illustration: Steri-Fix E

Thermal Wastewater Sterilisation AND Deactivation envirochemie - International competence in water and wastewater technology

Reliable and innovative technology for water and wastewater treat- Thus, we ensure that local needs for innovative and environmen- ment is what we stand for. As partners to the industry, we develop tally friendly water and wastewater technology are always satis- and implement customised solutions for our customers. fied. We concentrate our efforts in meeting the individual require- ments of each of our customers. We are an engineering company and offer a holistic range of ser- vices based on our long international experience. We have always We supply highly qualitative “Made in Germany” products based our clients on focus and assess them in the design, planning, engi- on chemical-physical, biological and membrane filtration pro- neering, building and commissioning of our plants. We remain al- cesses, whose state of the art relies on our long list of research ways close partners. Regardless if it is a common research project achievements and patents. Additionally, more than 25,000 plants or the operation of the wastewater treatment plant, we are always sold worldwide have provided us with the necessary know-how for nearby. Our commitment knows no limits, taking us to even accept further continuous development of innovative and reliable industrial the responsibility of taking over the whole water management in water and wastewater technologies. situ. Our international activities are supported by seven develop­ ment and production sites in Germany and . Together with our international sales and service offices, we are represented at fifteen different locations.

EnviroDTS in Friedberg (Germany)

EnviroChemie in Rossdorf (Germany)

Russia Sweden

Netherlands Germany

Austria Romania Switzerland

Spain

Brazil

2 ENVIRO Dts - RELIABLE TECHNOLOGY FOR thermal wastewater sterilisation and deactivation

EnviroChemie offers –through its subsidiary EnviroDTS in Friedberg (Germany)– intelligent solutions for a realiable and decentralised waste­ Our expertise and solutions at water treatment in biotechnology and healthcare facilities. These your service include: effluents are commonly characterised by their high or very high bioha- zard risk. Our EnviroDTS wastewater treatment plants are optimal for  Decontamination laboratories (even containment level 3 and 4 laboratories), universities, of radioactive wastewater research facilities, industrial applications, government agencies (e.g. ani-  Neutralisation mal disease control agencies) and healthcare facilities.  Precipitation EnviroDTS plants are designed to safely deactivate, sterilise or disin-  Ion exchange fect wastewater containing infectious or genetically altered materials via  Thermal disinfection thermal sterilisation. Simultaneously, microorganisms and bacteria are  Chemical disinfection eliminated in this process, while at the same time viruses, plasmids and  Softening DNA fragments can be deactivated. The EnviroDTS sterilisation process  Complete desalination additionally ensures an optimal sterilisation output at the most efficient  Ultra-filtration energy input.  Nano-filtration 30 years experience and a know-how based on circa 1000 reference in-  Reverse osmosis stallations blend the advantages of an innovative and proven technology  Electro-deionisation with a flexible process control.

3 s TeriFIX c

EnviroDTS SteriFix C 500 at the State Office for Consumer Friedrich-Loeffler-Institut in Jena (Germany) Protection in Saxony, located in Dresden (Germany)

SteriFix C 500 with steam generator (built in ISO shipping SteriFix C 2500 at the Friedrich-Loeffler-Institut in Jena ­containers) at the State Office for Food Monitoring and Con­ ­(Germany). Performance: 12 m³/d sumer Protection in Rostock (Germany)

SteriFix C – Batch technology for a safe Wastewater sterilisation

SteriFix C wastewater treatment plants are optimal for vol- By doing so, the heat of larger wastewater amounts can be umes up to 10 m3 per day. By using the EnviroDTS batch reused, and the cooling demand, that is required to reach the technology, all the desired retention times and sterilisation output temperature (sewer), is reduced. temperatures of up to 180°C can be reached, thereby achiev- ing a very high deactivation effectiveness. Additionally, the safety of the system is improved through re- dundant design. Nevertheless, in situations where very limited Wastewater is heated in this plants to the targeted sterilisa- room is available, a single container system can also be imple- tion temperature using either steam injection (SteriFix types mented. C 500 and C 2500) or –for smaller wastewater amounts– an electric heater (SteriFix C 100). Since safety has always the highest priority, a sterile filter at the air vent is installed to guarantee the sterility of the Highest energy efficiency is achieved by implementing a exhaust air coming out of the equipment. Moreover, a design special equipment design with the most modern process free of dead volumes with integrated magnetic stirrer or cir- technology, which includes the combination of two double culation pump ensures the safe sterilisation of every single jacketed vessels. drop of water.

4 s TeriFIX c

SteriFix C 2500 with two sterilisers at the vaccine factory The compact plant SteriFix C 100 for a maximum of 100 litres Impfstoffwerk Dessau GmbH in Rodleben-Tornau (Germany) per day and equipped with electrical heating and SPS S7 control system

I nstallation of a SteriFix C 2500 in a vaccine production Advantages of this technology: facility  Flexible operation The company Impfstoffwerk Dessau GmbH in Rodleben-  Limited operating and investment costs Tornau develops and produces high quality animal vaccines  No risk of bacterial contamination of treated water and veterinary drugs in Germany. Their products are exported  The plant can function under pressure, so that there worldwide. A broad palette of vaccines for domestic and farm is no need of an additional pumping station animals as well as certain pharmaceuticals for reproduction  Insensitive to the presence of solids in the wastewater control and parasitic prophylaxis characterise the product  Sterile air exhaust portfolio of Impfstoffwerk Dessau GmbH in the animal health sector. Wastewater generated at this facility cannot be discharged di- Characteristics: rectly into the sewer. For the disinfection of this occasionally produced and highly infectious wastewater, EnviroDTS de-  Complies all EU standards signed and built a thermal deactivation plant based on batch  Optimal for wastewater containing solids technology.  Easy validation Incoming wastewater leaves the stainless steel buffer tank  Safe sterilisation procedure and enters one of the two available sterilisers. Steam is di-  Wastewater volumes up to 10 m3 per day rectly injected into the wastewater to raise the temperature.  Avoidance of cross streams through leakage control Both temperature and retention time are closely monitored  Plant can be completely sterilised and recorded throughout the whole process.

The water-glycol mixture within the jacket space is used for heat recovery and to cool the batch. This mixture goes from Technical performance: the first to the second sterilizer and warms it up. For further cooling, additional coolants (e.g. an air cooler) may be used.  No dead volumes (100% safe sterilisation)  Temperature and time are variable and are monitored throughout the process SteriFix C 100 for a maximum of 100 litres  Electrically heated sterile air filter  Pneumatic draining, i.e. no need of pumping station The smallest of our plants, the SteriFix C 100, can be ap-  Free of clogging due to double jacket technology plied to wastewater volumes as low as 100 litres per day, and steam injector which are free of suspended solids. It has a double jacketed  Siemens SPS S7 control system steriliser with electrical heating. A magnetic stirrer ensures  Output temperature > 35°C a thorough mixing. After the sterilisation is completed, the  Plug valves without dead volumes sterilised wastewater is cooled down using coolants which  High operational safety due to redundant plant design are circulating inside the jacket space.

5 s TeriFIX E

Particularly large SteriFix plant at the Paul-Ehrlich Institute in CIP Station at the Clinic Großhadern, München (Germany) Langen (Germany). Performance 2 x 10 m³/h / 121°C / 20 min.

SteriFix E 250 at Phyton Biotech GmbH, Ahrensburg Retention phase at the CODA Institute of Veterinary, (Germany). Performance 250 l/h / 134°C / 2 min. Machelen (Belgium). Performance 3 m³/h / 121°C / 20 min.

SteriFix E – Continuous and reliable wastewater sterilisation

SteriFix E wastewater treatment plants are optimal for treat- ment of continuously incoming wastewater at amounts up to 120 m3/d. Using the EnviroDTS continuous process technol- ogy, the energy needed for sterilisation can be minimised by means of an effective heat recovery system.

Incoming wastewater is firstly pre-heated using the high temper- ature of the disinfected effluent leaving the plant. Directly after that, it is warmed up to the necessary sterilisation temperature using a steam injector. Due to this effective heat exchange be- tween outlet and inlet, the temperature at the discharge point is thus reached without any additional cooling. The disinfection process is monitored and regulated by the retention time and the output temperature. A sterile filter at the air vent ensures the sterility of the exhaust air. A design without dead volumes guar- antees a safe sterilisation at low operational costs. Robust and reliable equipment design results in a high availability of the plant. Design for a two phase SteriFix E 3000 (2 x 3000 l/h), University of Wageningen, CIDC Lelystad ()

6 s TeriFIX E

Straight tube heat exchanger with 1.2 m3/h at Roche in Penz­ Buffer tank with retention and cooling stage at Roche in Penzberg berg (Germany) (Germany)

SteriFix E 1000 at Roche‘s production site in Penzberg A dvantages of this technology: (Germany)  Flexible (continuous) operation Roche is a well-known biotechnology company specialised in  Energy efficient the research, development and the production of pharmaceu-  Limited operating and investment costs ticals. At its location in Penzberg, Roche has one of the largest  Minimal space requirements biotechnology centres in Europe. This production site focuses  No risk of bacterial contamination of treated water on cancer research as well as therapeutic protein agents.  Insensitive to the presence of solids in the wastewater Wastewater at Penzberg needs to be thermally deactivated  Sterile air exhaust before it may be discharged to the sewage system. This is done continuously using a SteriFix E 1000 plant. Characteristics: Process description  Complies all EU standards The plant in Penzberg has two buffer tanks each 11 m³.  Safe sterilisation procedure with special measurement Wastewater is brought in over a straight tube heat exchanger,  Wastewater volumes up to 120 m3 per day which uses the heat from the already deactivated wastewa-  Avoidance of cross streams through leakage control ter coming out of the treatment plant. Operating expenses  Plant can be completely sterilised can be reduced to a minimum thanks to this heat recovery system.

To attain the deactivation temperature, steam is injected into Technical Performance: the pipes. The actual inactivation occurs in the retention sta- ge. A special validation system guarantees a safe compliance  Compact design with the retention time being required. The retention time is  Efficient heat recovery system monitored all through this stage.  No dead volumes (safe sterilisation)  Leakage monitoring of the heat exchanger After the deactivation has been fulfilled, the effluent is cooled  Monitoring of temperature and retention time down in the straight tube heat ex-  Limited operating expenses through optimal heat recovery changer as already described before.  Very low noise level  Electrically heated sterile air filter  Spiral heat exchanger for wastewater containing solids Open spiral heat exchanger for can be optionally delivered wastewater with very high solid  Siemens SPS S7 control system content at a vaccine factory in  Output temperature > 35°C Lelystad (Netherlands)  Stand-by operation (no cooling / no initialisation time) 7 T echnical specifications sTERIFIX c

E TnviroD S SteriFix C 100 C 500 C 500 C 2500 1 steriliser 2 sterilisers

Performance Up to 500 l/d 500 to 2500 l/d 1000 to 3000 l/d 2500 to 12000 l/d

Volume per batch 100 l 500 l 500 l 2500 l

Electric heating 6 kW Upon request Upon request Upon request Steam heating 25-150 kg/d 150-750 kg/d 250-850 kg/d circa 2500 kg/d

Coolant needed 7000 l/d 8500 l/d 11000 l/d 42700 l/d (temp. difference 6 °C)

Electrical power 11 kW (electrical heater) 2 kW (steam heating) 4 kW (steam heating) 4 kW (steam heating)

Dimensions in mm 1000 x 1000 x 1500 1500 x 2000 x 2500 3000 x 2000 x 2500 3000 x 4000 x 3000 (L x W x H)

Options: Fields of application (examples):

 Electrical steam generator  Veterinary facilities  Air cooling, if no coolants are available  Food safety control institutes and laboratories  Shredder pump for solid containing wastewater  Vaccine production (animal tests)  Security pans with leak sensors  Research facilities (biotechnology and gene technology,  Pressurised air generation for pneumatic valves virology, hygiene, pathology, epidemiology, etc.)  Neutralisation of effluent, depending on pH-value  Security laboratories and research facilities with  Softening a containment level up to S4  Buffer tank PP / stainless steel  Quarantine areas  Botanical and animal research institutions  10 m³/d maximum wastewater flow (with high solid content)

8 T echnical specifications sTERIFIX e

E TnviroD S SteriFix E 250 E 500 E 1000 E 3000

Performance 250 l/h 500 l/h 1000 l/h 3000 l/h

Heating steam (5 bar) 35 kg/h 50 kg/h 80 kg/h 240 kg/h

Electrical power 2.5 kW 3 kW 4 kW 5 kW

Dimensions in mm 2500 x 1500 x 1800 3500 x 2000 x 1800 4000 x 3000 x 1800 4000 x 5000 x 2000 (L x W x H)

Heat exchanger Shell and tube heat Free flow plate heat Spiral heat exchanger Spiral heat exchanger (depending on solids exchanger exchanger content)

Validation system Yes (NaOH) Yes (NaOH) Yes (NaOH) Yes (NaOH)

Options: Fields of application (examples):

 Buffer tank (PP / stainless steel)  Pharmaceutical industry  Validation unit for monitoring the actual retention time  Food safety control institutes and laboratories  Straight tube heat exchanger for wastewater containing  Vaccine production solids  Research facilities (biotechnology and gene technology,  Spiral heat exchanger for wastewater with a high solids virology, hygiene, pathology, epidemiology, etc.) content  Security laboratories and research facilities  Electrical / gas driven steam generator with a containment level up to S3  Fully automatic CIP system (cold or warm)  Botanical and animal research institutions  Shredder pump for wastewater containing solids  High wastewater flows  Retention stage with smaller nominal diameter for  Ideal for applications with limited space available wastewater with a high solids content (e.g. sand) and bad accessibility (e.g. small cellars)  Heat exchanger for cooling in case of too high input temperatures  Complete sterilisation of the entire plant

9 tds

TDS 60 decentralised thermal TDS 30 twin decentralised thermal sterilisation sys­ sterilisation system equipped with tem equipped with two chambers (30 litres each) a single chamber (60 litres). and installed at the Federal Institute for Risk Assess­ nebt in Berlin (Germany). The two chamber system allows the system to work continuously.

TDS Equipment for Decentralised Wastewater Thermal Sterilisation

This kind of decentralised sterilisation systems are used, for ex- Specifications: ample, in S3 and S4 security laboratories. In these laboratories,  Stainless steel sink with a touch-free faucet wastewater has to be inactivated before it can be discharged fol-  Fully automatic system with a status indicator on the display, lowing very strict safety regulations. TDS 60 and TDS 30 twin are e.g. procedural step, error message, date/time and limits the optimal solution for flexible and decentralised wastewater  Documentation ability with a 4-point-matrix printer, sterilisation within the laboratory. Thereby long and unsafe trans- 20 characters per row for a hardcopy of the batch number, port paths to a centralised treatment system can be avoided. date, time, sterilisation parameters, etc. Options:  Fully automatic filling and automatic program start for the sterilisation  High performing cooling system by using fresh water or  Sterilised wastewater is automatically drained and other external coolant cooled (< 50°C) before being discharged to the sewage  2 sinks with automatic warm water inlet and level monitoring  Floor collecting pan with a moisture indicator and an  Connection for showers and eye showers automatic water shutoff  Documentation for the RS 232 interface to connect  TDS 30 twin can be operated continuously, since it is to a computer outside of the laboratory (S3) equipped with 2 autoclaves, which can sterilise alternately  Isolated system for error messages  Pneumatic valve with no dead volumes  Touch panel for an improved representation of the process  Level gauge and signal at a residual amount lower  Metal mirror and dispenser for soap and disinfection agent than 10 litres  Oil-free and dust-free pressurised air at 6 bar

T ype Volume Operational Dimensions Weight Heating Electrical Availability (mm, L x W x H) Connection

TDS 60 60 litres After 90 minutes 750x600x1500 240 kg 6.75 kW 400 V / 16 A

TDS 30 twin 2x30 litres Continuous operation 1400x700x1150 350 kg 12 kW 400 V / 32 A

10 Overview of a BioChroma plant for radioactive wastewater Overview of a delay and decay plant for radioactive wastewater biological treatment at hospitals treatment at healthcare facilities

ENVIRODTS - MORE THAN 30 YEARS DELIVERING WASTEWATER AND WATER TECHNOLOGY SOLUTIONS to the healthcare, biotechnological, pharmaceutical and research sectors

Reverse osmosis plant built in a modular way Mini-Fix, the solution for a flexible and decentralised wastewater neutralisation of up to 300 L/h

Plant equipped with both cationic and anionic exchangers for Neutralisation plant for centralised laboratory wastewater full water desalination treatment 11 www.envirochemie.com /www.envirodts.de [email protected] 8463066 2 +359 Fax 8463065 2 +359 Tel. Sofia 1705 3 Stock 7, App. ria 100 Georgiev Evlogi Bul. viroChemie Bulgarien E Bul [email protected] 24414393 21 +55 Tel./Fax RJ - Janeiro de Rio 22710-552 Curicica/Jacarepaguá 1280 Curicica, de Estrada E viroChemie E Brazil [email protected] 5345741 23 +31 Fax 5345405 23 +31 Tel. Haarlem BP 2031 c 52 Waarderweg rland viroChemie BV E t N [email protected] 2861800 55 +41 Fax 2861818 55 +41 Tel F Eschenbach/SG 8733 r T EN Switzerland i F T 6 I E Germany [email protected] n den Leppsteinswiesen 9 Leppsteinswiesen den n wirrenstrasse 6 wirrenstrasse 11 6998 6154 +49 ax 0 6998 6154 +49 el. Rossdorf 4380 n n n nviroChemie GmbH(HeadQuarters) s e pecializados pecializados V I h g O e a A L K

A T

r L G atamentos s t da.

[email protected] 2282579 343 +7 Fax 2282578 343 +7 Tel. Ekaterinburg 620026, viroChemie GmbH 6 Floor 83, Belinskogo Ul. a S 000 R [email protected] 8463845 22 +48 Fax 8463841 22 +48 Tel. Warschau 02-235 9A Równolegla ul. viro-Chemia Polska Sp. z.o.o. and E P [email protected] 7404415 41 +41 Fax 7404414 41 +41 Tel. F Cham 6330 r G EN [email protected] 3112871 21 +40 Fax 3112870 21 +40 Tel. Bukarest 711212 S viroChemie E mania R [email protected] 6998-40/-41 6031 +49 Fax 7318-0 6031 +49 Tel. Friedberg 61169 22 Pfingstweide E n n n tr. Visarion Nr. 13 Nr. Visarion tr. o ewerbestrasse 5 ewerbestrasse u O viro V l s E I n D O i T S A GmbH L K

A R G o mania S R L Fax +43 732 370334 732 +43 Fax 370332 732 +43 Tel. Wien 1010 8-10 Kohlmarkt A viroChemie ria E A [email protected] 6270301 40 +46 Fax 6270300 40 +46 Tel. Malmö 21119 19 Skeppsgatan Filial till Vattenrening E Sweden E [email protected] 9908-50 2663 +49 Fax 9908-0 2663 +49 Tel. Westerburg 56457 7 Gutenbergstraße n C n b u viroF wasserreinigungs Ges.m.b.H. s t A E L n K viroChemie GmbH GmbH T y skland

EC VK P 0031 GB