Deutsche Akkreditierungsstelle GmbH

Annex to the Accreditation Certificate D-PL-14602-01-00 according to DIN EN ISO/IEC 17025:2005

Period of validity: 09.07.2015 to 15.10.2017 Date of issue: 09.07.2015

Holder of certificate: Eurofins WEJ Contaminants GmbH Neuländer Kamp 1, 21079 Hamburg

Tests in the fields: physico-chemical and chemical analysis of , feed and raw materials for cosmetic products; selected immunochemical analysis of food and grain dust; sampling of food and feed

Within the given testing field marked with *), the testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, the modification, development and refinement of testing methods. The listed testing methods are exemplary. The testing laboratory maintains a current list of all testing methods within the flexible scope of accreditation.

Abbreviations used: see last page

This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/11

Annex to the accreditation certificate D-PL-14602-01-00

1 Physico-chemical and chemical analysis of food, feed and raw materials for cosmetic products

1.1 Determination of residues and contaminants by gas chromatography with standard detectors (FID, ECD, MS)

1.1.1 Determination in food and food raw materials *

US FDA/CFSAN Determination of furan in , FDA-Method 2006-10

CON-PV 00572 Determination of furan in foodstuffs by gas chromatographic 2015-04 headspace analysis (headspace GC/MS)

CON-PV 00627 Determination of polycyclic aromatic hydrocarbons (PAHs) in 2014-11 food, feed and cosmetic raw materials by GPC clean-up and GC/MS

CON-PV 00629 Determination of plasticizers in foodstuffs, cosmetics and 2015-03 cosmetic raw products by GC/MS

CON-PV 00864 Determination of in soft drinks and water with 2015-04 headspace GC/MS

CON-PV 01176 Determination of polycyclic aromatic hydrocarbons (PAHs) in 2015-06 food, feed and cosmetic raw materials by SPE GC/MS

in combination with: CON-PV 01322 Non-quantitative fat extraction 2013-07

CON-PV 01212 Determination of dichloromethane and ethyl acetate in raw 2014-12 coffee by headspace GC/MS

CON-PV 01300 Determination of 3-MCPD and DCP in foodstuffs by GC-MS 2014-09

in combination with: CON-PV 01322 Non-quantitative fat extraction 2013-07

CON-PV 01316 Determination of mineral oil saturated hydrocarbons in vegetable 2015-01 oil by LC-GC/FID coupling

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 2/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00

CON-PV 01317 MOSH-MOAH separation of mineral oil hydrocarbons in food by 2015-03 LC-GC / FID coupling

CON-PV 01321 Determination of 3-MCPD esters, 2-MCPD esters and glycidol 2014-04 (difference method) in oil, fat and fatty foodstuffs by GC/MS (DGF C-VI-18 [10]; modified)

CON-PV 01329 Determination of water-soluble solvents in foods, food additives 2014-04 and cosmetic raw materials by headspace GC/FID

CON-PV 01330 Determination of residues of volatile organic solvents in foods, 2015-04 food additives and cosmetic raw materials by headspace GC/MS

CON-PV 01342 Determination of chloroform in milk by headspace GC/MS 2014-10

1.1.2 Determination in feed *

CON-PV 00627 Determination of polycyclic aromatic hydrocarbons (PAHs) in 2014-11 food, feed and cosmetic raw materials by GPC clean-up and GC/MS

CON-PV 01176 Determination of polycyclic aromatic hydrocarbons (PAHs) in 2015-06 food, feed and cosmetic raw materials by SPE GC/MS

in combination with: CON-PV 01322 Non-quantitative fat extraction 2013-07

1.1.3 Determination in raw materials for cosmetics

CON-PV 00627 Determination of polycyclic aromatic hydrocarbons (PAHs) in 2014-11 food, feed and cosmetic raw materials by GPC clean-up and GC/MS

CON-PV 00629 Determination of plasticizers in foodstuffs, cosmetics and 2015-03 cosmetic raw products by GC/MS

CON-PV 01176 Determination of polycyclic aromatic hydrocarbons (PAHs) in 2015-06 food, feed and cosmetic raw materials by SPE GC/MS1

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 3/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00

in combination with: CON-PV 01322 Non-quantitative fat extraction 2013-07

CON-PV 01329 Determination of water-soluble solvents in foods, food additives 2014-04 and cosmetic raw materials by headspace GC/FID

CON-PV 01330 Determination of residues of volatile organic solvents in foods, 2013-08 food additives and cosmetic raw materials by headspace GC/MS

1.2 Determination of contaminants by high performance liquid chromatography with standard detectors (Fluorescence)

1.2.1 Determination in food *

DIN EN ISO 14501 Milk and milk powder - Determination of M1 content - 2008-01 Clean-up by immunoaffinity chromatography and determination by high-performance liquid chromatography (HPLC-FD) (Modification: Expansion of scope to milk products by modification of sample preparation)

DIN EN 14132 Foodstuffs - Determination of ochratoxin A in barley and roasted 2009-09 coffee - HPLC method with immunoaffinity column clean-up (HPLC-FD) (Modification: Expansion of scope to cereals, coffee, cocoa, pepper, dried fruits and liquorice containing samples, change of extraction solvent, additional post column derivatisation)

DIN EN 14133 Foodstuffs - Determination of ochratoxin A in wine and beer - 2009-09 HPLC method with immunoaffinity column clean-up (HPLC-FD) (Modification: Expansion of scope to beverages, additional post column derivatisation)

DIN EN 15829 Determination of ochratoxin A in dried fruit - HPLC method 2010-05

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 4/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00 prEN 14123 Foodstuffs - Determination of and the sum of 2007-05 aflatoxin B1, B2, G1 and G2 in hazelnuts, peanuts, pistachios, figs, and paprika powder - High performance liquid chromatographic method with post-column derivatisation and immunoaffinity column clean-up (Modification: Expansion of scope to nut-like products, dried fruits, cereals products, certain spices, tea, coffee, cocoa and different other foods, change of extraction solvent and measurement conditions) prEN 15851 Determination of aflatoxin B1, B2, G1 and G2 in baby food and 2008-09 dietary products

AOAC 84, No.5 Determination of ochratoxin A in baby food by HPLC-FD 2001

1.2.2 Determination in feed * prEN 14123 Foodstuffs - Determination of aflatoxin B1 and the sum of 2007-05 aflatoxin B1, B2, G1 and G2 in hazelnuts, peanuts, pistachios, figs, and paprika powder - High performance liquid chromatographic method with post-column derivatisation and immunoaffinity column clean-up (Modification: Expansion of scope to feed, change of extraction solvent and measurement conditions)

DIN EN 14132 Foodstuffs - Determination of ochratoxin A in barley and roasted 2009-09 coffee - HPLC method with immunoaffinity column clean-up (HPLC-FD) (Modification: Expansion of scope to feed, change of extraction solvent, additional post column derivatisation)

1.2.3 Determination in raw materials for cosmetics prEN 14123 Foodstuffs - Determination of aflatoxin B1 and the sum of 2007-05 aflatoxin B1, B2, G1 and G2 in hazelnuts, peanuts, pistachios, figs, and paprika powder - High performance liquid chromatographic method with post-column derivatisation and immunoaffinity column clean-up (Modification: Expansion of scope to cosmetic raw materials, change of extraction solvent and measurement conditions)

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 5/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00

1.3 Determination of additives, residues and contaminants by liquid chromatography with mass detectors (LC-MS/MS, LC-HRMS)

1.3.1 Determination in food *

ASU L 06.00-57 (V) Determination of residues of macrolides and lincosamides in 2009-06 kidney and milk by LC-MS/MS (Modification: Expansion of scope to fish, egg, egg powder, honey, water, milk powder, extraction at pH 8 with acetonitrile)

LG/GC Europe 17/11a, 25-30 Multi- method: Determination of Fusarium in vegetal 2004-11 foods by LC-MS/MS

CON-PV 00148 Determination of tetracyclines in honey and milk by LC-MS/MS 2015-05

CON-PV 00168 Determination of tetracyclines in meat, fish, crustaceans and eggs 2015-05 by LC-MS/MS

CON-PV 00566 Determination of dyes with a fungicide effect in fish , feeding 2013-03 stuffs and oleoresin by LC-MS/MS

CON-PV 00570 Determination of nitrofuran metabolites in animal foodstuffs by 2015-06 LC-MS/MS

CON-PV 00607 Determination of coccidiostats in eggs, egg products, feeding 2013-03 stuffs and poultry by LC-MS/MS

CON-PV 00630 Determination of sulphonamides in meat after direct extraction 2015-05 by LC-MS/MS

CON-PV 00700 Determination of sulphonamides in honey and milk by LC-MS/MS 2015-05

CON-PV 00840 Determination of patulin in apple juice and other fruit 2015-05 preparations by LC-MS/MS

CON-PV 00895 Determination of quinolones and fluoroquinolones respectively in 2013-07 meat by LC-MS/MS

CON-PV 00897 Determination of nicotine and cotinine in eggs, egg products, 2015-05 poultry, poultry products, mushrooms and herbs by LC-MS/MS

CON-PV 00915 Determination of fluoroquinolones in honey by LC-MS/MS 2013-03

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 6/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00

CON-PV 01012 Determination of ergot alkaloid content in foodstuffs by 2014-06 HPLC-MS/MS

CON-PV 01029 Determination of benzimidazoles in meat, liver and milk by 2015-05 LC-MS/MS

CON-PV 01085 Determination of fumonisins in foodstuffs and feeding stuffs by 2015-04 LC-MS/MS

CON-PV 01090 Determination of gestagens in meat and protein-rich foodstuffs 2015-05 by LC-MS/MS

CON-PV 01112 Determination of chloramphenicol and amphenicols in honey by 2013-01 LC-MS/MS

CON-PV 01126 Multi-toxin method: Determination of by LC-MS/MS 2015-05 (Screening)

CON-PV 01165 Determination of nitroimidazoles in meat, shrimps, egg and milk 2015-05 powder by LC-MS/MS

CON-PV 01211 Determination of amphenicols in meat, shrimp, egg and milk 2015-06 powder by LC-MS/MS

CON-PV 01291 Determination of heterocyclic aromatic amines in meat and 2015-06 flavours by LC-MS/MS

CON-PV 01303 Multi method for analysis of veterinary drugs in meat and 2012-06 protein-rich foodstuffs by LC-MS/MS

CON-PV 01308 Determination of estrogens in meat and protein-rich foodstuffs, 2015-05 water and urine by LC-MS/MS

CON-PV 01319 Determination of Alternaria toxins in vegetable oil by LC-MS/MS 2013-04

CON-PV 01320 Determination of androgens in meat and protein-rich foodstuffs, 2015-05 water and urine by LC-MS/MS

CON-PV 01324 Determination of amino glycosides in food LC-MS/MS 2015-06

CON-PV 01326 Determination of pyrrolizidine alkaloids and their N-oxides in 2015-05 food by LC-MS/MS

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 7/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00

CON-PV 01328 Determination of -lactams in protein-rich matrices and feed by 2015-06 LC-MS/MS

CON-PV 01334 Determination of beta-2-agonists in protein-rich and fatty food by 2014-08 LC-MS/MS

CON-PV 01335 Determination of acrylamide in food by LC-MS/MS 2015-06

CON-PV 01336 Multi method for high resolution analysis of veterinary drugs in 2014-12 meat and protein-rich foodstuffs by LC-MS/MS

CON-PV 01337 Determination of plasticizers in oil and fat by LC-ESI-MS/MS 2014-03

CON-PV 01339 Determination of bisphenols in food by LC-ESI-MS/MS 2014-03

CON-PV 01343 Determination of sedatives in meat and protein-rich matrices by 2014-10 LC-MS/MS

1.3.2 Determination in feed *

ASU L 06.00-57 (V) Determination of residues of macrolides and lincosamides in 2009-06 kidney and milk by LC-MS/MS (Modification: Expansion of scope to feed, extraction at pH 8 with acetonitrile)

CON-PV 00566 Determination of dyes with a fungicide effect in fish, feeding 2013-03 stuffs and oleoresins by LC-MS/MS

CON-PV 00607 Determination of coccidiostats in eggs, egg products, feeding 2013-03 stuffs and poultry by LC-MS/MS

CON-PV 01085 Determination of fumonisins in foodstuffs and feeding stuffs by 2015-04 LC-MS/MS

CON-PV 01126 Multi-toxin method: Determination of mycotoxins by 2015-05 LC-MS/MS

CON-PV 01298 Determination of estradiol in feeding stuffs by LC-MS/MS 2015-05

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 8/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00

CON-PV 01328 Determination of -lactams in protein-rich matrices and feed by 2015-06 LC-MS/MS

1.4 Determination of elements in food and feed by Atomic absorption spectrometry (GF-AAS, K-AAS, HG-AAS) *

ASU L 00.00-19/3 Determination of trace elements - Determination of lead, 2004-07 cadmium, chromium and molybdenum by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion (Modification: Expansion of analytes to Co, Ni, Ag, Te, Tl, Sn, V, Sb, Be, As, Se; Expansion of scope to feed)

ASU L 00.00-19/4 Determination of trace elements in food - 2003-12 Part 4: Determination of mercury by atomic absorption spectrometry (AAS) with cold vapour technique after pressure digestion (Modification: Expansion of scope to feed)

ASU L 25.06-1 Food analysis - Determination of inorganic arsenic in algae - 2008-12 atomic absorption spectrometry - hydride generation (HG-ASS) after acidic extraction (Modification: Expansion of scope to rice, fish, fish oil, fish meal) n combination with: ASU L 00.00-19/1 Determination of trace elements in food - 2003-12 Part 1: pressure digestion (Modification: Expansion of scope to feed, addition of direct digestion)

1.5 Determination of elements in food and feed by inductively coupled plasma with atomic emission spectrometry (ICP-OES) *

DIN EN ISO 11885 (E 22) Water quality - Determination of 33 elements by inductively 2009-05 coupled plasma optical emission spectrometry (ICP-OES) (Modification: Expansion of scope to food and feed, expansion of analytes to Au, Pd, Pt, Rh, Te, Tl, W, Y)

DIN 15510 Animal feeding stuffs - Determination of calcium, sodium, 2007-10 phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum, arsenic, lead and cadmium by ICP-AES

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 9/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00 in combination with: ASU L 00.00-19/1 Determination of trace elements in food - 2003-12 Part 1: pressure digestion (Modification: Expansion of scope to feed, addition of direct digestion)

1.6 Determination of elements in food and feed by inductively coupled plasma with mass spectrometry (ICP-MS) *

DIN EN 15111 Foodstuffs - Determination of trace elements - Determination of 2007-06 iodine by ICP-MS (Modification: Expansion of analytes to bromine; expansion of scope to feed)

DIN EN 15763 Foodstuffs - Determination of trace elements - Determination of 2010-04 arsenic, cadmium, mercury and lead in foodstuffs by inductively coupled plasma mass spectrometry (ICP-MS) after pressure digestion (including high resolution ICP-MS) (Modification: Expansion of analytes to match DIN EN ISO 17294- 2 (62 elements) plus selenium, expansion of scope to feed) in combination with: ASU L 00.00-19/1 Determination of trace elements in food - 2003-12 Part 1: pressure digestion (Modification: Expansion of scope to feed, addition of direct digestion)

1.7 Photometric determinations in food and feed

CON-PV 00394 Photometric determination of iodide via the Sandell-Kolthoff 2015-06 reaction after combusting according to Grote-Krekeler

1.8 Determination of radioactive nuclides in food, feed and raw materials for cosmetics

CON-PV 01305 Determination of radioactive nuclides by gamma spectrometry 2015-05

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 10/11 Date of issue: 09.07.2015

Annex to the accreditation certificate D-PL-14602-01-00

2 Determination of contaminants and biotoxins by immunoassay (dip sticks) in food and cereals dust

Eurofins rapidust® - Indirect determination of mycotoxins in cereals via rapidust® Mycotoxins analysis of dust samples by lateral flow immunoassay dip sticks 2015-06

3 Sampling of food and feed samples

CON-PV 01347 Sampling of Cereals and cereal 2015-06 (Based on regulations VO (EG) no. 401/2006, VO (EG) no. 333/2007, guideline 2002/63/EG, VO (EG) 1883/2006, DIN EN ISO 24333, Codex Alimentarius CAC/GL 50-2004, ICC 101/1, ICC 120, ICC 130, ICC 138)

CON-PV 01348 Sampling of food and food samples 2015-06 (except cereals and cereal products)

Eurofins rapidust® - Sampling of cereal lots via dust retrieval rapidust® Mycotoxins 2015-06

Abbreviations used:

AOAC Official Methods of Analysis of AOAC International ASU Official Collection of Testing Methods according to § 64 LFGB CON-PV XXXXX Methods of Eurofins WEJ Contaminants GmbH DIN German Institute for Standardization e. V. EN European Standard FDA Food and Drug Administration IEC International Electrotechnical Commission ISO International Organization for Standardization LFGB German Food and Feed Code prEN European Standard Draft

Period of validity: 09.07.2015 to 15.10.2017 - Translation - 11/11 Date of issue: 09.07.2015