Measuring Soil Ph
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Basic Soil Science W
Basic Soil Science W. Lee Daniels See http://pubs.ext.vt.edu/430/430-350/430-350_pdf.pdf for more information on basic soils! [email protected]; 540-231-7175 http://www.cses.vt.edu/revegetation/ Well weathered A Horizon -- Topsoil (red, clayey) soil from the Piedmont of Virginia. This soil has formed from B Horizon - Subsoil long term weathering of granite into soil like materials. C Horizon (deeper) Native Forest Soil Leaf litter and roots (> 5 T/Ac/year are “bio- processed” to form humus, which is the dark black material seen in this topsoil layer. In the process, nutrients and energy are released to plant uptake and the higher food chain. These are the “natural soil cycles” that we attempt to manage today. Soil Profiles Soil profiles are two-dimensional slices or exposures of soils like we can view from a road cut or a soil pit. Soil profiles reveal soil horizons, which are fundamental genetic layers, weathered into underlying parent materials, in response to leaching and organic matter decomposition. Fig. 1.12 -- Soils develop horizons due to the combined process of (1) organic matter deposition and decomposition and (2) illuviation of clays, oxides and other mobile compounds downward with the wetting front. In moist environments (e.g. Virginia) free salts (Cl and SO4 ) are leached completely out of the profile, but they accumulate in desert soils. Master Horizons O A • O horizon E • A horizon • E horizon B • B horizon • C horizon C • R horizon R Master Horizons • O horizon o predominantly organic matter (litter and humus) • A horizon o organic carbon accumulation, some removal of clay • E horizon o zone of maximum removal (loss of OC, Fe, Mn, Al, clay…) • B horizon o forms below O, A, and E horizons o zone of maximum accumulation (clay, Fe, Al, CaC03, salts…) o most developed part of subsoil (structure, texture, color) o < 50% rock structure or thin bedding from water deposition Master Horizons • C horizon o little or no pedogenic alteration o unconsolidated parent material or soft bedrock o < 50% soil structure • R horizon o hard, continuous bedrock A vs. -
Soil Ph Ranges Neutral Acidity Alkalinity
Sound Farm Idea #04 Lime For Pastures and Crops When it comes to managing soil health in the Northwest, it’s easy to focus on the big three nutrients (nitrogen, phosphorus, and potassium) in the soil, and overlook a fourth key aspect - soil pH. Soil pH refers to how acidic (sour) or alkaline (sweet) soil is on a scale between 0 and 14, with 7.0 being neutral. Most plants and crops prefer soil pH levels in the 6.0 – 7.0 range. Soil pH Ranges Neutral Acidity Alkalinity 10,000x 1,000x 100x 10x o 10x 100x 1,000x 10,000x 3 4 5 6 7 8 9 10 11 Here in Western Washington, our soils are typically mildly to strongly acidic (5.0 – 6.5). Soil pH is important for a number of reasons. First of all, it controls the rate of chemical reactions and the activity of soil microorganisms. As you move towards the ends of the scale, different nutrients will either become more or less available for plants. For example, phosphorus is readily available when soil pH is 6.5; decreasing the pH to 5.5 reduces its availability by half. Also, as soil pH decreases, the activity of beneficial nitrogen-fixing bacteria slows down and many detrimental disease-causing fungi become more active. It’s important to factor pH levels into your fertilizer applications to ensure that nutrients will be available to plants. Often, after a lime application, a lawn or pasture may quickly ‘green-up’. This is due to nutrients already in the soil becoming available during the pH adjustment. -
Review Article on Paleopedology And
PRELIMINARY STUDY OF SOIL SAMPLES FROM IRON AGE NECROPOLES AT CAMPO Christophe MBIDA MINDZIE, Antoine MVONDO ZE, Conny MEISTER & Manfred K.H. EGGERT ABSTRACT This work was undertaken on soil samples of six prospective graves and four ”rubbish pits” from Campo and Akonetye sites. The studied soil samples could be divided into two distinguishing groups. The first was characterized by relatively high values of pH, very high content of calcium, phosphorus and potassium compared to values commonly found in surrounding forest soils. This group was found to correspond to the dump pits, while the second group of samples with low pH, lower content of calcium, phosphorus came from the hypothesised burial places. Key words: soil features, soil analyses, calcium and phosphorus content, dump pits, necropolis, burial. INTRODUCTION The most common features encountered in iron age sites of Southern Cameroon are the so called “rubbish pits”, which seem to be most obviously, a final use of those pits, when the original purposes for which they were dug were over. One of the studied sites located in the vicinity of the Catholic Church at Campo, a small town of south Cameroon revealed specific structures different in their nature from the dump pits. There were dump pits alongside with alignments of overturned clay potteries. The first surveys (ZANA, 2000; OSLISLY et al, 2006) confirmed the latter features were different and their specificity shown by the disposition and types of the artefacts recovered. It was hypothesized they were graves. The preliminary chemical study of soil samples from few pits and those new features was performed to determine the nature of the deposits and how they were deposited, as well as to analyse the context of conservation of artefact in the equatorial soils. -
Soil Acidification
viti-notes [grapevine nutrition] Soil acidifi cation Viti-note Summary: Characteristics of acidic soils • Soil pH Calcium and magnesium are displaced • Soil acidifi cation in by aluminium (Al3+) and hydrogen (H+) vineyards and are leached out of the soil. Acidic soils below pH 6 often have reduced • Characteristics of acidic populations of micro-organisms. As soils microbial activity decreases, nitrogen • Acidifying fertilisers availability to plants also decreases. • Effect of soil pH on Sulfur availability to plants also depends rate of breakdown of on microbial activity so in acidic soils, ammonium to nitrate where microbial activity is reduced, Figure 1. Effect of soil pH on availability of minerals sulfur can become unavailable. (Sulfur • Management of defi ciency is not usually a problem for acidifi cation Soil pH vineyards as adequate sulfur can usually • Correction of soil pH All plants and soil micro-organisms have be accessed from sulfur applied as foliar with lime preferences for soil within certain pH fungicides). ranges, usually neutral to moderately • Strategies for mature • Phosphorus availability is reduced at acid or alkaline. Soil pH most suitable vines low pH because it forms insoluble for grapevines is between 5.5 and 8.5. phosphate compounds with In this range, roots can acquire nutrients aluminium, iron and manganese. from the soil and grow to their potential. As soils become more acid or alkaline, • Molybdenum is seldom defi cient in grapevines become less productive. It is neutral to alkaline soils but can form important to understand the impacts of insoluble compounds in acid soils. soil pH in managing grapevine nutrition, • In strongly acidic soil (pH <5), because the mobility and availability of aluminium may become freely nutrients is infl uenced by pH (Figure 1). -
Ph Meter Guide Ph Is a Measurement of Acidity Or Alkalinity in a Food Using a Numerical Scale from 1 to 14
FACT SHEET #31 pH Meter Guide pH is a measurement of acidity or alkalinity in a food using a numerical scale from 1 to 14. A pH below 7 is acidic, a pH of 7 is neutral, and a pH value above 7 is basic or alkaline. Monitoring pH levels during food processing is an important step in the production of some food since pH values affect microbial growth. Acidity and pH • Electrode: It is the part of the pH meter immersed in the sample. Select an electrode suitable for the food The acidity of food can be determined by measuring you are testing. For instance, some electrodes have its pH value. To preserve food with only acidity, it spear tips that are more suitable for measuring the pH needs to have an equilibrium pH value of 4.6 or lower. of semi-solid food. Equilibrium pH is the pH of a food after all components Use: of the food have achieved the same acidity. • Bench top models are suitable for laboratory use. If the pH meter will be taken into the plant, then a Foods with a pH greater than 4.6 are considered low handheld model may be more appropriate. acid foods. Foods with a pH less than 4.6 can be called acid foods. An acidified food is a low acid food Temperature with acidic ingredients added to it to lower the pH (ex: vinegar). Temperature can affect pH readings. To get an accurate reading, the pH meter must be calibrated at the same pH and micro-organisms temperature as the samples being tested. -
Developing a Non-Glass Ph Meter John Lyon Dr Raouf Selim
Developing a Non-Glass pH Meter John Lyon Dr Raouf Selim PCSE 498 Physics Capstone Project Fall 2014 - Spring 2015 Abstract I intended to develop and test a non-glass pH meter using an ion-selective field effect transistor (ISFET) for this project. The meter would have consisted of the ISFET, a reference electrode, and a voltmeter. The measurements made by this meter should agree with the Nernst equation which relates pH to potential difference. Unfortunately, materials for this project were very hard to come by, most notably, the ISFET itself. In lieu of this situation, I built a glass pH electrode instead. I used a test tube, potassium chloride, and silver wire to make the glass electrode. Upon building this meter, I found that the readings produced were very random and gave no conclusive results on how well the pH meter worked. Introduction I am interested in measuring the pH of a solution over a prolonged period of time. I decided that a non-glass pH meter would be appropriate because it does not contain a liquid solution within it. After some research about pH meters, I discovered that all potentiometric pH meters have a reference electrode, and generally these electrodes contain a reference solution, so my non-glass meter might still require this reference solution. Because I did not want to have an internal solution in my pH meter, I thought it would be interesting to develop a simulated reference electrode along with the non-glass electrode. The non-glass electrode to be used would be an ion-selective field effect transistor (ISFET) electrode. -
Soil Testing: Soil Ph and Salt Concentration
Soil Testing Soil pH and For those soils with a salt pH less than 5.4, the Lime Buffer Capacity (LBC) will be used to determine the soils lime requirement. The new LBC procedure is Salt Concentration described in another soil testing circular, Measurement THE UNIVERSITY OF GEORGIA of Lime Buffer Capacity. COOPERATIVE EXTENSION Colleges of Agricultural and Environmental Sciences & Family and Consumer Sciences College of Agricultural and Environmental Sciences The University of Georgia and Ft. Valley State University, the U.S. Department of Agriculture and counties of the state cooperating. Cooperative Extension, the University of Georgia College of Agricultural and Environmental Sciences offers educational programs, assistance and materials to all people without regard to race, color, national origin, age, sex or disability. An Equal Opportunity Employer/Affirmative Action Organization Committed to a Diverse Work Force Circular 875 Revised August, 2006 Issued in furtherance of Cooperative Extension work, Acts of May 8 and June 30, 1914, The University of Georgia College of Agricultural and Environmental Sciences and the U.S. Department of Agriculture cooperating. J. Scott Angle, Dean and Director D.E. Kissel and P.F. Vendrell Soil pH and Salt Concentration Soil pH is one of the most important measurements concentration, and soil samples collected at this time of soil fertility. It indicates whether a soil could contain of year may, for example, read pH 6.1. In this case, toxic levels of aluminum and manganese, whether it Is there a better way to measure pH? lime would not be recommended. For the same soil may be low in bases such as calcium and magnesium, in a dry winter, more salts may be present in the soil and therefore if lime is needed. -
2105 Soilstik
® SoilStik pH Meter PRODUCT MANUAL Item # 2105 2 Contents General Overview .....................................3 LCD Display................................................4 LCD Display Messages ............................5 Meter Components ...................................6 Calibration .................................................7 Changing the Temperature Units.............8 Taking Liquid/Soil Measurements ...........9 Storing/Recalling Measurements...........10 Sensor Replacement ...............................11 Battery Replacement...............................12 Meter Handling/Troubleshooting ..........13 Specifications .........................................14 Warranty ...................................................15 This manual will familiarize you with the features and operation of your new meter. Please read this manual thoroughly before using your meter. For customer support or to place an order, contact Spectrum Technologies, Inc between 7:30 a.m. and 5:30 p.m. CST. Phone: (800) 248-8873 or (815) 436-4440 Fax: (815) 436-4460 E-mail: [email protected] Website: www.specmeters.com Spectrum Technologies 12360 S. Industrial Dr. East Plainfield, IL 60585 3 General Overview Congratulations on the purchase of your Field Scout™ SoilStik™ Pro Meter. This manual describes how to use your pH meter and keep it working accurately. Read the manual thoroughly in order to make effective use of your meter. The SoilStik delivers high quality answers, with an accuracy of +/- 0.01 pH units. This self-contained digital meter allows you to test the pH levels in water, soil, and other liquids. The replaceable sensor makes the measurement of small samples much more convenient. The sensor provides a visual indication of when replacement is due. The meter has a two-point, automatic calibration (pH 4 and 7), with a range of pH 2.0-12.0. The display will show your results to a resolution of 0.01 pH units. -
Chapter 3 Ph Meter
MAINTENANCE MANUAL FOR LABORATORY EQUIPMENT Chapter 3 pH Meter GMDN Code 15164 ECRI Code 15-164 Denomination pH Meter The pH meter is used for determining the concentration of PHOTOGRAPH AND COMPONENTS OF THE hydrogen ions [H+] in a solution. This equipment, provided pH METER it is carefully used and calibrated, measures the acidity of an aqueous solution. pH meters are sometimes called pH analysers, pH monitors or potentiometers. 2 1 PURPOSE OF THE EQUIPMENT The pH meter is commonly used in any field of science related to aqueous solutions. It is used in areas such as agriculture, water treatment and purifi cation, in industrial processes such as petrochemicals, paper manufacture, foods, pharmaceuticals, research and development, metal mechanics, etc. In the health laboratory, its applications are related to the control of culture mediums and to the measurement of the alkalinity or acidity of broths and buff ers. In specialized laboratories, diagnostic equipment microelectrodes are used to measure the pH of liquid blood components. The plasma pH allows the patient’s health to be evaluated. It normally measures between 7.35 3 and 7.45. This value relates to the patient’s metabolism in which a multitude of reactions occurs where acids and 1 Electrode carrying arm and electrode bases are normally kept in balance. Acids constantly liberate 2 Digital display + 3 Control panel with temperature adjustment control, mode hydrogen ions [H ] and the organism neutralizes or balances selection (Standby/mV/pH) and calibration controls – acidity by liberating bicarbonate ions [HCO3 ]. The acid-base ratio in the organism is maintained by the kidneys, (organs courtesyPhoto of Consort in which any excesses present are eliminated). -
Buffers and Titrations
Chapter 2: Buffers and Titrations Purpose: 1) Get to know your pH meter 2) Make a common buffer used in biochemistry and perform titrations of that buffer with acid or base to find the pKa values for the buffer 3) Hydrolyze BSA with trypsin and calculate the number of Lys and Arg residues that BSA contains pH Meter ● Glass-electrode sensitive to hydrogen ions ● Electrode somewhat sensitive to other alkali metals ● Complete system contains: ● Electrometer – 5 ● Reference Electrode – 6 ● Solution to be measured – 1,4 ● Glass Electrode – 2,3 Titration Curves in Non-buffered Solutions Weak Acid = ● Equivalence Point 0.1 M Acetic Acid ● Point at which reaction is Strong Acid = neutralized 0.1 M Hydrochloric Acid ● Inflection point in titration curve ● Strong Acid – pH 7.0 ● Weak Acid – pH 8.8 ● Buffered solutions behave as weak acids ● Table of pKa values – Lab Manual p. 36 pH Changes in Buffered Solutions pKa of Buffer + More H More -OH present present Begin deprotonating buffer Titration ends Titration begins Add Fully deprotonated buffer with an acidic pH -OH at basic pH Acidic pH of the Solution Basic Buffered Titration Curve Titration of a Buffer 8 ● Modeled on 7 Henderson- Hasselbach 6 equation 5 4 pH 3 2 1 0 0 20 40 60 80 100 120 Quantities of -OH Added Buffered Titration Curve Titration of a Buffer 8 ● Empirically, H-H 7 equation useful 6 for buffering 5 range 4 ● Buffers most pH 3 effective near pKa 2 1 0 0 20 40 60 80 100 120 Quantities of -OH Added - pH = pKa when [A ] = [HA] Buffering Capacity ● Ability of buffer to resist changes -
Ph, Conductivity/TDS & DO Meters
M pH, Conductivity/TDS & DO Meters POCKET PAL METERS® Handheld, lab accurate and modestly priced, the Pocket Pal meters are an industrial standard. Pocket Pal series elec- trodes are field replaceable and usually can be changed and calibrated in a matter of minutes. Digital displays, rugged ABS plastic housings and precision two-point calibration potentiometers make all seven Pocket Pals perfect for field, plant or laboratory use. With Automatic Temperature Compensation standard (except PH-2), accurate response is just seconds away. Each Pocket Pal comes equipped with a 9-volt battery, calibration screwdriver, instruction card and a handy belt loop case. DUAL pH & CONDUCTIVITY - THE MOST POPULAR POCKET PAL METER DSPH-1 and DSPH-3 POCKET PAL meters measure pH and conductivity in a compact one-hand operation. There are no electrode cables to fool with. The electrodes simply fold under the instrument for storage. Two test buttons control all opera- tions. Temperature variations are automatically compensated for both pH and conductivity measurements. Easy screwdriv- er adjustments include Cal and Slope for pH, and Zero and Span for conductivity. The POCKET PAL operates on a 9-volt Water Quality / Analytical Water battery (included). DSPH-1/DSPH-3 METER Dimensions (Electrodes folded): For versatility in the field or the laboratory, the 159 mm L X 32 mm D (6.25" X 1,25"; DSPH-1US/1PPM and DSPH-3US/3PPM fea- 32 mm W (1.25") Handle; 57 mm W (2.25") LCD ture pH, conductivity and total dissolved solids Electrode Lengths (vertical or horizontal): measurements in one handheld instrument. The * 127 mm L (5"); 9.5 mm dia (3/8") DSPH-1US/1PPM measures pH from 0-14 and Power: One 9 V battery conductivity from 0 to19,999 in μmhos or ppm, *(Electrodes are independently interchange- and the DSPH-3US/3PPM extends the conduc- able by the user) tivity measuring range to 199,999 in μmhos or ppm. -
Soil Food Web: Implications to Soil Health
Soil Food Web: Implications to Soil Health Dr. Sajeemas “Mint” Pasakdee, Soil Scientist/Agronomist Advisor, Student Operated Organic Farm CIT-Jordan College of Agri. Sci. & Tech., Fresno State 1 Outline • Soil organisms and their interactions • What do soil organisms do? • Where do soil organisms live? • Food web structure • When are soil organisms active? • How is the food web measured? • Living soils—Bacteria; Fungi; Earthworms • Soil Environment 2 Organisms & Their Interaction 3 4 What do soil organisms do? Soil organisms support plant health as • decompose organic matter, • cycle nutrients, • enhance soil structure, • control the populations of soil organisms including crop pests. 5 Organic Matter • Food sources for soil organisms • Agricultural top soil ~1-6% (In CA, ~1-3% SOM) 6 Where do soil organisms live? • Around roots(rhizosphere) • Plant litter (C sources) • Humus (stabilized organic matter) • Surface of soil aggregates 7 Typical Food Web Structure • bacterial-dominated food webs o Grassland & Agri Soils o Ratio of fungi to bacteria, ~1:1 for productive agri. soils • fungal-dominated food webs o Ratio of fungal to bacterial, ~5:1 to 10:1 in a deciduous forest and 100:1 to 1000:1 in a coniferous forest 8 9 When are soil organisms active? 10 How is the food web measured? • Counting. Organism groups (bacteria, protozoa, arthropods, etc.); or subgroups (bacterial-feeding, fungal-feeding, and predatory nematodes), are counted and through calculations, can be converted to biomass. • Measuring activity levels. The amount of by-products, i.e., respiration (CO2); nitrification and decomposition rates • Measuring cellular constituents. Biomass carbon, nitrogen, or phosphorus; Enzymes; Phospholipids and other lipids; DNA and RNA 11 12 Soil Bacteria • One-celled organisms – generally 4/100,000 of an inch wide (1 µm) • A teaspoon of productive soil generally contains between 100 million and 1 billion bacteria (~two cows per acre).