XRD (X-Ray Diffractometer)

D8 ADVANCE (BRUKER) X-ray (XRD) is a high-tech, non-destructive technique for analyzing a wide range of materials, including fluids, metals,minerals, polymers,catalysts, plastics, pharmaceuticals,thin- film coatings, ceramics, solar cells and semiconductors. Throughout industry and research institutions, XRD has become an indispensable method for materials investigation, characterization and quality control. Example areas of application include qualitative and quantitative phase analysis, , structure and relaxation determination, texture and residual stress investigations. The Bruker D8 X-ray diffractometers are designed to easily accommodate all X-ray diffraction applications in material research, and high resolution diffraction. All new D8 goniometer are equipped with stepper motors with optical encoder to ensure extremely precise angular values. The D8 X-ray diffractometer can be used for nearly all X-ray diffraction application, such as structure determination, phase analysis, stress and texture measurement. The XRD at IIT Roorkee has catered to the need of various workers from all over India for the last many years. There is power as well as thin film XRD facility here with following features mentioned below.

Powder XRD:

Features:

• Computer controlled diffractometer and thus used for automatic operation. • High temperature (RT- 16000 C) in-situ XRD facility • Angle range: 50 -1200 • Target (Cu, Mo, Fe) • Scintillation counter detector. • Lynex eye detector controller. • Accelerating voltage up to 40KV • Electron probe current range up to 40mA • Sample spinners. • Nine sample can be simultaneously placed in sample holder. • Leptos and EVA software provide a common look and feel for measurement and analysis software

Contact Person: Mr.Shiv Kumar Office Tel: 01332-286302 Email id: [email protected] Charges Glancing Angle XRD:

Features: • Computer controlled diffractometer and thus used for automatic operation. • XRD grazing incidence. • Angle range 50 -1200 • Target : Cu • Accelerating voltage up to 40 KV • Electron probe current range up to 40mA • Leptos and EVA software provide a common look and feel for measurement and analysis software

Contact Person:

Mr. Paritosh Dubey Office Tel: 01332-286291 Email id:[email protected]

Charges

Single Crystal X-ray Diffractometer:

Bruker Kappa APEX II

This instrument has following components:

 Kappa 4-circle goniometer  APEX II CCD detector  X-ray generator (K780) having both Mo and Cu tube  Low temperature facility for data collection  Apex2 software for data acquisition and processing

This is one of the best systems for characterizing the chemical & mineral structures of a single crystal. This system has applications in the field of biotechnology, chemistry, physics, metallurgy etc.

Contact Person:

Dr. U P Singh (Dept. of Chemistry) Office Tel: +91-1332-285329 Emai id: [email protected]

Charges