead Pb AT(1);ES(1);GR(1);IT(2) 5 B3c Heavy Metals TOTAL B3c 24 SHEEP/GOATS TOTAL B3 TARGET +SUSPECT 33 HORSES Cadmium Cd AT(1);DE(1);ES(19);FR(4);IT(93);SE(1) 119 TARGET Lead Pb ES(2);FR(2) 4 B3c Heavy metals TOTAL B3 TARGET 123 HORSES Cadmium Cd ES(6); CZ(1); PL(6) 13 SUSPECT Lead Pb ES(3) 3 B3c Heavy Metals TOTAL B3c 16 TOTAL B3 SUSPECT 16 HORSES TOTAL B3 TARGET +SUSPECT 140 POULTRY Cadmium Cd ES(1); SI (1) 2 TARGET B3c Heavy metals 2 TARGET: 329 GRAND TOTAL B3 SUSPECT: 33
EN 31 EN
4.3.8. OVERALL DISTRIBUTION OF NON-COMPLIANT RESULTS IN THE EU BOVINES, PIGS, SHEEP, GOATS, HORSES, POULTRY
The boxes below show the overall distribution of non-compliant results in the EU.
With regard to targeted samples, 50% of the non-compliant results were non-compliant for antibacterials, 21% for environmental contaminants, 21 % for prohibited substances, 8% for veterinary medicinal products, 4 % for hormones and 2 % for Beta-agonists. Graph 2
Overall distribution of non-compliant results (targeted sampling)
% 60 50 50
40
30 21 21 20 8 10 4 2 0 Antibacterials Contaminants Prohibited Vet medicines Hormones B-agonists substances
For suspect samples, 82% were non-compliant for antibacterials, 9% for veterinary medicinal products, 4% for prohibited substances, 3 % for hormones 2% for environmental contaminants and 0.3 % for Beta-agonists.
The number of non-complaint results after suspect sampling is not indicative of prevalence of non-compliance since investigations of one single case of a non-compliant targeted sample may imply many suspect samples taken in the same farm. Graph 3
Overall distribution of non-compliant results (suspect sampling) % 90 82
60
30 9 4 3 2 0,3 0 Antibacterials Vet medicines Prohibited Hormones Contaminants B-agonists substances
EN 32 EN
The box below shows the overall distribution of non-compliant results, including targeted and suspect samples.
Graph 4
Overall distribution of non-compliant results % (targeted+suspect sampling)
70 66
60 50
40 30 21 20 99 10 4 1 0 Antibacterials Contaminants Vet medicines Hormones Prohibited B-agonists substances
The following boxes show the pattern of the overall distribution for targeted sampling in 2004 (EU 25) and 2005 (EU 25). There was a decrease in the rate of non-compliant results for antibacterials (from 51 in 2004 to 50% in 2005), for contaminants (from 25 to 21%), for hormones (10 % in 2004 and 4 % in 2005) for veterinary medicines (9 to 8 %) and for Beta-agonists (from 3 to 2 %). The non-compliant results for Beta-agonists and increased from 1% to 3% and for prohibited substances the percentage of non-compliant increased from 3 % of all non-compliant in 2004 to 21% in 2005. Graph 5
Overall distribution non-compliant results (targeted sampling) 2004-2005 % 2004 2005 60 51 50
40 25 21 21 20 10 9 8 4 332 0 Antibacterials Contaminants Hormones Vet.medicines Prohibited B-agonists subs.
EN 33 EN
5. ANIMAL PRODUCTS
5.1. AQUACULTURE
The number of samples to be collected each year must be at least 1 per 100 t of annual production. In 2004, EU production was 583 814 t (compared to 587 521 t in 2003). 8 289 targeted samples were taken (8 498 targeted samples in 2004) and 1 005 suspect samples in 2005 were collected (472 in 2004).
In the graph below, the columns show aquaculture production in ‘000 t in 2005. Member States are classified by volume of production. The numbers at the top represent the number of targeted samples per 100 t.
L had no production and took no samples. GR did not achieve the minimum number of samples.
Graph 6
Aquaculture: '000 of t and targeted samples/100 t
180 22,8 25
150 20 15,1 120 11,3 15 90 6,2 7,0 10 60
4,0 Samples/100 t Thousands of t of Thousands 2,8 3,2 2,5 2,4 2,4 5 30 1,1 0,9 1,3 1,5 1,1 1,2 1,6 1,0 1,6 1,3 1,5 1,3 1,4
0 0 UK GR IT ES FR PL DK DE CZ IE FI NL SE HU PT CY AT BE LT SI MT LV SK EE LU
There was a decrease in the number of non-compliant results in 2005 (95 targeted and 96 suspect) compared to 2004 (106 targeted and 153 suspect) with no significant change of production (0.7 %) and 2% decrease in the number of targeted samples.
In 2005 there were 5 non-compliant results for steroids in targeted samples and 5 non compliant for banned substances targeted and 39 for suspect samples. Most non- compliant results were as in previous years for malachite green (45 targeted and 49 suspect compared to 53 targeted and 235 suspect in 2004). Non-compliant results for malachite green were found in 12 Member States. Malachite green is a chemical pharmacologically active substance whose use as a veterinary medicinal product for food-producing animals is not authorised in the Community.
EN 34 EN
The following table shows the number of non-compliant results for aquaculture, broken down by group of substances.
Table 20: aquaculture non-compliant results targeted and suspect sampling
Aquaculture Group MS Substances NC TARGET Steroids A3 FR Estradiol-17-Beta 2 NL Estradiol-17-Beta 2 NL Trenbolone 1 5 Banned substances A6 DE AOZ 1 DK Metronidazol 1 FR Chloramphenicol 1 IT Chloramphenicol 2 5 Antibacterials B1 FR Sarafloxacin 1 GR Oxytetracyclin 1 PL Antibacterials 1 3 Anthelminitics B2a UK Emamectin 5 IE Emamectin 2 7 Organochlorine B3a FR PCB sum 1 1 Heavy Metals B3c ES Cadmium Cd 8 ES Cupper Cu 3 ES Mercury Hg 6 GR Mercury Hg 1 18 Dyes B3e AT Malachite Green 1 AT Malachite Green-Leuco 1 BE Malachite Green 3 CZ Malachite Green 9 DE Malachite Green-Leuco 11 DK Malachite Green-Leuco 1 ES Malachite Green 1 ES Malachite Green-Leuco 2 FI Malachite Green-Leuco 3 FR Malachite Green 3 FR Malachite Green-Leuco 3 UK Malachite Green 1 UK Malachite Green-Leuco 1 PL Malachite Green 5 SK Malachite Green 1 45 Other contaminants B3f DE Ethoxyquin 11
EN 35 EN
11 TOTAL TARGET 95
SUSPECT A6 DK Metronidazol* 31 IT Chloramphenicol 8 39 B3c CZ Cadmium Cd 1 1 B3e AT Malachite Green 3 AT Malachite Green-Leuco 5 CZ Malachite Green 3 DE Malachite Green-Leuco 29 FI Malachite Green-Leuco 1 IT Malachite Green 3 PL Malachite Green 5 49 B3f DE Ethoxyquin 1 1 TOTAL SUSPECT 96 TOTAL TARGET+SUSPECT 191 DK* Metronidazol suspect non-compliant results were all found in the same farm
EN 36 EN
5.2. MILK
The annual number of samples should be 1 per 15 000 t of annual milk production, with a minimum of 300 samples. In 2004, the EU produced 140 401 801 t (140 123 546 t in 2003) and more than 29 000 targeted samples were analysed in 2005 (32 000 in 2004). The following graph shows production in ´000 t and the number of samples taken/15 000 t. Member States are classified by volume of production.
For the whole of the EU there was an increase in the number of non-compliant results in 2005 (127 targeted and 207 suspect)) compared to 2004 (69 targeted, 20 suspect).
Graph 7
Milk: '000 of t and targeted samples/15 000 t
30.000 27,29 30
25.000 25 17,70 20.000 15,64 20 13,60 15.000 15 10,05 10,16 8,73 7,89 10.000 6,75 10 5,03 Thousands of t of Thousands 3,35 3,80 3,21 2,443,033,15 Samples/15t 000 5.000 1,161,840,98 1,89 1,64 1,96 1,67 5
0 0 DE FR UK PL IT NL ES IE DK SE AT BE CZ FI HU PT GR LT SK LV EE SI LUCY*MT*
*Cyprus, Malta
There were 2 targeted non-compliant results for chloramphenicol (LV and SK), 1 targeted non-compliant results for anthelmintics (BE) compared to 3 targeted non- compliant results for anthelmintics in 2004; NSAIDs 5 targeted non-complaint results for Salicilic acid in SI, organochlorine compounds with 21 targeted and 20 suspect non- compliant results; 59 non-compliant results targeted and 69 suspect for antibacterials (representing only 4 cases of non-compliance with feed and food law since 67 non- compliant results from Denmark represent samples from only 2 cases of non-compliance) and 3 non-compliant results for chemical elements and 29 non-compliant results targeted samples and 110 suspect for mycotoxins (108 in Italy) (M1). The number of non- compliant results for mycotoxins has increased from 21 targeted and 4 suspects in 2004 to 29 targeted and 110 suspect in 2005.
The following table shows the number of non-compliant results for milk, broken down by group of substances.
Table 21: milk non-compliant results targeted and suspect sampling
MILK Group MS Substances NC TARGET A6 LV Chloramphenicol 1 SK Chloramphenicol 1 2
EN 37 EN
Antibacterials B1 DE Ampicillin 2 IE Antibacterials 2 LT Antibacterials 18 MT Inhibitors 28 PL Antibacterials 9 59 Anthelmintics B2a BE Ivermectin 1 1 B2e SI Salicylicacid 5 NSAIDs 5 B3a BE1 PCB 101 1 BE PCB 118 BE PCB 138 BE PCB 153 BE PCB 180 BE PCB 28 BE PCB 52 BE PCDD 1 BE PCDF ES PCB sum 1 IT HCH-Beta 17 IT PCB sum 1 Organochlorine 21 B3c UK Lead Pb 1 GR Lead Pb 1 IT Lead Pb 1 Heavy Metals 3 B3d FI Aflatoxin M1 1 IT Aflatoxin M1 28 Mycotoxins 29 TOTAL TARGET 120 SUSPECT B1 DK Benzylpenicillin, Penicillin G 14 DK Cloxacillin 2 DK Dihydrostreptomycin 15 DK Lincomycin 2 DK Nafcillin 5 DK Oxytetracyclin 18 DK Streptomycin 5 DK Tetracyclin 6 EE Penicillins (group) 1 IT Benzylpenicillin, Penicillin G 1 Antibacterials 69 B3a BE1 Dioxins 1 BE PCB 101 1 BE PCB 118 BE PCB 138
EN 38 EN
BE PCB 153 BE PCB 180 BE PCB 28 BE PCB 52 DE PCB 138 DE PCB 153 IT HCH-Beta 17 IT PCB sum 1 Organochlorine 20 B3d FI Aflatoxin M1 2 IT Aflatoxin M1 108 Mycotoxins 110 TOTAL SUSPECT 199 TOTAL TARGET+SUSPECT 319 BE1 1 sample was NC for several PCB markers
EN 39 EN
EGGS
The number of samples to be taken each year must be at least equal to 1 per 1 000 t of annual egg production, with a minimum of 200 samples.
In 2004, the EU produced 6 038 225 t of eggs (5 903 313 t in 2003) and 11 880 targeted samples (compared to 13 296 targeted samples in 2004) were analysed.
In the graph below, the columns show egg production in ‘000 t in 2004. Member States are classified by volume of production. The numbers at the top represent the number of targeted samples per 1 000 t. L* took 81 samples for 1,2 thousand t, EE took 525 samples for 14.6 t and CY 312 samples for 7.7 t, which are figures well above the other Member States and which falls outside the graph below.
Graph 8
Eggs: '000 of t and targeted samples/'000 t
1200 20 16,83 15,88
900 12,79 15
8,53 8,98 8,89 600 7,82 10
' 000 t ' 000 5,64 4,21 3,44 300 2,68 2,72 5
1,94 1,921,98 t Samples/'000 1,271,251,051,05 1,201,25 1,61
0 0 FR IT DE ES NL UK PL BE CZ PT GR SE AT HU FI SK DK IE LV LT SI EE*CY*MTLU*
The number of non-compliant results has increased compared to 2004 for the targeted sampling (88 targeted, in 2005 and 68 targeted in 2004) and decreased for the suspect (7 suspect sampling 2005 and 98 suspect in 2004). Non-compliant results were mainly for anticoccidials (55 targeted and 6 suspect found in 19 different MS), followed by antibacterials (27 targeted) and organochlorine compounds (3 targeted). In 2005 no MS reported non-compliant results for A6 substances (ronidazol, metronidazol, hydroxydimetridazole, chloramphenicol or Nitrofurans) as it was the case in 2004.
The following table shows the number of non-compliant results for eggs, broken down by group of substances.
Table 22: eggs non-compliant results targeted and suspect sampling
EGGS Group MS Substances NC TARGET B1 ES Ciprofloxacin 1 ES Enrofloxacin 1 FR Sulfadiazine 4 FR Sulfadimethoxin 1 UK Chlortetracyclin 1 UK Epi-Chlortetracycline* 1
EN 40 EN
UK Sulfadiazine 3 GR Sulfonamides 2 IT Enrofloxacin 1 MT Inhibitors 5 PT Doxycyclin 1 PT Sulfadiazine 6 Antibacterials 27 B2b AT Lasalocid 1 BE Lasalocid 3 BE Salinomycin 1 CY Lasalocid-Sodium 2 CZ Nicarbazin 1 DE Lasalocid 1 DE Nicarbazin 1 DK Salinomycin 8 FR Diclazuril 1 FR Lasalocid 8 FR Nicarbazin 10 FR Robenidin 5 UK Lasalocid 1 UK Nicarbazin 3 UK Salinomycin 1 IT Nicarbazin 2 IT Robenidin 1 PL Lasalocid 3 SI Lasalocid 2 Anticoccidials 55 B3a DE Dioxins 1 FR Aldrin 1 FR Dieldrin 1 Organochlorine 3 TOTAL TARGET 85 SUSPECT B2b CZ Nicarbazin 1 IT Nicarbazin 1 IT Robenidin 1 PL Lasalocid 3 SI Lasalocid 0 Anticoccidials 5 6 Organochlorine DE DDT 1 TOTAL SUSPECT 7 TOTAL TARGET +SUSPECT 92 * UK same samples was NC for Epi-Chlortetracycline and Chlortetracycline
EN 41 EN
5.4. RABBIT MEAT
The number of samples to be taken each year must be equal to 10 per 300 t of annual production for the first 3 000 t, plus one sample for each additional 300 t. The following graph shows the production in t and the number of samples taken/300 t.
DK, IRL, FIN, S and UK reported no production for rabbits.
Total production in the EU in 2004 was 234 931 t (233 914 t in 2003) and 4 502 targeted samples (4 752 in 2004) were taken.
In the graph below, the columns show rabbit meat production in t in 2004. Member States are classified by volume of production. The numbers at the top represent the number of targeted samples.
Graph 9
Rabbits (t) and number of targeted samples t 100000 2000
1454 75000 1500
941 50000 829 1000
25000 269 210 500 143 84 139135104 88 98 Targeted samples 14 55 4 5 27 19 36 47 0 0 0 0 0 0 0 IT ES FR HU PT GR BE PL CZ CY SK DE NL MT SI LT LU LV EE AT DK FI UK IE SE
The number of non compliant results for targeted samples has not changed in relation to 2004 (38 targeted). In 2004 there were no suspect samples; in 2005 there have been 24 non-compliant results after suspect sampling in rabbits.
Most non-compliant results were for antibacterials (30 targeted and 13 suspect). ES, FR and IT reported non-compliant result for A 6 substances both for targeted samples (5 NC, and suspect samples 10 samples.
The following table shows the number of non-compliant results for rabbit meat, broken down by group of substances.
Table 23: rabbits non-compliant results targeted and suspect sampling
RABBIT Group MS Substances NC TARGET A6 ES AHD 1 ES SEM (semicarbazide) 1 FR Chloramphenicol 2 IT Chloramphenicol 1
EN 42 EN
Prohibited 5 B1 DE Inhibitors 7 ES Ciprofloxacin 1 ES Enrofloxacin 3 ES Oxytetracyclin 6 ES Sulfadiazine 2 FR Sulfadimethoxin 9 IT Sulfadimethoxin 1 SK Enrofloxacin 1 Antibacterials 30 B2b BE Robenidin 1 CZ Nicarbazin 1 Anticoccidials 2 B2e NL Sodiumsalicylate 1 NSAIDs 1 B3c IT Lead Pb 1 Heavy Metals 1 TOTAL TARGET 39 SUSPECT A6 ES AHD 4 ES SEM (semicarbazide) 3 IT Chloramphenicol 3 Prohibited 10 B1 ES Enrofloxacin 2 ES Oxytetracyclin 11 Antibacterials 13 B2b CZ Nicarbazin 1 Anticoccidials 1 TOTAL SUSPECT 24 TOTAL TARGET+SUSPECT 63
EN 43 EN
5.5. FARMED GAME
The number of samples to be taken each year must be at least 100. DE, FI, SE, PT, GR, DK, IE did not achieve this minimum.
Total production in the EU in 2004 was 42 290 t (54 775 t in 2003). 1 894 targeted samples were taken (1 978 in 2003).
In the graph below, the columns show farmed game production in t in 2004. The Member States are classified by volume of production. The numbers at the top represent the number of targeted samples.
Graph 10
Farmed game (t) and number of targeted samples t 16000 223 250 209 183 174 200 12000 157 149 116 150 106 104 8000 92 81 82 87 82 71 74 100 4000 50 0 0 0 0 0 0 0 0 8 Targeted samples 0 0 FR ES DE IT FI SE PT BE AT GRDK CY CZ IE LT EE LV NL UK HU LU MT PL SI SK
HU, LT, LU, LV, MT,PL, SI, SK* reported no production.
There was no change in the number of non-compliant targeted results compared with the figure for 2004 (22 in 2004 and 2005). There has been changes in the substances identified as non-compliant, 9 non-compliant results were for anticoccidials (lasalocid) and 13 non-compliant results for heavy metals in 2004 compared to 2 NC for A6 (nitrofurans) 3 antibacterials, 1 organochlorine and 15 heavy metals in 2005.
Table 24: farmed game non-compliant results targeted and suspect sampling
FARMED GAME Group MS Substances NC TARGET A6 ES AOZ 1 IT AOZ 1 Prohibited 2 B1 DE Inhibitors 0 ES Chlortetracyclin 1 ES Oxytetracyclin 1 ES Sulfadiazine 1 Antibacterials 3 B3a BE PCDD 1
EN 44 EN
BE PCDF Organochlorine 1 B3c FI Cadmium Cd 14 FR Cadmium Cd 1 Heavy Metals 15 TOTAL TARGET 22
EN 45 EN
5.6. WILD GAME
The number of samples to be taken each year must be at least 100. The following table shows production in t and the number of targeted samples in each Member State. The minimum number of 100 samples was not achieved by some MS. However, the minimum number of 100 samples was set as a provisional rule to be reviewed in light of the information provided by the Member States on their production figures
Table 25: wild game production and number of samples Country Production Samples DE 68.408 115 FR 17.088 72 ES 14.307 107 PL 12.000 181 AT 8.502 209 HU 6.533 192 CZ 5.500 269 UK 2.328 102 IT 1.560 40 BE 1.000 110 SI 796 98 LT 600 172 SK 375 94 LU 360 100 EE 275 99 FI 157 50 DK 156 100 NL 114 115 IE 106 96 CY 0 0 GR 2 LV 123 MT 0 0 PT 0 104 SE 0 141
EN 46 EN
Graph 11
Wild game (t) and targeted samples t 80.000 269 300
209 250 192 60.000 181 172 200 141 123 40.000 115 107 110 115 104 150 102 98 94 100 99 100 96 72 50 100 20.000 40
50 Targeted samples 0 2 0 0 0 DE FR ES PL AT HU CZ UK IT BE SI LT SK LU EE FI DK NL IE CY GRLV MT PT SE
There was an increase in the number of non-compliant results (159 in 2004 and 191 in 2005). With the exception of 9 non-compliant results for organochlorine compounds and 1 for organophosphorous compounds the rest (191 targeted and 3 suspect) of the non- compliant results reported were for chemical elements.
The following table shows the number of non-compliant results for wild game, broken down by group of substances.
Table 26: wild game non-compliant results targeted and suspect sampling
WILD GAME Group MS Substances NC TARGET B3a DE DDT: Sum DDT, DDE, DDD 5 DE HCH-Beta 1 DE Lindan 1 ES DDE, pp'- 1 ES HCH-Beta 1 Organochlorine 9 B3b DE Diazinon 1 Organophosphorous 1 B3c AT Lead Pb 12 DK Lead Pb 16 DK Mercury Hg 2 EE Cadmium Cd 45 EE Lead Pb 1 ES Cadmium Cd 4 FI Cadmium Cd 15 FR Cadmium Cd 3 GB Lead Pb 1 LV Cadmium Cd 46 LV Lead Pb 19
EN 47 EN
NL Cadmium Cd 9 NL Lead Pb 5 PL Cadmium Cd 7 PL Mercury Hg 1 SI Lead Pb 3 SK Lead Pb 2 Heavy Metals 191 TOTAL TARGET 201 SUSPECT B3a DE DDT: Sum DDT, DDE, DDD 2 DE PCB 153 1 Organochlorine 3 TOTAL SUSPECT 3 TOTLA TARGET+SUSPECT 204
EN 48 EN
5.7. HONEY
The number of samples to be taken must be at least 10 per 300 t of annual production for the first 3 000 t, plus one sample for each additional 300 t. The following graph shows the production in t and the number of samples taken/300 t. Member States are classified by volume of production. The numbers at the top represent the number of targeted samples per 300 t.
Total EU production in 2004 was 163 441 t (138.354 t in 2003) and the total number of targeted samples was 3 855 (4 428 in 2004).
Graph 12
Honey '000 t and targeted samples/300 t '000 t 235,7 40 250
200 30 142,2 122,4 150 113,3 20 100 41,1 10 32,0 21,0 28,5 22,0 50 13,4 15,4 12,5 10,5 Targeted samples 5,4 2,2 2,2 6,5 6,3 8,4 5,1 5,6 8,0 8,5 2,6 9,4 0 0 ES DE FR GR PL IT CZ UK PT AT HU SK DK SE SI FI BE LV NL EE CY IE LT LU MT
Most of the non-compliant results were for antibacterials (66 targeted and 14 suspects, compared to 109 targeted and 54 suspect in 2004). There is no MRL established for honey for antibacterial substances classified in Annex I, II or III of Council Regulation 2377/90 and therefore there are no authorised antibacterials substances for the treatment of bees.
Additionally 3 targeted non-compliant results were found for chemical elements (compared to 4 in 2004).
Table 27 shows the number of non-compliant results for honey, broken down by group of substances.
EN 49 EN
Table 27: honey non-compliant results targeted and suspect sampling
HONEY Group MS Substances NC TARGET B1 AT Sulfathiazol 3 BE Sulfamethazine 3 BE Sulfathiazol 1 CY Oxytetracyclin 1 CY Sulfadiazine 1 CY Sulfonamides 1 CY Sulphadimidine 3 CY Tetracyclin 1 DE Sulfamethazine 1 DE Sulfathiazol 1 DE Sulfamerazine 1 FI Oxytetracyclin 1 FI Sulfathiazol 1 FI Tetracyclin 1 FR Tetracyclin 2 GR Doxycyclin 10 GR Streptomycin 4 GR Sulfachlorpyridazin 1 GR Sulfamerazin 2 GR Sulfamethazine 3 GR Sulfamonomethoxin 1 GR Sulfathiazol 1 IT Oxytetracyclin 1 IT Sulfathiazol 3 IT Tetracyclin 3 PL Sulfonamides 4 SI Sulfamonomethoxin 2 SK Sulphadimidine 1 SK Tylosin 8 Antibacterials 66 B3c AT Lead Pb 1 CY Lead Pb 2 FR Lead Pb 1 Heavy Metals 4 TARGET SAMPLES 70 SUSPECT B1 AT Sulfathiazol 5 BE Sulfamethazine 2 DE Sulfamerazin 1 DE Sulfamethazine 1 IT Tylosin 2 SI Sulfamonomethoxin 3 Antibacterials 14 SUSPECT SAMPLES 14 TOTAL TARGET+SUSPECT 84
EN 50 EN
ANNEX 1
ANNEX I TO DIRECTIVE 96/23/EC
GROUP A – Substances having anabolic effect and unauthorized substances
A.1. Stilbenes, stilbene derivatives, and their salts and esters
A.2. Antithyroid agents
A.3. Steroids
A.4. Resorcyclic acid lactones, including zeranol
A.5. Beta-agonists
A.6. Compounds included in Annex IV to Council Regulation (EEC) N° 2377/90 of 26 June 1990
GROUP B – Veterinary drugs and contaminants
B.1. Antibacterial substances, including sulphonamides, quinolones
B.2. Other veterinary drugs
a) Anthelmintics
b) Anticoccidials, including nitroimidazoles
c) Carbamates and pyrethroids
d) Sedatives
e) Non-steroidal anti-inflammatory drugs (NSAIDs)
f) Other pharmacologically active substances
B.3. Other substances and environmental contaminants
a) Organochlorine compounds, including PCBs
b) Organophosphorus compounds
c) Chemical elements
d) Mycotoxins
e) Dyes
f) Others
EN 51 EN
EUROPEAN COMMISSION HEALTH & CONSUMER PROTECTION DIRECTORATE-GENERAL
Directorate E - Safety of the food chain E3 - Chemicals,contaminants,pesticides
ANNEX II
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State AUSTRIA
Date 8 June 2006
Group A substances
Modification of national residue Aggregate for all animal products and plan substances
Information with regard to Nitroimidazoles (A 6) will be analysed in the recommendations of the plasma; European Commission (2005) Pigs: A 5: on farm sampling of urine instead of blood. Horses: A1, A3 and A4: urine is sampled instead of liver Accreditation and validation See information that followed the of Group A substances or questionnaire. forbidden substances according to Council Decision 2002/657/EC Due to compliant results over A 1 and A 2 in bovines animals a two or more years period, A 5 in porcine animals at slaughterhouse level the number of samples will be decreased Due to non compliant results Testosterone: young bovines (yb) at farm in 2005, the number of level and veal calves (vc) at the samples will be increased slaughterhouse Boldenone: vc and yb at farm level Nortestosterone: lambs Zeranol: lambs Chloramphenicol: vc and cows -slaughter-
EN 52 EN
house, fattening pigs (fp) - slaughterhouse General information Rabbits: For years the production of rabbits was almost non existing. In 2005, the production of rabbits reached the zero level; therefore, Austria stopped testing for residues in the species rabbits.
Non-compliant results Follow-up actions Bovines Chloramphenicol-0.7 ppb-muscle The farm was investigated and placed under veal calf (targeted sample) official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act (28 days); 21 bovine animals were held in the farm as a consequence of the positive finding. Verification of the records and official samples were taken (3 blood samples, one feed sample from complementary feed); the analyses showed negative results. Intensified checks for the next twelve months. The veterinary practitioner`s dispensary of the veterinarian in charge of the farm was checked, too. There was no indication of an illegal use of Chloramphenicol. Chloramphenicol-1.1 ppb-muscle Emergency slaughter; The farm was investigated veal calf (suspect sample) and placed under official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act (26 days); 18 bovine animals were held in the farm as a consequence of the positive finding. Verification of the records and official samples were taken (5 blood samples); the analyses showed negative results. The carcass was impounded/rejected at the slaughterhouse and declared unfit for human consumption. Intensified checks for the next twelve months. The veterinary practitioner`s dispensary of the veterinarian in charge of the farm was checked, too. There was no indication of an illegal use of
EN 53 EN
Chloramphenicol. Chloramphenicol-0.4 ppb-muscle Emergency slaughter; The farm was investigated cow (suspect sample) and placed under official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act (23 days); 27 bovine animals were held in the farm as a consequence of the positive finding. Verification of the records and official samples were taken (6 blood samples, milk samples) ; the analyses showed negative results. The carcass was impounded/rejected at the slaughterhouse and declared unfit for human consumption. Intensified checks for the next twelve months. The veterinary practitioner`s dispensary of the veterinarian in charge of the farm was checked, too. There was no indication of an illegal use of Chloramphenicol. Chloramphenicol-0.5 ppb-muscle Emergency slaughter; The farm was investigated cow (suspect sample) and placed under official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act (12 days); 64 bovine animals were held in the farm as a consequence of the positive finding. Verification of the records and official samples were taken (6 blood samples); the analyses showed negative results. The carcass was impounded/rejected at the slaughterhouse and declared unfit for human consumption. Intensified checks for the next twelve months. There was no indication of an illegal use of Chloramphenicol. Pigs Chloramphenicol-0.3 ppb-muscle The farm was investigated and placed under fattening pig (suspect sample) official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act (8 days); 400 fattening pigs and 400 piglets were held in the farm as a consequence of the positive finding. Verification of the records and 25 fattening pigs were slaughtered in order to confirm a possible
EN 54 EN
illegal treatment (25 muscle samples); the analyses showed negative results. The carcass was impounded at the slaughterhouse and declared unfit for human consumption. Intensified checks for the next twelve months. There was no indication of an illegal use of Chloramphenicol.
EN 55 EN
Group B substances
Modification of national residue Aggregate for all animal products and plan substances Information with regard to the Benzimidazoles (B 2a): The Community recommendations of the Reference Laboratory Berlin provided a European Commission (2005) Multi-residue method for benzimidazoles in muscle by LC-MSMS. The laboratory is implementing this method; this group of substances will be included into the plan by beginning 2007, at the latest.
Aquaculture: Mercury has been included. Milk: Corticosteroids (B 2f) are part of the plan 2006. Eggs: Tetracyclines (B 1) have been included into the plan. Honey: Tylosin is tested for additionally.
Due to technical problems Chlordimeform is not included into the plan (recovery rate is too high). Amitraz is not part of the plan 2006, but in 2007, it is planned to start analysing honey for Amitraz. General information New: Eggs are analysed for nicarbazin. New: In B 2e the following substances are added to the analytic spectrum: Diclofenac, Mefenamin-Acid and Tolfenaminsacid. New: For testing for chemical elements a new method is used: ICP-MS New: Cadmium, Lead and Mercury are tested for in all animal tissues as a package (multi residue method), therefore all additional samples for Mercury are cancelled. Due to compliant results over a B 1 and B 3a in horses two or moreyear period, the B 1 in poultry (broiler) number of samples will be decreased
Due to non compliant results in Inhibitors: vc, cows and fp
EN 56 EN
2005, the number of samples Sulphonamides: fp and lambs will be increased Anthelmintics: fp Anticoccidials: poultry (broiler and turkey) NSAIDs: vc and other horses (oh) - slaughterhouse Metamizol: fp Chemical elements: yb, cows, fp, other sheep (osh), oh, poultry (broiler and turkey), deer (wild game), wild boar (wild game) Dyes (Malachite green): rainbow trout and carp
Non-compliant results Follow-up actions Bovines 1 sulfadimidin- 2,836 ppb-muscle- Investigations in the farm of origin by official veal calf (targeted sample) veterinarian including verification of records (no documentation of the withdrawal period),
identification of the animals, verification of administration and storage of veterinary medicines; Official samples were taken at the next slaughter, the analyses showed a negative result. Administrative proceedings were started. 1 sulfadimidin-15,895 ppb-muscle- Investigations in the farm of origin by official veal calf (suspect sample) veterinarian including verification of records. The carcass was impounded at the slaughterhouse and declared unfit for human consumption. Slaughtered during the withdrawal period. Administrative proceedings were started against the farmer and the veterinarian in charge of the farm. 1 sulfadimidin-2,115 ppb-muscle- Investigations in the farm of origin by official veal calf (suspect sample) veterinarian including verification of records. The carcass was impounded at the slaughterhouse and declared unfit for human consumption. 1 sulfadimidin-1,921 ppb and Investigations in the farm of origin by official Chlortetracycline 149 ppb-muscle- veterinarian including verification of records. veal calf (suspect sample)
EN 57 EN
The carcass was impounded at the slaughterhouse and declared unfit for human consumption. 2 sulfadimidin-1,375/8,835 ppb- Investigations in the farms of origin by official muscle-cows (suspect samples) veterinarians including verification of records. The carcass was impounded at the slaughterhouse and declared unfit for human consumption. 4 streptomycin-3,930-8,432 ppb- Investigations in the farms of origin by official kidney-cows (suspect samples) veterinarians including verification of records. The carcasses were impounded at the slaughterhouse and carcasses and/or offals were declared unfit for human consumption. 9 phenylbutazone-0.6-3.0 ppb-blood- The farm (farm of origin and a second location veal calves (targeted samples) of this farm in another province) was investigated and and placed under official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act (12 days); 66 bovine animals (veal calves) were held in the farm as a consequence of the positive findings. Verification of the records. Official samples were taken (12 blood samples); the analyses showed negative results. Intensified checks for the next twelve months. The veterinary practitioner`s dispensary of the veterinarian in charge of the farm was checked, too. 2 veal calves were killed and sent to a processing plant of catgory 1 material as defined by Regulation (EC) No. 1774/2002. Administrative proceedings were started against the farmer and the veterinarian in charge who administered phenylbutazon. Phenylbutazon had been mixed in the feed. 2 lead-0.14/0.97 ppm-muscle-cows Investigations in the farms of origin by official (targeted samples) veterinarians including verification of records; Additional sampling is planned. 8 cadmium-1.11-2.23 ppm-kidney- Investigations in the farms of origin by official cows (7) and young bovine (1) veterinarians including verification of records; (targeted samples)
EN 58 EN
Pigs 2 amoxicillin-186/4,936 ppb-muscle- Farm 1 and 2: Investigations in the farms of fattening pigs (targeted samples) origin by official veterinarians including verification of records, identification of the animals, verification of administration and storage of veterinary medicines Farm 1: An official sample was taken at the next slaughter, where the analysis showed a negative result. Farm 2: The animal had been slaughtered before the end of the withdrawal period. Administrative proceedings, penalty is final. 1 sulfadimidin-516 ppb-muscle- Investigations in the farm of origin by official fattening pig (targeted sample) veterinarian including verification of records (no documentation). The use of medicated feedingstuff was not in line with the provisions laid down in the Tierarzneimittelkontrolgesetz (Veterinary Medicinal Products Act). Additionnally, the farmer did not have the qualification in mixing medicated feedingstuffs. Administrative proceedings were started against the farmer. 1 tylosin-118 ppb-muscle- fattening Investigations in the farm of origin by official pig (suspect sample) veterinarian including verification of records. The carcass was impounded at the slaughterhouse and declared unfit for human consumption. 1 danofloxacin-421 ppb-muscle- Investigations in the farm of origin by official fattening pigs (suspect sample) veterinarian including verification of records. The carcass was impounded at the slaughterhouse and declared unfit for human consumption. The veterinary practitioner`s dispensary of the veterinarian in charge of the farm was checked. Oral instruction and oral caution. 1 abamectin-3.1 ppb-liver- fattening The farm was investigated and and placed under pig (targeted sample) official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act (32 days); 140 fattening pigs were held in the farm as a consequence of positive finding. Verification of the records. 11 fattening pigs were slaughtered in order to
EN 59 EN
confirm a possible illegal treatment (11 liver samples); one official feed sample was taken too; the analyses showed negative results. 1 metamizol-308 ppb-muscle- Investigations in the farm of origin by official fattening pig (targeted sample) veterinarian including verification of records and placing under official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act (32 days); 411 pigs (161 fattening pigs, 33 sows, 119 piglets, ..) were held in the farm as a consequence of the positive finding. 13 fattening pigs were slaughtered in order to confirm a possible illegal treatment; the analyses showed negative results. The carcass were impounded at the slaughterhouse and then based on the result of the analyse declared fit for human consumption. The administration of metamizol was documented correctly and the animal was not slaughtered during the withdrawal period. 1 ramifenazon-20 ppb-kidney- The farm was investigated; verification of the fattening pig (targeted sample) records. The veterinary practitioner`s dispensary of the veterinarian in charge of the farm was checked (non announced visit). Official samples taken at the slaughterhouse and official samples of feed, the analyses showed negative results. 1 lead-45 ppm-liver- fattening pig Investigations in the farm of origin by official (targeted sample) veterinarian including verification of records; Additional sampling is planned. 1 cadmium-3 ppm-kidney- fattening Investigations in the farm of origin by official pig (targeted sample) veterinarian including verification of records; Additional sampling is planned.
Poultry 3 nicarbacin-25.8/3.7/11.6 ppb-liver- Investigations in the farms of origin by official broiler veterinarians including verification of records; (targeted samples) Follow-up samples. Farm 3: additionally, feed of the feedmill was checked.
EN 60 EN
2 lasalocid-139/188 ppb-liver-turkey Farm1: Investigations in the farm of origin by (targeted samples) official veterinarian; official sample of feed. Oral instruction. Farm 2: Investigations in the farm of origin by official veterinarian; Labelling of feed was not correct, therefore the farmer mixed feed plus lasalocid and feed without lasalocid; Official samples were taken. Oral instruction and caution and time limit set to take all necessary corrective actions 1 flunixin-0.4 ppb-blood-turkey Investigations in the farm of origin by official (targeted sample) veterinarian including verification of records; 3 official samples were taken at the slaughterhouse, the analyses showed negative results. No indication of an illegal use of this substance. 3 cadmium-1.08-2.27 ppm-kidney- Investigations in the farms of origin by official broiler (1) and turkey (2) (targeted veterinarians including verification of records; samples) Additional samples.
Sheep and goat 1 sulfadimidin-223 ppb-muscle-lamb Investigations in the farm of origin by official (targeted sample) veterinarian including verification of records. 1 flunixin-0.4 ppb and Investigations in the farms of origin by official tolfenaminacid-0,1 ppb–blood-lamb veterinarians including verification of records; 1 flunixin-250 ppb ppb–blood-lamb The veterinary practitioner`s dispensaries of the (targeted samples) veterinarians in charge of the farm were checked, too. In both cases there was no indication of an illegal use of this substance; in the second case the farmer argued that there was a mix up of the samples in the slaughterhouse; Additional samples are planned for 2006. 4 cadmium-1.14-1.3 ppm-kidney- Investigations in the farms of origin by official other sheep (targeted samples) veterinarians including verification of records; Additional sampling. 1 lead-liver and cadmium-kidney- Investigations in the farm of origin by official 0.76 and 1.53 ppm-other sheep veterinarian including verification of records; (targeted sample) Additional sampling.
EN 61 EN
Horses 1 phenylbutazone-6 ppb-blood-other Investigations in the farm of origin by official horse veterinarian including verification of records, (targeted sample) Official samples were taken from three horses. Oral instruction. 1 cadmium-7.1 ppm-muscle-other Investigations in the farm of origin by official horse (targeted sample) veterinarian including verification of records; Additional sampling. Milk - - Eggs
1 lasalocid-6.5 ppb (targeted sample) Investigations in the farm of origin (farm of layers) by official veterinarian including verification of records). Official samples (eggs-9 and feed-1) were taken; the analyses showed negative results. Criminal proceedings were started against the farmer. Rabbit - - Aquaculture 1 malachite green-<2.5 ppb-muscle- The farm was investigated and placed under trout (targeted sample) official control by the district administrative authority in accordance with article 26b of the Meat Inspection Act. Verification of the records and official samples were taken (3 samples); the analyses showed non compliant results. Confirmation of the illegal use of malachite green. Due to the effect of a flood in the area of the farm, the whole farm had been destroyed. 3 malachite green-1.7/<1.2/<1.2 ppb- Additionally, official samples were taken at the muscle-trouts (suspect samples) above mentioned farm. 1 leukomalachite green-14.4 ppb- The farm was investigated and placed under muscle-trout (targeted sample) official control (75 days) by the district administrative authority in accordance with article 26b of the Meat Inspection Act. Verification of the records; Official samples
EN 62 EN
were taken (4 samples); the analyses showed non compliant results. Confirmation of the illegal use of leukomalachite green. The fishes were killed and sent to a processing plant of catgory 1 material as defined by Regulation (EC) No. 1774/2002. Administrative proceedings were srated against the farmer. 4 leukomalachite green- Additionally, official samples were taken at the 6.9/7.9/5.8/65.9 ppb-muscle-trouts above mentioned farm. (suspect samples) 1 leukomalachite green-15 ppb- The farm is placed under official control by the muscle-carp (suspect sample) district administrative authority in accordance with article 26b of the Meat Inspection Act. To date, the proceedings have not been concluded.
Farmed game - - Wild game 12 lead-1.2-282 ppm-muscle-deer In wild game (deer), the high level of lead is (9), red deer (1), chamois (1) and more or less due to bullets, especially to the wild boar (1) (targeted samples) modern construction of bullets and the type of bullets. The contamination of the meat is also depending from the way how the bullets penetrate the body of the animals. Honey 1 sulfathiazol-285 ppb Investigations in the bee farm by official (targeted sample) veterinarian including verification of records. Due to the effect that no more honey from this charge was available, no additional samlpling was possible. Administrative proceedings were started against the bee keeper. 1 sulfathiazol-29.8 ppb Investigation of the bee farm by official (targeted sample) veterinarian including verification of records. Official detention of the honey and a suspect sample was taken and analysed. The analysis showed a negative result.
EN 63 EN
No administrative proceedings were started against the bee keeper. 1 sulfathiazol-996 ppb Investigation of the bee farm by official (targeted sample) veterinarian including verification of records. As a consequence of the positive finding, all colonies of bees were held in the bee farm. Official detention of the honey and 3 samples were taken and analysed. The analysis showed positive results. 414.5 kg honey was declared unfit for human consumption. Due to the event of repeated infringements, checks will be intensified in 2006. Administrative proceedings were started against the bee keeper. 3 sulfathiazol-106/151/1526 ppb Suspect samples of above mentioned bee farm. (suspect samples)
2 sulfathiazol-428/1366 ppb Investigation of the bee farm by official (suspect samples) veterinarian including verification of records. As a consequence of the positive finding, all colonies of bees were held in the bee farm. Official detention of the honey and samples were taken and analysed. 108.5 kg honey was declared unfit for human consumption. Criminal proceedings were started against the bee keeper. 1 lead-4.7 ppm Investigation of the bee farm by official veterinarian including verification of records. (targeted sample) Official samples were taken and order given to improve the system of self control. Criminal proceedings were started against the bee keeper.
EN 64 EN
Accreditation and validation of Group A substances or forbidden substances according to Council Decision 2002/657/EC:
The accreditation and validation of the following substances are accomplished according to an internal action plan of the laboratory, the CC Veterinary Drugs and Hormones (AGES CC TAHO):
A 3: Trenbolone, Nortestosterone
A6: Chloramphenicol, Nitrofurane metabolites, Nifursol
B 2b: Anticoccidials
B 2e: Non Steroidal Anti-inflammatory Drugs (except Caprofen, Diclofenac, Mefenamin-Acid and Tolfenaminsacid)
For the rest of Group A substances and forbidden substances of Group B, the management of the Austrian Agency for Health and Food Safety signed a contract with the Community Reference Laboratories (CRLs) Bilthoven (A 1, A 2, some of A 3, A 4 and B 2f) and Berlin (Nitroimidazoles (A 6), A 5, B 2e - the above mentioned substances) for 2006.
Most of the accreditation and validation should be finished in 2006; in the meantime,screening positive samples will be confirmed by the above mentioned CRLs.
The following confirmatory methods will be established for the following subgroups or substances of Annex I of Council Directive 96/23/EC:
Subgroup Confirmatory method
A 1 LC-MS A 2 LC-MS A 3 Testosterone Estradiol LC-MS Boldenone Gestagenes A 4 LC-MS A 5 LC-MS A 6 GC-MS Nitroimidazoles B 2f LC-MS Corticosteroids
EN 65 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State BELGIUM
Date 12 July 2006
Group A substances
Modification of national residue Aggregate for all animal products and substances plan - The national production has been calculated on the basis of the sum of the last 3 years + normal deviation. Number of samples has been modified proportionally to the production amounts which were sometimes lower than the ones used for the 2005 plan; - The number of samples has been lowered by about 5 % for substance/species for which no non compliant results have been observed from 2000-2004 period; - The number of samples for thyreostats analysis was lowered to the minimal number fixed by the Council directive 96/23/EC; - Until now, several species were sampled for farmed game but often number of samples was very low (1 or 2). From this year we have chosen to target each year on one species in the aim to increase the statistical value of the results. In 2006 we target on pigeons as a result of the 2004 FVO inspection report. In 2006 about 167 samples will be taken in pigeons instead of 86 in 2005; - For nitroimidazoles analysis, plasma samples have been added : in pig, 25 plasma and 74 muscle samples; in chicken, 40 plasma and 40 muscle samples; in hens, 5 plasma and 10 muscle samples; in ducks, 5 plasma and 10 muscle samples; in guinea fowl, 5 plasma and 10 muscle samples; in turkeys, 10 plasma and 10 muscle samples; - A new approach using a risk assessment has been used to determine the number of samples for all substance groups in milk and eggs. A score is allocated to the nature of the hazard (0-4), the non compliance history/the risk of contamination (0-3) and the contribution to the diet of the product. The total score set a prevalence to check and a confidence level to respect and the number of samples to take is determine using a statistics software. Consequently, number of samples decreased for some substance groups; - Total milk samples for dapson analysis is decreased to 65; - Total milk samples for nitrofurans metabolites and nitroimidazoles analysis is increased to 156; - Samples of sheep, goat and mare milk are nom analysed for all substances groups; - In eggs, samples for nitroimidazoles analysis are decreased to 40.
EN 66 EN
Non-compliant results Follow-up actions Alpha boldenon-244 ppb-beta Farm was investigated; additional samples of animals, boldenon-10 ppb-alpha testosteron materials and feed have been taken, fattening animals 10 ppb-prednisolon-no value-feces- put under temporary seizure. 2 material samples non calf compliant for prednisolon, testosterone and ester- testosteron. H status allocated. Clenbuterol-2 material samples- In 1 farm investigated as follow up for animal bovine identification default. Additional samples of animal matrices, material and feed taken; fattening animals put under temporary seizure. Material samples (4) contained also phenylbutazone. Other samples compliant. Progesteron-methyltestosteron- In 1 farm investigated as follow up for prednisolon clenbuterol-dexamethason- non compliant result in slaughterhouse. Additional dexamethason isocotinoat- 19 samples of animal matrices and feed were also taken, material samples all compliant. Fattening animals put under temporary seizure. H status allocated. Some analysis results made on In all of these cases, an investigation on farm is samples taken during monitoring at performed, samples of animals, feed and material are farm or slaughterhouse levels taken and fattening animals are put under temporary showed presence of some seizure. These analysis enter in the account of suspect hormones/and corticosteroids. samples. These results could not been
considered as non compliant but were considered as suspects.
1/ Alpha boldenon- beta boldenon- alpha testosteron -feces-calf For cases 1 to 12 : no non compliant results in 2/ Alpha boldenon -feces-bovine additional samples. 3/ Alpha boldenon- feces-calf 4/ Alpha boldenon-alpha oestradiol- For the case 13 : non compliant results in samples of feces-calf material : chlortestosteron acetate, progesteron, fluoxymesteron, algenoneaceto-phenide. H status 5/ Alpha boldenon-feces-bovine allocated. 6/ Progesteron-bovine
7/ Alpha boldenon-beta boldenon- For the case 14 : non compliant result in material alphatestosteron-feces-bovine sample : methyltestosteron-medroxyprogesteron 8/ Alpha boldenon-feces-bovine acetate-testosteron decanoat-nortestosteron decanoat. 9/ Alpha boldenon-beta boldenon- alpha testosterone-feces-bovine 10/ Alpha boldenon-beta boldenon-
EN 67 EN
alpha testosterone-feces-calf 11/ Beta testosterone-matrix ?-pig 12/ Alpha oestradiol-urine-bovine 13/ Alpha boldenon-beta boldenon- alpha testosteron-matrix ?-bovine 14/ Dexamathason CAP-0,1 ppb-milk Result under MRPL CAP-<0.3 ppb-eggs Result under MRPL. Eggs put under seizure on farm, additional samples of feed and egg taken, compliant result, eggs released. Administrative measures H status : for 52 weeks animals from the farm may only be sent to slaughterhouse in Belgium where 10 % of them are analysed at the expense of the farmer. In case of new infringement during this period, another period of 104 weeks is added to the first one. H status was allocated to 1 pig farm due to furaltadone non compliant result in feed. CRIMINAL PENALTIES In all cases of infringements relating to group A substances (except A6), a Pro Justicia is sent to prosecutor who decides whether prosecution or not (Law 15 July 1985 Hormones1 e.a.). In 2005, there were verdicts and judgements imposing or confirming criminal penalties to 6 individuals relating to the Law 15 July 1985 Hormones and for some to the Law 24 February 1921 Traffic of substances2 One individual was convinced to effective jail sentence and an effective fine. Two were convinced to suspended jail sentences, effective fines and seizure of money. One was also convicted to closing of exploitation, to ban to market animals and to run a farm for 1 year. Three individuals were convinced to effective fines and also to suspended fines. Two were convinced to the publication of the sentences in papers. 1 Loi du 15 Juillet 1985 relative à l’utilisation de substances à effet hormonal, à effet anti- hormonal, à effet beta-adrénergique ou à effet stimulateur de production chez les animaux.
2 Loi du 24 Février 1921 concernant le trafic de substances vénéneuses, soporifiques, stupéfiantes, désinfectantes ou antiseptiques.
EN 68 EN
Group B substances
Modification of national residue Aggregate for all animal products and substances plan - The national production has been calculated on the basis of the sum of the last 3 years + normal deviation. Number of samples has been modified proportionally to the production amounts which were sometimes lower than the ones used for the 2005 plan; - The number of samples has been lowered by about 5 % for substance/species combination for which no non compliant results have been observed from 2000- 2004 period; - A new approach using a risk assessment has been used to determine the number of samples for B3 group in animals/animal matrices. A score is allocated to the nature of the hazard (0-4), the non compliance history/the risk of contamination (0-3) and the contribution to the diet of the meat. The total score set a prevalence to check and a confidence level to respect and the number of samples to take is determine using a statistics software. The number of samples is then allocated between the different species/animal categories using several criteria (non compliance history, probability of environmental contamination, probability of use, age of animals at slaughtering, etc). Generally more samples will be taken for dioxins and dioxin like PCB and less for marker PCB, pesticides and chemical elements; - Until now, several species were sampled for farmed game but often number of samples was very low (1 or 2). From this year we have chosen to target each year on one species in the aim to increase the statistical value of the results. In 2006, we target on pigeons as a result of the 2004 FVO inspection report. In 2006 about 167 samples will be taken in pigeons instead of 86 in 2005; - In bovine, 25 samples for benzimidazols analysis have been added; - In horses, 10 samples for corticosteroid analysis have been added; - The same risk assessment approach that for B3 substances in animal matrices has been applied for all substance groups in eggs and milk. Consequently, number of samples decreased for some substance groups; - In milk mercury and arsenic are now analysed; - Total milk samples for B1 analysis is decreased to 118; - In cow milk samples analysed for benzimidazoles and avermectines are decreased to 34; samples for NSAID are decreased to 12; samples for dioxins analysis are increased to 110, for dioxin like PCB and for marker PCB to 58. Samples analysed for OC pesticides are decreased to 30. Thirty samples are analysed for mercury and arsenic. Samples analysed for aflatoxin are decreased to 98. Samples of sheep, goat and mare milk are now analysed for all substances groups; - Milk of sheep : 10 samples for avermectins and benzimidazoles, 2 samples for NSAID; 10 samples are analysed for dioxins, dioxin like PCB and marker PCB; 10 samples are analysed for OC and OP pesticides; 15 samples are analysed for lead; 10 samples are analysed for cadmium, arsenic and mercury; - Milk of goat : 10 samples for avermectins and benzimidazoles, 6 samples for NSAID, 26 samples analysed for dioxins, 18 samples analysed for dioxin like
EN 69 EN
PCB and marker PCB, 10 samples analysed for OC pesticides and 10 samples analysed for OP pesticides and 15 samples analysed for chemical elements; - Milk of mare : 5 samples for avermectins and benzimidazoles, 2 samples for NSAID; 10 samples are analysed for dioxins, dioxin like PCB and marker PCB; 10 samples analysed for OC and OP pesticides; 5 samples analysed for lead; 10 samples analyse for cadmium, mercury and arsenic; 5 samples analysed for aflatoxin; - In eggs, samples for B1 analysis decreased to 59; samples for B2b decreased to 100; samples for marker PCB decreased to 80. 53 samples for lead, cadmium and arsenic analysis and 29 samples for mercury analysis have been added. Non-compliant results Follow-up actions Bovines In 2005, the Public Prosecutor Service opened an investigation concerning the use of feed supplement containing dexamethason. An investigation was made to identify the origin, the middlemen and the farms concerned. 68 farms were investigated, samples of animal matrices, feed and sometimes materials were taken. 13 of these farms were investigated due to 18 dexamethason non compliant results at slaughterhouse. Fattening animals were put under temporary seizure. Farms were put under surveillance. Suspect samples. These results have led to methason-animal matrix-slaughterhous investigation at farms (see above). Suspect samples. Concerned 33 farms. In 14 of methason-animal matrix-farm these farms, dexamethason was found in animal and feed samples. In 1 farm, dexamethason was methason-feed only found in feed. A total of 51 animals were slaughtered and destroyed. H status was allocated to the concerned farms. These cases are still under prosecution proceeding.
3 target and 1 suspect samples. One carcass isolon-at slaughterhouse-3 bovine destroyed. Three farms investigated. Samples of alf animal matrices and feed taken. Fattening animals put under temporary seizure. Additional samples compliant. In 1 farms, also material samples taken, see A substances non compliant result in material. Target samples. Investigation in these 2 farms. methason-at slaughterhouse Samples of animal matrices, material and feed taken. Animals put under temporary seizure until results. In 1 farm, feed sample non compliant for dexamethason.
EN 70 EN
Target sample. Investigation on farm. Record ne-1 kidney checked. R status allocated. Suspect samples. For one case, a attest of the n-4 injection site (+1meat) veterinarian was present, no investigation. Investigation on 3 farms and records checked. In 2 cases : Pro Justicia was established. In one case, withdrawal period was well respected. The 4 carcasses were destroyed. 1 target and 1 suspect samples. 1 farm tracyclin-1 kidney and 1 injection investigated, record checked. Suspect carcass was accompanied with vet attest, no investigation, carcass destroyed. Suspect samples. 2 carcasses with vet attest, no in-3 injection sites and 2 meat investigation, carcasses destroyed. In the other case, farm investigated, record checked and carcass destroyed. Target samples. In Belgium, kidneys from animal mium-kidney aged from more than 1 year are declared unfit for consumption. Target sample. In Belgium, kidneys from animal kidney aged from more than 1 year are declared unfit for consumption. Suspect samples. Farms investigated, records illin-injection sites checked. 1 Pro Justicia allocated, in one case the withdrawal time was respected. 5 carcasses destroyed. Suspect sample, farm investigated, record tracyclin-injection site checked, carcass destroyed. Suspect sample, investigation at farm, record hoprim-injection site checked, withdrawal time respected, carcass destroyed. Suspect sample, investigation at farm, record dimethoxin-trimethoprim-tolfenamic checked, carcass destroyed. ection site Suspect sample, investigation at farm, record ycillin-oxytetracyclin-injection site checked, carcass destroyed. PV to veterinarian. R status. Suspect sample, investigation at farm, record illin G-flunixin-injection site checked, carcass destroyed. Suspect sample, investigation at farm, record tracyclin-levamisol-injection site checked, carcass destroyed
EN 71 EN
Suspect sample, investigation at farm, record dimethoxin-trimethoprim- checked, carcass destroyed. R status allocated. mycin-injection site (meat non ant only for trimethoprim) Suspect samples, investigation at farms, records cosin-injection site checked, withdrawal time respected, carcasses destroyed. Suspect sample, investigation farm, record omycin-injection site checked, carcass destroyed. Suspect samples. Animal from Luxembourg, no tracyclin-tolfenamic acid-injection investigation, destruction.
Suspect sample, investigation farm, record n-tolfenamic acid-injection site checked, carcass destroyed. Suspect samples, investigation farms, records in-5 injection site (+ 1 meat) checked, carcasses destroyed. 3 R status allocated. In 1 case, Pro Justicia allocated to veterinarian. Suspect samples, investigation farms, records olfenamic-injection sites checked, carcasses destroyed. Suspect sample, carcass destroyed. amic acid-phenylbutazone-injection eat only NC for PBZ) Target sample, investigation farm, record checked. diazin-kidney R status allocated.
Some analysis results made on In all of these cases, an investigation on farm is samples taken during monitoring at performed, records checked, samples of animals, farm or slaughterhouse level feed and material are taken and fattening animals showed presence of are put under temporary seizure. These analysis corticosteroids. These results could enter in the account of suspect samples. not been considered as non compliant but were considered as suspects.
1/ Dexamethason-bovine 1/See A non compliant results in material samples slaughterhouse 2/Dexamethason-phenylbutazon- 2/1 farm investigated. Samples of animal matrices, bovine slaughterhouse material and feed taken. Material samples (1) non compliant for dexamethason.
EN 72 EN
Suspect samples. Tested by an inhibition test erial inhibitor-kidney (Belgian kidney test) when carcass at slaughterhouse presents deficiencies. In case of non compliant result, carcass is destroyed but no farm investigation is made. 58 carcasses destroyed.
Pigs 1 lead-kidney Target sample. No information 3 oxytetracyclin-2 kidney and meat, 2 target and 1 suspect samples.1 sow from 1 injection site and meat Netherland, no investigation, carcass destroyed. Investigation in 2 farms, records checked, 2 R status allocated. 1 doxyciclin- kidney and meat Target sample, investigation at farm, record checked, R status allocated. 1 amoxyciclin-kidney Target sample, investigation at farm, record checked, R status allocated. 2 penicillin-1 kidney + injection site Target and suspect samples. Investigation at and 1 kidney + meat farms, records checked, 1carcass destroyed, 2 R status allocated. 1 sulfadiazin-kidney Target sample, investigation farm, record examined, R status. 1 sulfadimidin-kidney Target sample, investigation farm, record examined,. 27 bacterial inhibitors-kidney Suspect samples. Tested by Belgian kidney test, 27 carcasses destroyed
Poultry 3 diclazuril-meat-broilers Target samples. Investigations at 3 farms, records checked, additional samples taken which showed non compliant results, the withdrawal time was respected in all cases, meat not authorised for be put on market in UE. 1 nicarbazine-meat-broiler Target sample. Investigation at farm, record checked. Carcasses already consumed. 1 flunixin-meat broiler Target sample. Investigation on farm, check of record. 700 kg carcasses destroyed.
EN 73 EN
Sheep and goat 1 cadmium-kidney Target sample. No information
Horses 15 Bacterial inhibitors-kidney Suspect samples. At slaughterhouse. Tested by Belgian kidney test, 15 carcasses destroyed.
Milk 1 Dioxin Target sample. Milk temporary seized at farm. Counter analyse conform. Milk released. 1 Marker PCB Target sample. Milk temporary seized at farm, commercial distribution only if skimmed, 3 suspect samples taken at different time, third sample compliant thus milk released. 1 Ivermectin Target sample. Milk temporary seized, suspect sample taken, result compliant, milk released. 4 samples suspected to contain Target samples. antibacterial substances No confirmatory analysis (sulfonamides, tetracyclines, tetracyclines or sulfonamides, No follow up tetracyclines or sulfonamides or macrolides)
Eggs 3 lasalocid Target samples. Investigation at 3 farms. In one case, hens have been slaughtered, no follow up. In two farms, eggs present blocked, additional samples taken of eggs and feed, compliant results, eggs released. 1 salinomycin Target sample. Investigation at farm, eggs put under seizure, additional sample taken, non compliant result, destruction of 23130 kg eggs.
Rabbit 1 robenidin-meat Target sample. No information
Aquaculture 3 malachite green-meat Target samples. Investigations at 3 farms. In one
EN 74 EN
farm, fish destroyed. In 2nd farm, 1320 kg fish destroyed. In 3rd farm, trade forbidden until compliant result. Farmed game Target sample. No follow up n-meat pigeon
Wild game
compliant result Honey 3-sulfamethazine Target samples. 3 producers. Investigations at production sites. Honey put under seizure. Additional samples on 6 lots, 5 non compliant results, non compliant lots destroyed (410 kg of honey). 1-sulfathiazole Target samples. Investigation on one production site, honey put under seizure. 6 kg destroyed. Administrative measures R status : R-status: for a 8 weeks period the identification document of the animals of the same species (bovine, pigs) from the herd are marked with a R symbol. These animals cannot be exported anymore, they can only be transported to national slaughterhouse. In the slaughterhouse, 10 % of these animals are sampled. In case of new infringements during this period, the period will be extended by 26 weeks. The analysis are at the expense of the responsible of the herd. 2 R status allocated to pig farms due to non compliant result for oxytetracyclin and doxycyclin-sulfadimidin in 2004.
3 H status have been allocated to pig farms due to corticosteroid non compliant results in 2004. Official reports sent to the legal service for the attribution of administrative penalty : 15. Fines paid : 11. Prosecution : 5
EN 75 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State CYPRUS
Date Period Covered: 2005
1. Sampling should take place over the entire year (January to December); 2. The tender of Veterinary Services of Cyprus for the interest of accredited laboratories to carry out the laboratory examinations of substances of animal tissues and food of animal origin that are included in the National Residues Plan concerning the year 2007 must be published in the European gazette early in July 2006. 3. Horsemeat. There is not slaughterhouse for horses. Horsemeat is not used for human consumption in Cyprus. Horses exported from Cyprus accompanied by a Passport (Commission Decision 200/68/EC) is implemented on the basis of “Genetic improvement of Animals” Law 86 (I) 2001, Κ.Δ.Π. 522/2005, Αρ. 4051., 18.11.2005 in which mentioned all the drugs used for this horse and the withdrawal period. 4. Efforts are in progress to arrange NRP tests to be carried out in foreign accredited laboratories in order to cover all the numbers on all substances provided in the programme for the year 2006. 5. WE CONFIRM that all methods used by the foreign laboratories to carry out analysis were validated and accredited. This is a basic term included in the Tender. During the evaluation of laboratories responded to the Tender, the evaluation committee checked first if the method used by the laboratory is validated and accredited and for which matrix and if this method is included in the list of the accreditation body.
EN 76 EN
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
1. BOVINES
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil URINE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Methyl Thiouracil, MRPL 100 μg/kg 4
4 Farm
Slaughter house Fattening Bovines
A3 Allyltrenbolone (Altrenogest) Chlormadinonacetat Medroxyprogesteronacetate Megestrolacetate Melengestrolacetate KIDNEY FAT GC-MS 1-5 μg/kg Same as screening Same as limit for screening method Medroxyprogesterone acetate,
MRPL 1 μg/kg 3 Slaughterhouse Fattening Bovines
A3 Allyltrenbolone (Altrenogest) Boldenone Trenbolone URINE GC-MS/MS 1 µg/kg Same as screening Same as limit for screening method MRPL 2 μg/L 2 Slaughterhouse Fattening Bovines
A5 Brombuterol Clenbuterol Mabuterol URINE LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/L 2
2
Farm
Slaughter house Fattening Bovines
A5 Cimaterol Ractopamine Salbutamol Terbutaline URINE LC-MSMS 0.5-1 μg/L Same as screening Same as limit for screening method MRPL 3 μg/L 2
2 Farm
Slaughter house Fattening Bovines
EN 77 EN
2. PORCINE
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil URINE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Methyl Thiuracil MRPL 100 μg/L 5
3 Slaughterhouse
Farm Fattening Pigs
A3 Allyltrenbolone (Altrenogest) Chlormadinonacetat Medroxyprogesteronacetate Megestrolacetate Melengestrolacetate KIDNEY FAT GC-MS 1-5 μg/kg Same as screening Same as limit for screening method Medroxy progesterone Acetate MRPL 1 μg/kg 8 Slaughterhouse Fattening Pigs
A5 Brombuterol Clenbuterol Mabuterol URINE LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/L 3 Farm Fattening Pigs
A5 Brombuterol Clenbuterol Mabuterol URINE LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/L 5 Slaughterhouse Fattening Pigs
A5 Cimaterol Ractopamine Salbutamol Terbutaline URINE LC-MSMS 0.5-1 μg/L Same as screening Same as limit for screening method MRPL 3 μg/L 3 Farm Fattening Pigs
A5 Cimaterol Ractopamine Salbutamol Terbutaline URINE LC-MSMS 0.5-1 μg/L Same as screening Same as limit for screening method MRPL 3 μg/L 5 Slaughterhouse Fattening Pigs
6. SHEEP AND GOATS
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil URINE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Methyl thiuracil MRPL 100 μg/L 1 Slaughterhouse Kids
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil URINE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Methyl thiuracil MRPL 100 μg/L 1 Farm Lambs
EN 78 EN
A3 Chlormadinonacetat Megestrolacetate Melengestrolacetate KIDNEY FAT GC-MS 5 µg/kg Same as screening Same as limit for screening method Presence 2 Slaughterhouse Goats
A3 Chlormadinonacetat Megestrolacetate Melengestrolacetate KIDNEY FAT GC-MS 5 µg/kg Same as screening Same as limit for screening method Presence 2 Slaughterhouse Ewes
A3 Medroxyprogesteronacetate KIDNEY FAT GC-MS 1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/kg 1 Slaughterhouse Goats
A3 Medroxyprogesteronacetate KIDNEY FAT GC-MS 1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/kg 1 Slaughterhouse Ewes
A5 Brombuterol Clenbuterol Mabuterol URINE LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/L 1 Farm Lambs
A5 Brombuterol Clenbuterol Mabuterol URINE LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/kg 1 Farm Kids
A5 Cimaterol Ractopamine Terbutaline URINE LC-MSMS 0.5 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/L 1 Farm Kids
A5 Cimaterol Ractopamine Terbutaline URINE LC-MSMS 0.5 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/L 1 Farm Lambs
4. POULTRY
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 5 Slaughterhouse Broiler
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 1 Slaughterhouse Turkey
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 1 Slaughterhouse Ducks
EN 79 EN
A3 Allyltrenbolone (Altrenogest) Boldenone Trenbolone LIVER GC-MS/MS 2 µg/kg Same as screening Same as limit for screening method Presence 5 Slaughterhouse Broiler
A3 Allyltrenbolone (Altrenogest) Boldenone Trenbolone LIVER GC-MS/MS 2 µg/kg Same as screening Same as limit for screening method Presence 1 Slaughterhouse Turkey
A3 Allyltrenbolone (Altrenogest) Boldenone Trenbolone LIVER GC-MS/MS 2 µg/kg Same as screening Same as limit for screening method Presence 1 Slaughterhouse Ducks
A5 Brombuterol Clenbuterol Mabuterol LIVER LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/kg 1 Slaughterhouse Turkey
A5 Brombuterol Clenbuterol Mabuterol LIVER LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/kg 1 Slaughterhouse Ducks
A5 Brombuterol Clenbuterol Mabuterol LIVER LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/kg 5 Slaughterhouse Broiler
A5 Cimaterol Ractopamine Terbutaline LIVER LC-MSMS 0.5 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/kg 5 Slaughterhouse Broiler
A5 Cimaterol Ractopamine Terbutaline LIVER LC-MSMS 0.5 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/kg 1 Slaughterhouse Turkey
A5 Cimaterol Ractopamine Terbutaline LIVER LC-MSMS 0.5 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/kg 1 Slaughterhouse Ducks
5. AQUACULTURE
A3 Allyltrenbolone (Altrenogest) Boldenone Trenbolone MUSCLE+SKIN (FISH) GC-MS/MS 2 µg/kg Same as screening Same as limit for screening method Presence 12
6. MILK
EN 80 EN
7. RABBITS
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRPL 100 μg/L for Thiouracil 3 Rabbits
A3 Allyltrenbolone (Altrenogest) Boldenone Trenbolone LIVER GC-MS/MS 2 µg/kg LC-MSMS Same as limit for screening method MRPL 2 μg/kg 3 Rabbits
A5 Brombuterol Clenbuterol Mabuterol URINE LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/L 3 Rabbits
A5 Salbutamol URINE LC-MSMS 1 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/L 3 Rabbits
A5 Cimaterol Ractopamine Terbutaline URINE LC-MSMS 0.5 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/L 3 Rabbits
8. FARMED WILD GAME
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 2 Slaughterhouse Quail
A2 Methylthiouracil Phenylthiouracil Propylthiouracil Thiouracil MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 2 Slaughterhouse Ostriches
A3 Allyltrenbolone (Altrenogest) Boldenone Trenbolone LIVER GC-MS/MS 2 µg/kg Same as screening Same as limit for screening method MRPL 2 μg/kg 2 Slaughterhouse Quail
A3 Allyltrenbolone (Altrenogest) Boldenone Trenbolone LIVER GC-MS/MS 2 µg/kg Same as screening Same as limit for screening method MRPL 2 μg/kg 2 Slaughterhouse Ostriches
A5 Brombuterol Clenbuterol Mabuterol LIVER LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1
EN 81 EN
μg/kg 5 Slaughterhouse Quail
A5 Cimaterol Ractopamine Salbutamol Terbutaline LIVER LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/kg 5 Slaughterhouse Quail
A5 Brombuterol Clenbuterol Mabuterol LIVER LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 1 μg/kg 5 Slaughterhouse Ostriches
A5 Cimaterol Ractopamine Salbutamol Terbutaline LIVER LC-MSMS 0.1 µg/kg Same as screening Same as limit for screening method MRPL 3 μg/kg 5 Slaughterhouse Ostriches
9. HEN EGGS
10. HONEY
A6 Chloramphenicol HONEY GC-MS (NCI) 0.1 µg/kg Same as screening Same as limit for screening method MRPL 0.3 μg/kg 13 Honey
A6 AHD AMOZ AOZ SEM (semicarbazide) HONEY LC-MSMS 0.6-0.7 μg/kg Same as screening Same as limit for screening method MRPL 1 μg/kg 13 Honey
Non-compliant results Follow-up actions NONE NONE
• Information to be included for each non-compliant result. In case of several non- compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 82 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances 1. BOVINES
B1 Flumequin MUSCLE HPLC-fluo 12 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 9 Slaughterhouse Fattening Bovines
B1 Oxolin acid MUSCLE HPLC-fluo 2 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 9 Slaughterhouse Fattening Bovines
B1 Gentamicin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 9 Slaughterhouse Fattening Bovines
B1 Thiamphenicol MUSCLE GC-MS (NCI) 0.1 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 10 Slaughterhouse Fattening Bovines
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 8 Slaughterhouse Fattening Bovines
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 8 Slaughterhouse Fattening Bovines
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 8 Slaughterhouse Fattening Bovines
B1 Amoxycillin Ampicillin Benzathin-Benzylpenicillin Beta-lactamics Penicillins (group) MUSCLE LC-MSMS 1-30 μg/kg Same as screening Same as limit for screening method Various Mrls,according to Counc. Reg. 2377/90/EEC 8 Slaughterhouse Fattening Bovines
B2b Chlopidol Diaveridin Diclazuril Lasalocid Maduramicin Monensin Narasin Nicarbazin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 9 Slaughterhouse Fattening Bovines
B2b Halofuginon LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method MRL 30 µg/kg 9 Slaughterhouse Fattening Bovines
2. PORCINE
B1 Flumequin MUSCLE HPLC-fluo 12 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 61 Slaughterhouse Fattening Pigs
B1 Oxolin acid MUSCLE HPLC-fluo 2 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 61 Slaughterhouse Fattening Pigs
B1 Gentamicin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 25 Slaughterhouse Fattening Pigs
EN 83 EN
B1 Tiamulin MUSCLE HPLC-MSMS 50 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 25 Slaughterhouse Fattening Pigs
B1 Lincomycin MUSCLE GC-MS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 25 Slaughterhouse Fattening Pigs
B1 Erythromycin Erythromycin A MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 25 Slaughterhouse Fattening Pigs
B1 Trimethoprim MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 25 Slaughterhouse Fattening Pigs
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 15 Slaughterhouse Fattening Pigs
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 25 Slaughterhouse Fattening Pigs
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 25 Slaughterhouse Fattening Pigs
B1 Tylosin MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 25 Slaughterhouse Fattening Pigs
B1 Spiramycin MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 250 µg/kg 25 Slaughterhouse Fattening Pigs
B1 Amoxycillin Ampicillin Benzathin-Benzylpenicillin Beta-lactamics Penicillins (group) MUSCLE LC-MSMS 1-30 μg/kg Same as screening Same as limit for screening method Mrls according to Counc. Reg. 2377/90/EEC 25 Slaughterhouse Fattening Pigs
B2a Albendazol Fenbendazol Flubendazol Oxfendazol Thiabendazol MUSCLE HPLC-PDA, HPLC-FLD Various 25-50 μg/kg Same as screening Same as limit for screening method Various Mrls According to Counc. reg. 2377/90/EEC 61 Slaughterhouse Fattening Pigs
B2b Chlopidol Diaveridin Diclazuril Halofuginon Lasalocid Maduramicin Monensin Narasin Nicarbazin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Various Mrls According to Counc. Reg. 2377/90/EEC 61 Slaughterhouse Fattening Pigs
3.SHEEP AND GOATS
EN 84 EN
B1 Flumequin MUSCLE HPLC-fluo 12 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 17 Slaughterhouse Lambs
B1 Flumequin MUSCLE HPLC-fluo 12 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 18 Slaughterhouse Kids
B1 Oxolin acid MUSCLE HPLC-fluo 2 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 17 Slaughterhouse Kids
B1 Oxolin acid MUSCLE HPLC-fluo 2 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 18 Slaughterhouse Lambs
B1 Gentamicin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 2 Slaughterhouse Ewes
B1 Gentamicin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 2 Slaughterhouse Goats
B1 Gentamicin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 3 Slaughterhouse Lambs
B1 Gentamicin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 3 Slaughterhouse Kids
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 2 Slaughterhouse Ewes
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 2 Slaughterhouse Goats
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 3 Slaughterhouse Lambs
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 3 Slaughterhouse Kids
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 2 Slaughterhouse Ewes
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 2 Slaughterhouse Goats
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 3 Slaughterhouse Lambs
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 3 Slaughterhouse Kids
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 2 Slaughterhouse Ewes
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 2 Slaughterhouse Goats
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 3 Slaughterhouse Kids
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 3 Slaughterhouse Lambs
EN 85 EN
B1 Amoxycillin Ampicillin Benzylpenicillin, Penicillin G Beta-lactamics Oxacillin Penicillins (group) MUSCLE LC-MSMS Various 1-30 μg/kg Same as screening Same as limit for screening method Mrls According to Coun. Reg. 2377/90/EEC 2 Slaughterhouse Ewes
B1 Amoxycillin Ampicillin Benzylpenicillin, Penicillin G Beta-lactamics Oxacillin Penicillins (group) MUSCLE LC-MSMS Various 1-30 μg/kg Same as screening Same as limit for screening method Mrls According to Coun. Reg. 2377/90/EEC 2 Slaughterhouse Goats
B1 Amoxycillin Ampicillin Benzylpenicillin, Penicillin G Beta-lactamics Oxacillin Penicillins (group) MUSCLE LC-MSMS Various 1-30 μg/kg Same as screening Same as limit for screening method Mrls According to Coun. Reg. 2377/90/EEC 3 Slaughterhouse Lambs
B1 Amoxycillin Ampicillin Benzylpenicillin, Penicillin G Beta-lactamics Oxacillin Penicillins (group) MUSCLE LC-MSMS Various 1-30 μg/kg Same as screening Same as limit for screening method Mrls According to Coun. Reg. 2377/90/EEC 3 Slaughterhouse Kids
B2a Abamectin (Avermectin B1) Doramectin Eprinomectin Ivermectin Moxidectin LIVER HPLC-fluo 1 µg/kg Same as screening Same as limit for screening method Mrls According to Counc. Reg. 2377/90/EEC 7 Slaughterhouse Ewes
B2a Abamectin (Avermectin B1) Doramectin Eprinomectin Ivermectin Moxidectin LIVER HPLC-fluo 1 µg/kg Same as screening Same as limit for screening method Mrls According to Counc. Reg. 2377/90/EEC 8 Slaughterhouse Goats
B2a Abamectin (Avermectin B1) Doramectin Eprinomectin Ivermectin Moxidectin LIVER HPLC-fluo 1 µg/kg Same as screening Same as limit for screening method Mrls According to Counc. Reg. 2377/90/EEC 10 Slaughterhouse Kids
B2a Abamectin (Avermectin B1) Doramectin Eprinomectin Ivermectin Moxidectin LIVER HPLC-fluo 1 µg/kg Same as screening Same as limit for screening method Mrls According to Counc. Reg. 2377/90/EEC 10 Slaughterhouse Lambs
B2b Chlopidol
EN 86 EN
Diaveridin Diclazuril Halofuginon Lasalocid Maduramicin Monensin Narasin Nicarbazin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 10 Slaughterhouse Kids
B2b Chlopidol Diaveridin Diclazuril Halofuginon Lasalocid Maduramicin Monensin Narasin Nicarbazin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 10 Slaughterhouse Lambs
B2b Chlopidol Diaveridin Diclazuril Halofuginon Lasalocid Maduramicin Monensin Narasin Nicarbazin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 8 Slaughterhouse Goats
B2b Chlopidol Diaveridin Diclazuril Halofuginon Lasalocid Maduramicin Monensin Narasin Nicarbazin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 7 Slaughterhouse Ewes
4. POULTRY
B1 Tiamulin MUSCLE HPLC-MSMS 50 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 25 Slaughterhouse Broiler
B1 Tiamulin MUSCLE HPLC-MSMS 50 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 3 Slaughterhouse Turkey
B1 Tiamulin MUSCLE HPLC-MSMS 50 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 2 Slaughterhouse Ducks
EN 87 EN
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 25 Slaughterhouse Broiler
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 3 Slaughterhouse Turkey
B1 Spectinomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 300 µg/kg 2 Slaughterhouse Ducks
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 25 Slaughterhouse Broiler
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 3 Slaughterhouse Turkey
B1 Lincomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 2 Slaughterhouse Ducks
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 15 Slaughterhouse Broiler
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 3 Slaughterhouse Turkey
B1 Neomycin MUSCLE LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 500 µg/kg 2 Slaughterhouse Ducks
B1 Tylosin Tylosin A MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 25 Slaughterhouse Broiler
B1 Tylosin Tylosin A MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 5 Slaughterhouse Turkey
B1 Tylosin Tylosin A MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 3 Slaughterhouse Ducks
B1 Spiramycin MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 25 Slaughterhouse Broiler
B1 Spiramycin MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 5 Slaughterhouse Turkey
B1 Spiramycin MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 3 Slaughterhouse Ducks
B1 Trimethoprim MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 25 Slaughterhouse Broiler
B1 Trimethoprim MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 5 Slaughterhouse Turkey
B1 Trimethoprim MUSCLE HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 3 Slaughterhouse Ducks
B1 Erythromycin MUSCLE LC-MSMS 50 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 25 Slaughterhouse Broiler
B1 Erythromycin MUSCLE LC-MSMS 50 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 5 Slaughterhouse Turkey
EN 88 EN
B1 Erythromycin MUSCLE LC-MSMS 50 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 3 Slaughterhouse Ducks
B1 Amoxycillin Ampicillin Benzylpenicillin, PenicillinG Beta-lactamics Oxacillin MUSCLE LC-MSMS 1-30 μg/kg Same as screening Same as limit for screening method Various 50-300 μg/kg 25 Slaughterhouse Broiler
B1 Amoxycillin Ampicillin Benzylpenicillin, PenicillinG Beta-lactamics Oxacillin MUSCLE LC-MSMS 1-30 μg/kg Same as screening Same as limit for screening method Various 50-300 μg/kg 5 Slaughterhouse Turkey
B1 Amoxycillin Ampicillin Benzylpenicillin, PenicillinG Beta-lactamics Oxacillin MUSCLE LC-MSMS 1-30 μg/kg Same as screening Same as limit for screening method Various 50-300 μg/kg 3 Slaughterhouse Ducks
B2a Albendazol Febantel Fenbendazol Oxfendazol Thiabendazol MUSCLE HPLC-PDA, HPLC-FLD Various 25-50 μg/kg Same as screening Same as limit for screening method Presence 25 Slaughterhouse Broiler
B2a Albendazol Febantel Fenbendazol Oxfendazol Thiabendazol MUSCLE HPLC-PDA, HPLC-FLD Various 25-50 μg/kg Same as screening Same as limit for screening method Presence 1 Slaughterhouse Turkey
B2a Albendazol Febantel Fenbendazol Oxfendazol Thiabendazol MUSCLE HPLC-PDA, HPLC-FLD Various 25-50 μg/kg Same as screening Same as limit for screening method Presence 1 Slaughterhouse Ducks
B2b Chlopidol Diaveridin Diclazuril Halofuginon Maduramicin Monensin Narasin Nicarbazin Robenidin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 25 Slaughterhouse Broiler
B2b Chlopidol Diaveridin Diclazuril Halofuginon Maduramicin Monensin
EN 89 EN
Narasin Nicarbazin Robenidin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 2 Slaughterhouse Turkey
B2b Chlopidol Diaveridin Diclazuril Halofuginon Maduramicin Monensin Narasin Nicarbazin Robenidin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 2 Slaughterhouse Ducks
5. AQUACULTURE
B1 Amoxycillin Ampicillin Benzathin-Benzylpenicillin Beta-lactamics Oxacillin Penicillins (group) MUSCLE+SKIN (FISH) LC-MSMS 1-30 μg/kg Same as screening Same as limit for screening method Presence 23
B1 Sulfadiazine Sulfadimethoxin Sulfamethoxazol Sulfamethoxypyridazin Sulfathiazol Sulfonamides Sulphadimidine MUSCLE+SKIN (FISH) HPLC-PDA 30 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 24
B1 Chlortetracyclin Oxytetracyclin Tetracyclin MUSCLE+SKIN (FISH) HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method All food producing species 100 μg/kg.
In this category included aquaculture? 23
B1 Enrofloxacin MUSCLE+SKIN (FISH) HPLC-fluo 12 µg/kg Same as screening Same as limit for screening method Presence 23
B1 Doxycyclin MUSCLE+SKIN (FISH) HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method Presence 23
B1 Thiamphenicol MUSCLE+SKIN (FISH) GC-MS (NCI) 0.1 µg/kg Same as screening Same as limit for screening method Presence 23
B2a Fenbendazol Flubendazol Oxfendazol MUSCLE+SKIN (FISH) HPLC-PDA 25 µg/kg Same as screening Same as limit for screening method Presence 23
B2a Albendazol Thiabendazol MUSCLE+SKIN (FISH) HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method Presence 23
EN 90 EN
6. MILK
B1 Doxycyclin MILK (RAW) HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method Presence 14 Cow milk
B1 Doxycyclin MILK (RAW) HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method Presence 4 Goat milk
B1 Doxycyclin MILK (RAW) HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method Presence 4 Sheep milk
B1 Tylosin Tylosin A MILK (RAW) LC-MSMS 25 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 14 Cow milk
B1 Tylosin Tylosin A MILK (RAW) LC-MSMS 25 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 4 Goat milk
B1 Tylosin Tylosin A MILK (RAW) LC-MSMS 25 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 4 Sheep milk
B1 Gentamicin MILK (RAW) LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 14 Cow milk
B1 Gentamicin MILK (RAW) LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 4 Goat milk
B1 Gentamicin MILK (RAW) LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 4 Sheep milk
B1 Erythromycin Erythromycin A MILK (RAW) LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 40 µg/kg 14 Cow milk
B1 Erythromycin Erythromycin A MILK (RAW) LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 40 µg/kg 4 Goat milk
B1 Erythromycin Erythromycin A MILK (RAW) LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 40 µg/kg 4 Sheep milk
B1 Thiamphenicol MILK (RAW) GC-MS (NCI) 0.1 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 14 Cow milk
B1 Thiamphenicol MILK (RAW) GC-MS (NCI) 0.1 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 4 Goat milk
B1 Thiamphenicol MILK (RAW) GC-MS (NCI) 0.1 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 4 Sheep milk
B1 Amoxycillin Ampicillin Benzylpenicillin, Penicillin G MILK (RAW) LC-MSMS 1 µg/kg Same as screening Same as limit for screening method MRL 4 µg/kg 14 Cow milk
B1 Amoxycillin
EN 91 EN
Ampicillin Benzylpenicillin, Penicillin G MILK (RAW) LC-MSMS 1 µg/kg Same as screening Same as limit for screening method MRL 4 µg/kg 4 Goat milk
B1 Amoxycillin Ampicillin Benzylpenicillin, Penicillin G MILK (RAW) LC-MSMS 1 µg/kg Same as screening Same as limit for screening method MRL 4 µg/kg 4 Sheep milk
B1 Sulfachlorpyridazin Sulfadiazine Sulfadimethoxin Sulfadoxin Sulfamethazine Sulfamethoxazol Sulfamethoxypyridazin Sulfathiazol Sulfonamides Sulphadimidine MILK (RAW) HPLC-PDA Various from 12-36 μg/L Same as screening Same as limit for screening method MRL 100 µg/kg 4 Goat milk
B1 Sulfachlorpyridazin Sulfadiazine Sulfadimethoxin Sulfadoxin Sulfamethazine Sulfamethoxazol Sulfamethoxypyridazin Sulfathiazol Sulfonamides Sulphadimidine MILK (RAW) HPLC-PDA Various from 12-36 μg/L Same as screening Same as limit for screening method MRL 100 µg/kg 4 Sheep milk
B2a Eprinomectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method MRL 20 µg/kg 14 Cow milk
B2a Thiabendazol MILK (RAW) HPLC-PDA-FLD 1 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 14 Cow milk
B2a Oxfendazol MILK (RAW) HPLC-PDA-FLD 1 µg/kg Same as screening Same as limit for screening method MRL 10 µg/kg 4 Sheep milk
B2a Oxfendazol MILK (RAW) HPLC-PDA-FLD 1 µg/kg Same as screening Same as limit for screening method MRL 10 µg/kg 4 Goat milk
B2a Eprinomectin MILK (RAW) HPLC-fluo 0.5 µg/kg Same as screening Same as limit for screening method MRL 20 µg/kg 4 Goat milk
B2a Eprinomectin MILK (RAW) HPLC-fluo 0.5 µg/kg Same as screening Same as limit for screening method MRL 20 µg/kg 4 Sheep milk
B2a Thiabendazol MILK (RAW) HPLC-PDA-FLD 1 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 4 Goat milk
B2a Thiabendazol MILK (RAW) HPLC-PDA-FLD 1 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 4 Sheep milk
B2a Albendazol Thiabendazol MILK (RAW) HPLC-PDA-FLD 50 µg/kg Same as screening Same as limit for
EN 92 EN
screening method MRL 100 µg/kg 14 Cow milk
B2a Eprinomectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method MRL 20 µg/kg 4 Goat milk
B2a Eprinomectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method MRL 20 µg/kg 4 Sheep milk
B2a Moxidectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method MRL 40 µg/kg 14 Cow milk
B2a Moxidectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method MRL 40 µg/kg 4 Goat milk
B2a Moxidectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method MRL 40 µg/kg 4 Sheep milk
B2a Doramectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method Presence 14 Cow milk
B2a Doramectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method Presence 4 Goat milk
B2a Doramectin MILK (RAW) HPLC-fluo 5 µg/kg Same as screening Same as limit for screening method Presence 4 Sheep milk
B2a Abamectin (Avermectin B1) Ivermectin MILK (RAW) HPLC-fluo 7 µg/kg Same as screening Same as limit for screening method Presence 14 Cow milk
B2a Abamectin (Avermectin B1) Ivermectin MILK (RAW) HPLC-fluo 7 µg/kg Same as screening Same as limit for screening method Presence 4 Goat milk
B2a Abamectin (Avermectin B1) Ivermectin MILK (RAW) HPLC-fluo 7 µg/kg Same as screening Same as limit for screening method Presence 4 Sheep milk
B2a Albendazol Thiabendazol MILK (RAW) HPLC-PDA-FLD 50 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 4 Goat milk
B2a Albendazol Thiabendazol MILK (RAW) HPLC-PDA-FLD 50 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 4 Sheep milk
7. RABBITS
B1 Doxycyclin KIDNEY HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method Presence 10 Rabbits
B1 Oxolin acid MUSCLE HPLC-fluo 2 µg/kg Same as screening 100 µg/kg MRL 200 µg/kg 10 Rabbits
B1 Trimethoprim MUSCLE HPLC-PDA 10 µg/kg Same as screening Same as limit for screening method MRL 50 µg/kg 10 Rabbits
EN 93 EN
B2a Albendazol Thiabendazol MUSCLE HPLC-PDA, HPLC-FLD 50 µg/kg Same as screeningSame as limit for screening method Presence 6 Rabbits
B2a Fenbendazol Flubendazol Oxfendazol MUSCLE HPLC-PDA, HPLC-FLD 25 µg/kg Same as screeningSame as limit for screening method Presence 6 Rabbits
B2b Chlopidol Diaveridin Diclazuril Halofuginon Maduramicin Monensin Narasin Nicarbazin Robenidin Salinomycin Toltrazuril LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 6 Rabbits
B2b Chlopidol Diaveridin Diclazuril Halofuginon Maduramicin Monensin Narasin Nicarbazin Robenidin Salinomycin Toltrazuril FEED+WATER LC-MSMS 3 µg/kg Same as screening Same as limit for screening method Presence 6 Rabbits
8. FARMED WILD GAME
B1 Chlortetracyclin Doxycyclin Oxytetracyclin Tetracyclines KIDNEY HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method MRL 600 µg/kg 10 Slaughterhouse Quail
B1 Sulfadiazine Sulfadimethoxin Sulfamethoxypyridazin Sulfathiazol Sulfonamides Sulphadimidine Trimethoprim MUSCLE HPLC-PDA 30 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 10 Slaughterhouse Quail
B1 Chlortetracyclin Doxycyclin
EN 94 EN
Oxytetracyclin Tetracyclines KIDNEY HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method MRL 600 µg/kg 10 Slaughterhouse Ostriches
B1 Sulfadiazine Sulfadimethoxin Sulfamethoxypyridazin Sulfathiazol Sulfonamides Sulphadimidine Trimethoprim MUSCLE HPLC-PDA 30 µg/kg Same as screening Same as limit for screening method MRL 100 µg/kg 10 Slaughterhouse Ostriches
B2b Chlopidol Diaveridin Diclazuril Halofuginon Lasalocid Maduramicin Monensin Narasin Nicarbazin Robenidin Salinomycin LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 10 Slaughterhouse Quail
B2b Chlopidol Diaveridin Diclazuril Halofuginon Lasalocid Maduramicin Monensin Narasin Nicarbazin Robenidin Salinomycin LIVER LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 10 Slaughterhouse Ostriches
9. HEN EGGS
B1 Flumequin EGGS HPLC 10 µg/kg Same as screening Same as limit for screening method Presence 10 Hen
B1 Doxycyclin EGGS HPLC-PDA 50 µg/kg Same as screening Same as limit for screening method Presence 10 Hen
B1 Tylosin Tylosin A EGGS LC-MSMS 100 µg/kg Same as screening Same as limit for screening method MRL 200 µg/kg 10 Hen
B1 Spiramycin EGGS LC-MS 20 µg/kg Same as screening Same as limit for screening method Presence 10 Hen
B1 Framycetin Neomycin EGGS LC-MSMS 10 µg/kg Same as screening Same as limit for screening method
EN 95 EN
MRL 500 µg/kg 10 Hen
B1 Amoxycillin Ampicillin Benzylpenicillin, PenicillinG Beta-lactamics Oxacillin EGGS LC-MSMS 1-30 μg/kg Same as screening Same as limit for screening method Presence 10 Hen
B1 Erythromycin Erythromycin A EGGS LC-MSMS 10 µg/kg Same as screening Same as limit for screening method MRL 150 µg/kg 10 Hen
B1 Trimethoprim EGGS HPLC-DAD 10 µg/kg Same as screening Same as limit for screening method Presence 10 Hen
B2b Chlopidol Diaveridin Diclazuril Halofuginon Lasalocid Maduramicin Monensin Narasin Nicarbazin Robenidin Salinomycin Toltrazuril EGGS LC-MSMS 2 µg/kg Same as screening Same as limit for screening method Presence 10 Hen
10. HONEY
B1 Fumagillin HONEY LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 13 Honey
B1 Dihydrostreptomycin Streptomycin HONEY LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 13 Honey
B1 Sulfadiazine Sulfadimethoxin Sulfamethoxazol Sulfamethoxypyridazin Sulfathiazol Sulfonamides Sulphadimidine Trimethoprim HONEY HPLC-fluo 30 µg/kg Same as screening Same as limit for screening method Presence 15 Honey
B1 Chlortetracyclin Doxycyclin Oxytetracyclin Tetracyclin Tetracyclines HONEY LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 15 Honey
B1 Erythromycin HONEY LC-MSMS 10 µg/kg Same as screening Same as limit for screening method Presence 5 Honey
EN 96 EN
B3d Ochratoxin A HONEY HPLC-fluo 0.2- 0.5 μg/kg Same as screening Same as limit for screening method Presence 11 Honey
B3d Aflatoxin B1 HONEY HPLC-fluo 0.2- 0.5 μg/kg Same as screening Same as limit for screening method Presence 11 Honey
NON-COMPLIANT RESULTS
Non-compliant results Follow-up actions Bovines • B1.Antibiotics/Chemotherapeu • Bovine farms tics
• Sulphonamides • Bovine/Fattening–Feedingstuffs (Two bovine farms) 1. Sulphadiazine – LCMSMS- • 1. (CY B 4127002) Níkos Nikolaou, Aglisides - 87 μg/kg -feeding stuffs and Larnaca Sulphamethazine – LCMSMS- • Investigation in the farm of origin √ 94 μg/kg -feeding stuffs • Verification of records √ • Additional sampling √
• Animals held in the farm (60 young bovines / 67 lactating cows ) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE)
• Administrative measures (NONE) • Others
• 2. (CY B 51279001) Charis Farm Ltd, Pareklisia, Limassol • Investigation in the farm of origin √ 2. Sulphamethazine – • Verification of records √ LCMSMS-60 μg/kg -feeding • Additional sampling √ stuffs • Animals held in the farm (310 young bovines / 270 lactating cows ) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human
EN 97 EN
consumption (NONE) • Administrative measures (NONE) • Others
Pigs • B1.Antibiotics/Chemotherapeu • B1. Antibiotics/Chemotherapeutics tics • Porcine/ Fattening pigs (One porcine farm) • Porcine/ Fattening pigs (One 1. (CY 107) Atalianis bros Ltd, Akaki- porcine farm) Nicosia Four plate test • Investigation in the farm of origin √ • Verification of records √
• Additional sampling √ • Animals held in the farm (2140 fattening pigs / 390 sows) • Intensified checks on the animals and products
from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (21 pigs carcasses confiscated
and destroyed) • Administrative measures (NONE) • Others
• Sulphonamides • Porcine/ Fattening pigs (Two porcine farm)
• Sulphonamides • 1. (CY 426) Savvas Agapiou , Aradippou • Porcine/ Fattening pigs (Two Larnaca porcine farms) • Investigation in the farm of origin √ • 1.Sulphadimidine-HPLC-DAD- 128 μg/kg-muscle • Verification of records √ • Additional sampling √
• Animals held in the farm (4800 fattening pigs) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √
• Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• 2. (CY 446) Auxentiou bros Ltd, Maroni - Larnaca
EN 98 EN
• Investigation in the farm of origin √ • Verification of records √
• Additional sampling √ • Animals held in the farm (1370 fattening pigs / • 2. Sulphadimidine-HPLC- 547 sows) DAD-133 μg/kg-muscle • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• Feeding stuffs • Porcine farms
• 1. (CY 413) Pagonis brothers ltd, Aradippou Larnaca Sulphonamides Investigation in the farm of origin • Porcine/ Fattening pigs – • √ Feeding stuffs (Four porcine • Verification of records √ farms) • Additional sampling √ • Animals held in the farm (1960 fattening pigs /
415 sows ) • Intensified checks on the animals and products 1. Sulphadiazine– LCMSMS- from the farm / establishment in the event of 360 μg/kg -feeding stuffs repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE)
• Administrative measures (NONE) • Others
• 2. (CY 414) Sikkis brothers ltd, Aradippou Larnaca
• Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (1390 fattening pigs / 190 sows) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √
EN 99 EN
2. Sulphadiazine –LCMSMS- • Carcasses and products declare unfit for human 310 μg/kg -feeding stuffs consumption (NONE) • Administrative measures (NONE) • Others
• 3. (CY 415) N. Markou, Aradippou Larnaca • Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (2940 fattening pigs / 824 sows ) • Intensified checks on the animals and products from the farm / establishment in the event of
repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE)
• Others 3. Sulphadiazine –LCMSMS- 280 μg/kg -feeding stuffs • 4. (CY 405) Andreas Kkailas ans sons Ltd, Athienou Larnaca • Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (1400 fattening pigs /
770 sows) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √
• Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
4. Sulphadiazine –LCMSMS- 80 μg/kg -feeding stuffs • B3d Mycotoxins • Ochratoxin A • Feeding stuffs • Porcine farm
• 1. (CY 102) Marinos Chrisostomou, Agia Marina Xyliatou - Nicosia
• Investigation in the farm of origin √ • Verification of records √ • Additional sampling √
EN 100 EN
• Animals held in the farm (1300 fattening pigs) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • B3d Mycotoxins- Ochratoxin • Others A • Feeding stuffs Porcine/ Fattening pigs (One porcine farm)
1. Ochratoxin A- HPLC-FLD- 3 μg/kg- feeding stuffs
Poultry • Poultry/Broilers • Poultry/Broilers B2a Coccidiostats B2a Coccidiostats • Nicarbazin (One broilers farm) • Nicarbazin (One broilers farm)
1. Nicarbazin- HPLC-PDA-22.4 1. Epauli Giorkis Kouzalis Ltd, Paralimni- mg/kg –broilers liver Ammochostos 1.Investigation in the farm of origin √ 2. Verification of records √
3. Additional sampling √ 4. Animals held in the farm (30000 broilers) 5. Intensified checks on the animals and products from the farm / establishment in
the event of repeated infringements √ 6. Carcasses and products declare unfit for human consumption (NONE) 7. Administrative measures (YES) 8. Others
• Diclazuril (8 broilers farms) • 1. Epauli Giorkis Kouzalis Ltd, Paralimni-
Ammochostos • Diclazuril (8 broiler farms) Investigation in the farm of origin √ • 1. Diclazuril- LCMSMS- 17 • μg/kg- broilers muscle, • Verification of records √ Diclazuril- LCMSMS- 35 • Additional sampling √ μg/kg- broilers muscle • Animals held in the farm (30000 broilers) • Intensified checks on the animals and products from the farm / establishment in the event of
EN 101 EN
repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• 2. Renos Hadjioannou Ltd , Nicosia
• Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (35000 broilers)
• 2. Diclazuril- LCMSMS- 3 • Intensified checks on the animals and products μg/kg- broilers muscle from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE)
• Others
• 3. Marios Sergiou, Kophinou – Larnaca • Investigation in the farm of origin √ • Verification of records √ • Additional sampling √
• Animals held in the farm (2500 broilers) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √
• Carcasses and products declare unfit for human • 3. Diclazuril- LCMSMS- 3 consumption (NONE) μg/kg- broilers muscle • Administrative measures (NONE) • Others
• 4. Georgios Georgiou, Monagrouli – Limassol • Investigation in the farm of origin √ • Verification of records √
• Additional sampling √ • Animals held in the farm (20000 broilers) • Intensified checks on the animals and products from the farm / establishment in the event of
repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • 4. Diclazuril- LCMSMS- 6 • Administrative measures (NONE) μg/kg- broilers muscle • Others
EN 102 EN
• 5. Savvas Alexandrou, Agios Georgios Kaukalou – Nicosia • Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (3000 broilers)
• Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human
consumption (NONE) • Administrative measures (NONE) • Others • 5. Diclazuril- LCMSMS- 12 μg/kg- broilers muscle • 6. Karaoli bros Ltd, Tseri – Nicosia • Investigation in the farm of origin √ • Verification of records √ • Additional sampling √
• Animals held in the farm (13000 broilers) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √
• Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• 7. Loucas Loucaides, Agia Marinouda – Paphos • Investigation in the farm of origin √ • 6. Diclazuril- LCMSMS- 3 • Verification of records √ μg/kg- broilers muscle • Additional sampling √ • Animals held in the farm (8000 broilers) • Intensified checks on the animals and products from the farm / establishment in the event of
repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• 8. Costas Constantinou, Monagrouli, - Limassol • Investigation in the farm of origin √
EN 103 EN
• Verification of records √ • 7. Diclazuril- LCMSMS- 13 • Additional sampling √ μg/kg- broilers muscle, • Animals held in the farm (8000 broilers) Diclazuril- LCMSMS- 7 μg/kg- • Intensified checks on the animals and products broilers muscle from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• Maduramycin • Ducks (One farm) • 1. Comet Farm Ltd, Nicosia • Investigation in the farm of origin √ • Verification of records √
• Additional sampling √ • Animals held in the farm (9171 ducks) • 8. Diclazuril- LCMSMS- 11 • Intensified checks on the animals and products μg/kg- broilers muscle, from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
Lasalocid (One broiler farm) • 1. Stelios Zampas, Peristerona, - Nicosia
• Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (7000 broilers) • Intensified checks on the animals and products from the farm / establishment in the event of • Maduramycin repeated infringements √ • Poultry /Duck (One farm) • Carcasses and products declare unfit for human • 1. Maduramycin- LCMSMS- consumption (NONE) 120 μg/kg- ducks muscle • Administrative measures (NONE) • Others
B3c Chemical elements (Heavy metals)
EN 104 EN
• Lead (Pb) • Poultry/Broilers (One farm)
• Christakis Christoforou, Kinousa - Paphos • Investigation in the farm of origin √ • Verification of records √ Lasalocid (One broiler farm) • Additional sampling √ • 1. Lasalocid- LCMSMS- 36 • Animals held in the farm (2500 broilers) μg/kg- broilers muscle • Intensified checks on the animals and products from the farm / establishment in the event of
repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
B3c Chemical elements – Heavy metals • Lead (Pb) • Poultry/Broilers (1 broilers farm)
1. Lead- ASS- 0.22 mg/kg- broilers muscle
Sheep and goat None None
Horses None None
EN 105 EN
Milk None None
Eggs • B2a Coccidiostats • B2a Coccidiostats • Lasalocid • Lasalocid • Eggs (2 laying hens (egg) farms) • Laying hens (eggs) (Two farms) • 1. Lasalocid- LCMSMS-9 • 1. Comitis Farm Ltd, Agious Trimithias, Nicosia μg/kg-eggs • Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (40000 laying hens ) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• 2. P. Homatenos and sons ltd, Athienou – Larnaca • Investigation in the farm of origin √ • 2. Lasalocid- LCMSMS-3 • Verification of records √ μg/kg-eggs • Additional sampling √ • Animals held in the farm (9000 laying hens ) • Intensified checks on the animals and products
from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
Rabbit None None
Aquaculture None None
EN 106 EN
Farmed game None None
Wild game None None
Honey • B1.Antibiotics/Chemotherapeuti • B1.Antibiotics/Chemotherapeutics cs Sulphonamides • Sulphonamides • Bees / Honey (5 beekeepers) • Bees / Honey (5 beekeepers)
• 1. George Euthimiou, Tremithousa – Paphos • 1. Sulphaclozin- LCMSMS - 85 μg/kg- Honey • Investigation in the farm of origin √ • Verification of records √
• Additional sampling √ • Animals held in the farm (110 beehives) • Intensified checks on the animals and products from the farm / establishment in the event of
repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• 2. Giannakis Americanos- Dromolaxia- Larnaca • Investigation in the farm of origin √ 2. Sulphadiazine- LCMSMS - • Verification of records √ 13 μg/kg- Honey • Additional sampling √ • Animals held in the farm (450 beehives) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• 3. Gianakis Ioannou Ghristofi -Kaimakli- Nicosia
EN 107 EN
• Investigation in the farm of origin √ • Verification of records √
3. Sulphadimidine-LCMSMS • Additional sampling √ - 56 μg/kg- Honey • Animals held in the farm (350 beehives) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• 4. Panicos Leandrou, Pachna – Limassol • Investigation in the farm of origin √
• Verification of records √ • Additional sampling √ • Animals held in the farm (1000 beehives) 4. Sulphadimidine- • Intensified checks on the animals and products HPLC/MS/MS - 11 μg/kg- from the farm / establishment in the event of Honey repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE)
• Administrative measures (NONE) • Others
• 5. Andreas Hatjigerasimou, Kakopetria – Nicosia
• (Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (65 beehives) • Intensified checks on the animals and products from the farm / establishment in the event of 5. Sulphadimidine- repeated infringements √ HPLC/MS/MS -7 μg/kg- • Carcasses and products declare unfit for human Honey consumption (NONE) • Administrative measures (NONE) • Others
EN 108 EN
Tetracycline’s
• Panicos Leandrou, Pachna – Limassol • Investigation in the farm of origin √ • Verification of records √ • Additional sampling √
• Animals held in the farm (1000 beehives) • Intensified checks on the animals and products from the farm / establishment in the event of • Tetracycline’s repeated infringements √ • Bees / Honey (2 beekeepers) • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) 1. Tetracycline- LCMSMS- • Others 12 μg/kg- Honey
• Anastasios Glaukou, Marathounta – Paphos • Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (305 beehives) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
• B3c Chemical elements –Heavy metals 2. Oxytetracycline- LCMSMS- 17 μg/kg- • Lead (Pb) Honey • Bees /Honey
• 1. Christos Petrinas, Aradipou-Larnaca
• Investigation in the farm of origin √ • Verification of records √ • Additional sampling √ • Animals held in the farm (1050 beehives) • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √
EN 109 EN
• Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others • B3c Chemical elements – Heavy metals • 2. Tasos Christofides, Mesogi – Paphos • Lead (Pb) 1. Investigation in the farm of origin √ • Bees / Honey (2 beekeepers) 2. Verification of records √
• 3. Additional sampling √ 1. Lead- ICP- 0.032 mg/kg- 4. Animals held in the farm (187 beehives) honey 5. Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements √ 6. Carcasses and products declare unfit for human consumption (NONE) 7. Administrative measures (NONE) 8. Others
2. Lead- ICP- 0.017 mg/kg- honey
IMPORTS
EN 110 EN
NON-COMPLIANT RESULTS
Non-compliant results Follow-up actions Bovines • B1.Antibiotics/Chemotherapeu • Imported Bovine tender loin for the Cyprus tics National Guard needs. • Tetracyclines • Exporter country: ITALY • National Guard- Nicosia • Bovine, Tender loin • Importer: Michalis Papaeustathiou ltd., Nicosia 1. Oxytetracycline – HPLC- • Investigation in the farm of origin Not apply PDA - 9610 μg/kg - muscle • Verification of records √ • Additional sampling √
• Imported quantity: 13000 kg • Confiscated quantity: 40 kg • Intensified checks on the animals and products from the farm / establishment in the event of repeated infringements Not apply • Carcasses and products declare unfit for human
consumption (40 kg) • Administrative measures (Against the court. Still pending)
• Others
IMPORTS NON-COMPLIANT RESULTS
Non-compliant results Follow-up actions Aquaculture • B1.Antibiotics/Chemotherapeu • Imported Frozen Surimi products (Imitation crab tics sticks) • Antimicrobials • Exported country: CHINA • Domestic consumption • Frozen Surimi products (Imitation crab sticks) • Importer: G.D.L Trading Ltd., CY R 20, Dafnis str, Limassol. • 1. Antimicrobials – Screening • Investigation in the farm of origin Not apply test - PREMI test- Imitation crab • Verification of records √ sticks • Additional sampling √ • Imported quantity: 12000 kg • Confiscated and destroyed quantity: 8842 kg • Intensified checks on the animals and products from the farm / establishment in the event of repeated
EN 111 EN
infringements Not apply
• Carcasses and products declare unfit for human consumption (8842 kg) • Administrative measures (NONE)
• Others
IMPORTS NON-COMPLIANT RESULTS
Non-compliant results Follow-up actions Honey • B1.Antibiotics/Chemotherapeu • Imported Packaged Honey tics • Exported country: GREECE • Antimicrobials • Domestic consumption • Packaged Honey • Importer: C.T.C Public Ltd, Argosy Operations, Industrial Area, Nissou, Nicosia • Number of samples checked: 3 (Three) • Investigation in the farm of origin Not apply
• 1. Sulphadimidine-HPLC-FLD • Verification of records √ • Additional sampling √ – 24,9 μg/kg- Honey • Imported quantity: 3996 kg 2. Sulphadimidine-HPLC-FLD • • Confiscated and destroyed quantity: NONE – 25.6 μg/kg- Honey • Intensified checks on the animals and products from • 3. Sulphadimidine-HPLC-FLD the farm / establishment in the event of repeated – 32,3 μg/kg- Honey infringements Not apply • Carcasses and products declare unfit for human consumption (NONE) • Administrative measures (NONE) • Others
EN 112 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State THE CZECH REPUBLIC
Date 29 May 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances The increase in total number of CAP tests within the national monitoring plan. A dedicated control action for CAP will be performed. Instruction to veterinary inspectors –pay due attention to the correct sampling from pigs, exclude cryptorchids, recently castrated animals and animals under stress (19- nortestosteron).
Non-compliant results Follow-up actions Chloramphenicol (CAP) – 0,54 ppb Other actions: Investigations were carried out on – muscle – chicken broiler the farm, at the veterinary practitioner and at the supplier of feeds; samples of feed and water and
additional samples of chicken were taken (3 slaughtering batches – 10 chicken per each) – CAP has not been found Chloramphenicol (CAP) – 0,39 ppb – muscle – chicken broiler Other actions: Investigations were carried out on the farm, at the veterinary practitioner and at the supplier of feeds; samples of feed and water and additional samples of chickens were taken (3 slaughtering batches – 10 chickens per each) – CAP has not been found Chloramphenicol (CAP) – 0,3 ppb – urine - cow Other actions: Investigations were carried out on the farm and at the veterinary practitioner; samples of urine from three additional cows and from the positive animal were taken – CAP has not been found; samples of milk, feed and water Choramphenicol (CAP) – 0,9 ppb – were taken – CAP has not been found muscle – laying hen
Other actions: Investigations were carried out on
the farm, at the veterinary practitioner and at the
EN 113 EN
supplier of feeds; samples of feed, water and Chloramphenikol (CAP) – 1,4 ppb – other hens were taken - CAP has not been found muscle - pig
Other actions: Investigations were carried out on
the farm, at the veterinary practitioner; samples of Chloramphenicol (CAP) – 3,1 ppb – muscle, urine and feed and water were taken – muscle - laying hen CAP has not been found
Other actions: Investigations were carried out on the farm (129,050 laying hens), at the feed supplier and at the veterinary practitioner; repeated investigations confirmed CAP in the muscle of the hens, no CAP has been found in eggs; extraordinary veterinary measures were imposed (ban on slaughtering and movement of animals); CAP origin – probably fish meal processed in the feed; at the time when
investigation was carried out, the fish meal was no Chloramphenicol (CAP) – 0,5 ppb – longer available; the farm is under targeted urine - young bovine (heifer) in the veterinary surveillance for the period of 1 year ; farm repeated testing of laying hens and eggs are carried out at the expenses of the farm owner (126 samples in total).
Chloramphenicol (CAP) – 0,65 ppb – urine - cow Other actions: Investigations were carried out on the farm and at the veterinary practitioner; samples of urine from 3 animals were taken – CAP has not been found. Origin of CAP has not been identified.
19-nortestosteron – 1,1 ppb – urine - pig Other actions: Investigations were carried out on the farm and at the veterinary practitioner; samples of milk, feed, water and urine from 3 animals were taken – CAP has not been found; repeated sampling of urine from the positive cow 19-nortestosteron – 1,4 ppb – urine – CAP has not been found. Origin of the CAP has – pig not been identified.
Other actions: Investigation was carried out on the farm; samples of urine from three additional pigs were taken for the targeted testing – these were compliant. Probably, sample was taken from an 19-nortestosteron – 1,0 ppb – urine cryptorchid animal in error. – pig
Other actions: : Investigation was carried out on
EN 114 EN
the farm; samples of urine from three additional
pigs were taken for the targeted testing – these 19-nortestosteron – 3,4 ppb – urine were compliant. Until the testing was been – pig completed ban on movement of the animals (200 heads) had been imposed. Probably, sample was taken from an cryptorchid animal in error.
Other actions: Investigation was carried out on the farm; samples of urine from three additional pigs were taken for the targeted testing – these were compliant. Until the testing was been completed 19-nortestosteron – 22,7 ppb – urine ban on movement of the animals (200 heads) had – pig been imposed. Probably, sample was taken from an cryptorchid animal in error. Other actions: Investigation was carried out on the farm; samples of urine from three additional pigs 19-nortestosteron – 38,0 ppb – urine were taken for the targeted testing – these were – pig compliant. Until the testing was been completed ban on movement of the animals (200 heads) had been imposed. Probably, sample was taken from an cryptorchid animal in error.
19-nortestosteron – 81,0 ppb – urine – pig Other actions: Investigation was carried out on the farm; samples of urine from three additional pigs were taken for the targeted testing – these were compliant. Until the testing was been completed ban on movement of the animals (200 heads) had been imposed. Probably, sample was taken from an cryptorchid animal in error. Other actions: Investigation was carried out on the farm; samples of urine from two additional pigs were taken for the targeted testing – these were compliant. Until the testing was been completed ban on movement of the animals (200 heads) had been imposed. Probably, sample was taken from an cryptorchid animal in error.
Other actions: Investigation was carried out on the farm; samples of urine from three additional pigs were taken for the targeted testing – these were compliant. Until the testing was been completed ban on movement of the animals (200 heads) had been imposed. Probably, sample was taken from an cryptorchid animal in error. Aggregate: CAP - poultry - 4x non-compliant 145 additional samples (18 non-compliant),
EN 115 EN
extraordinary veterinary measures were imposed
CAP - bovine animals - 3x non- compliant 20 additional samples (all compliant) CAP - pig - 1x non-compliant 4 additional samples (all compliant) 19-nortestosteron - pigs - 7x non- 20 additional samples (all compliant) compliant * Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 116 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances Malachite green (MG/LMG) more stringent inspections at the trout farms, increase in numbers of trout tested in frame of monitoring programme, a dedicated action for control of residues of MG/LMG will be performed Non-compliant results Follow-up actions Bovines PCB´s - 1x - muscle (cow) 14 additional samples (all compliant); Cadmium (Cd) - 8x - kidney (cow) 75 additional samples (13 non-compliant); testing of kidney of each slaughtered animal has been
imposed at the farm with the most frequent occurrence of non-compliant samples Tilmicosin - 1x - kidney (calf) 1 additional sample (compliant) Pigs PCB´s - 1x - muscle 13 additional samples (7 in the farm, 6 in the Doxycycline - 1x (muscle and liver) slaughterhouse – all compliant) 8 additional samples (2 in the farm, 6 in the
slaughterhouse -all compliant) Cadmium (Cd)- 1x (kidney) l additional sample (compliant)
Poultry Nicarbazin - 2x (liver) 12 additional samples (8 in the farm, 4 in the slaughterhouse – all compliant) Sheep and goat & @ Horses & @ Milk & @ Eggs Nicarbazin - 1x (quail eggs) 11 additional samples (4 non-compliant); eggs was declared unfit for human consumption (31 671 eggs). Rabbit
EN 117 EN
Nicarbazin - 1x (muscle) 3 additional samples (all compliant) Aquaculture Cadmium (Cd) - 1x (carp) 1 additional sample (compliant) Malachite green (MG) - 9x (trout) 10 additional samples of trout (3 non-compliant) Investigations in the farms of origin - 23 samples (4 non-compliant), other 7 additional samples (2 non-compliant). Majority of the positive samples originated from the early stages (young fish). Bans on movement of animals were imposed (extraordinary veterinary measures), and testing of samples at the farmers´ costs was ordered. If the fish at the time of their marketing maturity was free from the MG residues, they were allowed to be put on the market, in the other cases, the fish were seized (4470 kg); financial penalties were laid on. Farmed game & @
Wild game & @
Honey & @
EN 118 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State DENMARK Date 9 April 2006
Group A substances
Modification of national residue Aggregate for all animal products and substances plan A3: Nandrolone, number of samples in slaughtered porcine animals were not increased since further investigations of 5 samples on each farm of origin did not confirm non- compliance. A6: Metronidazol, number of samples in aquaculture were not increased since they already comprise more than 60 % of the required number of samples in group A for farm trout. Non-compliant results Follow-up actions 17-beta-19-Nortestosterone – 82 In each of the 3 cases of Nandrolone found in µg/kg – urine – castrated pig porcine
17-beta-19-Nortestosterone – presence – urine – castrated pig animals, 5 additional samples were taken from the
17-beta-19-Nortestosterone – 2 µg/kg – urine – porcine sow same holding. All results were negative.
Metronidazol – 7 µg/kg – muscle – farm trout Investigations in the farm of origin were carried out in terms of 84 suspicion samples. Metronidazol was found in 31 samples in concentrations ranging from 0,6 to 872 µg/kg. Trout were held on farm during analysis. Herds with one or more non-compliant result were destroyed. Slaughtered trout were also held back and later destroyed. Intensified sampling in related farms led to negative results. The police is informed and is preparing a court case aiming at a fine.
EN 119 EN
* Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
Group B substances
Modification of national residue Aggregate for all animal products and substances plan B1: Antibiotics, only found in porcine sows (except for 1 cow). Number of samples of sows were not increased since they were already many times greater than required and furthermore the frequency of non-compliant results were decreased compared to 2004. B2b: Anticoccidials, number of samples of eggs were not increased since only one of 140 samples contained more than 10 µg/kg of Salinomycin. B3c: Pb, Hg + Cd, only found in wild game, except for 1 cow. The number of samples were not increased since they were already relatively large. B3e: Malachite green, number of samples were not increased since it was already much larger than required.
Non-compliant results Follow-up actions Bovines 1 Oxytetracycline – kidney Verification of medicine records on farm, no administrative measures nor information of the
police
1 Cadmium - kidney 2 additional samples were taken from the same holding as soon as possible. Another 2 samples were taken from another holding, where the content in one animal was compliant but close to the limit. All 4 results were negative.
Pigs 2 Benzylpenicillin in sow muscles 1 sow muscle: Verification of medicine records, information of police, fine accepted by owner. 1 sow muscle: Follow up was too late – the ownership had been changed to a new person
EN 120 EN
9 suspect samples from one holding due to 1 Oxytetracycline – Muscle from suspicion based on local information, pigs On Farm administrative measures.
1 Amoxicillin – sow kidney Verification of records on farm, information of police, fine accepted by owner
1 sow: Verification of records on farm, 2 Benzylpenicillin in sow kidneys information of police, fine accepted by owner. 1 sow: No follow-up action in the file.
No follow-up action in the file. 1 Oxytetracycline – sow kidney
Poultry & @
Sheep and goat & @
Horses & @
Milk 40 Lincomycin / tetracycline / 47 suspect samples taken during one visit to a oxytetracycline / Penicillin G / dairy farm in order to verify a suspicion based on Cloxacillin / Streptomycin / local information. The information on the 40 Dihydrostreptomycin / positive results are given to the police.
17 Streptomycin / 26 suspect samples from one dairy farm represent Dihydrostreptomycin / Penicillin G / one case due to suspicion based on local information, information of police. Nafcillin / Oxytetracyclin
Eggs Our provisional experiences suggest that good omycin - eggs manufacturing practice enables the reduction of
EN 121 EN
contaminating ionophoric coccidiostats to a level less than 10 µg/kg for each of the substances salinomycin, monensin and narasin. 1 sample containing more than 10 µg/kg of salinomycin led to information of the Plant Directorate
Rabbit & @
Aquaculture Verification of medicine records on farm and chite green – trout muscle visual observation of presence of medicine on farm, animals held back in the farm, no administrative measures nor information of police since it was not possible to prove that trout were treated by the present owner.
Farmed game & @ Wild game The problem is now solved in deer. In 2006 the Meat of 1 wild duck + 15 pheasants same approach will be applied on feathered game: Suppliers must guarantee pollution-free habitats Meat of wild duck and ammunition. Visual inspection of random samples of game regarding used ammunition is also introduced. Honey & @
EN 122 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State ESTONIA Date 16 June 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
Non-compliant results Follow-up actions CAP – 10,6 ppm - muscle - young The farm of origin was investigated immediately bovine but the origin of CAP was not identified; it was impossible to take additional samples, because the owner of the animal has recently finished the animal breeding. CAP – 0,11 ppm – muscle – young The farm of origin was investigated immediately bovine but the origin of CAP was not identified; additional samples from milk were taken with negative results. β-nor-testosterone – 5,5 ppm – The farm of origin was investigated immediately urine – fattening pig and the final identified reason was that the animal where from the sample was taken was chrypthorhid; also 2 additional samples were taken from urine with negative results. Zeranole – 0,211 ppm; Taleranole – The farm of origin was investigated immediately, 0,547 ppm;Zearalenone – 0,724 the use of zeranole or other substances were not ppm – F2 mycotoxine; α-zearaleole identified; 2 samples were taken from animal feed 1,864 ppm; β-zearaleole were with 1 positive sample for F2 mycotoxine. detected form – urine – bovine Additional sample from the same animal was animal from farm taken with negative result. * Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 123 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances Non-compliant results Follow-up actions Bovines F2-mycotoxine – urine – young The farm of origin was investigated immediately, bovine the use of zeranole or other substances was not identified; 3 samples were taken from animal feed
with positive sample. Pigs - - Poultry - - Sheep and goat - - Horses - - Milk Microbiological screening – The farm of origin was investigated immediately; positive result – for further additional sample from raw milk was taken with examination with LC-MS/MS - negative result. The farm was allocated to Penicillin G – 18,7 ppm intensified checks. Eggs - - Rabbit - - Aquaculture - - Farmed game - - Wild game & @ Honey - -
EN 124 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State FINLAND
Date 30 June 2006
Group A substances
Modification of national residue Aggregate for all animal products and substances plan
Modifications 2005 Æ 2006
A2 Thiouracil is added to the group of thyreostats for bovine, pigs, sheep and farmed game
A5 The confirmation of beta-agonists is made using LC-MS insteadt GC-MS, also for the screenig of liver samplse is made using LC-MS
A6 The screenig and confirmation of chloramphenicol is made using LC-MS.
Non-compliant results Follow-up actions
There were no non-complinat -- results in 2005 in group A substances.
EN 125 EN
Group B substances
Modification of national residue Aggregate for all animal products and substances plan
Modifications 2005 Æ 2006 - The number of microbiological test is redused from 700 to 50 for bovine and from 4000 to 250 for pigs. The chemical analysis for antimicrobials is increased and the range of sulfonamides has been enlarged up to 10. - The number of tetracyclines in honey is addded from 20 to 30 due to positive findings. - The number of fattenig pig samples intended for mycotoxin analysis is increased (25 Æ 40) due to positive findings. - Nicarbazin for poultry and eggs is added to the plan - Dexamethason and phenylbutazon for milk are added to the plan. - The number of farmed game samples will be at the same level as 2005 (even there were positive reindeer liver and kidney) - The number of wild game samples will be at the same level as 2005 (even there were positive elks liver and kidney) - Some changes are also made do to changes in production numbers.
Non-compliant results Follow-up actions
Bovines
No positive --
Pigs
One liver sample of sow was @ List actions: positive for ivermectin (38 µg/kg). According to the investigations on the farm the sow has been medicated by the owner itself with ivermectin containing product 36 days before it has been sent to the slaughterhouse. The WP for preparation is 28 days.
According to investigations on the farm no One kidney sample of pig was violation was detected. It was assumed that the positive for ochratoxin ( < 2,5 reason for the positive finding was feed from the µg/kg) year 2003. There was no feed left to take
EN 126 EN
additional samples.
Poultry
& @
Sheep and goat
& @
Horses
& @
Milk
One milk sample (collection milk in Milk collection route was sampled farm by farm. car tank) was positive for aflatoxin Positive farm was found and investigated. The (86 ng/kg) reason in farm was mouldy fodder corn preserved with acid. Dairy products made of the milk in question were investigated.
Eggs
& @
Rabbit
& @
Aquaculture
One sample of fish eggs from lake Accordiong to investigations on the fish farm it trout (Salmo trutta lacustris) was was assumed that the reason for the positive positive for leucomalachite founding were the old dark colored “containers” , green(6,3 µg/kg). which were made of wood and used for fish egg preservation. New samples of older fish from the farm and younger fish from this part of fish eggs were taken, but they all were negative. During the investigations transfer of the young fishes was forbidden. Samples were taken also from another farm using the same part of fish eggs, but no positive samples were found.
(New samples from the farms were taken, but no
EN 127 EN
positive were found.)
(2 fish samples contained LMG < 1 µg/kg)
Farmed game
6 liver samples and 8 kidney @ samples were positive for cadmium.
Wild game
7 liver samples and 8 kidney @ According to Finnish legislation livers and kidneys samples were positive for cadmium. of over one year old elks are not accepted for human consumption
Honey
2 honey samples were positive for No actions made. The intension is to take new sulfathiazole ( < 20 µg/kg) samples from these farms this summer.
One honey sample was positive for oksitetracycline ( 18µg/kg) and tetracycline (8 µg/kg)
EN 128 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State FRANCE Date 18 mai 2006
Group A substances
Modification of national residue Aggregate for all animal products and substances plan En France, toute mise en évidence de substances interdites par une DDSV (direction départementale des services vétérinaires) doit être transmise à la Brigade Nationale d’Enquêtes Vétérinaires et Phytosanitaires (BNEVP) qui mène les enquêtes et informe les autorités juridiques. Dans le but de démanteler des trafics de substances interdites, les enquêtes sont longues et les rapports ne parviennent à la DGAL (Direction Générale de l’Alimentation) qu’une fois l’affaire jugée (secret de l’instruction). Tous les élevages et établissements ayant eu des résultats non conformes au cours des plans de contrôle 2005 seront ciblés prioritairement pour les plans 2006. Non-compliant results Follow-up actions Chloramphénicol - 0.90µg/kg - La Brigade Nationale d’Enquêtes Vétérinaires et muscle - veau Phytosanitaires (BNEVP) a été informée et le parquet n’a pas été saisi. Une enquête d’environnement est en cours. Chloramphénicol - 0.33, 0.41, La BNEVP a été informée des dossiers. Pour 3 1.09, 1.27 et 4.51µg/kg - muscle - cas, une enquête est en cours et le dossier a été ovins transmis à la justice. Chloramphénicol - 0.3 et 14µg/kg La BNEVP a été informée, le parquet n’a pas été - muscle - lapins saisi. Une enquête environnement est en cours et de nouveaux prélèvements sont prévus au 2nd semestre 2006. Un prélèvement en contrôle renforcé s’est révélé être conforme. Chloramphénicol - 1µg/kg - chair - La BNEVP a été informée. Le rapport de cette Poisson d’élevage (truite arc en enquête n’est pas finalisé. La DDSV a prévu de ciel) prélever cette pisciculture en priorité dans le cadre du plan de contrôle 2006. Nitroïmidazoles : métronidazole - Une enquête est en cours mais le rapport n’est pas 2.2µg/kg - muscle - poulet de chair finalisé. Thyréostatique : thiouracile - 4.2, La BNEVP a été informée de ces 3 cas de non- 5.2 et 68µg/kg - thyroïde - une conformité. Des enquêtes environnement sont en
EN 129 EN
génisse et deux jeunes bovins cours et de nouveaux prélèvements sont prévus en 2006. Thyréostatique : thiouracile - 3.5, La BNEVP a été informée de ces 4 cas de non- 6.0, 7.3 et 11.3µg/l - urine - veau conformité. Une enquête préliminaire a été menée en collaboration avec une unité de la gendarmerie Thyréostatique : thiouracile – 104 (Office Central de Lutte contre les Atteintes à µg/kg – aliment bovin l’Environnement et à la Santé Publique) et le dossier est en cours d’instruction au pôle santé publique de Paris. Stéroïdes : 17 béta-oestradiol - La DDSV doit prélever cet élevage dans le cadre 2µg/kg - foie - poule de réforme du plan de contrôle 2006. La BNEVP n’a pas été informée de ce cas. Stéroïdes : 17 béta-oestradiol - 3 La BNEVP a été informée de ces 2 cas et des et 45µg/kg - foie - truite enquêtes d’environnement sont en cours. Il a été demandé de faire des recherches bibliographiques sur ce sujet car la non-conformité est difficile à confirmer. La DDSV prévoit de prélever ces piscicultures dans le cadre du plan 2006. Stéroïdes : 17 béta-nandrolone - Cinq cas ont été recensés sur des animaux de sexe 1.0, 150µg/kg - urine - porcin mâle ou indéterminé et un seul cas sur un animal de sexe femelle. La BNEVP a été informée mais elle n’a entrepris aucune action sachant que seuls les prélèvements sur des femelles sont pertinents. Le Laberca, laboratoire national de référence, ne se prononce pas sur la présence anormale de cette molécule dans les urines de porc. La DGAL va sensibiliser les DDSV pour que seules les truies soient ciblées pour la recherche de stéroïdes. Béta-agonistes : clenbutérol - La BNEVP a été informée et une enquête est en 5µg/l - urine - veau cours. Acides résorcyliques : taléranol et La DDSV a fait une enquête et a conclu à la zéranol - 0.1 et 0.2µg/kg - foie - distribution aux animaux d’un foin de mauvaise bovin qualité. La consommation d’aliment contaminé par des moisissures de type fusarium pourrait être à l’origine de cette non-conformité. • Information to be included for each non-compliant result. In case of several non- compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 130 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances Tous les élevages et établissements ayant eu des résultats non conformes au cours des plans de contrôle 2005 seront ciblés prioritairement pour les plans 2006. Des courriers rappelant la bonne tenue obligatoire du registre d’élevage ont été transmis aux éleveurs concernés. Dans la plupart des cas, des mesures correctives ont été mises en place pour pallier aux erreurs de gestion du registre d’élevage (conservation des ordonnances). Il a été rappelé aux éleveurs : - Le respect des posologies et des durées de traitement. - La nécessité du respect du temps d’attente après administration de médicaments vétérinaires et avant abattage. - D’assurer la gestion des stocks de médicaments vétérinaires par une surveillance accrue et une élimination régulière des médicaments périmés. Non-compliant results Follow-up actions Bovines La matrice est le muscle Oxytétracycline : 8 vaches de réforme, 4 jeunes bovins, 1 veau Spiramycine, OTC et tétracycline – 1 jeune bovin Danofloxacine – 1 jeune bovin Amoxycilline – 2 vaches de réforme Amoxycilline et tétracycline – 1 vache de réforme Les DDSV ont envoyé des courriers de rappel Ampicilline – 2 veaux aux éleveurs. Les enquêtes menées dans les Spiramycine – 1 vache de réforme élevages ont souvent mis en évidence la OTC et sulfadiméthoxine – 1 vache mauvaise tenue du registre d’élevage : absence de réforme des temps d’attente, absence de l’identification Tylosine et DHS – 1 vache de réforme de l’animal traité, absence de la date de fin de Benzylpénicilline – 1 veau traitement. Pénicilline G et DHS – 1 bovin Le non respect des temps d’attente est généralement à l’origine des non-conformités.
1 phénylbutazone – muscle de vache de réforme
La DDSV a constaté au cours de l’enquête qu’aucun enregistrement d’administration des médicaments n’était inscrit dans le registre. L’élevage est placé en contrôle orienté en 2006 et une nouvelle visite est prévue dans cet exploitation afin de contrôler la bonne tenue du 1 dexaméthasone – muscle et poils de registre d’élevage.
EN 131 EN
vache de réforme Mise en évidence de déxaméthasone dans le muscle avec dépassement de LMR. La DDSV a réalisé une enquête dans l’élevage et a constaté la bonne tenue du registre d’élevage concernant les mouvements des animaux mais les interventions du vétérinaire concernant l’animal en question manquent (notamment les injections que l’animal a subies). La DDSV n’a pas pu conclure sur le fait qu’une éventuelle autre injection ait été faite. Pigs La matrice est le muscle Pour l’oxytétracycline, l’enquête dans l’élevage a montré la bonne tenue du registre 1 Oxytétracycline, d’élevage et de la pharmacie. Le dépassement 1 Tétracycline, est sans doute dû à une erreur humaine. 1 Amoxycilline, Pour les autres molécules, l’enquête sur le 1PénicillineG+déhydrostreptomycine terrain n’a pas permis de déterminer la cause exacte de la non-confomité du fait de l’absence d’enregistrement de l’ensemble des traitements administrés aux animaux. Les DDSV ont 3 Sulfadiméthoxine adressé des courriers de rappel aux éleveurs concernant leurs obligations
Les enquêtes ont mis en évidence des erreurs de manipulation des animaux qui ont entraîné leur introduction accidentelle à l’abattoir avant 1 Diazinon – graisse périrénale et rein la fin des temps d’attente. Les DDSV ont adressé des courriers aux éleveurs pour leur rappeler leurs obligations.
L’exploitant a été informé par courrier de son résultat défavorable. De nouveaux contrôles sur ses animaux sont prévus dans le cadre du plan de contrôle 2006. Poultry Aucune non-conformité n’a été mise en évidence en 2005 pour les substances du groupe B. Sheep and goat Oxytétracycline : 3 caprins et 1 ovin – Une enquête a révélé la délivrance d’un muscle médicament sans ordonnance pour traiter une mammite et le non-respect du temps d’attente.
Pour l’une des non-conformités, la DDSV n’a pas effectué d’enquête car l’élevage concerné est surveillé par la BNEVP pour utilisation de 1 sulfaméthazine – muscle d’ovin substances interdites.
EN 132 EN
4 sulfadiméthoxine – muscle d’ovin L’enquête n’a pas permis de déterminer la HCH alpha et HCH béta - graisse cause de la non-conformité. périrénale et rein de caprin L’exploitant a été informé par courrier de son résultat défavorable. De nouveaux contrôles sur ses animaux sont prévus dans le cadre du plan de contrôle 2006.
Horses 1 phénylbutazone - muscle Au cours de la visite, l’éleveur n’a pas été en mesure de présenter le registre d’élevage. Les documents établis par les vétérinaires ayant traité la jument ne mentionnaient pas le temps d’attente : les médicaments n’ont donc pas pu être utilisés à bon escient. L’animal n’était pas identifié. La DDSV a rappelé à l’éleveur ses obligations et lui a demandé de mettre en place les mesures correctives nécessaires. Milk Aucune non-conformité n’a été mise en évidence en 2005 pour les substances du groupe B. Eggs 4 sulfadiazine Les enquêtes réalisées n’ont pas permis de définir la cause des non-conformités sachant 1sulfadimérazine et que les traitements à base de sulfamides ne sulfadiméthoxine – œufs de poules sont pas autorisés chez les poules pondeuses.
Une DDSV a effectué un contrôle renforcé sur un prélèvement d’œufs de caille suite à une non-conformité mise en évidence dans le plan 2004. Le résultat est conforme. L’enquête a conclu à la bonne tenue du registre d’élevage et a permis de retrouver les ordonnances, les traitements administrés et les
délais. La non-conformité est sans doute due à une erreur de manipulation dans l’abreuvement des animaux, ou le traitement a été prolongé en absence d’indication sur le registre d’élevage. Dans tous les cas, le médicament à base de sulfamides ne devait pas être prescrit par le vétérinaire aux cailles dont les oeufs sont destinés à la consommation humaine.
EN 133 EN
Les DDSV ont réalisé des enquêtes dans les
élevages concernés. La présence d’anticoccidiens dans les prélèvements n’a pas pu être expliquée. Les hypothèses formulées sont les suivantes : - contamination au cours de la fabrication Anticoccidiens : robénidine, des aliments médicamenteux à l’usine lasalocide, nicarbazine, diclazuril et (mauvais nettoyage entre 2 fabrications maduramycine – 19 œufs de poules et d’aliments médicamenteux destinés à 5 œufs de cailles des espèces différentes). - Les résultats sont de faux positifs (il s’agit d’un plan expérimental géré par le LNR).
Dans le cadre du plan de contrôle 2006, la DDSV va prélever en priorité cet élevage.
Aldrine et dieldrine – oeufs de poules Rabbit 9 sulfadiméthoxine - muscle Les non-conformités sont souvent dues à des contaminations croisées. Une DDSV a constaté qu’un même silo recevait de l’aliment blanc et de l’aliment médicamenteux ; seul une paroi séparatrice à l’intérieur du silo permettait de le scinder en 2 compartiments. Deux contrôles renforcés sur des muscles de lapins ont été réalisés suite à des non- conformités, et les résultats sont sortis conformes. Aquaculture 1 quinolone : sarafloxacine - chair La DDSV a rappelé au pisciculteur ses obligations. Un prélèvement supplémentaire a
été effectué et le résultat s’est avéré être conforme.
3 vert malachite – chair de truite arc Les DDSV ont effectué des enquêtes dans les en ciel, truite Fario et tanche trois piscicultures. Au cours d’une visite, la DDSV a trouvé un reste de vert malachite. Le pisciculteur a déclaré en avoir utilisé uniquement sur des reproducteurs, après la
EN 134 EN
période de ponte et que ces poissons ne sont pas destinés à la consommation humaine. L’interdiction du vert malachite concerne les poissons à n’importe quel stade de la production. Une visite a également mis en évidence que la dernière utilisation de vert malachite remontait à 2 ans (date d’interdiction) mais que la retenue d’eau dans laquelle a été réalisé le prélèvement, n’avait jamais été vidangée ni nettoyée.
Suite aux résultats non conformes, 7 prélèvements en contrôle renforcé ont été effectués : les résultats sont tous conformes.
L’ensemble des étangs est situé en partie basse de bassins versants à dominantes cultures de céréales et de maïs avec épandage d’intrants spécifiques notamment de boues de papeterie,
de boues industrielles, d’engrais et autres pesticides. La DDSV a prévu de prélever cette PCB – chair de poisson d’étang pisciculture en contrôle ciblé sans consigne au cours du plan 2006, à peu près à la même période que lors de la réalisation du prélèvement en 2005. Farmed game and Wild game Aucune non-conformité n’a été mise en évidence en 2005 pour les substances du groupe B. Honey 2 tétracyclines – miel Les DDSV vont prélever en priorité ces apiculteurs dans le cadre du plan de contrôle 2006.
EN 135 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State GERMANY Date 29 June 2006
Modification of national residue plan – general
Screening methods
In the course of standardising transmission of residue control plan data to the Commission, it has been agreed that Member States should also report their screening methods on-line from 2005 on. Accordingly, screening methods have been included in the plan.
Matrices
The Commission found that the plan contains too many substance-matrix combinations. It was agreed to list only those matrices which were in fact to be examined. Therefore, irrelevant matrices have been eliminated from the 2006 plan.
Group A substances
Modification of national residue plan Aggregate for all animal products and substances Group A3
Cattle, swine, sheep/goat and horses 17-alpha-Trenbolon was included as a new substance. Rabbits The following substances were included in the plan: methyltestosterone, 17 alphatrenbolon, 17 beta-trenbolon, stanozolol, 17 alpha-nortestosterone und 17 betanortestosterone.
Group A4
EN 136 EN
Cattle, swine, sheep/goat and horses Liver was added to the matrices listed in the national residue control plan because there are plans for an MRPL of 2 μg/kg of zeranol and zearalenone in liver.
Group A5
Cattle, swine, sheep/goat and horses Sample numbers have been reduced to 15% of the total sample number in group A, both in the producer’s establishment and in the slaughterhouse, because there have not been any findings of beta-agonists since 2002, except for one unclear finding of mabuterol in turkeys in 2003. The capacities released by this step have been added “Group A1-A6, free choice”.
Poultry Given the fact that the poultry’s drinking water is as well suited to control administration of ß-agonists as actual birds, sample numbers prescribed for birds and drinking water/birds in 2005 have been swapped, so that more samples can be drawn from drinking water instead in 2006. In order to check administration of ß-agonists by feed, the plan provides for feed samples to be drawn in addition to drinking water samples.
Group A6
Poultry Analysis of the metabolite DSH has been included in the plan.
Milk The CRL in Fougéres recommended to test milk for nitrofuranes. Yet, discussion with experts of Germany’s federal states brought out that nitrofuranes do not play a role dairy farming. The states therefore did not deem it necessary to perform such analyses.
Eggs The CRL in Fougéres recommended to test eggs for chloramphenicol. Therefore, 25% of the tests provided for in group A6 are targeted on chloramphenicol. The CRL in Berlin recommended to test eggs for metronidazol. As this substance is analysed together with nitro-imidazols by the same method, metronidazol has been included as an additional obligatory substance in the 2006 plan. Honey Because of a number of rapid alert notices, the Commission recommended to test honey
EN 137 EN
for nitrofurane metabolites. Therefore, 17 samples will be tested for group-A6 substances (chloramphenicol and nitrofurane metabolites). Non-compliant results Follow-up actions Chloramphenicol -2,1 Investigations at the farm of origin; follow-up μg/kgdrinking water – turkey samples of animal drinking water positive; followup samples of animals negative; drinking water pipes exchanged Chloramphenicol -0,41 No information μg/kgmuscle fattening pig Chloramphenicol -0,93 On-site controls; follow-up samples (slaughter μg/kgmuscle fattening cow animals and drinking water) with negative result; check of veterinary dispensary, notice of slaughter, case handed over to public prosecutor Chloramphenicol -0,39 Analysis of 10 follow-up samples from the μg/kgplasma cattle original stock (cattle plasma), all follow-up samples were free of CAP, the cause of the positive finding could not be established. Chloramphenicol -2,5 μg/kgmuscle On-site investigations in the slaughterhouse, chicken closure of stock of origin, analysis of follow-up samples from the stock of origin, analysis of feed and drinking water, release after all follow-up samples turned out to be free of CAP. Cause could not be finally clarified. Chloramphenicol -2 μg/kg- muscle On-site inspection of flock by responsible duck authority, taking of suspicious and follow-up samples to establish cause, inspection of farm dispensary. Preliminarily seized product was released by responsible authority after negative result of follow-up samples. All follow-up samples below limit of detection. AOZ- 3 μg/kg- muscle eel Investigations at the farm of origin: follow-up samples of animals and feed negative. Investigations in the supplier farm: follow-up samples of animals negative; intensified checks of stocks for 12 months; criminal proceedings. Hydroxymetronidazol/metronidazol On-site inspection; taking of 3 suspicious samples 0,23 / 0,058 μg/l plasma fattening in which residues of hydroxymetronidazol / pig metronidazol were found (between 0.33 and 5.55 μg/l). Farm closed until 25 follow-up plasma samples are analysed with negative result. Analysis of 4 feed samples (2 positive), inspection of veterinary dispensary, intensified checks of livestock; case handed to public prosecutor
EN 138 EN
Testosterone -5,4 μg/kg- Investigations at farm of origin; follow-up plasmaheifer samplesnegative; inspection of the farm’s veterinary dispensary, no signs of illegal treatment; intensified checks of livestock. Nandrolone -82,4 μg/kg- urine-bore Investigations in the farm of origin; follow-up samples negative; no signs of illegal treatment; intensified checks of livestock
* Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 139 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances
Group B1
Milk With regard to sulfonamides, the standard range of substances is taken over as target.
Farmed game In order to put Annex II of Directive 96/23/EC into practice, and comply with the Commission’s requirements for transmission of data, sample numbers provided for group B1 have been distributed over the following sub-groups: sulfonamides, tetracyclines, and chinolones. Analyses are made for the standard range of substances.
Group B2a
Cattle, swine, sheep/goat and horses Numbers of samples for avermectins have been halved, except for with horses, as there have been no positive findings for these substances. Freed sample capacities have been distributed over the B2d and B2e groups, because there, positive findings must be expected rather than with avermectins. The benzimidazoles albendazole, albendazole sulfoxide, fenbendazole, flubendazole, oxfendazole, oxibendazole, thiabendazole, triclabendazole and mebendazole have been included in the plan as obligatory substances. „Other anti-helminthics“ (levamisole to niclosamide): these substances have been deleted from the plan for capacity reasons and lack of importance. From group B2a, 416 samples will again be tested for benzimidazoles in 2006, while 999 samples will be tested for substances of the B2b and B2c groups.
Poultry Analysis of levamisole and flubendazole has been included in the plan.
Rabbits In order to put Annex II of Directive 96/23/EC into practice, the following substances have been fixed: ivermectin, abamectin, doramectin, eprinomectin, and moxidectin.
Group B2b
EN 140 EN
Cattle, swine, sheep/goat and horses Use of the feed additives monesin-Na (for cattle) and salinomycin-Na (for piglets and fattening pigs) has been banned without transition since 01 January 2006. Apart from for these two substances, tests are also made for lasalocid, because of the problem of unintentional transfer to successive production lots of feed. Some 470 samples will therefore be tested for the substances mentioned. To survey compliance with that ban, it is recommended to draw most of the samples in the first half of 2006.
Rabbits In order to put Annex II of Directive 96/23/EC into practice, and comply with the Commission’s requirements for transmission of data, the following substances have been fixed: monesin, nicarbacin, salinomycin, and metylchlopidol.
Farmed game In order to put Annex II of Directive 96/23/EC into practice, and comply with the Commission’s requirements for transmission of data, the following substances have been fixed: monesin, nicarbacin, and salinomycin.
Group B2c
Cattle, swine, sheep/goat and horses To comply with annex II of Directive 96/23/EC, the number of 172 samples was fixed to be analysed in group B2c.
Poultry Tests for cypermethrin, alpha-cypermethrin, deltamethrin, and permethrin have been added.
Rabbits In order to put Annex II of Directive 96/23/EC into practice, and comply with the Commission’s requirements for transmission of data, the following substances have been fixed: diallat, bifenthrin, cyhalothrin, cypermethrin, deltamethrin, esfenvalerate, fenvalerate, fluvalinate and permethrin.
Farmed game In order to put Annex II of Directive 96/23/EC into practice, and comply with the Commission’s requirements for transmission of data, the following substances have been fixed: cyhalothrin, cypermethrin, deltamethrin, and permethrin.
Group B2e
EN 141 EN
Cattle, swine, sheep/goat and horses Tests for phenylbutazon repeatedly produced positive findings, in majority with cattle, in contrast to tests for the other NSAIDs on the plan. Sample numbers of phenylbutazon tests have therefore been raised by 40%, while the numbers for the other NSAIDs have been reduced correspondingly. For horses, sample numbers for phenylbutazon tests have been doubled. Sample numbers for other NSAIDs have been distributed as follows: - 50 % of samples will be analysed for carprofen, vedaprofen, tolfenamin acid, flunixin, meloxicam and diclofenac, and - 50 % of samples will be analysed for metamizol, aminopyrin and ramifenazon.
Poultry Tests for carprofen, vedaprofen, tolfenamin acid, flunixin, meloxicam and diclofenac have been included in the plan.
Farmed game In order to put Annex II of Directive 96/23/EC into practice, and comply with the Commission’s requirements for transmission of data, the following substances have been fixed: phenylbutazon, carprofen, vedaprofen and tolfenamin acid.
Group B2f
Cattle, swine, sheep/goat and horses Dexamethasone, betamethasone, prednisolone and methylprednisolone have been added to the 2006 Plan, because they are analysed by one and the same method.
Rabbits In order to put Annex II of Directive 96/23/EC into practice, and comply with the Commission’s requirements for transmission of data, the following substances have been fixed: phenylbutazon, carprofen, vedaprofen, tolfenamin acid, flunixin, meglumin, diclofenac, ketoprofen, mefenamin acid, nifluminin acid, oxyphenbutazon anhydrat, suxibuzon.
Group B3a
All animal species and products Simazine and methoxychlor have been deleted from the test scheme because there have been no findings – as far as BVL knows – above the maximum residue limits during the sampling period 2003to 2005, and because these substances hardly any longer play a role as environmental contaminants. They had been included in the plan in 2002 in the wake of a nitrofen scandal.
Eggs
EN 142 EN
The Commission has issued Regulation No. (EC) 684/2004 revising maximum limits for dioxins in food. Under these regulations, the maximum permissible dioxin level of 3pg WHO-PCDD/F- TEQ/g fat in hens’ eggs and egg products stemming from extensive farming was suspended until 31 December 2004. The availability of data being still unsatisfactory, and dioxin testing of eggs being part of a large- scale dioxin monitoring anyhow, it is planned that 111 samples will be analysed for dioxins and dioxin-like PCBs in 2006.
Group B3b
Cattle, swine, sheep/goat and horses In order to put Annex II of Directive 96/23/EC into practice, the following substances have been included as obligatory substances: phoxim, propetamphos, and diazinone.
Group B3c
Eggs Sixty-five samples will be analysed for the following elements in line with the provisions of the National Food Monitoring scheme: arsenic, lead, cadmium, copper, mercury, selenium, and zinc. The data are needed for comparison with the National Food Monitoring.
Group B3d
Poultry / Aquacultures Aflatoxin M1 has been deleted as irrelevant. It is formed only in the rumen of ruminants.
Aquacultures To act in conformity with Directive 96/23/EG, Annex II, aflatoxin B1and ochratoxin A were fixed as obligatory substances in group B3d.
Group B3e
Aquacultures The high numbers of samples prescribed for 2005 are maintained in 2006 because of the positive findings of malachite green in 2004 and 2005.
Non-compliant results Follow-up actions Bovines 1 PCB 153, PCB 138, PCB 180 – Examination of the producer farm; analysis of
EN 143 EN
fat feed; identified as cause was an old, PCB- containing silo wall paint. Change of feed; several analyses of milk at the farm. No further findings and information. 5 investigations at the farm of origin: 5 document reviews; 3 notifications of slaughter and intensified controls of livestock, 5 inspections of veterinary drug dispensaries; 5 criminal cases, 1 caution.
5 Neomycin – kidney 2 investigations at the farm of origin: 2 document reviews; 1 inspection of the farm’s veterinary drug dispensary; 1 casefined; 1 action unknown (producer farm in Belgium)
2 Gentamicin – kidney 1 investigation at the farm of origin: 1 document review; 1 criminal case
1 Gentamicin – kidney and muscles On-site inspection of livestock and farm: review of documents, inspection of the farm’s veterinary dispensary
1 Gentamicin – kidney 3 investigations at the farms of origin: 3 document reviews; 2 notifications of slaughter; 2 intensified checks of livestock; 2 inspections of veterinary drug dispensaries; 3 criminal proceedings
3 Dihydrostreptomycin – kidney 2 investigations at the farm of origin: 2 document reviews; 2 intensified checks of livestock; 1 criminal proceedings, 1 x no further action
2 Tetracycline – kidney 2 investigations at the farm of origin: 2 document reviews; 2 intensified checks of livestock; 1 criminal proceedings, 1 x no further action
1 Penicillin – kidney 1 investigation at the farm of origin: 1 document review; 1 criminal proceedings
1 Ampicillin – kidney 1 investigation at the farm of origin; 1 document review; 1 inspection of the farm’s veterinary drug dispensary; 1 criminal proceedings 1 Enrofloxacin/ciprofloxacin – 1 investigation at the farm of origin: 1 document kidney and muscles review; 1 inspection of the farm’s veterinary drug dispensary; 1 criminal proceedings
1 Dexamethason – liver 1 investigation at the farm of origin: 1 document review; 1 criminal proceedings 2 Phenylbutazon – plasma investigations at the farm of origin: document reviews; follow-up samples; ban on transport and delivery of livestock; inspection of the farm’s veterinary drug dispensary; criminal proceedings
EN 144 EN
4 Cadmium - kidney and muscles No information
Pigs
2 Tetracycline – muscle and kidney On-site inspection of the livestock: review of documents, non-compliance with prescribed waiting periods. Intensified checks of livestock ordered in case of recurrence, caution or institution of criminal proceedings
1 Tetracycline – kidney 1 investigation at the farm of origin: 1 document reviews; 1 criminal proceedings 1 Oxytetracycline – muscle 1 action not known (producer farm in the Netherlands)
1 Benzylpenicillin – kidney 1 on-site inspection, 1 inspection of the farm’s veterinary drug dispensary, 1 notification of slaughter, 1 intensified checks of livestock, 1 institution of fine/criminal proceedings
2 Gentamicin - kindey – muscle 2 investigations at the farm of origin: 2 document reviews; 2 inspections of veterinary drug dispensaries; 2 criminal proceedings
2 Dihydrostreptomycin – kidney 2 investigations at the farm of origin: 2 document reviews; 1 notification of slaughter; 2 criminal proceedings
1 Sulphadimidine – kidney On-site inspection of the livestock, intensified checks of livestock, inspection of the farm’s veterinary drug dispensary, institution of fine / criminal proceedings
1 Sulphadimidine – muscle 1 investigation at the farm of origin: 1 document reviews; 1 inspection of the farm’s veterinary drug dispensary; "private slaughter", meat for private consumption 2 Sulphadimidine – kidney and 2 investigations at the farms of origin: 2 document muscle reviews; 1 intensified checks of livestock; 2 criminal proceedings
1 Sulphadimidine – muscle 1 on-site inspection, 1 follow-up samples, 1 notification of slaughter, 1 institution of fine/criminal proceedings 1 Sulphamerazine, Sulphadimidine 1 investigation at the farm of origin: 1 document –kidney review; 1 inspection of the farm’s veterinary drug dispensary; 1 criminal proceedings 2 Sulphadiazine – kidney and 2 investigations at the farms of origin: 2 document
EN 145 EN
muscle reviews; 1 intensified checks of livestock; 2 inspections of veterinary drug dispensaries; 2 criminal proceedings
1 Diclofenac – kidney 1 investigation at the farm of origin: 1 document review; 1 criminal proceedings 1 Cadmium – kidney 1 on-site inspection, 1 follow-up samples, 1 intensified checks of livestock 1 Sulphadimidine – muscle, 1 No information Sulfadoxin - muscle, 1 Tetracycline – kidney, 1 Cadmium – kidney
Poultry & @
Sheep and goat
1 Dexamethasone – muscle 1 on-site inspection, 1 follow-up samples, 1 inspection of the farm’s veterinary drug dispensary, 1 notification of slaughter, 1 intensified checks of livestock, 1 institution of fine/criminal proceedings
Horses
1 Cadmium, muscle No information
Milk
2 Ampicillin – milk 2 on-site inspections, 2 follow-up samples, 2 inspections of the farms’ veterinary drug dispensaries, 1 case of recurrence, 2 intensified checks of livestock, 2 institution of fine/criminal proceedings
Eggs
1 Nicarbazin – egg 1 investigation at the farm of origin: 1 document review; follow-up samples of eggs and feed negative
1 Lasalocid – egg Establishment will be sampled again in 2006
EN 146 EN
1 WHO-PCDD/F-TEQ (Dioxin) – 1 on-site inspection, 1 follow-up samples egg
Rabbit & @
Aquaculture 1 Leuko-malachite green - muscle – Four follow-up samples taken (four of four trout samples are positive), there is no further information available yet 1 Leuko-malachite green - muscle – On-site inspection of the livestock, six follow-up trout samples taken (three of six samples positive), institution of administrative action: ban on delivery according to § 41 (2) Food and Feed Code, intensified checks of stocks announced for 12 months, criminal proceedings /case handed to public prosecutor 2 Malachite green and On-site inspection of the livestock: document Leukomalachite green – muscle and review, recurrent case, ban on delivery, follow-up skin – trout sampling of all ponds where fish with residues of malachite green were found. Fishing and killing of
all fish in ponds where fish with residues of malachite green were found. 2 Malachite green and leuko 2 on-site inspections, 2 follow-up samples, 1 malachite green – muscle/skin – inspection of the farm’s veterinary drug trout dispensary, 2 institution of fine/criminal proceedings
1 Malachite green and 1 on-site inspection, 1 follow-up samples, 1 leukomalachite green – muscle – institution of fine/ criminal proceedings carp
1 sample malachite green – muscle Follow-up sample was negative of rainbow trout
1 Leuko-malachite green – On-site re-examination of the livestock by muscle/skin – trout responsible authority, livestock concerned was import from Poland, fish were about 12 months old 2 Leuko-malachite green No information muscle/skin – carp and trout
8 Ethoxyquin – muscle – trout Samples from eight farms dispersed in Bavaria;
EN 147 EN
cause: use ethoxyquin in feed as an anti-oxidant agent according to EU authorisation (confirmed by feed analyses in two cases);
2 Ethoxyquin – muscle/skin – trout 2 on-site inspections, 2 follow-up samples, 2 intensified checks of fish stocks 1 Ethoxyquin – muscle – trout 1 on-site inspection, 1 follow-up samples
Farmed game & @
Wild game 1 Total DDT, pp-DDE – fat Taking more samples in hit areas is planned
1 Total DDT – fat Total of 30 follow-up samples from the district concerned; among them, some carried residues above the maximum level; likely cause: environmental contamination (soil); attempt at regional demarcation; no more findings available 1 Total DDT – fat, pp-DDE –fat No information 1 Total DDT – fat, pp-DDE, pp- On-site inspection by responsible authority, DDT – fat follow-up samples 1 Total DDT – fat, p,p-DDE –fat Responsible authority takes suspicious and follow- up samples, informs entitled hunters 1 ß-Hexachlorocyclohexane –fat Contamination of game; no producer responsible; cause hard to clarify; more samples in the framework of the National Residue Control Plan in 2006 and later will show whether there are recurrent cases which indicate unusual environmental contamination. 1 Lindane - fat, 1 Diazinone –fat No information Honey 1 Sulphadimidine, sulfamerazine 1 on-site inspection, 1 follow-up samples, 1 and sulfathiazol – honey intensified checks of stocks, 1 institution of fine / criminal proceedings
EN 148 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State GREECE Date For the year 2005 June 2006
GROUP A SUBSTANCES
Non-compliant results Follow-up actions AOZ- 2,6μg/kg-muscle-pig AOZ-5 μg/kg-muscle-poultry
GROUP B SUBSTANCES
Modification of national residue Aggregate for all animal products and substances plan
Non-compliant results Pigs 3 chlortetracyclin- kidney 6 sulfadiazine-kidney 1 sulfamethoxypyridazine- kidney 7 sulphadimidine - kidney Poultry 1 Lead Sheep and goat 1 chlortetracyclin 1dihydrostreptomycin 1 Lead 2 Cd Milk
EN 149 EN
1 Lead Eggs 2 sulfonamides Aquaculture 1 oxytetracyclin fish 1 Hg fish
Follow-up actions investigations in the farm of origin, verification of records, additional sampling, intensified checks on the animals and products from the farm, carcasses and products declare unfit for human consumption, administrative measures Honey 10 doxycyclin investigations in the farm of origin, verification of records, additional sampling, intensified checks 4 streptomycin on the products from the farm, products declare 1sulfachlorpyridazin unfit for human consumption, administrative 2 sulfamerazin measures 1 sulfamonomethoxin 3 sulfamethazine 1 sulfathiazol
Modifications to the residue monitoring plan for the year 2006
The number of samples for each group of substances is estimated to fulfill the minimum requirements of the Council Directive 96/23/EC & the Commission Decision 97/747/EC. So, taking into account the volume of production in 2005 and 2004 (fish, honey) and the fact that there were positive results in several groups of substances, the number of samples is slightly changed.
EN 150 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State IRELAND
Date June 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
Agriculture • Sample numbers for Nitrofurans have increased following positive findings in 2005 • Stanozolol has been added to the plan for bovines and equines • Metyltestosterone has been added to the plan for bovines • Matrix changes – Thyrostats in Poultry changing from Muscle to Serum • Sampling numbers adjusted downwards to reflect no positive findings for Bovines and Porcines for groups A3, A4, A5 & A6. Aquaculture In 2005 plan, Dexamethasone was categorised as a Group A3 compound however on request from the Commission in order to have the aquaculture plan in line with the rest of the national plans in Ireland it has been inserted in the 2006 plan as B2f ( other pharmacologically active substances). Non-compliant results Follow-up actions • 5 non-compliant results 1 target sample taken at a slaughter house in April • Furazolidone 2005 showed a positive level of 0.27 μg/kg. • Range from 0.10 μg/kg to Following extensive investigations at farm of 0.27 μg/kg origin of the animal, no evidence was found of • Liver presence or use of Furazolidone. 10 feed samples • Bovine were taken from the farm and all proved negative for the presence of Furazolidone. All sampling points instructed to implement sampling of 10% of animals presented from this herd. 4 further samples taken at a slaughter house in July 2005 showed positive for Furazolidone at levels ranging from 0.10 to 0.16 μg/kg. Inspectors from the Department’s Special Investigation Unit and at the sampling points continue to monitor this herd through increased sampling and no further positive findings or evidence of use of Furazolidone have been identified. • 1 non-compliant result 1 target sample taken at a slaughter house in July • Furazolidone
EN 151 EN
• 0.10 μg/kg 2005 showed a positive level of 0.10 μg/kg. • Liver Following extensive investigations at farm of • Bovine origin of the animal, no evidence was found of presence or use of Furazolidone. 26 blood samples were taken from the farm and all proved negative for the presence of Furazolidone. * Information to be included for each non-compliant result. In case of several non- compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
Group B substances
Modification of national residue Aggregate for all animal products and substances plan Agriculture • Confirmatory analysis for B1 shall be carried out by the CRL pending validation of a full confirmatory suite by the Central Meat Control Laboratory. • Equine sampling has been expanded to include B2(b) – Anticoccidials, B2(c) – Carbamates and Pyrethroids, B3(a) – OCs and PCBs, B3(b) – OPs. • Milk sampling has been expanded to include B2(a) – Benzimidazoles, B2(e) – Nsaids and B2(f) – Dexamethazone. • Sampling numbers for Antibiotic testing in porcines adjusted downwards to reflect the continued low incidence of positive residue results. • Mycotoxins added to the plan for Honey.
Non-compliant results Follow-up actions Bovines • 1 non-compliant result 1 target sample taken from a live animal on 15 • Phenylbutazone June 2005 proved positive for phenylbutazone. • Serum Extensive on-farm investigation carried out and inspection of private veterinary practitioners records also conducted. No evidence found of possession or use of phenylbutazone. • 35 non-compliant results 7 target samples screened positive for • Antimicrobials Antimicrobials. In addition 27 suspect samples • Muscle also screened positive for antimicrobials and 1 suspect sample was confirmed positive by the CRL for Oxytetracyclines. In all cases where suspect samples prove positive the carcasses are declared unfit for human consumption. On farm investigations including examination of animal
EN 152 EN
remedies record were carried out in all cases. Pigs • 26 non-compliant results 24 target samples and 2 suspect samples screened • Antimicrobials positive for antimicrobials. All carcasses were • Muscle declared unfit for human consumption. 20 farms were inspected and 6 positives were referred to the Northern Ireland Authorities for further action. Poultry • 16 non-compliant results 15 target samples proved positive for nicarbazin at • Anticoccidials a level in excess of 200μg/kg and 1 sample was • Liver positive for Monensin at a level of 13.5μg/kg. On farm inspections were carried out in all cases, animal remedies records were examined and on- going communication continues between the Department’s inspectorate, poultry growers and the poultry industry in order to address the issue. Sheep and goat • 6 non-compliant results 5 target samples and 1 suspect sample taken at • Antimicrobials • Muscle slaughter houses screened positive for antimicrobials. The suspect carcass was declared unfit for human consumption. On farm investigations including examination of animal remedies record were carried out in all cases.
Milk • 2 non-compliant results 2 samples screened positive for antimicrobials. On • Antimicrobials farm investigations including examination of • Milk animal remedies record were carried out in both cases. Aquaculture • 2 non-compliant results 2 samples from 2 farms proved positive for Emamectin B1a. Additional sampling took place • Emamectin B1a at both sites with no further positive findings. Following discussions at the Residues Case
Management group attended by The Food Safety • Muscle/Skin Authority of Ireland, the Marine Institute and the Department of Communications, Marine & Natural Resources, both farms will be targeted in 2006 as part of the target surveillance monitoring programme.
EN 153 EN
DETAILS OF NON-COMPLIANT RESULTS – TARGETED SAMPLING
GROUP SUBSTANCE ANIMAL FARM/ NON- CATEGORY/ COMPLIANT RESIDUE SLAUGHTERHOUSE/OTHERS SPECIES
A6 FURAZOLIDONE BOVINE SLAUGHTER 2
B1 ANTIBIOTICS BOVINE SLAUGHTER 7 B1 ANTIBIOTICS PORINE SLAUGHTER 24 B1 ANTIBIOTICS OVINE SLAUGHTER 5 B1 ANTIBIOTICS MILK SLAUGHTER 2
B2b NICARBAZIN POULTRY SLAUGHTER 15
B2b MONENSIN POULTRY SLAUGHTER 1
B2e PHENYLBUTAZONE BOVINE FARM 1
B2a EMAMECTIN B1a FARMED SLAUGHTER HOUSE (i.e. 2 FINFISH processing plant) SUM 59
DETAILS OF NON-COMPLIANT RESULTS – SUSPECT SAMPLING
Ireland 2005
GROUP SUBSTANCE ANIMAL FARM/ NON- CATEGORY/ COMPLIANT RESIDUE SLAUGHTERHOUSE/OTHERS SPECIES
A6 FURAZOLIDONE BOVINE SLAUGHTER 4 B1 ANTIBIOTICS BOVINE SLAUGHTER 28 B1 ANTIBIOTICS PORCINE SLAUGHTER 2 B1 ANTIBIOTICS OVINE SLAUGHTER 1
SUM 35
EN 154 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State ITALIA
Date 26 GIUGNO 2006
Group A substances
modification of national residue aggregate for all animal products and substances plan 2006 proportional increase number of samples for boldenone, corticosteroids, nandrolone, beta-agonists, nitrofurans metabolites, chloramphenicol.
because of scientific uncertainty, removal of samples for nandrolone and boldenone in pigs
non-compliant results follow-up actions
dexamethasone - liver - bovine investigations in the farm of origin: check records - intensification checks; intensified checks in 1 related farm; products declared unfit for human consumption: 1 carcass.
dexamethasone - liver - bovine (5 investigations in the farm of origin: check records samples) - 46 samples - intensification checks; animals held in farms: 102; intensified checks in 2 related farms; products declared unfit for human consumption: 5 carcases.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 50 samples - intensification checks; animals held in farms: 900; intensified checks in 1 related farm; products declared unfit for human consumption: 1 carcass.
dexamethasone - urine - bovine investigations in the farm of origin: check records - 40 samples - intensification checks; animals held in farms: 284; intensified checks in 2 related farms; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 3 samples - intensification checks; animals held in farms: 5; intensified checks in 1 related farm;
EN 155 EN
products declared unfit for human consumption: 1 carcass; denial ec aid: yes.
dexamethasone - liver - bovine investigations in the farm of origin: check records - intensification checks; intensified checks in 1 related farm; products declared unfit for human consumption: 1 carcass; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 20 samples - intensification checks; animals held in farms: 585; intensified checks in 1 related farm; administrative measures: yes; denial ec aid: yes; penal crime; others: 1 carcass impound at slaughterhouse.
dexamethasone - liver - bovine investigations in the farm of origin: check records - intensification checks; animals held in farms: 824; intensified sampling in related farms: 57 samples in 3 farms; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - urine - bovine (3 investigations in the farm of origin: check records samples) - 7 samples - intensification checks; animals held in farms: 42; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - urine - bovine investigations in the farm of origin: check records - 18 samples - intensification checks; animals held in farms: 121; slaughtered animals: 1; penal crime.
dexamethasone - urine - bovine investigations in the farm of origin: check records - 20 samples - intensification checks; animals held in farms: 139; slaughtered animals: 1; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - liver - bovine (5 investigations in the farm of origin: check records samples) - intensification checks; intensified checks in 2 related farms; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - urine - bovine investigations in the farm of origin: check records; animals held in farms: 139; slaughtered animals: 4; intensified checks in 1 related farm; administrative measures: yes; penal crime.
dexamethasone - liver - bovine investigations in the farm of origin: check records
EN 156 EN
- 11 samples - intensification checks; animals held in farms: 393; intensified checks in 1 related farm; administrative measures: yes; denial ec aid: yes; penal crime; others: 1 carcass impound at slaughterhouse.
dexamethasone - urine - bovine investigations in the farm of origin: check records - 8 samples - intensification checks;, animals held in farms: 1; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 21 samples - intensification checks; animals held in farms: 1875; products declared unfit for human consumption: 1 carcass; administrative measures: yes.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 10 samples - intensification checks; animals held in farms: 170; intensified checks in 1 related farm; administrative measures: yes.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 40 samples - intensification checks; animals held in farms: 284; intensified checks in 2 related farms; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - liver - bovine investigations in the farm of origin: check records - samples - intensification checks; animals held in farms: 34; intensified checks in 1 related farms; denial ec aid: yes.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 13 samples - intensification checks.
dexamethasone - urine - bovine investigations in the farm of origin: check records - 13 samples - intensification checks; administrative measures: yes; denial ec aid: yes; penal crime.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 17 samples - intensification checks; animals held in farms: 36; intensification checks in 2 farms; intensified sampling in related farms: 19 samples.
dexamethasone - liver - bovine investigations in the farm of origin: check records - 42 samples - intensification checks; animals held in farms: all; slaughtered animals: no;
EN 157 EN
intensified checks in related farms: 2 farms; administrative measures: yes
dexamethasone - bovine investigations in the farm of origin; products declared unfit for human consumption: 1 carcass; penal crime
dexamethasone - bovine products declared unfit for human consumption: 1 carcass; penal crime
dexamethasone - bovine products declared unfit for human consumption: 1 carcass; administrative measures: yes;
dexamethasone - bovine investigations in the farm of origin: 18 samples
dexamethasone - bovine investigations in the farm of origin: 55 samples; animals held in farms: 127; intensified checks in 3 related farms; 1 carcass impound
dexamethasone - bovine products declared unfit for human consumption: 1 carcass; administrative measures: yes
dexamethasone - bovine investigations in the farm of origin: 8 samples; animals held in farms: 34; intensified checks in 1 related farm; 1 carcass impound
dexamethasone - bovine investigations in the farm of origin: 13 samples; animals held in farms: 115; 1 carcass impound
dexamethasone - bovine investigations in the farm of origin: 105 samples; animals held in farms: 1500; administrative measures: yes
dexamethasone - bovine products declared unfit for human consumption: 1 carcass; administrative measures: yes
dexamethasone - bovine investigations in the farm of origin: 29 samples; animals held in farms: 650; administrative measures: yes
dexamethasone - bovine investigations in the farm of origin: 19 samples; animals held in farms: 77; administrative measures: yes
dexamethasone - bovine products declared unfit for human consumption: 1 carcass; administrative measures: yes
dexamethasone - bovine investigations in the farm of origin: 28 samples; animals held in farms: 984; intensified checks in 1 related farm; products declared unfit for human consumption: 2 carcasses; administrative
EN 158 EN
measures: yes
dexamethasone - bovine investigations in the farm of origin check records - intensification checks; 1 carcass impound; administrative measures: yes
dexamethasone - bovine investigations in the farm of origin: 31 samples; animals held in farms: 280; intensified checks in 1 related farm;
dexamethasone - bovine investigations in the farm of origin: 14 samples; animals held in farms: 7; intensified checks in 1 related farm;
epinandrolone - urine - bovines investigations in the farm of origin: check records - 8 samples - intensification checks; animals held in farms: 3; products declared unfit for human consumption: 1 carcass. unknow n.c. origin
nandrolone - urine - bovines 1 carcass impound - investigation is still carrying out
clenbuterol - eye - bovines investigations in the farm of origin: check records - 12 samples urina - intensification checks; animals held in farms: 16.
clenbuterol - bovines investigations in the farm of origin: 21 samples; animals held in farms: 311; intensified checks in 3 related farms; products declared unfit for human consumption: 33 carcasses; administrative measures: yes'
clenbuterol - bovines investigations in the farm of origin: 184 samples; animals held in farms: 6835; intensified checks in 13 related farms; 33 carcasses impound
clenbuterol - bovines investigations in the farm of origin: 19 samples; animals held in farms: 34; intensified checks in 1 related farm; administrative measures: yes'
clenbuterol - bovines investigations in the farm of origin: 79 samples; animals held in farms: 1295; intensified checks in 5 related farms
clenbuterol - bovines investigations in the farm of origin: check records - 22 samples - intensification checks; animals held in farms: all.
nandrolone - urine - pigs investigations in the farm of origin: check records - intensification checks; animals held in farms: all
EN 159 EN
during investigation. unknown cause of n.c.
nandrolone - urine - pigs investigations in the farm of origin: check records - intensification checks unknown cause of n.c.
nandrolone - urine - pigs investigations in the farm of origin: check records - intensification checks; animals held in farms: all; administrative measures: yes. unknown cause of n.c.
nandrolone - urine - pigs investigations in the farm of origin: check records - 42 samples - intensification checks; animals held in farms: all; intensified checks in 2 related farms; products declared unfit for human consumption: 11722kg. unknown cause of n.c.
aoz - muscle - pigs investigations in the farm of origin: check records - 2 samples - intensification checks; animals held in farms: no; slaughtered animals: 3 separate slaughtering; intensified checks in related farms: 2 farms; products declared unfit for human consumption: 1 carcass.
chloramphenicol - muscle - poultry investigations in the farm of origin: check records - intensification checks
chloramphenicol - drinking water - investigations in the farm of origin: 11 samples; rabbit animals held in farms: 6000
chloramphenicol - rabbit investigations in the farm of origin: 29 samples; animals held in farms: 6000; impound carcasses 4000
chloramphenicol - muscle - investigation is still carrying out aquaculture
aoz muscle + dimetridazol drinking as a consequence of aoz n.c.: investigations in the water farm of origin: check records - intensification checks - 1 sample of drinking water. this sample farmed game was positive for dimetridazol. than: 878 animals held in farm. investigation is still carrying out. penal crime - unknown cause of nc • Information to be included for each non-compliant result. In case of several non- compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 160 EN
Group B substances
modification of national residue aggregate for all animal products and substances plan 2006
samples for: carazolol, azaperon and azaperol in pigs; streptomycin in honey; ionophore coccidiostats in eggs.
proportional increase number of samples for tetracyclines, sulphonamides, nicarbazin, robenidin, ivermectin, tylosin, organophosphorate pesticides, aflatoxines, malachite green, chemical elements.
non-compliant results follow-up actions bovines B1 group intensification checks; products declared unfit for human consumption: 12 carcasses; administrative measures; penal crime
aflatoxin B1 - feed 4 samples; intensification checks; destruction of 250 kg feed
HCH-beta emergency plan after 1 non compliant sample of milk. cause of problem was contamination of water and ground by an old chemical industry
32 bovine farm; 3068 separated slaughtering; distruction of 1000 tons of feed
sheep&goats HCH-beta emergency plan after 1 non compliant sample of milk. cause of problem was contamination of water and ground by an old chemical industry
9 ovine farms; 2480 separated slaughtering distruction of 300 tons of feed
pigs B1 group check records and intensification checks in farm; intensification checks in 3 others farms; products declared unfit for human consumption: 1 carcass; administrative measures
lead - muscle check records; impound 320 animals
poultry B1 group intensification checks; samples; products declared unfit for human consumption: 5280 carcasses;
EN 161 EN
administrative measures milk PCB intensification checks; samples HCH-beta emergency plan after 1 non compliant sample of milk. cause of problem was contamination of water and ground by an old chemical industry
products declared unfit for human consumption: 34264 litree of ovine milk and 1218128 of bovine milk aflatoxin M1 intensification checks; samples; products declared unfit for human consumption: 50 tons of milk, 2 tons of cheeses; penal crime B1 group check records; intensification checks; samples; products declared unfit for human consumption: 8 tons of milk lead samples; impound milk until compliant results penicillin G check records; intensification checks; 1 samples; products declared unfit for human consumption: 8 tons of milk administrative measures eggs robenidin - eggs check records in farm; intensification checks in 1 other farm; products declared unfit for human consumption: 710 hens, 770 eggs administrative measures; nicarbazin - eggs check records in farm; 5 samples; intensification checks; products declared unfit for human consumption: 800kg of eggs. investigation is still carrying out enrofloxacin - eggs check records in farm; 2 samples; intensification checks; aquaculture malachite green cause of non compliance was contamination of water by chemical industry honey tetracyclines check records; samples; products declared unfit for human consumption:100 kg miele; administrative measures; penal crime tylosin check records, intensification checks, unknown cause of nc impound 18 kg of honey penal crime
EN 162 EN
EN 163 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State LATVIA
Date 30.May.2006.
Group A substances
Modification of national residue Aggregate for all animal products and substances plan • Increased the number of samples of horses for A3 group.
• Gas chromatography – mass spectrometry is used for detection of stilbenes both for screening and confirmation purposes.
• The number of substances of group A3 is enlarged with ethynylestradiol, 17 and 17 - trenbolone.
• The number of substances of group A5 is enlarged. The method now includes the following compounds: brombuterol, cimaterol, cimbuterol, clenbuterol, mabuterol, mapenterol, salbutamol, terbutaline.
• The testing for nitroimidazoles includes the following compounds: hydroxydimetridazol, metronidazol, ronidazol, hydroxymetronidazol.
Non-compliant results Follow-up actions
Chloramphenicol - 3,4 µg/kg - 1 farm (60 cows held in the farm) was bovine muscle investigated and the origin of CAP was not identified. Stopping of meat realization till situation will clarified. Additional sampling – 1 feed sample, 1 milk sample.
Chloramphenicol - 0,28 µg/kg - The sample was taken from tank (milk from 6 bovine milk farms – 1351 cows together). The milk products production establishment has to intensify the control of milk from particular farms. Additional sampling – 6 milk samples.
Chloramphenicol* - 4,6 µg/kg - 1 farm (5 cows, 4 calves held in the farm) was bovine milk investigated and the origin of CAP was not identified. Stopping of meat realization till situation will clarified. Additional sampling – 1 milk sample.
EN 164 EN
Chloramphenicol* - 0,88 µg/kg - 1 farm (5 cows held in the farm) was investigated bovine milk and the origin of CAP was not identified. Stopping of meat realization till situation will clarified. Additional sampling – 5 milk samples. Notification through Rapid Alert System for Food and Feed.
Chloramphenicol* - 0,35 µg/kg - 1 farm (1 cows held in the farm) was investigated bovine milk and the origin of CAP was not identified. Stopping of meat realization till situation will clarified. Additional sampling – 1 milk sample.
Chloramphenicol* - 0,36 µg/kg - 1 farm (1 cows held in the farm) was investigated bovine milk and the origin of CAP was not identified. Stopping of meat realization till situation will clarified. Additional sampling – 1 milk sample.
Chloramphenicol* - 0,22 µg/kg - 1 farm (15 cows, 2 calves held in the farm) was bovine milk investigated and the origin of CAP was not identified. Stopping of meat realization till situation will clarified. Additional sampling – 1 feed sample, 1 milk sample.
* Chloramhenicol was found within additional control programme for antibacterial substances (the results are indicated in results table “Others”)
Group B substances
Modification of national residue Aggregate for all animal products and substances plan
• The number of samples of rabbits was a little decreased (group B1) because of low production amount.
• Increased the number of samples of goats for B1 group.
• Included the group B1 for testing horses.
• Increased the number of samples of aquacultures for B1 group.
• The number of substances of group B2a is enlarged with following compounds: abamectine, doramectine, emamectine, moxydextine.
• The testing of nicarbazine with HPLC-MS-MS has been introduced for the B2b group substances.
• The number of substances of group B1 is enlarged with following compounds: ciprofloxacin, enrofloxacin.
EN 165 EN
Non-compliant results Follow-up actions Bovines Lead – 1 cow liver 1 farm (138 cows held in the farm) was investigated. Additional sampling – 1 feed sample, 1 kidney sample, 1 liver sample.
Cadmium – 1 cow kidney 1 farm (2 cows held in the farm) was investigated. Additional sampling – 1 feed sample.
Pigs @
Poultry & @ Sheep and goat & @ Horses & @ Milk & @ Eggs & @ Rabbit & @ Aquaculture & @ Farmed game & @ Wild game & @ Honey & @
EN 166 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State LITHUANIA
Date 10 May 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
More analytes were introduced for A1: DES, dienestriol, hexestrol for all animal species. Confirmatory method is foreseen to implement.
Confirmatory method for A2 will be implemented till October 2006 and then the Community action limit of 100 mg/kg will be satisfied.
Confirmatory method for A3 group is introduced (final implementation this year) for all animal species.
Extended scope of tested beta-agonists A5 group (Orciprenalin, Terbutalin, Salbutamol, Zilpaterol, Cimaterol, Cimbuterol, Fenoterol, Ritodrin, Clencyclohexerol, Clenproperol, Hydroxymethyl-clenbuterol, Ractopamin, Tulobuterol, Clenbuterol, Chlorbrombuterol, Brombuterol, Clenpenterol, Isoxsuprine, Mabuterol, Mapenterol, Salmeterol) for all animal species.
Addition of A5 samples to be tested on farm in poultry. Discussions are going if the legal acts allow taking live poultry samples on the farm.
Non-compliant results Follow-up actions
During additional CAP prevention In 30 cases CAP was detected in milk collection programme in 2005, 62 suspected tanks and additional samples were taken to milk samples (out of 3638 targeted identify certain milk farms. Milk farms were samples taken) were confirmed as identified in 32 cases and milk collection from the CAP positive. farms was suspended for 15 days and after the control of the farms was strengthened for 6 months.
EN 167 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances
General information about the amounts of antimicrobial substances sold in Lithuania in 2005 was added.
Extended scope of tested coccidiostats B2b group (Amprolium, Clopidol, Ternidazol, Secnidazol, Tinidazol, Halofuginon, Cernidazol, Arprinocid, Athopabat, Robenidin, Decoquinat, Lasalocid, Semduramicin, Maduramicin, Laidlomycin, Nitromide, Dinitolimid, DNC, Clazuril, Diclazuril) for all animal species.
Extended scope of tested NSAIDs B2e group (Oxyphenbutazone, Flunixin hydroxide, Flunixin Meglumine, Carprofen, Diclofenac, Niflumic acid, Phenylbutazone, Mefemanic acid, Tolfenamic acid, Vedaprofen, Naproxen, Ibuprofen, Ketoprofen, Meloxicam) for all animal species.
More groups of substances are foreseen to test in sheep and goats.
Samples of slaughtered horses are foreseen to be tested.
More groups of substances are foreseen to test in rabbits.
Samples of farmed game are foreseen to be tested (A5, B1, B2a)
Extended scope of tested sulfonamides in milk (Sulphacetamide, Sulphadiazine, Sulphathiasole, Sulphamerazine, Sulphamethisole, Sulphametasine, Sulphabenzamide, Sulphamethoxasole, Sulphadimethoxine).
The limit for detection of some penicillin’s (ampicillin, benzylpenicillin, amoxycillin) (as it is too high comparing with the MRLs) in milk is going to be revised during the Twinning project, but as the final limits are not validated, the old ones are presented in the Plan.
Confirmatory method (GS-MS) for A3 group in aquaculture is planned to introduce.
Non-compliant results Follow-up actions Bovines 2 cadmium – kidney. 2 farms were investigated. On spot checks showed
EN 168 EN
that no more animals were held in the farms.
Heavy metals, which include lead and cadmium, are found in the environment and if absorbed by animals over a long period of time they may accumulate in animal tissues and be found in animal products.
Milk 17 inhibitors – bovine milk by 17 farms were investigated and the origin of DELVO-SP method antimicrobial substances was identified in 2 cases. 17 positive bovine milk samples 8 additional milk samples were tested and none of were sent to chemistry for them was non-compliant. confirmation. Milk samples usually are taken from milk- CAP, penicillines and collecting points, milk collecting reservoir in sulphonamides were not confirmed farms and milk floats, so it is difficult to identify in any milk sample. exact number of animals held in the farm. In every case administrative warning was made to the milk establishment and the establishment was obliged to prepare plan for elimination of violations. Milk collection from the farms was suspended for 15 days and notifications together with financial measures (fine) were applied. The inspections were intensified in the region of private veterinarians, in working area of which findings were detected.
EN 169 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
To be submitted in June 2006
Member State LUXEMBOURG
Date 31 MayI 2006
Group A substances
Modification of national residue Aggregate for all animal products and substances plan
Non-compliant results Follow-up actions
0 .
* Information to be included for each non-compliant result.
In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated.
Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 170 EN
Group B substances
Modification of national residue Aggregate for all animal products and substances plan Non-compliant results Follow-up actions Bovines &0 @. Pigs &0 @. Poultry & @ Sheep and goat &0 @ Horses & @ Milk &0 @ Eggs &0 @ Rabbit &0 @ Aquaculture & @ Farmed game & @ Wild game &0 @ Honey &0 @
EN 171 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State MALTA Date
Group A substances
Modification of national residue Aggregate for all animal products and substances plan
Non-compliant results Follow-up actions Substance-Concentration-Matrix- animal or animal product*
---
* Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
Group B substances
Modification of national residue Aggregate for all animal products and substances plan
Non-compliant results Follow-up actions Bovines 2 inhibitors – kidney ------1 inhibitor - muscle Additional sampling from establishment; visit on
EN 172 EN
farm of origin. Pigs 1 inhibitor – kidney ------Poultry Investigations on farms of origin; targeted mycin – liver sampling from establishments Sheep and goat
Horses
--- Milk Additional sampling from dairy bitors Eggs 5 inhibitors ------Rabbit
--- Aquaculture
--- Farmed game
Wild game
Honey
---
EN 173 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State THE NETHERLANDS Date 1 June 2006
Group A substances
Modification of national residue Although positive findings for conjugated alfa- plan boldenon are not yet non-compliant from a scientific point of view, sampling for this substance was raised as a result of positive findings and farm investigations.
The production system of farmed fish will be monitored as a result of low positives in fish tissue for beta-oestradiol and trenbolon. Additional sampling of feed for oestradiol analysis introduced to investigate the source of residues of this substance in fish.
Non-compliant results Follow-up actions Carbuterol; 1 non-compliant result; One farm blocked; origin of carbuterol was not urine of veal calf; 0.6 ppb identified Chloramphenicol; 1 non-compliant Investigations on-going; no source for residues result; urine of porcine; 0.3 ppb found Dexamethason; 2 positive results; One farm investigated; findings are related to urine of bovine legal use of dexamethason Beta-oestradiol/trenbolon; 2 non- The whole production system of farmed fish in compliant results; tissue of farmed The Netherlands is investigated in 2005. The use fish; 0.6-0.8 ppb of androgenic compounds to change the sex of young animals was observed. Problem under discussion. AOZ-furazolidone; 1 non-compliant Imported product; next ten deliveries from the result; shrimps same country were sampled.
EN 174 EN
Group B substances
Modification of national residue Sampling for analysis of residues of antibiotics plan increased for porcines and veal-calves because positive findings were observed for tetracyclin residues. Sampling raised for levamisole in pig liver because positive findings were observed.
Non-compliant results Follow-up actions Bovines
- 9 non-compliant results for Nine farm visits; investigation of records; 2 crime- tetracycline residues in muscle penalties; 2 warnings. tissue of veal-calves; 8 for oxytetracyclin and 1 for chlortetracyclin - 25 non-compliant results for cadmium in bovine kidney Eighteen farms investigated; additional sampling of feed and water. No explanation found for the high levels of cadmium. Among the positive tested animals 4 were originating from Belgium. Pigs
- 2 non-compliant results for Two farms visited. In both farms oral levamisol in liver administration of levamisol was observed. However, the withdrawal period was obeyed.
- 1 non-compliant result for Farm visited. Records were adequate. Withdrawal sulfadimidine time obeyed.
- 11 non-compliant results for tetracyclins (7 oxytetracyclin ; 4 Five farms visited. Investigation of records. Three doxycyclin) warnings for farmers. Poultry
- 3 non-compliant results for One farm visited. Investigations of records. No deviations observed. Results of investigations in doxycyclin two other farms not yet reported.
Two farms investigated. No special findings. - 2 non-compliant results for
ium-salycilate Sheep and goat
EN 175 EN
- 1 non-compliant result for Results of farm investigations unknown ivermectin Horses
Milk None Eggs None Rabbit
- 2 non-compliant results for One farm visited. Investigations of records. No natrium-salycilate deviations observed. Aquaculture
Farmed game None Wild game - 7 non-compliant results for No action. Traceability impossible. cadmium in kidney of wild deer. Furthermore high levels for lead and cadmium were observed in kidneys from wild ducks (3 x) and hares (3 x).
Honey None
EN 176 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State POLAND Date May 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
Increased number of samples for: • A3 Steroids in pigs • A6 Chloramphenicol in pigs Increased of testing for: • A3 Steroids: Stanozolol in urine of bovines and Chlormadinonacetat, Megestrolacetate in fat of bovines and pigs • A5 Beta – agonists: Mapenterol in drinking water, urine and liver of bovines, pigs, poultry, sheep/goats, horses and rabbit • A6 Hydroxymetabolites of nitroimidazoles (HMMNI, MNZOH) in eggs and in plasma and muscle of bovines, pigs, sheep/goats, horses, poultry and rabbit
Non-compliant results Follow-up actions 3 – A3 Nandrolone – 3 investigations in the farm of origin, verification of records, additional sampling, origin of 23,2 ppb – urine - pig Nandrolone was not identified, 52,5 ppb – urine - pig in all cases animals were held until the results of 54,0 ppb – urine - pig additional analysis were available (462 pigs), 3 farms subject to intensified checks, 3 administrative decisions 2 – A6 Chloramphenicol – 1 investigation in the farm of origin, additional sampling, origin of CAP was not identified, 4,7 ppb - muscle - pig animals were held until the results of additional 2,1 ppb - honey (import) analysis were available, 1 farm subject to intensified checks, 1 administrative decision * Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 177 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances Increased number of samples for: • B1 Sulfonamides in honey • B2b Lasalocid in poultry • B2f Dexamethasone in bovines • B3e Malachite and leucomalachite green in fish Increased of testing for: • B2a Anthelmintics – Macrocyclic lactones (Abamectin, Doramectin, Eprinomectin, Moxidectin, Ivermectin) in liver of bovines, pigs, sheep/goats, horses, poultry and rabbit, in muscle of fish and in milk • B2a Anthelmintics – Benzimidazoles (Albendazol, Cambendazol, Fenbendazol, Flubendazol, Mebendazol, Oxfendazol, Thiabendazol, Triclabendazol) in liver of bovines, pigs, sheep/goats, horses, poultry and in milk • B2e Non-steroidal anti-inflammatory drugs, NSAIDs (Antipyrin-4-Methylamino, Carprofen, Diclofenac, Flunixin, Meloxicam, Oxyphenbutazon-Monohydrat, Phenylbutazone, Tolfenamic acid, Vedaprofen) in plasma and liver of bovines, pigs and horses, plasma of sheep/goats, liver of poultry and rabbit and in milk • B2f Corticosteroids (Betamethasone, Dexamethasone, Flumethasone, Prednisolone, Triamcinolonacetonid) in liver of bovines, pigs and horses Non-compliant results Follow-up actions Bovines 8 – Antibacterials–muscle+kidney 14 investigations in the farm of origin, verification of records, additional sampling, 1 – Dexametasone - liver in all cases animals were held until the results of 5 – Cadmium - liver additional analysis were available, carcasses declare unfit for human consumption (300 kg), 14 administrative measures Pigs 7 – Antibacterials–muscle+kidney 23 investigations in the farm of origin, verification of records, additional sampling, 12 – Cadmium - liver 72 animals held in the farm until the results of 6 – Lead - liver additional analysis were available, 2 - Ochratoxin A - kidney 6 intensified checks on the animals from the farm in the event of repeated infringements, carcasses from 33 pigs declare unfit for human consumption, 27 administrative measures
EN 178 EN
Poultry 3 – Antibacterials - muscle + liver 6 investigations in the farm of origin, verification of records, additional sampling, 1 – Lazalocyd – liver in all cases animals were held until the results of 1 – Lead – muscle additional analysis were available (6700 ducks), 1 – Cadmium – liver 6 administrative measures Sheep and goat & @ Horses & @ Milk 9 – Antibacterials – milk 9 investigations in the farm of origin, verification of records, additional sampling, 9 administrative measures Eggs 6 – Lazalocyd - eggs 6 investigations in the farm of origin, verification of records, additional sampling, in all cases animals were held until the results of additional analysis were available, 3 intensified checks on the animals from the farm in the event of repeated infringements, products held (1798 kg), products declare unfit for human consumption (1868 kg), 6 administrative measures Rabbit & @ Aquaculture 1 – Antibacterials – muscle (fish) 10 investigations in the farm of origin, verification of records, additional sampling, 10–Malachite green–muscle (fish) animals held in the farm until the results of additional analysis were available (about 46000 kg of carp or trout), 5 intensified checks on the animals from the farm in the event of repeated infringements, 11 administrative measures
EN 179 EN
Farmed game & @ Wild game 7 – Cadmium – liver investigations, verification of records, additional sampling, 1 – Mercury - liver carcasses declare unfit for human consumption (2545 kg), 8 administrative measures Honey 5 – Sulfonamides - honey 5 investigations in the farm of origin, verification of records, additional sampling, products held (190 kg), products declare unfit for human consumption (100 kg), 4 administrative measures
EN 180 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State PORTUGAL Date 2 June 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances Horses There were only two samples in 2005, that’s why we have decided do increase the total number of samples in 2006.
Our annual production is too low (on average 1500 animals per year)
They couldn’t collect samples because the visit to the slaughterhouses had not coincided with slaughter of the horses.
Poultry
Significant increase in the collection of samples of ducks. For the
fulfilment of Directive 96/23/CE 29 of April chapter 2 of Annex IV,
if the annual production is superior than 5 000 tons, than a minimum of 100 samples for each group of substances must be collected.
Our production of ducks was 6148 tons.
Aquaculture
A significant increase in the number of collection of samples due to suspicion, of illegal substance use.
Plan of Laboratorial Execution
Reduction of the limits of detection in the groups A3 and A4.
EN 181 EN
Non-compliant results Follow-up actions Substance-Concentration-Matrix-animal or animal product*
Example: MPA-3 ppb-kidney fat-pig Other actions: (investigations in the farm of origin, animals held in farms, slaughtered animals, intensified sampling in related farms, products declared unfit for human consumption, administrative measures, denial EC aid, others). Substance Matrix Specie Follow-up actions Held in farms Additional sampling Non-compliant results Slaughtered animals/ Carcasses unfit for human consumption Administrative measures Denial EC aid Clenbuterol (A5) Urine Bovine Yes Yes 1- water 0 Criminal Process Yes Clenbuterol (A5) Liver Bovine Yes Yes 1-urine 1/1 Criminal Process Yes Clenbuterol (A5) Liver+ urine Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) 2 Livers Pig Yes Yes No 0 Criminal Process Not applicable Clenbuterol (A5) 2 Livers Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) Liver Sheep/Goats Yes Yes No 0 Criminal Process Not applicable Clenbuterol (A5) Urine+ water Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) 2 urines Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) Water Sheep/Goats Yes Yes No 0 Criminal Process Not applicable Clenbuterol (A5) Urine Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) Liver Sheep/Goats Yes Clenbuterol (A5) Liver Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) 2 urines Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) Liver Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) 2 urines Pig Yes Yes No 12/0 Criminal Process Not applicable Clenbuterol (A5) Liver Pig Yes Yes No 12/0 Criminal Process Not applicable Clenbuterol (A5) 3 Livers Bovine Yes Yes No 12/4 Criminal Process Yes
EN 182 EN
Clenbuterol (A5) Liver Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) 3 Urines Pig Yes Yes No 33/2 Criminal Process Not applicable Clenbuterol (A5) Liver Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) Liver Bovine Yes Yes No 0 Criminal Process Yes Clenbuterol (A5) Liver Bovine Yes Yes No 0 Criminal Process Yes
* Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 183 EN
Group B substances
Modification of national residue Aggregate for all animal products and substances plan Horses
Significant increase in the collection for the same reasons pointed in
the Group A. The increase is still more significant in the B3c group
because we conducting a study concerning the presence of cadmium in
liver and muscle of horses.
Poultry
Significant increase in the collection for the same reasons pointed out in Group A.
Products of Aquaculture
Significant increase in the collection for the
same reasons pointed out in Group A.
Plan of Laboratorial Execution
The inclusion of new substances to search in the groups B1, B2a, B2e and B3a.
Establishment of limits of detection for the B2b group.
Non-compliant results Follow-up actions Bovines Non-compliant results Substance Matrix Administrative measures 1 Tylosin (B1) Muscle Miss minor Process with the payment of a fine 1 Sulfamethazine (B1) Muscle Miss minor Process with the payment of a fine
& Number of non-compliant @ List actions: (investigations in the farm of results-substance (if possible origin: verification of records, additional matrix) sampling; animals held in the farm, iintensified checks on the animals and products from the farm/establishment in the event of repeated Example: 2 difloxacin-kidney infringements, carcasses and products declare
EN 184 EN
unfit for human consumption, administrative measures, others). Pigs Non-compliant results Substance Matrix Administrative measures 4 Sulfamethazine (B1) Muscle Miss minor Process with the payment of a fine 3 Sulfadimethoxin (B1) Muscle Miss minor Process with the payment of a fine 2 Sulfadiazine (B1) Muscle Miss minor Process with the payment of a fine
& Number of non-compliant @ List actions: (investigations in the farm of results-substance (if possible origin: verification of records, additional matrix) sampling; animals held in the farm, intensified checks on the animals and products from the farm/establishment in the event of repeated infringements, carcasses and products declare unfit for human consumption, administrative measures, others). Poultry Non-compliant results Substance Matrix Held in farms Administrative measures 2 Enrofloxacin (B1) Muscle 0 Miss minor Process with the payment of a fine 2 Olaquindox (B2f) Liver 2 Miss minor Process with the payment of a fine 1 Oxytetracyclin (B1) Muscle 0 Miss minor Process with the payment of a fine 1 Sulfadiazine (B1) Muscle 0 Miss minor Process with the payment of a fine 2 Sulfaquinoxaline (B1) Muscle 0 Miss minor Process with the payment of a fine
& @
Sheep and goat Non-compliant results Substance Matrix Administrative measures 5 Sulfadiazine (B1) Muscle Miss minor Process with the payment
EN 185 EN
of a fine
Horses & @
Milk & @
Eggs Non-compliant results Substance Matrix Administrative measures 6 Sulfadiazine (B1) Eggs Miss minor Process with the payment of a fine 1 Doxycyclin (B1) Eggs Miss minor Process with the payment of a fine
& @ Rabbit & @ Aquaculture & @ Farmed game & @ Wild game & @ Honey & @
EN 186 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State SLOVAK REPUBLIC Date For the year 2005. May 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances At the check of the prohibited substances (Group A3) we introduced the control of methyltestosteron and ethinylestradiol in the urine of live and slaughtered cows by the ELISA method; At the check of the prohibited substances (Group A5) we introduced the control of beta-agonists – mabuterol, brombuterol, cimaterol, cimbuterol, mapenterol by the ELISA method and confirmatory GC/MS method (ISCVBM Brno) in urine and liver of the bovine, ovine and pigs;
Non-compliant results Follow-up actions 1- Chloramphenicol - Poultry – 1 farm of the origin of the broilers was broilers - muscle investigated, however the origin of chloramphenicol was not identified; 172 000 broilers were in 7 halls; District Veterinary and Food Administration imposed to the producer of broilers to examine sample for the presence of residues of chloramphenicol on his own costs; The respective District Veterinary and Food Administration ordered the following measures: – ban to move animals from the farm and to the farm, – ban to sell and to distribute broilers, – DVFA ordered the sampling of suspect samples of broilers, drinking water and feedingstuffs, – the respective DVFA performed the control of the book of veterinary interventions, – DVFA made sampling of the suspect samples: i.4 samples of broilers were compliant, ii. 1 sample of drinking water (own well), which was compliant, iii. 4 suspect samples of feedingstuffs were compliant;
EN 187 EN
The penalty was not imposed to the producer of broilers, because there were no proofs of illegal treatment. 1 - Chloramphenicol - Poultry – 1 farm of the origin of the broilers was broilers - muscle investigated, however the origin of chloramphenicol was not identified; 20 678 broilers were in 2 halls; Strict control of broilers was imposed to the producer of broilers – to examine broilers for the presence of residues of chloramphenicol once a month during the period of 12 month. – the respective DVFA performed the control of the book of veterinary interventions, The respective District Veterinary and Food Administration ordered the following measures: - strict control of broilers was imposed to the producer of broilers – to examine broilers for the presence of residues of chloramphenicol once a month during the period of 12 month, The penalty was not imposed to the producer of broilers, because there were no proofs of illegal treatment. 1 - Chloramphenicol - Raw cow’s 1 bovine farm of the origin of the raw cow’s milk milk was investigated, however the origin of chloramphenicol was not identified; On the farm, there were 99 cows and 10 calves at the time of positive finding; Strict control of raw cow’s milk was imposed to the producer of cows – to examine raw cow’s milk for the presence of residues of chloramphenicol once a month during the period of 5 month. – the respective DVFA performed the control of the book of veterinary interventions, – DVFA ordered the sampling of suspect samples of raw cow’s milk, i. 1 sample of raw cow’s milk, which was compliant - to designate a person responsible for drug dispensation from the store under the supervision of a private veterinarian. The penalty was not imposed to the producer of raw cow’s milk, because there were no proofs of illegal treatment.
EN 188 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances At the check of antibacterial substances (Group B 2a) we extended the scale of the analyzed antihelmintics by doramectine in the liver of slaughtered animals of bovine and ovine;
At the check of coccidiostatics (Group B 2b) we extended the control of coccidiostatics by the control of residues of narazin in the muscle of poultry; we extended the control of coccidiostatics by the control of residues of nicarbazin in the liver of poultry; we extended the control of coccidiostatics by the control of residues of narazin in the eggs;
At the check of carbamates (Group B 2e) we extended the National Plan by the control of diclofenac and vedaprofen in the muscle of bovine, ovine and pigs by the GC/MS methods; we extended the National Plan by the control of vedaprofen in the muscle of horses by the GC/MS methods.
At the check of antibacterial substances (Group B 1) we extended the scale of the analyzed antibiotics by tilmicosin and lincomycin in the muscles of slaughtered pigs and poultry by the LC/MS/MS methods;
On the basis of the production data of raw materials, we made the following changes in the National Plan of Residue Control in Live Animals and Animal Products in the Slovak Republic for the Year 2006: we have planed to increase the number of targeting samples from rabbits and broiler chickens; we have increased targeted samplings of honey for the Group B1.
We made modifications and extensions in the National Plan for the Slovak Republic for the year 2006 in compliance with the requirements of the valid EU legislation as well as according to the comments of EU experts and actual situation in the Slovak Republic.
Non-compliant results Follow-up actions Bovines 1 - Dihydrostreptomycine, 1 farm of bovine; additional sampling: on 1 farm, benzylpeniciline – kidney- fatting 6 suspect samples were taken; bovine
EN 189 EN
On the farm there were 767 bovines; For the reason of the occurrence of residues of Dihydrostreptomycine, benzylpeniciline in bovine the respective veterinary administration authority prohibited the movement of animals; District Veterinary and Food Administration (DVFA) ordered the below-mentioned measures to farmers. - to stop the movements of animals to slaughterhouse; - penalties 10 000 SKK,-; - keeping of precise recording about used veterinary drugs and withdrawal periods in the register according to § 10, para 3 of the Ordinance of the Government of the Slovak Republic No. 320/2003 Coll. As amendment; - to buy veterinary drugs only according to § 57, para 1 of Act on Medicinal Products and Medical Devices No. 140/1998 Coll. - to perform sampling of suspect samples of muscle, liver and kidney of bovine;
1 – Tetracycline – liver –cow 1 farm of bovine; additional sampling: on 1 farm, 2 suspect samples were taken; 1 – Tetracycline – kidney -cow On the farm there were 601 bovines; DVFA ordered the below-mentioned measures to farmers.
– all drugs administered to animals shall be recorded in the book of veterinary intervention and in the register; – to make sampling of suspect samples by the DVFA; – to increase the pharmaceutical controls by veterinary inspectors of DVFA during next six months;
1 – Oxytetracycline – kidney - 1 farm of bovine; additional sampling: on 1 farm, calf 1 suspect samples was taken; On the farm there were 406 calves; Findings of residues of Oxytetracycline in calf’s kidney – exclusion of kidneys from human
EN 190 EN
consumption; DVFA ordered the below-mentioned measures to farmers. – to take the suspect samples;
2 – Cd – kidney - cows 2 farms of bovine; additional sampling: on 2 farm, 5 suspect samples were taken;
On the 1st farm there were 765 bovines, On the 2nd farm there were 370 cows; – DVFA prohibited to slaughter animals till the results from the analyses of suspect samples are negative; – to make sampling of suspect samples of kidney, feedingstuffs and drinking water by the DVFA; – DVFA will include the farm in question into the monitoring “veterinary prevention and protection” in the year 2006;
1 - Fe – in the drinking water for 1 farm of bovine, additional sampling: on 1 farm; bovine 1 suspect sample of drinking water was taken; DVFA ordered the below-mentioned measures to farmers. – to make sampling of suspect samples;
Pigs 1 - Antibacterial substances 1 pig farm; additional sampling: on 1 farm, 3 (inhibitors) – kidney - pig suspect samples were taken; On the farm there were 380 pigs; For the reason of the occurrence of residues of inhibitory substances in pigs the obligation was imposed to the person responsible for animals to notify the respective veterinary administration authority the movement of animals to a slaughterhouse 1 day before for the purpose of taking the suspect samples for residues of inhibitory substances and for the purpose of more intensive control till the confirmatory results of the examination will be known; DVFA ordered the below-mentioned measures to farmers. – to mark animals, that will be sent to the slaughterhouse for the purpose of taking
EN 191 EN
suspects official samples; – to make repeated samplings; 1 - Chlorpyrifos-methyl in the 1 pig farm, additional sampling: on 1 farm; 3 feedingstuffs for pigs suspect samples of feedingstuffs were taken; Feedingstuffs for pigs DVFA ordered the below-mentioned measures to farmers. – to make sampling of suspect samples by the DVFA;
1 - Fe – in the drinking water for 1 pig farm, additional sampling: on 1 farm; 3 pigs suspect samples of drinking water were taken;
1 - DON – in the feedingstuffs for 1 pig farm, additional sampling: on 1 farm; 2 pigs suspect samples of feedingstuffs were taken; DVFA ordered the below-mentioned measures to farmers. – to make sampling of suspect samples by the DVFA ; – Repeated sampling was performed by the respective veterinary administration authority;
Poultry 1 - Fe – in the drinking water for 1 farm of poultry, additional sampling: on 1 farm; poultry 1 suspect sample of drinking water was taken. Drinking water for poultry DVFA ordered the below-mentioned measures to farmers. – to make sampling of suspect samples; – farmer will ensure reconstruction of a piping system for a water intended for animals
Sheep and goat 1 - Antibacterial substances 1 mountain establishment; additional sampling: on (inhibitors) - liver - sheep 1 mountain establishment, 3 suspect samples were taken; 1 - Antibacterial substances (inhibitors) - muscle - sheep On mountain establishment there were 332 sheep; For the reason of the occurrence of residues of
EN 192 EN
inhibitory substances in sheep the respective veterinary administration authority prohibited the movement of animals till the confirmatory results of the examination will be known; DVFA ordered the below-mentioned measures to farmers. – to observe the withdrawal periods of veterinary medical products by private veterinary doctors; – pharmaceutical control was carried out;
Horses No No Milk No No Eggs No No Rabbit 1 – Enrofloxacine – muscle - 1 rabbit farm; additional sampling: on 1 farm, 1 rabbit suspect samples was taken; DVFA ordered the below-mentioned measures to farmers. – to take the suspect samples; – to stop the movements of animals to slaughterhouse;
Aquaculture 1 - Malachite green - muscle 1 farm of aquaculture, additional sampling: on 1 aquaculture farm of aquaculture, 4 suspect samples were taken;
84,4 kg of frozen trout that was produced from a fishpond with a positive finding of malachite green; The respective veterinary administration authority ordered to safely dispose 84,4 kg of frozen trout that was produced from a fishpond with a positive finding of malachite green; Aquaculture- trout DVFA ordered the below-mentioned measures to farmers.
EN 193 EN
– to make sampling of suspect samples by the DVFA – The respective veterinary administration authority ordered to safely dispose 84,4 kg of frozen trout that was produced from a fishpond with a positive finding of malachite green – The owner shall submit the document on a safe disposal of the product
Farmed game No No Wild game 1 – Pb – muscle - deer 2 wild games; additional sampling: 0; 1 – Pb – muscle - wild sow Deer – the respective DVFA will perform the
repeated sampling from the said hunting association at the next shooting; – to place eviscerated deer in game collection centre until obtaining laboratory results wild sow – to make sampling of suspect samples by the DVFA during the next shooting; – ban on meat consumption until obtaining laboratory results – to safely dispose internal organs from hunted animals Honey 9 - Tylosine, Sulphadimidine, 7 producers of honey; additional sampling: in 2 Sulphatiazole - honey producers; 2 suspect sample were taken; 7 producers of honey; 523 kg of honey were declared as unfit for human consumption; 1085 kg of honey were suspended till the examination results from the State Veterinary and Food Institute were known; Honey – to stop the honey in amount of 523 kg for human consumption for the reason of findings of tylosine sulfadimidine, sulfatiazole residues; DVFA ordered the below-mentioned measures to farmers. – to stop the honey in amount of 523 kg for human consumption for the reason of findings of tylosine sulphadimidine,
EN 194 EN
sulphatiazole residues; – to withdraw honey from the shops and stores by DVFAs; – ban on placing the raw honey in question on the market, its movement and distribution – DVFA ordered to the owner to ensure at his/her own costs an analysis of the honey for antibiotic residues – DVFA ordered to suspend 1085 kg of honey until the time of delivery of the result from the SVFI
EN 195 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State SLOVENIA Date 12 June 2006
Group A substances
Modification of national residue Aggregate for all animal products and substances plan A1 : Aquaculture excluded. A3 : New substances : Androstadiendion, androstenediol, alfa-boldenon, 17 alfa metiltestosteron, epitestosteron, equilin, 17 alfa – etilinestradiol,medroxyprogesteron, metiltestosteron, norandrostenedion, progesteron, stanozolol, trenbolon acetate – matrix musculature. For A3 substances excluded matrices : plasma, fat, kidney. No aquaculture included. A4 : Taleranol ( beta – tearalanol) – matrix urine, kidney, potable water and feed. A5 : Bametan, isoxsuprin, ritodrin – matrix liver. Excluded combination of matrices : eye+liver; matrix is only liver. A6 : Nitrofurans – matrix honey. Excluded matrices : urine, milk and eggs. A6: Dapson : Aquaculture excluded. A6: Colhicin : excluded. A6: Diaminodiphenylsulphon : excluded. Ostriches have been excluded from the monitoring plan as at present there is no approved ostrich slaughter establishment in Slovenia. Non-compliant results 0 Follow-up actions 0 Substance-Concentration-Matrix- Other actions: animal or animal product*
0 0 * Information to be included for each non-compliant result. In case of several non- compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 196 EN
Group B substances
Modification of national residue Aggregate for all animal products and substances plan B2e (NSAID) : New substances included ( matrix milk) :acetilsalicilic acid, flunixin, flunixin – 5 hidroxy, mefenaminic acid, nifluminic acid, salicylic acid, vedaprofen. As matrix excluded from the plan : liver. As substance excluded from the plan : sodiumsalicylat. B3b : Added new substances : chlorpiryfos, chlorpiryfos metil and pirimyfos metal. B3c : Honey excluded. B3d : Aquaculture excluded. Bivalve molluscs have been included in the monitoring plan, under the analyses for heavy metals (lead, cadmium and mercury). Ostriches have been excluded from the monitoring plan as at present there is no approved ostrich slaughter establishment in Slovenia. Non-compliant results Follow-up actions Bovines & 2 CADMIUM ( 2.070 mg/kg, @ 1 (one) investigation on the farm of origin 1.11 mg/kg) – kidney old bovine Pigs & 0 @ List actions: 0 Poultry & @ 3 ANTICOCCIDIALS : Ad 1. ) Amprolium :Investigation at animal owner, at slaughterhouse, at the veterinary organisation. 1.) 1 Amprolium Resampling : 4 samples ( 1 sample of poultry liver, (0.330 mg/kg) – liver broilers 1 sample of potable water, 1 sample of corn, 1 sample of compound feed bro-f - negative for amprolium). Analyses were performing on amprolium – all negative. One administrative measure - the customer was admonished on the basis of a decision issued within the violations procedure.
Ad 2.) Lasalocid 46 µg/kg : Investigation at slaughterhouse, in a feed mill, and at animal keeper. Resampling : 1 sample (result: 190 μg/kg
of lasalocid). Declare unfit for human 2.) 2 Lasalocid consumption : 511 kg of poultry meat. One (400µg/kg,46 µg/kg) – liver administrative measure was issued to customer.
EN 197 EN
broilers Lasalocid 400 µg/kg : Investigation at : animal keeper. OV asked for opinion an expert of the VF,
NVI. Resampling : 1 sample (poultry liver - negative result).
Ad 3.) /
3.) 1 CADMIUM (1.44 mg/kg) - kidney hens Sheep and goat & 0 @ 0 Horses & 0 @ 0 Milk & @ 1.) 3 SALICILTES Ad 1.) In all three cases there was investigation at (0.011 mg/kg, 0.071 mg/kg, 0.011 the farm of origin. Only in one case there was one mg/kg) - cow milk administrative measure ( oral admonition). Ad 2.) In both two cases was investigation at the
farm of origin. Because it was repeated 2.) 2 SALICILATES infringement at the same owner, the official vet (0.071 mg/kg, 0.013 mg/kg) did the intensified check. According to findings off. vet gave the customer an administrative - sheep milk measure.
Eggs & @ 2 LASALOCID 1.)Lasalocid 470 µg/kg : Investigation at animal (470 µg/kg, < 25 µg/kg) – hen eggs owner. Resampling : 1 sample of feed – negative result. 2.)Lasalocid < 25 µg/kg) : Investigation at animal owner and in a feed mill. Resampling : 1 sample of feed – negative result. According to findings off. vet gave the customer an administrative measure. Rabbit
EN 198 EN
& 0 @ 0 Aquaculture & @ 1 MERCURY Non-compliant result from monitoring on BIP ( 1.2 mg/kg) Jelšane ! Resampling : 6 samples. All results were negative. - muscule freshwater sea finfish Farmed game & 0 @ 0 Wild game & @ 3 LEAD In all three cases there was an investigation at the (1.51 mg/kg, 0.92 mg/kg, 1.92 wild game processing house. No additional mg/kg) - musculature wild game samples were taken. In one case 3 kg declare unfit for human consumption. Honey & @ 2 SULPHAMONOMETHOXIN In both two cases there was an investigation at the animal owner and at the honey processing (15 µg/kg, 21 µg/kg) – honey bees establishment. Resampling : in one case they were taken 3 samples – all three non-compliant, in the other case 1 sample was taken – result non – compliant. Together there was declare unfit for human consumption : 2.368 kg of honey. Other measures : trade in honey was banned, and the honey processing establishment was notified thereof (honey was returned to the owner).
EN 199 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State SPAIN
Date September 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
Los cambios que se han introducido en el plan 2006 con respecto al plan 2005 son los siguientes: • Inclusión dentro del grupo A5 de nuevas sustancias a investigar como raptopamina e isoxupruina. • Iniciación de la investigación dentro del grupo B1 de compuestos B-lactamicos (amoxicilina y amplicilina) y Cefalosporinas (ceftiofur y cefalexina) en bovino, porcino y ovino. • Inclusión dentro del grupo de las quinolonas de nuevas sustancias como flumequina y acido oxolínico. • Inclusión para investigar ciertas sustancias del grupo B2b (diclazuril, monensina, narasina, nicarbacina y salinomicina) en especies distintas a avicultura, conejos y huevos. • Iniciación de la investigación de otras sustancias del grupo B2b (halofuginona, maduramicina, robenidina y toltrazuril) en especies distintas de animales y en huevos. • Ampliación de la investigación de la ocratoxina A en especies distintas del porcino.
Non-compliant results Follow-up actions
Substance-Concentration- Other actions: (investigations in the farm of Matrixanimal origin, animals held in farms, slaughtered animals, intensified sampling in related farms, or animal product* products declared unfit for human consumption, administrative measures, denial EC aid, others). Example: MPA-3 ppb-k idney fat- pig GRUPO A6
SEM-0,76 ppb-Musculo-ovino Actuaciones Conselleria de Agricultura, Pesca y AHD Y AMOZ- 0,58 Y 0,16 ppb- Alimentación: • comunicación interesado Músculo-ovino • inmovilización explotación
EN 200 EN
7AHD-1,28; 0,73; 0,77; 0,98; 0,97; • toma de 4 muestras agua y 10 de pienso resultado negativo 1,24; 0,75 ppb- músculo-ovino • inspección explotación y libro de registro • adopción de medidas cautelares • adopción de medidas cautelares a explotación nº ES120400000140 por compartir medios de producción • remisión animales a matadero restringida • levantamiento inmovilización cautelar
Actuaciones de Conselleria de Sanidad: • Inclusión Red de alerta
• sacrificio de lote representativo de 8 ovinos, con intervención en matadero • decomiso de las 8 canales positivas. • Mantenido en Red de Alerta durante tres meses
• exclusión de Red de Alerta hasta completar investigaciones.
Actuaciones de Conselleria de Sanidad: • Inclusión Red de alerta. • Exclusión de Red de Alerta por resultados analíticos de contradictorio y dirimente negativos • Comunicación del expediente a la CCAA de
origen AHD-0,32 ppb- músculo-ovino
Actuaciones de Conselleria de Sanidad:
1. Inclusión Red de alerta.
2. Mantenido en Red de Alerta durante tres meses y exclusión de Red de Alerta hasta completar investigaciones. Comunicación del expediente a la CCAA de origen
Actuaciones Conselleria de Agricultura, Pesca y Alimentación: AHD- 0,64 ppb-músculo-porcino 1. comunicación interesado 2. inmovilización explotación 3. toma de 2 muestra agua y 3 de pienso resultado negativo 4. inspección explotación y libro de registro
EN 201 EN
5. Investigación fabrica de piensos 2AHD-2,17;0,57 ppb-músculo-aves 6. Remisión a sacrificio muestra animales toma de muestras de músculo resultado negativo 7. Levantamiento de la inmovilización
Actuaciones de Conselleria de Sanidad: 1. Inclusión Red de alerta, 2. sacrificio de lotes representativos, 8 muestras en plan de sospechosos. 1 positiva al inicial. Contradictorio y dirimente negativo 3. Mantenido en Red de Alerta durante tres meses y exclusión de Red de Alerta hasta completar investigaciones.
Actuaciones Conselleria de Agricultura, Pesca y Alimentación: 1. comunicación interesado 2. inmovilización explotación 3. toma de 1 muestra de agua y 1 de pienso resultado negativo 4. inspección explotación y libro de registro 5. Investigación fabrica de piensos 6. Remisión a sacrificio muestra animales toma de muestras de músculo resultado negativo
7. Levantamiento de la inmovilización 2 AHD-1,05;2,6 ppb-músculo- equino Actuaciones de Conselleria de Sanidad: 1. Inclusión Red de alerta, 2. sacrificio de lotes representativos, 2 canales intervenidas, 2 muestras en plan de sospechosos. 1 muestra positiva al análisis inicial. Decomiso de la canal por este positivo y por deterioro de la canal. Contradictorio y
dirimente negativo
Mantenido en Red de Alerta durante tres meses y exclusión de Red de Alerta hasta completar investigaciones.
Actuaciones Conselleria de Agricultura, Pesca y
EN 202 EN
Alimentación: • omunicación interesado • inmovilización explotación • toma de 1 muestra de agua y 4 de pienso resultado negativo
• inspección explotación y libro de registro • Análisis contradictorio y dirimente negativo • Levantamiento de la inmovilización
Actuaciones de Conselleria de Sanidad: • nclusión Red de alerta, • sacrificio de lotes representativos, 4 muestras
en plan de sospechosos, con resultado negativo.El ejemplar contradictorio y dirimente negativos. • Exclusión de Red de Alerta por resultados AHD 0,55 ppb-músculo-aves analíticos negativos.
Actuaciones Conselleria de Agricultura, Pesca y Alimentación:
1. comunicación interesado
2. inmovilización explotación
3. toma de 2 muestras de agua y 3 de pienso resultado negativo 4. inspección explotación y libro de registro 5. Investigación fabrica de piensos 6. Remisión a sacrificio muestra animales toma de muestras de músculo resultado positivo 7. sacrificio de todos los animales presentes en explotación por bienestar animal y congelación
de las canales
8. Análisis contradictorio y dirimente negativo
9. Levantamiento de la inmovilización
Actuaciones de Conselleria de Sanidad: (1) Inclusión Red de alerta, (2) sacrificio de lotes representativos, 16 muestras en plan de sospechosos. 3 muestras positivas al analisis inicial a diferentes 2AHD-0,53;0,61 ppb-músculo-aves metabolitos de nitrofuranos. Contradictorio y dirimente negativos. AMOZ-0,58 ppb-músculo-aves
EN 203 EN
AOZ-0,79 ppb-músculo-aves Mantenido en Red de Alerta durante tres meses y exclusión de Red de Alerta hasta completar investigaciones.
Actuaciones Conselleria de Agricultura, Pesca y Alimentación: • omunicación interesado • inmovilización explotación
• inspección explotación y libro de registro • toma de 1 muestras de agua y 3 de pienso en • explotación • resultado negativo toma de muestras en explotación • Investigación fabrica de piensos • Toma de 10 muestras de pienso en fabrica • Resultado negativo en fabrica de piensos • Análisis contradictorio negativo • dirimente positivo SEM • Levantamiento de la inmovilización
Actuaciones de Conselleria de Sanidad:
• Inclusión Red de alerta, • sacrificio de lotes representativos, 23 muestras en plan de sospechosos:1 muestra positiva a SEM en el análisis dirimente, 3 muestras positivas al dirimente (Inicial, contradictorio y dirimente en el mismo acto). El resto de dirimentes (4) fueron negativos
• animales decomisados por partida con resultado SEM Y AHD- 1,28 Y 0,9 ppb- positivo al inicial. Dirimente negativo. músculoconejo • 22 animales con sacrificio, intervención y SEM Y AHD- 0,57 Y 0,55 decomiso por inicial, contradictorio y dirimente ppbmúsculo- positivos en el mismo acto • Mantenido en Red de Alerta durante cinco conejo meses y exclusión de Red de Alerta hasta 2 SEM- 0,65; 0,58 ppb-músculo- completar investigaciones. conejo 4AHD- 1,44:0,77;1,24;0,62ppbmúsculo-
conejo
EN 204 EN
Actuaciones de Conselleria de Sanidad:
Inclusión Red de alerta, • 13 muestras en plan de sospechosos, intervención de 24.600 canales en matadero hasta resultados,. 4 muestras positivas al inicial. Todos los contradictorios y dirimentes negativos. • Exclusión de Red de Alerta por resultados analíticos negativos y liberación de las canales
intervenidas. • Comunicación del expediente a la CCAA de origen
Actuaciones de Conselleria de Sanidad: 1. Inclusión Red de alerta, 2. 15 muestras en plan de sospechosos, intervención de 5.500 canales en matadero. Resultados analíticos negativos,y liberación de las canales intervenidas. 3. Mantenido en Red de Alerta durante tres meses y exclusión de Red de Alerta hasta completar investigaciones. Comunicación del expediente a la CCAA de origen: Murcia
Actuaciones de Conselleria de Sanidad: 1. Inclusión Red de alerta durante un mes y medio y
2. exclusión por defecto de forma.
Comunicación del expediente a la CCAA de
origen
AHD-0,5-Músculo-Aves
4MOZ-0,26;0,22;0,16;0,29 Archivo por defecto de forma ppbmúsculo-
aves
Comunicación al Departamento de Ganadería , al Juzgado de Primera Instancia y a la Red de Alerta Alimentaria Investigación en la granja de origen y otras
EN 205 EN
relacionadas por trazabilidad Seguimiento de los animales en matadero con toma de muestras e inmovilización de canales
Declaración de canales positivas no aptas para el consumo humano AMOZ-0,16 ppb-músculo-aves Incoación de expediente administrativo sancionador
Comunicación al Departamento de Ganadería , al Juzgado de Primera Instancia y a la Red de Alerta Alimentaria Investigación en la granja de origen y otras relacionadas por trazabilidad Seguimiento de los animales en matadero con toma de muestras e inmovilización de canales
Declaración de canales positivas no aptas para el AHD-1,34ppb-Músculo-ovino consumo humano Incoación de expediente administrativo sancionador
Medidas en explotación: Inmovilización de granjas afectadas. Control de número de animales existentes. Control
de mortalidad.
Control del libro de medicamentos. AHD-0,6 ppb-Músculo-porcino Estudio de Piensos: Identificación de las fábricas suministradoras. Composición y formulación de los distintos piensos suministrados a lo largo de la vida de los pollos. 1 AOZ musculo paloma: Toma de muestras de agua, de piensos 3 microgramos/kg elaborados, además de toma de muestras de músculo (sacrificio de ejemplares. Inspección a la fábrica de piensos. Recogida de muestras de la muestro teca. Recogida de muestras de materias primas, aditivos y correctores.
Inspección en granja de origen de los
EN 206 EN
pollitos (nodrizas)
Eliminación de la autorización de
expedición de animales al matadero sin autorización sanitaria.
Investigación que comprendió toma de muestras de agua, pienso y músculo, además de inspección de los libros de medicamentos a todas 1 AOZ musculo bovino: las granjas relacionadas (mismo titular)y a todas 2 microgramos/kg las granjas que se suministraban de pienso procedente de la misma fábrica.
Se estableció un plan de seguimiento con toma de muestras al azar de las granjas relacionadas (pertenecientes a la misma razón social, y/o a aquellas que se suministraban de
pienso procedente de la misma fábrica), con el fin de detectar una prevalencia de residuos de 21 Cloranfenicol músculo avícola: cloranfenicol del 10%, con un nivel de confianza del 99%, tomándose muestras de músculo, en la explotación, en cualquier momento de la vida contradictorio 0,2ppb productiva de los animales. Este seguimiento se mantuvo a lo largo de 2005. dirimente 0,3ppb Para las tres granjas que con resultados contradictorio 0,9ppb positivos, y para cada uno de los lotes de contradictorio 2,0ppb producción, se tomaron muestras para investigar residuos de cloranfenicol con prevalencias del 5% contradictorio 0.6ppb y niveles de confianza del 99%. Estas muestreos contradictorio 0.7ppb se realizaron al azar, y e cualquier momento de la contradictorio 1.1ppb vida productiva de los animales. contradictorio 0.3ppb No se permitió que ninguna partida fuera destinada a consumo humano sin éste muestreo contradictorio 0.6ppb previo. Este seguimiento se ha prolongado a lo contradictorio 0.7ppb largo de un año, finalizando en marzo de 2006. contradictorio 2.5ppb contradictorio 0.2ppb contradictorio 1.8ppb contradictorio 1.4ppb Medidas en matadero: contradictorio 2.4ppb Comunicación de inmovilización de granjas positivas. contradictorio 0,2ppb Remisión semanal del listado de granjas contradictorio 0,2ppb avícolas autorizadas para el sacrificio de animales. contradictorio 1.5ppb Incremento de investigación (toma de
EN 207 EN
contradictorio 0,4ppb muestras) de animales de otras especies (vacuno, ovino, porcino) dirimente 1.5ppb Incremento de toma de muestras para dirimente 0.2ppb investigar residuos de inhibidores en animales de la especie aviar.
GRUPO A3 19 17-beta estradiol orina porcino Sin cuantificar.Presencia 21 Comunicación a Servicios de Agricultura 18 positivos a nortestosterona Controles aleatorios en explotaciones de origen.
24 muestras positivas a 17 _ testosterona orina bovino Inmovilizados 440 animales en 5 subexplotaciones por acción de Policía Judicial (Explotación 3ppb, 2ppb, 3ppb, 6ppb, 3ppb, sospechosa de utilizar sustancias prohibidas para 5ppb,3ppb, 2ppb, 2ppb, 4ppb, 2ppb, el engorde de terneros). Se establece Alerta en 7ppb, 3ppb, 3ppb, 7ppb, 2ppb, mataderos. 2ppb, 5ppb, 3ppb, 4ppb, 2ppb, 2ppb, 2ppb, 3ppb
8 muestras positivas a 17 _ estradiol Comunicación a Servicios de Agricultura. orina bovino Control aleatorio en explotaciones de origen de 2ppb, 3ppb, 4ppb, 3ppb, 3ppb, trazabilidad de las materias primas. 3ppb, 3ppb, 4ppb en orina de bovino
GRUPO A4 1 Zearalenona orina ovino sin cuantificar. Presencia 36+12 Zearalenona orina porcino. Sin cuantificar.Presencia * Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 208 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances
Non-compliant results Follow-up actions Bovines 1 Dexametasona higado 5 ug/Kg Comunicación a Servicios de Agricultura de la CCAA correspondiente
Iniciación de expediente
Investigación en granja: verificación de registros,
muestreo adicional de agua, pienso y orina, inmovilización de 200 animales y seguimiento 6 meses. Todas las muestras negativas.
Comunicación al Departamento de Ganadería , al Juzgado de 1 Dexametasona higado 3 ppb Primera Instancia y a la Red de Alerta Alimentaria
Investigación en la granja de origen y otras relacionadas por trazabilidad 2 Dexametasona- hígado Seguimiento de los animales en matadero con toma de muestras e inmovilización de canales Declaración de canales positivas no aptas para el consumo humano
Incoación de expediente administrativo sancionador
10 explotaciones ganaderas intervenidas (803 bovinos intervenidos). Toma de muestras: 14 agua, 32 orina, 10 paja, 21 pienso 1 Dexametasona higado bovino
EN 209 EN
Debido a que el origen del positivo era de otra CCAA a aquella donde se determinó el positivo se
remitió la documentación a la CA de origen con 1 Muestra de hígado de toro de lidia carácter inhibitorio por cuestión de territorialidad. positiva a betametasona (35 ppb) 3 positivos B1 en bovino, (1 músculo y2 riñon)
2 Explotaciones de vacuno investigadas por antimicrobianos 7 canales de vacuno intervenidas por antimicrobianos 2 positivos confirmados a 1 expediente administrativo a una explotación de vacuno por antimicrobianos oxitetraciclina en Bovinos
mayores de 2 años.
Decomiso y destrucción de la canal y vísceras.
En total se incoaron 6 expedientes, de los cuales 6 han sido sobreseídos.
1 positivo dexametasona higado de Se Incoa un expediente en el año 2006, por un bovino positivo (dexametasona) del año 2005.
4 positivos Cadmio riñon bovino PNIR DIRIGIDO: Cuatro positivos a cadmio en riñón de animales bovinos, hembras, raza Asturiana de los valles (10, 8 y 9 años con 1,49 – 1,37 y 2, 24 mg/Kg. respectivamente) y Cruce (15 años con 3,19 mg/Kg). Animales nacidos y criados en la misma explotación hasta su
sacrificio en dos casos, pero en todo caso nunca abandonaron esta C.A. (son animales de 4
EN 210 EN
explotaciones diferentes). Al ser un contaminante ambiental, se trasladó la información a la Consejería de Medio Rural y Pesca. 1 positivo dexametasona higado Verificación de registros en granja. bovino
PNIR DIRIGIDO: 1 positivo en bovino por screening a antiinflamatorios con resultado positivo. Las investigaciones posteriores realizadas en L.S.P. DE Zaragoza detectan 5 PPB DE DEXAMETASONA por lo que no se incoa expediente sancionador relacionado con la presencia de residuos. Comunicado a la la Consejería de Medio Rural y Pesca. Actualmente está en la vía penal pendiente de juicio
1 positivo dexametasona higado bovino
Procedente de una explotación distinta a la del hallazgo. Envío de documentación a la CCAA de 1- B1 sulfametoxipiridacina, origen. Inclusión red de Alerta. músculo Toma de muestras en plan de sospechosos. 1- B1 Sulfametacina, músculo Propuesta de sanción a la explotación (15.025,31€). Supervisión de autocontrol de matadero
Investigación en la granja de piensos, con resultado negativo; investigación de las partidas de animales procedentes de la explotación, con inmovilización cautelar hasta la obtención de resultados negativos. La misma explotación es la positiva a Sulfametacina. Destrucción de 1 canal positiva a esta sustancia. 1- B2 Dexametasona, hígado Se repite la investigación en la granja de origen.
EN 211 EN
Identificación del bovino afectado; investigación movimientos relativos al lote de cebo; visita a explotación; investigación de las partidas de animales procedentes de la explotación, con inmovilización cautelar hasta la obtención de resultados negativos 1 hígado positivo a cadmio
Decomiso del hígado. En plan 2006 se recogerán muestras de pienso y forraje de las zonas de procedencia del animal.
10 explotaciones ganaderas (803 bovinos 1 dexametasona higado bovino intervenidos) Muestras: 14 de agua, 32 de orina, 10 de paja, 21 de pienso
1 Doxiciclina (pienso)
3 Oxitetraciclina (pienso)
1 Sulfadiazina (pienso
1 explotación ganadera (159 bovinos intervenidos)
Muestras: 2 de agua, 2 de pienso
Ningún expediente sancionador iniciado
1. comunicación interesado 1positivo tetraciclina pienso bovino 2. inspección explotación y libro de registro
3. toma de muestras pienso en explotación resultado negativo <2años 4. intensificación de controles
Comunicación CCAA de origen
Cadmio-hígado
Pigs
EN 212 EN
1 Sulfametazina músculo 308 Comunicación a Servicios de Agricultura ug/Kg Iniciación de expediente. Investigación en granja: verificación de registros, muestreo adicional de agua y pienso, inmovilización de 400 animales y seguimiento 6
meses. Todas las muestras negativas
2 enrofloxacina músculo 145 y 510
ug/kg 2 Comunicación a Servicios de Agricultura. Iniciación de expediente Investigación en granja: verificación de registros, muestreo adicional de agua y pienso, inmovilización de 430 y 340 animales y seguimiento 6 meses. Todas las muestras negativas
Comunicación a Servicios de Agricultura. 1 plomo hígado 1,37 mg/Kg. Investigación en granja: verificación de registros, muestreo adicional de agua y pienso, inmovilización de 800 animales y toma de muestras de pienso en la fábrica de origen del pienso con resultados negativos
8 Sulfametazina músculo 355,283, 1 Comunicación a Servicios de Agricultura 290, 156, 186, 218, 276, 202 Investigación en granja: verificación de registros, ug/Kg) muestreo adicional de agua y pienso, inmovilización de 240 animales y seguimiento 6
meses. Todas las muestras negativas.
76 canales retiradas del consumo. Se envía documentación a la CCAA de origen.
1- B1 Sulfametacina, riñón Investigación en la granja de piensos, con resultado negativo; investigación de las partidas de animales procedentes de la explotación, con inmovilización cautelar hasta la obtención de
EN 213 EN
resultados negativos.
1 Doxiciclina 6 explotaciones ganaderas (6.044 porcinos 1 Doxiciclina y Sulfadiazina intervenidos + 548 ovinos-caprinos) 1 Sulfadiazina Muestras: 25 de agua, 36 de pienso 1 Ciprofloxacina + Enrofloxacina
Medidas totales generadas en este grupo de positivos 13 Clortetraciclina (pienso) 33 explotaciones ganaderas (32.120 porcinos 7 Doxiciclina (pienso) intervenidos) 30 Oxitetraciclina (pienso) Muestras: 59 de agua, 104 de pienso 15 Sulfadiazina (pienso) 17 Expedientes sancionadores iniciados: 2 Clortetraciclina+Tetraciclina ° 7 Resolución de advertimiento (pienso) ° 1 Resolución por sobreseimiento 3 Clortetraciclina+Sulfadiazina ° 1 Pendiente de Recurso de alzada (600€) (pienso) ° 2 Propuesta de resolución (600€) 1 Sulfadiazina+Oxitetraciclina (pienso) ° 3 Resueltos con sanción (1.300€) 1 Oxitetraciclina+Clortetraciclina 1 Archivado (pienso) 2 Sulfadiazina+Doxicilina (pienso) 1 Clortetraciclina+Doxiciclina (pienso) Doxiciclina: justificado el tratamiento en la explotación, no hubo salida de animales hasta completado plazo de espera. Se comprobó el libro de Registro de Tratamientos Medicamentosos y 2 positivos a oxitetraciclina Pienso la correspondiente receta. Todo fue correcto 1 positivo a doxiciclina Agua
1 comunicación interesado
2 inmovilización explotación
3 inspección explotación y libro de registro
4 toma de muestras de pienso en explotación 1positivo tilosina pienso cebo resultado negativo
EN 214 EN
5 Levantamiento de la inmovilización 6 Intensificación de controles
Poultry 1 Doxiciclina 3 explotaciones ganaderas (20.200 animales intervenidos) 2 Enrofloxacina Muestras: 3 de agua, 5 de pienso
4 explotaciones ganaderas (35.100 pollos y 6.300 1 Clortetraciclina (pienso) perdices intervenidas) 10 Oxitetraciclina (pienso) Muestras: 6 de agua, 8 de pienso 3 Doxiciclina (pienso) 2 Expedientes sancionadores iniciados: 1 Sulfadiazian (pienso) ° 1 Resolución de advertimiento 1 Cortetraciclina+Sulfadiazina 1 Resolución por sobreseimiento (pienso)
2 positivos a oxitetraciclina pienso P1 P2 Positivo P1: inmovilización 19 machos y 30 hembras. Nuevo control, resultado negativo.
Positivo P2: inmovilizado de explotación. Nuevo
control, resultado negativo. 1 positivos a enrofloxacina agua
Inmovilización 140000 aves de puesta. Nuevo control en agua, resultado negativo. 1positivo tilosina pienso
comunicación interesado inspección explotación y libro de registro toma muestra pienso en explotación resultado Clortetraciclina-músculo negativo intensificación de controles
EN 215 EN
Comunicación CCAA de origen: Castilla la Mancha Comunicación Red de Alerta. AESA.
Sheep and goat 1 Sulfadiacina musculo (261 Comunicación a Servicios de Agricultura. ug/Kg) Iniciación de expediente Investigación en granja: verificación de registros, muestreo adicional de agua y pienso, inmovilización de 400 animales y seguimiento 6 meses. Todas las muestras negativas
Comunicación desde otra CCAA distinta. 1 Sulfadiazina músculo (295 ppb) Investigación en granja: verificación de registros, muestreo adicional de agua y pienso, inmovilización de 400 animales y seguimiento 6 meses. Todas las muestras negativas.
2 sulfadiacina músculo ( 176;140 Se envía el expediente a Comunidad Autónoma de origen de los animales. ug/Kg)
Investigación en las explotaciones ganaderas de ovino y caprino de engorde, verificación de 1 positivos a Sulfadiazina en registros de la explotación, especialmente de musculo de ovino. tratamientos veterinarios y prescripciones de pienso medicamentoso con sulfamidas.
Implantación de medidas cautelares
(inmovilización de 109 corderos, y 32 caprinos 1 positivo a Sulfadiazina en recogida de 4 muestras de pienso para
EN 216 EN
musculo de caprino investigación de la presencia de sulfamidas, resultando positiva una en cada explotación.
Comunicación oficial del resultado y recogida de
nuevas muestras del pienso de recambio con resultados negativos a sulfamidas. Sacrificio bajo control sanitario de un lote en cada explotación de 19 ovinos y 15 caprinos, resultando aptos para el consumo.
Sacrificio del resto de animales inmovilizados, bajo control sanitario.
Iniciación de expediente sancionador a las dos explotaciones calificados como graves (3.005, 07 € cada uno) habiendo sido resueltos.
Acciones: investigación en la granja de piensos, con resultado positivo a sulfadiazina; investigación de las partidas de animales procedentes de la explotación, con inmovilización cautelar hasta la
obtención de resultados negativos. Destrucción de 100 canales de ovino positivas o sospechosas. 1-B1 sulfadiazina, músculo Iniciación de expediente sancionador.
Acciones: remisión del expediente a la Comunidad de Origen de la explotación al no pertenecer a la Comunidad autónoma donde se descubrió el caso positivo
1- B1 sulfadiazina, músculo
1- B1 sulfadiazina, músculo Acciones: investigación en la granja, ampliación a dos de las explotaciones en vigilancia, al compartir medios de producción. Iniciación de expediente sancionador.
EN 217 EN
Acciones: investigación en la granja. Iniciación de expediente sancionador.
1- B1 sulfadiazina, músculo
2 explotaciones ganaderas (291 ovinos-caprinos
intervenidos)
Muestras: 2 de agua, 2 de pienso
8 explotaciones ganaderas (5.089 ovinos-caprinos intervenidos) Muestras: 11 de agua, 45 de pienso 1 Sulfadiazina 3 Expedientes sancionadores iniciados: ° 1 Resolución de advertimiento 1 Pendiente de Recurso de alzada 6 Clortetraciclina (pienso) 3 Sulfadiazina (pienso) 2 Oxitetraciclina (pienso) 1 Doxicilina (pienso) 1 Sulfadiazina + Oxitetraciclina + Clortetraciclina (pienso)
Iniciado procedimiento sancionador con falta tipificada como muy grave. El procedimiento esta “pendiente de propuesta de resolución”.
Iniciado procedimiento sancionador con falta 2 Muestras de músculo de lechazo tipificada como grave y suspendido en vía positivas a ciprofloxacina y administrativa pendiente de resolución judicial en enrofloxacina vía penal.
1 Muestras de músculo de ovino comunicación interesado positivas a sulfadiazina.
EN 218 EN
inspección explotación y libro de registro toma muestra pienso en explotación resultado negativo
intensificación de controles 1positivo tilosina pienso
Detectado por CCAA de Cataluña.. Sulfadiazina- Músculo • Conselleria de Agricultura. • comunicación interesado • inspección explotación y libro de registro • toma muestra pienso en explotación resultado
negativo • intensificación de controles Conselleria de Sanidad Tramitado a la Unidad de Sanciones para la incoación de expediente sancionador
Conselleria de Agricultura, Pesca y Alimentación 1. comunicación interesado Plomo-hígado 2. inspección explotación y libro de registro 3. toma de 2 muestras pienso y 1 de agua en explotación resultado negativo 4. intensificación de controles
Horses
7 cadmio en equino 3 Explotaciones investigadas de equino por 4 plomo equino metales pesados con recogida de muestras de agua, pienso, correctores, hierba, tierra y leche
Decomiso directo de hígado y riñón. En el Plan 6 hígados positivos a Cadmio 2006 se recogerán muestras de pienso y forraje 1 hígado positivo a plomo de las zonas de las que procedían o pastaban los animales.
EN 219 EN
12 riñones positivos a cadmio
Milk & @ PCB,s-leche caprina Muestra tomada en fábrica de queso. Conselleria de Agricultura, Pesca y Alimentación 1. comunicación interesado 2. inmovilización explotación 3. inspección explotación y libro de registro 4. Leche de la explotación material de categoria 2 Reglamento 1774/2002, destrucción en planta autorizada. 5. toma de muestras de pienso, agua y leche en explotación resultado negativo 6. Levantamiento de la inmovilización Conselleria de Sanidad Prohibición de proveerse de leche procedente de esta explotación hasta obtención de resultados satisfactorios.
Eggs & @ Rabbit & @ 13 Oxitetraciclina (pienso) 1 explotación ganadera (2.540 conejos intervenidos) 2 Sulfadiazina (pienso) Muestras: 7 de agua, 10 de pienso
1 Expediente sancionador iniciado y resuelto con
sanción de 600€.
Positivo 1P : inmovilización de explotación 1400 4 positivos a Oxitetraciclina en cebo y 1450 hembras. pienso P Positivo 2P: justificado el tratamiento no se tomaron medidas adicionales.
EN 220 EN
5 positivos a Enrofloxacina y 1 Positivo 3P: justificado el tratamiento no se tomaron medidas adicionales. positivo a Ciprofloxacina en Agua Positivo 4P: justificado el tratamiento. Nuevo
control en piensos resultado negativo.
Positivo 1A: inmovilizados 1500 cebo, 100 machos y 550 hembras. Positivo 2A: inmovilizados 1200 cebos, 100 reposición y 400 hembras. Positivo 3A+4A: (enrofloxacina+ciprofloxacina) inmovilización 800 hembras, 4000 gazapos. Expediente sancionador. Nuevo control en agua resultado negativo. Positivo 5A: inmovilizados 500 reproductores, 2500 cebo y 2517 gazapos. Nuevo control, resultado negativo. Positivo 6A: nuevo control, resultado negativo.
Aquaculture & @ Por alerta RASFF 2005 AXC, de 14 1 explotación de cría de alevines intervenida, con de abril de 2005, relativa a la restricción de movimiento durante la presencia de Cadmio en pienso de investigación. Se tomaron un total de 15 muestras peces de peces para la determinación de Cadmio. Se restringió el movimiento de 210.000 alevines en 5 tanques, desde el 18 de abril de 2005 hasta el 18 de mayo de 2005 (resultado negativo en los peces)
2 Cadmio-músculo de ánguila Investigación en la empresa de acuicultura de origen. 4 análisis de agua y 4 análisis de músculo de ánguila con resultados negativos. Contradictorio y dirimente negativo. Farmed game & @ Wild game & @ Honey
EN 221 EN
& @
EN 222 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State SWEDEN
Date 19 May 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
Control of more Beta-agonist substances for alla species
Non-compliant results Follow-up actions
* Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
Group B substances
Modification of national residue plan Aggregate for all animal products and substances
Control of more coccidiostat substances for all species Control of more sulfonamides for all species incl honey Control of tylosin in pigs introduced
Non-compliant results Follow-up actions Bovines
4penicillin-G,-kidney investigations in the farm of origin: verification of records, carcasses and products declare unfit for human consumption, administrative measures, 1Cadmium, kidney investigation ongoing
Pigs
EN 223 EN
1 Penicillin-G, kidney investigations in the farm of origin: verification of records, carcasses and products declare unfit for human consumption, administrative measures
Poultry
Sheep and goat
Horses 1 Cadmium, muscle investigation ongoing Milk @ Eggs @ Rabbit @ Aquaculture @ Farmed game @ Wild game @ Honey @
EN 224 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State UNITED KINGDOM
Date 10 July 2006
Group A substances
Modification of national residue plan Aggregate for all animal products and substances
Boldenone analysis included for cattle samples taken on farm
Non-compliant results Follow-up actions Nortestosterone 3, 3, 10, and All animals were female animals and one confirmed to be ‘in calf’, likely to have naturally 11µg/kgcattle urine elevated levels Nortestosterone sheep urine No evidence of abuse. 53 follow up samples taken, all negative. 0.2,0.5,0.5,0.5,0.5,0.5,0.6,0.6,0.7,0.7, 0.7,0.7,0.7,0.8,0.8,1,1,1,1,1,1,1,1,1,1, 1,1,1,1.4,2,2,2,2,2µg/kg
Progesterone cattle serum 39 follow up samples taken from 4 farms. No 0.5,0.7,0.9,1,1,1,1.1,2,3µg/kg evidence of abuse. Additional farms to be targeted as part of 2006 plan. Animals on 4 farms were under restriction pending analytical results. SEM 0.5µg/kg sheep kidney No evidence of use on farm.
Zeranol 0.7, 0.9, 1, 1 and 2 µg/kg Evidence from laboratory results indicates that cattle urine residue is likely to be due to feed contamination.
* Information to be included for each non-compliant result. In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated. Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 225 EN
Group B substances
Modification of national residue plan Aggregate for all animal products and substances
Mercury included for aquaculture samples.
Increased testing of calf samples for antimicrobials as a result of positives in 2005.
Non-compliant results Follow-up actions Bovines Kidney Lead 780µg/kg Source of residue not established
Kidney Lead 551µg/kg
Calf kidney1600µg/kg Investigated with a view to prosecution oxytetracycline
Calf kidney Sulphadiazine 250µg/kg Medication administered to wrong animal, warning letter sent to farmer concerning medicine records.
Plasma Phenylbutazone 20µg/kg Source of residue not established
Pigs
Kidney sulphadiazine 170,520, Investigated on farm 910µg/kg
Kidney chlortetracycline 626 µg/kg Possible cross contamination of withdrawal ration with medicated feed
Kidney chlortetracycline 640µg/kg SVS have written to farmer about record keeping.
Kidney chlortetracycline 2480µg/kg, On farm investigation found no evidence of the misuse of this substance. Further animals to be targeted at slaughter. Kidney 860µg/kg oxytetracycline Possible cross contamination of withdrawal ration with medicated feed. Warning letter sent to farmer.
Liver 30µg/kg salinomycin 2 pig feed samples tested contained salinomycin at 34 and 35mg/kg suggested rate of inclusion should be 30mg/kg. Advice provided to farmer.
Liver 35µg/kg salinomycin Source of residue not established.
EN 226 EN
Poultry Hens liver cadmium 809µg/kg No evidence of substance on the farm. Heavy metals accumulate in offal. Turkey liver lead 529µg/kg No evidence of substance on the farm. Heavy metals accumulate in offal. Broiler liver monensin 6,7µg/kg Advice provided to farmer. Broiler liver nicarbazin 210,215,220,220,230,240,240,260, 270,280,300,300,340,350,350,390, 465,600,730,800,1100,1310,1515, 1800,20470,2900,3030µg/kg Sheep and goat Sheep Kidney 2100 Oxytetracycline SVS have written to farmer about record keeping Liver Fenbendazole 670µg/kg Kidney Cadmium 1030,1276,3287, 3873µg/kg
Horses Plasma Phenylbutazone 64µg/kg Animal sent to slaughter in error. Milk Lead 88µg/kg On farm investigation found no evidence of lead poisoning in farm stock. Further blood and milk samples all negative.
Eggs Sulphadiazine 110, 180, 1800µg/kg Follow up investigations carried out Chlortetracycline 290µg/kg Salinomycin 15µg/kg Lasalocid 760µg/kg Nicarbazin 70,100,182µg/kg Rabbit
Aquaculture
EN 227 EN
Muscle malachite green 5µg/kg Site under restriction. Muscle leuco malachite green 20µg/kg Farmed game
Wild game
Honey
EN 228 EN
QUESTIONNAIRE ON THE ACTIONS TAKEN AS A CONSEQUENCE OF NON-COMPLIANT RESULTS IN 2005
Member State HUNGARY
Date 31 May 2006
Group A substances
Modification of national residue Aggregate for all animal products and substances plan
Accepting EU comments Dexamethasone, 16-OH-stanosolol & OH metronidasol have been added to the plan.
Method development of dexamethasone is not ready.
If ordered standards of 16-OH-stanosolol & OH metronidasol will arrive then we will incorporate them into our NRMP.
Non-compliant results Follow-up actions
Substance-Concentration-Matrix- Other actions: (investigations in the farm of origin, animal or animal product* animals held in farms, slaughtered animals, intensified sampling in related farms, products declared unfit for human consumption, administrative measures, denial EC aid, others). Example: MPA-3 ppb-kidney fat-pig
* Information to be included for each non-compliant result.
In case of several non-compliant results for the same substance in the same holding or related holdings, data could be aggregated.
Data on concentration and matrix is very useful to be used as background information for the monitoring of the prevalence of use of group A substances.
EN 229 EN
Group B substances
Modification of national residue Aggregate for all animal products and substances plan
Accepting EU comments Group of B.1. Quinolones, B.2.a (Avermectin, Moxidectin), B.2.b.(Narasin, Lasalocid) B.2.e. (Diclofenac, Flunixin) have been enlarged.
Non-compliant results Follow-up actions
Bovines
& Number of non-compliant @ List actions: (investigations in the farm of results-substance (if possible origin: verification of records, additional matrix) sampling; animals held in the farm, iintensified checks on the animals and products from the farm/establishment in the event of repeated infringements, carcasses and products declare Example: 2 difloxacin-kidney unfit for human consumption, administrative measures, others).
Additional sampling; animals held in the farm, intensified checks on the animals and products from the farm
B3C : 2 CADMIUM KIDNEYS
Pigs
& Number of non-compliant @ List actions: (investigations in the farm of results-substance (if possible origin: verification of records, additional matrix) sampling; animals held in the farm, intensified checks on the animals and products from the farm/establishment in the event of repeated infringements, carcasses and products declare unfit for human consumption, administrative measures, others).
Additional sampling; animals held in the farm, intensified checks on the animals and products from the farm.
B3C : 1 CADMIUM KIDNEY
EN 230 EN
Poultry
B3c : 1 Cadmium 1 Lead- liver Additional sampling; animals held in the farm, intensified checks on the animals and products from the farm.
& @
Sheep and goat
& @
Horses
& @
Milk
& @
Eggs
& @
Rabbit
& @
Aquaculture
& @
Farmed game
& @
Wild game
& @
Honey
& @
EN 231 EN