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Acetylferrocene, Alkali flame detector determination of, 538, 539, 541 for, Acetylene, organolead compounds, 406 determination of arsine in, organosilicon compounds, 236 490, 491 organotin compounds, 345 Active hydrogen, Alkidane tri-carbonyl chromium determination of in compounds, dichlorodimethylsilane, determination of, 517 252-253 Alkoxy groups, organoboron compounds, 74 in organosilicon compounds, 104-111 determination of, 252 organosi1icon compounds, Alkyl groups, 222-223, 252, 284 in organosilicon polymers, Active sites on separation determination of, 262-268, 284 columns, 306-307 Alkoxysilanes, Air, determination of, 178-218 determination of, reaction gas chromatography of, alkyl mercury compounds in, 252 343 Alkylaluminium compounds, diethylmercury in, 73 determination of, 7, 113-128 ethylmercury dicyanidamide Alkylantimony compounds, in, 73 determination of, 7 organo1ead compounds in, Alkyl arsenic acids, 399-404, 415-432, 450 determination of, 476 organomercury compounds in, microwave plasma detector for, 73 476 dimethyldiselenide in, 525 Alkylarsines, dimethylselenide in, 525 determination of, 452-472 Alcoholysis-hydrolysis Alkylberyllium compounds, of, determination of, 7 alkylaluminium compounds, Alkylboron compounds, 114-121 determination of, 7, 74-83 alkylzinc compounds, 19-20 Alkylbromosilanes, Algae, retention data of, 139 determination of organomercury Alkylchlorosilanes, compounds in, 50 determination of, 160-178 NMR of, 164-165

569 570 INDEX

A1ky1ch1orosi1anes (continued) Apples (continued) determination of (continued) determination of (continued) retention data of, 139-176 organomercury compounds in, A1ky1cyc1osi1oxanes 31-34 determina.tion of vinyl groups Arene tricarbony1 chromium in, 255 compounds, pyrolysis-gas chromatography determination of, 491-518 of, 255 glow discharge detector for, Alkyl dise1enides, 519 determination of, 519-525 NMR of, 512-513 A1ky1germanium compounds, pyrolysis of, 502, 505-507 determination of, 295-299 retention data for, 514 retention data of, 295-299 Argon plasma detector, Alkyl groups in organosi1icon for, compounds, organomanganese compounds, determination of, 252, 284- 526, 532 294 Arsanilic acid, A1ky1ead compounds, determination of, 489 determination of in gasoline, Arsine, 361-451 determination of, 483, 489-490 x-ray fluorescence of, 376, Arsine, 378 determination of in, A1ky1magnesium compounds, acetylene, 489 determination of, 8-18 silane. 489 determination of in, Ary1arsines, blood, 36 determination of, 452-472 fish, 61-70 Ary1ch1orosi1anes, hair, 36 determination of, 160-178 marine sediments, 36 Ary1magnesium compounds, urine, 36 determination of, 8-18, 28-73 A1ky1si1anes, Ary1mercury compounds, determination of, 129-156 determination of in, reaction gas chromatography fish, 61-70 of, 252 Ary1tin compounds, retention data for, 129-156 determination of, 316-323 A1ky1tin compounds, retention data of, 316-323 determination of, 316-323 Ary1tricarbony1 chromium compounds, retention data of, 316-323 mass spectrometry of, 507-511 A1ky1tinha1ides, Ary1trimethy1si1anes, determination of, 320-322, 343 thermal decomposition of, 136 A1ky1tin hydride compounds, Ary1si1anes, determination of, 313 determination of, 129-156 A1ky1zinc compounds, pyrolysis-gas chromatography determination of, 7, 19-28 of, 272-284 Aluminium a1koxides, reaction gas chromatography determination of, 114 of, 252, 272-284 Antimony tetraethyl, retention data of, 129-156 determination of, 406 thermal decomposition of, Apples, 272-284 determination of, Atomic absorption detector for, INDEX 571

Atomic absorption detector for, Bis(tributyltin) oxide, (continued) determination of, 343 organoarsenic compounds, 458- pyrolysis-gas chromatography 472 of, 343 organolead compounds, 367, 4l6-Bis(triethylgermanyl) sulphide, 425 determination of, 300 organomercury compounds, 56-60 Bis(triethylselenyl) sulphide, organoselenium compounds, 524 determination of, 525 Bis(triethylsilyl) sulphide, Benzene, determination of, 232 determination of in, Bis(trimethylgermanyl)ethylene, organosilicon compounds, 234 determination of, 299, 233 silicon tetrachloride, 234 Bis(trimethylsilyl)acetamide, trichlorsilane, 234 determination of, 232 Benzenestannoic acid, 1,2-Bis(trimethylsilyl) ethylenes, determination of, 323-331 determination of, 233 Benzene tricarbonyl chromium, Blood, determination of, 491, 493-498, determination of organomercury 507-513, 517 compounds in, 36, 47, 61- Benzyltrimethylsilane, 70 pyrolysis gas chromatography Borazoles, of, 275-276 determination of, 83-90 reaction gas chromatography determination of active hydrogen of, 275-276 in, 111-112 Bile, Boron halides, determination of organomercury determination of, 74, 111-113 compounds in, 47, 50 Boron hydrides, Biological materials, detection by, determination of organoarsenic flame photometric dector, 95 compounds in, 56, 489 determination of, 74, 90-95 Biphenyl, determination of boron- determination of, hydrogen bonds in, 106-107 in organosilicon monomers, Boron-hydrogen bonds, 234 determination of in, Bis(diethylbenzene)molybdenum, organoboron compounds, 104-107 determination of, 519 Boron pentafluoride, Bis(dimethylmercury) sulphide, determination of, III determination of, 54 Boron trichloride, 1,4-Bis(dimethylsilyl) benzene, determination of, 95-103, 111-112 determination of, 233 impurities in, 112 Bis(4-dimethylsilylphenyl) ether, retention time of, 112 determination of, 233 Bromoarsines, Bis(ethylbenzene) molybdenum, determination of, 452-457 determination of, 519 retention data for, 453-457 impurities in, 519 n-Butylbenzene tricarbonyl chromium Bis(ethylbenzene) tricarbonyl compounds, chromium compounds, determination of, 513 determination of, 515, 517 Butyldiperfluoromethyl arsine, l,l'-Bis(hydroxymethyl) ferrocene determination of, 474 determination of, 539-540 Butylferrocene, 572 INDEX

Butylferrocene (continued) Chlorophenyl groups, determination of, 539-540 determination of, n-Butylmercuric bromide, in organosilicon compounds, determination of, 28-29 252, 284 Butyltin bromides, Chlorophenyl silanes determination of, 333-341 determination of, redistribution reactions of, in organosilicon monomers, 340 234 Butyltin chlorides, retention data for, 176 determination of, 332, 340-341 Chlorophenylsiloxanes, redistribution reactions of, reaction gas chromatography of, 342 294 Butyltin halides, Chlorosilanes, determination of, 332-340 determination of, 156-160, Butyltin trichloride 170, 172 determination of, 332, 341-343 reaction gas chromatography ~t-Butyl-l-triethylsilylferrocene, of, 252 determination of, 544 Chlorovinylsilane, determination of, 176 Carbarsone, Chromium acetylacetonate, determination of, 489 determination of, 483 Cereals, Chromium hexacarbonyl, determination of organomercury determination of, 502 compounds in, 55 Copper-hexafluoroacetylacetonate, Chemically active gas chromato• determination of, 483 graphy, Crops, use of in estimating, determination of, boron-hydrogen bonds, 104-107 organomercury compounds in, Chloralkyl groups 31 in organosilicon compounds, Crustacea, determination of, 252, 284 determination of organomercury Chlorobenzene, compounds in, 55 determination of, Cumene tricarbonyl chromium in organosilicon monomers, compounds, 234 determination of, 513 Chlorobiphenyl, Cyanopropyldimethylchlorosilane, determination of, determination of, 254 in organosilicon monomers, Cyanopropylmethyldichlorosilane, determination of, 254 Chloroboranes, Cyanopropyltrichlorosilane, determination of, 74, 95-103 determination of, 254 Chloroborane, Cyc1ohexyltinbromides, determination of boron-hydrogen determination of, 323-331 bonds in, 106-107 Cyclopentadienylmanganese tri Chlorodiphenylsilane, carbonyl, determination of, determination of, 526 in organosilicon monomers, Cyclosilazanes, 234 determination of, 234 Chloro-fluororganosilicon Cymantrene, compounds, 176 determination of, 526-530 INDEX 573

Decaborone, Diethoxydimethy1si1ane determination of, 75-77 determination of, 178-179 Detectors for, Diethoxydipheny1si1ane, organosi1icon compounds, 234- determination of, 179 251 Diethy1a1uminium chloride Deuteratedethoxymethy1si1anes, determination of, 120, 124-125, determination of, 178 127 1,1'-Diacety1ferrocene, Diethy1a1uminium ethoxide, determination of, 535, 539, 541 determination of, 119 543, 546 Diethy1dimethy11ead, Diacy1ferrocene, determination of, 363, 373, 385, determination of, 538 389-390, 398-451 Dia1ky1se1enides, Diethy1dise1enide, determination of, 519-525 determination of, 522-524 Diborane, Diethy1mercury, determination of, 77-83, 90-103 determination of, 31 determination of boron-hydrogen Diethy1mercury, bonds in, 107 determination of in, impurities in, 95 air, 73 1,2-Dibromoethane, Diethy1se1enide, determination of in organo1ead determination of, 522-524 compounds, 382, 385-398 Diethy1zinc, 1,1'-Dibuty1ferrocene, determination of, 19-20, 126 determination of, 539-540 Dif1uoroborane, Dibuty1mercury, determination of, 112 determination of, 31 Dihydropentaborane, Dibuty1tindich1oride, determination of, 90-94 determination of, 322, 341-343 Di-iso-buty1a1uminium hydride, Dich1oroborane, determination of, 126 determination of, 95-103 Dimethy1a1uminium chloride, Dich1orodiborane, determination of, 125 determination of boron-hydrogen Dimethy1benzenetricarbony1 chromium bonds in, 107 determination of, 498-507 Dich1orodimethy1si1ane, Dimethy1bromoarsine, determination of, determination of, 453, 455-456, active hydrogen in, 252-253 457-458 1,2-Dich1oroethane, retention data for, 453 determination of in, Dimethy1dich1orosi1ane, organo1ead compounds, 390~398 determination of, 160-166, 170- Dich1oromethy1viny1si1ane, 174 determination of, 176 Dimethy1diethy1tin, Dich1oropheny1si1ane, determination of, 315-316 determination of, retention data for, 316 in organosi1icon monomers, Dimethy1dise1enide, 234 determination of, 522, 525 Dich1orsi1ane, Dimethy1-1,1'-ferrocene determination of, 156 dicarboxy1ate, Dicyanoferrocene, determination of, 541-544 determination of, 538 Dimethyl gallium chloride determination of, 113 574 INDEX

Dimethylmagnesium, Divinylbromoarsine determination of, 8 retention data for, 454 Dimethylmercury, Durene tricarbonyl chromium, determination of, 30-31, 70-72 determination of, 491, 493-496 Dimethylmercury, determination of in, 60 Effluents, fish, 60 determination of organomercury Dimethyldiboranes, compounds in, 34-36 determination of, 77-83 Eggs, 2,3-Dimethy1naphthalene tricarbo• determination of, nyl chromium, methylmercuric chloride in, determination of, 507-512 42-53 mass spectrometry of, 507-511 organomercury compounds in, Dimethyl (phenoxyphenyl) silane, 30, 37-73 determination of, 233 Electron capture detectors, Dimethylselenium, use of, 30, 53-56 determination of, 470-472, 522- Electron capture detector, 525 for, Dimethylsiloxane polymers, organochromium compounds, determination of, 220 495-498 Dimethylsilylarenes, 233 organolead compounds, 367-385, Dimethylvinylsiloxanes, 398-406, 448, 450 retention data for, 176 Emission detector, Diphenyldichlorosilane, for, determination of, 174-175 organoarsenic compounds, 476 Diphenylferrocene, Ethanol, determination of, 538 determination of, Diphenylfluoropropylarsine, in triethoxysilane, 234 determination of, 473-474 Ethoxychlorosi1anes, Diphenylmercury, determination of, 179 determination of, 29-30, 70-72 Ethoxyethylmercury, Diphenylperfluoromethyl arsine, determination of in crops, 31 determination of, 473-474 Ethoxymercuric chloride, Diphenyltin oxide, determination of in, determination of, 323-331 potatoes, 32-34 Di-n-propylaluminium isopropoxide apples, 32-34 determination of, 119 tomatoes, 32-34 Dipropyldiselenide, Ethoxyphenylsilanes, determination of, 522, 524 determination of, 179 Dipropylmercury, Ethoxytrimethy1silane, determination of, 31 determination of, 178-179 Dipropylselenide, Ethoxytriphenylsilane, determination of, 522, 524 determination of, 179 Dipropyltindihydride, Ethoxyviny~siloxanes, determination of, 313 retention data for, 176 Dithizone, Ethylaluminium dichloride, use of in estimating determination of, 125 organolead compounds, 361, Ethylaluminium sesquichloride, 368, 402 determination of, 126 INDEX 575

Ethylbenzenemolybdenum Ethyltrimethyllead determination of, 519 determination of, 363, 374-385, Ethylbenzenetricarbonyl chromium 389-390. 398-451 compound Etioporphyrin magnesium determination of, 513-515 determination of, 17-18 Ethylborazodes, retention times of, 87 Faeces, Ethylchlorosilanes, determination of, determination of, 160-166 inorganic mercury compounds Ethylene, in, 61-70 determination of in, organic mercury compounds in, arsine, 490 61-70 Ethylene dibromide Feeding stuffs, determination of in, determination of, gasoline, 370, 385 organoarsenic compounds in, Ethylene dichloride, 489 determination of in, Ferrocene derivatives, gasoline, 370, 385 determination of, 538-545 Ethylferrocene, infrared spectroscopy of, 539 determination of, 539-540 microwave emission detector Ethyl groups, for, 545 determination of, retention data for, 540-541 in organosilicon polymers. 1,1'-Ferrocene dimethano1, 252 determination of, 541-544 in siloxane polymers. 270-272 Ferrocene mercury chloride, Ethylhydrosiloxanes, determination of, 541-544 determination of, 223-226 Ferrocene methanol, Ethylmercuric bromide, determination of, 541-544 determination of, 28-29 Fish, Ethylmercuric bromide, determination of, determination of in, alkyl mercury compounds in, fish, 66 61-70 Ethylmercuric chloride, aryl mercury compounds in, determination of in, 61-70 apples, 32-34 ethyl mercuric bromide in, 66 effluents, 35 ethyl mercuric chloride in, fish, 61-70 60-70 potatoes, 32-34 inorganic mercury in, 61-70 tomatoes, 32-34 methyl mercuric bromide in, 66 water, 35 methyl mercuric chloride in, Ethylmercury dicyanidamide, 42-53, 61-70 determination of in, organomercury compounds in, air, 73 30, 37-73, 407-412, 450- Ethylmercuric halides, 451 determination of in crops, 31 phenyl mercuric bromide in, Ethylpropyldiselenide, 66, 70 determination of, 522-524 phenyl mercuric chloride in, Ethylselenocyanate, 61-70 determination of, 519-524 576 INDEX

Flame emission detector, Germanium alkoxides, use of in estimating, determination of, 114 organotin compounds, 345-360 Germanium alkyls, organolead compounds. 367 determination of, 297 Flame ionization detector, retention data of, 297 for use in estimating, Germanium silicon compounds, organoarsenic compounds, 485, determination of, 233 489 Germanium tetraalkyls, organochromium compounds, 491- retention parameters of, 86 495, 498-512 Germanium tetrachloride, organolead compounds, 368, determination of impurities in, 386-395, 436-437, 440-441, 300 448-450 determination of, 300-305 Flame photometric detector, Germanium tetraiodide, for use in estimating, determination of, 300 boron hydrides, 95 Glow discharge detector, organolead compounds, 95, for, 404-406 arene tricarbonyl chromium Fluoroarsines, compounds, 519 determination of, 452 organocopper compounds, 548 Fluorobenzenetricarbonyl chromium, organosilicon compounds, 236 determination of, 491, 495, 497 Grain, Fluoroorganosilicon compounds, determination of, determination of, 176-177 inorganic mercury compounds in, 61-70 Gas chromatography - mass spectro organomercury compounds in, metry, 53-54 61-70 Gas density balance, Grass, used in estimating, determination of, organosilicon compounds, 175 organomercury compounds in, organotin compounds, 310, 30 3l2-3l3 Gas-solid chromatography, 233 HAFID detector, Gasoline, for, determination of, organosilicon compounds, ethylene dibromide in, 370, 240-251 385 Hair, ethylene dichloride in, 370, determination of, 385 inorganic mercury compounds methyl cyclopentadienyl• in, 61-70 manganese in, 535, 537 organomercury compounds in, methyl cyclopentadienyl• 36, 61-76 manganese tricarbonyl in, Halogenated alkylgermanium 526-532 compounds, organolead compounds in, 361- determination of, 299 451 Halogenated scavengers, Germanes, in, determination of, 295-300 organolead compounds, 370, Germanium, 382, 385-399, 448-449 determination of, 300-305 INDEX 577

Helium microwave glow discharge Inorganic mercury compounds, detector determination of in, use in estimating, blood, 61-70 organoarsenic compounds, 476- grain, 61-70 489 faeces, 61-70 organomercury compounds, 70-73 fish, 61-70 Hexaalkyldigermanes, hair, 61-70 determination of, 297, 300 milk, 61-70 retention data of, 297, 300 sediments, 61-70 Hexaethy1borazo1e, serum, 36 retention time of, 87 tissues, 61-70 Hexamethy1benzene tricarbony1 urine, 36, 61-70 chromium, water, 36, 61-70 determination of, 491, 493-495 Inorganic nickel, Hexamethy1disi1oxane, determination of, 548 determination of, 168, 226-227, Inorganic ruthenium 230, 232 determination of, 549 Hexamethy1ditin, Inorganic selenium, determination of, 345 determination of, 525 photolysis of, 345 Iodoferrocene retention data of, 345 determination of, 541- 544 High pressure gas chromatography, Isobutylbenzene tricarbonyl for, chromium compounds, nickel porphyrins, 548 determination of, 513 Hydridic hydrogen, determination of in, Kidney, organoboron compounds, 109- determination of organomercury III compounds in, 47 Hydrogen flame ionization (HAFID) detector, Lauric acid, for, decomposition of organoa1uminium organo1ead compounds, 432-448 compounds with, 116, 121- organomanganese compounds, 124 532-537 Liver, Hydroxymethy1ferrocene, determination of, determination of, 539-540 methyl mercuric chloride in, Hydroxypheny1stannane, 42-54 determination of, 323-331 organomercury compounds in, Hyperpressure gas chromatography, 47-50, 67 use in estimating, etioporphyrin mangnesium Marine sediments, che1ates, 17-18' determination of, zinc etioporphyrin che1ates, organomercury compounds in, 20-21 36 Mass spectrometric detector, Infrared spectroscopy of for, ferrocene derivatives, 539 organo1ead compounds, 404-406, decaborane, 75-77 419-421 tetraalkylsilanes, 272 vinyl lithium, 1 578 INDEX

Mass spectrometric detector Methy1buty1bromoarsine (continued) determination of, 453, 455, 456 organosi1icon compounds, 227 retention data for, 453 Mass spectrometry, Methy1ch1orosi1anes, of, determination of, 156, 160-168, a1ky1boranes, 94 170 ary1tricarbony1 chromium Methy1cyc1opentadieny1manganese, compounds, 507-511 determination of. 532-537 methyl mercury compounds, 53- determination in gasoline, 54 535-537 methy1po1ysi1oxanes, 270 Methy1cyc1opentadieny1manganese, organo1ead compounds, 415. tricarbony1, 419-421 determination of, 526-532 organomercury compounds, 52- Methy1diborane, 54 determination of, 77-83, 94 organosi1icon compounds, 227 Methy1dibromoarsine, phenyl mercury salts, 29-30 determination of, 453, 455 tetraa1ky1si1anes, 272 Methy1ethoxysi1anes, vinyl lithium, 1 determination of, 168-169 Meat, retention data of, 168-169 determination of methyl mercuric Methy1ethy1bromoarsine, chloride in, 42-53 .determination of, 453, 455, 456 mercuric chloride, determination retention data for, 453 of, 70 Methy1ethy1dise1enide, Methylene tricarbony1 chromium, determination of, 522-524 determination of, 491-493-498, Methy1ga11iumdich1oride, 507-511, 513-514 determination of, 113 Methane, Methy1hydrocyc1osi1oxanes, determination of, determination of, 219, 223-226 in arsine, 490 Methyl lithium, p-Methoxy anisole tricarbonyl determination of, 7 chromium, Methy1magnesium bromide, determination of, 507-514 determination of, 8 mass spectrometry, 507-511 Methy1mercuric bromide, Methoxy ch1orosi1ane, determination of in, determination of, 179 fish, 66 Methoxyethy1mercury, Methy1mercuric chloride, determination of in crops, 31 determination of, 54, 70 Methy1benzoatetricarbony1 chromium mass spectrum of, 53-54 determination of, 491, 495, 497 Methy1mercuric chloride p-Methylbenzyltrimethylsilane, determination of in, pyrolysis gas chromatography of apples, 32-34 276-279 eggs, 42-53 reaction gas chromatography of, liver, 42-53 276-279 meat, 42-53 Methy1borate, potatoes, 32-34 determination of, 74, 113 Methyl mercury compounds, Methy1borazo1es, determination of, 30 retention times of, 87 INDEX 579

Methyl mercury compounds(continued)Microwave plasma detector determination of (continued) (continued) effluents, 35 organolead compounds, 425- fish, 37-73 432 water, 35 organoselenium compounds, Methyl mercury dithizonate, 525 determination of, 39-40 Milk, Methylmercuric halides, determination of, determination of in crops, 31 inorganic mercury compounds, Methylmercuric iodide, 61-70 determination of, 54 organomercury compounds in, mass spectrum of, 53-54 61-70 Methylmethylthiomercury, Minimata disease, 37 cause of, Molybdenum tricarbonyls, minimata disease, 37 determination of, 519 Methylphenyldiethoxysilane, Monochlorodiborane, determination of, 178 determination of, 95-103 Methylphenylpolysiloxanes, determination of BH bonds ~n, determination of, 219 106-107 retention data of, 176 Moss, Methylpolysiloxanes, determination of organomercury determination of, 221-223 compounds in, 47 mass spectrometry of, 270 Mussels, pyrolysis gas chromatography of, determination of, 270 organolead compounds in, 45 Methyltrichlorosilane, determination of, 160-166, 170- 174 Neutron activation analysis, 1-Methy1-1'-triethy1si1y1ferrocene, use of in estimating, determination of, 544 organoboron compounds, 76 Methyltriethyltin, organomercury compounds, 45 determination of, 315-316 Nickel actioporphyrin, retention data of, 316 determination of, 548 Methylvinylsiloxane, Nickel mesoporphyrin, retention data for, 176 determination of, 548 Microreactors, Nickel porphyrins, use of in estimating, determination of, 548 organomagnesium compounds, 9 Nitroferrocene, Microwave emission detector, determination of, 538 detector for, Nuclear magnetic resonance ferrocene derivatives, 545 spectroscopy, organoaluminium compounds, of, 128 a1ky1ch1orosi1anes, 164-165 organoberyllium compounds, 7 arenetricarbony1 chromium organogallium compounds, 113 compounds, 512-513 organosilicon compounds, 236- tetraa1kylsilanes, 272 239 Microwave plasma detector, Octyltin bromides, for, determination of, 340-341 alkylarsenic acids, 476 INDEX

:y1 tin chlorides Organoga11ium compounds letermination of, 340-341 determination of, 113-114 :yltin halides, Organoga11ium compounds, letermination of, 332-340 detection by, ;anoa1uminium compounds, microwave emission detector, L1coho1ysis - hydrolysis of, 113 114-121 Organo1ead compounds, letermination of, 113-128 determination of, :eaction with lauric acid, 116, dibromoethane in, 382, 385- 121-124 398 ~anoa1uminium compounds, dich1oroethane in, 385-398 letection by, halogenated scavengers in, microwave emission detector, 370,382, 385-399, 448- 128 450 ~anoarsenic compounds, Organo1ead compounds, ltomic absorption detector for, determination of in, !mission detector for, 476 air, 399-404, 415-432, 450 :lame ionization detector for, fish, 407-412, 450-451 485, 489 mussels, 451 le1ium glow discharge detector sediments, 407-412, 450-451 for, 476-489 water, 407-412, 450-451 lotassium chloride thermonic Organo1ead compounds, detector for, 489 alkali flame detector for, 406 ~anoarsenic compounds, atomic absorption detector ietermination of in, for, 367, 406-425, 436-437, biological materials, 489 440-441 feeding stuffs, 489 electron capture detector for, ~anobery11ium compounds, 367-385, 398-406, 448- nicrowave emission detector 450 for, 7 flame emission detector for, ~anoboron compounds, 367 ietermination of active hydrogen flame ionization detector for, in, 109-111 368, 386-395, 436-437, ~anobromoarsines, 440,441, 448-450 ietermination of, 452-457 flame photometric detector for, ~anochromium compounds, 404-406 E1ame ionization detector for, HAFID detector for, 432-448 491-495, 498-512 mass spectrometric detector electron capture detector for, for, 404-406, 419-321 495-498 mass spectrometry of, 415, 419- ganocoba1t compounds, 421 determination of, 548 microwave plasma-detector for, ganocopper compounds, 425-432 determination of, 548 retention data for, 406 glow discharge detector for, spectrophotometric detector 548 for, 367, 406 ganoiron compounds, Organomanganese compounds, spectrophotometric detector determination of, 526-537 for, 546 argon plasma detector for, 526-532 INDEX 581

Organomanganese compounds Organosilicon compounds(continued) (continued) determination of (continued) flame ionization detector for, alkoxy groups in, 262-268, 529, 532-536 284 hydrogen flame ionization benzene in, 234 detector for, 532-537 biphenyl in, 234 Organomercury compounds, chloroalkyl groups in, 284- determination of, 28-73 294 Organomercury compounds, chlorobenzene in, 234 determination of in, chlorobipheny1 in, 234 air, 73 chlorodiphenylsilane in, 234 algae, 50 chlorophenylsilane in, 234 apples, 31-34 chlorophenyl groups in, 284 bile, 47, 50 dich1orophenylsilane in, 234 biological tissues, 56 ethyl groups in, 252 blood, 47, 61-70 impurities in, 234 cereals, 55 oxya1kylene groups in, 284 crustacea, 55 phenyl groups in, 252, 284-294 eggs, 30, 34-73 Si-Si groups in, 284 fish, 30, 37-73 o/p-terphenyls in, 234 grain, 61-70 vinyl groups in, 252, 256-268, grass, 30 284 hair, 61-70 Organosilicon compounds, kidney, 47 alkali flame detectors for, 236 liver, 47-50, 67 detectors for, 227, 234-251 milk, 47-50, 61-70 glow discharge detectors for, organs, 37-73 236 potatoes, 31-34 HAFID detector for, 240-251 respirant gases, 31-34 mass spectrometric detector sediments, 61-70 for, 227 tissues, 61-70 microwave detector for, 236- tomatoes, 31-34 239 urine, 61-70 peak inversion of, 235-236 water, 34-36, 54, 61-70 reaction gas chromatography Organomercury compounds, of, 252-294 atomic absorption detector for, retention data for, 236 56-60 Organotellurium compounds, mass spectrometry of, 53-70 determination for, 307-314 Organoruthenium compounds, determination of, 525 determination of, 548 transesterification of, 306-307 Organose1enium compounds, Organotin compounds, atomic absorption detector for, alkali flame detector for, 345- 524 360 microwave plasma detector for, detectors for, 307-314, 345- 525 360

retention data for, 520-524 determination of ~n seashells, Organosilicon compounds, 360 determination of, determination of in urine, 345- active hydrogen in, 284 360 determination of ~n water, 345- 360 582 INDEX

Organotin compounds (continued) Phenyl mercury chloride, flame emission detector for, determination of in, 29-30 345-360 effluents, 35 preparative gas chromatography fish, 61-70 of, 321 water, 35 transesterification of, 306-307 Phenyl mercury dithizonate, Organs, determination of, 32 determination of organomercury Phenylmercuric halides, compounds in, 37-73 determination of in crops, 31 Oxophenylstannane, Phenyl mercury salts, determination of, 323-331 determination of, 29-30, 32-35. Oxyalkylene groups in organo 61-70 silicon compounds, Phenylmethyldichlorosilane, determination of, 284 determination of, 253 Phenylmethylperfluoropropylarsine, Peak inversion, determination of, 474 of, Phenylmethylsilicon dichloride organosilicon compounds, 235- determination of, 253-254 236 Phenylsilicon trichloride, Pentaborane, determination of. 253-254 determination of, 90-94, 107- Phenylsilicon trifluoride, 109 determination of, 254 determination of BH bonds in, Phenyltin bromides, 106-107 determination of, 340-341 Perfluoroalkyltin compounds, Phenyl tin chlorides, determination of, 343 determination of, 340-341 Perfluoroarsenic compounds, Phenyltirt halides, determination of, 472-475 determination of, 332-340 Perfluorovinyltin compounds, Phenyltrichlorosilane, determination of, 343 determination of, 174-175 Phenylarsenic acid, Phenyltrimethylsilane, determination of, 485, 488 reaction gas chromatography of, Phenylchlorosilanes, 273-274 determination of. 174-176 thermal cracking of, 284 Phenylferrocene, pyrolysis gas chromatography determination of, 541-544 of, 273-274 Phenyl groups in organosilicon Phosphorus oxychloride, compounds, determination of, 164 determination of. 252. 270, 272. Phosphorus trichloride, 284-294 determination of, 164 Phenylli thium, separation from silicon tetra determination of, 6-7 chloride, 157 Phenylmercuric acetate, Polycyclomethylpo1ysi1oxanes, determination of in, determination of, 223 apples, 32-34 Polydimethylsiloxanes, potatoes, 32-34 alkyl groups in, 290 tomatoes. 32-34 aryl groups in, 290 Phenylmercuric bromide determination of, 219, 227 determination of in, reaction gas chromatography of, fish, 66, 70 290-291 INDEX 583

Polymethylphenylsiloxane, Pyrolysis (continued) determination of, 223 of (continued) reaction gas chromatography of, bis(tributyltin) oxide, 290, 292-293 p-methylbenztrimethylsilane, Polymethylsiloxanes, 276-279 retention data of, 168 methylpolysiloxanes, 270 Polymethylvinylsiloxanes, phenyltrimethylsilane, 273- determination of vinyl groups 274 in, 255 polymethylviny1siloxanes, 255 pyrolysis gas chromatography of, polysiloxanes, 220-221 255 silicondichloride polymer, Polysiloxanes, 157-159 alkyl groups in, 284-294 siloxanes, 235, 256-270 aryl groups in, 284-294 tetraalkylsilanes, 272 determination of, 218-221 o-tolyltrimethylsilane, 279- reaction gas chromatography of, 281 284-294 p-tolyltrimethylsilane, 281- pyrolysis gas chromatography of, 283 220-221 Pyrolysis - gas chromatography, Potassium chloride thermionic structure of, detector, zinc dibutyldithiophosphate, for, 24-27 organoarsenic compounds, 489 zinc O,O'-dicyclohexylthiono• Potatoes, thiophosphate, 27-28 determination of, zinc O,O'-di-n-dodecylthiono• organomercury compounds in, 31- thiophosphate, 27-28 34 zinc diisopropyldithio• Preparative gas chromatography, phosphate, 24 of, zinc O,O'-dineopentylthiono• organoselenium compounds, 519 thiophosphate, 27-28 organotin compounds, 321 zinc di(4-methyl-2-pentyl)• n-Propylbenzene tricarbonyl dithiophosphate, 24-27 chromium compounds, Pyrolysis - gas chromatography, determination of, 513 use of in estimating, Propylchlorosilanes, deuterium in boron hydrides, determination of, 168-169 94-95 retention data for, 168-169 zinc dialkyldithiophosphates, n-Propylmagnesium bromide, 21-28 determination of, 8 zinc diethyldithiophosphates, Pseudocumenetricarbonyl chromium 21 compounds, determination of, 513-514 Reaction chromatography, Pyrolysis, determination of, of, active hydrogen groups, 284 alkylcyclosiloxanes, 255 a1koxy groups, 284 arene tricarbonyl chromium alkyl groups, 284-294 compounds, 502, 505-507 chloroalkyl groups, 284 arylsilanes, 272-284 chlorophenyl groups, 284 benzyltrimethylsilane, 275- oxyalky1ene groups, 284 276 phenyl groups, 284-294 584 INDEX

Reaction chromatography(continued) Respirent gases(continued) determination of (continued) determination of (continued) Si-Si groups, 284 tetramethy1tin in, 470-472 vinyl groups, 284 trimethy1arsine in, 458-472 Reaction gas chromatography, Retention parameters, of, of, a1koxy si1anes, 252 a1ky1bromosi1anes. 139 a1ky1cyc1osi1oxanes, 255 a1ky1borazo1es, 87-89 a1ky1si1anes, 252 a1ky1boron compounds, 98 ary1si1anes, 252, 272-284 a1ky1ch1orosi1anes, 139-176 benzy1trimethy1si1ane, 275- a1ky1germanium compounds, 276 295-299 ch1oropheny1si1oxanes, 294 a1ky1si1anes, 129-156 ch1orosi1anes, 252 a1kyltin compounds, 316-323 p-methy1benzy1trimethy1si1ane, arene tricarbony1 chromium 276-279 compounds, 514 methy1po1ysi1oxanes, 270 ary1si1anes, 129-156 organosi1icon compounds, 252- ary1tin compounds, 316-323 294 bromoarsines, 453-457 pheny1methy1dich1orosi1ane, ch1oropheny1si1anes, 176 253-254 dimethy1viny1si1oxanes, 176 pheny1trimethy1si1ane, 273- ethoxyviny1si1oxanes, 176 274 ferrocene derivatives, 540- pheny1methy1si1icondich1oride, 541 253-254 germanes, 295-299 pheny1si1icontrich1oride, 253- germanium a1ky1s, 297 254 hexaa1ky1digermanes, 297,300 po1ydimethy1si1oxanes, 290- hexamethy1disi1oxane, 230 291 hexamethy1ditin, 345 po1ymethy1pheny1si1oxane. 290, methy1pheny1si1oxanes, 176 292-293 methy1viny1si1oxanes, 176 po1ymethy1viny1si1oxanes. 255 organo1ead compounds, 406 si10xane polymers. 256-268, organose1enium compounds, 270-272 520-524 tetraa1ky1si1anes, 272 organosi1icon compounds, 236 o-to1y1trimethy1si1ane, 279- propy1ch1orosi1anes, 168-169 283 si1icogermanes, 295-296 viny1si1anes, 252 silicon hydrides, 129, 132 Reaction gas chromatography, tetraa1koxysi1anes, 143, 144, use of in estimating, 146, 148, 150, 152, 154, active hydrogen in organoboron 179-218 compounds, 109-111 tetraa1ky1si1anes, 139-156 Redistribution reactions of, tetraethy1si1ane, 156 buty1tin bromides, 340 tetramethy1germanium, 297 butyl tin chlorides, 342 triethy1si1ane, 156 Respirent gases, trimethy1si1y1 ethers, 228- determination of, 237 dimethy1senenium in, 470-472 trimethy1si1y1thio ethers, organomercury compounds in, 228-232 56 viny1tin compounds, 316-323 INDEX 585

Ruthenium 4(hexachlorobiscyclo• Silicon tetrachloride(continued) heptane-2-methylene)thio determination of (continued) semicarbazide, separation from phosphorus determination of, 549 chloride, 157 Ruthenocene derivatives, Silicon tetrafluoride determination of, 538, 548-549 determination of, 254 Siloxanes, Seashells, determination of, 168, 170, 172, determination of organotin 218-227 compounds in, 360 ethyl groups in, 270-272 Sediments, identification of, 268-270 determination of phenyl groups in, 270-272 inorganic mercury in, 61-70 pyrolysis-gas chromatography organolead compounds in, 407- of, 235, 268-270 412, 450-451 reaction gas chromatography organomercury compounds in, of, 252 61-70 retention data for, 168-169 Selenous acid, vinyl groups in, 255-268 determination of, 525 Si-Si groups in organosi1icon Serium, compounds, determination of inorganic determination of. 284 mercury in, 36 Silyl arenes, Silane, determination of, 233 determination of arsine in, 491 Silyl ethers, Silanic hydrogen, determination of, 228-232 determination of, 222-223 Silyl sulphides, Silicogermanes, determination of, 232 determination of, 295-296 Silythioethers, retention data of, 295-296 determination of, 228-232 Silicon alkoxides, Spectrophotometric detector, determination of, 114 for, Silicon dichloride polymer, organoiron compounds. 546 pyrolysis of, 157-159 organolead compounds, 367, Silicon germanium compounds, 406 determination of, 233 Stannic chloride. Silicon heterocyclic compounds, determination of. 343 determination of, 233 Silicon hydrides, Tert-butylbenzenetricarbonyl determination of, 129, 132 chromium compounds, Silicon nitrogen compounds, determination of, 513 determination of, 232 4-Tert-butyl-2,6-bis(trimethy1 Silicon phenols, sily1) phenol , determination of, 232 determination of, 232 Silicon tetraalkyls, p-Tert-buty1pheny1magnesium retention parameters of, 86 bromide, Silicon tetrachloride, determination of, 9-12 determination of, 156-157, 159- o/p-Terpheny1s, 166, 171-174 determination of, benzene in, 234 in organosilicon monomers, impurities in, 159-160 234 586 INDEX

Tetraacety1tin compounds, Tetramethy1stannane determination of, 322 photolysis of, 345 Tetraa1koxysi1anes, Tetramethy1tin, retention data for, 143, 144, detectors for, 307-314 146, 148, 150, 152, 154, determination of, 313, 315-316, 179-182 40-472, 524 Tetraa1ky1germanium compounds, retention data of, 316 determination of, 295-299 Tetracty1tin, retention data of, 295-299 determination of, 340-341 Tetraa1ky1si1anes, Tetrapheny1tin, infrared spectroscopy of, 272 determination of, 322, 340-341 mass spectrometry of, 272 Tetraviny1tin, nuclear magnetic resonance determination of, 316 spectroscopy of, 272 retention data of, 316 pyrolysis-gas chromatography of,Thermionic detector, 272 for, retention data for, 139-156 organoarsenic compounds, 489 Tetraa1ky1tin compounds, Thermal cracking, determination of, 313 of, solubility in water, 323 ary1si1anes, 284 Tetraborane, pheny1trimethy1si1ane, 284 determination of, 90-94 Thermal decomposition, Tetrabuty1stannane, of, determination of, 322 ary1s~lanes, 272-284 Tetrabuty1tin, ary1trimethy1si1anes, 136 determination of, 332, 340-343 benzy1ytrime.thy1si1ane, 275- thermal decomposition of, 322 276 determination of in air, 343 p-methy1benzy1trimethy1si1ane, Tetraethoxysi1ane, 276-279 determination of, 178-179 pheny1trimethy1silane, 273- Tetraethy1si1ane, 274 determination of, 242-248 tetrabuty1tin, 322 Tetraethy1tin, o-to1y1trimethy1si1ane, 279- determination of, 315-316, 361- 283 451 Thin layer chromatography, determination in air, 343 of, retention data of, 316 organomercury dithizonates, Tetramethoxysi1ane, 40-41 determination of, 179 zinc dia1kyldithiophosphates, Tetramethy1benzenetricarbony1 21-22 chromium, Thiophen arene tricarbony1 determination of, 498-507 chromium compounds, Tetramethy1diborane, determination of, 517-518 determination of, 82 Tin, Tetramethy1germane, determination of in, determination of, 297 water, 343 retention data of, 297 Tin tetraethyl, Tetramethy11ead, determination of, 406 determination of, 361-451 INDEX 587

Tissues, Tricarbony1cyclopentadieny1 determination of manganese inorganic mercury in, 61-70 determination of, 526 organic mercury in, 61-70 Tricarbony1iron complexes, Titanium a1koxides, determination of, 545 determination of, 114 Trich1orsi1ane, Toluene tricarbonyl chromium determination of, determination of, 491, 493-496, benzene in, 156, 166, 170-174 507-513, 517 Trich1oroviny1si1ane, Toly1mercuric acetate, determination of, 176-177 determination of in, Triethoxymethylsi1ane, apples, 32-34 determination of, 178-179 potatoes, 32-34 Triethoxypheny1si1ane, tomatoes, 32-34 determination of, 179 Tolylmercury dithizonate, Triethoxysi1ane, determination of. 32 determination of, To1y1mercuric halides, ethanol in, 234 determination of in crops, 31 Triethyla1uminium, o-Tolyltrimethy1si1ane, determination of, 114-121, 123- reaction gas chromatography of, 124, 127 279-281 Triethylboron, pyrolysis gas chromatography of, determination of, 74 279-281 Triethylmethyllead, p-To1y1trimethy1si1ane, determination of, 363, 374-385, reaction gas chromatography of, 389-390, 398-451 281-283 Triethylsilylisopropy1ferrocene, pyrolysis gas chromatography of, determination of, 544 281-283 retention data for, 156 Tomatoes, Trimethylaluminium, determination of, determination of, 124-125 organomercury compounds in, Trimethy1aminomonoborane, 31-34 determination of active hydrogen Transestrification, in, 111-112 of, Trimethylarsine, organotin compounds, 306-307 determination of, 458-472, 524 1,3,5-Tria1ky1borazo1es, Trimethy1benzene tricarbonyl determination of, 83-90 chromium, retention time of, 83-89 determination of, 498-507 Tri-B-a1ky1borazoles, Trimethylborane, determinatiun of, 83-90 determination of, 77-83 retention parameters of, 84-89 Trimethylchlorosilane, Tri-iso-buty1 aluminium, determination of, 160-166, 170- determination of, 114-121, 124- 174, 218-219 125 Trimethyldiboranes, Tributy1arsene, determination of, 82 determination of, 475, 453 Trimethylethyltin, retention data for, 453 determination of, 315-316 Tributy1tin chloride, retention data of, 316 determination of, 332, 341-343 Trimethylgallium, determination of, 113 588 INDEX

1-Trimethy1germany1ethy1ene, Vinylarsines, determination of, 299 determination of, 453 1-Trimethy1germanyl-2-trimethyl• Vinylchlorosi1anes, si1y1ethy1ene, determination of, 160-178 determination of, 233 Vinyldibromoarsine, Trimethy1si1y1acetamide, determination of, 453 determination of, 232 retention data for. 453 Trimethy1si1yl ethers, Vinylethoxysilanes. retention data for, 228-232 determination of, 178 determination of, 228-232 Vinylferrocene. Trimethy1silylthioethers, determination of, 539-540 retention data for, 228-232 Vinyl groups, determination of, 228-232 in organosilicon compounds, Trimethyltin hydride, determination of, 252, 256-268. determination of, 313 284 photolysis of, 345 Vinyl groups, Tri-N-alkylborazoles, in siloxanes, determination of, 83-90 determination of, 255 retention parameters of, 84-89 Vinyl li thiurn, Triphenylarsine, determination of, 1-6 determination of, 453 Vinyl magnesium chloride, 2,4,6-Tripheny1cyc1otrisi1oxane, determination of, 12-17 determination of, 218-219 Vinyl magnesium halides, Triphenyltinhydroxide, determination of, 12-17 determination of, 323-331 Vinyl silanes, Tri-N-propylaluminiurn, reaction gas chromatography of, determination of, 118, 124 252 Tri-N-propylboron, Vinyltin compounds, determination of, 74 retention data of, 316-323 Trisilane, determination of. 316-323 determination of, 130 Vitamin K. Tris(N-alkyl hexamethyl)cyclo determination of, 548 siloxanes, determination of, 234 Water, Tritium detectors, determination of, poisoning of, 32 inorganic mercury in, 36, 61- Trivinylarsine, 70 determination of, 453, 454, 457- organolead compounds in, 407- 458 412. 450-451 organomercury compounds in, Ultraviolet spectroscopy, 34-36, 54, 61-70 use of in estimating, organotin compounds ~n, 323- decaborane, 75-77 331, 345-360 Urine, tin in, 343 determination of, inorganic mercury in, 36, 61- X-ray fluorescence analysis of, 70 organolead compounds, 376-378 organic mercury in, 36, 61-70 Xylenetricarbony1 chromium, organotin compounds in, 345- determination of, 507-511, 513- 360 515 INDEX 589

Xy1enetricarbony1 chromium (continued) determination of (continued) mass spectrometry of, 507-511

Zinc dia1ky1dithiophosphates, determination of, 21-28 Zinc dibuty1dithiophosphate, structure of, 24-27 Zinc O,O'-dicyclohexylthionothio• phosphate, structure of, 27-28 Zinc O,O'-di-n-dodenylthionothio• phosphate, structure of, 27-28 Zinc diethy1dithiophosphates, determination of, 21 Zinc diisopropy1dithiophosphate, structure of, 24 Zinc di(4-methyl-2-pentyl)dithio• phosphate, structure of, 24-27 Zinc O,O'-dineopentylthionothio• phosphate, structure of, 27-28 Zinc etioporphyrin chelates, determination of, 20-21