I. TRIR Experiments (Step-Scan FTIR Set Up)

IR Inventory MAMOO 2006

I. TRIR Experiments (Step-Scan FTIR set up)

 Nicolet Nexus 870 FTIR Spectrometer and PC.  TOM kit.  Kolmar Technologies, Inc. MCT (HgCdTe) detector (Model No. KMPV11-1- J1/dc).  Lambda Physik OpTex excimer laser (XeCl, 308 nm).  Quanta-Ray INDI Pulsed Nd:YAG Laser.  Stanford Research Systems, Inc. pulse generator (Model No. DG535).  Stanford Research Systems, Inc. pre-amplifier (Model No. SR560).  Tetronix two-channel oscilloscope (100 MHz, Model No. TDS 320).  On Loan from Thermo Electron: TRS MCT-A detector (1 mm, 20MHz, 50 ns rise time).

A. Step-Scan FTIR in solution

 Harrick demountable liquid cell (25 mm windows, Model No. DLC-M25)

 6 Harrick CaF2 windows (size: 25 mm x 2 mm, Part No. WFD-U25).

 6 Crystan Ltd CaF2 windows (size: 25 mm x 2 mm, Order No. XA1E1Z)  Assorted Harrick Teflon spacers (diameter: 25 mm, thickness(quantity): 6(1), 12(1), 25(1), 56(1), 100(1), 250(1), 390(1), 500 (10), 630(1), 750(1), 950(12).  Harrick demountable liquid cell plus stainless steel spacers (13 mm windows, Model No.).

 4 Harrick CaF2 windows (size: 13 mm x 2 mm, Part No. WFD-U22).  Series 180 Micropump (G184) plus drive (HG0024) and power supply.  2 clear flow system glass vessels (Omnifit) with 4 valve caps.  2 clear flow system glass vessels (Omnifit) with 8 valve caps.

II. FTIR Experiments

A. Diffuse Reflectance FTIR

 Smart Collector (Diffuse Reflectance Accessory) for Nexus 870 FTIR Spectrometer plus temperature controller and dual sample environment chamber.  Spectra-Tech Diffuse Reflectance Accessory (Model No. 0032-032).  Perkin Elmer Diffuse Reflectance Accessory (Model No. 0186-2765).

B. FTIR in solution/film  2 Thermo Nicolet/Spectra-Tech, Inc FTIR demountable liquid cell kits (Model No. FT04-036).  Assorted Thermo Nicolet Teflon spacers (diameter: 32 mm).

 3 Thermo Nicolet CaF2 windows (size: 32 mm x 3 mm, Part No. 7000-453).

 2 Thermo Nicolet/Spectra-Tech, Inc.CaF2 windows drilled (size: 32 mm x 3 mm, Part No. 7000-468).  2 KBr windows (size: 25 mm x 2 mm)  Spectra-Tech, Inc. Presslok holder for 32 mm windows (film FTIR) (Model No. 0018-014).

C. FTIR in KBr, Nujol mulls etc.

 Spectra-Tech, Inc. Magnetic KBr pellet holder (Model No. 0016-008).  4 Wilks Infrared Accessories/ Perkin Elmer pellet press (manual) and holder.  5 Spectra-Tech, Inc. agate pestle and mortar kits (Part No. 0026-105).  Spectra-Tech Inc. Nujol (Part No. 0026-110).  Electric Grinder plus Spectra-Tech, Inc. vial (Part No. WIG-3114).  Pellet making and pressing facilities also available in Chemical Engineering (c/o Prof. Lavicky. Rm 801).