BH10 1 PROJECT: BH13 BH12 GW Results Compared to MECP Table 3 Standards Phase II ESA - East Screen Concentrations Above and/or Sample ID Depth End of Chenail Parameter Suites Below Table 31 BH14 (mbgs) BH5 GW Results Compared to MECP Table 3 Standards1 Boulevard BH12 1.8 - 4.9 PAH, PHC, VOC
FIGURE NO: 5 \\mh.local\data\Proj\2019\190441800-Phase II ESA Blvd du Chenail\09. CAD\05 Model\Supplemental Investigation - Round 2.dwg LEGEND Approximate Property Parcels Borehole/Monitoring Well Locations
Indicated Concentration(s) Measured in Soil Exceed the Site Condition Standard(s)
Estimated Groundwater Plume Based on 600 PHC F2 Results (ug/L)
Potentially Contaminating Activities (PCA)
Approximate Boundary Former/Current Ancillary Building Former Rail Line Former/Current AST/UST - Horizontal AST BH8 - Vertical AST BH4 - UST BH7
BH3
Notes:
PHC - Petroleum Hydrocarbon F - Fraction BH2 AST - Above Ground Storage Tank UST - Underground Storage Tank BH1 BH6
PROJECT: BH5 Phase II ESA - East BH12 End of Chenail Boulevard
BH11 PREPARED FOR:
600 BH9 DESIGNED BY: BH10 M.D DRAWN BY: BH13 R.H CHECKED BY: A.W
400 DATE: BH14 8/20/2020 SCALE: 200 As Shown PROJECT NO: 190441800 TITLE:
Inferred Groundwater Plume Extent - Plume 1
FIGURE NO: 6 \\mh.local\data\Proj\2019\190441800-Phase II ESA Blvd du Chenail\09. CAD\05 Model\Supplemental Investigation - Round 2.dwg LEGEND Approximate Property Parcels Borehole/Monitoring Well Locations
Indicated Concentration(s) Measured in Soil Exceed the Site Condition Standard(s)
Estimated Groundwater Plume Based on 600 PHC F3 Results (ug/L)
Potentially Contaminating Activities (PCA)
Approximate Boundary Former/Current Ancillary Building Former Rail Line Former/Current AST/UST - Horizontal AST BH8 - Vertical AST BH4 - UST BH7
BH3
Notes:
PHC - Petroleum Hydrocarbon F - Fraction BH2 AST - Above Ground Storage Tank UST - Underground Storage Tank BH1 BH6
1,000 PROJECT: BH5 10,000 Phase II ESA - East 500 BH12 End of Chenail Boulevard
BH11 PREPARED FOR:
BH9 DESIGNED BY: BH10 M.D DRAWN BY: BH13 R.H CHECKED BY: A.W DATE: BH14 8/20/2020 SCALE: As Shown PROJECT NO: 190441800 TITLE:
Inferred Groundwater Plume Extent - Plume 2
FIGURE NO: 7 \\mh.local\data\Proj\2019\190441800-Phase II ESA Blvd du Chenail\09. CAD\05 Model\Supplemental Investigation - Round 2.dwg APPENDIX C: Borehole Logs
Morrison Hershfield Ltd RECORD OF BOREHOLE BH1 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2019-09-26 COMPLETED 2019-09-26 ELEVATION 43.7 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 2.10 mbgs / Elev 41.60 m ASL LOGGED BY MD CHECKED BY CZ MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.1 ASPHALTIC CONCRETE 5 3 0 Flush Mount 6 11 Casing FILL - (SM) SILTY SAND, trace to SS1 5 some gravel; light brown to brown, 6 amber mottling; non-cohesive; moist 26 3 0 11 24 1 SS2 13 1.2 12 Bentonite Seal 1.3 FILL - ASPHALTIC CONCRETE 9 4 0 FILL - (SM) SILTY SAND, trace to 26 51 SS3 25 some gravel; brownish grey; 14 non-cohesive; moist 8 2 Silica Sand #2 7 3 25 14 SS4 7 Metals, PAH 6 1 2.7 2 3 (SM) SILTY SAND; grey; SS5 1 3 non-cohesive; wet; some organics 1 (brown decaying wood) 1 0 1 SS6 1 1 50mm Diam. 3.9 1 2 85 PVC #10 Slot 4 Screen (SM) SILTY SAND, some gravel to SS7 1 51 PHC, VOC gravelly, trace clay (GLACIAL TILL), 50 cobbles; grey; non-cohesive; wet; very 7 12 2 0 dense 52 SS8 40 50 5 5.2 End of Borehole at 5.2 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH2 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2019-09-26 COMPLETED 2019-09-26 ELEVATION 44.04 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 2.52 mbgs / Elev 41.52 m ASL LOGGED BY MD CHECKED BY CZ MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.1 TOPSOIL - SILTY SAND; brown; 2 1 0 Stickup moist 4 16 Casing SS1 12 0.6 FILL - (SP) GRAVELLY SAND, trace 12 silt; grey; non-cohesive; moist; some 7 glass and brick pieces, trace asphalt 1 0 Bentonite Seal 1 SS2 11 23 FILL - (SM) SILTY SAND, trace to 12 some gravel; light brown to greyish 12 brown, some amber mottling; 3 Silica Sand #2 4 2 15 non-cohesive; moist; some organics SS3 7 Metals, PAH 1.7 3 (decomposing wood and humus) 5 2 2.0 FILL - (SP) SAND, some silt, trace 6 4 2 10 gravel; dark brown to black; SS4 5 non-cohesive; moist; some coal 1 fragments 1 2 2.7 FILL - (SP) SAND, some gravel; 1 2 brown; non-cohesive; moist SS5 1 3 1 (SM) SILTY SAND, some gravel to 50mm Diam. gravelly, trace clay (GLACIAL TILL), 1 PVC #10 Slot 1 3 Screen cobbles and boulders; grey; SS6 2 non-cohesive; wet; loose to dense 2 2 1 10 4 5 11 SS7 6 PHC, VOC 13 12 19 2 20 46 SS8 27 Silica Sand #2 4.9 40 End of Borehole at 4.9 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH3 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2019-09-26 COMPLETED 2019-09-26 ELEVATION 43.87 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 2.46 mbgs / Elev 41.41 m ASL LOGGED BY MD CHECKED BY CZ MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.1 TOPSOIL - (SM) SILTY SAND; 2 1 0 Stickup brown; moist; rootlets 5 11 Casing SS1 6 Metals, PAH 0.6 FILL - (SM) SILTY SAND, some 20 gravel; greyish brown; moist; some 12 concrete pieces 2 0 19 41 1 SS2 22 1.2 FILL - BOULDER, rock fragements; Bentonite Seal red 7 13 FILL - (SP) SAND, trace to some 20 36 gravel; light brown; moist SS3 16 10 2 5 Silica Sand #2 2.1 2 6 25 5 (CL) SILTY CLAY, some sand; grey; SS4 3 cohesive; low-plasticity; w>PL; very 4 soft to firm 2 1 0 1 2 SS5 1 3 1 1 2 70 SS6 2 52 50 3.7 50mm Diam. (SM) SILTY SAND, some gravel to 3 2 25 PVC #10 Slot 4 gravelly, trace clay (GLACIAL TILL), 7 16 Screen SS7 9 cobbles and boulders; grey; 37 non-cohesive; wet; compact to very dense 21 2 190 SS8 34 84 PHC, VOC 50 5 12 1 170 26 60 SS9 34 Silica Sand #2 5.5 31 End of Borehole at 5.5 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH4 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2019-09-26 COMPLETED 2019-09-26 ELEVATION 44.45 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 3.34 mbgs / Elev 41.12 m ASL LOGGED BY MD CHECKED BY CZ MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.2 TOPSOIL - (SM) SILTY SAND; 1 2 0 Stickup brown; moist; rootlets 2 10 Casing SS1 8 FILL - (SP) GRAVELLY SAND; 13 0.7 greyish brown; moist 8 2 35 1 FILL - (SP) SAND; red to light brown; SS2 12 62 non-cohesive; moist 50 Bentonite Seal 1.2 FILL - (SM) SILTY SAND, some 3 1 7 gravel; brown; non-cohesive; moist; 8 19 SS3 11 bricl pieces, trace wood fragements 13 2 3 Silica Sand #2 5 2 10 16 2.3 SS4 11 Metals, PAH 2 2.5 FILL - (PT) PEAT; dark brown; moist; slightly fibrous 2 2 20 1 3 (CL) SILTY CLAY, some sand; SS5 2 PHC, VOC 3 brownish grey, amber mottling; 2 cohesive; low-plasticity; w>PL, soft 1 0 SS6
50mm Diam. 1 2 5 PVC #10 Slot 4 1 3 Screen SS7 2 4.3 2 (SM) SILTY SAND, some gravel to 2 2 40 gravelly, trace clay (GLACIAL TILL), SS8 12 62 cobbles and boulders; grey; 50 5 non-cohesive; wet, dense to very dense 11 2 60 16 42 SS9 26 Silica Sand #2 5.5 35 End of Borehole at 5.5 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH5 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2019-11-29 COMPLETED 2019-11-29 ELEVATION 43.26 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 1.60 mbgs / Elev 41.66 m ASL LOGGED BY MD CHECKED BY CZ MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.1 ASPHALTIC CONCRETE - 9cm 4 0 5 Flush Mount 0.4 5 10 Casing FILL - (GP) SANDY GRAVEL; greyish SS1 5 0.6 brown; moist 3 FILL - (SM) SILTY SAND, some 3 1 5 Bentonite Seal gravel; light brown; moist 5 8 1 SS2 3 Metals, PAH 1.2 FILL - (SM) SILTY SAND, some 4 gravel; light brown to dark brown; 1 moist; loose; decaying wood (black); 0 3 90 2 Silica Sand #2 brick pieces SS3 2 (CL) SILTY CLAY; grey; cohesive; 1 2 w>PL; soft; trace rootlets wh 2.1 1 1 5 SS4 6 (SM) SILTY SAND, some gravel to 5 gravelly, trace clay, (GLACIAL TILL); 11 grey; non-cohesive; wet; compact to 7 1 30 8 25 very dense SS5 17 3 50mm Diam. 22 PVC #10 Slot Screen 24 1 85 26 56 SS6 30 PHC, VOC 25 18 1 40 4 SS7 33 83 4.1 50 End of Borehole at 4.1 meters. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH6 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2019-11-29 COMPLETED 2019-11-29 ELEVATION 43.51 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 1.89 mbgs / Elev 41.62 m ASL LOGGED BY MD CHECKED BY CZ MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.1 ASPALTIC CONCRETE - 8cm 7 1 55 Flush Mount 0.3 8 16 Casing FILL - (GP) SANDY GRAVEL; dark SS1 8 grey; moist 9 FILL - (SM) SILTY SAND, some 3 1 10 Bentonite Seal 1 gravel; greyish brown to brownish SS2 1 6 grey; moist; loose to compact; trace 5 asphalt pieces 6 8 1 20 Silica Sand #2 13 21 SS3 8 1.8 13 2 FILL - (SM) SILTY SAND, some 6 7 1 10 gravel; grey; wet; loose 9 SS4 2 2.4 1 FILL - WOOD chips and pieces, 0 fibrous organic matter; brown to dark 1 2 105 SS5 1 brown; moist; noticeable odour 0 3 1 3.1 50mm Diam. PVC #10 Slot (CL) SILTY CLAY, some sand; grey; 4 95 Metals, PAH, SS6 Screen w>PL; some wood pieces; noticeable PHC, VOC 3.7 odour (SP-SM) SAND to SILTY SAND; grey; 9 1 10 4 wet; loose 3 7 SS7 4 4.3 4 (SM) SILTY SAND. some gravel, 4.6 (GLACIAL TILL); grey; non-cohesive; wet End of Borehole at 4.6 meters. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH7 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2019-11-29 COMPLETED 2019-11-29 ELEVATION 44.73 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 3.05 mbgs / Elev 41.69 m ASL LOGGED BY MD CHECKED BY CZ MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.1 ASPHALTIC CONCRETE - 10cm Flush Mount Hydrovac excavation to 1.3m to Casing confirm absence of COGECO cable
1
1.3 Bentonite Seal FILL - (SM) SILTY SAND, some 7 gravel; brownish grey; non-cohesive; 1 0 8 19 moist; compact to dense; some SS1 11 Metals, PAH 2 organic matter; trace debris (brick, 8 metal) 5 1 15 17 33 SS2 16 18 Silica Sand #2 3 5 3 30 7 13 SS3 6 3.7 5 (SM) SILTY SAND, trace gravel, trace 5 1 95 4 clay; grey; moist; loose 5 8 SS4 3 PHC, VOC 4.3 2 (CL) SILTY CLAY, trace sand; grey; 1 1 1 0 cohesive; w>PL; very soft to firm; SS5 2 50mm Diam. trace rootlets 1 PVC #10 Slot 1 Screen 5 3 5.2 1 0 SS6 3 6 (SM) SILTY SAND, trace clay; 3 brownish grey; moist; loose; some 3 rootlets and organic matter (wood 2 1 0 pieces) SS7 6 8 6 2 6.1 1 End of Borehole at 6.1 meters. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH8 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2019-11-29 COMPLETED 2019-11-29 ELEVATION 44.69 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 3.01 mbgs / Elev 41.68 m ASL LOGGED BY MD CHECKED BY CZ MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.1 ASPHALTIC CONCRETE - 9 cm Flush Mount Hydrovac excavation to 1.3m to Casing confirm absence of COGECO cable
1 Bentonite Seal
1.3 FILL - (SM) SILTY SAND, some 5 gravel; brownish grey; moist; loose to 5 0 25 9 Silica Sand #2 compact SS1 4 Metals, PAH 2 3 3 0 20 6 18 SS2 12 11
3 3.0 (SM) SILTY SAND, some gravel, trace 7 clay; grey; wet; loose 0 35 SS3 5 6 PHC, VOC 1 50mm Diam. 1 PVC #10 Slot Screen 0 35 4 SS4 4.3 0 10 (CL) SILTY CLAY; greenish grey to SS5 10 50 grey; cohesive; w>PL; trace rootlets 50
5 5.0 Auger Refusal at 5 meters due to possible bedrock surface or boulder. End of Borehole. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH9 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2020-07-24 COMPLETED 2020-07-24 ELEVATION 43.41 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 1.85 mbgs / Elev 41.56 m ASL LOGGED BY MD CHECKED BY AW MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.2 TOPSOIL - (SM) SILTY SAND; 1 0 20 Stickup brown; moist; rootlets 1 5 Casing SS1 4 0.6 FILL - (SM) SILTY SAND, trace 4 gravel; brown; moist; brick pieces 4 0 30 Bentonite Seal 1 FILL - (SP) SAND, fine to medium, SS2 7 13 trace silt; light brown; moist 6 1.2 5 FILL - (SP) SAND, fine to medium, 4 0 30 Silica Sand #2 trace silt; light brown; moist to wet 3 6 SS3 3 1.8 4 2 FILL - (GM) SILTY GRAVEL, some 7 7 77 450 sand to sandy; dark brown; wet; SS4 13 PHC F2-F4 hydrocarbon odour 6 2.4 2 (SM) SILTY SAND, some gravel to 3 5 30 280 PHC F1, gravelly, cobbles and boulders, SS5 12 7 VOC 3 (GLACIAL TILL); grey; non-cohesive; 29 wet; hydrocarbon odour 50mm Diam. PVC #10 Slot 36 125 PAH, PHC SS6 50/0.05 100+ Screen F2-F4
6 90 4 SS7 50/0.13 100+
Silica Sand #2 4.9 End of Borehole at 4.9 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH10 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2020-07-24 COMPLETED 2020-07-24 ELEVATION 43.25 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 1.60 mbgs / Elev 41.65 m ASL LOGGED BY MD CHECKED BY AW MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.2 TOPSOIL - (SM) SILTY SAND; 2 1 0 Stickup brown; moist; rootlets 3 7 Casing SS1 4 Metals, PAH FILL - (SP) SAND, fine to medium, 6 Bentonite Seal 0.8 trace silt; black; moist; coal pieces, 5 brick and slag 620 700 3 7 1 SS2 4 1.2 FILL - (SP) SAND, fine to medium; Silica Sand #2 light brown to black; moist 4 3 (CL) SILTY CLAY; dark grey; w~PL to 4 2000 2700 PAH, PHC, SS3 9 w>PL; hydrocarbon odour; black 5 VOC staining 12 2 2.0 3 4 2000 2900 (SM) SILTY SAND, some gravel, SS4 14 cobbles and boulders, (GLACIAL 10 2.4 TILL); dark grey; wet; black staining; 19 faint hydrocarbon odour 13 23 16 470 56 50mm Diam. (SM) SILTY SAND, some gravel, SS5 33 PHC F2-F4 3 PVC #10 Slot cobbles and boulders, (GLACIAL 50/0.15 Screen TILL); dark grey; wet; faint 297 360 hydrocarbon odour SS6 50/0.10 100+
2 170 4 SS7 50/0.13 100+ 4.3 End of Borehole at 4.3 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH11 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2020-07-23 COMPLETED 2020-07-23 ELEVATION 43.47 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 1.89 mbgs / Elev 41.58 m ASL LOGGED BY MD CHECKED BY AW MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.2 TOPSOIL - (SM) SILTY SAND; 3 20 150 Stickup brown; moist; rootlets 7 17 Casing SS1 10 0.6 FILL - (SM) SILTY SAND, some 13 gravel to gravelly, cobbles; brown, 4 Bentonite Seal 0.9 amber mottling; moist 4 170 1 SS2 6 19 Metals FILL - (SP) SAND, fine to medium; 13 1.2 light brown; moist 25 11 Silica Sand #2 FILL - (CL) SILTY CLAY, some sand; 12 78 320 PAH, PHC, SS3 15 brown; moist; trace coal and slag 3 VOC 1.8 (CL) SILTY CLAY; brown to grey, 3 2 amber mottling; cohesize; w>PL; 3 3 110 800 7 strong hydrocarbon odour, black SS4 4 staining 6 (CL) SILTY CLAY; grey to dark grey; 2 38 280 cohesive; w>PL; hydrocarbon odour 4 7 SS5 3 3 4 50mm Diam. 3.2 2 35 300 PVC #10 Slot (SP-SM) SAND to SILTY SAND, SS6 12 24 Screen some gravel to gravelly; grey; wet; 12 hydrocarbon odour 8 6 23 110 4 7 20 SS7 13 PHC F2-F4 7 6 5 19 85 12 SS8 7 Silica Sand #2 4.9 7 End of Borehole at 4.9 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH12 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2020-07-23 COMPLETED 2020-07-23 ELEVATION 43.49 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 1.92 mbgs / Elev 41.58 m ASL LOGGED BY MD CHECKED BY AW MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.2 TOPSOIL - (SM) SILTY SAND; 2 0 70 Stickup 0.4 brown; moist; rootlets 6 35 Casing SS1 29 0.6 FILL - (SC) CLAYEY SAND; light 23 brown; moist 8 1 15 1 FILL - (GP) SANDY GRAVEL. coarse; SS2 10 18 Metals Bentonite Seal 1.1 angular; light grey to brown; moist 8 1.2 7 FILL - (SP) SAND, fine to medium, 4 some gravel; light brown; moist 0 0 SS3 5 8 1.7 FILL - COAL and SLAG; black 3 Silica Sand #2 3 FILL - (SM) SILTY SAND; brown, 2 2 some amber mottling; moist 2 0 170 4 (CL) SILTY CLAY; grey, some red SS4 2 mottling; cohesive; w>PL 2 1 1 240 0 0 SS5 0 3 1 1 3.4 1 0 180 SS6 2 50mm Diam. (SP-SM) SAND to SILTY SAND, 1 PVC #10 Slot some gravel, cobbles and boulders; 3 Screen grey; wet; faint hydrocarbon odour 5 20 1 620 PAH, PHC, 4 SS7 22 2 VOC 20 5 10 0 90 15 SS8 5 4 5 5 7 1 70 16 Silica Sand #2 SS9 9 5.5 9 End of Borehole at 5.5 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH13 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2020-07-23 COMPLETED 2020-07-23 ELEVATION 43.24 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 1.70 mbgs / Elev 41.54 m ASL LOGGED BY MD CHECKED BY AW MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.1 ASHPHALTIC CONCRETE 6 6 0 Flush Mount 0.4 14 34 Casing FILL - (SP) GRAVELLY SAND, SS1 20 0.6 medium to coarse; dark brown; moist 19 FILL - (GP) SANDY GRAVEL, coarse; 10 0 0 Bentonite Seal angular; grey; moist 10 20 1 SS2 10 FILL - (SP) SAND, fine to medium; 13 light brown; moist 6 0 140 Silica Sand #2 8 16 1.7 SS3 8 FILL - (SP) SAND, fine to medium; 7 2 brownish grey; wet; hydrocarbon 10 2.1 12 3 170 odour 25 SS4 13 FILL - (GM) SILTY GRAVEL, some 8 sand to sandy; brownish grey; wet; 4 hydrocarbon odour; black staining 2 19 60 PAH, PHC, SS5 4 2 VOC 3 3.1 2 50mm Diam. (SM) SILTY SAND, trace gravel; dark 2 3 200 PVC #10 Slot grey; wet; hydrocarbon odour 3 13 Screen SS6 10 3.7 10 (SM) SILTY SAND, some gravel to 3 570 4 gravelly, cobbles and boulders, SS7 14 100+ PHC F2-F4 (GLACIAL TILL), grey; wet; faint 50/0.13 hydrocarbon odour 3 25 0 150 61 SS8 36 Silica Sand #2 4.9 39 End of Borehole at 4.9 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL Morrison Hershfield Ltd RECORD OF BOREHOLE BH14 2932 Baseline Rd PAGE 1 OF 1 Nepean, ON K2H 1B1 Telephone: 613 739 2910 CLIENT Town of Hawkesbury PROJECT NAME Phase II ESA - East End of Chenail Blvd PROJECT NUMBER 190441800 PROJECT LOCATION Hawkesbury, ON
DATE STARTED 2020-07-23 COMPLETED 2020-07-23 ELEVATION 43.41 mASL DRILLING CONTRACTOR George Downing Estate Drilling Ltd. GROUNDWATER LEVELS:
METHOD Power Auger - 200mm Diam. (Hollow Stem) STATIC WATER LEVEL 1.83 mbgs / Elev 41.58 m ASL LOGGED BY MD CHECKED BY AW MEASUREMENT DATE 2020-07-28
Headspace Organic Headspace Combustible Vapour Concentrations Vapour Concentrations ANALYSES HEX (ppm) & SOIL DESCRIPTION IBL (ppm) 2500 5000 7500 WELL DIAGRAM (m)
LOG ROCK CORE DEPTH SAMPLE
N VALUE PARAMETERS NUMBER GRAPHIC HEX (%LEL) BLOW COUNTS 0 500 1000 1500 2000 25 50 75 0.0 ASHPHALTIC CONCRETE 12 6 0 Flush Mount 21 33 Casing FILL - (GP) SANDY GRAVEL, fine; SS1 12 0.6 dark grey; moist 10 FILL - (SP) SAND, fine to medium; 10 0 0 Bentonite Seal light brown; moist 10 19 1 SS2 9 1.2 10 FILL - (SP) SAND, fine to medium, 4 0 Silica Sand #2 trace silt, trace gravel; light brown; SS3 moist; brick pieces 2 8 12 3 220 20 2.3 SS4 8 FILL - (GM) SILTY GRAVEL, some 6 2.6 sand; angular; brownish grey; wet 10 47 230 PAH, PHC, (SM) SILTY SAND, trace gravel, trace SS5 20 100+ 50/0.15 VOC 3 3.1 clay (GLACIAL TILL); brownish grey, 50mm Diam. some amber mottling; moist to wet; 12 PVC #10 Slot dark staining; hydrocarbon odour 3 270 SS6 26 62 Screen (SM) SILTY SAND, some gravel, trace 36 clay (GLACIAL TILL); brownish grey; 34 wet; faint hydrocarbon odour 2 150 4 26 100+ SS7 50/0.13
4.6 End of Borehole at 4.6 m. ENVIRONMENTAL BH WITH BLOW COUNTS HAWKESBURY PROJECT FILE - GOOD - COPY.GPJ GINT STD CANADA LAB.GDT 20-8-22 LAB.GDT CANADA STD GINT - COPY.GPJ FILE - GOOD PROJECT HAWKESBURY COUNTS WITH BLOW BH ENVIRONMENTAL APPENDIX D: Analytical Results
Phase II ESA - Table D1: Soil Analytical Results - Metals 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Soil Investigation
BH2 SA31 BH5 SA12 Sample ID: BH1 SA4 BH2 SA3 BH3 SA1 BH4 SA4 BH5 SA2 BH6 SA6 BH7 SA1 BH8 SA1 BH10 SA1 BH 11 SA2 BH 12 SA2 (SA3 DUP) (SA2 DUP) MECP Sample Date: 26-Sep-19 26-Sep-19 26-Sep-19 26-Sep-19 26-Sep-19 29-Nov-19 29-Nov-19 29-Nov-19 29-Nov-19 29-Nov-19 24-Jul-20 23-Jul-20 23-Jul-20 Units Table 3 Sample Depth (mbgs) 1.8 - 2.4 1.2 - 1.8 1.2 - 1.8 0 - 0.6 1.8 - 2.4 0.6 - 1.2 0.6 - 1.2 3.1 - 3.7 1.4 - 2.0 1.4 - 2.0 0 - 0.61 0.61 - 1.22 0.61 - 1.22 Standards(1) Certificate of Analysis L2356568 L2356568 L2356568 L2356568 L2356568 L2390921 L2390921 L2390921 L2390921 L2390921 L2480127 L2479593 L2479593 Parameter Antimony µg/g 7.5 2.4 4.7 3.1 <1.0 1.3 1.7 2.9 <1.0 <1.0 1.5 6.3 <1.0 1.3 Arsenic µg/g 18 2.4 16.9 12.2 3.8 3.9 3.6 3.4 1.6 2 12.5 39.7 2.2 8 Barium µg/g 390 101 174 129 207 106 149 151 128 101 235 145 33.8 82.3 Beryllium µg/g 4 <0.50 0.55 <0.50 <0.50 <0.50 0.69 0.61 <0.50 <0.50 0.56 0.7 <0.50 <0.50 Boron (Hot Water Soluble) µg/g 1.5 0.32 1.41 1.44 0.17 0.85 0.25 0.24 0.46 0.35 0.36 0.35 0.34 0.24 Boron µg/g 120 6.4 9.2 6.1 6.2 7.1 9.3 8.4 5.7 7 6.5 8.1 <5.0 5.8 Cadmium µg/g 1.2 <0.50 0.59 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.2 <0.50 <0.50 <0.50 Chromium µg/g 160 18.4 25 17.2 20.3 23.4 30.9 27.6 41.2 22.2 27.9 33.2 16.2 18 Chromium VI µg/g 8 <0.2 <0.2 <0.2 <0.2 <0.2 0.48 0.24 <0.20 0.59 <0.20 <0.20 <0.20 <0.20 Cobalt µg/g 22 5.9 7.6 5.1 7.3 6.8 9.1 8 11.1 7.2 9 9.3 3.6 6.9 Copper µg/g 140 15.3 46.5 33.1 19.5 162 34 32.1 16.2 15.3 35.5 99.2 7.6 23.6 Lead µg/g 120 66.8 335 199 38.3 79.1 100 117 12.9 150 376 160 22 61.3 Mercury µg/g 0.27 0.0812 0.159 0.139 0.0442 0.0726 0.124 0.223 0.0503 0.32 0.301 0.267 0.0172 0.0793 Molybdenum µg/g 6.9 <1.0 3.4 2.4 <1.0 1 <1.0 <1.0 <1.0 <1.0 2.3 10.2 <1.0 2.6 Nickel µg/g 100 12.5 19.8 14.7 15 14.8 21.2 17.5 23.8 14.8 19.8 23.3 9.2 14.9 Selenium µg/g 2.4 <1.0 1.4 1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.4 <1.0 <1.0 Silver µg/g 20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 Thallium µg/g 1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Uranium µg/g 23 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Vanadium µg/g 86 30.8 29.7 20.6 33.7 30.9 45.5 39.9 41 37.4 35.3 36.4 22.1 27.9 Zinc µg/g 340 51.7 138 99.8 69.2 117 157 177 71.6 169 536 150 224 98.3
Notes: All values in µg/g <0.02 - Not detected above the reported detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - Residential/Parkland/Institutional Property Use and Coarse Textured Soils
Page 1 of 14 Phase II ESA - Table D2: Soil Analytical Results - Polycyclic Aromatic Hydrocarbons 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Soil Investigation
BH2 SA31 BH5 SA12 Sample ID: BH1 SA4 BH2 SA3 BH3 SA1 BH4 SA4 BH5 SA2 BH6 SA6 BH7 SA1 BH8 SA1 (SA3 DUP) (SA2 DUP) MECP Sample Date: 26-Sep-19 26-Sep-19 26-Sep-19 26-Sep-19 26-Sep-19 29-Nov-19 29-Nov-19 29-Nov-19 29-Nov-19 29-Nov-19 Units Table 3 Sample Depth (mbgs) 1.8 - 2.4 1.2 - 1.8 1.2 - 1.8 0 - 0.6 1.8 - 2.4 0.6 - 1.2 0.6 - 1.2 3.1 - 3.7 1.4 - 2.0 1.4 - 2.0 Standards(1) Certificate of Analysis L2356568 L2356568 L2356568 L2356568 L2356568 L2390921 L2390921 L2390921 L2390921 L2390921 Parameter Acenaphthene µg/g 7.9 4.38 0.069 <0.050 <0.050 <0.050 <0.050 <0.050 0.098 <0.050 <0.050 Acenaphthylene µg/g 0.15 0.313 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.061 Anthracene µg/g 0.67 11.4 0.138 0.052 0.085 0.077 0.082 <0.050 0.257 <0.050 0.151 Benz(a)anthracene µg/g 0.5 16.3 0.309 0.171 0.201 0.327 0.217 0.109 0.446 0.082 0.586 Benzo(a)pyrene µg/g 0.3 13.8 0.243 0.12 0.168 0.306 0.203 0.1 0.422 0.076 0.574 Benzo(b)fluoranthene µg/g 0.78 17.9 0.358 0.207 0.237 0.426 0.297 0.138 0.501 0.104 0.758 Benzo(g,h,i)perylene µg/g 6.6 8.28 0.172 0.095 0.109 0.211 0.138 0.07 0.279 0.051 0.39 Benzo(k)fluoranthene µg/g 0.78 4.72 0.113 0.056 0.071 0.128 0.061 <0.050 0.183 <0.050 0.277 Chrysene µg/g 7 15.4 0.371 0.258 0.201 0.348 0.238 0.126 0.442 0.095 0.685 Dibenz(a,h)anthracene µg/g 0.1 2.26 <0.050 <0.050 <0.050 0.059 <0.050 <0.050 0.075 <0.050 0.094 Fluoranthene µg/g 0.69 37.7 0.626 0.276 0.451 0.662 0.459 0.212 1.03 0.154 1.33 Fluorene µg/g 62 6.58 0.058 <0.050 <0.050 <0.050 <0.050 <0.050 0.135 <0.050 0.059 Indeno(1,2,3,-cd)pyrene µg/g 0.38 8.83 0.157 0.077 0.111 0.217 0.124 0.062 0.264 <0.050 0.358 1-Methylnaphthalene µg/g NV 1.01 0.229 0.395 0.071 <0.030 <0.030 <0.030 0.035 <0.030 <0.030 2-Methylnaphthalene µg/g NV 0.554 0.255 0.432 0.086 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 Methylnaphthalene, 2-(1-) µg/g 0.99 1.56 0.484 0.827 0.157 <0.042 <0.042 <0.042 <0.042 <0.042 <0.042 Naphthalene µg/g 0.6 1.37 0.202 0.319 0.053 <0.013 0.032 <0.013 0.036 <0.013 0.032 Phenanthrene µg/g 6.2 35.9 0.617 0.399 0.343 0.277 0.348 0.106 0.748 0.081 0.726 Pyrene µg/g 78 29.9 0.507 0.239 0.377 0.55 0.384 0.187 0.865 0.139 1.12
Notes: All values in µg/g <0.02 - Not detected above the reported detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - Residential/Parkland/Institutional Property Use and Coarse Textured Soils
Page 2 of 14 Phase II ESA - Table D2: Soil Analytical Results - Polycyclic Aromatic Hydrocarbons 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Soil Investigation
BH 12 SA17 Sample ID: BH9 SA6 BH10 SA1 BH10 SA3 BH 11 SA3 BH 12 SA7 BH 13 SA5 BH 14 SA5 (SA7 DUP) MECP Sample Date: 24-Jul-20 24-Jul-20 24-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 Units Table 3 Sample Depth (mbgs) 3.05 - 3.66 0 - 0.61 1.22 - 1.83 1.22 - 1.83 3.66 - 4.27 3.66 - 4.27 2.44 - 3.05 2.44 - 3.05 Standards(1) Certificate of Analysis L2480127 L2480127 L2480127 L2479593 L2479593 L2479593 L2479593 L2479593 Parameter Acenaphthene µg/g 7.9 0.122 0.205 0.514 <0.050 <0.050 <0.050 <0.050 <0.050 Acenaphthylene µg/g 0.15 <0.050 0.137 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Anthracene µg/g 0.67 <0.050 0.319 0.094 <0.050 <0.050 <0.050 <0.050 <0.050 Benz(a)anthracene µg/g 0.5 0.064 0.659 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Benzo(a)pyrene µg/g 0.3 <0.050 0.399 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Benzo(b)fluoranthene µg/g 0.78 0.065 0.501 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Benzo(g,h,i)perylene µg/g 6.6 <0.050 0.176 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Benzo(k)fluoranthene µg/g 0.78 <0.050 0.122 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Chrysene µg/g 7 0.07 0.851 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Dibenz(a,h)anthracene µg/g 0.1 <0.050 0.074 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Fluoranthene µg/g 0.69 0.109 0.991 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Fluorene µg/g 62 0.154 0.216 0.758 <0.050 <0.050 <0.050 <0.050 <0.050 Indeno(1,2,3,-cd)pyrene µg/g 0.38 <0.050 0.13 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 1-Methylnaphthalene µg/g NV 1.51 3.87 7.55 0.063 <0.030 <0.030 0.045 0.061 2-Methylnaphthalene µg/g NV 1.6 3.95 12.5 <0.030 <0.030 <0.030 0.037 <0.030 Methylnaphthalene, 2-(1-) µg/g 0.99 3.1 7.82 20 0.063 <0.042 <0.042 0.082 0.061 Naphthalene µg/g 0.6 0.515 2.07 4.4 <0.013 <0.013 <0.013 0.023 0.021 Phenanthrene µg/g 6.2 0.311 2.74 1.16 <0.046 <0.046 <0.046 <0.046 <0.046 Pyrene µg/g 78 0.1 0.962 0.057 <0.050 <0.050 <0.050 <0.050 <0.050
Notes: All values in µg/g <0.02 - Not detected above the reported detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - Residential/Parkland/Institutional Property Use and Coarse Textured Soils
Page 3 of 14 Phase II ESA - Table D3: Soil Analytical Results - Petroleum Hydrocarbons 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Soil Investigation
BH1 SA21 BH6 SA16 Sample ID: BH1 SA7 BH2 SA7 BH3 SA8 BH4 SA5 BH5 SA6 BH6 SA6 BH7 SA4 BH8 SA3 BH9 SA4 BH9 SA5 BH9 SA6 (SA7 DUP) (SA6 DUP) Sample Date: MECP 26-Sep-19 26-Sep-19 26-Sep-19 26-Sep-19 26-Sep-19 29-Nov-19 29-Nov-19 29-Nov-19 29-Nov-19 29-Nov-19 24-Jul-20 24-Jul-20 24-Jul-20 Sample Depth (mbgs) Units Table 3 3.7 - 4.3 3.7 - 4.3 3.7 - 4.3 4.3 - 4.9 2.4 - 3.1 3.1 - 3.7 3.1 - 3.7 3.1 - 3.7 3.7 - 4.3 3.1 - 3.7 1.83 - 2.44 2.44 - 3.05 3.05 - 3.66 CGI Measurement (ppm) Standards(1) 85 85 10 190 20 85 95 95 95 35 450 280 90 Certificate of Analysis L2356568 L2356568 L2356568 L2356568 L2356568 L2390921 L2390921 L2390921 L2390921 L2390921 L2480127 L2480127 L2480127 Parameter Benzene µg/g 0.21 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 0.0106 0.0071 <0.0068 <0.0068 - 0.141 - Ethylbenzene µg/g 2 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 - 0.05 - Toluene µg/g 2.3 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 - <0.080 - o-Xylene µg/g NV <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 - <0.020 - p+m-Xylene µg/g NV <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 - 0.067 - Total Xylenes µg/g 3.1 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 - 0.067 - PHC F1 (C6-C10) µg/g 55 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 - 7.5 - PHC F2 (>C10-C16) µg/g 98 <10 <10 <10 <10 <10 <10 <10 <10 62 <10 477 - 568 PHC F3 (>C16-C34) µg/g 300 <50 58 <50 <50 <50 <50 125 77 870 <50 241 - 286 PHC F4 (>C34-C50) µg/g 2800 <50 58 <50 <50 <50 <50 133 60 190 93 <50 - <50 PHC F4G-SG (GHH-Silica) µg/g 2800 ------550 - 490 - - - -
Notes: All values in µg/g <0.02 - Not detected above the reported detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - Residential/Parkland/Institutional Property Use and Coarse Textured Soils
Page 4 of 14 Phase II ESA - Table D3: Soil Analytical Results - Petroleum Hydrocarbons 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Soil Investigation
BH 12 SA17 BH 13 SA15 Sample ID: BH10 SA3 BH10 SA5 BH 11 SA3 BH 11 SA7 BH 12 SA7 BH 13 SA5 BH 13 SA7 BH 14 SA5 (SA7 DUP) (SA5 DUP) Sample Date: MECP 24-Jul-20 24-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 Sample Depth (mbgs) Units Table 3 1.22 - 1.83 2.44 - 3.05 1.22 - 1.83 3.66 - 4.27 3.66 - 4.27 3.66 - 4.27 2.44 - 3.05 2.44 - 3.05 3.66 - 4.27 2.44 - 3.05 CGI Measurement (ppm) Standards(1) 2700 470 320 110 620 620 60 60 570 230 Certificate of Analysis L2480127 L2480127 L2479593 L2479593 L2479593 L2479593 L2479593 L2479593 L2479593 L2479593 Parameter Benzene µg/g 0.21 0.79 - 0.0299 - <0.0068 - 0.0388 0.199 - <0.0068 Ethylbenzene µg/g 2 38 - <0.018 - <0.018 - 0.024 0.087 - <0.018 Toluene µg/g 2.3 0.504 - <0.080 - <0.080 - <0.080 0.148 - <0.080 o-Xylene µg/g NV 1.64 - <0.020 - <0.020 - <0.020 0.052 - <0.020 p+m-Xylene µg/g NV 8.86 - <0.030 - <0.030 - 0.055 0.202 - <0.030 Total Xylenes µg/g 3.1 10.5 - <0.050 - <0.050 - 0.055 0.255 - <0.050 PHC F1 (C6-C10) µg/g 55 1800 - <5.0 - <5.0 - 6.7 17.1 - <5.0 PHC F2 (>C10-C16) µg/g 98 1780 <10 <10 <10 <10 <10 <10 - 84 34 PHC F3 (>C16-C34) µg/g 300 1520 <50 <50 <50 <50 <50 <50 - 72 <50 PHC F4 (>C34-C50) µg/g 2800 173 <50 <50 <50 <50 <50 <50 - <50 <50 PHC F4G-SG (GHH-Silica) µg/g 2800 ------
Notes: All values in µg/g <0.02 - Not detected above the reported detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - Residential/Parkland/Institutional Property Use and Coarse Textured Soils
Page 5 of 14 Phase II ESA - Table D4: Soil Analytical Results - 190441800 East End of Chenail Blvd Volatile Organic Compounds
Phase II ESA - East End of Chenail Blvd Soil Investigation
BH1 SA21 BH6 SA16 Sample ID: BH1 SA7 BH2 SA7 BH3 SA8 BH4 SA5 BH5 SA6 BH6 SA6 BH7 SA4 BH8 SA3 BH9 SA5 BH10 SA3 BH 11 SA3 (SA7 DUP) (SA6 DUP) MECP Sample Date: 26-Sep-19 26-Sep-19 26-Sep-19 26-Sep-19 26-Sep-19 29-Nov-19 29-Nov-19 29-Nov-19 29-Nov-19 29-Nov-19 24-Jul-20 24-Jul-20 23-Jul-20 Units Table 3 Sample Depth (mBGS) 3.7 - 4.3 3.7 - 4.3 3.7 - 4.3 4.3 - 4.9 2.4 - 3.1 3.1 - 3.7 3.1 - 3.7 3.1 - 3.7 3.7 - 4.3 3.1 - 3.7 2.44 - 3.05 1.22 - 1.83 1.22 - 1.83 Standards(1) Certificate of Analysis L2356568 L2356568 L2356568 L2356568 L2356568 L2390921 L2390921 L2390921 L2390921 L2390921 L2480127 L2480127 L2479593 Parameter Acetone µg/g 16 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <8.0 <0.50 Benzene µg/g 0.21 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 0.0106 0.0071 <0.0068 <0.0068 0.141 0.79 0.0299 Bromodichloromethane µg/g 13 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Bromoform µg/g 0.27 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Bromomethane µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Carbon Tetrachloride µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Chlorobenzene µg/g 2.4 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Chloroform µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Dibromochloromethane µg/g 9.4 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Dichlorobenzene,1,2- µg/g 3.4 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Dichlorobenzene,1,3- µg/g 4.8 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Dichlorobenzene,1,4- µg/g 0.083 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Dichlorodifluoromethane µg/g 16 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Dichloroethane,1,1- µg/g 3.5 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Dichloroethane,1,2- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Dichloroethylene,1,1- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Dichloroethylene, cis-1,2- µg/g 3.4 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Dichloroethylene, trans-1,2- µg/g 0.084 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Dichloropropane,1,2- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Dichloropropene, cis-1,3- µg/g NV <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.48 <0.030 Dichloropropene, trans-1,3- µg/g NV <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 Dichloropropene 1,3- cis+trans µg/g 0.05 <0.042 <0.042 <0.042 <0.042 <0.042 <0.042 <0.042 <0.042 <0.042 <0.042 <0.042 <0.48 <0.042 Ethylbenzene µg/g 2 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 <0.018 0.05 38 <0.018 Ethylene Dibromide µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Hexane µg/g 2.8 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.457 37.3 <0.050 Methyl Ethyl Ketone µg/g 16 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <8.0 <0.50 Methyl Isobutyl Ketone µg/g 1.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <8.0 <0.50 Methyl-t-butyl Ether µg/g 0.75 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Methylene Chloride µg/g 0.1 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Styrene µg/g 0.7 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Tetrachloroethane,1,1,1,2- µg/g 0.058 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Tetrachloroethane,1,1,2,2- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Tetrachloroethylene µg/g 0.28 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Toluene µg/g 2.3 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 0.504 <0.080 Trichloroethane,1,1,1- µg/g 0.38 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Trichloroethane,1,1,2- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Trichloroethylene µg/g 0.061 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.16 <0.010 Trichlorofluoromethane µg/g 4 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.80 <0.050 Vinyl Chloride µg/g 0.02 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.32 <0.020 Xylene, m,p- µg/g NV <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 <0.020 1.64 <0.030 Xylene, o- µg/g NV <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 <0.030 0.067 8.86 <0.020 Xylene, m,p,o- µg/g 3.1 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.067 10.5 <0.050
Notes: All values in µg/g <0.02 - Not detected above the reported detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - Residential/Parkland/Institutional Property Use and Coarse Textured Soils
Page 6 of 14 Phase II ESA - Table D4: Soil Analytical Results - 190441800 East End of Chenail Blvd Volatile Organic Compounds
Phase II ESA - East End of Chenail Blvd Soil Investigation
BH 13 SA15 Sample ID: BH 12 SA7 BH 13 SA5 BH 14 SA5 (SA5 DUP) MECP Sample Date: 23-Jul-20 23-Jul-20 23-Jul-20 23-Jul-20 Units Table 3 Sample Depth (mBGS) 3.66 - 4.27 2.44 - 3.05 2.44 - 3.05 2.44 - 3.05 Standards(1) Certificate of Analysis L2479593 L2479593 L2479593 L2479593 Parameter Acetone µg/g 16 <0.50 <0.50 <0.50 <0.50 Benzene µg/g 0.21 <0.0068 0.0388 0.199 <0.0068 Bromodichloromethane µg/g 13 <0.050 <0.050 <0.050 <0.050 Bromoform µg/g 0.27 <0.050 <0.050 <0.050 <0.050 Bromomethane µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Carbon Tetrachloride µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Chlorobenzene µg/g 2.4 <0.050 <0.050 <0.050 <0.050 Chloroform µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Dibromochloromethane µg/g 9.4 <0.050 <0.050 <0.050 <0.050 Dichlorobenzene,1,2- µg/g 3.4 <0.050 <0.050 <0.050 <0.050 Dichlorobenzene,1,3- µg/g 4.8 <0.050 <0.050 <0.050 <0.050 Dichlorobenzene,1,4- µg/g 0.083 <0.050 <0.050 <0.050 <0.050 Dichlorodifluoromethane µg/g 16 <0.050 <0.050 <0.050 <0.050 Dichloroethane,1,1- µg/g 3.5 <0.050 <0.050 <0.050 <0.050 Dichloroethane,1,2- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Dichloroethylene,1,1- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Dichloroethylene, cis-1,2- µg/g 3.4 <0.050 <0.050 <0.050 <0.050 Dichloroethylene, trans-1,2- µg/g 0.084 <0.050 <0.050 <0.050 <0.050 Dichloropropane,1,2- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Dichloropropene, cis-1,3- µg/g NV <0.030 <0.030 <0.030 <0.030 Dichloropropene, trans-1,3- µg/g NV <0.030 <0.030 <0.030 <0.030 Dichloropropene 1,3- cis+trans µg/g 0.05 <0.042 <0.042 <0.042 <0.042 Ethylbenzene µg/g 2 <0.018 0.024 0.087 <0.018 Ethylene Dibromide µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Hexane µg/g 2.8 <0.050 <0.050 0.107 <0.050 Methyl Ethyl Ketone µg/g 16 <0.50 <0.50 <0.50 <0.50 Methyl Isobutyl Ketone µg/g 1.7 <0.50 <0.50 <0.50 <0.50 Methyl-t-butyl Ether µg/g 0.75 <0.050 <0.050 <0.050 <0.050 Methylene Chloride µg/g 0.1 <0.050 <0.050 <0.050 <0.050 Styrene µg/g 0.7 <0.050 <0.050 <0.050 <0.050 Tetrachloroethane,1,1,1,2- µg/g 0.058 <0.050 <0.050 <0.050 <0.050 Tetrachloroethane,1,1,2,2- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Tetrachloroethylene µg/g 0.28 <0.050 <0.050 <0.050 <0.050 Toluene µg/g 2.3 <0.080 <0.080 0.148 <0.080 Trichloroethane,1,1,1- µg/g 0.38 <0.050 <0.050 <0.050 <0.050 Trichloroethane,1,1,2- µg/g 0.05 <0.050 <0.050 <0.050 <0.050 Trichloroethylene µg/g 0.061 <0.010 <0.010 <0.010 <0.010 Trichlorofluoromethane µg/g 4 <0.050 <0.050 <0.050 <0.050 Vinyl Chloride µg/g 0.02 <0.020 <0.020 <0.020 <0.020 Xylene, m,p- µg/g NV <0.030 0.055 0.202 <0.030 Xylene, o- µg/g NV <0.020 <0.020 0.052 <0.020 Xylene, m,p,o- µg/g 3.1 <0.050 0.055 0.255 <0.050
Notes: All values in µg/g <0.02 - Not detected above the reported detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - Residential/Parkland/Institutional Property Use and Coarse Textured Soils
Page 7 of 14 Phase II ESA - Table D5: Groundwater Analytical Results - Dissolved Metals 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Groundwater Investigation
BH21 DUP Sample ID: BH1 BH2 BH3 BH4 BH5 BH6 BH7 BH8 MECP (BH1 DUP) (BH6 DUP) Sample Date: Units Table 3 2-Oct-19 2-Oct-19 2-Oct-19 2-Oct-19 2-Oct-19 6-Dec-19 6-Dec-19 6-Dec-19 6-Dec-19 6-Dec-19 (1) Certificate of Analysis Standards L2359740 L2359740 L2359740 L2359740 L2359740 L2395477 L2395477 L2395477 L2395477 L2395477 Parameter Antimony µg/L 20000 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Arsenic µg/L 1900 1.6 1.6 1.5 1.5 1.1 <1.0 <1.0 <1.0 1 6.3 Barium µg/L 29000 848 905 917 692 288 462 988 1010 485 777 Beryllium µg/L 67 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Boron µg/L 45000 120 120 <100 250 <100 <100 <100 <100 <100 <100 Cadmium µg/L 2.7 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.061 <0.050 Chromium µg/L 810 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Chromium VI µg/L 140 ------<0.50 - - - Cobalt µg/L 66 <1.0 <1.0 2.6 2 4.9 6.8 <1.0 <1.0 6.9 1.3 Copper µg/L 87 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 3.2 <2.0 Lead µg/L 25 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Mercury µg/L 0.29 ------<0.0050 - - - Molybdenum µg/L 9200 0.63 0.64 1.85 1.27 0.78 2.25 <0.50 <0.50 1.35 0.82 Nickel µg/L 490 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Selenium µg/L 63 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.72 0.57 <0.50 <0.50 Silver µg/L 1.5 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Sodium µg/L 2300000 330000 345000 126000 336000 109000 365000 621000 611000 99000 142000 Thallium µg/L 510 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 Uranium µg/L 420 0.22 0.22 0.62 0.31 2.14 0.88 <0.10 <0.10 2.07 0.48 Vanadium µg/L 250 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Zinc µg/L 1100 <10 <10 <10 <10 <10 <10 <10 <10 <10 13
Notes: All values in µg/L <0.02 - Not detected above the reported detection limits NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - All Types of Property Use and Coarse Textured Soils
Page 8 of 14 Phase II ESA - Table D6: Groundwater Analytical Results - Polycyclic Aromatic Hydrocarbons 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Groundwater Investigation
BH21 DUP DUP Sample ID: BH1 BH2 BH3 BH4 BH5 BH6 BH7 BH8 BH9 BH10 MECP (BH1 DUP) (BH6 DUP) (BH10 DUP) Sample Date: Units Table 3 2-Oct-19 2-Oct-19 2-Oct-19 2-Oct-19 2-Oct-19 6-Dec-19 6-Dec-19 6-Dec-19 6-Dec-19 6-Dec-19 28-Jul-20 28-Jul-20 28-Jul-20 (1) Certificate of Analysis Standards L2359740 L2359740 L2359740 L2359740 L2359740 L2395477 L2395477 L2395477 L2395477 L2395477 L2481358 L2481358 L2481358 Parameter Acenaphthene µg/L 600 8.41 10.5 <0.020 <0.020 <0.020 <0.025 3.98 2.72 0.112 0.032 0.248 0.12 0.121 Acenaphthylene µg/L 1.8 0.354 0.451 <0.020 <0.020 <0.020 <0.020 0.236 0.185 <0.020 <0.020 <0.062 <0.020 <0.020 Anthracene µg/L 2.4 9.7 14.1 <0.020 <0.020 0.035 0.035 7.17 4.44 0.022 0.082 <0.040 <0.020 <0.020 Benzo(a)anthracene µg/L 4.7 9.22 13.5 <0.020 <0.020 0.082 0.104 14.3 10.5 0.034 0.24 <0.020 <0.020 <0.020 Benzo(a)pyrene µg/L 0.81 6.35 9.35 <0.010 <0.010 0.06 0.091 12 8.43 0.026 0.197 <0.010 <0.010 <0.010 Benzo(b)fluoranthene µg/L 0.75 7.13 10.3 <0.020 <0.020 0.077 0.119 14.2 10.7 0.034 0.249 <0.020 <0.020 <0.020 Benzo(g,h,i)perylene µg/L 0.2 3.86 5.86 <0.020 <0.020 0.043 0.066 6.25 5.61 <0.020 0.131 <0.020 <0.020 <0.020 Benzo(k)fluoranthene µg/L 0.4 2.66 3.68 <0.020 <0.020 0.031 0.045 4.49 3.12 <0.020 0.093 <0.020 <0.020 <0.020 Chrysene µg/L 1 7.26 10.4 <0.020 <0.020 0.072 0.114 11.5 7.99 0.031 0.244 <0.020 <0.020 <0.020 Dibenzo(a,h)anthracene µg/L 0.52 0.909 1.42 <0.020 <0.020 <0.020 <0.020 1.3 1.16 <0.020 0.03 <0.020 <0.020 <0.020 Fluoranthene µg/L 130 26.3 38.5 0.032 0.037 0.23 0.243 29.3 20.6 0.081 0.608 0.056 0.033 0.03 Fluorene µg/L 400 18.8 24.3 <0.020 0.027 0.026 0.048 5.34 3.39 0.064 0.063 0.265 0.068 0.067 Indeno(1,2,3,-cd)pyrene µg/L 0.2 4.61 7.17 <0.020 <0.020 0.052 0.076 8.36 7.12 0.021 0.152 <0.020 <0.020 <0.020 Methylnaphthalene, 1- µg/L 1800 4.33 5.11 <0.020 <0.020 <0.020 0.026 0.778 0.538 0.054 0.023 6.36 0.82 0.81 Methylnaphthalene, 2- µg/L 1800 0.981 1.22 <0.020 0.024 <0.020 0.03 0.162 0.092 0.043 0.039 3.93 1.05 1.03 Methylnaphthalene, 2-(1-) µg/L 1800 5.31 6.32 <0.028 <0.028 <0.028 0.056 0.94 0.63 0.097 0.062 10.3 1.87 1.84 Naphthalene µg/L 1400 4.92 5.48 <0.050 <0.050 <0.050 <0.050 <0.34 <0.26 0.099 <0.050 <1.62 1.91 <1.90 Phenanthrene µg/L 580 49.7 76 0.054 0.119 0.214 0.257 20.6 13.9 0.147 0.571 0.256 0.072 0.069 Pyrene µg/L 68 22.4 33 0.102 0.105 0.274 0.235 25.8 18.4 0.073 0.562 0.087 0.035 0.03
Notes: All values in µg/L <0.02 - Not detected above the reported detection limits NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - All Types of Property Use and Coarse Textured Soils
Page 9 of 14 Phase II ESA - Table D6: Groundwater Analytical Results - Polycyclic Aromatic Hydrocarbons 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Groundwater Investigation
Sample ID: BH1 BH11 BH12 BH13 BH14 MECP Sample Date: Units Table 3 2-Oct-19 28-Jul-20 28-Jul-20 28-Jul-20 28-Jul-20 (1) Certificate of Analysis Standards L2359740 L2481358 L2481358 L2481358 L2481358 Parameter Acenaphthene µg/L 600 8.41 0.304 <0.020 0.083 0.331 Acenaphthylene µg/L 1.8 0.354 0.062 <0.020 <0.035 <0.075 Anthracene µg/L 2.4 9.7 <0.060 <0.020 <0.035 <0.110 Benzo(a)anthracene µg/L 4.7 9.22 0.075 0.036 0.051 0.074 Benzo(a)pyrene µg/L 0.81 6.35 0.055 0.025 0.035 0.051 Benzo(b)fluoranthene µg/L 0.75 7.13 0.075 0.034 0.05 0.064 Benzo(g,h,i)perylene µg/L 0.2 3.86 0.031 <0.020 0.026 0.033 Benzo(k)fluoranthene µg/L 0.4 2.66 0.026 <0.020 <0.020 0.022 Chrysene µg/L 1 7.26 0.067 0.029 0.043 0.056 Dibenzo(a,h)anthracene µg/L 0.52 0.909 <0.020 <0.020 <0.020 <0.020 Fluoranthene µg/L 130 26.3 0.168 0.088 0.124 0.284 Fluorene µg/L 400 18.8 0.372 <0.020 <0.042 0.197 Indeno(1,2,3,-cd)pyrene µg/L 0.2 4.61 0.04 <0.020 0.032 0.04 Methylnaphthalene, 1- µg/L 1800 4.33 3.52 0.025 0.067 0.361 Methylnaphthalene, 2- µg/L 1800 0.981 1.29 0.027 0.028 0.062 Methylnaphthalene, 2-(1-) µg/L 1800 5.31 4.8 0.052 0.096 0.423 Naphthalene µg/L 1400 4.92 <2.35 <0.050 <0.130 <0.120 Phenanthrene µg/L 580 49.7 0.315 0.089 0.034 0.362 Pyrene µg/L 68 22.4 0.225 0.11 0.133 0.295
Notes: All values in µg/L <0.02 - Not detected above the reported detection limits NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - All Types of Property Use and Coarse Textured Soils
Page 10 of 14 Phase II ESA - Table D7: Groundwater Analytical Results - Petroleum Hydrocarbons 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Groundwater Investigation
BH21 DUP Sample ID: BH1 BH2 BH3 BH4 BH5 BH6 BH7 BH8 BH9 BH10 MECP (BH1 DUP) (BH6 DUP) Sample Date: Units Table 3 2-Oct-19 2-Oct-19 2-Oct-19 2-Oct-19 2-Oct-19 6-Dec-19 6-Dec-19 6-Dec-19 6-Dec-19 6-Dec-19 28-Jul-20 28-Jul-20 (1) Certificate of Analysis Standards L2359740 L2359740 L2359740 L2359740 L2359740 L2395477 L2395477 L2395477 L2395477 L2395477 L2481358 L2481358 Parameter Total Suspended Solids mg/L NV ------1060 1730 Benzene µg/L 44 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 88.3 5.65 Ethylbenzene µg/L 2300 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 12.4 17.9 Toluene µg/L 18000 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 6.73 1.26 o-Xylene µg/L NV <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 1.32 1.41 p+m-Xylene µg/L NV <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 10 6.2 Total Xylenes µg/L 4200 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 11.4 7.61 PHC F1 (C6-C10) µg/L 750 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 394 177 PHC F2 (>C10-C16) µg/L 150 210 210 <100 <100 <100 <100 140 120 <100 <100 620 100 PHC F3 (>C16-C34) µg/L 500 870 1150 <250 <250 <250 300 10800 8710 <250 <250 320 <250 PHC F4 (>C34-C50) µg/L 500 630 890 <250 <250 <250 360 5190 4100 <250 360 <250 <250
Notes: All values in µg/L <0.02 - Not detected above the reporting detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - All Types of Property Use and Coarse Textured Soils
Page 11 of 14 Phase II ESA - Table D7: Groundwater Analytical Results - Petroleum Hydrocarbons 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Groundwater Investigation
DUP Sample ID: BH11 BH12 BH13 BH14 MECP (BH10 DUP) Sample Date: Units Table 3 28-Jul-20 28-Jul-20 28-Jul-20 28-Jul-20 28-Jul-20 (1) Certificate of Analysis Standards L2481358 L2481358 L2481358 L2481358 L2481358 Parameter Total Suspended Solids mg/L NV - 11800 4490 8010 11400 Benzene µg/L 44 5.43 8.51 <0.50 0.7 0.54 Ethylbenzene µg/L 2300 16.8 19.4 <0.50 <0.50 <0.50 Toluene µg/L 18000 1.2 <0.50 <0.50 <0.50 <0.50 o-Xylene µg/L NV 1.33 0.33 <0.30 <0.30 <0.30 p+m-Xylene µg/L NV 5.79 0.94 <0.40 0.51 0.46 Total Xylenes µg/L 4200 7.12 1.27 <0.50 0.51 <0.50 PHC F1 (C6-C10) µg/L 750 169 151 <25 <25 66 PHC F2 (>C10-C16) µg/L 150 110 240 <100 230 450 PHC F3 (>C16-C34) µg/L 500 <250 <250 <250 270 320 PHC F4 (>C34-C50) µg/L 500 <250 <250 <250 <250 <250
Notes: All values in µg/L <0.02 - Not detected above the reporting detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards(1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - All Types of Property Use and Coarse Textured Soils
Page 12 of 14 Phase II ESA - Table D8: Groundwater Analytical Results - 190441800 East End of Chenail Blvd Volatile Organic Compounds
Phase II ESA - East End of Chenail Blvd Groundwater Investigation
BH21 DUP DUP Sample ID: BH1 BH2 BH3 BH4 BH5 BH6 BH7 BH8 BH9 BH10 MECP (BH1 DUP) (BH6 DUP) (BH10 DUP) Sample Date: Units Table 3 2-Oct-19 2-Oct-19 2-Oct-19 2-Oct-19 2-Oct-19 6-Dec-19 6-Dec-19 6-Dec-19 6-Dec-19 6-Dec-19 28-Jul-20 28-Jul-20 28-Jul-20 (1) Certificate of Analysis Standards L2359740 L2359740 L2359740 L2359740 L2359740 L2395477 L2395477 L2395477 L2395477 L2395477 L2481358 L2481358 L2481358 Parameter Acetone µg/L 130000 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 Benzene µg/L 44 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 88.3 5.65 5.43 Bromodichloromethane µg/L 85000 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 Bromoform µg/L 380 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Bromomethane µg/L 5.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Carbon Tetrachloride µg/L 0.79 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 Chlorobenzene µg/L 630 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Chloroform µg/L 2.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.7 <1.0 <1.0 Dibromochloromethane µg/L 82000 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 Dichlorobenzene,1,2- µg/L 4600 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Dichlorobenzene,1,3- µg/L 9600 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Dichlorobenzene,1,4- µg/L 8 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Dichlorodifluoromethane µg/L 4400 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 Dichloroethane,1,1- µg/L 320 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Dichloroethane,1,2- µg/L 1.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Dichloroethylene,1,1- µg/L 1.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Dichloroethene, cis-1,2- µg/L 1.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.3 <0.50 <0.50 Dichloroethene, trans-1,2- µg/L 1.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Dichloropropane,1,2- µg/L 16 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Dichloropropene, cis-1,3- µg/L NV <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 Dichloropropene, trans-1,3- µg/L NV <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 Dichloropropene 1,3- cis+trans µg/L 5.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Ethylbenzene µg/L 2300 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 12.4 17.9 16.8 Ethylene Dibromide µg/L 0.25 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.28 <0.46 <0.40 Hexane µg/L 51 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 14 3.42 2.62 Methyl Ethyl Ketone µg/L 470000 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 Methyl Isobutyl Ketone µg/L 140000 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 Methyl-t-butyl Ether µg/L 190 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 Methylene Chloride µg/L 610 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Styrene µg/L 1300 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Tetrachloroethane,1,1,1,2- µg/L 3.3 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Tetrachloroethane,1,1,2,2- µg/L 3.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.60 <0.50 <0.50 Tetrachloroethylene µg/L 1.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Toluene µg/L 18000 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 6.73 1.26 1.2 Trichloroethane,1,1,1- µg/L 640 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trichloroethane,1,1,2- µg/L 4.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trichloroethylene µg/L 1.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trichlorofluoromethane µg/L 2500 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Vinyl Chloride µg/L 0.5 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Xylene, m,p- µg/L NV <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 1.32 1.41 1.33 Xylene, o- µg/L NV <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 10 6.2 5.79 Xylene, m,p,o- µg/L 4200 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 11.4 7.61 7.12
Notes: All values in µg/L <0.02 - Not detected above the reporting detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards (1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - All Types of Property Use and Coarse Textured Soils
Page 13 of 14 Phase II ESA - Table D8: Groundwater Analytical Results - 190441800 East End of Chenail Blvd Volatile Organic Compounds
Phase II ESA - East End of Chenail Blvd Groundwater Investigation
Sample ID: BH11 BH12 BH13 BH14 MECP Sample Date: Units Table 3 28-Jul-20 28-Jul-20 28-Jul-20 28-Jul-20 (1) Certificate of Analysis Standards L2481358 L2481358 L2481358 L2481358 Parameter Acetone µg/L 130000 <30 <30 <30 <30 Benzene µg/L 44 8.51 <0.50 0.7 0.54 Bromodichloromethane µg/L 85000 <2.0 <2.0 <2.0 <2.0 Bromoform µg/L 380 <5.0 <5.0 <5.0 <5.0 Bromomethane µg/L 5.6 <0.50 <0.50 <0.50 <0.50 Carbon Tetrachloride µg/L 0.79 <0.20 <0.20 <0.20 <0.20 Chlorobenzene µg/L 630 <0.50 <0.50 <0.50 <0.50 Chloroform µg/L 2.4 <1.0 <1.0 <1.0 <1.0 Dibromochloromethane µg/L 82000 <2.0 <2.0 <2.0 <2.0 Dichlorobenzene,1,2- µg/L 4600 <0.50 <0.50 <0.50 <0.50 Dichlorobenzene,1,3- µg/L 9600 <0.50 <0.50 <0.50 <0.50 Dichlorobenzene,1,4- µg/L 8 <0.50 <0.50 <0.50 <0.50 Dichlorodifluoromethane µg/L 4400 <2.0 <2.0 <2.0 <2.0 Dichloroethane,1,1- µg/L 320 <0.50 <0.50 <0.50 <0.50 Dichloroethane,1,2- µg/L 1.6 <0.50 <0.50 <0.50 <0.50 Dichloroethylene,1,1- µg/L 1.6 <0.50 <0.50 <0.50 <0.50 Dichloroethene, cis-1,2- µg/L 1.6 <0.50 <0.50 <0.50 <0.50 Dichloroethene, trans-1,2- µg/L 1.6 <0.50 <0.50 <0.50 <0.50 Dichloropropane,1,2- µg/L 16 <0.50 <0.50 <0.50 <0.50 Dichloropropene, cis-1,3- µg/L NV <0.30 <0.30 <0.30 <0.30 Dichloropropene, trans-1,3- µg/L NV <0.30 <0.30 <0.30 <0.30 Dichloropropene 1,3- cis+trans µg/L 5.2 <0.50 <0.50 <0.50 <0.50 Ethylbenzene µg/L 2300 19.4 <0.50 <0.50 <0.50 Ethylene Dibromide µg/L 0.25 <0.20 <0.20 <0.20 <0.20 Hexane µg/L 51 2.96 <0.50 <0.50 <0.50 Methyl Ethyl Ketone µg/L 470000 <20 <20 <20 <20 Methyl Isobutyl Ketone µg/L 140000 <20 <20 <20 <20 Methyl-t-butyl Ether µg/L 190 <2.0 <2.0 <2.0 <2.0 Methylene Chloride µg/L 610 <5.0 <5.0 <5.0 <5.0 Styrene µg/L 1300 <0.50 <0.50 <0.50 <0.50 Tetrachloroethane,1,1,1,2- µg/L 3.3 <0.50 <0.50 <0.50 <0.50 Tetrachloroethane,1,1,2,2- µg/L 3.2 <0.50 <0.50 <0.50 <0.50 Tetrachloroethylene µg/L 1.6 <0.50 <0.50 <0.50 <0.50 Toluene µg/L 18000 <0.50 <0.50 <0.50 <0.50 Trichloroethane,1,1,1- µg/L 640 <0.50 <0.50 <0.50 <0.50 Trichloroethane,1,1,2- µg/L 4.7 <0.50 <0.50 <0.50 <0.50 Trichloroethylene µg/L 1.6 <0.50 <0.50 <0.50 <0.50 Trichlorofluoromethane µg/L 2500 <5.0 <5.0 <5.0 <5.0 Vinyl Chloride µg/L 0.5 <0.50 <0.50 <0.50 <0.50 Xylene, m,p- µg/L NV 0.33 <0.30 <0.30 <0.30 Xylene, o- µg/L NV 0.94 <0.40 0.51 0.46 Xylene, m,p,o- µg/L 4200 1.27 <0.50 0.51 <0.50
Notes: All values in µg/L <0.02 - Not detected above the reporting detection limits mbgs - metres below ground surface NV - No Value NA - Not Analyzed
Screening: BOLD Parameter exceeded MECP (April 15, 2011) Table 3 Standards (1)
References: 1- MECP Soil, Groundwater and Sediment Standards for Use Under Part XV.1 of the Environmental Protection Act (April 15, 2011) - Table 3 - Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition - All Types of Property Use and Coarse Textured Soils
Page 14 of 14 Phase II ESA - Table D9: TCLP Results 190441800 East End of Chenail Blvd
Phase II ESA - East End of Chenail Blvd Soil Investigation
Soil Sample ID O.Reg.347 TCLP-HK TCLP-HK TCLP-3 Sample Date Schedule 4 26-Sep-19 29-Nov-19 23-Jul-20 Units Certificate of Analysis Leachate Quality L2356576 L2390935 L2479604 (1) Parameter Criteria Inorganics Final pH mg/L NV 9.09 8.48 7.53 Initial pH mg/L NV 6.25 6.17 5.13 Metals Leachable Arsenic (As) mg/L 2.5 <0.050 <0.050 <0.050 Leachable Barium (Ba) mg/L 100 1.1 0.78 1.09 Leachable Boron (B) mg/L 500 <2.5 <2.5 <2.5 Leachable Cadmium (Cd) mg/L 0.5 <0.0050 <0.0050 <0.0050 Leachable Chromium (Cr) mg/L 5 <0.050 <0.050 <0.050 Leachable Lead (Pb) mg/L 5 <0.050 <0.050 <0.025 Leachable Mercury (Hg) mg/L 0.1 <0.00010 <0.00010 <0.00010 Leachable Selenium (Se) mg/L 1 <0.025 <0.025 <0.025 Leachable Silver (Ag) mg/L 5 <0.0050 <0.0050 <0.0050 Leachable Uranium (U) mg/L 10 <0.25 <0.25 <0.25 Volatile Organics Leachable Benzene mg/L 0.5 - <0.025 <0.025 Leachable Carbon Tetrachloride mg/L 0.5 - <0.025 <0.025 Leachable Chlorobenzene mg/L 8 - <0.025 <0.025 Leachable Chloroform mg/L 10 - <0.10 <0.10 Leachable 1,2-Dichlorobenzene mg/L 20 - <0.025 <0.025 Leachable 1,4-Dichlorobenzene mg/L 0.5 - <0.025 <0.025 Leachable 1,2-Dichloroethane mg/L 0.5 - <0.025 <0.025 Leachable 1,1-Dichloroethylene mg/L 1.4 - <0.025 <0.025 Leachable Methyl Ethyl Ketone mg/L 200 - <1.0 <1.0 Leachable Tetrachloroethylene mg/L 3 - <0.025 <0.025 Leachable Trichloroethylene mg/L 5 - <0.025 <0.025 Leachable Vinyl Chloride mg/L 0.2 - <0.050 <0.050 Polycyclic Aromatic Hydrocarbons Leachable Benzo(a)pyrene mg/L 0.001 <0.0010 <0.0010 <0.0010
Notes: <0.02 - Not detected above the reporting detection limits NV - No Value NA - Not Analyzed NI - Not Ignitable
References: 1 - Schedule 4 of Ontario Regulation 347 – General Waste Management: Leachate Quality Criteria. Soils producing leachate above these standards would be considered hazadous waste under the regulation APPENDIX E: Certificates of Analysis
Morrison Hershfield Limited (Ottawa) Date Received: 30-SEP-19 ATTN: Cindy Zhao Report Date: 08-OCT-19 15:27 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2356568 Project P.O. #: NOT SUBMITTED Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2356568 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 17 190441800 08-OCT-19 15:27 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2356568-1 BH1-SA4 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 9.98 0.10 % 01-OCT-19 Metals Antimony (Sb) 2.4 1.0 ug/g 04-OCT-19 *1 *1.3 *1.3 Arsenic (As) 2.4 1.0 ug/g 04-OCT-19 11 18 18 Barium (Ba) 101 1.0 ug/g 04-OCT-19 210 220 220 Beryllium (Be) <0.50 0.50 ug/g 04-OCT-19 2.5 2.5 2.5 Boron (B) 6.4 5.0 ug/g 04-OCT-19 36 36 36 Boron (B), Hot Water Ext. 0.32 0.10 ug/g 04-OCT-19 36 36 1.5 Cadmium (Cd) <0.50 0.50 ug/g 04-OCT-19 1 1.2 1.2 Chromium (Cr) 18.4 1.0 ug/g 04-OCT-19 67 70 70 Cobalt (Co) 5.9 1.0 ug/g 04-OCT-19 19 21 22 Copper (Cu) 15.3 1.0 ug/g 04-OCT-19 62 92 92 Lead (Pb) 66.8 1.0 ug/g 04-OCT-19 *45 120 120 Mercury (Hg) 0.0812 0.0050 ug/g 04-OCT-19 0.16 0.27 0.27 Molybdenum (Mo) <1.0 1.0 ug/g 04-OCT-19 2 2 2 Nickel (Ni) 12.5 1.0 ug/g 04-OCT-19 37 82 82 Selenium (Se) <1.0 1.0 ug/g 04-OCT-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-OCT-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-OCT-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-OCT-19 1.9 2.5 2.5 Vanadium (V) 30.8 1.0 ug/g 04-OCT-19 86 86 86 Zinc (Zn) 51.7 5.0 ug/g 04-OCT-19 290 290 290 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 02-OCT-19 0.66 0.66 0.66 Polycyclic Aromatic Hydrocarbons Acenaphthene 4.38 0.050 ug/g 04-OCT-19 *0.05 *0.072 *0.072 Acenaphthylene 0.313 0.050 ug/g 04-OCT-19 *0.093 *0.093 *0.093 Anthracene 11.4 0.050 ug/g 04-OCT-19 *0.05 *0.16 *0.22 Benzo(a)anthracene 16.3 0.050 ug/g 04-OCT-19 *0.095 *0.36 *0.36 Benzo(a)pyrene 13.8 0.050 ug/g 04-OCT-19 *0.05 *0.3 *0.3 Benzo(b)fluoranthene 17.9 0.050 ug/g 04-OCT-19 *0.3 *0.47 *0.47 Benzo(g,h,i)perylene 8.28 0.050 ug/g 04-OCT-19 *0.2 *0.68 *0.68 Benzo(k)fluoranthene 4.72 0.050 ug/g 04-OCT-19 *0.05 *0.48 *0.48 Chrysene 15.4 0.050 ug/g 04-OCT-19 *0.18 *2.8 *2.8 Dibenzo(ah)anthracene 2.26 0.050 ug/g 04-OCT-19 *0.1 *0.1 *0.1 Fluoranthene 37.7 0.050 ug/g 04-OCT-19 *0.24 *0.56 *0.69 Fluorene 6.58 0.050 ug/g 04-OCT-19 *0.05 *0.12 *0.19 Indeno(1,2,3-cd)pyrene 8.83 0.050 ug/g 04-OCT-19 *0.11 *0.23 *0.23 1+2-Methylnaphthalenes 1.56 0.042 ug/g 07-OCT-19 *0.05 *0.59 *0.59 1-Methylnaphthalene 1.01 0.030 ug/g 04-OCT-19 *0.05 *0.59 *0.59 2-Methylnaphthalene 0.554 0.030 ug/g 04-OCT-19 *0.05 0.59 0.59 Naphthalene 1.37 DLHC 0.033 ug/g 04-OCT-19 *0.05 *0.09 *0.09 Phenanthrene 35.9 0.046 ug/g 04-OCT-19 *0.19 *0.69 *0.69 Pyrene 29.9 0.050 ug/g 04-OCT-19 *0.19 *1 *1 Surrogate: 2-Fluorobiphenyl 99.8 50-140 % 04-OCT-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use L2356568 CONTD.... ANALYTICAL GUIDELINE REPORT Page 3 of 17 190441800 08-OCT-19 15:27 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2356568-1 BH1-SA4 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Surrogate: p-Terphenyl d14 85.7 50-140 % 04-OCT-19
L2356568-2 BH1-SA7 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 26.3 0.10 % 01-OCT-19 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Benzene <0.0068 0.0068 ug/g 07-OCT-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromoform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 07-OCT-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 07-OCT-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 07-OCT-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 07-OCT-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 07-OCT-19 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use L2356568 CONTD.... ANALYTICAL GUIDELINE REPORT Page 4 of 17 190441800 08-OCT-19 15:27 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2356568-2 BH1-SA7 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 07-OCT-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 07-OCT-19 m+p-Xylenes <0.030 0.030 ug/g 07-OCT-19 Xylenes (Total) <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 81.9 50-140 % 07-OCT-19 Surrogate: 1,4-Difluorobenzene 96.7 50-140 % 07-OCT-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 07-OCT-19 17 25 25 F2 (C10-C16) <10 10 ug/g 03-OCT-19 10 10 10 F3 (C16-C34) <50 50 ug/g 03-OCT-19 240 240 240 F4 (C34-C50) <50 50 ug/g 03-OCT-19 120 120 120 Chrom. to baseline at nC50 YES No Unit 03-OCT-19 Surrogate: 2-Bromobenzotrifluoride 87.8 60-140 % 03-OCT-19 Surrogate: 3,4-Dichlorotoluene 74.1 60-140 % 07-OCT-19
L2356568-3 BH2-SA3 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 33.4 0.10 % 01-OCT-19 Metals Antimony (Sb) 4.7 1.0 ug/g 04-OCT-19 *1 *1.3 *1.3 Arsenic (As) 16.9 1.0 ug/g 04-OCT-19 *11 18 18 Barium (Ba) 174 1.0 ug/g 04-OCT-19 210 220 220 Beryllium (Be) 0.55 0.50 ug/g 04-OCT-19 2.5 2.5 2.5 Boron (B) 9.2 5.0 ug/g 04-OCT-19 36 36 36 Boron (B), Hot Water Ext. 1.41 0.10 ug/g 04-OCT-19 36 36 1.5 Cadmium (Cd) 0.59 0.50 ug/g 04-OCT-19 1 1.2 1.2 Chromium (Cr) 25.0 1.0 ug/g 04-OCT-19 67 70 70 Cobalt (Co) 7.6 1.0 ug/g 04-OCT-19 19 21 22 Copper (Cu) 46.5 1.0 ug/g 04-OCT-19 62 92 92 Lead (Pb) 335 1.0 ug/g 04-OCT-19 *45 *120 *120 Mercury (Hg) 0.159 0.0050 ug/g 04-OCT-19 0.16 0.27 0.27 Molybdenum (Mo) 3.4 1.0 ug/g 04-OCT-19 *2 *2 *2 Nickel (Ni) 19.8 1.0 ug/g 04-OCT-19 37 82 82 Selenium (Se) 1.4 1.0 ug/g 04-OCT-19 *1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-OCT-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-OCT-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-OCT-19 1.9 2.5 2.5 Vanadium (V) 29.7 1.0 ug/g 04-OCT-19 86 86 86 Zinc (Zn) 138 5.0 ug/g 04-OCT-19 290 290 290 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 02-OCT-19 0.66 0.66 0.66 Polycyclic Aromatic Hydrocarbons
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use L2356568 CONTD.... ANALYTICAL GUIDELINE REPORT Page 5 of 17 190441800 08-OCT-19 15:27 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2356568-3 BH2-SA3 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Acenaphthene 0.069 0.050 ug/g 04-OCT-19 *0.05 0.072 0.072 Acenaphthylene <0.050 0.050 ug/g 04-OCT-19 0.093 0.093 0.093 Anthracene 0.138 0.050 ug/g 04-OCT-19 *0.05 0.16 0.22 Benzo(a)anthracene 0.309 0.050 ug/g 04-OCT-19 *0.095 0.36 0.36 Benzo(a)pyrene 0.243 0.050 ug/g 04-OCT-19 *0.05 0.3 0.3 Benzo(b)fluoranthene 0.358 0.050 ug/g 04-OCT-19 *0.3 0.47 0.47 Benzo(g,h,i)perylene 0.172 0.050 ug/g 04-OCT-19 0.2 0.68 0.68 Benzo(k)fluoranthene 0.113 0.050 ug/g 04-OCT-19 *0.05 0.48 0.48 Chrysene 0.371 0.050 ug/g 04-OCT-19 *0.18 2.8 2.8 Dibenzo(ah)anthracene <0.050 0.050 ug/g 04-OCT-19 0.1 0.1 0.1 Fluoranthene 0.626 0.050 ug/g 04-OCT-19 *0.24 *0.56 0.69 Fluorene 0.058 0.050 ug/g 04-OCT-19 *0.05 0.12 0.19 Indeno(1,2,3-cd)pyrene 0.157 R 0.050 ug/g 04-OCT-19 *0.11 0.23 0.23 1+2-Methylnaphthalenes 0.484 0.042 ug/g 07-OCT-19 *0.05 0.59 0.59 1-Methylnaphthalene 0.229 0.030 ug/g 04-OCT-19 *0.05 0.59 0.59 2-Methylnaphthalene 0.255 0.030 ug/g 04-OCT-19 *0.05 0.59 0.59 Naphthalene 0.202 0.013 ug/g 04-OCT-19 *0.05 *0.09 *0.09 Phenanthrene 0.617 0.046 ug/g 04-OCT-19 *0.19 0.69 0.69 Pyrene 0.507 0.050 ug/g 04-OCT-19 *0.19 1 1 Surrogate: 2-Fluorobiphenyl 91.5 50-140 % 04-OCT-19 Surrogate: p-Terphenyl d14 81.8 50-140 % 04-OCT-19
L2356568-4 BH2-SA7 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 12.6 0.10 % 01-OCT-19 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Benzene <0.0068 0.0068 ug/g 07-OCT-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromoform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2356568-4 BH2-SA7 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds cis-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 07-OCT-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 07-OCT-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 07-OCT-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 07-OCT-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 07-OCT-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 07-OCT-19 m+p-Xylenes <0.030 0.030 ug/g 07-OCT-19 Xylenes (Total) <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 88.3 50-140 % 07-OCT-19 Surrogate: 1,4-Difluorobenzene 106.2 50-140 % 07-OCT-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 07-OCT-19 17 25 25 F1-BTEX <5.0 5.0 ug/g 07-OCT-19 17 25 25 F2 (C10-C16) <10 10 ug/g 03-OCT-19 10 10 10 F3 (C16-C34) <50 50 ug/g 03-OCT-19 240 240 240 F4 (C34-C50) <50 50 ug/g 03-OCT-19 120 120 120 Total Hydrocarbons (C6-C50) <72 72 ug/g 07-OCT-19 Chrom. to baseline at nC50 YES No Unit 03-OCT-19 Surrogate: 2-Bromobenzotrifluoride 94.7 60-140 % 03-OCT-19 Surrogate: 3,4-Dichlorotoluene 82.1 60-140 % 07-OCT-19
L2356568-5 BH4-SA4 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 27.7 0.10 % 01-OCT-19 Metals Antimony (Sb) 1.3 1.0 ug/g 04-OCT-19 *1 1.3 1.3 Arsenic (As) 3.9 1.0 ug/g 04-OCT-19 11 18 18 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2356568-5 BH4-SA4 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Metals Barium (Ba) 106 1.0 ug/g 04-OCT-19 210 220 220 Beryllium (Be) <0.50 0.50 ug/g 04-OCT-19 2.5 2.5 2.5 Boron (B) 7.1 5.0 ug/g 04-OCT-19 36 36 36 Boron (B), Hot Water Ext. 0.85 0.10 ug/g 04-OCT-19 36 36 1.5 Cadmium (Cd) <0.50 0.50 ug/g 04-OCT-19 1 1.2 1.2 Chromium (Cr) 23.4 1.0 ug/g 04-OCT-19 67 70 70 Cobalt (Co) 6.8 1.0 ug/g 04-OCT-19 19 21 22 Copper (Cu) 162 1.0 ug/g 04-OCT-19 *62 *92 *92 Lead (Pb) 79.1 1.0 ug/g 04-OCT-19 *45 120 120 Mercury (Hg) 0.0726 0.0050 ug/g 04-OCT-19 0.16 0.27 0.27 Molybdenum (Mo) 1.0 1.0 ug/g 04-OCT-19 2 2 2 Nickel (Ni) 14.8 1.0 ug/g 04-OCT-19 37 82 82 Selenium (Se) <1.0 1.0 ug/g 04-OCT-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-OCT-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-OCT-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-OCT-19 1.9 2.5 2.5 Vanadium (V) 30.9 1.0 ug/g 04-OCT-19 86 86 86 Zinc (Zn) 117 5.0 ug/g 04-OCT-19 290 290 290 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 02-OCT-19 0.66 0.66 0.66 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 04-OCT-19 0.05 0.072 0.072 Acenaphthylene <0.050 0.050 ug/g 04-OCT-19 0.093 0.093 0.093 Anthracene 0.077 0.050 ug/g 04-OCT-19 *0.05 0.16 0.22 Benzo(a)anthracene 0.327 0.050 ug/g 04-OCT-19 *0.095 0.36 0.36 Benzo(a)pyrene 0.306 0.050 ug/g 04-OCT-19 *0.05 *0.3 *0.3 Benzo(b)fluoranthene 0.426 0.050 ug/g 04-OCT-19 *0.3 0.47 0.47 Benzo(g,h,i)perylene 0.211 0.050 ug/g 04-OCT-19 *0.2 0.68 0.68 Benzo(k)fluoranthene 0.128 0.050 ug/g 04-OCT-19 *0.05 0.48 0.48 Chrysene 0.348 0.050 ug/g 04-OCT-19 *0.18 2.8 2.8 Dibenzo(ah)anthracene 0.059 0.050 ug/g 04-OCT-19 0.1 0.1 0.1 Fluoranthene 0.662 0.050 ug/g 04-OCT-19 *0.24 *0.56 0.69 Fluorene <0.050 0.050 ug/g 04-OCT-19 0.05 0.12 0.19 Indeno(1,2,3-cd)pyrene 0.217 R 0.050 ug/g 04-OCT-19 *0.11 0.23 0.23 1+2-Methylnaphthalenes <0.042 0.042 ug/g 07-OCT-19 0.05 0.59 0.59 1-Methylnaphthalene <0.030 0.030 ug/g 04-OCT-19 0.05 0.59 0.59 2-Methylnaphthalene <0.030 0.030 ug/g 04-OCT-19 0.05 0.59 0.59 Naphthalene <0.013 0.013 ug/g 04-OCT-19 0.05 0.09 0.09 Phenanthrene 0.277 0.046 ug/g 04-OCT-19 *0.19 0.69 0.69 Pyrene 0.550 0.050 ug/g 04-OCT-19 *0.19 1 1 Surrogate: 2-Fluorobiphenyl 92.6 50-140 % 04-OCT-19 Surrogate: p-Terphenyl d14 86.0 50-140 % 04-OCT-19
L2356568-6 BH4-SA5 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use L2356568 CONTD.... ANALYTICAL GUIDELINE REPORT Page 8 of 17 190441800 08-OCT-19 15:27 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2356568-6 BH4-SA5 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 19.7 0.10 % 01-OCT-19 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Benzene <0.0068 0.0068 ug/g 07-OCT-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromoform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 07-OCT-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 07-OCT-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 07-OCT-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 07-OCT-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 07-OCT-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 07-OCT-19 m+p-Xylenes <0.030 0.030 ug/g 07-OCT-19 Xylenes (Total) <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 85.3 50-140 % 07-OCT-19 Surrogate: 1,4-Difluorobenzene 102.9 50-140 % 07-OCT-19 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2356568-6 BH4-SA5 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 07-OCT-19 17 25 25 F1-BTEX <5.0 5.0 ug/g 07-OCT-19 17 25 25 F2 (C10-C16) <10 10 ug/g 03-OCT-19 10 10 10 F3 (C16-C34) <50 50 ug/g 03-OCT-19 240 240 240 F4 (C34-C50) <50 50 ug/g 03-OCT-19 120 120 120 Total Hydrocarbons (C6-C50) <72 72 ug/g 07-OCT-19 Chrom. to baseline at nC50 YES No Unit 03-OCT-19 Surrogate: 2-Bromobenzotrifluoride 85.1 60-140 % 03-OCT-19 Surrogate: 3,4-Dichlorotoluene 74.2 60-140 % 07-OCT-19
L2356568-7 BH3-SA1 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 7.85 0.10 % 01-OCT-19 Metals Antimony (Sb) <1.0 1.0 ug/g 04-OCT-19 1 1.3 1.3 Arsenic (As) 3.8 1.0 ug/g 04-OCT-19 11 18 18 Barium (Ba) 207 1.0 ug/g 04-OCT-19 210 220 220 Beryllium (Be) <0.50 0.50 ug/g 04-OCT-19 2.5 2.5 2.5 Boron (B) 6.2 5.0 ug/g 04-OCT-19 36 36 36 Boron (B), Hot Water Ext. 0.17 0.10 ug/g 04-OCT-19 36 36 1.5 Cadmium (Cd) <0.50 0.50 ug/g 04-OCT-19 1 1.2 1.2 Chromium (Cr) 20.3 1.0 ug/g 04-OCT-19 67 70 70 Cobalt (Co) 7.3 1.0 ug/g 04-OCT-19 19 21 22 Copper (Cu) 19.5 1.0 ug/g 04-OCT-19 62 92 92 Lead (Pb) 38.3 1.0 ug/g 04-OCT-19 45 120 120 Mercury (Hg) 0.0442 0.0050 ug/g 04-OCT-19 0.16 0.27 0.27 Molybdenum (Mo) <1.0 1.0 ug/g 04-OCT-19 2 2 2 Nickel (Ni) 15.0 1.0 ug/g 04-OCT-19 37 82 82 Selenium (Se) <1.0 1.0 ug/g 04-OCT-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-OCT-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-OCT-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-OCT-19 1.9 2.5 2.5 Vanadium (V) 33.7 1.0 ug/g 04-OCT-19 86 86 86 Zinc (Zn) 69.2 5.0 ug/g 04-OCT-19 290 290 290 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 02-OCT-19 0.66 0.66 0.66 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 04-OCT-19 0.05 0.072 0.072 Acenaphthylene <0.050 0.050 ug/g 04-OCT-19 0.093 0.093 0.093 Anthracene 0.085 0.050 ug/g 04-OCT-19 *0.05 0.16 0.22 Benzo(a)anthracene 0.201 0.050 ug/g 04-OCT-19 *0.095 0.36 0.36 Benzo(a)pyrene 0.168 0.050 ug/g 04-OCT-19 *0.05 0.3 0.3 Benzo(b)fluoranthene 0.237 0.050 ug/g 04-OCT-19 0.3 0.47 0.47
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2356568-7 BH3-SA1 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Benzo(g,h,i)perylene 0.109 0.050 ug/g 04-OCT-19 0.2 0.68 0.68 Benzo(k)fluoranthene 0.071 0.050 ug/g 04-OCT-19 *0.05 0.48 0.48 Chrysene 0.201 0.050 ug/g 04-OCT-19 *0.18 2.8 2.8 Dibenzo(ah)anthracene <0.050 0.050 ug/g 04-OCT-19 0.1 0.1 0.1 Fluoranthene 0.451 0.050 ug/g 04-OCT-19 *0.24 0.56 0.69 Fluorene <0.050 0.050 ug/g 04-OCT-19 0.05 0.12 0.19 Indeno(1,2,3-cd)pyrene 0.111 0.050 ug/g 04-OCT-19 *0.11 0.23 0.23 1+2-Methylnaphthalenes 0.157 0.042 ug/g 07-OCT-19 *0.05 0.59 0.59 1-Methylnaphthalene 0.071 0.030 ug/g 04-OCT-19 *0.05 0.59 0.59 2-Methylnaphthalene 0.086 0.030 ug/g 04-OCT-19 *0.05 0.59 0.59 Naphthalene 0.053 0.013 ug/g 04-OCT-19 *0.05 0.09 0.09 Phenanthrene 0.343 0.046 ug/g 04-OCT-19 *0.19 0.69 0.69 Pyrene 0.377 0.050 ug/g 04-OCT-19 *0.19 1 1 Surrogate: 2-Fluorobiphenyl 91.1 50-140 % 04-OCT-19 Surrogate: p-Terphenyl d14 82.7 50-140 % 04-OCT-19
L2356568-8 BH3-SA8 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 11.0 0.10 % 01-OCT-19 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Benzene <0.0068 0.0068 ug/g 07-OCT-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromoform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 07-OCT-19 0.05 0.05 0.05 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2356568-8 BH3-SA8 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds Ethylbenzene <0.018 0.018 ug/g 07-OCT-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 07-OCT-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 07-OCT-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 07-OCT-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 07-OCT-19 m+p-Xylenes <0.030 0.030 ug/g 07-OCT-19 Xylenes (Total) <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 91.7 50-140 % 07-OCT-19 Surrogate: 1,4-Difluorobenzene 112.3 50-140 % 07-OCT-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 08-OCT-19 17 25 25 F1-BTEX <5.0 5.0 ug/g 08-OCT-19 17 25 25 F2 (C10-C16) <10 10 ug/g 03-OCT-19 10 10 10 F3 (C16-C34) <50 50 ug/g 03-OCT-19 240 240 240 F4 (C34-C50) <50 50 ug/g 03-OCT-19 120 120 120 Total Hydrocarbons (C6-C50) <72 72 ug/g 08-OCT-19 Chrom. to baseline at nC50 YES No Unit 03-OCT-19 Surrogate: 2-Bromobenzotrifluoride 86.3 60-140 % 03-OCT-19 Surrogate: 3,4-Dichlorotoluene 105.0 60-140 % 08-OCT-19
L2356568-9 BH2-SA31 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 29.2 0.10 % 01-OCT-19 Metals Antimony (Sb) 3.1 1.0 ug/g 04-OCT-19 *1 *1.3 *1.3 Arsenic (As) 12.2 1.0 ug/g 04-OCT-19 *11 18 18 Barium (Ba) 129 1.0 ug/g 04-OCT-19 210 220 220 Beryllium (Be) <0.50 0.50 ug/g 04-OCT-19 2.5 2.5 2.5 Boron (B) 6.1 5.0 ug/g 04-OCT-19 36 36 36 Boron (B), Hot Water Ext. 1.44 0.10 ug/g 04-OCT-19 36 36 1.5 Cadmium (Cd) <0.50 0.50 ug/g 04-OCT-19 1 1.2 1.2 Chromium (Cr) 17.2 1.0 ug/g 04-OCT-19 67 70 70 Cobalt (Co) 5.1 1.0 ug/g 04-OCT-19 19 21 22 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2356568-9 BH2-SA31 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Metals Copper (Cu) 33.1 1.0 ug/g 04-OCT-19 62 92 92 Lead (Pb) 199 1.0 ug/g 04-OCT-19 *45 *120 *120 Mercury (Hg) 0.139 0.0050 ug/g 04-OCT-19 0.16 0.27 0.27 Molybdenum (Mo) 2.4 1.0 ug/g 04-OCT-19 *2 *2 *2 Nickel (Ni) 14.7 1.0 ug/g 04-OCT-19 37 82 82 Selenium (Se) 1.0 1.0 ug/g 04-OCT-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-OCT-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-OCT-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-OCT-19 1.9 2.5 2.5 Vanadium (V) 20.6 1.0 ug/g 04-OCT-19 86 86 86 Zinc (Zn) 99.8 5.0 ug/g 04-OCT-19 290 290 290 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 02-OCT-19 0.66 0.66 0.66 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 04-OCT-19 0.05 0.072 0.072 Acenaphthylene <0.050 0.050 ug/g 04-OCT-19 0.093 0.093 0.093 Anthracene 0.052 0.050 ug/g 04-OCT-19 *0.05 0.16 0.22 Benzo(a)anthracene 0.171 0.050 ug/g 04-OCT-19 *0.095 0.36 0.36 Benzo(a)pyrene 0.120 0.050 ug/g 04-OCT-19 *0.05 0.3 0.3 Benzo(b)fluoranthene 0.207 0.050 ug/g 04-OCT-19 0.3 0.47 0.47 Benzo(g,h,i)perylene 0.095 0.050 ug/g 04-OCT-19 0.2 0.68 0.68 Benzo(k)fluoranthene 0.056 0.050 ug/g 04-OCT-19 *0.05 0.48 0.48 Chrysene 0.258 0.050 ug/g 04-OCT-19 *0.18 2.8 2.8 Dibenzo(ah)anthracene <0.050 0.050 ug/g 04-OCT-19 0.1 0.1 0.1 Fluoranthene 0.276 0.050 ug/g 04-OCT-19 *0.24 0.56 0.69 Fluorene <0.050 0.050 ug/g 04-OCT-19 0.05 0.12 0.19 Indeno(1,2,3-cd)pyrene 0.077 R 0.050 ug/g 04-OCT-19 0.11 0.23 0.23 1+2-Methylnaphthalenes 0.827 0.042 ug/g 07-OCT-19 *0.05 *0.59 *0.59 1-Methylnaphthalene 0.395 0.030 ug/g 04-OCT-19 *0.05 0.59 0.59 2-Methylnaphthalene 0.432 0.030 ug/g 04-OCT-19 *0.05 0.59 0.59 Naphthalene 0.319 0.013 ug/g 04-OCT-19 *0.05 *0.09 *0.09 Phenanthrene 0.399 0.046 ug/g 04-OCT-19 *0.19 0.69 0.69 Pyrene 0.239 0.050 ug/g 04-OCT-19 *0.19 1 1 Surrogate: 2-Fluorobiphenyl 90.6 50-140 % 04-OCT-19 Surrogate: p-Terphenyl d14 80.4 50-140 % 04-OCT-19
L2356568-10 BH1-SA21 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 30.9 0.10 % 01-OCT-19 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Benzene <0.0068 0.0068 ug/g 07-OCT-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use L2356568 CONTD.... ANALYTICAL GUIDELINE REPORT Page 13 of 17 190441800 08-OCT-19 15:27 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2356568-10 BH1-SA21 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds Bromoform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 07-OCT-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 07-OCT-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 07-OCT-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 07-OCT-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 07-OCT-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 07-OCT-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 07-OCT-19 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 07-OCT-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 07-OCT-19 m+p-Xylenes <0.030 0.030 ug/g 07-OCT-19 Xylenes (Total) <0.050 0.050 ug/g 07-OCT-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 79.9 50-140 % 07-OCT-19 Surrogate: 1,4-Difluorobenzene 95.7 50-140 % 07-OCT-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 07-OCT-19 17 25 25 17 25 25 F1 (C6-C10) <5.0 5.0 ug/g 07-OCT-19 17 25 25 17 25 25
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use L2356568 CONTD.... ANALYTICAL GUIDELINE REPORT Page 14 of 17 190441800 08-OCT-19 15:27 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2356568-10 BH1-SA21 Sampled By: CLIENT on 26-SEP-19 #1 #2 #3 Matrix: SOIL
Hydrocarbons F1-BTEX <5.0 5.0 ug/g 07-OCT-19 17 25 25 F2 (C10-C16) <10 10 ug/g 07-OCT-19 10 10 10 F3 (C16-C34) 58 50 ug/g 07-OCT-19 240 240 240 F4 (C34-C50) 58 50 ug/g 07-OCT-19 120 120 120 Total Hydrocarbons (C6-C50) 116 72 ug/g 07-OCT-19 Chrom. to baseline at nC50 YES No Unit 07-OCT-19 Surrogate: 2-Bromobenzotrifluoride 88.5 60-140 % 07-OCT-19 Surrogate: 3,4-Dichlorotoluene 68.9 60-140 % 07-OCT-19
Surrogate: 3,4-Dichlorotoluene 75.2 60-140 % 07-OCT-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use 190441800 L2356568 CONTD.... Page 15 of 17 08-OCT-19 15:27 (MT) Reference Information
Sample Parameter Qualifier key listed: Qualifier Description
R The ion abundance ratio(s) did not meet the acceptance criteria. Value is an estimated maximum. DLHC Detection Limit Raised: Dilution required due to high concentration of test analyte(s).
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
B-HWS-R511-WT Soil Boron-HWE-O.Reg 153/04 (July HW EXTR, EPA 6010B 2011)
A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). CR-CR6-IC-WT Soil Hexavalent Chromium in Soil SW846 3060A/7199
This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in a sulphuric acid solution.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
F1-F4-511-CALC-WT Soil F1-F4 Hydrocarbon Calculated CCME CWS-PHC, Pub #1310, Dec 2001-S Parameters
Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.
Hydrocarbon results are expressed on a dry weight basis.
In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines and the gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes has been subtracted from F1.
In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.
Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range: 1. All extraction and analysis holding times were met. 2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene. 3. Linearity of gasoline response within 15% throughout the calibration range.
Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges: 1. All extraction and analysis holding times were met. 2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average. 3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors. 4. Linearity of diesel or motor oil response within 15% throughout the calibration range. F1-HS-511-WT Soil F1-O.Reg 153/04 (July 2011) E3398/CCME TIER 1-HS
Fraction F1 is determined by extracting a soil or sediment sample as received with methanol, then analyzing by headspace-GC/FID.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). 190441800 L2356568 CONTD.... Page 16 of 17 08-OCT-19 15:27 (MT) Reference Information
F2-F4-511-WT Soil F2-F4-O.Reg 153/04 (July 2011) CCME Tier 1
Petroleum Hydrocarbons (F2-F4 fractions) are extracted from soil with 1:1 hexane:acetone using a rotary extractor. Extracts are treated with silica gel to remove polar organic interferences. F2, F3, & F4 are analyzed by GC-FID. F4G-sg is analyzed gravimetrically.
Notes: 1. F2 (C10-C16): Sum of all hydrocarbons that elute between nC10 and nC16. 2. F3 (C16-C34): Sum of all hydrocarbons that elute between nC16 and nC34. 3. F4 (C34-C50): Sum of all hydrocarbons that elute between nC34 and nC50. 4. F4G: Gravimetric Heavy Hydrocarbons 5. F4G-sg: Gravimetric Heavy Hydrocarbons (F4G) after silica gel treatment. 6. Where both F4 (C34-C50) and F4G-sg are reported for a sample, the larger of the two values is used for comparison against the relevant CCME guideline for F4. 7. F4G-sg cannot be added to the C6 to C50 hydrocarbon results to obtain an estimate of total extractable hydrocarbons. 8. This method is validated for use. 9. Data from analysis of validation and quality control samples is available upon request. 10. Reported results are expressed as milligrams per dry kilogram, unless otherwise indicated.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). HG-200.2-CVAA-WT Soil Mercury in Soil by CVAAS EPA 200.2/1631E (mod)
Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
MET-200.2-CCMS-WT Soil Metals in Soil by CRC ICPMS EPA 200.2/6020A (mod)
Soil/sediment is dried, disaggregated, and sieved (2 mm). For tests intended to support Ontario regulations, the <2mm fraction is ground to pass through a 0.355 mm sieve. Strong Acid Leachable Metals in the <2mm fraction are solubilized by heated digestion with nitric and hydrochloric acids. Instrumental analysis is by Collision / Reaction Cell ICPMS.
Limitations: This method is intended to liberate environmentally available metals. Silicate minerals are not solubilized. Some metals may be only partially recovered (matrix dependent), including Al, Ba, Be, Cr, S, Sr, Ti, Tl, V, W, and Zr. Elemental Sulfur may be poorly recovered by this method. Volatile forms of sulfur (e.g. sulfide, H2S) may be excluded if lost during sampling, storage, or digestion.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). METHYLNAPS-CALC-WT Soil ABN-Calculated Parameters SW846 8270 MOISTURE-WT Soil % Moisture CCME PHC in Soil - Tier 1 (mod) PAH-511-WT Soil PAH-O.Reg 153/04 (July 2011) SW846 3510/8270
A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Results for benzo(b) fluoranthene may include contributions from benzo(j)fluoranthene, if also present in the sample.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). VOC-1,3-DCP-CALC-WT Soil Regulation 153 VOCs SW8260B/SW8270C VOC-511-HS-WT Soil VOC-O.Reg 153/04 (July 2011) SW846 8260 (511)
Soil and sediment samples are extracted in methanol and analyzed by headspace-GC/MS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). XYLENES-SUM-CALC- Soil Sum of Xylene Isomer CALCULATION WT Concentrations
Total xylenes represents the sum of o-xylene and m&p-xylene.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: 190441800 L2356568 CONTD.... Page 17 of 17 08-OCT-19 15:27 (MT) Reference Information
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 1 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
B-HWS-R511-WT Soil Batch R4859159 WG3181516-4 DUP L2356568-1 Boron (B), Hot Water Ext. 0.32 0.34 ug/g 6.8 30 04-OCT-19 WG3181516-2 IRM WT SAR3 Boron (B), Hot Water Ext. 107.4 % 70-130 04-OCT-19 WG3181516-3 LCS Boron (B), Hot Water Ext. 101.6 % 70-130 04-OCT-19 WG3181516-1 MB Boron (B), Hot Water Ext. <0.10 ug/g 0.1 04-OCT-19
CR-CR6-IC-WT Soil Batch R4856129 WG3178015-4 CRM WT-SQC012 Chromium, Hexavalent 91.0 % 70-130 02-OCT-19 WG3178015-3 DUP L2356477-1 Chromium, Hexavalent <0.20 <0.20 RPD-NA ug/g N/A 35 02-OCT-19 WG3178015-2 LCS Chromium, Hexavalent 93.5 % 80-120 02-OCT-19 WG3178015-1 MB Chromium, Hexavalent <0.20 ug/g 0.2 02-OCT-19
F1-HS-511-WT Soil Batch R4860425 WG3181461-4 DUP WG3181461-3 F1 (C6-C10) <5.0 <5.0 RPD-NA ug/g N/A 30 07-OCT-19 WG3181461-2 LCS F1 (C6-C10) 91.0 % 80-120 07-OCT-19 WG3181461-1 MB F1 (C6-C10) <5.0 ug/g 5 07-OCT-19 Surrogate: 3,4-Dichlorotoluene 80.4 % 60-140 07-OCT-19 WG3181461-6 MS L2356568-6 F1 (C6-C10) 93.5 % 60-140 07-OCT-19
F2-F4-511-WT Soil Batch R4858914 WG3178836-3 DUP WG3178836-5 F2 (C10-C16) <10 <10 RPD-NA ug/g N/A 30 03-OCT-19 F3 (C16-C34) <50 <50 RPD-NA ug/g N/A 30 03-OCT-19 F4 (C34-C50) <50 <50 RPD-NA ug/g N/A 30 03-OCT-19 WG3178836-2 LCS F2 (C10-C16) 96.6 % 80-120 03-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 2 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
F2-F4-511-WT Soil Batch R4858914 WG3178836-2 LCS F3 (C16-C34) 80.4 % 80-120 03-OCT-19 F4 (C34-C50) 54.0 LCS-L % 80-120 03-OCT-19 WG3178836-1 MB F2 (C10-C16) <10 ug/g 10 03-OCT-19 F3 (C16-C34) <50 ug/g 50 03-OCT-19 F4 (C34-C50) <50 ug/g 50 03-OCT-19 Surrogate: 2-Bromobenzotrifluoride 85.4 % 60-140 03-OCT-19 WG3178836-4 MS WG3178836-5 F2 (C10-C16) 99.6 % 60-140 03-OCT-19 F3 (C16-C34) 104.0 % 60-140 03-OCT-19 F4 (C34-C50) 113.3 % 60-140 03-OCT-19
Batch R4860641 WG3181754-3 DUP WG3181754-5 F2 (C10-C16) <10 <10 RPD-NA ug/g N/A 30 04-OCT-19 F3 (C16-C34) <50 <50 RPD-NA ug/g N/A 30 04-OCT-19 F4 (C34-C50) <50 <50 RPD-NA ug/g N/A 30 04-OCT-19 WG3181754-2 LCS F2 (C10-C16) 98.9 % 80-120 04-OCT-19 F3 (C16-C34) 98.4 % 80-120 04-OCT-19 F4 (C34-C50) 103.6 % 80-120 04-OCT-19 WG3181754-1 MB F2 (C10-C16) <10 ug/g 10 04-OCT-19 F3 (C16-C34) <50 ug/g 50 04-OCT-19 F4 (C34-C50) <50 ug/g 50 04-OCT-19 Surrogate: 2-Bromobenzotrifluoride 77.9 % 60-140 04-OCT-19 WG3181754-4 MS WG3181754-5 F2 (C10-C16) 99.9 % 60-140 04-OCT-19 F3 (C16-C34) 100.6 % 60-140 04-OCT-19 F4 (C34-C50) 107.7 % 60-140 04-OCT-19
HG-200.2-CVAA-WT Soil Batch R4858956 WG3181500-2 CRM WT-CANMET-TILL2 Mercury (Hg) 111.1 % 70-130 04-OCT-19 WG3181500-6 DUP WG3181500-5 Mercury (Hg) 0.0383 0.0321 ug/g 18 40 04-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 3 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
HG-200.2-CVAA-WT Soil Batch R4858956 WG3181500-3 LCS Mercury (Hg) 115.0 % 80-120 04-OCT-19 WG3181500-1 MB Mercury (Hg) <0.0050 mg/kg 0.005 04-OCT-19
MET-200.2-CCMS-WT Soil Batch R4859054 WG3181500-2 CRM WT-CANMET-TILL2 Antimony (Sb) 120.3 % 70-130 04-OCT-19 Arsenic (As) 102.3 % 70-130 04-OCT-19 Barium (Ba) 97.6 % 70-130 04-OCT-19 Beryllium (Be) 96.9 % 70-130 04-OCT-19 Boron (B) 3.4 mg/kg 0-8.6 04-OCT-19 Cadmium (Cd) 98.7 % 70-130 04-OCT-19 Chromium (Cr) 101.1 % 70-130 04-OCT-19 Cobalt (Co) 99.0 % 70-130 04-OCT-19 Copper (Cu) 98.1 % 70-130 04-OCT-19 Lead (Pb) 106.7 % 70-130 04-OCT-19 Molybdenum (Mo) 105.9 % 70-130 04-OCT-19 Nickel (Ni) 100.8 % 70-130 04-OCT-19 Selenium (Se) 0.37 mg/kg 0.15-0.55 04-OCT-19 Silver (Ag) 103.6 % 70-130 04-OCT-19 Thallium (Tl) 105.8 % 70-130 04-OCT-19 Uranium (U) 105.1 % 70-130 04-OCT-19 Vanadium (V) 100.5 % 70-130 04-OCT-19 Zinc (Zn) 95.8 % 70-130 04-OCT-19 WG3181500-6 DUP WG3181500-5 Antimony (Sb) 0.13 0.15 ug/g 9.2 30 04-OCT-19 Arsenic (As) 2.86 3.13 ug/g 9.0 30 04-OCT-19 Barium (Ba) 65.2 70.1 ug/g 7.3 40 04-OCT-19 Beryllium (Be) 0.49 0.54 ug/g 8.9 30 04-OCT-19 Boron (B) 6.7 6.9 ug/g 2.8 30 04-OCT-19 Cadmium (Cd) 0.237 0.254 ug/g 7.0 30 04-OCT-19 Chromium (Cr) 18.5 19.6 ug/g 5.6 30 04-OCT-19 Cobalt (Co) 5.66 6.16 ug/g 8.3 30 04-OCT-19 Copper (Cu) 10.4 11.4 ug/g 8.5 30 04-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 4 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R4859054 WG3181500-6 DUP WG3181500-5 Lead (Pb) 12.0 13.6 ug/g 13 40 04-OCT-19 Molybdenum (Mo) 0.30 0.34 ug/g 9.5 40 04-OCT-19 Nickel (Ni) 11.0 11.8 ug/g 7.1 30 04-OCT-19 Selenium (Se) 0.28 0.31 ug/g 12 30 04-OCT-19 Silver (Ag) <0.10 <0.10 RPD-NA ug/g N/A 40 04-OCT-19 Thallium (Tl) 0.120 0.128 ug/g 6.1 30 04-OCT-19 Uranium (U) 0.512 0.559 ug/g 8.7 30 04-OCT-19 Vanadium (V) 33.2 35.2 ug/g 6.1 30 04-OCT-19 Zinc (Zn) 42.8 46.7 ug/g 8.8 30 04-OCT-19 WG3181500-4 LCS Antimony (Sb) 109.5 % 80-120 04-OCT-19 Arsenic (As) 100.9 % 80-120 04-OCT-19 Barium (Ba) 104.5 % 80-120 04-OCT-19 Beryllium (Be) 102.1 % 80-120 04-OCT-19 Boron (B) 98.5 % 80-120 04-OCT-19 Cadmium (Cd) 100.3 % 80-120 04-OCT-19 Chromium (Cr) 102.3 % 80-120 04-OCT-19 Cobalt (Co) 99.4 % 80-120 04-OCT-19 Copper (Cu) 97.5 % 80-120 04-OCT-19 Lead (Pb) 104.5 % 80-120 04-OCT-19 Molybdenum (Mo) 106.6 % 80-120 04-OCT-19 Nickel (Ni) 99.5 % 80-120 04-OCT-19 Selenium (Se) 102.3 % 80-120 04-OCT-19 Silver (Ag) 107.2 % 80-120 04-OCT-19 Thallium (Tl) 102.1 % 80-120 04-OCT-19 Uranium (U) 108.0 % 80-120 04-OCT-19 Vanadium (V) 103.8 % 80-120 04-OCT-19 Zinc (Zn) 95.9 % 80-120 04-OCT-19 WG3181500-1 MB Antimony (Sb) <0.10 mg/kg 0.1 04-OCT-19 Arsenic (As) <0.10 mg/kg 0.1 04-OCT-19 Barium (Ba) <0.50 mg/kg 0.5 04-OCT-19 Beryllium (Be) <0.10 mg/kg 0.1 04-OCT-19 Boron (B) <5.0 mg/kg 5 04-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 5 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R4859054 WG3181500-1 MB Cadmium (Cd) <0.020 mg/kg 0.02 04-OCT-19 Chromium (Cr) <0.50 mg/kg 0.5 04-OCT-19 Cobalt (Co) <0.10 mg/kg 0.1 04-OCT-19 Copper (Cu) <0.50 mg/kg 0.5 04-OCT-19 Lead (Pb) <0.50 mg/kg 0.5 04-OCT-19 Molybdenum (Mo) <0.10 mg/kg 0.1 04-OCT-19 Nickel (Ni) <0.50 mg/kg 0.5 04-OCT-19 Selenium (Se) <0.20 mg/kg 0.2 04-OCT-19 Silver (Ag) <0.10 mg/kg 0.1 04-OCT-19 Thallium (Tl) <0.050 mg/kg 0.05 04-OCT-19 Uranium (U) <0.050 mg/kg 0.05 04-OCT-19 Vanadium (V) <0.20 mg/kg 0.2 04-OCT-19 Zinc (Zn) <2.0 mg/kg 2 04-OCT-19
MOISTURE-WT Soil Batch R4851551 WG3177952-3 DUP L2355736-1 % Moisture 8.39 7.82 % 6.9 20 01-OCT-19 WG3177952-2 LCS % Moisture 101.7 % 90-110 01-OCT-19 WG3177952-1 MB % Moisture <0.10 % 0.1 01-OCT-19
PAH-511-WT Soil Batch R4859572 WG3177695-3 DUP WG3177695-5 1-Methylnaphthalene <0.030 0.041 RPD-NA ug/g N/A 40 04-OCT-19 2-Methylnaphthalene 0.032 0.043 ug/g 28 40 04-OCT-19 Acenaphthene <0.050 0.058 RPD-NA ug/g N/A 40 04-OCT-19 Acenaphthylene <0.050 <0.050 RPD-NA ug/g N/A 40 04-OCT-19 Anthracene 0.145 0.196 ug/g 30 40 04-OCT-19 Benzo(a)anthracene 0.400 0.487 ug/g 20 40 04-OCT-19 Benzo(a)pyrene 0.357 0.419 ug/g 16 40 04-OCT-19 Benzo(b)fluoranthene 0.525 0.625 ug/g 17 40 04-OCT-19 Benzo(g,h,i)perylene 0.238 0.271 ug/g 13 40 04-OCT-19 Benzo(k)fluoranthene 0.161 0.187 ug/g 15 40 04-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 6 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R4859572 WG3177695-3 DUP WG3177695-5 Chrysene 0.427 0.504 ug/g 16 40 04-OCT-19 Dibenzo(ah)anthracene 0.067 0.079 ug/g 15 40 04-OCT-19 Fluoranthene 0.895 1.13 ug/g 23 40 04-OCT-19 Fluorene 0.068 0.076 ug/g 11 40 04-OCT-19 Indeno(1,2,3-cd)pyrene 0.245 0.283 ug/g 14 40 04-OCT-19 Naphthalene 0.069 0.081 ug/g 16 40 04-OCT-19 Phenanthrene 0.621 0.873 ug/g 34 40 04-OCT-19 Pyrene 0.704 0.873 ug/g 21 40 04-OCT-19 WG3177695-2 LCS 1-Methylnaphthalene 91.0 % 50-140 04-OCT-19 2-Methylnaphthalene 86.4 % 50-140 04-OCT-19 Acenaphthene 93.1 % 50-140 04-OCT-19 Acenaphthylene 95.3 % 50-140 04-OCT-19 Anthracene 90.7 % 50-140 04-OCT-19 Benzo(a)anthracene 91.9 % 50-140 04-OCT-19 Benzo(a)pyrene 88.3 % 50-140 04-OCT-19 Benzo(b)fluoranthene 92.0 % 50-140 04-OCT-19 Benzo(g,h,i)perylene 82.3 % 50-140 04-OCT-19 Benzo(k)fluoranthene 86.9 % 50-140 04-OCT-19 Chrysene 98.7 % 50-140 04-OCT-19 Dibenzo(ah)anthracene 86.2 % 50-140 04-OCT-19 Fluoranthene 87.9 % 50-140 04-OCT-19 Fluorene 91.9 % 50-140 04-OCT-19 Indeno(1,2,3-cd)pyrene 89.0 % 50-140 04-OCT-19 Naphthalene 89.6 % 50-140 04-OCT-19 Phenanthrene 89.3 % 50-140 04-OCT-19 Pyrene 88.1 % 50-140 04-OCT-19 WG3177695-1 MB 1-Methylnaphthalene <0.030 ug/g 0.03 04-OCT-19 2-Methylnaphthalene <0.030 ug/g 0.03 04-OCT-19 Acenaphthene <0.050 ug/g 0.05 04-OCT-19 Acenaphthylene <0.050 ug/g 0.05 04-OCT-19 Anthracene <0.050 ug/g 0.05 04-OCT-19 Benzo(a)anthracene <0.050 ug/g 0.05 04-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 7 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R4859572 WG3177695-1 MB Benzo(a)pyrene <0.050 ug/g 0.05 04-OCT-19 Benzo(b)fluoranthene <0.050 ug/g 0.05 04-OCT-19 Benzo(g,h,i)perylene <0.050 ug/g 0.05 04-OCT-19 Benzo(k)fluoranthene <0.050 ug/g 0.05 04-OCT-19 Chrysene <0.050 ug/g 0.05 04-OCT-19 Dibenzo(ah)anthracene <0.050 ug/g 0.05 04-OCT-19 Fluoranthene <0.050 ug/g 0.05 04-OCT-19 Fluorene <0.050 ug/g 0.05 04-OCT-19 Indeno(1,2,3-cd)pyrene <0.050 ug/g 0.05 04-OCT-19 Naphthalene <0.013 ug/g 0.013 04-OCT-19 Phenanthrene <0.046 ug/g 0.046 04-OCT-19 Pyrene <0.050 ug/g 0.05 04-OCT-19 Surrogate: 2-Fluorobiphenyl 90.2 % 50-140 04-OCT-19 Surrogate: p-Terphenyl d14 82.9 % 50-140 04-OCT-19 WG3177695-4 MS WG3177695-5 1-Methylnaphthalene 109.7 % 50-140 04-OCT-19 2-Methylnaphthalene 111.1 % 50-140 04-OCT-19 Acenaphthene 120.3 % 50-140 04-OCT-19 Acenaphthylene 99.2 % 50-140 04-OCT-19 Anthracene 150.1 E % 50-140 04-OCT-19 Benzo(a)anthracene 181.9 E % 50-140 04-OCT-19 Benzo(a)pyrene 155.7 E % 50-140 04-OCT-19 Benzo(b)fluoranthene 198.6 E % 50-140 04-OCT-19 Benzo(g,h,i)perylene 122.7 % 50-140 04-OCT-19 Benzo(k)fluoranthene 106.4 % 50-140 04-OCT-19 Chrysene 178.4 E % 50-140 04-OCT-19 Dibenzo(ah)anthracene 101.7 % 50-140 04-OCT-19 Fluoranthene N/A MS-B % - 04-OCT-19 Fluorene 131.0 % 50-140 04-OCT-19 Indeno(1,2,3-cd)pyrene 136.4 % 50-140 04-OCT-19 Naphthalene 155.8 E % 50-140 04-OCT-19 Phenanthrene 373.0 E % 50-140 04-OCT-19 Pyrene 252.3 E % 50-140 04-OCT-19
VOC-511-HS-WT Soil Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 8 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4860425 WG3181461-4 DUP WG3181461-3 1,1,1,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,1,2,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,1,1-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,1,2-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,1-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,1-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,2-Dibromoethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,2-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,2-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,2-Dichloropropane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,3-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 1,4-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Acetone <0.50 <0.50 RPD-NA ug/g N/A 40 07-OCT-19 Benzene <0.0068 <0.0068 RPD-NA ug/g N/A 40 07-OCT-19 Bromodichloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Bromoform <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Bromomethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Carbon tetrachloride <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Chlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Chloroform <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 cis-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 cis-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 07-OCT-19 Dibromochloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Dichlorodifluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Ethylbenzene <0.018 <0.018 RPD-NA ug/g N/A 40 07-OCT-19 n-Hexane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Methylene Chloride <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 MTBE <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 m+p-Xylenes <0.030 <0.030 RPD-NA ug/g N/A 40 07-OCT-19 Methyl Ethyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 07-OCT-19 Methyl Isobutyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 07-OCT-19 o-Xylene <0.020 <0.020 RPD-NA ug/g N/A 40 07-OCT-19 Styrene <0.050 <0.050 ug/g 07-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 9 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4860425 WG3181461-4 DUP WG3181461-3 Styrene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Tetrachloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Toluene <0.080 <0.080 RPD-NA ug/g N/A 40 07-OCT-19 trans-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 trans-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 07-OCT-19 Trichloroethylene <0.010 <0.010 RPD-NA ug/g N/A 40 07-OCT-19 Trichlorofluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 07-OCT-19 Vinyl chloride <0.020 <0.020 RPD-NA ug/g N/A 40 07-OCT-19 WG3181461-2 LCS 1,1,1,2-Tetrachloroethane 107.8 % 60-130 07-OCT-19 1,1,2,2-Tetrachloroethane 104.1 % 60-130 07-OCT-19 1,1,1-Trichloroethane 106.5 % 60-130 07-OCT-19 1,1,2-Trichloroethane 106.9 % 60-130 07-OCT-19 1,1-Dichloroethane 109.3 % 60-130 07-OCT-19 1,1-Dichloroethylene 101.7 % 60-130 07-OCT-19 1,2-Dibromoethane 106.2 % 70-130 07-OCT-19 1,2-Dichlorobenzene 107.8 % 70-130 07-OCT-19 1,2-Dichloroethane 107.5 % 60-130 07-OCT-19 1,2-Dichloropropane 107.5 % 70-130 07-OCT-19 1,3-Dichlorobenzene 107.5 % 70-130 07-OCT-19 1,4-Dichlorobenzene 107.0 % 70-130 07-OCT-19 Acetone 107.9 % 60-140 07-OCT-19 Benzene 109.7 % 70-130 07-OCT-19 Bromodichloromethane 107.7 % 50-140 07-OCT-19 Bromoform 108.0 % 70-130 07-OCT-19 Bromomethane 94.3 % 50-140 07-OCT-19 Carbon tetrachloride 105.2 % 70-130 07-OCT-19 Chlorobenzene 106.4 % 70-130 07-OCT-19 Chloroform 106.8 % 70-130 07-OCT-19 cis-1,2-Dichloroethylene 103.7 % 70-130 07-OCT-19 cis-1,3-Dichloropropene 99.9 % 70-130 07-OCT-19 Dibromochloromethane 105.7 % 60-130 07-OCT-19 Dichlorodifluoromethane 75.9 % 50-140 07-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 10 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4860425 WG3181461-2 LCS Ethylbenzene 104.8 % 70-130 07-OCT-19 n-Hexane 94.9 % 70-130 07-OCT-19 Methylene Chloride 104.5 % 70-130 07-OCT-19 MTBE 106.4 % 70-130 07-OCT-19 m+p-Xylenes 105.1 % 70-130 07-OCT-19 Methyl Ethyl Ketone 99.5 % 60-140 07-OCT-19 Methyl Isobutyl Ketone 93.8 % 60-140 07-OCT-19 o-Xylene 104.8 % 70-130 07-OCT-19 Styrene 106.3 % 70-130 07-OCT-19 Tetrachloroethylene 104.5 % 60-130 07-OCT-19 Toluene 107.8 % 70-130 07-OCT-19 trans-1,2-Dichloroethylene 103.6 % 60-130 07-OCT-19 trans-1,3-Dichloropropene 107.8 % 70-130 07-OCT-19 Trichloroethylene 106.6 % 60-130 07-OCT-19 Trichlorofluoromethane 101.4 % 50-140 07-OCT-19 Vinyl chloride 106.4 % 60-140 07-OCT-19 WG3181461-1 MB 1,1,1,2-Tetrachloroethane <0.050 ug/g 0.05 07-OCT-19 1,1,2,2-Tetrachloroethane <0.050 ug/g 0.05 07-OCT-19 1,1,1-Trichloroethane <0.050 ug/g 0.05 07-OCT-19 1,1,2-Trichloroethane <0.050 ug/g 0.05 07-OCT-19 1,1-Dichloroethane <0.050 ug/g 0.05 07-OCT-19 1,1-Dichloroethylene <0.050 ug/g 0.05 07-OCT-19 1,2-Dibromoethane <0.050 ug/g 0.05 07-OCT-19 1,2-Dichlorobenzene <0.050 ug/g 0.05 07-OCT-19 1,2-Dichloroethane <0.050 ug/g 0.05 07-OCT-19 1,2-Dichloropropane <0.050 ug/g 0.05 07-OCT-19 1,3-Dichlorobenzene <0.050 ug/g 0.05 07-OCT-19 1,4-Dichlorobenzene <0.050 ug/g 0.05 07-OCT-19 Acetone <0.50 ug/g 0.5 07-OCT-19 Benzene <0.0068 ug/g 0.0068 07-OCT-19 Bromodichloromethane <0.050 ug/g 0.05 07-OCT-19 Bromoform <0.050 ug/g 0.05 07-OCT-19 Bromomethane <0.050 ug/g 0.05 07-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 11 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4860425 WG3181461-1 MB Carbon tetrachloride <0.050 ug/g 0.05 07-OCT-19 Chlorobenzene <0.050 ug/g 0.05 07-OCT-19 Chloroform <0.050 ug/g 0.05 07-OCT-19 cis-1,2-Dichloroethylene <0.050 ug/g 0.05 07-OCT-19 cis-1,3-Dichloropropene <0.030 ug/g 0.03 07-OCT-19 Dibromochloromethane <0.050 ug/g 0.05 07-OCT-19 Dichlorodifluoromethane <0.050 ug/g 0.05 07-OCT-19 Ethylbenzene <0.018 ug/g 0.018 07-OCT-19 n-Hexane <0.050 ug/g 0.05 07-OCT-19 Methylene Chloride <0.050 ug/g 0.05 07-OCT-19 MTBE <0.050 ug/g 0.05 07-OCT-19 m+p-Xylenes <0.030 ug/g 0.03 07-OCT-19 Methyl Ethyl Ketone <0.50 ug/g 0.5 07-OCT-19 Methyl Isobutyl Ketone <0.50 ug/g 0.5 07-OCT-19 o-Xylene <0.020 ug/g 0.02 07-OCT-19 Styrene <0.050 ug/g 0.05 07-OCT-19 Tetrachloroethylene <0.050 ug/g 0.05 07-OCT-19 Toluene <0.080 ug/g 0.08 07-OCT-19 trans-1,2-Dichloroethylene <0.050 ug/g 0.05 07-OCT-19 trans-1,3-Dichloropropene <0.030 ug/g 0.03 07-OCT-19 Trichloroethylene <0.010 ug/g 0.01 07-OCT-19 Trichlorofluoromethane <0.050 ug/g 0.05 07-OCT-19 Vinyl chloride <0.020 ug/g 0.02 07-OCT-19 Surrogate: 1,4-Difluorobenzene 108.2 % 50-140 07-OCT-19 Surrogate: 4-Bromofluorobenzene 90.7 % 50-140 07-OCT-19 WG3181461-5 MS L2356568-2 1,1,1,2-Tetrachloroethane 107.4 % 50-140 07-OCT-19 1,1,2,2-Tetrachloroethane 115.8 % 50-140 07-OCT-19 1,1,1-Trichloroethane 106.1 % 50-140 07-OCT-19 1,1,2-Trichloroethane 108.1 % 50-140 07-OCT-19 1,1-Dichloroethane 104.7 % 50-140 07-OCT-19 1,1-Dichloroethylene 100.1 % 50-140 07-OCT-19 1,2-Dibromoethane 107.8 % 50-140 07-OCT-19 1,2-Dichlorobenzene 104.8 % 50-140 07-OCT-19 Quality Control Report
Workorder: L2356568 Report Date: 08-OCT-19 Page 12 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4860425 WG3181461-5 MS L2356568-2 1,2-Dichloroethane 108.3 % 50-140 07-OCT-19 1,2-Dichloropropane 108.8 % 50-140 07-OCT-19 1,3-Dichlorobenzene 102.4 % 50-140 07-OCT-19 1,4-Dichlorobenzene 103.2 % 50-140 07-OCT-19 Acetone 147.9 MES % 50-140 07-OCT-19 Benzene 108.2 % 50-140 07-OCT-19 Bromodichloromethane 109.3 % 50-140 07-OCT-19 Bromoform 110.1 % 50-140 07-OCT-19 Bromomethane 92.2 % 50-140 07-OCT-19 Carbon tetrachloride 104.0 % 50-140 07-OCT-19 Chlorobenzene 104.8 % 50-140 07-OCT-19 Chloroform 107.0 % 50-140 07-OCT-19 cis-1,2-Dichloroethylene 102.6 % 50-140 07-OCT-19 cis-1,3-Dichloropropene 98.0 % 50-140 07-OCT-19 Dibromochloromethane 106.1 % 50-140 07-OCT-19 Dichlorodifluoromethane 69.7 % 50-140 07-OCT-19 Ethylbenzene 101.2 % 50-140 07-OCT-19 n-Hexane 92.5 % 50-140 07-OCT-19 Methylene Chloride 104.0 % 50-140 07-OCT-19 MTBE 105.4 % 50-140 07-OCT-19 m+p-Xylenes 101.9 % 50-140 07-OCT-19 Methyl Ethyl Ketone 88.0 % 50-140 07-OCT-19 Methyl Isobutyl Ketone 103.1 % 50-140 07-OCT-19 o-Xylene 101.1 % 50-140 07-OCT-19 Styrene 99.5 % 50-140 07-OCT-19 Tetrachloroethylene 101.5 % 50-140 07-OCT-19 Toluene 106.0 % 50-140 07-OCT-19 trans-1,2-Dichloroethylene 101.8 % 50-140 07-OCT-19 trans-1,3-Dichloropropene 103.6 % 50-140 07-OCT-19 Trichloroethylene 106.5 % 50-140 07-OCT-19 Trichlorofluoromethane 100.5 % 50-140 07-OCT-19 Vinyl chloride 104.1 % 50-140 07-OCT-19 Quality Control Report Workorder: L2356568 Report Date: 08-OCT-19
Client: Morrison Hershfield Limited (Ottawa) Page 13 of 13 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description E Matrix Spike recovery outside ALS DQO due to heterogeneous analyte background in sample. LCS-L Lab Control Sample recovery was below ALS DQO. Reference Material and/or Matrix Spike results were acceptable. Non-detected sample results are considered reliable. Other results, if reported, have been qualified. MES Data Quality Objective was marginally exceeded (by < 10% absolute) for < 10% of analytes in a Multi-Element Scan / Multi-Parameter Scan (considered acceptable as per OMOE & CCME). MS-B Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order. ALS Sample ID: L2356568-2 Client Sample ID: BH1-SA7 500
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Printed on 10/4/2019 2:56:48 PM ALS Sample ID: L2356568-4 Client Sample ID: BH2-SA7 500
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Printed on 10/4/2019 2:56:50 PM ALS Sample ID: L2356568-8 Client Sample ID: BH3-SA8 500
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Printed on 10/4/2019 3:02:22 PM ALS Sample ID: L2356568-10 Client Sample ID: BH1-SA21 500
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Printed on 10/7/2019 4:29:22 PM
Morrison Hershfield Limited (Ottawa) Date Received: 30-SEP-19 ATTN: Cindy Zhao Report Date: 07-OCT-19 13:44 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2356576 Project P.O. #: NOT SUBMITTED Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2356576 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 3 190441800 07-OCT-19 13:44 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2356576-1 TCLP-HK Sampled By: CLIENT on 26-SEP-19 #1 Matrix: SOIL
Sample Preparation Initial pH 9.09 0.10 pH units 03-OCT-19 Final pH 6.25 0.10 pH units 03-OCT-19 TCLP Extractables Acenaphthene <0.0050 0.0050 mg/L 07-OCT-19 Acenaphthylene <0.0050 0.0050 mg/L 07-OCT-19 Anthracene <0.0050 0.0050 mg/L 07-OCT-19 Benzo(a)anthracene <0.0050 0.0050 mg/L 07-OCT-19 Benzo(a)pyrene <0.0010 0.0010 mg/L 07-OCT-19 0.001 Benzo(b)fluoranthene <0.0050 0.0050 mg/L 07-OCT-19 Benzo(g,h,i)perylene <0.0050 0.0050 mg/L 07-OCT-19 TCLP Metals Arsenic (As) <0.050 0.050 mg/L 03-OCT-19 2.5 Barium (Ba) 1.10 0.50 mg/L 03-OCT-19 100 Boron (B) <2.5 2.5 mg/L 03-OCT-19 500 Cadmium (Cd) <0.0050 0.0050 mg/L 03-OCT-19 0.5 Chromium (Cr) <0.050 0.050 mg/L 03-OCT-19 5.0 Lead (Pb) <0.050 0.050 mg/L 03-OCT-19 5.0 Mercury (Hg) <0.00010 0.00010 mg/L 03-OCT-19 0.1 Selenium (Se) <0.025 0.025 mg/L 03-OCT-19 1.0 Silver (Ag) <0.0050 0.0050 mg/L 03-OCT-19 5.0 Uranium (U) <0.25 0.25 mg/L 03-OCT-19 10 Polycyclic Aromatic Hydrocarbons Benzo(k)fluoranthene <0.0050 0.0050 mg/L 07-OCT-19 Chrysene <0.0050 0.0050 mg/L 07-OCT-19 Dibenzo(ah)anthracene <0.0050 0.0050 mg/L 07-OCT-19 Fluoranthene <0.0050 0.0050 mg/L 07-OCT-19 Fluorene <0.0050 0.0050 mg/L 07-OCT-19 Indeno(1,2,3-cd)pyrene <0.0050 0.0050 mg/L 07-OCT-19 Naphthalene <0.0050 0.0050 mg/L 07-OCT-19 Phenanthrene <0.0050 0.0050 mg/L 07-OCT-19 Pyrene <0.0050 0.0050 mg/L 07-OCT-19 Quinoline <0.0050 0.0050 mg/L 07-OCT-19 Surrogate: d10-Acenaphthene 94.9 50-150 % 07-OCT-19 Surrogate: d12-Chrysene 100.2 50-150 % 07-OCT-19 Surrogate: d8-Naphthalene 93.9 50-150 % 07-OCT-19 Surrogate: d10-Phenanthrene 97.3 50-150 % 07-OCT-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Ministry of the Environment, General Waste Control Regulation No. 347/90 #1: Ontario Ministry of the Environment, General Waste Control Regulation No. 347/90 190441800 L2356576 CONTD.... Page 3 of 3 07-OCT-19 13:44 (MT) Reference Information
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
HG-TCLP-WT Waste Mercury (CVAA) for O.Reg 347 EPA 1631E
This analysis is carried out in accordance with the extraction procedure outlined in "Test Methods for Evaluating Solid Waste - Physical/Chemical Methods Volume 1C" SW-846 EPA Method 1311, published by the United States Environmental Protection Agency (EPA). In summary, the sample is extracted at a 20:1 liquid to solids ratio for 16 to 20 hours using either extraction fluid #1 (glacial acetic acid, water and sodium hydroxide) or extraction fluid #2 (glacial acetic acid), depending on the pH of the original sample. The extract is then filtered through a 0.6 to 0.8 micron glass fibre filter and analysed using atomic absorption spectrophotometry (EPA 1631E). LEACH-TCLP-WT Waste Leachate Procedure for Reg 347 EPA 1311
Inorganic and Semi-Volatile Organic contaminants are leached from waste samples in strict accordance with US EPA Method 1311, "Toxicity Characteristic Leaching Procedure" (TCLP). Test results are reported in leachate concentration units (normally mg/L). MET-TCLP-WT Waste O.Reg 347 TCLP Leachable EPA 6020B Metals
This analysis is carried out in accordance with the extraction procedure outlined in "Test Methods for Evaluating Solid Waste - Physical/Chemical Methods Volume 1C" SW-846 EPA Method 1311, published by the United States Environmental Protection Agency (EPA). In summary, the sample is extracted at a 20:1 liquid to solids ratio for 16 to 20 hours using either extraction fluid #1 (glacial acetic acid, water and sodium hydroxide) or extraction fluid #2 (glacial acetic acid), depending on the pH of the original sample. The extract is then filtered through a 0.6 to 0.8 micron glass fibre filter. Instrumental analysis of the digested extract is by collision cell inductively coupled plasma - mass spectrometry (modifed from EPA Method 6020B). PAH-TCLP-WT Waste PAH for O. Reg 347 SW846 8270 (PAH)
Samples are leached according to TCLP protocol and then the aqueous leachate is extracted and the resulting extracts are analyzed on GC/MSD. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA
GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2356576 Report Date: 07-OCT-19 Page 1 of 6
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
HG-TCLP-WT Waste Batch R4858141 WG3180611-3 DUP L2357661-1 Mercury (Hg) <0.00010 <0.00010 RPD-NA mg/L N/A 50 03-OCT-19 WG3180611-2 LCS Mercury (Hg) 104.0 % 70-130 03-OCT-19 WG3180611-1 MB Mercury (Hg) <0.00010 mg/L 0.0001 03-OCT-19 WG3180611-4 MS L2357661-1 Mercury (Hg) 108.4 % 50-140 03-OCT-19
MET-TCLP-WT Waste Batch R4858292 WG3180627-4 DUP WG3180627-3 Silver (Ag) <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Arsenic (As) <0.050 <0.050 RPD-NA mg/L N/A 50 03-OCT-19 Boron (B) <2.5 <2.5 RPD-NA mg/L N/A 50 03-OCT-19 Barium (Ba) 0.70 0.71 mg/L 1.4 50 03-OCT-19 Cadmium (Cd) <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Chromium (Cr) <0.050 <0.050 RPD-NA mg/L N/A 50 03-OCT-19 Lead (Pb) <0.050 <0.050 RPD-NA mg/L N/A 50 03-OCT-19 Selenium (Se) <0.025 <0.025 RPD-NA mg/L N/A 50 03-OCT-19 Uranium (U) <0.25 <0.25 RPD-NA mg/L N/A 50 03-OCT-19 WG3180627-2 LCS Silver (Ag) 102.2 % 70-130 03-OCT-19 Arsenic (As) 96.2 % 70-130 03-OCT-19 Boron (B) 99.96 % 70-130 03-OCT-19 Barium (Ba) 102.3 % 70-130 03-OCT-19 Cadmium (Cd) 98.4 % 70-130 03-OCT-19 Chromium (Cr) 99.3 % 70-130 03-OCT-19 Lead (Pb) 100.5 % 70-130 03-OCT-19 Selenium (Se) 96.1 % 70-130 03-OCT-19 Uranium (U) 101.2 % 70-130 03-OCT-19 WG3180627-1 MB Silver (Ag) <0.0050 mg/L 0.005 03-OCT-19 Arsenic (As) <0.050 mg/L 0.05 03-OCT-19 Boron (B) <2.5 mg/L 2.5 03-OCT-19 Barium (Ba) <0.50 mg/L 0.5 03-OCT-19 Quality Control Report
Workorder: L2356576 Report Date: 07-OCT-19 Page 2 of 6
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-TCLP-WT Waste Batch R4858292 WG3180627-1 MB Cadmium (Cd) <0.0050 mg/L 0.005 03-OCT-19 Chromium (Cr) <0.050 mg/L 0.05 03-OCT-19 Lead (Pb) <0.050 mg/L 0.05 03-OCT-19 Selenium (Se) <0.025 mg/L 0.025 03-OCT-19 Uranium (U) <0.25 mg/L 0.25 03-OCT-19 WG3180627-5 MS WG3180627-3 Silver (Ag) 116.3 % 50-140 03-OCT-19 Arsenic (As) 97.6 % 50-140 03-OCT-19 Boron (B) 102.9 % 50-140 03-OCT-19 Barium (Ba) 102.9 % 50-140 03-OCT-19 Cadmium (Cd) 96.7 % 50-140 03-OCT-19 Chromium (Cr) 99.4 % 50-140 03-OCT-19 Lead (Pb) 99.5 % 50-140 03-OCT-19 Selenium (Se) 99.2 % 50-140 03-OCT-19 Uranium (U) 97.6 % 50-140 03-OCT-19
PAH-TCLP-WT Waste Batch R4858173 WG3180450-4 DUP WG3180450-5 Acenaphthene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Acenaphthylene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Anthracene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Benzo(a)anthracene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Benzo(a)pyrene <0.0010 <0.0010 RPD-NA mg/L N/A 50 03-OCT-19 Benzo(b)fluoranthene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Benzo(g,h,i)perylene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Benzo(k)fluoranthene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Chrysene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Dibenzo(ah)anthracene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Fluoranthene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Fluorene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Indeno(1,2,3-cd)pyrene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Naphthalene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Phenanthrene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Quality Control Report
Workorder: L2356576 Report Date: 07-OCT-19 Page 3 of 6
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-TCLP-WT Waste Batch R4858173 WG3180450-4 DUP WG3180450-5 Pyrene <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 Quinoline <0.0050 <0.0050 RPD-NA mg/L N/A 50 03-OCT-19 WG3180450-2 LCS Acenaphthene 96.2 % 50-130 03-OCT-19 Acenaphthylene 98.7 % 50-130 03-OCT-19 Anthracene 92.7 % 50-130 03-OCT-19 Benzo(a)anthracene 110.2 % 50-140 03-OCT-19 Benzo(a)pyrene 90.9 % 60-140 03-OCT-19 Benzo(b)fluoranthene 77.9 % 50-140 03-OCT-19 Benzo(g,h,i)perylene 102.3 % 50-140 03-OCT-19 Benzo(k)fluoranthene 131.5 % 50-150 03-OCT-19 Chrysene 124.7 % 50-140 03-OCT-19 Dibenzo(ah)anthracene 103.2 % 50-140 03-OCT-19 Fluoranthene 95.8 % 50-150 03-OCT-19 Fluorene 98.2 % 50-150 03-OCT-19 Indeno(1,2,3-cd)pyrene 111.4 % 50-140 03-OCT-19 Naphthalene 93.1 % 50-130 03-OCT-19 Phenanthrene 98.4 % 50-130 03-OCT-19 Pyrene 94.0 % 50-140 03-OCT-19 Quinoline 97.9 % 50-150 03-OCT-19 WG3180450-1 MB Acenaphthene <0.0050 mg/L 0.005 03-OCT-19 Acenaphthylene <0.0050 mg/L 0.005 03-OCT-19 Anthracene <0.0050 mg/L 0.005 03-OCT-19 Benzo(a)anthracene <0.0050 mg/L 0.005 03-OCT-19 Benzo(a)pyrene <0.0010 mg/L 0.001 03-OCT-19 Benzo(b)fluoranthene <0.0050 mg/L 0.005 03-OCT-19 Benzo(g,h,i)perylene <0.0050 mg/L 0.005 03-OCT-19 Benzo(k)fluoranthene <0.0050 mg/L 0.005 03-OCT-19 Chrysene <0.0050 mg/L 0.005 03-OCT-19 Dibenzo(ah)anthracene <0.0050 mg/L 0.005 03-OCT-19 Fluoranthene <0.0050 mg/L 0.005 03-OCT-19 Fluorene <0.0050 mg/L 0.005 03-OCT-19 Indeno(1,2,3-cd)pyrene <0.0050 mg/L 0.005 03-OCT-19 Quality Control Report
Workorder: L2356576 Report Date: 07-OCT-19 Page 4 of 6
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-TCLP-WT Waste Batch R4858173 WG3180450-1 MB Naphthalene <0.0050 mg/L 0.005 03-OCT-19 Phenanthrene <0.0050 mg/L 0.005 03-OCT-19 Pyrene <0.0050 mg/L 0.005 03-OCT-19 Quinoline <0.0050 mg/L 0.005 03-OCT-19 Surrogate: d8-Naphthalene 94.6 % 50-150 03-OCT-19 Surrogate: d10-Phenanthrene 102.2 % 50-150 03-OCT-19 Surrogate: d12-Chrysene 107.3 % 50-150 03-OCT-19 Surrogate: d10-Acenaphthene 96.6 % 50-150 03-OCT-19 WG3180450-6 MB Acenaphthene <0.0050 mg/L 0.005 07-OCT-19 Acenaphthylene <0.0050 mg/L 0.005 07-OCT-19 Anthracene <0.0050 mg/L 0.005 07-OCT-19 Benzo(a)anthracene <0.0050 mg/L 0.005 07-OCT-19 Benzo(a)pyrene <0.0010 mg/L 0.001 07-OCT-19 Benzo(b)fluoranthene <0.0050 mg/L 0.005 07-OCT-19 Benzo(g,h,i)perylene <0.0050 mg/L 0.005 07-OCT-19 Benzo(k)fluoranthene <0.0050 mg/L 0.005 07-OCT-19 Chrysene <0.0050 mg/L 0.005 07-OCT-19 Dibenzo(ah)anthracene <0.0050 mg/L 0.005 07-OCT-19 Fluoranthene <0.0050 mg/L 0.005 07-OCT-19 Fluorene <0.0050 mg/L 0.005 07-OCT-19 Indeno(1,2,3-cd)pyrene <0.0050 mg/L 0.005 07-OCT-19 Naphthalene <0.0050 mg/L 0.005 07-OCT-19 Phenanthrene <0.0050 mg/L 0.005 07-OCT-19 Pyrene <0.0050 mg/L 0.005 07-OCT-19 Quinoline <0.0050 mg/L 0.005 07-OCT-19 Surrogate: d8-Naphthalene 96.5 % 50-150 07-OCT-19 Surrogate: d10-Phenanthrene 96.7 % 50-150 07-OCT-19 Surrogate: d12-Chrysene 103.7 % 50-150 07-OCT-19 Surrogate: d10-Acenaphthene 95.1 % 50-150 07-OCT-19 WG3180450-3 MS WG3180450-5 Acenaphthene N/A MS-B % 50-150 03-OCT-19 Acenaphthylene N/A MS-B % 50-150 03-OCT-19 Anthracene 100.9 % 50-150 03-OCT-19 Quality Control Report
Workorder: L2356576 Report Date: 07-OCT-19 Page 5 of 6
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-TCLP-WT Waste Batch R4858173 WG3180450-3 MS WG3180450-5 Benzo(a)anthracene 110.7 % 50-150 03-OCT-19 Benzo(a)pyrene 98.0 % 50-150 03-OCT-19 Benzo(b)fluoranthene 77.1 % 50-150 03-OCT-19 Benzo(g,h,i)perylene 105.3 % 50-150 03-OCT-19 Benzo(k)fluoranthene 96.9 % 50-150 03-OCT-19 Chrysene 130.8 % 50-150 03-OCT-19 Dibenzo(ah)anthracene 96.0 % 50-150 03-OCT-19 Fluoranthene 102.2 % 50-150 03-OCT-19 Fluorene N/A MS-B % 50-150 03-OCT-19 Indeno(1,2,3-cd)pyrene 99.7 % 50-150 03-OCT-19 Naphthalene 121.8 % 50-150 03-OCT-19 Phenanthrene N/A MS-B % 50-150 03-OCT-19 Pyrene 101.3 % 50-150 03-OCT-19 Quinoline 74.5 % 50-150 03-OCT-19 Quality Control Report Workorder: L2356576 Report Date: 07-OCT-19
Client: Morrison Hershfield Limited (Ottawa) Page 6 of 6 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description MS-B Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.
Morrison Hershfield Limited (Ottawa) Date Received: 03-OCT-19 ATTN: Cindy Zhao Report Date: 17-OCT-19 12:53 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2359740 Project P.O. #: NOT SUBMITTED Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-1 BH1 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 04-OCT-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 1.5 16000 Arsenic (As)-Dissolved 1.6 DLHC 1.0 ug/L 04-OCT-19 13 1500 Barium (Ba)-Dissolved 848 DLHC 1.0 ug/L 04-OCT-19 *610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 **0.5 53 Boron (B)-Dissolved 120 DLHC 100 ug/L 04-OCT-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 04-OCT-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 11 640 Cobalt (Co)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 3.8 52 Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 04-OCT-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 1.9 20 Molybdenum (Mo)-Dissolved 0.63 DLHC 0.50 ug/L 04-OCT-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 14 390 Selenium (Se)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 **0.3 1.2 Sodium (Na)-Dissolved 330000 DLHC 500 ug/L 04-OCT-19 490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 04-OCT-19 0.5 400 Uranium (U)-Dissolved 0.22 DLHC 0.10 ug/L 04-OCT-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 04-OCT-19 160 890 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 08-OCT-19 2700 100000 Benzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 44 Bromodichloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 67000 Bromoform <5.0 OWP 5.0 ug/L 08-OCT-19 5 380 Bromomethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.89 5.6 Carbon tetrachloride <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.79 Chlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 500 Dibromochloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 65000 Chloroform <1.0 OWP 1.0 ug/L 08-OCT-19 2 2.4 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.25 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 7600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 8 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 08-OCT-19 590 3500 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 320 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 Methylene Chloride <5.0 OWP 5.0 ug/L 08-OCT-19 5 610 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 16 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 08-OCT-19 0.5 5.2 Ethylbenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1800 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 3 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-1 BH1 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Volatile Organic Compounds n-Hexane <0.50 OWP 0.50 ug/L 08-OCT-19 5 51 Methyl Ethyl Ketone <20 OWP 20 ug/L 08-OCT-19 400 470000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 08-OCT-19 640 140000 MTBE <2.0 OWP 2.0 ug/L 08-OCT-19 15 190 Styrene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 3.2 Tetrachloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Toluene <0.50 OWP 0.50 ug/L 08-OCT-19 0.8 14000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 640 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4.7 Trichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 08-OCT-19 150 2000 Vinyl chloride <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 0.5 o-Xylene <0.30 OWP 0.30 ug/L 08-OCT-19 m+p-Xylenes <0.40 OWP 0.40 ug/L 08-OCT-19 Xylenes (Total) <0.50 0.50 ug/L 08-OCT-19 72 3300 Surrogate: 4-Bromofluorobenzene 95.8 70-130 % 08-OCT-19 Surrogate: 1,4-Difluorobenzene 100.2 70-130 % 08-OCT-19 Hydrocarbons F1 (C6-C10) <25 OWP 25 ug/L 08-OCT-19 420 420 F1-BTEX <25 25 ug/L 17-OCT-19 420 420 F2 (C10-C16) 210 100 ug/L 08-OCT-19 *150 *150 F2-Naphth 200 100 ug/L 17-OCT-19 F3 (C16-C34) 870 250 ug/L 08-OCT-19 *500 *500 F3-PAH 740 250 ug/L 17-OCT-19 F4 (C34-C50) 630 250 ug/L 08-OCT-19 *500 *500 Total Hydrocarbons (C6-C50) 1710 370 ug/L 17-OCT-19 Chrom. to baseline at nC50 YES No Unit 08-OCT-19 Surrogate: 2-Bromobenzotrifluoride 88.8 60-140 % 08-OCT-19 Surrogate: 3,4-Dichlorotoluene 67.5 60-140 % 08-OCT-19 Polycyclic Aromatic Hydrocarbons Acenaphthene 8.41 DLHC 0.040 ug/L 17-OCT-19 *4.1 600 Acenaphthylene 0.354 DLHC 0.040 ug/L 17-OCT-19 1 1.4 Anthracene 9.70 DLHC 0.040 ug/L 17-OCT-19 *0.1 *1 Benzo(a)anthracene 9.22 DLHC 0.040 ug/L 17-OCT-19 *0.2 *1.8 Benzo(a)pyrene 6.35 DLHC 0.040 ug/L 17-OCT-19 *0.01 *0.81 Benzo(b)fluoranthene 7.13 DLHC 0.040 ug/L 17-OCT-19 *0.1 *0.75 Benzo(g,h,i)perylene 3.86 DLHC 0.040 ug/L 17-OCT-19 *0.2 *0.2 Benzo(k)fluoranthene 2.66 DLHC 0.040 ug/L 17-OCT-19 *0.1 *0.4 Chrysene 7.26 DLHC 0.040 ug/L 17-OCT-19 *0.1 *0.7 Dibenzo(ah)anthracene 0.909 DLHC 0.040 ug/L 17-OCT-19 *0.2 *0.4 Fluoranthene 26.3 DLHC 0.040 ug/L 17-OCT-19 *0.4 73 Fluorene 18.8 DLHC 0.040 ug/L 17-OCT-19 120 290 Indeno(1,2,3-cd)pyrene 4.61 DLHC 0.040 ug/L 17-OCT-19 *0.2 *0.2 1+2-Methylnaphthalenes 5.31 0.057 ug/L 17-OCT-19 *2 1500 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 4 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-1 BH1 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Polycyclic Aromatic Hydrocarbons 1-Methylnaphthalene 4.33 DLHC 0.040 ug/L 17-OCT-19 *2 1500 2-Methylnaphthalene 0.981 DLHC 0.040 ug/L 17-OCT-19 2 1500 Naphthalene 4.92 0.050 ug/L 17-OCT-19 7 1400 Phenanthrene 49.7 DLHC 0.040 ug/L 17-OCT-19 *0.1 380 Pyrene 22.4 DLHC 0.040 ug/L 17-OCT-19 *0.2 *5.7 Surrogate: d10-Acenaphthene 96.5 60-140 % 17-OCT-19 Surrogate: d12-Chrysene 98.7 60-140 % 17-OCT-19 Surrogate: d8-Naphthalene 94.2 60-140 % 17-OCT-19 Surrogate: d10-Phenanthrene 88.9 60-140 % 17-OCT-19
L2359740-2 BH2 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 04-OCT-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 1.5 16000 Arsenic (As)-Dissolved 1.5 DLHC 1.0 ug/L 04-OCT-19 13 1500 Barium (Ba)-Dissolved 917 DLHC 1.0 ug/L 04-OCT-19 *610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 **0.5 53 Boron (B)-Dissolved <100 DLHC 100 ug/L 04-OCT-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 04-OCT-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 11 640 Cobalt (Co)-Dissolved 2.6 DLHC 1.0 ug/L 04-OCT-19 3.8 52 Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 04-OCT-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 1.9 20 Molybdenum (Mo)-Dissolved 1.85 DLHC 0.50 ug/L 04-OCT-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 14 390 Selenium (Se)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 **0.3 1.2 Sodium (Na)-Dissolved 126000 DLHC 500 ug/L 04-OCT-19 490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 04-OCT-19 0.5 400 Uranium (U)-Dissolved 0.62 DLHC 0.10 ug/L 04-OCT-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 04-OCT-19 160 890 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 08-OCT-19 2700 100000 Benzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 44 Bromodichloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 67000 Bromoform <5.0 OWP 5.0 ug/L 08-OCT-19 5 380 Bromomethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.89 5.6 Carbon tetrachloride <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.79 Chlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 500 Dibromochloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 65000 Chloroform <1.0 OWP 1.0 ug/L 08-OCT-19 2 2.4 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.25 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4600 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 5 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-2 BH2 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Volatile Organic Compounds 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 7600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 8 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 08-OCT-19 590 3500 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 320 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 Methylene Chloride <5.0 OWP 5.0 ug/L 08-OCT-19 5 610 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 16 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 08-OCT-19 0.5 5.2 Ethylbenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1800 n-Hexane <0.50 OWP 0.50 ug/L 08-OCT-19 5 51 Methyl Ethyl Ketone <20 OWP 20 ug/L 08-OCT-19 400 470000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 08-OCT-19 640 140000 MTBE <2.0 OWP 2.0 ug/L 08-OCT-19 15 190 Styrene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 3.2 Tetrachloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Toluene <0.50 OWP 0.50 ug/L 08-OCT-19 0.8 14000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 640 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4.7 Trichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 08-OCT-19 150 2000 Vinyl chloride <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 0.5 o-Xylene <0.30 OWP 0.30 ug/L 08-OCT-19 m+p-Xylenes <0.40 OWP 0.40 ug/L 08-OCT-19 Xylenes (Total) <0.50 0.50 ug/L 08-OCT-19 72 3300 Surrogate: 4-Bromofluorobenzene 95.8 70-130 % 08-OCT-19 Surrogate: 1,4-Difluorobenzene 100.9 70-130 % 08-OCT-19 Hydrocarbons F1 (C6-C10) <25 OWP 25 ug/L 08-OCT-19 420 420 F1-BTEX <25 25 ug/L 08-OCT-19 420 420 F2 (C10-C16) <100 100 ug/L 07-OCT-19 150 150 F3 (C16-C34) <250 250 ug/L 07-OCT-19 500 500 F4 (C34-C50) <250 250 ug/L 07-OCT-19 500 500 Total Hydrocarbons (C6-C50) <370 370 ug/L 08-OCT-19 Chrom. to baseline at nC50 YES No Unit 07-OCT-19 Surrogate: 2-Bromobenzotrifluoride 81.4 60-140 % 07-OCT-19 Surrogate: 3,4-Dichlorotoluene 70.4 60-140 % 08-OCT-19 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.020 0.020 ug/L 17-OCT-19 4.1 600 Acenaphthylene <0.020 0.020 ug/L 17-OCT-19 1 1.4 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 6 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-2 BH2 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Polycyclic Aromatic Hydrocarbons Anthracene <0.020 0.020 ug/L 17-OCT-19 0.1 1 Benzo(a)anthracene <0.020 0.020 ug/L 17-OCT-19 0.2 1.8 Benzo(a)pyrene <0.010 0.010 ug/L 17-OCT-19 0.01 0.81 Benzo(b)fluoranthene <0.020 0.020 ug/L 17-OCT-19 0.1 0.75 Benzo(g,h,i)perylene <0.020 0.020 ug/L 17-OCT-19 0.2 0.2 Benzo(k)fluoranthene <0.020 0.020 ug/L 17-OCT-19 0.1 0.4 Chrysene <0.020 0.020 ug/L 17-OCT-19 0.1 0.7 Dibenzo(ah)anthracene <0.020 0.020 ug/L 17-OCT-19 0.2 0.4 Fluoranthene 0.032 0.020 ug/L 17-OCT-19 0.4 73 Fluorene <0.020 0.020 ug/L 17-OCT-19 120 290 Indeno(1,2,3-cd)pyrene <0.020 0.020 ug/L 17-OCT-19 0.2 0.2 1+2-Methylnaphthalenes <0.028 0.028 ug/L 17-OCT-19 2 1500 1-Methylnaphthalene <0.020 0.020 ug/L 17-OCT-19 2 1500 2-Methylnaphthalene <0.020 0.020 ug/L 17-OCT-19 2 1500 Naphthalene <0.050 0.050 ug/L 17-OCT-19 7 1400 Phenanthrene 0.054 0.020 ug/L 17-OCT-19 0.1 380 Pyrene 0.102 0.020 ug/L 17-OCT-19 0.2 5.7 Surrogate: d10-Acenaphthene 98.2 60-140 % 17-OCT-19 Surrogate: d12-Chrysene 101.3 60-140 % 17-OCT-19 Surrogate: d8-Naphthalene 98.0 60-140 % 17-OCT-19 Surrogate: d10-Phenanthrene 93.5 60-140 % 17-OCT-19
L2359740-3 BH3 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 04-OCT-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 1.5 16000 Arsenic (As)-Dissolved 1.5 DLHC 1.0 ug/L 04-OCT-19 13 1500 Barium (Ba)-Dissolved 692 DLHC 1.0 ug/L 04-OCT-19 *610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 **0.5 53 Boron (B)-Dissolved 250 DLHC 100 ug/L 04-OCT-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 04-OCT-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 11 640 Cobalt (Co)-Dissolved 2.0 DLHC 1.0 ug/L 04-OCT-19 3.8 52 Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 04-OCT-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 1.9 20 Molybdenum (Mo)-Dissolved 1.27 DLHC 0.50 ug/L 04-OCT-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 14 390 Selenium (Se)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 **0.3 1.2 Sodium (Na)-Dissolved 336000 DLHC 500 ug/L 04-OCT-19 490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 04-OCT-19 0.5 400 Uranium (U)-Dissolved 0.31 DLHC 0.10 ug/L 04-OCT-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 04-OCT-19 160 890 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 7 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-3 BH3 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Volatile Organic Compounds Acetone <30 OWP 30 ug/L 08-OCT-19 2700 100000 Benzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 44 Bromodichloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 67000 Bromoform <5.0 OWP 5.0 ug/L 08-OCT-19 5 380 Bromomethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.89 5.6 Carbon tetrachloride <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.79 Chlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 500 Dibromochloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 65000 Chloroform <1.0 OWP 1.0 ug/L 08-OCT-19 2 2.4 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.25 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 7600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 8 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 08-OCT-19 590 3500 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 320 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 Methylene Chloride <5.0 OWP 5.0 ug/L 08-OCT-19 5 610 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 16 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 08-OCT-19 0.5 5.2 Ethylbenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1800 n-Hexane <0.50 OWP 0.50 ug/L 08-OCT-19 5 51 Methyl Ethyl Ketone <20 OWP 20 ug/L 08-OCT-19 400 470000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 08-OCT-19 640 140000 MTBE <2.0 OWP 2.0 ug/L 08-OCT-19 15 190 Styrene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 3.2 Tetrachloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Toluene <0.50 OWP 0.50 ug/L 08-OCT-19 0.8 14000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 640 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4.7 Trichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 08-OCT-19 150 2000 Vinyl chloride <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 0.5 o-Xylene <0.30 OWP 0.30 ug/L 08-OCT-19 m+p-Xylenes <0.40 OWP 0.40 ug/L 08-OCT-19 Xylenes (Total) <0.50 0.50 ug/L 08-OCT-19 72 3300 Surrogate: 4-Bromofluorobenzene 96.4 70-130 % 08-OCT-19 Surrogate: 1,4-Difluorobenzene 99.9 70-130 % 08-OCT-19 Hydrocarbons F1 (C6-C10) <25 OWP 25 ug/L 08-OCT-19 420 420 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 8 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-3 BH3 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Hydrocarbons F1-BTEX <25 25 ug/L 08-OCT-19 420 420 F2 (C10-C16) <100 100 ug/L 07-OCT-19 150 150 F3 (C16-C34) <250 250 ug/L 07-OCT-19 500 500 F4 (C34-C50) <250 250 ug/L 07-OCT-19 500 500 Total Hydrocarbons (C6-C50) <370 370 ug/L 08-OCT-19 Chrom. to baseline at nC50 YES No Unit 07-OCT-19 Surrogate: 2-Bromobenzotrifluoride 85.4 60-140 % 07-OCT-19 Surrogate: 3,4-Dichlorotoluene 69.8 60-140 % 08-OCT-19 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.020 0.020 ug/L 17-OCT-19 4.1 600 Acenaphthylene <0.020 0.020 ug/L 17-OCT-19 1 1.4 Anthracene <0.020 0.020 ug/L 17-OCT-19 0.1 1 Benzo(a)anthracene <0.020 0.020 ug/L 17-OCT-19 0.2 1.8 Benzo(a)pyrene <0.010 0.010 ug/L 17-OCT-19 0.01 0.81 Benzo(b)fluoranthene <0.020 0.020 ug/L 17-OCT-19 0.1 0.75 Benzo(g,h,i)perylene <0.020 0.020 ug/L 17-OCT-19 0.2 0.2 Benzo(k)fluoranthene <0.020 0.020 ug/L 17-OCT-19 0.1 0.4 Chrysene <0.020 0.020 ug/L 17-OCT-19 0.1 0.7 Dibenzo(ah)anthracene <0.020 0.020 ug/L 17-OCT-19 0.2 0.4 Fluoranthene 0.037 0.020 ug/L 17-OCT-19 0.4 73 Fluorene 0.027 0.020 ug/L 17-OCT-19 120 290 Indeno(1,2,3-cd)pyrene <0.020 0.020 ug/L 17-OCT-19 0.2 0.2 1+2-Methylnaphthalenes <0.028 0.028 ug/L 17-OCT-19 2 1500 1-Methylnaphthalene <0.020 0.020 ug/L 17-OCT-19 2 1500 2-Methylnaphthalene 0.024 0.020 ug/L 17-OCT-19 2 1500 Naphthalene <0.050 0.050 ug/L 17-OCT-19 7 1400 Phenanthrene 0.119 0.020 ug/L 17-OCT-19 *0.1 380 Pyrene 0.105 0.020 ug/L 17-OCT-19 0.2 5.7 Surrogate: d10-Acenaphthene 97.7 60-140 % 17-OCT-19 Surrogate: d12-Chrysene 100.7 60-140 % 17-OCT-19 Surrogate: d8-Naphthalene 95.2 60-140 % 17-OCT-19 Surrogate: d10-Phenanthrene 93.8 60-140 % 17-OCT-19
L2359740-4 BH4 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 04-OCT-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 1.5 16000 Arsenic (As)-Dissolved 1.1 DLHC 1.0 ug/L 04-OCT-19 13 1500 Barium (Ba)-Dissolved 288 DLHC 1.0 ug/L 04-OCT-19 610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 **0.5 53 Boron (B)-Dissolved <100 DLHC 100 ug/L 04-OCT-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 04-OCT-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 11 640 Cobalt (Co)-Dissolved 4.9 DLHC 1.0 ug/L 04-OCT-19 *3.8 52 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 9 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-4 BH4 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Dissolved Metals Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 04-OCT-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 1.9 20 Molybdenum (Mo)-Dissolved 0.78 DLHC 0.50 ug/L 04-OCT-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 14 390 Selenium (Se)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 **0.3 1.2 Sodium (Na)-Dissolved 109000 DLHC 500 ug/L 04-OCT-19 490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 04-OCT-19 0.5 400 Uranium (U)-Dissolved 2.14 DLHC 0.10 ug/L 04-OCT-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 04-OCT-19 160 890 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 08-OCT-19 2700 100000 Benzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 44 Bromodichloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 67000 Bromoform <5.0 OWP 5.0 ug/L 08-OCT-19 5 380 Bromomethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.89 5.6 Carbon tetrachloride <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.79 Chlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 500 Dibromochloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 65000 Chloroform <1.0 OWP 1.0 ug/L 08-OCT-19 2 2.4 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.25 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 7600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 8 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 08-OCT-19 590 3500 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 320 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 Methylene Chloride <5.0 OWP 5.0 ug/L 08-OCT-19 5 610 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 16 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 08-OCT-19 0.5 5.2 Ethylbenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1800 n-Hexane <0.50 OWP 0.50 ug/L 08-OCT-19 5 51 Methyl Ethyl Ketone <20 OWP 20 ug/L 08-OCT-19 400 470000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 08-OCT-19 640 140000 MTBE <2.0 OWP 2.0 ug/L 08-OCT-19 15 190 Styrene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 3.2 Tetrachloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Toluene <0.50 OWP 0.50 ug/L 08-OCT-19 0.8 14000 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 10 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-4 BH4 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Volatile Organic Compounds 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 640 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4.7 Trichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 08-OCT-19 150 2000 Vinyl chloride <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 0.5 o-Xylene <0.30 OWP 0.30 ug/L 08-OCT-19 m+p-Xylenes <0.40 OWP 0.40 ug/L 08-OCT-19 Xylenes (Total) <0.50 0.50 ug/L 08-OCT-19 72 3300 Surrogate: 4-Bromofluorobenzene 96.6 70-130 % 08-OCT-19 Surrogate: 1,4-Difluorobenzene 100.3 70-130 % 08-OCT-19 Hydrocarbons F1 (C6-C10) <25 OWP 25 ug/L 08-OCT-19 420 420 F1-BTEX <25 25 ug/L 08-OCT-19 420 420 F2 (C10-C16) <100 100 ug/L 07-OCT-19 150 150 F3 (C16-C34) <250 250 ug/L 07-OCT-19 500 500 F4 (C34-C50) <250 250 ug/L 07-OCT-19 500 500 Total Hydrocarbons (C6-C50) <370 370 ug/L 08-OCT-19 Chrom. to baseline at nC50 YES No Unit 07-OCT-19 Surrogate: 2-Bromobenzotrifluoride 75.4 60-140 % 07-OCT-19 Surrogate: 3,4-Dichlorotoluene 67.4 60-140 % 08-OCT-19 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.020 0.020 ug/L 17-OCT-19 4.1 600 Acenaphthylene <0.020 0.020 ug/L 17-OCT-19 1 1.4 Anthracene 0.035 0.020 ug/L 17-OCT-19 0.1 1 Benzo(a)anthracene 0.082 0.020 ug/L 17-OCT-19 0.2 1.8 Benzo(a)pyrene 0.060 0.010 ug/L 17-OCT-19 *0.01 0.81 Benzo(b)fluoranthene 0.077 0.020 ug/L 17-OCT-19 0.1 0.75 Benzo(g,h,i)perylene 0.043 0.020 ug/L 17-OCT-19 0.2 0.2 Benzo(k)fluoranthene 0.031 0.020 ug/L 17-OCT-19 0.1 0.4 Chrysene 0.072 0.020 ug/L 17-OCT-19 0.1 0.7 Dibenzo(ah)anthracene <0.020 0.020 ug/L 17-OCT-19 0.2 0.4 Fluoranthene 0.230 0.020 ug/L 17-OCT-19 0.4 73 Fluorene 0.026 0.020 ug/L 17-OCT-19 120 290 Indeno(1,2,3-cd)pyrene 0.052 0.020 ug/L 17-OCT-19 0.2 0.2 1+2-Methylnaphthalenes <0.028 0.028 ug/L 17-OCT-19 2 1500 1-Methylnaphthalene <0.020 0.020 ug/L 17-OCT-19 2 1500 2-Methylnaphthalene <0.020 0.020 ug/L 17-OCT-19 2 1500 Naphthalene <0.050 0.050 ug/L 17-OCT-19 7 1400 Phenanthrene 0.214 0.020 ug/L 17-OCT-19 *0.1 380 Pyrene 0.274 0.020 ug/L 17-OCT-19 *0.2 5.7 Surrogate: d10-Acenaphthene 96.4 60-140 % 17-OCT-19 Surrogate: d12-Chrysene 101.0 60-140 % 17-OCT-19 Surrogate: d8-Naphthalene 94.6 60-140 % 17-OCT-19 Surrogate: d10-Phenanthrene 93.4 60-140 % 17-OCT-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 11 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-5 BH21 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 04-OCT-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 1.5 16000 Arsenic (As)-Dissolved 1.6 DLHC 1.0 ug/L 04-OCT-19 13 1500 Barium (Ba)-Dissolved 905 DLHC 1.0 ug/L 04-OCT-19 *610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 **0.5 53 Boron (B)-Dissolved 120 DLHC 100 ug/L 04-OCT-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 04-OCT-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 11 640 Cobalt (Co)-Dissolved <1.0 DLHC 1.0 ug/L 04-OCT-19 3.8 52 Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 04-OCT-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 1.9 20 Molybdenum (Mo)-Dissolved 0.64 DLHC 0.50 ug/L 04-OCT-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 14 390 Selenium (Se)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 04-OCT-19 **0.3 1.2 Sodium (Na)-Dissolved 345000 DLHC 500 ug/L 04-OCT-19 490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 04-OCT-19 0.5 400 Uranium (U)-Dissolved 0.22 DLHC 0.10 ug/L 04-OCT-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 04-OCT-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 04-OCT-19 160 890 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 08-OCT-19 2700 100000 Benzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 44 Bromodichloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 67000 Bromoform <5.0 OWP 5.0 ug/L 08-OCT-19 5 380 Bromomethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.89 5.6 Carbon tetrachloride <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.79 Chlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 500 Dibromochloromethane <2.0 OWP 2.0 ug/L 08-OCT-19 2 65000 Chloroform <1.0 OWP 1.0 ug/L 08-OCT-19 2 2.4 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 08-OCT-19 0.2 0.25 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 7600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 8 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 08-OCT-19 590 3500 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 320 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 1.6 1.6 Methylene Chloride <5.0 OWP 5.0 ug/L 08-OCT-19 5 610 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 16 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 08-OCT-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 08-OCT-19 0.5 5.2 Ethylbenzene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1800 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 12 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-5 BH21 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Volatile Organic Compounds n-Hexane <0.50 OWP 0.50 ug/L 08-OCT-19 5 51 Methyl Ethyl Ketone <20 OWP 20 ug/L 08-OCT-19 400 470000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 08-OCT-19 640 140000 MTBE <2.0 OWP 2.0 ug/L 08-OCT-19 15 190 Styrene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 3.2 Tetrachloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Toluene <0.50 OWP 0.50 ug/L 08-OCT-19 0.8 14000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 640 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 4.7 Trichloroethylene <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 1.6 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 08-OCT-19 150 2000 Vinyl chloride <0.50 OWP 0.50 ug/L 08-OCT-19 0.5 0.5 o-Xylene <0.30 OWP 0.30 ug/L 08-OCT-19 m+p-Xylenes <0.40 OWP 0.40 ug/L 08-OCT-19 Xylenes (Total) <0.50 0.50 ug/L 08-OCT-19 72 3300 Surrogate: 4-Bromofluorobenzene 95.6 70-130 % 08-OCT-19 Surrogate: 1,4-Difluorobenzene 100.9 70-130 % 08-OCT-19 Hydrocarbons F1 (C6-C10) <25 OWP 25 ug/L 08-OCT-19 420 420 F1-BTEX <25 25 ug/L 08-OCT-19 420 420 F2 (C10-C16) 210 100 ug/L 07-OCT-19 *150 *150 F3 (C16-C34) 1150 250 ug/L 07-OCT-19 *500 *500 F4 (C34-C50) 890 250 ug/L 07-OCT-19 *500 *500 Total Hydrocarbons (C6-C50) 2260 370 ug/L 08-OCT-19 Chrom. to baseline at nC50 YES No Unit 07-OCT-19 Surrogate: 2-Bromobenzotrifluoride 84.6 60-140 % 07-OCT-19 Surrogate: 3,4-Dichlorotoluene 66.0 60-140 % 08-OCT-19 Polycyclic Aromatic Hydrocarbons Acenaphthene 10.5 DLHC 0.040 ug/L 17-OCT-19 *4.1 600 Acenaphthylene 0.451 DLHC 0.040 ug/L 17-OCT-19 1 1.4 Anthracene 14.1 DLHC 0.040 ug/L 17-OCT-19 *0.1 *1 Benzo(a)anthracene 13.5 DLHC 0.040 ug/L 17-OCT-19 *0.2 *1.8 Benzo(a)pyrene 9.35 DLHC 0.040 ug/L 17-OCT-19 *0.01 *0.81 Benzo(b)fluoranthene 10.3 DLHC 0.040 ug/L 17-OCT-19 *0.1 *0.75 Benzo(g,h,i)perylene 5.86 DLHC 0.040 ug/L 17-OCT-19 *0.2 *0.2 Benzo(k)fluoranthene 3.68 DLHC 0.040 ug/L 17-OCT-19 *0.1 *0.4 Chrysene 10.4 DLHC 0.040 ug/L 17-OCT-19 *0.1 *0.7 Dibenzo(ah)anthracene 1.42 DLHC 0.040 ug/L 17-OCT-19 *0.2 *0.4 Fluoranthene 38.5 DLHC 0.040 ug/L 17-OCT-19 *0.4 73 Fluorene 24.3 DLHC 0.040 ug/L 17-OCT-19 120 290 Indeno(1,2,3-cd)pyrene 7.17 DLHC 0.040 ug/L 17-OCT-19 *0.2 *0.2 1+2-Methylnaphthalenes 6.32 0.057 ug/L 17-OCT-19 *2 1500 1-Methylnaphthalene 5.11 DLHC 0.040 ug/L 17-OCT-19 *2 1500 2-Methylnaphthalene 1.22 DLHC 0.040 ug/L 17-OCT-19 2 1500 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2359740 CONTD.... ANALYTICAL GUIDELINE REPORT Page 13 of 15 190441800 17-OCT-19 12:53 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2359740-5 BH21 Sampled By: CLIENT on 02-OCT-19 #1 #2 Matrix: WATER
Polycyclic Aromatic Hydrocarbons Naphthalene 5.48 0.050 ug/L 17-OCT-19 7 1400 Phenanthrene 76.0 DLHC 0.040 ug/L 17-OCT-19 *0.1 380 Pyrene 33.0 DLHC 0.040 ug/L 17-OCT-19 *0.2 *5.7 Surrogate: d10-Acenaphthene 100.4 60-140 % 17-OCT-19 Surrogate: d12-Chrysene 101.9 60-140 % 17-OCT-19 Surrogate: d8-Naphthalene 96.0 60-140 % 17-OCT-19 Surrogate: d10-Phenanthrene 90.8 60-140 % 17-OCT-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use 190441800 L2359740 CONTD.... Page 14 of 15 17-OCT-19 12:53 (MT) Reference Information
Sample Parameter Qualifier key listed: Qualifier Description
OWP Organic water sample contained visible sediment (must be included as part of analysis). Measured concentrations of organic substances in water can be biased high due to presence of sediment. DLHC Detection Limit Raised: Dilution required due to high concentration of test analyte(s).
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
F1-F4-511-CALC-WT Water F1-F4 Hydrocarbon Calculated CCME CWS-PHC, Pub #1310, Dec 2001-L Parameters
Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.
In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines and the gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes has been subtracted from F1.
In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.
Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range: 1. All extraction and analysis holding times were met. 2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene. 3. Linearity of gasoline response within 15% throughout the calibration range.
Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges: 1. All extraction and analysis holding times were met. 2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average. 3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors. 4. Linearity of diesel or motor oil response within 15% throughout the calibration range. F1-HS-511-WT Water F1-O.Reg 153/04 (July 2011) E3398/CCME TIER 1-HS
Fraction F1 is determined by analyzing by headspace-GC/FID.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). F2-F4-511-WT Water F2-F4-O.Reg 153/04 (July 2011) EPA 3511/CCME Tier 1
Petroleum Hydrocarbons (F2-F4 fractions) are extracted from water using a hexane micro-extraction technique. Instrumental analysis is by GC-FID, as per the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Tier 1 Method, CCME, 2001.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). MET-D-UG/L-MS-WT Water Diss. Metals in Water by ICPMS EPA 200.8 (ug/L)
The metal constituents of a non-acidified sample that pass through a membrane filter prior to ICP/MS analysis.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). METHYLNAPS-CALC-WT Water PAH-Calculated Parameters SW846 8270 PAH-511-WT Water PAH-O. Reg 153/04 (July 2011) SW846 3510/8270
Aqueous samples, fortified with surrogates, are extracted using liquid/liquid extraction technique. The sample extracts are concentrated and then analyzed using GC/MS. Results for benzo(b) fluoranthene may include contributions from benzo(j)fluoranthene, if also present in the sample.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). VOC-1,3-DCP-CALC-WT Water Regulation 153 VOCs SW8260B/SW8270C VOC-511-HS-WT Water VOC by GCMS HS O.Reg SW846 8260 153/04 (July 2011)
Liquid samples are analyzed by headspace GC/MSD.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). 190441800 L2359740 CONTD.... Page 15 of 15 17-OCT-19 12:53 (MT) Reference Information
XYLENES-SUM-CALC- Water Sum of Xylene Isomer CALCULATION WT Concentrations
Total xylenes represents the sum of o-xylene and m&p-xylene.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 1 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
F1-HS-511-WT Water Batch R4861166 WG3183541-4 DUP WG3183541-3 F1 (C6-C10) <25 <25 RPD-NA ug/L N/A 30 08-OCT-19 WG3183541-1 LCS F1 (C6-C10) 99.0 % 80-120 08-OCT-19 WG3183541-2 MB F1 (C6-C10) <25 ug/L 25 08-OCT-19 Surrogate: 3,4-Dichlorotoluene 97.1 % 60-140 08-OCT-19 WG3183541-5 MS WG3183541-3 F1 (C6-C10) 90.7 % 60-140 08-OCT-19
F2-F4-511-WT Water Batch R4861692 WG3182365-2 LCS F2 (C10-C16) 88.1 % 70-130 07-OCT-19 F3 (C16-C34) 90.2 % 70-130 07-OCT-19 F4 (C34-C50) 92.3 % 70-130 07-OCT-19 WG3182365-1 MB F2 (C10-C16) <100 ug/L 100 07-OCT-19 F3 (C16-C34) <250 ug/L 250 07-OCT-19 F4 (C34-C50) <250 ug/L 250 07-OCT-19 Surrogate: 2-Bromobenzotrifluoride 77.1 % 60-140 07-OCT-19
MET-D-UG/L-MS-WT Water Batch R4860330 WG3182532-4 DUP WG3182532-3 Antimony (Sb)-Dissolved <0.10 <0.10 RPD-NA ug/L N/A 20 04-OCT-19 Arsenic (As)-Dissolved <0.10 <0.10 RPD-NA ug/L N/A 20 04-OCT-19 Barium (Ba)-Dissolved 10.5 10.2 ug/L 2.9 20 04-OCT-19 Beryllium (Be)-Dissolved <0.10 <0.10 RPD-NA ug/L N/A 20 04-OCT-19 Boron (B)-Dissolved <10 <10 RPD-NA ug/L N/A 20 04-OCT-19 Cadmium (Cd)-Dissolved <0.0050 <0.0050 RPD-NA ug/L N/A 20 04-OCT-19 Chromium (Cr)-Dissolved <0.50 <0.50 RPD-NA ug/L N/A 20 04-OCT-19 Cobalt (Co)-Dissolved <0.10 <0.10 RPD-NA ug/L N/A 20 04-OCT-19 Copper (Cu)-Dissolved 2.13 2.11 ug/L 1.1 20 04-OCT-19 Lead (Pb)-Dissolved <0.050 <0.050 RPD-NA ug/L N/A 20 04-OCT-19 Molybdenum (Mo)-Dissolved 1.45 1.45 ug/L 0.4 20 04-OCT-19 Nickel (Ni)-Dissolved <0.50 <0.50 RPD-NA ug/L N/A 20 04-OCT-19 Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 2 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-D-UG/L-MS-WT Water Batch R4860330 WG3182532-4 DUP WG3182532-3 Selenium (Se)-Dissolved 0.136 0.135 ug/L 0.4 20 04-OCT-19 Silver (Ag)-Dissolved <0.050 <0.050 RPD-NA ug/L N/A 20 04-OCT-19 Sodium (Na)-Dissolved 761 751 ug/L 1.4 20 04-OCT-19 Thallium (Tl)-Dissolved 0.013 0.012 ug/L 5.5 20 04-OCT-19 Uranium (U)-Dissolved 7.82 7.98 ug/L 2.1 20 04-OCT-19 Vanadium (V)-Dissolved 0.53 0.53 ug/L 1.0 20 04-OCT-19 Zinc (Zn)-Dissolved <1.0 <1.0 RPD-NA ug/L N/A 20 04-OCT-19 WG3182532-2 LCS Antimony (Sb)-Dissolved 100.4 % 80-120 04-OCT-19 Arsenic (As)-Dissolved 95.3 % 80-120 04-OCT-19 Barium (Ba)-Dissolved 92.1 % 80-120 04-OCT-19 Beryllium (Be)-Dissolved 101.0 % 80-120 04-OCT-19 Boron (B)-Dissolved 100.4 % 80-120 04-OCT-19 Cadmium (Cd)-Dissolved 95.4 % 80-120 04-OCT-19 Chromium (Cr)-Dissolved 95.1 % 80-120 04-OCT-19 Cobalt (Co)-Dissolved 95.9 % 80-120 04-OCT-19 Copper (Cu)-Dissolved 93.3 % 80-120 04-OCT-19 Lead (Pb)-Dissolved 99.6 % 80-120 04-OCT-19 Molybdenum (Mo)-Dissolved 94.4 % 80-120 04-OCT-19 Nickel (Ni)-Dissolved 95.5 % 80-120 04-OCT-19 Selenium (Se)-Dissolved 98.0 % 80-120 04-OCT-19 Silver (Ag)-Dissolved 97.2 % 80-120 04-OCT-19 Sodium (Na)-Dissolved 101.0 % 80-120 04-OCT-19 Thallium (Tl)-Dissolved 100.2 % 80-120 04-OCT-19 Uranium (U)-Dissolved 95.0 % 80-120 04-OCT-19 Vanadium (V)-Dissolved 97.4 % 80-120 04-OCT-19 Zinc (Zn)-Dissolved 93.1 % 80-120 04-OCT-19 WG3182532-1 MB Antimony (Sb)-Dissolved <0.10 ug/L 0.1 04-OCT-19 Arsenic (As)-Dissolved <0.10 ug/L 0.1 04-OCT-19 Barium (Ba)-Dissolved <0.10 ug/L 0.1 04-OCT-19 Beryllium (Be)-Dissolved <0.10 ug/L 0.1 04-OCT-19 Boron (B)-Dissolved <10 ug/L 10 04-OCT-19 Cadmium (Cd)-Dissolved <0.0050 ug/L 0.005 04-OCT-19 Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 3 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-D-UG/L-MS-WT Water Batch R4860330 WG3182532-1 MB Chromium (Cr)-Dissolved <0.50 ug/L 0.5 04-OCT-19 Cobalt (Co)-Dissolved <0.10 ug/L 0.1 04-OCT-19 Copper (Cu)-Dissolved <0.20 ug/L 0.2 04-OCT-19 Lead (Pb)-Dissolved <0.050 ug/L 0.05 04-OCT-19 Molybdenum (Mo)-Dissolved <0.050 ug/L 0.05 04-OCT-19 Nickel (Ni)-Dissolved <0.50 ug/L 0.5 04-OCT-19 Selenium (Se)-Dissolved <0.050 ug/L 0.05 04-OCT-19 Silver (Ag)-Dissolved <0.050 ug/L 0.05 04-OCT-19 Sodium (Na)-Dissolved <50 ug/L 50 04-OCT-19 Thallium (Tl)-Dissolved <0.010 ug/L 0.01 04-OCT-19 Uranium (U)-Dissolved <0.010 ug/L 0.01 04-OCT-19 Vanadium (V)-Dissolved <0.50 ug/L 0.5 04-OCT-19 Zinc (Zn)-Dissolved <1.0 ug/L 1 04-OCT-19 WG3182532-5 MS WG3182532-3 Antimony (Sb)-Dissolved 102.5 % 70-130 04-OCT-19 Arsenic (As)-Dissolved 103.9 % 70-130 04-OCT-19 Barium (Ba)-Dissolved 91.2 % 70-130 04-OCT-19 Beryllium (Be)-Dissolved 105.3 % 70-130 04-OCT-19 Boron (B)-Dissolved 97.9 % 70-130 04-OCT-19 Cadmium (Cd)-Dissolved 100.6 % 70-130 04-OCT-19 Chromium (Cr)-Dissolved 96.9 % 70-130 04-OCT-19 Cobalt (Co)-Dissolved 96.0 % 70-130 04-OCT-19 Copper (Cu)-Dissolved 93.0 % 70-130 04-OCT-19 Lead (Pb)-Dissolved 97.6 % 70-130 04-OCT-19 Molybdenum (Mo)-Dissolved 94.7 % 70-130 04-OCT-19 Nickel (Ni)-Dissolved 95.4 % 70-130 04-OCT-19 Selenium (Se)-Dissolved 116.4 % 70-130 04-OCT-19 Silver (Ag)-Dissolved 96.4 % 70-130 04-OCT-19 Sodium (Na)-Dissolved 104.5 % 70-130 04-OCT-19 Thallium (Tl)-Dissolved 96.6 % 70-130 04-OCT-19 Uranium (U)-Dissolved N/A MS-B % - 04-OCT-19 Vanadium (V)-Dissolved 99.7 % 70-130 04-OCT-19 Zinc (Zn)-Dissolved 103.1 % 70-130 04-OCT-19
PAH-511-WT Water Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 4 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Water Batch R4872760 WG3182365-2 LCS 1-Methylnaphthalene 96.6 % 50-140 17-OCT-19 2-Methylnaphthalene 82.5 % 50-140 17-OCT-19 Acenaphthene 106.6 % 50-140 17-OCT-19 Acenaphthylene 110.7 % 50-140 17-OCT-19 Anthracene 118.6 % 50-140 17-OCT-19 Benzo(a)anthracene 133.6 % 50-140 17-OCT-19 Benzo(a)pyrene 118.6 % 50-140 17-OCT-19 Benzo(b)fluoranthene 119.4 % 50-140 17-OCT-19 Benzo(g,h,i)perylene 130.6 % 50-140 17-OCT-19 Benzo(k)fluoranthene 119.0 % 50-140 17-OCT-19 Chrysene 127.8 % 50-140 17-OCT-19 Dibenzo(ah)anthracene 116.5 % 50-140 17-OCT-19 Fluoranthene 122.1 % 50-140 17-OCT-19 Fluorene 104.8 % 50-140 17-OCT-19 Indeno(1,2,3-cd)pyrene 133.4 % 50-140 17-OCT-19 Naphthalene 98.9 % 50-140 17-OCT-19 Phenanthrene 114.2 % 50-140 17-OCT-19 Pyrene 123.2 % 50-140 17-OCT-19 WG3182365-1 MB 1-Methylnaphthalene <0.020 ug/L 0.02 17-OCT-19 2-Methylnaphthalene <0.020 ug/L 0.02 17-OCT-19 Acenaphthene <0.020 ug/L 0.02 17-OCT-19 Acenaphthylene <0.020 ug/L 0.02 17-OCT-19 Anthracene <0.020 ug/L 0.02 17-OCT-19 Benzo(a)anthracene <0.020 ug/L 0.02 17-OCT-19 Benzo(a)pyrene <0.010 ug/L 0.01 17-OCT-19 Benzo(b)fluoranthene <0.020 ug/L 0.02 17-OCT-19 Benzo(g,h,i)perylene <0.020 ug/L 0.02 17-OCT-19 Benzo(k)fluoranthene <0.020 ug/L 0.02 17-OCT-19 Chrysene <0.020 ug/L 0.02 17-OCT-19 Dibenzo(ah)anthracene <0.020 ug/L 0.02 17-OCT-19 Fluoranthene <0.020 ug/L 0.02 17-OCT-19 Fluorene <0.020 ug/L 0.02 17-OCT-19 Indeno(1,2,3-cd)pyrene <0.020 ug/L 0.02 17-OCT-19 Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 5 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Water Batch R4872760 WG3182365-1 MB Naphthalene <0.050 ug/L 0.05 17-OCT-19 Phenanthrene <0.020 ug/L 0.02 17-OCT-19 Pyrene <0.020 ug/L 0.02 17-OCT-19 Surrogate: d8-Naphthalene 97.3 % 60-140 17-OCT-19 Surrogate: d10-Phenanthrene 93.3 % 60-140 17-OCT-19 Surrogate: d12-Chrysene 96.9 % 60-140 17-OCT-19 Surrogate: d10-Acenaphthene 97.4 % 60-140 17-OCT-19
VOC-511-HS-WT Water Batch R4861166 WG3183541-4 DUP WG3183541-3 1,1,1,2-Tetrachloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,1,2,2-Tetrachloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,1,1-Trichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,1,2-Trichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,1-Dichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,1-Dichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,2-Dibromoethane <0.20 <0.20 RPD-NA ug/L N/A 30 08-OCT-19 1,2-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,2-Dichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,2-Dichloropropane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,3-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 1,4-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 Acetone <30 <30 RPD-NA ug/L N/A 30 08-OCT-19 Benzene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 Bromodichloromethane <2.0 <2.0 RPD-NA ug/L N/A 30 08-OCT-19 Bromoform <5.0 <5.0 RPD-NA ug/L N/A 30 08-OCT-19 Bromomethane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 Carbon tetrachloride <0.20 <0.20 RPD-NA ug/L N/A 30 08-OCT-19 Chlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 Chloroform <1.0 <1.0 RPD-NA ug/L N/A 30 08-OCT-19 cis-1,2-Dichloroethylene 2.59 2.60 ug/L 0.4 30 08-OCT-19 cis-1,3-Dichloropropene <0.30 <0.30 RPD-NA ug/L N/A 30 08-OCT-19 Dibromochloromethane <2.0 <2.0 RPD-NA ug/L N/A 30 08-OCT-19 Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 6 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4861166 WG3183541-4 DUP WG3183541-3 Dichlorodifluoromethane <2.0 <2.0 RPD-NA ug/L N/A 30 08-OCT-19 Ethylbenzene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 n-Hexane <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 m+p-Xylenes <0.40 <0.40 RPD-NA ug/L N/A 30 08-OCT-19 Methyl Ethyl Ketone <20 <20 RPD-NA ug/L N/A 30 08-OCT-19 Methyl Isobutyl Ketone <20 <20 RPD-NA ug/L N/A 30 08-OCT-19 Methylene Chloride <5.0 <5.0 RPD-NA ug/L N/A 30 08-OCT-19 MTBE <2.0 <2.0 RPD-NA ug/L N/A 30 08-OCT-19 o-Xylene <0.30 <0.30 RPD-NA ug/L N/A 30 08-OCT-19 Styrene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 Tetrachloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 Toluene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 trans-1,2-Dichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 trans-1,3-Dichloropropene <0.30 <0.30 RPD-NA ug/L N/A 30 08-OCT-19 Trichloroethylene 1.55 1.51 ug/L 2.6 30 08-OCT-19 Trichlorofluoromethane <5.0 <5.0 RPD-NA ug/L N/A 30 08-OCT-19 Vinyl chloride <0.50 <0.50 RPD-NA ug/L N/A 30 08-OCT-19 WG3183541-1 LCS 1,1,1,2-Tetrachloroethane 102.7 % 70-130 08-OCT-19 1,1,2,2-Tetrachloroethane 98.7 % 70-130 08-OCT-19 1,1,1-Trichloroethane 96.4 % 70-130 08-OCT-19 1,1,2-Trichloroethane 95.0 % 70-130 08-OCT-19 1,1-Dichloroethane 104.2 % 70-130 08-OCT-19 1,1-Dichloroethylene 95.3 % 70-130 08-OCT-19 1,2-Dibromoethane 92.8 % 70-130 08-OCT-19 1,2-Dichlorobenzene 101.0 % 70-130 08-OCT-19 1,2-Dichloroethane 92.8 % 70-130 08-OCT-19 1,2-Dichloropropane 101.4 % 70-130 08-OCT-19 1,3-Dichlorobenzene 92.9 % 70-130 08-OCT-19 1,4-Dichlorobenzene 93.2 % 70-130 08-OCT-19 Acetone 102.3 % 60-140 08-OCT-19 Benzene 105.3 % 70-130 08-OCT-19 Bromodichloromethane 97.9 % 70-130 08-OCT-19 Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 7 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4861166 WG3183541-1 LCS Bromoform 98.8 % 70-130 08-OCT-19 Bromomethane 92.4 % 60-140 08-OCT-19 Carbon tetrachloride 96.2 % 70-130 08-OCT-19 Chlorobenzene 101.5 % 70-130 08-OCT-19 Chloroform 102.2 % 70-130 08-OCT-19 cis-1,2-Dichloroethylene 98.8 % 70-130 08-OCT-19 cis-1,3-Dichloropropene 93.4 % 70-130 08-OCT-19 Dibromochloromethane 96.9 % 70-130 08-OCT-19 Dichlorodifluoromethane 129.1 % 50-140 08-OCT-19 Ethylbenzene 95.4 % 70-130 08-OCT-19 n-Hexane 93.4 % 70-130 08-OCT-19 m+p-Xylenes 94.7 % 70-130 08-OCT-19 Methyl Ethyl Ketone 90.3 % 60-140 08-OCT-19 Methyl Isobutyl Ketone 90.9 % 60-140 08-OCT-19 Methylene Chloride 97.5 % 70-130 08-OCT-19 MTBE 102.6 % 70-130 08-OCT-19 o-Xylene 95.5 % 70-130 08-OCT-19 Styrene 101.0 % 70-130 08-OCT-19 Tetrachloroethylene 95.3 % 70-130 08-OCT-19 Toluene 97.6 % 70-130 08-OCT-19 trans-1,2-Dichloroethylene 93.9 % 70-130 08-OCT-19 trans-1,3-Dichloropropene 93.1 % 70-130 08-OCT-19 Trichloroethylene 95.1 % 70-130 08-OCT-19 Trichlorofluoromethane 99.4 % 60-140 08-OCT-19 Vinyl chloride 118.8 % 60-140 08-OCT-19 WG3183541-2 MB 1,1,1,2-Tetrachloroethane <0.50 ug/L 0.5 08-OCT-19 1,1,2,2-Tetrachloroethane <0.50 ug/L 0.5 08-OCT-19 1,1,1-Trichloroethane <0.50 ug/L 0.5 08-OCT-19 1,1,2-Trichloroethane <0.50 ug/L 0.5 08-OCT-19 1,1-Dichloroethane <0.50 ug/L 0.5 08-OCT-19 1,1-Dichloroethylene <0.50 ug/L 0.5 08-OCT-19 1,2-Dibromoethane <0.20 ug/L 0.2 08-OCT-19 1,2-Dichlorobenzene <0.50 ug/L 0.5 08-OCT-19 Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 8 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4861166 WG3183541-2 MB 1,2-Dichloroethane <0.50 ug/L 0.5 08-OCT-19 1,2-Dichloropropane <0.50 ug/L 0.5 08-OCT-19 1,3-Dichlorobenzene <0.50 ug/L 0.5 08-OCT-19 1,4-Dichlorobenzene <0.50 ug/L 0.5 08-OCT-19 Acetone <30 ug/L 30 08-OCT-19 Benzene <0.50 ug/L 0.5 08-OCT-19 Bromodichloromethane <2.0 ug/L 2 08-OCT-19 Bromoform <5.0 ug/L 5 08-OCT-19 Bromomethane <0.50 ug/L 0.5 08-OCT-19 Carbon tetrachloride <0.20 ug/L 0.2 08-OCT-19 Chlorobenzene <0.50 ug/L 0.5 08-OCT-19 Chloroform <1.0 ug/L 1 08-OCT-19 cis-1,2-Dichloroethylene <0.50 ug/L 0.5 08-OCT-19 cis-1,3-Dichloropropene <0.30 ug/L 0.3 08-OCT-19 Dibromochloromethane <2.0 ug/L 2 08-OCT-19 Dichlorodifluoromethane <2.0 ug/L 2 08-OCT-19 Ethylbenzene <0.50 ug/L 0.5 08-OCT-19 n-Hexane <0.50 ug/L 0.5 08-OCT-19 m+p-Xylenes <0.40 ug/L 0.4 08-OCT-19 Methyl Ethyl Ketone <20 ug/L 20 08-OCT-19 Methyl Isobutyl Ketone <20 ug/L 20 08-OCT-19 Methylene Chloride <5.0 ug/L 5 08-OCT-19 MTBE <2.0 ug/L 2 08-OCT-19 o-Xylene <0.30 ug/L 0.3 08-OCT-19 Styrene <0.50 ug/L 0.5 08-OCT-19 Tetrachloroethylene <0.50 ug/L 0.5 08-OCT-19 Toluene <0.50 ug/L 0.5 08-OCT-19 trans-1,2-Dichloroethylene <0.50 ug/L 0.5 08-OCT-19 trans-1,3-Dichloropropene <0.30 ug/L 0.3 08-OCT-19 Trichloroethylene <0.50 ug/L 0.5 08-OCT-19 Trichlorofluoromethane <5.0 ug/L 5 08-OCT-19 Vinyl chloride <0.50 ug/L 0.5 08-OCT-19 Surrogate: 1,4-Difluorobenzene 99.2 % 70-130 08-OCT-19 Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 9 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4861166 WG3183541-2 MB Surrogate: 4-Bromofluorobenzene 96.8 % 70-130 08-OCT-19 WG3183541-5 MS WG3183541-3 1,1,1,2-Tetrachloroethane 103.0 % 50-140 08-OCT-19 1,1,2,2-Tetrachloroethane 101.0 % 50-140 08-OCT-19 1,1,1-Trichloroethane 96.4 % 50-140 08-OCT-19 1,1,2-Trichloroethane 95.0 % 50-140 08-OCT-19 1,1-Dichloroethane 103.6 % 50-140 08-OCT-19 1,1-Dichloroethylene 94.2 % 50-140 08-OCT-19 1,2-Dibromoethane 92.7 % 50-140 08-OCT-19 1,2-Dichlorobenzene 102.1 % 50-140 08-OCT-19 1,2-Dichloroethane 94.4 % 50-140 08-OCT-19 1,2-Dichloropropane 102.1 % 50-140 08-OCT-19 1,3-Dichlorobenzene 94.6 % 50-140 08-OCT-19 1,4-Dichlorobenzene 94.5 % 50-140 08-OCT-19 Acetone 97.6 % 50-140 08-OCT-19 Benzene 105.9 % 50-140 08-OCT-19 Bromodichloromethane 99.4 % 50-140 08-OCT-19 Bromoform 98.7 % 50-140 08-OCT-19 Bromomethane 90.9 % 50-140 08-OCT-19 Carbon tetrachloride 96.4 % 50-140 08-OCT-19 Chlorobenzene 102.2 % 50-140 08-OCT-19 Chloroform 103.3 % 50-140 08-OCT-19 cis-1,2-Dichloroethylene 99.3 % 50-140 08-OCT-19 cis-1,3-Dichloropropene 99.0 % 50-140 08-OCT-19 Dibromochloromethane 96.3 % 50-140 08-OCT-19 Dichlorodifluoromethane 116.0 % 50-140 08-OCT-19 Ethylbenzene 95.6 % 50-140 08-OCT-19 n-Hexane 91.4 % 50-140 08-OCT-19 m+p-Xylenes 95.4 % 50-140 08-OCT-19 Methyl Ethyl Ketone 90.6 % 50-140 08-OCT-19 Methyl Isobutyl Ketone 92.5 % 50-140 08-OCT-19 Methylene Chloride 97.7 % 50-140 08-OCT-19 MTBE 103.9 % 50-140 08-OCT-19 o-Xylene 95.7 % 50-140 08-OCT-19 Quality Control Report
Workorder: L2359740 Report Date: 17-OCT-19 Page 10 of 11
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4861166 WG3183541-5 MS WG3183541-3 Styrene 101.6 % 50-140 08-OCT-19 Tetrachloroethylene 94.8 % 50-140 08-OCT-19 Toluene 96.8 % 50-140 08-OCT-19 trans-1,2-Dichloroethylene 94.8 % 50-140 08-OCT-19 trans-1,3-Dichloropropene 97.9 % 50-140 08-OCT-19 Trichloroethylene 96.7 % 50-140 08-OCT-19 Trichlorofluoromethane 97.2 % 50-140 08-OCT-19 Vinyl chloride 113.9 % 50-140 08-OCT-19 Quality Control Report Workorder: L2359740 Report Date: 17-OCT-19
Client: Morrison Hershfield Limited (Ottawa) Page 11 of 11 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Cindy Zhao
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description MS-B Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order. ALS Sample ID: L2359740-1 Client Sample ID: BH1 500
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Printed on 10/9/2019 10:43:13 PM ALS Sample ID: L2359740-2 Client Sample ID: BH2 500
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Printed on 10/8/2019 8:07:07 PM ALS Sample ID: L2359740-3 Client Sample ID: BH3 500
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Printed on 10/8/2019 8:07:09 PM ALS Sample ID: L2359740-4 Client Sample ID: BH4 500
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Printed on 10/8/2019 8:07:12 PM ALS Sample ID: L2359740-5 Client Sample ID: BH21 500
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Printed on 10/8/2019 8:07:14 PM
Morrison Hershfield Limited (Ottawa) Date Received: 02-DEC-19 ATTN: Mitchell Dawley Report Date: 10-DEC-19 14:07 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2390921 Project P.O. #: 20102333 Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2390921 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 17 190441800 10-DEC-19 14:07 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2390921-1 BH5 SA2 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 15.9 0.25 % 04-DEC-19 Metals Antimony (Sb) 1.7 1.0 ug/g 04-DEC-19 *1 *1.3 *1.3 Arsenic (As) 3.6 1.0 ug/g 04-DEC-19 11 18 18 Barium (Ba) 149 1.0 ug/g 04-DEC-19 210 220 220 Beryllium (Be) 0.69 0.50 ug/g 04-DEC-19 2.5 2.5 2.5 Boron (B) 9.3 5.0 ug/g 04-DEC-19 36 36 36 Boron (B), Hot Water Ext. 0.25 0.10 ug/g 10-DEC-19 36 36 1.5 Cadmium (Cd) <0.50 0.50 ug/g 04-DEC-19 1 1.2 1.2 Chromium (Cr) 30.9 1.0 ug/g 04-DEC-19 67 70 70 Cobalt (Co) 9.1 1.0 ug/g 04-DEC-19 19 21 22 Copper (Cu) 34.0 1.0 ug/g 04-DEC-19 62 92 92 Lead (Pb) 100 1.0 ug/g 04-DEC-19 *45 120 120 Mercury (Hg) 0.124 0.0050 ug/g 10-DEC-19 0.16 0.27 0.27 Molybdenum (Mo) <1.0 1.0 ug/g 04-DEC-19 2 2 2 Nickel (Ni) 21.2 1.0 ug/g 04-DEC-19 37 82 82 Selenium (Se) <1.0 1.0 ug/g 04-DEC-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-DEC-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-DEC-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-DEC-19 1.9 2.5 2.5 Vanadium (V) 45.5 1.0 ug/g 04-DEC-19 86 86 86 Zinc (Zn) 157 5.0 ug/g 04-DEC-19 290 290 290 Speciated Metals Chromium, Hexavalent 0.48 0.20 ug/g 10-DEC-19 0.66 0.66 0.66 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 05-DEC-19 0.05 0.072 0.072 Acenaphthylene <0.050 0.050 ug/g 05-DEC-19 0.093 0.093 0.093 Anthracene 0.082 0.050 ug/g 05-DEC-19 *0.05 0.16 0.22 Benzo(a)anthracene 0.217 0.050 ug/g 05-DEC-19 *0.095 0.36 0.36 Benzo(a)pyrene 0.203 0.050 ug/g 05-DEC-19 *0.05 0.3 0.3 Benzo(b)fluoranthene 0.297 0.050 ug/g 05-DEC-19 0.3 0.47 0.47 Benzo(g,h,i)perylene 0.138 0.050 ug/g 05-DEC-19 0.2 0.68 0.68 Benzo(k)fluoranthene 0.061 0.050 ug/g 05-DEC-19 *0.05 0.48 0.48 Chrysene 0.238 0.050 ug/g 05-DEC-19 *0.18 2.8 2.8 Dibenzo(ah)anthracene <0.050 0.050 ug/g 05-DEC-19 0.1 0.1 0.1 Fluoranthene 0.459 0.050 ug/g 05-DEC-19 *0.24 0.56 0.69 Fluorene <0.050 0.050 ug/g 05-DEC-19 0.05 0.12 0.19 Indeno(1,2,3-cd)pyrene 0.124 0.050 ug/g 05-DEC-19 *0.11 0.23 0.23 1+2-Methylnaphthalenes <0.042 0.042 ug/g 05-DEC-19 0.05 0.59 0.59 1-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 2-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 Naphthalene 0.032 0.013 ug/g 05-DEC-19 0.05 0.09 0.09 Phenanthrene 0.348 0.046 ug/g 05-DEC-19 *0.19 0.69 0.69 Pyrene 0.384 0.050 ug/g 05-DEC-19 *0.19 1 1 Surrogate: 2-Fluorobiphenyl 100.5 50-140 % 05-DEC-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use L2390921 CONTD.... ANALYTICAL GUIDELINE REPORT Page 3 of 17 190441800 10-DEC-19 14:07 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2390921-1 BH5 SA2 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Surrogate: p-Terphenyl d14 98.4 50-140 % 05-DEC-19
L2390921-2 BH5 SA6 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 8.31 0.25 % 04-DEC-19 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Benzene <0.0068 0.0068 ug/g 06-DEC-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromoform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 06-DEC-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 06-DEC-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 06-DEC-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 06-DEC-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 06-DEC-19 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T9-Soil-Res/Park/Inst/Ind/Com/Commu Property Use L2390921 CONTD.... ANALYTICAL GUIDELINE REPORT Page 4 of 17 190441800 10-DEC-19 14:07 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2390921-2 BH5 SA6 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 06-DEC-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 06-DEC-19 m+p-Xylenes <0.030 0.030 ug/g 06-DEC-19 Xylenes (Total) <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 87.2 50-140 % 06-DEC-19 Surrogate: 1,4-Difluorobenzene 98.9 50-140 % 06-DEC-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 06-DEC-19 17 25 25 F1-BTEX <5.0 5.0 ug/g 06-DEC-19 17 25 25 F2 (C10-C16) <10 10 ug/g 05-DEC-19 10 10 10 F3 (C16-C34) <50 50 ug/g 05-DEC-19 240 240 240 F4 (C34-C50) <50 50 ug/g 05-DEC-19 120 120 120 Total Hydrocarbons (C6-C50) <72 72 ug/g 06-DEC-19 Chrom. to baseline at nC50 YES No Unit 05-DEC-19 Surrogate: 2-Bromobenzotrifluoride 92.9 60-140 % 05-DEC-19 Surrogate: 3,4-Dichlorotoluene 84.9 60-140 % 06-DEC-19
L2390921-3 BH5 SA12 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 15.5 0.25 % 04-DEC-19 Metals Antimony (Sb) 2.9 1.0 ug/g 04-DEC-19 *1 *1.3 *1.3 Arsenic (As) 3.4 1.0 ug/g 04-DEC-19 11 18 18 Barium (Ba) 151 1.0 ug/g 04-DEC-19 210 220 220 Beryllium (Be) 0.61 0.50 ug/g 04-DEC-19 2.5 2.5 2.5 Boron (B) 8.4 5.0 ug/g 04-DEC-19 36 36 36 Boron (B), Hot Water Ext. 0.24 0.10 ug/g 10-DEC-19 36 36 1.5 Cadmium (Cd) <0.50 0.50 ug/g 04-DEC-19 1 1.2 1.2 Chromium (Cr) 27.6 1.0 ug/g 04-DEC-19 67 70 70 Cobalt (Co) 8.0 1.0 ug/g 04-DEC-19 19 21 22 Copper (Cu) 32.1 1.0 ug/g 04-DEC-19 62 92 92 Lead (Pb) 117 1.0 ug/g 04-DEC-19 *45 120 120 Mercury (Hg) 0.223 0.0050 ug/g 10-DEC-19 *0.16 0.27 0.27 Molybdenum (Mo) <1.0 1.0 ug/g 04-DEC-19 2 2 2 Nickel (Ni) 17.5 1.0 ug/g 04-DEC-19 37 82 82 Selenium (Se) <1.0 1.0 ug/g 04-DEC-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-DEC-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-DEC-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-DEC-19 1.9 2.5 2.5 Vanadium (V) 39.9 1.0 ug/g 04-DEC-19 86 86 86 Zinc (Zn) 177 5.0 ug/g 04-DEC-19 290 290 290 Speciated Metals Chromium, Hexavalent 0.24 0.20 ug/g 10-DEC-19 0.66 0.66 0.66 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-3 BH5 SA12 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 05-DEC-19 0.05 0.072 0.072 Acenaphthylene <0.050 0.050 ug/g 05-DEC-19 0.093 0.093 0.093 Anthracene <0.050 0.050 ug/g 05-DEC-19 0.05 0.16 0.22 Benzo(a)anthracene 0.109 0.050 ug/g 05-DEC-19 *0.095 0.36 0.36 Benzo(a)pyrene 0.100 0.050 ug/g 05-DEC-19 *0.05 0.3 0.3 Benzo(b)fluoranthene 0.138 0.050 ug/g 05-DEC-19 0.3 0.47 0.47 Benzo(g,h,i)perylene 0.070 0.050 ug/g 05-DEC-19 0.2 0.68 0.68 Benzo(k)fluoranthene <0.050 0.050 ug/g 05-DEC-19 0.05 0.48 0.48 Chrysene 0.126 0.050 ug/g 05-DEC-19 0.18 2.8 2.8 Dibenzo(ah)anthracene <0.050 0.050 ug/g 05-DEC-19 0.1 0.1 0.1 Fluoranthene 0.212 0.050 ug/g 05-DEC-19 0.24 0.56 0.69 Fluorene <0.050 0.050 ug/g 05-DEC-19 0.05 0.12 0.19 Indeno(1,2,3-cd)pyrene 0.062 0.050 ug/g 05-DEC-19 0.11 0.23 0.23 1+2-Methylnaphthalenes <0.042 0.042 ug/g 05-DEC-19 0.05 0.59 0.59 1-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 2-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 Naphthalene <0.013 0.013 ug/g 05-DEC-19 0.05 0.09 0.09 Phenanthrene 0.106 0.046 ug/g 05-DEC-19 0.19 0.69 0.69 Pyrene 0.187 0.050 ug/g 05-DEC-19 0.19 1 1 Surrogate: 2-Fluorobiphenyl 95.7 50-140 % 05-DEC-19 Surrogate: p-Terphenyl d14 94.0 50-140 % 05-DEC-19
L2390921-4 BH6 SA6 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 37.1 0.25 % 04-DEC-19 Metals Antimony (Sb) <1.0 1.0 ug/g 04-DEC-19 1 1.3 1.3 Arsenic (As) 1.6 1.0 ug/g 04-DEC-19 11 18 18 Barium (Ba) 128 1.0 ug/g 04-DEC-19 210 220 220 Beryllium (Be) <0.50 0.50 ug/g 04-DEC-19 2.5 2.5 2.5 Boron (B) 5.7 5.0 ug/g 04-DEC-19 36 36 36 Boron (B), Hot Water Ext. 0.46 0.10 ug/g 10-DEC-19 36 36 1.5 Cadmium (Cd) <0.50 0.50 ug/g 04-DEC-19 1 1.2 1.2 Chromium (Cr) 41.2 1.0 ug/g 04-DEC-19 67 70 70 Cobalt (Co) 11.1 1.0 ug/g 04-DEC-19 19 21 22 Copper (Cu) 16.2 1.0 ug/g 04-DEC-19 62 92 92 Lead (Pb) 12.9 1.0 ug/g 04-DEC-19 45 120 120 Mercury (Hg) 0.0503 0.0050 ug/g 10-DEC-19 0.16 0.27 0.27 Molybdenum (Mo) <1.0 1.0 ug/g 04-DEC-19 2 2 2 Nickel (Ni) 23.8 1.0 ug/g 04-DEC-19 37 82 82 Selenium (Se) <1.0 1.0 ug/g 04-DEC-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-DEC-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-DEC-19 1 1 1
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-4 BH6 SA6 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Metals Uranium (U) <1.0 1.0 ug/g 04-DEC-19 1.9 2.5 2.5 Vanadium (V) 41.0 1.0 ug/g 04-DEC-19 86 86 86 Zinc (Zn) 71.6 5.0 ug/g 04-DEC-19 290 290 290 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 10-DEC-19 0.66 0.66 0.66 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Benzene 0.0106 0.0068 ug/g 06-DEC-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromoform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 06-DEC-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 06-DEC-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 06-DEC-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 06-DEC-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 06-DEC-19 0.02 0.02 0.02
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-4 BH6 SA6 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds o-Xylene <0.020 0.020 ug/g 06-DEC-19 m+p-Xylenes <0.030 0.030 ug/g 06-DEC-19 Xylenes (Total) <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 73.7 50-140 % 06-DEC-19 Surrogate: 1,4-Difluorobenzene 83.0 50-140 % 06-DEC-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 06-DEC-19 17 25 25 F1-BTEX <5.0 5.0 ug/g 06-DEC-19 17 25 25 F2 (C10-C16) <10 10 ug/g 05-DEC-19 10 10 10 F2-Naphth <10 10 ug/g 06-DEC-19 F3 (C16-C34) 130 50 ug/g 05-DEC-19 240 240 240 F3-PAH 125 50 ug/g 06-DEC-19 F4 (C34-C50) 133 50 ug/g 05-DEC-19 *120 *120 *120 F4G-SG (GHH-Silica) 550 250 ug/g 03-DEC-19 *120 *120 *120 Total Hydrocarbons (C6-C50) 262 72 ug/g 06-DEC-19 Chrom. to baseline at nC50 NO No Unit 05-DEC-19 Surrogate: 2-Bromobenzotrifluoride 94.0 60-140 % 05-DEC-19 Surrogate: 3,4-Dichlorotoluene 68.8 60-140 % 06-DEC-19 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.098 0.050 ug/g 05-DEC-19 *0.05 *0.072 *0.072 Acenaphthylene <0.050 0.050 ug/g 05-DEC-19 0.093 0.093 0.093 Anthracene 0.257 0.050 ug/g 05-DEC-19 *0.05 *0.16 *0.22 Benzo(a)anthracene 0.446 0.050 ug/g 05-DEC-19 *0.095 *0.36 *0.36 Benzo(a)pyrene 0.422 0.050 ug/g 05-DEC-19 *0.05 *0.3 *0.3 Benzo(b)fluoranthene 0.501 0.050 ug/g 05-DEC-19 *0.3 *0.47 *0.47 Benzo(g,h,i)perylene 0.279 0.050 ug/g 05-DEC-19 *0.2 0.68 0.68 Benzo(k)fluoranthene 0.183 0.050 ug/g 05-DEC-19 *0.05 0.48 0.48 Chrysene 0.442 0.050 ug/g 05-DEC-19 *0.18 2.8 2.8 Dibenzo(ah)anthracene 0.075 0.050 ug/g 05-DEC-19 0.1 0.1 0.1 Fluoranthene 1.03 0.050 ug/g 05-DEC-19 *0.24 *0.56 *0.69 Fluorene 0.135 0.050 ug/g 05-DEC-19 *0.05 *0.12 0.19 Indeno(1,2,3-cd)pyrene 0.264 0.050 ug/g 05-DEC-19 *0.11 *0.23 *0.23 1+2-Methylnaphthalenes <0.042 0.042 ug/g 05-DEC-19 0.05 0.59 0.59 1-Methylnaphthalene 0.035 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 2-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 Naphthalene 0.036 0.013 ug/g 05-DEC-19 0.05 0.09 0.09 Phenanthrene 0.748 0.046 ug/g 05-DEC-19 *0.19 *0.69 *0.69 Pyrene 0.865 0.050 ug/g 05-DEC-19 *0.19 1 1 Surrogate: 2-Fluorobiphenyl 91.9 50-140 % 05-DEC-19 Surrogate: p-Terphenyl d14 90.1 50-140 % 05-DEC-19
L2390921-5 BH6 SA16 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 38.1 0.25 % 04-DEC-19 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-5 BH6 SA16 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds Acetone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Benzene 0.0071 0.0068 ug/g 06-DEC-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromoform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 06-DEC-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 06-DEC-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 06-DEC-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 06-DEC-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 06-DEC-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 06-DEC-19 m+p-Xylenes <0.030 0.030 ug/g 06-DEC-19 Xylenes (Total) <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 76.1 50-140 % 06-DEC-19 Surrogate: 1,4-Difluorobenzene 86.1 50-140 % 06-DEC-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 06-DEC-19 17 25 25 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-5 BH6 SA16 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Hydrocarbons F1-BTEX <5.0 5.0 ug/g 06-DEC-19 17 25 25 F2 (C10-C16) <10 10 ug/g 05-DEC-19 10 10 10 F3 (C16-C34) 77 50 ug/g 05-DEC-19 240 240 240 F4 (C34-C50) 60 50 ug/g 05-DEC-19 120 120 120 Total Hydrocarbons (C6-C50) 137 72 ug/g 06-DEC-19 Chrom. to baseline at nC50 YES No Unit 05-DEC-19 Surrogate: 2-Bromobenzotrifluoride 90.5 60-140 % 05-DEC-19 Surrogate: 3,4-Dichlorotoluene 61.1 60-140 % 06-DEC-19
L2390921-6 BH7 SA1 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 11.6 0.25 % 04-DEC-19 Metals Antimony (Sb) <1.0 1.0 ug/g 04-DEC-19 1 1.3 1.3 Arsenic (As) 2.0 1.0 ug/g 04-DEC-19 11 18 18 Barium (Ba) 101 1.0 ug/g 04-DEC-19 210 220 220 Beryllium (Be) <0.50 0.50 ug/g 04-DEC-19 2.5 2.5 2.5 Boron (B) 7.0 5.0 ug/g 04-DEC-19 36 36 36 Boron (B), Hot Water Ext. 0.35 0.10 ug/g 10-DEC-19 36 36 1.5 Cadmium (Cd) <0.50 0.50 ug/g 04-DEC-19 1 1.2 1.2 Chromium (Cr) 22.2 1.0 ug/g 04-DEC-19 67 70 70 Cobalt (Co) 7.2 1.0 ug/g 04-DEC-19 19 21 22 Copper (Cu) 15.3 1.0 ug/g 04-DEC-19 62 92 92 Lead (Pb) 150 1.0 ug/g 04-DEC-19 *45 *120 *120 Mercury (Hg) 0.320 0.0050 ug/g 10-DEC-19 *0.16 *0.27 *0.27 Molybdenum (Mo) <1.0 1.0 ug/g 04-DEC-19 2 2 2 Nickel (Ni) 14.8 1.0 ug/g 04-DEC-19 37 82 82 Selenium (Se) <1.0 1.0 ug/g 04-DEC-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-DEC-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-DEC-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-DEC-19 1.9 2.5 2.5 Vanadium (V) 37.4 1.0 ug/g 04-DEC-19 86 86 86 Zinc (Zn) 169 5.0 ug/g 04-DEC-19 290 290 290 Speciated Metals Chromium, Hexavalent 0.59 0.20 ug/g 10-DEC-19 0.66 0.66 0.66 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 05-DEC-19 0.05 0.072 0.072 Acenaphthylene <0.050 0.050 ug/g 05-DEC-19 0.093 0.093 0.093 Anthracene <0.050 0.050 ug/g 05-DEC-19 0.05 0.16 0.22 Benzo(a)anthracene 0.082 0.050 ug/g 05-DEC-19 0.095 0.36 0.36 Benzo(a)pyrene 0.076 0.050 ug/g 05-DEC-19 *0.05 0.3 0.3 Benzo(b)fluoranthene 0.104 0.050 ug/g 05-DEC-19 0.3 0.47 0.47 Benzo(g,h,i)perylene 0.051 0.050 ug/g 05-DEC-19 0.2 0.68 0.68
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-6 BH7 SA1 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Benzo(k)fluoranthene <0.050 0.050 ug/g 05-DEC-19 0.05 0.48 0.48 Chrysene 0.095 0.050 ug/g 05-DEC-19 0.18 2.8 2.8 Dibenzo(ah)anthracene <0.050 0.050 ug/g 05-DEC-19 0.1 0.1 0.1 Fluoranthene 0.154 0.050 ug/g 05-DEC-19 0.24 0.56 0.69 Fluorene <0.050 0.050 ug/g 05-DEC-19 0.05 0.12 0.19 Indeno(1,2,3-cd)pyrene <0.050 0.050 ug/g 05-DEC-19 0.11 0.23 0.23 1+2-Methylnaphthalenes <0.042 0.042 ug/g 05-DEC-19 0.05 0.59 0.59 1-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 2-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 Naphthalene <0.013 0.013 ug/g 05-DEC-19 0.05 0.09 0.09 Phenanthrene 0.081 0.046 ug/g 05-DEC-19 0.19 0.69 0.69 Pyrene 0.139 0.050 ug/g 05-DEC-19 0.19 1 1 Surrogate: 2-Fluorobiphenyl 92.0 50-140 % 05-DEC-19 Surrogate: p-Terphenyl d14 87.3 50-140 % 05-DEC-19
L2390921-7 BH7 SA4 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 17.1 0.25 % 04-DEC-19 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Benzene <0.0068 0.0068 ug/g 06-DEC-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromoform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 06-DEC-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 06-DEC-19 0.05 0.05 0.05 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-7 BH7 SA4 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds n-Hexane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 06-DEC-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 06-DEC-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 06-DEC-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 06-DEC-19 m+p-Xylenes <0.030 0.030 ug/g 06-DEC-19 Xylenes (Total) <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 84.7 50-140 % 06-DEC-19 Surrogate: 1,4-Difluorobenzene 96.6 50-140 % 06-DEC-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 06-DEC-19 17 25 25 F1-BTEX <5.0 5.0 ug/g 06-DEC-19 17 25 25 F2 (C10-C16) 62 DLM 20 ug/g 05-DEC-19 *10 *10 *10 F3 (C16-C34) 870 DLM 100 ug/g 05-DEC-19 *240 *240 *240 F4 (C34-C50) 190 DLM 100 ug/g 05-DEC-19 *120 *120 *120 F4G-SG (GHH-Silica) 490 250 ug/g 03-DEC-19 *120 *120 *120 Total Hydrocarbons (C6-C50) 1120 140 ug/g 06-DEC-19 Chrom. to baseline at nC50 NO No Unit 05-DEC-19 Surrogate: 2-Bromobenzotrifluoride 99.6 60-140 % 05-DEC-19 Surrogate: 3,4-Dichlorotoluene 86.5 60-140 % 06-DEC-19
L2390921-8 BH8 SA1 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 14.1 0.25 % 04-DEC-19 Metals Antimony (Sb) 1.5 1.0 ug/g 04-DEC-19 *1 *1.3 *1.3 Arsenic (As) 12.5 1.0 ug/g 04-DEC-19 *11 18 18 Barium (Ba) 235 1.0 ug/g 04-DEC-19 *210 *220 *220 Beryllium (Be) 0.56 0.50 ug/g 04-DEC-19 2.5 2.5 2.5 Boron (B) 6.5 5.0 ug/g 04-DEC-19 36 36 36 Boron (B), Hot Water Ext. 0.36 0.10 ug/g 10-DEC-19 36 36 1.5 Cadmium (Cd) 1.20 0.50 ug/g 04-DEC-19 *1 1.2 1.2 Chromium (Cr) 27.9 1.0 ug/g 04-DEC-19 67 70 70 Cobalt (Co) 9.0 1.0 ug/g 04-DEC-19 19 21 22 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-8 BH8 SA1 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Metals Copper (Cu) 35.5 1.0 ug/g 04-DEC-19 62 92 92 Lead (Pb) 376 1.0 ug/g 04-DEC-19 *45 *120 *120 Mercury (Hg) 0.301 0.0050 ug/g 10-DEC-19 *0.16 *0.27 *0.27 Molybdenum (Mo) 2.3 1.0 ug/g 04-DEC-19 *2 *2 *2 Nickel (Ni) 19.8 1.0 ug/g 04-DEC-19 37 82 82 Selenium (Se) <1.0 1.0 ug/g 04-DEC-19 1.2 1.5 1.5 Silver (Ag) <0.20 0.20 ug/g 04-DEC-19 0.5 0.5 0.5 Thallium (Tl) <0.50 0.50 ug/g 04-DEC-19 1 1 1 Uranium (U) <1.0 1.0 ug/g 04-DEC-19 1.9 2.5 2.5 Vanadium (V) 35.3 1.0 ug/g 04-DEC-19 86 86 86 Zinc (Zn) 536 5.0 ug/g 04-DEC-19 *290 *290 *290 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 10-DEC-19 0.66 0.66 0.66 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 05-DEC-19 0.05 0.072 0.072 Acenaphthylene 0.061 0.050 ug/g 05-DEC-19 0.093 0.093 0.093 Anthracene 0.151 0.050 ug/g 05-DEC-19 *0.05 0.16 0.22 Benzo(a)anthracene 0.586 0.050 ug/g 05-DEC-19 *0.095 *0.36 *0.36 Benzo(a)pyrene 0.574 0.050 ug/g 05-DEC-19 *0.05 *0.3 *0.3 Benzo(b)fluoranthene 0.758 0.050 ug/g 05-DEC-19 *0.3 *0.47 *0.47 Benzo(g,h,i)perylene 0.390 0.050 ug/g 05-DEC-19 *0.2 0.68 0.68 Benzo(k)fluoranthene 0.277 0.050 ug/g 05-DEC-19 *0.05 0.48 0.48 Chrysene 0.685 0.050 ug/g 05-DEC-19 *0.18 2.8 2.8 Dibenzo(ah)anthracene 0.094 0.050 ug/g 05-DEC-19 0.1 0.1 0.1 Fluoranthene 1.33 0.050 ug/g 05-DEC-19 *0.24 *0.56 *0.69 Fluorene 0.059 0.050 ug/g 05-DEC-19 *0.05 0.12 0.19 Indeno(1,2,3-cd)pyrene 0.358 0.050 ug/g 05-DEC-19 *0.11 *0.23 *0.23 1+2-Methylnaphthalenes <0.042 0.042 ug/g 05-DEC-19 0.05 0.59 0.59 1-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 2-Methylnaphthalene <0.030 0.030 ug/g 05-DEC-19 0.05 0.59 0.59 Naphthalene 0.032 0.013 ug/g 05-DEC-19 0.05 0.09 0.09 Phenanthrene 0.726 0.046 ug/g 05-DEC-19 *0.19 *0.69 *0.69 Pyrene 1.12 0.050 ug/g 05-DEC-19 *0.19 *1 *1 Surrogate: 2-Fluorobiphenyl 94.6 50-140 % 05-DEC-19 Surrogate: p-Terphenyl d14 88.5 50-140 % 05-DEC-19
L2390921-9 BH8 SA3 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 12.4 0.25 % 04-DEC-19 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Benzene <0.0068 0.0068 ug/g 06-DEC-19 0.02 0.02 0.02 Bromodichloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-9 BH8 SA3 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds Bromoform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Bromomethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dibromochloromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Chloroform <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dibromoethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,3-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,4-Dichlorobenzene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Dichlorodifluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methylene Chloride <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,2-Dichloropropane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 cis-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 trans-1,3-Dichloropropene <0.030 0.030 ug/g 06-DEC-19 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 06-DEC-19 0.05 0.05 0.05 Ethylbenzene <0.018 0.018 ug/g 06-DEC-19 0.05 0.05 0.05 n-Hexane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Methyl Ethyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 Methyl Isobutyl Ketone <0.50 0.50 ug/g 06-DEC-19 0.5 0.5 0.5 MTBE <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Styrene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Toluene <0.080 0.080 ug/g 06-DEC-19 0.2 0.2 0.2 1,1,1-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 1,1,2-Trichloroethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 06-DEC-19 0.05 0.05 0.05 Trichlorofluoromethane <0.050 0.050 ug/g 06-DEC-19 0.05 0.25 0.25 Vinyl chloride <0.020 0.020 ug/g 06-DEC-19 0.02 0.02 0.02 o-Xylene <0.020 0.020 ug/g 06-DEC-19 m+p-Xylenes <0.030 0.030 ug/g 06-DEC-19 Xylenes (Total) <0.050 0.050 ug/g 06-DEC-19 0.05 0.05 0.05 Surrogate: 4-Bromofluorobenzene 85.5 50-140 % 06-DEC-19 Surrogate: 1,4-Difluorobenzene 97.7 50-140 % 06-DEC-19 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 06-DEC-19 17 25 25 F1-BTEX <5.0 5.0 ug/g 06-DEC-19 17 25 25 F2 (C10-C16) <10 10 ug/g 05-DEC-19 10 10 10 F3 (C16-C34) <50 50 ug/g 05-DEC-19 240 240 240 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2390921-9 BH8 SA3 Sampled By: CLIENT on 29-NOV-19 #1 #2 #3 Matrix: SOIL
Hydrocarbons F4 (C34-C50) 93 50 ug/g 05-DEC-19 120 120 120 Total Hydrocarbons (C6-C50) 93 72 ug/g 06-DEC-19 Chrom. to baseline at nC50 YES No Unit 05-DEC-19 Surrogate: 2-Bromobenzotrifluoride 92.0 60-140 % 05-DEC-19 Surrogate: 3,4-Dichlorotoluene 79.9 60-140 % 06-DEC-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-SOIL #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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Sample Parameter Qualifier key listed: Qualifier Description
DLM Detection Limit Adjusted due to sample matrix effects (e.g. chemical interference, colour, turbidity).
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
B-HWS-R511-WT Soil Boron-HWE-O.Reg 153/04 (July HW EXTR, EPA 6010B 2011)
A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). CR-CR6-IC-WT Soil Hexavalent Chromium in Soil SW846 3060A/7199
This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in a sulphuric acid solution.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
F1-F4-511-CALC-WT Soil F1-F4 Hydrocarbon Calculated CCME CWS-PHC, Pub #1310, Dec 2001-S Parameters
Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.
Hydrocarbon results are expressed on a dry weight basis.
In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines and the gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes has been subtracted from F1.
In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.
Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range: 1. All extraction and analysis holding times were met. 2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene. 3. Linearity of gasoline response within 15% throughout the calibration range.
Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges: 1. All extraction and analysis holding times were met. 2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average. 3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors. 4. Linearity of diesel or motor oil response within 15% throughout the calibration range. F1-HS-511-WT Soil F1-O.Reg 153/04 (July 2011) E3398/CCME TIER 1-HS
Fraction F1 is determined by extracting a soil or sediment sample as received with methanol, then analyzing by headspace-GC/FID.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). 190441800 L2390921 CONTD.... Page 16 of 17 10-DEC-19 14:07 (MT) Reference Information
F2-F4-511-WT Soil F2-F4-O.Reg 153/04 (July 2011) CCME Tier 1
Petroleum Hydrocarbons (F2-F4 fractions) are extracted from soil with 1:1 hexane:acetone using a rotary extractor. Extracts are treated with silica gel to remove polar organic interferences. F2, F3, & F4 are analyzed by GC-FID. F4G-sg is analyzed gravimetrically.
Notes: 1. F2 (C10-C16): Sum of all hydrocarbons that elute between nC10 and nC16. 2. F3 (C16-C34): Sum of all hydrocarbons that elute between nC16 and nC34. 3. F4 (C34-C50): Sum of all hydrocarbons that elute between nC34 and nC50. 4. F4G: Gravimetric Heavy Hydrocarbons 5. F4G-sg: Gravimetric Heavy Hydrocarbons (F4G) after silica gel treatment. 6. Where both F4 (C34-C50) and F4G-sg are reported for a sample, the larger of the two values is used for comparison against the relevant CCME guideline for F4. 7. F4G-sg cannot be added to the C6 to C50 hydrocarbon results to obtain an estimate of total extractable hydrocarbons. 8. This method is validated for use. 9. Data from analysis of validation and quality control samples is available upon request. 10. Reported results are expressed as milligrams per dry kilogram, unless otherwise indicated.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). F4G-ADD-511-WT Soil F4G SG-O.Reg 153/04 (July MOE DECPH-E3398/CCME TIER 1 2011) F4G, gravimetric analysis, is determined if the chromatogram does not return to baseline at or before C50. A soil sample is extracted with a solvent mix, the solvent is evaporated and the weight of the residue is determined.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). HG-200.2-CVAA-WT Soil Mercury in Soil by CVAAS EPA 200.2/1631E (mod)
Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
MET-200.2-CCMS-WT Soil Metals in Soil by CRC ICPMS EPA 200.2/6020A (mod)
Soil/sediment is dried, disaggregated, and sieved (2 mm). For tests intended to support Ontario regulations, the <2mm fraction is ground to pass through a 0.355 mm sieve. Strong Acid Leachable Metals in the <2mm fraction are solubilized by heated digestion with nitric and hydrochloric acids. Instrumental analysis is by Collision / Reaction Cell ICPMS.
Limitations: This method is intended to liberate environmentally available metals. Silicate minerals are not solubilized. Some metals may be only partially recovered (matrix dependent), including Al, Ba, Be, Cr, S, Sr, Ti, Tl, V, W, and Zr. Elemental Sulfur may be poorly recovered by this method. Volatile forms of sulfur (e.g. sulfide, H2S) may be excluded if lost during sampling, storage, or digestion.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). METHYLNAPS-CALC-WT Soil ABN-Calculated Parameters SW846 8270 MOISTURE-WT Soil % Moisture CCME PHC in Soil - Tier 1 (mod) PAH-511-WT Soil PAH-O.Reg 153/04 (July 2011) SW846 3510/8270
A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Results for benzo(b) fluoranthene may include contributions from benzo(j)fluoranthene, if also present in the sample.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). VOC-1,3-DCP-CALC-WT Soil Regulation 153 VOCs SW8260B/SW8270C VOC-511-HS-WT Soil VOC-O.Reg 153/04 (July 2011) SW846 8260 (511)
Soil and sediment samples are extracted in methanol and analyzed by headspace-GC/MS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). XYLENES-SUM-CALC- Soil Sum of Xylene Isomer CALCULATION WT Concentrations
Total xylenes represents the sum of o-xylene and m&p-xylene. 190441800 L2390921 CONTD.... Page 17 of 17 10-DEC-19 14:07 (MT) Reference Information
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 1 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
B-HWS-R511-WT Soil Batch R4940002 WG3239017-4 DUP L2392838-7 Boron (B), Hot Water Ext. 0.25 0.25 ug/g 0.3 30 10-DEC-19 WG3239017-2 IRM WT SAR3 Boron (B), Hot Water Ext. 102.7 % 70-130 10-DEC-19 WG3239017-3 LCS Boron (B), Hot Water Ext. 106.0 % 70-130 10-DEC-19 WG3239017-1 MB Boron (B), Hot Water Ext. <0.10 ug/g 0.1 10-DEC-19
CR-CR6-IC-WT Soil Batch R4939891 WG3238419-4 CRM WT-SQC012 Chromium, Hexavalent 88.3 % 70-130 10-DEC-19 WG3238419-3 DUP L2393796-1 Chromium, Hexavalent 0.32 0.29 ug/g 9.6 35 10-DEC-19 WG3238419-2 LCS Chromium, Hexavalent 97.0 % 80-120 10-DEC-19 WG3238419-1 MB Chromium, Hexavalent <0.20 ug/g 0.2 10-DEC-19
F1-HS-511-WT Soil Batch R4936320 WG3234484-4 DUP WG3234484-3 F1 (C6-C10) <5.0 <5.0 RPD-NA ug/g N/A 30 08-DEC-19 WG3234484-2 LCS F1 (C6-C10) 113.3 % 80-120 06-DEC-19 WG3234484-1 MB F1 (C6-C10) <5.0 ug/g 5 06-DEC-19 Surrogate: 3,4-Dichlorotoluene 96.1 % 60-140 06-DEC-19 WG3234484-6 MS L2390498-2 F1 (C6-C10) 108.9 % 60-140 06-DEC-19
F2-F4-511-WT Soil Batch R4932927 WG3233647-3 DUP WG3233647-5 F2 (C10-C16) <10 <10 RPD-NA ug/g N/A 30 03-DEC-19 F3 (C16-C34) <50 <50 RPD-NA ug/g N/A 30 03-DEC-19 F4 (C34-C50) <50 <50 RPD-NA ug/g N/A 30 03-DEC-19 WG3233647-2 LCS F2 (C10-C16) 101.9 % 80-120 03-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 2 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
F2-F4-511-WT Soil Batch R4932927 WG3233647-2 LCS F3 (C16-C34) 104.5 % 80-120 03-DEC-19 F4 (C34-C50) 106.0 % 80-120 03-DEC-19 WG3233647-1 MB F2 (C10-C16) <10 ug/g 10 03-DEC-19 F3 (C16-C34) <50 ug/g 50 03-DEC-19 F4 (C34-C50) <50 ug/g 50 03-DEC-19 Surrogate: 2-Bromobenzotrifluoride 89.3 % 60-140 03-DEC-19 WG3233647-4 MS WG3233647-5 F2 (C10-C16) 103.9 % 60-140 03-DEC-19 F3 (C16-C34) 106.1 % 60-140 03-DEC-19 F4 (C34-C50) 107.5 % 60-140 03-DEC-19
F4G-ADD-511-WT Soil Batch R4937440 WG3237968-2 LCS F4G-SG (GHH-Silica) 66.6 % 60-140 03-DEC-19 WG3237968-1 MB F4G-SG (GHH-Silica) <250 ug/g 250 03-DEC-19
HG-200.2-CVAA-WT Soil Batch R4939982 WG3238711-2 CRM WT-CANMET-TILL2 Mercury (Hg) 108.5 % 70-130 10-DEC-19 WG3238711-9 DUP WG3238711-8 Mercury (Hg) <0.0050 <0.0050 RPD-NA ug/g N/A 40 10-DEC-19 WG3238711-3 LCS Mercury (Hg) 117.5 % 80-120 10-DEC-19 WG3238711-1 MB Mercury (Hg) <0.0050 mg/kg 0.005 10-DEC-19
MET-200.2-CCMS-WT Soil Batch R4933890 WG3234498-9 CRM WT-CANMET-TILL2 Antimony (Sb) 86.4 % 70-130 04-DEC-19 Arsenic (As) 98.4 % 70-130 04-DEC-19 Barium (Ba) 94.6 % 70-130 04-DEC-19 Beryllium (Be) 94.3 % 70-130 04-DEC-19 Boron (B) 3.2 mg/kg 0-8.6 04-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 3 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R4933890 WG3234498-9 CRM WT-CANMET-TILL2 Cadmium (Cd) 100.0 % 70-130 04-DEC-19 Chromium (Cr) 95.7 % 70-130 04-DEC-19 Cobalt (Co) 95.8 % 70-130 04-DEC-19 Copper (Cu) 97.3 % 70-130 04-DEC-19 Lead (Pb) 98.6 % 70-130 04-DEC-19 Molybdenum (Mo) 96.0 % 70-130 04-DEC-19 Nickel (Ni) 98.5 % 70-130 04-DEC-19 Selenium (Se) 0.32 mg/kg 0.15-0.55 04-DEC-19 Silver (Ag) 0.26 mg/kg 0.16-0.36 04-DEC-19 Thallium (Tl) 97.8 % 70-130 04-DEC-19 Uranium (U) 95.5 % 70-130 04-DEC-19 Vanadium (V) 95.3 % 70-130 04-DEC-19 Zinc (Zn) 95.7 % 70-130 04-DEC-19 WG3234498-11 DUP WG3234498-13 Antimony (Sb) 0.19 0.17 ug/g 11 30 04-DEC-19 Arsenic (As) 2.37 2.13 ug/g 11 30 04-DEC-19 Barium (Ba) 65.2 62.5 ug/g 4.3 40 04-DEC-19 Beryllium (Be) 0.16 0.15 ug/g 6.3 30 04-DEC-19 Boron (B) <5.0 <5.0 RPD-NA ug/g N/A 30 04-DEC-19 Cadmium (Cd) 0.176 0.179 ug/g 2.0 30 04-DEC-19 Chromium (Cr) 24.8 22.7 ug/g 8.7 30 04-DEC-19 Cobalt (Co) 5.16 4.72 ug/g 8.9 30 04-DEC-19 Copper (Cu) 29.1 27.1 ug/g 7.3 30 04-DEC-19 Lead (Pb) 32.1 30.3 ug/g 5.9 40 04-DEC-19 Molybdenum (Mo) 0.31 0.28 ug/g 9.3 40 04-DEC-19 Nickel (Ni) 12.0 11.2 ug/g 7.1 30 04-DEC-19 Selenium (Se) <0.20 <0.20 RPD-NA ug/g N/A 30 04-DEC-19 Silver (Ag) 0.13 0.12 ug/g 4.4 40 04-DEC-19 Thallium (Tl) 0.086 0.079 ug/g 8.8 30 04-DEC-19 Uranium (U) 0.654 0.593 ug/g 9.7 30 04-DEC-19 Vanadium (V) 29.1 26.2 ug/g 11 30 04-DEC-19 Zinc (Zn) 64.5 62.8 ug/g 2.7 30 04-DEC-19 WG3234498-10 LCS Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 4 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R4933890 WG3234498-10 LCS Antimony (Sb) 101.5 % 80-120 04-DEC-19 Arsenic (As) 97.5 % 80-120 04-DEC-19 Barium (Ba) 98.9 % 80-120 04-DEC-19 Beryllium (Be) 98.6 % 80-120 04-DEC-19 Boron (B) 93.1 % 80-120 04-DEC-19 Cadmium (Cd) 95.5 % 80-120 04-DEC-19 Chromium (Cr) 99.99 % 80-120 04-DEC-19 Cobalt (Co) 97.4 % 80-120 04-DEC-19 Copper (Cu) 97.1 % 80-120 04-DEC-19 Lead (Pb) 95.8 % 80-120 04-DEC-19 Molybdenum (Mo) 100.1 % 80-120 04-DEC-19 Nickel (Ni) 97.6 % 80-120 04-DEC-19 Selenium (Se) 92.3 % 80-120 04-DEC-19 Silver (Ag) 97.3 % 80-120 04-DEC-19 Thallium (Tl) 95.7 % 80-120 04-DEC-19 Uranium (U) 94.1 % 80-120 04-DEC-19 Vanadium (V) 101.9 % 80-120 04-DEC-19 Zinc (Zn) 94.7 % 80-120 04-DEC-19 WG3234498-8 MB Antimony (Sb) <0.10 mg/kg 0.1 04-DEC-19 Arsenic (As) <0.10 mg/kg 0.1 04-DEC-19 Barium (Ba) <0.50 mg/kg 0.5 04-DEC-19 Beryllium (Be) <0.10 mg/kg 0.1 04-DEC-19 Boron (B) <5.0 mg/kg 5 04-DEC-19 Cadmium (Cd) <0.020 mg/kg 0.02 04-DEC-19 Chromium (Cr) <0.50 mg/kg 0.5 04-DEC-19 Cobalt (Co) <0.10 mg/kg 0.1 04-DEC-19 Copper (Cu) <0.50 mg/kg 0.5 04-DEC-19 Lead (Pb) <0.50 mg/kg 0.5 04-DEC-19 Molybdenum (Mo) <0.10 mg/kg 0.1 04-DEC-19 Nickel (Ni) <0.50 mg/kg 0.5 04-DEC-19 Selenium (Se) <0.20 mg/kg 0.2 04-DEC-19 Silver (Ag) <0.10 mg/kg 0.1 04-DEC-19 Thallium (Tl) <0.050 mg/kg 0.05 04-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 5 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R4933890 WG3234498-8 MB Uranium (U) <0.050 mg/kg 0.05 04-DEC-19 Vanadium (V) <0.20 mg/kg 0.2 04-DEC-19 Zinc (Zn) <2.0 mg/kg 2 04-DEC-19
MOISTURE-WT Soil Batch R4932008 WG3234067-3 DUP L2390921-4 % Moisture 37.1 37.5 % 1.1 20 04-DEC-19 WG3234067-2 LCS % Moisture 100.4 % 90-110 04-DEC-19 WG3234067-1 MB % Moisture <0.25 % 0.25 04-DEC-19
PAH-511-WT Soil Batch R4935889 WG3234012-3 DUP WG3234012-5 1-Methylnaphthalene <0.030 <0.030 RPD-NA ug/g N/A 40 05-DEC-19 2-Methylnaphthalene <0.030 <0.030 RPD-NA ug/g N/A 40 05-DEC-19 Acenaphthene <0.050 <0.050 RPD-NA ug/g N/A 40 05-DEC-19 Acenaphthylene <0.050 <0.050 RPD-NA ug/g N/A 40 05-DEC-19 Anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 05-DEC-19 Benzo(a)anthracene <0.050 0.092 RPD-NA ug/g N/A 40 05-DEC-19 Benzo(a)pyrene <0.050 0.071 RPD-NA ug/g N/A 40 05-DEC-19 Benzo(b)fluoranthene <0.050 0.100 RPD-NA ug/g N/A 40 05-DEC-19 Benzo(g,h,i)perylene <0.050 <0.050 RPD-NA ug/g N/A 40 05-DEC-19 Benzo(k)fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 05-DEC-19 Chrysene <0.050 0.089 RPD-NA ug/g N/A 40 05-DEC-19 Dibenzo(ah)anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 05-DEC-19 Fluoranthene 0.065 0.169 DUP-H,J ug/g 0.103 0.1 05-DEC-19 Fluorene <0.050 <0.050 RPD-NA ug/g N/A 40 05-DEC-19 Indeno(1,2,3-cd)pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 05-DEC-19 Naphthalene <0.013 <0.013 RPD-NA ug/g N/A 40 05-DEC-19 Phenanthrene <0.046 0.052 RPD-NA ug/g N/A 40 05-DEC-19 Pyrene 0.058 0.143 J ug/g 0.085 0.1 05-DEC-19 WG3234012-2 LCS 1-Methylnaphthalene 93.6 % 50-140 05-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 6 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R4935889 WG3234012-2 LCS 2-Methylnaphthalene 88.0 % 50-140 05-DEC-19 Acenaphthene 96.0 % 50-140 05-DEC-19 Acenaphthylene 94.4 % 50-140 05-DEC-19 Anthracene 95.4 % 50-140 05-DEC-19 Benzo(a)anthracene 96.6 % 50-140 05-DEC-19 Benzo(a)pyrene 96.3 % 50-140 05-DEC-19 Benzo(b)fluoranthene 94.2 % 50-140 05-DEC-19 Benzo(g,h,i)perylene 87.4 % 50-140 05-DEC-19 Benzo(k)fluoranthene 102.5 % 50-140 05-DEC-19 Chrysene 112.1 % 50-140 05-DEC-19 Dibenzo(ah)anthracene 89.8 % 50-140 05-DEC-19 Fluoranthene 95.1 % 50-140 05-DEC-19 Fluorene 95.4 % 50-140 05-DEC-19 Indeno(1,2,3-cd)pyrene 87.1 % 50-140 05-DEC-19 Naphthalene 91.3 % 50-140 05-DEC-19 Phenanthrene 97.7 % 50-140 05-DEC-19 Pyrene 96.3 % 50-140 05-DEC-19 WG3234012-1 MB 1-Methylnaphthalene <0.030 ug/g 0.03 05-DEC-19 2-Methylnaphthalene <0.030 ug/g 0.03 05-DEC-19 Acenaphthene <0.050 ug/g 0.05 05-DEC-19 Acenaphthylene <0.050 ug/g 0.05 05-DEC-19 Anthracene <0.050 ug/g 0.05 05-DEC-19 Benzo(a)anthracene <0.050 ug/g 0.05 05-DEC-19 Benzo(a)pyrene <0.050 ug/g 0.05 05-DEC-19 Benzo(b)fluoranthene <0.050 ug/g 0.05 05-DEC-19 Benzo(g,h,i)perylene <0.050 ug/g 0.05 05-DEC-19 Benzo(k)fluoranthene <0.050 ug/g 0.05 05-DEC-19 Chrysene <0.050 ug/g 0.05 05-DEC-19 Dibenzo(ah)anthracene <0.050 ug/g 0.05 05-DEC-19 Fluoranthene <0.050 ug/g 0.05 05-DEC-19 Fluorene <0.050 ug/g 0.05 05-DEC-19 Indeno(1,2,3-cd)pyrene <0.050 ug/g 0.05 05-DEC-19 Naphthalene <0.013 ug/g 0.013 05-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 7 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R4935889 WG3234012-1 MB Phenanthrene <0.046 ug/g 0.046 05-DEC-19 Pyrene <0.050 ug/g 0.05 05-DEC-19 Surrogate: 2-Fluorobiphenyl 96.0 % 50-140 05-DEC-19 Surrogate: p-Terphenyl d14 87.3 % 50-140 05-DEC-19 WG3234012-4 MS WG3234012-5 1-Methylnaphthalene 92.7 % 50-140 05-DEC-19 2-Methylnaphthalene 87.6 % 50-140 05-DEC-19 Acenaphthene 95.1 % 50-140 05-DEC-19 Acenaphthylene 93.6 % 50-140 05-DEC-19 Anthracene 97.0 % 50-140 05-DEC-19 Benzo(a)anthracene 99.3 % 50-140 05-DEC-19 Benzo(a)pyrene 94.1 % 50-140 05-DEC-19 Benzo(b)fluoranthene 96.3 % 50-140 05-DEC-19 Benzo(g,h,i)perylene 92.4 % 50-140 05-DEC-19 Benzo(k)fluoranthene 98.8 % 50-140 05-DEC-19 Chrysene 112.0 % 50-140 05-DEC-19 Dibenzo(ah)anthracene 96.1 % 50-140 05-DEC-19 Fluoranthene 96.4 % 50-140 05-DEC-19 Fluorene 93.8 % 50-140 05-DEC-19 Indeno(1,2,3-cd)pyrene 95.5 % 50-140 05-DEC-19 Naphthalene 90.5 % 50-140 05-DEC-19 Phenanthrene 99.3 % 50-140 05-DEC-19 Pyrene 96.7 % 50-140 05-DEC-19
VOC-511-HS-WT Soil Batch R4936320 WG3234484-4 DUP WG3234484-3 1,1,1,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,1,2,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,1,1-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,1,2-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,1-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,1-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,2-Dibromoethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,2-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 8 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4936320 WG3234484-4 DUP WG3234484-3 1,2-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,2-Dichloropropane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,3-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 1,4-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Acetone <0.50 <0.50 RPD-NA ug/g N/A 40 08-DEC-19 Benzene <0.0068 <0.0068 RPD-NA ug/g N/A 40 08-DEC-19 Bromodichloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Bromoform <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Bromomethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Carbon tetrachloride <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Chlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Chloroform <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 cis-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 cis-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 08-DEC-19 Dibromochloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Dichlorodifluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Ethylbenzene <0.018 <0.018 RPD-NA ug/g N/A 40 08-DEC-19 n-Hexane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Methylene Chloride <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 MTBE <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 m+p-Xylenes <0.030 <0.030 RPD-NA ug/g N/A 40 08-DEC-19 Methyl Ethyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 08-DEC-19 Methyl Isobutyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 08-DEC-19 o-Xylene <0.020 <0.020 RPD-NA ug/g N/A 40 08-DEC-19 Styrene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Tetrachloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Toluene <0.080 <0.080 RPD-NA ug/g N/A 40 08-DEC-19 trans-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 trans-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 08-DEC-19 Trichloroethylene <0.010 <0.010 RPD-NA ug/g N/A 40 08-DEC-19 Trichlorofluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 08-DEC-19 Vinyl chloride <0.020 <0.020 RPD-NA ug/g N/A 40 08-DEC-19 WG3234484-2 LCS Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 9 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4936320 WG3234484-2 LCS 1,1,1,2-Tetrachloroethane 90.4 % 60-130 06-DEC-19 1,1,2,2-Tetrachloroethane 97.2 % 60-130 06-DEC-19 1,1,1-Trichloroethane 100.1 % 60-130 06-DEC-19 1,1,2-Trichloroethane 95.4 % 60-130 06-DEC-19 1,1-Dichloroethane 100.3 % 60-130 06-DEC-19 1,1-Dichloroethylene 97.0 % 60-130 06-DEC-19 1,2-Dibromoethane 95.2 % 70-130 06-DEC-19 1,2-Dichlorobenzene 93.3 % 70-130 06-DEC-19 1,2-Dichloroethane 99.5 % 60-130 06-DEC-19 1,2-Dichloropropane 95.7 % 70-130 06-DEC-19 1,3-Dichlorobenzene 94.7 % 70-130 06-DEC-19 1,4-Dichlorobenzene 95.2 % 70-130 06-DEC-19 Acetone 98.7 % 60-140 06-DEC-19 Benzene 102.4 % 70-130 06-DEC-19 Bromodichloromethane 100.5 % 50-140 06-DEC-19 Bromoform 98.2 % 70-130 06-DEC-19 Bromomethane 93.2 % 50-140 06-DEC-19 Carbon tetrachloride 94.6 % 70-130 06-DEC-19 Chlorobenzene 90.6 % 70-130 06-DEC-19 Chloroform 101.2 % 70-130 06-DEC-19 cis-1,2-Dichloroethylene 98.3 % 70-130 06-DEC-19 cis-1,3-Dichloropropene 107.3 % 70-130 06-DEC-19 Dibromochloromethane 94.7 % 60-130 06-DEC-19 Dichlorodifluoromethane 80.6 % 50-140 06-DEC-19 Ethylbenzene 90.8 % 70-130 06-DEC-19 n-Hexane 87.1 % 70-130 06-DEC-19 Methylene Chloride 99.1 % 70-130 06-DEC-19 MTBE 99.6 % 70-130 06-DEC-19 m+p-Xylenes 91.4 % 70-130 06-DEC-19 Methyl Ethyl Ketone 98.5 % 60-140 06-DEC-19 Methyl Isobutyl Ketone 99.2 % 60-140 06-DEC-19 o-Xylene 89.9 % 70-130 06-DEC-19 Styrene 91.1 % 70-130 06-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 10 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4936320 WG3234484-2 LCS Tetrachloroethylene 94.1 % 60-130 06-DEC-19 Toluene 91.1 % 70-130 06-DEC-19 trans-1,2-Dichloroethylene 94.4 % 60-130 06-DEC-19 trans-1,3-Dichloropropene 98.1 % 70-130 06-DEC-19 Trichloroethylene 101.3 % 60-130 06-DEC-19 Trichlorofluoromethane 97.2 % 50-140 06-DEC-19 Vinyl chloride 106.8 % 60-140 06-DEC-19 WG3234484-1 MB 1,1,1,2-Tetrachloroethane <0.050 ug/g 0.05 06-DEC-19 1,1,2,2-Tetrachloroethane <0.050 ug/g 0.05 06-DEC-19 1,1,1-Trichloroethane <0.050 ug/g 0.05 06-DEC-19 1,1,2-Trichloroethane <0.050 ug/g 0.05 06-DEC-19 1,1-Dichloroethane <0.050 ug/g 0.05 06-DEC-19 1,1-Dichloroethylene <0.050 ug/g 0.05 06-DEC-19 1,2-Dibromoethane <0.050 ug/g 0.05 06-DEC-19 1,2-Dichlorobenzene <0.050 ug/g 0.05 06-DEC-19 1,2-Dichloroethane <0.050 ug/g 0.05 06-DEC-19 1,2-Dichloropropane <0.050 ug/g 0.05 06-DEC-19 1,3-Dichlorobenzene <0.050 ug/g 0.05 06-DEC-19 1,4-Dichlorobenzene <0.050 ug/g 0.05 06-DEC-19 Acetone <0.50 ug/g 0.5 06-DEC-19 Benzene <0.0068 ug/g 0.0068 06-DEC-19 Bromodichloromethane <0.050 ug/g 0.05 06-DEC-19 Bromoform <0.050 ug/g 0.05 06-DEC-19 Bromomethane <0.050 ug/g 0.05 06-DEC-19 Carbon tetrachloride <0.050 ug/g 0.05 06-DEC-19 Chlorobenzene <0.050 ug/g 0.05 06-DEC-19 Chloroform <0.050 ug/g 0.05 06-DEC-19 cis-1,2-Dichloroethylene <0.050 ug/g 0.05 06-DEC-19 cis-1,3-Dichloropropene <0.030 ug/g 0.03 06-DEC-19 Dibromochloromethane <0.050 ug/g 0.05 06-DEC-19 Dichlorodifluoromethane <0.050 ug/g 0.05 06-DEC-19 Ethylbenzene <0.018 ug/g 0.018 06-DEC-19 n-Hexane <0.050 ug/g 0.05 06-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 11 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4936320 WG3234484-1 MB Methylene Chloride <0.050 ug/g 0.05 06-DEC-19 MTBE <0.050 ug/g 0.05 06-DEC-19 m+p-Xylenes <0.030 ug/g 0.03 06-DEC-19 Methyl Ethyl Ketone <0.50 ug/g 0.5 06-DEC-19 Methyl Isobutyl Ketone <0.50 ug/g 0.5 06-DEC-19 o-Xylene <0.020 ug/g 0.02 06-DEC-19 Styrene <0.050 ug/g 0.05 06-DEC-19 Tetrachloroethylene <0.050 ug/g 0.05 06-DEC-19 Toluene <0.080 ug/g 0.08 06-DEC-19 trans-1,2-Dichloroethylene <0.050 ug/g 0.05 06-DEC-19 trans-1,3-Dichloropropene <0.030 ug/g 0.03 06-DEC-19 Trichloroethylene <0.010 ug/g 0.01 06-DEC-19 Trichlorofluoromethane <0.050 ug/g 0.05 06-DEC-19 Vinyl chloride <0.020 ug/g 0.02 06-DEC-19 Surrogate: 1,4-Difluorobenzene 109.9 % 50-140 06-DEC-19 Surrogate: 4-Bromofluorobenzene 96.7 % 50-140 06-DEC-19 WG3234484-5 MS L2390498-1 1,1,1,2-Tetrachloroethane 93.3 % 50-140 08-DEC-19 1,1,2,2-Tetrachloroethane 92.9 % 50-140 08-DEC-19 1,1,1-Trichloroethane 99.8 % 50-140 08-DEC-19 1,1,2-Trichloroethane 96.9 % 50-140 08-DEC-19 1,1-Dichloroethane 96.9 % 50-140 08-DEC-19 1,1-Dichloroethylene 98.2 % 50-140 08-DEC-19 1,2-Dibromoethane 96.7 % 50-140 08-DEC-19 1,2-Dichlorobenzene 92.0 % 50-140 08-DEC-19 1,2-Dichloroethane 96.8 % 50-140 08-DEC-19 1,2-Dichloropropane 97.9 % 50-140 08-DEC-19 1,3-Dichlorobenzene 98.0 % 50-140 08-DEC-19 1,4-Dichlorobenzene 97.5 % 50-140 08-DEC-19 Acetone 101.6 % 50-140 08-DEC-19 Benzene 102.2 % 50-140 08-DEC-19 Bromodichloromethane 95.3 % 50-140 08-DEC-19 Bromoform 96.3 % 50-140 08-DEC-19 Bromomethane 88.5 % 50-140 08-DEC-19 Quality Control Report
Workorder: L2390921 Report Date: 10-DEC-19 Page 12 of 13
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R4936320 WG3234484-5 MS L2390498-1 Carbon tetrachloride 100.3 % 50-140 08-DEC-19 Chlorobenzene 92.1 % 50-140 08-DEC-19 Chloroform 94.8 % 50-140 08-DEC-19 cis-1,2-Dichloroethylene 99.2 % 50-140 08-DEC-19 cis-1,3-Dichloropropene 99.3 % 50-140 08-DEC-19 Dibromochloromethane 95.0 % 50-140 08-DEC-19 Dichlorodifluoromethane 70.0 % 50-140 08-DEC-19 Ethylbenzene 99.5 % 50-140 08-DEC-19 n-Hexane 92.8 % 50-140 08-DEC-19 Methylene Chloride 90.3 % 50-140 08-DEC-19 MTBE 99.3 % 50-140 08-DEC-19 m+p-Xylenes 99.1 % 50-140 08-DEC-19 Methyl Ethyl Ketone 93.9 % 50-140 08-DEC-19 Methyl Isobutyl Ketone 99.3 % 50-140 08-DEC-19 o-Xylene 97.8 % 50-140 08-DEC-19 Styrene 96.8 % 50-140 08-DEC-19 Tetrachloroethylene 99.3 % 50-140 08-DEC-19 Toluene 101.2 % 50-140 08-DEC-19 trans-1,2-Dichloroethylene 98.6 % 50-140 08-DEC-19 trans-1,3-Dichloropropene 101.5 % 50-140 08-DEC-19 Trichloroethylene 97.9 % 50-140 08-DEC-19 Trichlorofluoromethane 97.4 % 50-140 08-DEC-19 Vinyl chloride 103.9 % 50-140 08-DEC-19 Quality Control Report Workorder: L2390921 Report Date: 10-DEC-19
Client: Morrison Hershfield Limited (Ottawa) Page 13 of 13 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description DUP-H,J Duplicate results outside ALS DQO, due to sample heterogeneity. Duplicate results and limits are expressed in terms of absolute difference. J Duplicate results and limits are expressed in terms of absolute difference. RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order. ALS Sample ID: L2390921-2 Client Sample ID: BH5 SA6 500
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Printed on 12/6/2019 12:27:20 PM ALS Sample ID: L2390921-4 Client Sample ID: BH6 SA6 500
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Printed on 12/6/2019 12:27:34 PM ALS Sample ID: L2390921-9 Client Sample ID: BH8 SA3 500
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Morrison Hershfield Limited (Ottawa) Date Received: 02-DEC-19 ATTN: Mitchell Dawley Report Date: 09-DEC-19 14:58 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2390935 Project P.O. #: 20102333 Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2390935 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 4 190441800 09-DEC-19 14:58 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2390935-1 TCLP-HK Sampled By: CLIENT on 29-NOV-19 #1 #2 Matrix: SOIL
Sample Preparation Initial pH 8.48 0.10 pH units 05-DEC-19 Final pH 6.17 0.10 pH units 05-DEC-19 TCLP Extractables Acenaphthene <0.0050 0.0050 mg/L 09-DEC-19 Acenaphthylene <0.0050 0.0050 mg/L 09-DEC-19 Anthracene <0.0050 0.0050 mg/L 09-DEC-19 Benzo(a)anthracene <0.0050 0.0050 mg/L 09-DEC-19 Benzo(a)pyrene <0.0010 0.0010 mg/L 09-DEC-19 0.001 Benzo(b)fluoranthene <0.0050 0.0050 mg/L 09-DEC-19 Benzo(g,h,i)perylene <0.0050 0.0050 mg/L 09-DEC-19 TCLP Metals Arsenic (As) <0.050 0.050 mg/L 05-DEC-19 2.5 Barium (Ba) 0.78 0.50 mg/L 05-DEC-19 100 Boron (B) <2.5 2.5 mg/L 05-DEC-19 500 Cadmium (Cd) <0.0050 0.0050 mg/L 05-DEC-19 0.5 Chromium (Cr) <0.050 0.050 mg/L 05-DEC-19 5.0 Lead (Pb) <0.050 0.050 mg/L 05-DEC-19 5.0 Mercury (Hg) <0.00010 0.00010 mg/L 05-DEC-19 0.1 Selenium (Se) <0.025 0.025 mg/L 05-DEC-19 1.0 Silver (Ag) <0.0050 0.0050 mg/L 05-DEC-19 5.0 Uranium (U) <0.25 0.25 mg/L 05-DEC-19 10 TCLP VOCs 1,1-Dichloroethylene <0.025 0.025 mg/L 08-DEC-19 1.4 1,2-Dichlorobenzene <0.025 0.025 mg/L 08-DEC-19 20.0 1,2-Dichloroethane <0.025 0.025 mg/L 08-DEC-19 0.5 1,4-Dichlorobenzene <0.025 0.025 mg/L 08-DEC-19 0.5 Benzene <0.025 0.025 mg/L 08-DEC-19 0.5 Carbon tetrachloride <0.025 0.025 mg/L 08-DEC-19 0.5 Chlorobenzene <0.025 0.025 mg/L 08-DEC-19 8 Chloroform <0.10 0.10 mg/L 08-DEC-19 10 Dichloromethane <0.50 0.50 mg/L 08-DEC-19 5.0 Methyl Ethyl Ketone <1.0 1.0 mg/L 08-DEC-19 200.0 Tetrachloroethylene <0.025 0.025 mg/L 08-DEC-19 3 Trichloroethylene <0.025 0.025 mg/L 08-DEC-19 5 Vinyl chloride <0.050 0.050 mg/L 08-DEC-19 0.2 Surrogate: 4-Bromofluorobenzene 98.2 70-130 % 08-DEC-19 Volatile Organic Compounds Surrogate: 1,4-Difluorobenzene 100.9 70-130 % 08-DEC-19 Polycyclic Aromatic Hydrocarbons Benzo(k)fluoranthene <0.0050 0.0050 mg/L 09-DEC-19 Chrysene <0.0050 0.0050 mg/L 09-DEC-19 Dibenzo(ah)anthracene <0.0050 0.0050 mg/L 09-DEC-19 Fluoranthene <0.0050 0.0050 mg/L 09-DEC-19 Fluorene <0.0050 0.0050 mg/L 09-DEC-19 Indeno(1,2,3-cd)pyrene <0.0050 0.0050 mg/L 09-DEC-19 Naphthalene <0.0050 0.0050 mg/L 09-DEC-19 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Federal & Provincial Waste Regulations (MAR, 2008) = [Suite] - ON-REG347/90 - Schedule 4 Leachate + Bulk PCB #1: Ontario Ministry of the Environment, General Waste Control Regulation No. 347/90
#2: Polychlorinated Biphenyls (PCBs) - Ontario Regulation 347/90 L2390935 CONTD.... ANALYTICAL GUIDELINE REPORT Page 3 of 4 190441800 09-DEC-19 14:58 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2390935-1 TCLP-HK Sampled By: CLIENT on 29-NOV-19 #1 #2 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Phenanthrene <0.0050 0.0050 mg/L 09-DEC-19 Pyrene <0.0050 0.0050 mg/L 09-DEC-19 Quinoline <0.0050 0.0050 mg/L 09-DEC-19 Surrogate: d10-Acenaphthene 101.1 50-150 % 09-DEC-19 Surrogate: d12-Chrysene 104.7 50-150 % 09-DEC-19 Surrogate: d8-Naphthalene 99.3 50-150 % 09-DEC-19 Surrogate: d10-Phenanthrene 104.3 50-150 % 09-DEC-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Federal & Provincial Waste Regulations (MAR, 2008) = [Suite] - ON-REG347/90 - Schedule 4 Leachate + Bulk PCB #1: Ontario Ministry of the Environment, General Waste Control Regulation No. 347/90
#2: Polychlorinated Biphenyls (PCBs) - Ontario Regulation 347/90 190441800 L2390935 CONTD.... Page 4 of 4 09-DEC-19 14:58 (MT) Reference Information
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
HG-TCLP-WT Waste Mercury (CVAA) for O.Reg 347 EPA 1631E
This analysis is carried out in accordance with the extraction procedure outlined in "Test Methods for Evaluating Solid Waste - Physical/Chemical Methods Volume 1C" SW-846 EPA Method 1311, published by the United States Environmental Protection Agency (EPA). In summary, the sample is extracted at a 20:1 liquid to solids ratio for 16 to 20 hours using either extraction fluid #1 (glacial acetic acid, water and sodium hydroxide) or extraction fluid #2 (glacial acetic acid), depending on the pH of the original sample. The extract is then filtered through a 0.6 to 0.8 micron glass fibre filter and analysed using atomic absorption spectrophotometry (EPA 1631E). LEACH-TCLP-WT Waste Leachate Procedure for Reg 347 EPA 1311
Inorganic and Semi-Volatile Organic contaminants are leached from waste samples in strict accordance with US EPA Method 1311, "Toxicity Characteristic Leaching Procedure" (TCLP). Test results are reported in leachate concentration units (normally mg/L). MET-TCLP-WT Waste O.Reg 347 TCLP Leachable EPA 6020B Metals
This analysis is carried out in accordance with the extraction procedure outlined in "Test Methods for Evaluating Solid Waste - Physical/Chemical Methods Volume 1C" SW-846 EPA Method 1311, published by the United States Environmental Protection Agency (EPA). In summary, the sample is extracted at a 20:1 liquid to solids ratio for 16 to 20 hours using either extraction fluid #1 (glacial acetic acid, water and sodium hydroxide) or extraction fluid #2 (glacial acetic acid), depending on the pH of the original sample. The extract is then filtered through a 0.6 to 0.8 micron glass fibre filter. Instrumental analysis of the digested extract is by collision cell inductively coupled plasma - mass spectrometry (modifed from EPA Method 6020B). PAH-TCLP-WT Waste PAH for O. Reg 347 SW846 8270 (PAH)
Samples are leached according to TCLP protocol and then the aqueous leachate is extracted and the resulting extracts are analyzed on GC/MSD. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene. VOC-TCLP-WT Waste VOC for O. Reg 347 SW846 8260
A sample of waste is leached in a zero headspace extractor at 30–2 rpm for 18–2.0 hours with the appropriate leaching solution. After tumbling the leachate is analyzed directly by headspace technology, followed by GC/MS using internal standard quantitation.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA
GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2390935 Report Date: 09-DEC-19 Page 1 of 7
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
HG-TCLP-WT Waste Batch R4935787 WG3235811-3 DUP L2389614-1 Mercury (Hg) <0.00010 <0.00010 RPD-NA mg/L N/A 50 05-DEC-19 WG3235811-2 LCS Mercury (Hg) 103.0 % 70-130 05-DEC-19 WG3235811-1 MB Mercury (Hg) <0.00010 mg/L 0.0001 05-DEC-19 WG3235811-4 MS L2389614-1 Mercury (Hg) 99.6 % 50-140 05-DEC-19
MET-TCLP-WT Waste Batch R4935870 WG3235821-4 DUP WG3235821-3 Silver (Ag) <0.0050 <0.0050 RPD-NA mg/L N/A 50 05-DEC-19 Arsenic (As) <0.050 <0.050 RPD-NA mg/L N/A 50 05-DEC-19 Boron (B) <2.5 <2.5 RPD-NA mg/L N/A 50 05-DEC-19 Barium (Ba) <0.50 <0.50 RPD-NA mg/L N/A 50 05-DEC-19 Cadmium (Cd) 0.0176 0.0176 mg/L 0.5 50 05-DEC-19 Chromium (Cr) <0.050 <0.050 RPD-NA mg/L N/A 50 05-DEC-19 Lead (Pb) 0.106 0.108 mg/L 1.7 50 05-DEC-19 Selenium (Se) <0.025 <0.025 RPD-NA mg/L N/A 50 05-DEC-19 Uranium (U) <0.25 <0.25 RPD-NA mg/L N/A 50 05-DEC-19 WG3235821-2 LCS Silver (Ag) 91.3 % 70-130 05-DEC-19 Arsenic (As) 91.8 % 70-130 05-DEC-19 Boron (B) 90.8 % 70-130 05-DEC-19 Barium (Ba) 92.9 % 70-130 05-DEC-19 Cadmium (Cd) 88.4 % 70-130 05-DEC-19 Chromium (Cr) 91.7 % 70-130 05-DEC-19 Lead (Pb) 88.9 % 70-130 05-DEC-19 Selenium (Se) 92.4 % 70-130 05-DEC-19 Uranium (U) 87.0 % 70-130 05-DEC-19 WG3235821-1 MB Silver (Ag) <0.0050 mg/L 0.005 05-DEC-19 Arsenic (As) <0.050 mg/L 0.05 05-DEC-19 Boron (B) <2.5 mg/L 2.5 05-DEC-19 Barium (Ba) <0.50 mg/L 0.5 05-DEC-19 Quality Control Report
Workorder: L2390935 Report Date: 09-DEC-19 Page 2 of 7
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-TCLP-WT Waste Batch R4935870 WG3235821-1 MB Cadmium (Cd) <0.0050 mg/L 0.005 05-DEC-19 Chromium (Cr) <0.050 mg/L 0.05 05-DEC-19 Lead (Pb) <0.050 mg/L 0.05 05-DEC-19 Selenium (Se) <0.025 mg/L 0.025 05-DEC-19 Uranium (U) <0.25 mg/L 0.25 05-DEC-19 WG3235821-5 MS WG3235821-3 Silver (Ag) 99.8 % 50-140 05-DEC-19 Arsenic (As) 96.7 % 50-140 05-DEC-19 Boron (B) 97.1 % 50-140 05-DEC-19 Barium (Ba) 99.7 % 50-140 05-DEC-19 Cadmium (Cd) 88.8 % 50-140 05-DEC-19 Chromium (Cr) 96.6 % 50-140 05-DEC-19 Lead (Pb) 94.7 % 50-140 05-DEC-19 Selenium (Se) 95.0 % 50-140 05-DEC-19 Uranium (U) 96.8 % 50-140 05-DEC-19
PAH-TCLP-WT Waste Batch R4937966 WG3237102-4 DUP WG3237102-6 Acenaphthene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Acenaphthylene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Anthracene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Benzo(a)anthracene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Benzo(a)pyrene <0.0010 <0.0010 RPD-NA mg/L N/A 50 09-DEC-19 Benzo(b)fluoranthene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Benzo(g,h,i)perylene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Benzo(k)fluoranthene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Chrysene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Dibenzo(ah)anthracene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Fluoranthene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Fluorene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Indeno(1,2,3-cd)pyrene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Naphthalene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Phenanthrene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Quality Control Report
Workorder: L2390935 Report Date: 09-DEC-19 Page 3 of 7
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-TCLP-WT Waste Batch R4937966 WG3237102-4 DUP WG3237102-6 Pyrene <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 Quinoline <0.0050 <0.0050 RPD-NA mg/L N/A 50 09-DEC-19 WG3237102-2 LCS Acenaphthene 97.5 % 50-130 09-DEC-19 Acenaphthylene 99.5 % 50-130 09-DEC-19 Anthracene 101.3 % 50-130 09-DEC-19 Benzo(a)anthracene 122.3 % 50-140 09-DEC-19 Benzo(a)pyrene 105.3 % 60-140 09-DEC-19 Benzo(b)fluoranthene 106.5 % 50-140 09-DEC-19 Benzo(g,h,i)perylene 116.2 % 50-140 09-DEC-19 Benzo(k)fluoranthene 99.4 % 50-150 09-DEC-19 Chrysene 119.2 % 50-140 09-DEC-19 Dibenzo(ah)anthracene 113.4 % 50-140 09-DEC-19 Fluoranthene 107.5 % 50-150 09-DEC-19 Fluorene 101.6 % 50-150 09-DEC-19 Indeno(1,2,3-cd)pyrene 119.2 % 50-140 09-DEC-19 Naphthalene 86.2 % 50-130 09-DEC-19 Phenanthrene 110.0 % 50-130 09-DEC-19 Pyrene 109.0 % 50-140 09-DEC-19 Quinoline 108.8 % 50-150 09-DEC-19 WG3237102-1 MB Acenaphthene <0.0050 mg/L 0.005 09-DEC-19 Acenaphthylene <0.0050 mg/L 0.005 09-DEC-19 Anthracene <0.0050 mg/L 0.005 09-DEC-19 Benzo(a)anthracene <0.0050 mg/L 0.005 09-DEC-19 Benzo(a)pyrene <0.0010 mg/L 0.001 09-DEC-19 Benzo(b)fluoranthene <0.0050 mg/L 0.005 09-DEC-19 Benzo(g,h,i)perylene <0.0050 mg/L 0.005 09-DEC-19 Benzo(k)fluoranthene <0.0050 mg/L 0.005 09-DEC-19 Chrysene <0.0050 mg/L 0.005 09-DEC-19 Dibenzo(ah)anthracene <0.0050 mg/L 0.005 09-DEC-19 Fluoranthene <0.0050 mg/L 0.005 09-DEC-19 Fluorene <0.0050 mg/L 0.005 09-DEC-19 Indeno(1,2,3-cd)pyrene <0.0050 mg/L 0.005 09-DEC-19 Quality Control Report
Workorder: L2390935 Report Date: 09-DEC-19 Page 4 of 7
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-TCLP-WT Waste Batch R4937966 WG3237102-1 MB Naphthalene <0.0050 mg/L 0.005 09-DEC-19 Phenanthrene <0.0050 mg/L 0.005 09-DEC-19 Pyrene <0.0050 mg/L 0.005 09-DEC-19 Quinoline <0.0050 mg/L 0.005 09-DEC-19 Surrogate: d8-Naphthalene 94.5 % 50-150 09-DEC-19 Surrogate: d10-Phenanthrene 100.3 % 50-150 09-DEC-19 Surrogate: d12-Chrysene 103.4 % 50-150 09-DEC-19 Surrogate: d10-Acenaphthene 98.1 % 50-150 09-DEC-19 WG3237102-3 MB Acenaphthene <0.0050 mg/L 0.005 09-DEC-19 Acenaphthylene <0.0050 mg/L 0.005 09-DEC-19 Anthracene <0.0050 mg/L 0.005 09-DEC-19 Benzo(a)anthracene <0.0050 mg/L 0.005 09-DEC-19 Benzo(a)pyrene <0.0010 mg/L 0.001 09-DEC-19 Benzo(b)fluoranthene <0.0050 mg/L 0.005 09-DEC-19 Benzo(g,h,i)perylene <0.0050 mg/L 0.005 09-DEC-19 Benzo(k)fluoranthene <0.0050 mg/L 0.005 09-DEC-19 Chrysene <0.0050 mg/L 0.005 09-DEC-19 Dibenzo(ah)anthracene <0.0050 mg/L 0.005 09-DEC-19 Fluoranthene <0.0050 mg/L 0.005 09-DEC-19 Fluorene <0.0050 mg/L 0.005 09-DEC-19 Indeno(1,2,3-cd)pyrene <0.0050 mg/L 0.005 09-DEC-19 Naphthalene <0.0050 mg/L 0.005 09-DEC-19 Phenanthrene <0.0050 mg/L 0.005 09-DEC-19 Pyrene <0.0050 mg/L 0.005 09-DEC-19 Quinoline <0.0050 mg/L 0.005 09-DEC-19 Surrogate: d8-Naphthalene 91.6 % 50-150 09-DEC-19 Surrogate: d10-Phenanthrene 97.4 % 50-150 09-DEC-19 Surrogate: d12-Chrysene 97.9 % 50-150 09-DEC-19 Surrogate: d10-Acenaphthene 94.8 % 50-150 09-DEC-19 WG3237102-5 MS WG3237102-6 Acenaphthene 100.9 % 50-150 09-DEC-19 Acenaphthylene 102.3 % 50-150 09-DEC-19 Anthracene 100.5 % 50-150 09-DEC-19 Quality Control Report
Workorder: L2390935 Report Date: 09-DEC-19 Page 5 of 7
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-TCLP-WT Waste Batch R4937966 WG3237102-5 MS WG3237102-6 Benzo(a)anthracene 117.3 % 50-150 09-DEC-19 Benzo(a)pyrene 101.5 % 50-150 09-DEC-19 Benzo(b)fluoranthene 103.9 % 50-150 09-DEC-19 Benzo(g,h,i)perylene 112.5 % 50-150 09-DEC-19 Benzo(k)fluoranthene 99.8 % 50-150 09-DEC-19 Chrysene 111.4 % 50-150 09-DEC-19 Dibenzo(ah)anthracene 104.0 % 50-150 09-DEC-19 Fluoranthene 106.2 % 50-150 09-DEC-19 Fluorene 102.9 % 50-150 09-DEC-19 Indeno(1,2,3-cd)pyrene 114.1 % 50-150 09-DEC-19 Naphthalene 95.9 % 50-150 09-DEC-19 Phenanthrene 110.0 % 50-150 09-DEC-19 Pyrene 107.4 % 50-150 09-DEC-19 Quinoline 106.2 % 50-150 09-DEC-19
VOC-TCLP-WT Waste Batch R4937385 WG3237127-1 LCS 1,1-Dichloroethylene 101.0 % 70-130 08-DEC-19 1,2-Dichlorobenzene 84.0 % 70-130 08-DEC-19 1,2-Dichloroethane 107.0 % 70-130 08-DEC-19 1,4-Dichlorobenzene 85.5 % 70-130 08-DEC-19 Benzene 104.0 % 70-130 08-DEC-19 Carbon tetrachloride 100.8 % 60-140 08-DEC-19 Chlorobenzene 88.1 % 70-130 08-DEC-19 Chloroform 98.1 % 70-130 08-DEC-19 Dichloromethane 97.6 % 70-130 08-DEC-19 Methyl Ethyl Ketone 112.0 % 50-150 08-DEC-19 Tetrachloroethylene 90.7 % 70-130 08-DEC-19 Trichloroethylene 97.3 % 70-130 08-DEC-19 Vinyl chloride 111.2 % 60-130 08-DEC-19 WG3237127-2 MB 1,1-Dichloroethylene <0.025 mg/L 0.025 08-DEC-19 1,2-Dichlorobenzene <0.025 mg/L 0.025 08-DEC-19 1,2-Dichloroethane <0.025 mg/L 0.025 08-DEC-19 Quality Control Report
Workorder: L2390935 Report Date: 09-DEC-19 Page 6 of 7
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-TCLP-WT Waste Batch R4937385 WG3237127-2 MB 1,4-Dichlorobenzene <0.025 mg/L 0.025 08-DEC-19 Benzene <0.025 mg/L 0.025 08-DEC-19 Carbon tetrachloride <0.025 mg/L 0.025 08-DEC-19 Chlorobenzene <0.025 mg/L 0.025 08-DEC-19 Chloroform <0.10 mg/L 0.1 08-DEC-19 Dichloromethane <0.50 mg/L 0.5 08-DEC-19 Methyl Ethyl Ketone <1.0 mg/L 1 08-DEC-19 Tetrachloroethylene <0.025 mg/L 0.025 08-DEC-19 Trichloroethylene <0.025 mg/L 0.025 08-DEC-19 Vinyl chloride <0.050 mg/L 0.05 08-DEC-19 Surrogate: 1,4-Difluorobenzene 100.5 % 70-130 08-DEC-19 Surrogate: 4-Bromofluorobenzene 97.8 % 70-130 08-DEC-19 Quality Control Report Workorder: L2390935 Report Date: 09-DEC-19
Client: Morrison Hershfield Limited (Ottawa) Page 7 of 7 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.
Morrison Hershfield Limited (Ottawa) Date Received: 09-DEC-19 ATTN: Mitchell Dawley Report Date: 16-DEC-19 14:32 (MT) Version: FINAL 2932 Baseline Rd Ottawa ON K2H 1B1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2395477 Project P.O. #: 20102333 Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-1 BH5 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 12-DEC-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 1.5 16000 Arsenic (As)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 13 1500 Barium (Ba)-Dissolved 462 DLHC 1.0 ug/L 12-DEC-19 610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 **0.5 53 Boron (B)-Dissolved <100 DLHC 100 ug/L 12-DEC-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 12-DEC-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 11 640 Cobalt (Co)-Dissolved 6.8 DLHC 1.0 ug/L 12-DEC-19 *3.8 52 Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 12-DEC-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 1.9 20 Molybdenum (Mo)-Dissolved 2.25 DLHC 0.50 ug/L 12-DEC-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 14 390 Selenium (Se)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 **0.3 1.2 Sodium (Na)-Dissolved 365000 DLHC 500 ug/L 12-DEC-19 490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 12-DEC-19 0.5 400 Uranium (U)-Dissolved 0.88 DLHC 0.10 ug/L 12-DEC-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 12-DEC-19 160 890 Volatile Organic Compounds Acetone <30 30 ug/L 16-DEC-19 2700 100000 Benzene <0.50 0.50 ug/L 16-DEC-19 0.5 44 Bromodichloromethane <2.0 2.0 ug/L 16-DEC-19 2 67000 Bromoform <5.0 5.0 ug/L 16-DEC-19 5 380 Bromomethane <0.50 0.50 ug/L 16-DEC-19 0.89 5.6 Carbon tetrachloride <0.20 0.20 ug/L 16-DEC-19 0.2 0.79 Chlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 500 Dibromochloromethane <2.0 2.0 ug/L 16-DEC-19 2 65000 Chloroform <1.0 1.0 ug/L 16-DEC-19 2 2.4 1,2-Dibromoethane <0.20 0.20 ug/L 16-DEC-19 0.2 0.25 1,2-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 4600 1,3-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 7600 1,4-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 8 Dichlorodifluoromethane <2.0 2.0 ug/L 16-DEC-19 590 3500 1,1-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 320 1,2-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 1,1-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 Methylene Chloride <5.0 5.0 ug/L 16-DEC-19 5 610 1,2-Dichloropropane <0.50 0.50 ug/L 16-DEC-19 0.5 16 cis-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 trans-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 16-DEC-19 0.5 5.2 Ethylbenzene <0.50 0.50 ug/L 16-DEC-19 0.5 1800 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 3 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-1 BH5 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Volatile Organic Compounds n-Hexane <0.50 0.50 ug/L 16-DEC-19 5 51 Methyl Ethyl Ketone <20 20 ug/L 16-DEC-19 400 470000 Methyl Isobutyl Ketone <20 20 ug/L 16-DEC-19 640 140000 MTBE <2.0 2.0 ug/L 16-DEC-19 15 190 Styrene <0.50 0.50 ug/L 16-DEC-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 3.2 Tetrachloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Toluene <0.50 0.50 ug/L 16-DEC-19 0.8 14000 1,1,1-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 640 1,1,2-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 4.7 Trichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Trichlorofluoromethane <5.0 5.0 ug/L 16-DEC-19 150 2000 Vinyl chloride <0.50 0.50 ug/L 16-DEC-19 0.5 0.5 o-Xylene <0.30 0.30 ug/L 16-DEC-19 m+p-Xylenes <0.40 0.40 ug/L 16-DEC-19 Xylenes (Total) <0.50 0.50 ug/L 16-DEC-19 72 3300 Surrogate: 4-Bromofluorobenzene 95.3 70-130 % 16-DEC-19 Surrogate: 1,4-Difluorobenzene 101.4 70-130 % 16-DEC-19 Hydrocarbons F1 (C6-C10) <25 25 ug/L 16-DEC-19 420 420 F1-BTEX <25 25 ug/L 16-DEC-19 420 420 F2 (C10-C16) <100 OWP 100 ug/L 13-DEC-19 150 150 F2-Naphth <100 100 ug/L 16-DEC-19 F3 (C16-C34) 300 OWP 250 ug/L 13-DEC-19 500 500 F3-PAH 300 250 ug/L 16-DEC-19 F4 (C34-C50) 360 OWP 250 ug/L 13-DEC-19 500 500 Total Hydrocarbons (C6-C50) 670 370 ug/L 16-DEC-19 Chrom. to baseline at nC50 YES No Unit 13-DEC-19 Surrogate: 2-Bromobenzotrifluoride 99.2 60-140 % 13-DEC-19 Surrogate: 3,4-Dichlorotoluene 85.1 60-140 % 16-DEC-19 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.025 DLQ 0.025 ug/L 13-DEC-19 4.1 600 Acenaphthylene <0.020 0.020 ug/L 13-DEC-19 1 1.4 Anthracene 0.035 0.020 ug/L 13-DEC-19 0.1 1 Benzo(a)anthracene 0.104 0.020 ug/L 13-DEC-19 0.2 1.8 Benzo(a)pyrene 0.091 0.010 ug/L 13-DEC-19 *0.01 0.81 Benzo(b)fluoranthene 0.119 0.020 ug/L 13-DEC-19 *0.1 0.75 Benzo(g,h,i)perylene 0.066 0.020 ug/L 13-DEC-19 0.2 0.2 Benzo(k)fluoranthene 0.045 0.020 ug/L 13-DEC-19 0.1 0.4 Chrysene 0.114 0.020 ug/L 13-DEC-19 *0.1 0.7 Dibenzo(ah)anthracene <0.020 0.020 ug/L 13-DEC-19 0.2 0.4 Fluoranthene 0.243 0.020 ug/L 13-DEC-19 0.4 73 Fluorene 0.048 0.020 ug/L 13-DEC-19 120 290 Indeno(1,2,3-cd)pyrene 0.076 0.020 ug/L 13-DEC-19 0.2 0.2 1+2-Methylnaphthalenes 0.056 0.028 ug/L 13-DEC-19 2 1500 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 4 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-1 BH5 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Polycyclic Aromatic Hydrocarbons 1-Methylnaphthalene 0.026 0.020 ug/L 13-DEC-19 2 1500 2-Methylnaphthalene 0.030 0.020 ug/L 13-DEC-19 2 1500 Naphthalene <0.050 0.050 ug/L 13-DEC-19 7 1400 Phenanthrene 0.257 0.020 ug/L 13-DEC-19 *0.1 380 Pyrene 0.235 0.020 ug/L 13-DEC-19 *0.2 5.7 Surrogate: d10-Acenaphthene 96.2 60-140 % 13-DEC-19 Surrogate: d12-Chrysene 99.2 60-140 % 13-DEC-19 Surrogate: d8-Naphthalene 98.0 60-140 % 13-DEC-19 Surrogate: d10-Phenanthrene 102.1 60-140 % 13-DEC-19
L2395477-2 BH6 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Mercury Filtration Location FIELD No Unit 13-DEC-19 Dissolved Metals Filtration Location FIELD No Unit 12-DEC-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 1.5 16000 Arsenic (As)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 13 1500 Barium (Ba)-Dissolved 988 DLHC 1.0 ug/L 12-DEC-19 *610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 **0.5 53 Boron (B)-Dissolved <100 DLHC 100 ug/L 12-DEC-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 12-DEC-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 11 640 Cobalt (Co)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 3.8 52 Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 12-DEC-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 1.9 20 Mercury (Hg)-Dissolved <0.0050 0.0050 ug/L 13-DEC-19 0.1 0.29 Molybdenum (Mo)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 14 390 Selenium (Se)-Dissolved 0.72 DLHC 0.50 ug/L 12-DEC-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 **0.3 1.2 Sodium (Na)-Dissolved 621000 DLHC 500 ug/L 12-DEC-19 *490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 12-DEC-19 0.5 400 Uranium (U)-Dissolved <0.10 DLHC 0.10 ug/L 12-DEC-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 12-DEC-19 160 890 Speciated Metals Chromium, Hexavalent <0.50 0.50 ug/L 13-DEC-19 25 110 Volatile Organic Compounds Acetone <30 30 ug/L 16-DEC-19 2700 100000 Benzene <0.50 0.50 ug/L 16-DEC-19 0.5 44 Bromodichloromethane <2.0 2.0 ug/L 16-DEC-19 2 67000 Bromoform <5.0 5.0 ug/L 16-DEC-19 5 380 Bromomethane <0.50 0.50 ug/L 16-DEC-19 0.89 5.6 Carbon tetrachloride <0.20 0.20 ug/L 16-DEC-19 0.2 0.79 Chlorobenzene <0.50 0.50 ug/L 16-DEC-19 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 5 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-2 BH6 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Volatile Organic Compounds 0.5 500 Dibromochloromethane <2.0 2.0 ug/L 16-DEC-19 2 65000 Chloroform <1.0 1.0 ug/L 16-DEC-19 2 2.4 1,2-Dibromoethane <0.20 0.20 ug/L 16-DEC-19 0.2 0.25 1,2-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 4600 1,3-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 7600 1,4-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 8 Dichlorodifluoromethane <2.0 2.0 ug/L 16-DEC-19 590 3500 1,1-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 320 1,2-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 1,1-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 Methylene Chloride <5.0 5.0 ug/L 16-DEC-19 5 610 1,2-Dichloropropane <0.50 0.50 ug/L 16-DEC-19 0.5 16 cis-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 trans-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 16-DEC-19 0.5 5.2 Ethylbenzene <0.50 0.50 ug/L 16-DEC-19 0.5 1800 n-Hexane <0.50 0.50 ug/L 16-DEC-19 5 51 Methyl Ethyl Ketone <20 20 ug/L 16-DEC-19 400 470000 Methyl Isobutyl Ketone <20 20 ug/L 16-DEC-19 640 140000 MTBE <2.0 2.0 ug/L 16-DEC-19 15 190 Styrene <0.50 0.50 ug/L 16-DEC-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 3.2 Tetrachloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Toluene <0.50 0.50 ug/L 16-DEC-19 0.8 14000 1,1,1-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 640 1,1,2-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 4.7 Trichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Trichlorofluoromethane <5.0 5.0 ug/L 16-DEC-19 150 2000 Vinyl chloride <0.50 0.50 ug/L 16-DEC-19 0.5 0.5 o-Xylene <0.30 0.30 ug/L 16-DEC-19 m+p-Xylenes <0.40 0.40 ug/L 16-DEC-19 Xylenes (Total) <0.50 0.50 ug/L 16-DEC-19 72 3300 Surrogate: 4-Bromofluorobenzene 95.7 70-130 % 16-DEC-19 Surrogate: 1,4-Difluorobenzene 101.3 70-130 % 16-DEC-19 Hydrocarbons F1 (C6-C10) <25 25 ug/L 16-DEC-19 420 420 F1-BTEX <25 25 ug/L 16-DEC-19 420 420 F2 (C10-C16) 140 OWP 100 ug/L 13-DEC-19 150 150 F2-Naphth 140 100 ug/L 16-DEC-19 F3 (C16-C34) 10900 OWP 250 ug/L 13-DEC-19 *500 *500 F3-PAH 10800 250 ug/L 16-DEC-19 F4 (C34-C50) 5190 OWP 250 ug/L 13-DEC-19 *500 *500 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 6 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-2 BH6 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Hydrocarbons Total Hydrocarbons (C6-C50) 16200 370 ug/L 16-DEC-19 Chrom. to baseline at nC50 YES No Unit 13-DEC-19 Surrogate: 2-Bromobenzotrifluoride 102.6 60-140 % 13-DEC-19 Surrogate: 3,4-Dichlorotoluene 76.9 60-140 % 16-DEC-19 Polycyclic Aromatic Hydrocarbons Acenaphthene 3.98 0.020 ug/L 13-DEC-19 4.1 600 Acenaphthylene 0.236 R 0.020 ug/L 13-DEC-19 1 1.4 Anthracene 7.17 0.020 ug/L 13-DEC-19 *0.1 *1 Benzo(a)anthracene 14.3 DLHC 0.040 ug/L 16-DEC-19 *0.2 *1.8 Benzo(a)pyrene 12.0 DLHC 0.040 ug/L 16-DEC-19 *0.01 *0.81 Benzo(b)fluoranthene 14.2 DLHC 0.040 ug/L 16-DEC-19 *0.1 *0.75 Benzo(g,h,i)perylene 6.25 0.020 ug/L 13-DEC-19 *0.2 *0.2 Benzo(k)fluoranthene 4.49 0.020 ug/L 13-DEC-19 *0.1 *0.4 Chrysene 11.5 DLHC 0.040 ug/L 16-DEC-19 *0.1 *0.7 Dibenzo(ah)anthracene 1.30 0.020 ug/L 13-DEC-19 *0.2 *0.4 Fluoranthene 29.3 DLHC 0.040 ug/L 16-DEC-19 *0.4 73 Fluorene 5.34 0.020 ug/L 13-DEC-19 120 290 Indeno(1,2,3-cd)pyrene 8.36 0.020 ug/L 13-DEC-19 *0.2 *0.2 1+2-Methylnaphthalenes 0.940 0.028 ug/L 16-DEC-19 2 1500 1-Methylnaphthalene 0.778 0.020 ug/L 13-DEC-19 2 1500 2-Methylnaphthalene 0.162 0.020 ug/L 13-DEC-19 2 1500 Naphthalene <0.34 DLQ 0.34 ug/L 13-DEC-19 7 1400 Phenanthrene 20.6 DLHC 0.040 ug/L 16-DEC-19 *0.1 380 Pyrene 25.8 DLHC 0.040 ug/L 16-DEC-19 *0.2 *5.7 Surrogate: d10-Acenaphthene 99.5 60-140 % 13-DEC-19 Surrogate: d12-Chrysene 106.0 60-140 % 13-DEC-19 Surrogate: d8-Naphthalene 95.3 60-140 % 13-DEC-19 Surrogate: d10-Phenanthrene 112.0 60-140 % 13-DEC-19
L2395477-3 BH7 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 12-DEC-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 1.5 16000 Arsenic (As)-Dissolved 1.0 DLHC 1.0 ug/L 12-DEC-19 13 1500 Barium (Ba)-Dissolved 485 DLHC 1.0 ug/L 12-DEC-19 610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 **0.5 53 Boron (B)-Dissolved <100 DLHC 100 ug/L 12-DEC-19 1700 36000 Cadmium (Cd)-Dissolved 0.061 DLHC 0.050 ug/L 12-DEC-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 11 640 Cobalt (Co)-Dissolved 6.9 DLHC 1.0 ug/L 12-DEC-19 *3.8 52 Copper (Cu)-Dissolved 3.2 DLHC 2.0 ug/L 12-DEC-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 1.9 20 Molybdenum (Mo)-Dissolved 1.35 DLHC 0.50 ug/L 12-DEC-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 14 390 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 7 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-3 BH7 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Dissolved Metals Selenium (Se)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 **0.3 1.2 Sodium (Na)-Dissolved 99000 DLHC 500 ug/L 12-DEC-19 490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 12-DEC-19 0.5 400 Uranium (U)-Dissolved 2.07 DLHC 0.10 ug/L 12-DEC-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 12-DEC-19 160 890 Volatile Organic Compounds Acetone <30 30 ug/L 16-DEC-19 2700 100000 Benzene <0.50 0.50 ug/L 16-DEC-19 0.5 44 Bromodichloromethane <2.0 2.0 ug/L 16-DEC-19 2 67000 Bromoform <5.0 5.0 ug/L 16-DEC-19 5 380 Bromomethane <0.50 0.50 ug/L 16-DEC-19 0.89 5.6 Carbon tetrachloride <0.20 0.20 ug/L 16-DEC-19 0.2 0.79 Chlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 500 Dibromochloromethane <2.0 2.0 ug/L 16-DEC-19 2 65000 Chloroform <1.0 1.0 ug/L 16-DEC-19 2 2.4 1,2-Dibromoethane <0.20 0.20 ug/L 16-DEC-19 0.2 0.25 1,2-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 4600 1,3-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 7600 1,4-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 8 Dichlorodifluoromethane <2.0 2.0 ug/L 16-DEC-19 590 3500 1,1-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 320 1,2-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 1,1-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 Methylene Chloride <5.0 5.0 ug/L 16-DEC-19 5 610 1,2-Dichloropropane <0.50 0.50 ug/L 16-DEC-19 0.5 16 cis-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 trans-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 16-DEC-19 0.5 5.2 Ethylbenzene <0.50 0.50 ug/L 16-DEC-19 0.5 1800 n-Hexane <0.50 0.50 ug/L 16-DEC-19 5 51 Methyl Ethyl Ketone <20 20 ug/L 16-DEC-19 400 470000 Methyl Isobutyl Ketone <20 20 ug/L 16-DEC-19 640 140000 MTBE <2.0 2.0 ug/L 16-DEC-19 15 190 Styrene <0.50 0.50 ug/L 16-DEC-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 3.2 Tetrachloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Toluene <0.50 0.50 ug/L 16-DEC-19 0.8 14000 1,1,1-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 640 1,1,2-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 4.7 Trichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Trichlorofluoromethane <5.0 5.0 ug/L 16-DEC-19 150 2000 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 8 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-3 BH7 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Volatile Organic Compounds Vinyl chloride <0.50 0.50 ug/L 16-DEC-19 0.5 0.5 o-Xylene <0.30 0.30 ug/L 16-DEC-19 m+p-Xylenes <0.40 0.40 ug/L 16-DEC-19 Xylenes (Total) <0.50 0.50 ug/L 16-DEC-19 72 3300 Surrogate: 4-Bromofluorobenzene 95.3 70-130 % 16-DEC-19 Surrogate: 1,4-Difluorobenzene 101.6 70-130 % 16-DEC-19 Hydrocarbons F1 (C6-C10) <25 25 ug/L 16-DEC-19 420 420 F1-BTEX <25 25 ug/L 16-DEC-19 420 420 F2 (C10-C16) <100 100 ug/L 13-DEC-19 150 150 F2-Naphth <100 100 ug/L 16-DEC-19 F3 (C16-C34) <250 250 ug/L 13-DEC-19 500 500 F3-PAH <250 250 ug/L 16-DEC-19 F4 (C34-C50) <250 250 ug/L 13-DEC-19 500 500 Total Hydrocarbons (C6-C50) <370 370 ug/L 16-DEC-19 Chrom. to baseline at nC50 YES No Unit 13-DEC-19 Surrogate: 2-Bromobenzotrifluoride 96.7 60-140 % 13-DEC-19 Surrogate: 3,4-Dichlorotoluene 78.0 60-140 % 16-DEC-19 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.112 0.020 ug/L 13-DEC-19 4.1 600 Acenaphthylene <0.020 0.020 ug/L 13-DEC-19 1 1.4 Anthracene 0.022 0.020 ug/L 13-DEC-19 0.1 1 Benzo(a)anthracene 0.034 0.020 ug/L 13-DEC-19 0.2 1.8 Benzo(a)pyrene 0.026 0.010 ug/L 13-DEC-19 *0.01 0.81 Benzo(b)fluoranthene 0.034 0.020 ug/L 13-DEC-19 0.1 0.75 Benzo(g,h,i)perylene <0.020 0.020 ug/L 13-DEC-19 0.2 0.2 Benzo(k)fluoranthene <0.020 0.020 ug/L 13-DEC-19 0.1 0.4 Chrysene 0.031 0.020 ug/L 13-DEC-19 0.1 0.7 Dibenzo(ah)anthracene <0.020 0.020 ug/L 13-DEC-19 0.2 0.4 Fluoranthene 0.081 0.020 ug/L 13-DEC-19 0.4 73 Fluorene 0.064 0.020 ug/L 13-DEC-19 120 290 Indeno(1,2,3-cd)pyrene 0.021 0.020 ug/L 13-DEC-19 0.2 0.2 1+2-Methylnaphthalenes 0.097 0.028 ug/L 13-DEC-19 2 1500 1-Methylnaphthalene 0.054 0.020 ug/L 13-DEC-19 2 1500 2-Methylnaphthalene 0.043 0.020 ug/L 13-DEC-19 2 1500 Naphthalene 0.099 0.050 ug/L 13-DEC-19 7 1400 Phenanthrene 0.147 0.020 ug/L 13-DEC-19 *0.1 380 Pyrene 0.073 0.020 ug/L 13-DEC-19 0.2 5.7 Surrogate: d10-Acenaphthene 100.5 60-140 % 13-DEC-19 Surrogate: d12-Chrysene 92.4 60-140 % 13-DEC-19 Surrogate: d8-Naphthalene 102.3 60-140 % 13-DEC-19 Surrogate: d10-Phenanthrene 103.8 60-140 % 13-DEC-19
L2395477-4 BH8 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 9 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-4 BH8 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 12-DEC-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 1.5 16000 Arsenic (As)-Dissolved 6.3 DLHC 1.0 ug/L 12-DEC-19 13 1500 Barium (Ba)-Dissolved 777 DLHC 1.0 ug/L 12-DEC-19 *610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 **0.5 53 Boron (B)-Dissolved <100 DLHC 100 ug/L 12-DEC-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 12-DEC-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 11 640 Cobalt (Co)-Dissolved 1.3 DLHC 1.0 ug/L 12-DEC-19 3.8 52 Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 12-DEC-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 1.9 20 Molybdenum (Mo)-Dissolved 0.82 DLHC 0.50 ug/L 12-DEC-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 14 390 Selenium (Se)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 **0.3 1.2 Sodium (Na)-Dissolved 142000 DLHC 500 ug/L 12-DEC-19 490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 12-DEC-19 0.5 400 Uranium (U)-Dissolved 0.48 DLHC 0.10 ug/L 12-DEC-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 **3.9 200 Zinc (Zn)-Dissolved 13 DLHC 10 ug/L 12-DEC-19 160 890 Volatile Organic Compounds Acetone <30 30 ug/L 16-DEC-19 2700 100000 Benzene <0.50 0.50 ug/L 16-DEC-19 0.5 44 Bromodichloromethane <2.0 2.0 ug/L 16-DEC-19 2 67000 Bromoform <5.0 5.0 ug/L 16-DEC-19 5 380 Bromomethane <0.50 0.50 ug/L 16-DEC-19 0.89 5.6 Carbon tetrachloride <0.20 0.20 ug/L 16-DEC-19 0.2 0.79 Chlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 500 Dibromochloromethane <2.0 2.0 ug/L 16-DEC-19 2 65000 Chloroform <1.0 1.0 ug/L 16-DEC-19 2 2.4 1,2-Dibromoethane <0.20 0.20 ug/L 16-DEC-19 0.2 0.25 1,2-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 4600 1,3-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 7600 1,4-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 8 Dichlorodifluoromethane <2.0 2.0 ug/L 16-DEC-19 590 3500 1,1-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 320 1,2-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 1,1-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 Methylene Chloride <5.0 5.0 ug/L 16-DEC-19 5 610 1,2-Dichloropropane <0.50 0.50 ug/L 16-DEC-19 0.5 16 cis-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 trans-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 16-DEC-19 0.5 5.2 Ethylbenzene <0.50 0.50 ug/L 16-DEC-19 0.5 1800 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 10 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-4 BH8 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Volatile Organic Compounds n-Hexane <0.50 0.50 ug/L 16-DEC-19 5 51 Methyl Ethyl Ketone <20 20 ug/L 16-DEC-19 400 470000 Methyl Isobutyl Ketone <20 20 ug/L 16-DEC-19 640 140000 MTBE <2.0 2.0 ug/L 16-DEC-19 15 190 Styrene <0.50 0.50 ug/L 16-DEC-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 3.2 Tetrachloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Toluene <0.50 0.50 ug/L 16-DEC-19 0.8 14000 1,1,1-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 640 1,1,2-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 4.7 Trichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Trichlorofluoromethane <5.0 5.0 ug/L 16-DEC-19 150 2000 Vinyl chloride <0.50 0.50 ug/L 16-DEC-19 0.5 0.5 o-Xylene <0.30 0.30 ug/L 16-DEC-19 m+p-Xylenes <0.40 0.40 ug/L 16-DEC-19 Xylenes (Total) <0.50 0.50 ug/L 16-DEC-19 72 3300 Surrogate: 4-Bromofluorobenzene 95.5 70-130 % 16-DEC-19 Surrogate: 1,4-Difluorobenzene 102.1 70-130 % 16-DEC-19 Hydrocarbons F1 (C6-C10) <25 25 ug/L 16-DEC-19 420 420 F1-BTEX <25 25 ug/L 16-DEC-19 420 420 F2 (C10-C16) <100 OWP 100 ug/L 13-DEC-19 150 150 F2-Naphth <100 100 ug/L 16-DEC-19 F3 (C16-C34) <250 OWP 250 ug/L 13-DEC-19 500 500 F3-PAH <250 250 ug/L 16-DEC-19 F4 (C34-C50) 360 OWP 250 ug/L 13-DEC-19 500 500 Total Hydrocarbons (C6-C50) <370 370 ug/L 16-DEC-19 Chrom. to baseline at nC50 YES No Unit 13-DEC-19 Surrogate: 2-Bromobenzotrifluoride 99.6 60-140 % 13-DEC-19 Surrogate: 3,4-Dichlorotoluene 79.4 60-140 % 16-DEC-19 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.032 0.020 ug/L 13-DEC-19 4.1 600 Acenaphthylene <0.020 0.020 ug/L 13-DEC-19 1 1.4 Anthracene 0.082 0.020 ug/L 13-DEC-19 0.1 1 Benzo(a)anthracene 0.240 0.020 ug/L 13-DEC-19 *0.2 1.8 Benzo(a)pyrene 0.197 0.010 ug/L 13-DEC-19 *0.01 0.81 Benzo(b)fluoranthene 0.249 0.020 ug/L 13-DEC-19 *0.1 0.75 Benzo(g,h,i)perylene 0.131 0.020 ug/L 13-DEC-19 0.2 0.2 Benzo(k)fluoranthene 0.093 0.020 ug/L 13-DEC-19 0.1 0.4 Chrysene 0.244 0.020 ug/L 13-DEC-19 *0.1 0.7 Dibenzo(ah)anthracene 0.030 0.020 ug/L 13-DEC-19 0.2 0.4 Fluoranthene 0.608 0.020 ug/L 13-DEC-19 *0.4 73 Fluorene 0.063 0.020 ug/L 13-DEC-19 120 290 Indeno(1,2,3-cd)pyrene 0.152 0.020 ug/L 13-DEC-19 0.2 0.2 1+2-Methylnaphthalenes 0.062 0.028 ug/L 13-DEC-19 2 1500 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 11 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-4 BH8 Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Polycyclic Aromatic Hydrocarbons 1-Methylnaphthalene 0.023 0.020 ug/L 13-DEC-19 2 1500 2-Methylnaphthalene 0.039 0.020 ug/L 13-DEC-19 2 1500 Naphthalene <0.050 0.050 ug/L 13-DEC-19 7 1400 Phenanthrene 0.571 0.020 ug/L 13-DEC-19 *0.1 380 Pyrene 0.562 0.020 ug/L 13-DEC-19 *0.2 5.7 Surrogate: d10-Acenaphthene 91.8 60-140 % 13-DEC-19 Surrogate: d12-Chrysene 90.6 60-140 % 13-DEC-19 Surrogate: d8-Naphthalene 92.1 60-140 % 13-DEC-19 Surrogate: d10-Phenanthrene 99.1 60-140 % 13-DEC-19
L2395477-5 DUP Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Dissolved Metals Dissolved Metals Filtration Location FIELD No Unit 12-DEC-19 Antimony (Sb)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 1.5 16000 Arsenic (As)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 13 1500 Barium (Ba)-Dissolved 1010 DLHC 1.0 ug/L 12-DEC-19 *610 23000 Beryllium (Be)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 **0.5 53 Boron (B)-Dissolved <100 DLHC 100 ug/L 12-DEC-19 1700 36000 Cadmium (Cd)-Dissolved <0.050 DLHC 0.050 ug/L 12-DEC-19 0.5 2.1 Chromium (Cr)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 11 640 Cobalt (Co)-Dissolved <1.0 DLHC 1.0 ug/L 12-DEC-19 3.8 52 Copper (Cu)-Dissolved <2.0 DLHC 2.0 ug/L 12-DEC-19 5 69 Lead (Pb)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 1.9 20 Molybdenum (Mo)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 23 7300 Nickel (Ni)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 14 390 Selenium (Se)-Dissolved 0.57 DLHC 0.50 ug/L 12-DEC-19 5 50 Silver (Ag)-Dissolved <0.50 DLHC 0.50 ug/L 12-DEC-19 **0.3 1.2 Sodium (Na)-Dissolved 611000 DLHC 500 ug/L 12-DEC-19 *490000 1800000 Thallium (Tl)-Dissolved <0.10 DLHC 0.10 ug/L 12-DEC-19 0.5 400 Uranium (U)-Dissolved <0.10 DLHC 0.10 ug/L 12-DEC-19 8.9 330 Vanadium (V)-Dissolved <5.0 DLHC 5.0 ug/L 12-DEC-19 **3.9 200 Zinc (Zn)-Dissolved <10 DLHC 10 ug/L 12-DEC-19 160 890 Volatile Organic Compounds Acetone <30 30 ug/L 16-DEC-19 2700 100000 Benzene <0.50 0.50 ug/L 16-DEC-19 0.5 44 Bromodichloromethane <2.0 2.0 ug/L 16-DEC-19 2 67000 Bromoform <5.0 5.0 ug/L 16-DEC-19 5 380 Bromomethane <0.50 0.50 ug/L 16-DEC-19 0.89 5.6 Carbon tetrachloride <0.20 0.20 ug/L 16-DEC-19 0.2 0.79 Chlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 500 Dibromochloromethane <2.0 2.0 ug/L 16-DEC-19 2 65000 Chloroform <1.0 1.0 ug/L 16-DEC-19 2 2.4 1,2-Dibromoethane <0.20 0.20 ug/L 16-DEC-19 0.2 0.25 1,2-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 4600 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 12 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-5 DUP Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Volatile Organic Compounds 1,3-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 7600 1,4-Dichlorobenzene <0.50 0.50 ug/L 16-DEC-19 0.5 8 Dichlorodifluoromethane <2.0 2.0 ug/L 16-DEC-19 590 3500 1,1-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 320 1,2-Dichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 1,1-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 cis-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 trans-1,2-Dichloroethylene <0.50 0.50 ug/L 16-DEC-19 1.6 1.6 Methylene Chloride <5.0 5.0 ug/L 16-DEC-19 5 610 1,2-Dichloropropane <0.50 0.50 ug/L 16-DEC-19 0.5 16 cis-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 trans-1,3-Dichloropropene <0.30 0.30 ug/L 16-DEC-19 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 16-DEC-19 0.5 5.2 Ethylbenzene <0.50 0.50 ug/L 16-DEC-19 0.5 1800 n-Hexane <0.50 0.50 ug/L 16-DEC-19 5 51 Methyl Ethyl Ketone <20 20 ug/L 16-DEC-19 400 470000 Methyl Isobutyl Ketone <20 20 ug/L 16-DEC-19 640 140000 MTBE <2.0 2.0 ug/L 16-DEC-19 15 190 Styrene <0.50 0.50 ug/L 16-DEC-19 0.5 1300 1,1,1,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 1.1 3.4 1,1,2,2-Tetrachloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 3.2 Tetrachloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Toluene <0.50 0.50 ug/L 16-DEC-19 0.8 14000 1,1,1-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 640 1,1,2-Trichloroethane <0.50 0.50 ug/L 16-DEC-19 0.5 4.7 Trichloroethylene <0.50 0.50 ug/L 16-DEC-19 0.5 1.6 Trichlorofluoromethane <5.0 5.0 ug/L 16-DEC-19 150 2000 Vinyl chloride <0.50 0.50 ug/L 16-DEC-19 0.5 0.5 o-Xylene <0.30 0.30 ug/L 16-DEC-19 m+p-Xylenes <0.40 0.40 ug/L 16-DEC-19 Xylenes (Total) <0.50 0.50 ug/L 16-DEC-19 72 3300 Surrogate: 4-Bromofluorobenzene 94.9 70-130 % 16-DEC-19 Surrogate: 1,4-Difluorobenzene 101.5 70-130 % 16-DEC-19 Hydrocarbons F1 (C6-C10) <25 25 ug/L 16-DEC-19 420 420 F1-BTEX <25 25 ug/L 16-DEC-19 420 420 F2 (C10-C16) 120 OWP 100 ug/L 13-DEC-19 150 150 F2-Naphth 120 100 ug/L 16-DEC-19 F3 (C16-C34) 8810 OWP 250 ug/L 13-DEC-19 *500 *500 F3-PAH 8710 250 ug/L 16-DEC-19 F4 (C34-C50) 4100 OWP 250 ug/L 13-DEC-19 *500 *500 Total Hydrocarbons (C6-C50) 13000 370 ug/L 16-DEC-19 Chrom. to baseline at nC50 YES No Unit 13-DEC-19 Surrogate: 2-Bromobenzotrifluoride 105.4 60-140 % 13-DEC-19 Surrogate: 3,4-Dichlorotoluene 77.4 60-140 % 16-DEC-19 Polycyclic Aromatic Hydrocarbons
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use L2395477 CONTD.... ANALYTICAL GUIDELINE REPORT Page 13 of 15 190441800 16-DEC-19 14:32 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2395477-5 DUP Sampled By: CLIENT on 06-DEC-19 #1 #2 Matrix: WATER
Polycyclic Aromatic Hydrocarbons Acenaphthene 2.72 0.020 ug/L 13-DEC-19 4.1 600 Acenaphthylene 0.185 R 0.020 ug/L 13-DEC-19 1 1.4 Anthracene 4.44 0.020 ug/L 13-DEC-19 *0.1 *1 Benzo(a)anthracene 10.5 0.020 ug/L 16-DEC-19 *0.2 *1.8 Benzo(a)pyrene 8.43 0.010 ug/L 13-DEC-19 *0.01 *0.81 Benzo(b)fluoranthene 10.7 0.020 ug/L 16-DEC-19 *0.1 *0.75 Benzo(g,h,i)perylene 5.61 0.020 ug/L 13-DEC-19 *0.2 *0.2 Benzo(k)fluoranthene 3.12 0.020 ug/L 13-DEC-19 *0.1 *0.4 Chrysene 7.99 0.020 ug/L 13-DEC-19 *0.1 *0.7 Dibenzo(ah)anthracene 1.16 0.020 ug/L 13-DEC-19 *0.2 *0.4 Fluoranthene 20.6 0.020 ug/L 16-DEC-19 *0.4 73 Fluorene 3.39 0.020 ug/L 13-DEC-19 120 290 Indeno(1,2,3-cd)pyrene 7.12 0.020 ug/L 13-DEC-19 *0.2 *0.2 1+2-Methylnaphthalenes 0.630 0.028 ug/L 16-DEC-19 2 1500 1-Methylnaphthalene 0.538 0.020 ug/L 13-DEC-19 2 1500 2-Methylnaphthalene 0.092 0.020 ug/L 13-DEC-19 2 1500 Naphthalene <0.26 DLQ 0.26 ug/L 13-DEC-19 7 1400 Phenanthrene 13.9 0.020 ug/L 16-DEC-19 *0.1 380 Pyrene 18.4 0.020 ug/L 16-DEC-19 *0.2 *5.7 Surrogate: d10-Acenaphthene 106.0 60-140 % 13-DEC-19 Surrogate: d12-Chrysene 120.6 60-140 % 13-DEC-19 Surrogate: d8-Naphthalene 100.9 60-140 % 13-DEC-19 Surrogate: d10-Phenanthrene 115.8 60-140 % 13-DEC-19
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T9-WATER #1: T1-Ground Water-All Types of Property Uses #2: T9-Non-Potable Ground Water-All Types of Property Use 190441800 L2395477 CONTD.... Page 14 of 15 16-DEC-19 14:32 (MT) Reference Information
Sample Parameter Qualifier key listed: Qualifier Description
R The ion abundance ratio(s) did not meet the acceptance criteria. Value is an estimated maximum. DLQ Detection Limit raised due to co-eluting interference. GCMS qualifier ion ratio did not meet acceptance criteria. OWP Organic water sample contained visible sediment (must be included as part of analysis). Measured concentrations of organic substances in water can be biased high due to presence of sediment. DLHC Detection Limit Raised: Dilution required due to high concentration of test analyte(s).
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
CR-CR6-IC-R511-WT Water Hex Chrom-O.Reg 153/04 (July EPA 7199 2011) This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in a sulphuric acid solution. Chromium (III) is calculated as the difference between the total chromium and the chromium (VI) results.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). F1-F4-511-CALC-WT Water F1-F4 Hydrocarbon Calculated CCME CWS-PHC, Pub #1310, Dec 2001-L Parameters
Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.
In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines and the gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes has been subtracted from F1.
In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.
Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range: 1. All extraction and analysis holding times were met. 2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene. 3. Linearity of gasoline response within 15% throughout the calibration range.
Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges: 1. All extraction and analysis holding times were met. 2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average. 3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors. 4. Linearity of diesel or motor oil response within 15% throughout the calibration range. F1-HS-511-WT Water F1-O.Reg 153/04 (July 2011) E3398/CCME TIER 1-HS
Fraction F1 is determined by analyzing by headspace-GC/FID.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). F2-F4-511-WT Water F2-F4-O.Reg 153/04 (July 2011) EPA 3511/CCME Tier 1
Petroleum Hydrocarbons (F2-F4 fractions) are extracted from water using a hexane micro-extraction technique. Instrumental analysis is by GC-FID, as per the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Tier 1 Method, CCME, 2001.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). HG-D-UG/L-CVAA-WT Water Diss. Mercury in Water by EPA 1631E (mod) CVAAS (ug/L)
Water samples are filtered (0.45 um), preserved with hydrochloric acid, then undergo a cold-oxidation using bromine monochloride prior to reduction with stannous chloride, and analyzed by CVAAS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). MET-D-UG/L-MS-WT Water Diss. Metals in Water by ICPMS EPA 200.8 (ug/L)
The metal constituents of a non-acidified sample that pass through a membrane filter prior to ICP/MS analysis.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). 190441800 L2395477 CONTD.... Page 15 of 15 16-DEC-19 14:32 (MT) Reference Information
METHYLNAPS-CALC-WT Water PAH-Calculated Parameters SW846 8270 PAH-511-WT Water PAH-O. Reg 153/04 (July 2011) SW846 3510/8270
Aqueous samples, fortified with surrogates, are extracted using liquid/liquid extraction technique. The sample extracts are concentrated and then analyzed using GC/MS. Results for benzo(b) fluoranthene may include contributions from benzo(j)fluoranthene, if also present in the sample.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). VOC-1,3-DCP-CALC-WT Water Regulation 153 VOCs SW8260B/SW8270C VOC-511-HS-WT Water VOC by GCMS HS O.Reg SW846 8260 153/04 (July 2011)
Liquid samples are analyzed by headspace GC/MSD.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). XYLENES-SUM-CALC- Water Sum of Xylene Isomer CALCULATION WT Concentrations
Total xylenes represents the sum of o-xylene and m&p-xylene.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 1 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
CR-CR6-IC-R511-WT Water Batch R4943667 WG3241702-4 DUP WG3241702-3 Chromium, Hexavalent 18.5 17.7 ug/L 4.1 20 13-DEC-19 WG3241702-2 LCS Chromium, Hexavalent 100.3 % 80-120 13-DEC-19 WG3241702-1 MB Chromium, Hexavalent <0.50 ug/L 0.5 13-DEC-19 WG3241702-5 MS WG3241702-3 Chromium, Hexavalent 97.4 % 70-130 13-DEC-19
F1-HS-511-WT Water Batch R4943663 WG3235779-4 DUP WG3235779-3 F1 (C6-C10) <25 <25 RPD-NA ug/L N/A 30 16-DEC-19 WG3235779-1 LCS F1 (C6-C10) 95.4 % 80-120 16-DEC-19 WG3235779-2 MB F1 (C6-C10) <25 ug/L 25 16-DEC-19 Surrogate: 3,4-Dichlorotoluene 106.9 % 60-140 16-DEC-19 WG3235779-5 MS WG3235779-3 F1 (C6-C10) 89.3 % 60-140 16-DEC-19
F2-F4-511-WT Water Batch R4943015 WG3241503-2 LCS F2 (C10-C16) 100.2 % 70-130 13-DEC-19 F3 (C16-C34) 101.2 % 70-130 13-DEC-19 F4 (C34-C50) 102.6 % 70-130 13-DEC-19 WG3241503-1 MB F2 (C10-C16) <100 ug/L 100 13-DEC-19 F3 (C16-C34) <250 ug/L 250 13-DEC-19 F4 (C34-C50) <250 ug/L 250 13-DEC-19 Surrogate: 2-Bromobenzotrifluoride 94.2 % 60-140 13-DEC-19
HG-D-UG/L-CVAA-WT Water Batch R4942684 WG3241732-3 DUP L2395477-2 Mercury (Hg)-Dissolved <0.0050 <0.0050 RPD-NA ug/L N/A 20 13-DEC-19 WG3241732-2 LCS Mercury (Hg)-Dissolved 102.0 % 80-120 13-DEC-19 WG3241732-1 MB Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 2 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
HG-D-UG/L-CVAA-WT Water Batch R4942684 WG3241732-1 MB Mercury (Hg)-Dissolved <0.0050 ug/L 0.005 13-DEC-19 WG3241732-4 MS L2395727-6 Mercury (Hg)-Dissolved 93.2 % 70-130 13-DEC-19
MET-D-UG/L-MS-WT Water Batch R4941530 WG3241047-4 DUP WG3241047-3 Antimony (Sb)-Dissolved <1.0 <1.0 RPD-NA ug/L N/A 20 12-DEC-19 Arsenic (As)-Dissolved <1.0 <1.0 RPD-NA ug/L N/A 20 12-DEC-19 Barium (Ba)-Dissolved 462 464 ug/L 0.6 20 12-DEC-19 Beryllium (Be)-Dissolved <1.0 <1.0 RPD-NA ug/L N/A 20 12-DEC-19 Boron (B)-Dissolved <100 <100 RPD-NA ug/L N/A 20 12-DEC-19 Cadmium (Cd)-Dissolved <0.050 <0.050 RPD-NA ug/L N/A 20 12-DEC-19 Chromium (Cr)-Dissolved <5.0 <5.0 RPD-NA ug/L N/A 20 12-DEC-19 Cobalt (Co)-Dissolved 6.8 6.8 ug/L 0.2 20 12-DEC-19 Copper (Cu)-Dissolved <2.0 <2.0 RPD-NA ug/L N/A 20 12-DEC-19 Lead (Pb)-Dissolved <0.50 <0.50 RPD-NA ug/L N/A 20 12-DEC-19 Molybdenum (Mo)-Dissolved 2.25 2.26 ug/L 0.3 20 12-DEC-19 Nickel (Ni)-Dissolved <5.0 <5.0 RPD-NA ug/L N/A 20 12-DEC-19 Selenium (Se)-Dissolved <0.50 <0.50 RPD-NA ug/L N/A 20 12-DEC-19 Silver (Ag)-Dissolved <0.50 <0.50 RPD-NA ug/L N/A 20 12-DEC-19 Sodium (Na)-Dissolved 365000 362000 ug/L 0.8 20 12-DEC-19 Thallium (Tl)-Dissolved <0.10 <0.10 RPD-NA ug/L N/A 20 12-DEC-19 Uranium (U)-Dissolved 0.88 0.88 ug/L 0.1 20 12-DEC-19 Vanadium (V)-Dissolved <5.0 <5.0 RPD-NA ug/L N/A 20 12-DEC-19 Zinc (Zn)-Dissolved <10 <10 RPD-NA ug/L N/A 20 12-DEC-19 WG3241047-2 LCS Antimony (Sb)-Dissolved 98.9 % 80-120 12-DEC-19 Arsenic (As)-Dissolved 98.2 % 80-120 12-DEC-19 Barium (Ba)-Dissolved 102.9 % 80-120 12-DEC-19 Beryllium (Be)-Dissolved 98.6 % 80-120 12-DEC-19 Boron (B)-Dissolved 102.8 % 80-120 12-DEC-19 Cadmium (Cd)-Dissolved 100.9 % 80-120 12-DEC-19 Chromium (Cr)-Dissolved 101.4 % 80-120 12-DEC-19 Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 3 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-D-UG/L-MS-WT Water Batch R4941530 WG3241047-2 LCS Cobalt (Co)-Dissolved 97.3 % 80-120 12-DEC-19 Copper (Cu)-Dissolved 100.4 % 80-120 12-DEC-19 Lead (Pb)-Dissolved 102.1 % 80-120 12-DEC-19 Molybdenum (Mo)-Dissolved 99.6 % 80-120 12-DEC-19 Nickel (Ni)-Dissolved 99.0 % 80-120 12-DEC-19 Selenium (Se)-Dissolved 98.7 % 80-120 12-DEC-19 Silver (Ag)-Dissolved 102.6 % 80-120 12-DEC-19 Sodium (Na)-Dissolved 101.3 % 80-120 12-DEC-19 Thallium (Tl)-Dissolved 100.6 % 80-120 12-DEC-19 Uranium (U)-Dissolved 104.0 % 80-120 12-DEC-19 Vanadium (V)-Dissolved 102.5 % 80-120 12-DEC-19 Zinc (Zn)-Dissolved 96.7 % 80-120 12-DEC-19 WG3241047-1 MB Antimony (Sb)-Dissolved <0.10 ug/L 0.1 12-DEC-19 Arsenic (As)-Dissolved <0.10 ug/L 0.1 12-DEC-19 Barium (Ba)-Dissolved <0.10 ug/L 0.1 12-DEC-19 Beryllium (Be)-Dissolved <0.10 ug/L 0.1 12-DEC-19 Boron (B)-Dissolved <10 ug/L 10 12-DEC-19 Cadmium (Cd)-Dissolved <0.0050 ug/L 0.005 12-DEC-19 Chromium (Cr)-Dissolved <0.50 ug/L 0.5 12-DEC-19 Cobalt (Co)-Dissolved <0.10 ug/L 0.1 12-DEC-19 Copper (Cu)-Dissolved <0.20 ug/L 0.2 12-DEC-19 Lead (Pb)-Dissolved <0.050 ug/L 0.05 12-DEC-19 Molybdenum (Mo)-Dissolved <0.050 ug/L 0.05 12-DEC-19 Nickel (Ni)-Dissolved <0.50 ug/L 0.5 12-DEC-19 Selenium (Se)-Dissolved <0.050 ug/L 0.05 12-DEC-19 Silver (Ag)-Dissolved <0.050 ug/L 0.05 12-DEC-19 Sodium (Na)-Dissolved <50 ug/L 50 12-DEC-19 Thallium (Tl)-Dissolved <0.010 ug/L 0.01 12-DEC-19 Uranium (U)-Dissolved <0.010 ug/L 0.01 12-DEC-19 Vanadium (V)-Dissolved <0.50 ug/L 0.5 12-DEC-19 Zinc (Zn)-Dissolved <1.0 ug/L 1 12-DEC-19 WG3241047-5 MS WG3241047-6 Antimony (Sb)-Dissolved 90.9 % 70-130 12-DEC-19 Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 4 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-D-UG/L-MS-WT Water Batch R4941530 WG3241047-5 MS WG3241047-6 Arsenic (As)-Dissolved 96.2 % 70-130 12-DEC-19 Barium (Ba)-Dissolved N/A MS-B % - 12-DEC-19 Beryllium (Be)-Dissolved 93.1 % 70-130 12-DEC-19 Boron (B)-Dissolved N/A MS-B % - 12-DEC-19 Cadmium (Cd)-Dissolved 94.9 % 70-130 12-DEC-19 Chromium (Cr)-Dissolved 90.9 % 70-130 12-DEC-19 Cobalt (Co)-Dissolved 90.7 % 70-130 12-DEC-19 Copper (Cu)-Dissolved 88.5 % 70-130 12-DEC-19 Lead (Pb)-Dissolved 93.4 % 70-130 12-DEC-19 Molybdenum (Mo)-Dissolved 97.0 % 70-130 12-DEC-19 Nickel (Ni)-Dissolved 90.3 % 70-130 12-DEC-19 Selenium (Se)-Dissolved 94.4 % 70-130 12-DEC-19 Silver (Ag)-Dissolved 87.3 % 70-130 13-DEC-19 Sodium (Na)-Dissolved N/A MS-B % - 12-DEC-19 Thallium (Tl)-Dissolved 90.4 % 70-130 12-DEC-19 Uranium (U)-Dissolved 77.4 % 70-130 12-DEC-19 Vanadium (V)-Dissolved 94.2 % 70-130 12-DEC-19 Zinc (Zn)-Dissolved 82.5 % 70-130 12-DEC-19
PAH-511-WT Water Batch R4942807 WG3241503-2 LCS 1-Methylnaphthalene 97.9 % 50-140 13-DEC-19 2-Methylnaphthalene 91.4 % 50-140 13-DEC-19 Acenaphthene 107.5 % 50-140 13-DEC-19 Acenaphthylene 110.6 % 50-140 13-DEC-19 Anthracene 116.2 % 50-140 13-DEC-19 Benzo(a)anthracene 122.6 % 50-140 13-DEC-19 Benzo(a)pyrene 115.7 % 50-140 13-DEC-19 Benzo(b)fluoranthene 113.4 % 50-140 13-DEC-19 Benzo(g,h,i)perylene 121.0 % 50-140 13-DEC-19 Benzo(k)fluoranthene 114.2 % 50-140 13-DEC-19 Chrysene 124.2 % 50-140 13-DEC-19 Dibenzo(ah)anthracene 116.7 % 50-140 13-DEC-19 Fluoranthene 119.5 % 50-140 Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 5 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Water Batch R4942807 WG3241503-2 LCS Fluoranthene 119.5 % 50-140 13-DEC-19 Fluorene 112.7 % 50-140 13-DEC-19 Indeno(1,2,3-cd)pyrene 130.2 % 50-140 13-DEC-19 Naphthalene 98.9 % 50-140 13-DEC-19 Phenanthrene 121.0 % 50-140 13-DEC-19 Pyrene 119.4 % 50-140 13-DEC-19 WG3241503-1 MB 1-Methylnaphthalene <0.020 ug/L 0.02 13-DEC-19 2-Methylnaphthalene <0.020 ug/L 0.02 13-DEC-19 Acenaphthene <0.020 ug/L 0.02 13-DEC-19 Acenaphthylene <0.020 ug/L 0.02 13-DEC-19 Anthracene <0.020 ug/L 0.02 13-DEC-19 Benzo(a)anthracene <0.020 ug/L 0.02 13-DEC-19 Benzo(a)pyrene <0.010 ug/L 0.01 13-DEC-19 Benzo(b)fluoranthene <0.020 ug/L 0.02 13-DEC-19 Benzo(g,h,i)perylene <0.020 ug/L 0.02 13-DEC-19 Benzo(k)fluoranthene <0.020 ug/L 0.02 13-DEC-19 Chrysene <0.020 ug/L 0.02 13-DEC-19 Dibenzo(ah)anthracene <0.020 ug/L 0.02 13-DEC-19 Fluoranthene <0.020 ug/L 0.02 13-DEC-19 Fluorene <0.020 ug/L 0.02 13-DEC-19 Indeno(1,2,3-cd)pyrene <0.020 ug/L 0.02 13-DEC-19 Naphthalene <0.050 ug/L 0.05 13-DEC-19 Phenanthrene <0.020 ug/L 0.02 13-DEC-19 Pyrene <0.020 ug/L 0.02 13-DEC-19 Surrogate: d8-Naphthalene 95.3 % 60-140 13-DEC-19 Surrogate: d10-Phenanthrene 98.1 % 60-140 13-DEC-19 Surrogate: d12-Chrysene 95.1 % 60-140 13-DEC-19 Surrogate: d10-Acenaphthene 93.7 % 60-140 13-DEC-19
VOC-511-HS-WT Water Batch R4943663 WG3235779-4 DUP WG3235779-3 1,1,1,2-Tetrachloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,1,2,2-Tetrachloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 6 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4943663 WG3235779-4 DUP WG3235779-3 1,1,1-Trichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,1,2-Trichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,1-Dichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,1-Dichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,2-Dibromoethane <0.20 <0.20 RPD-NA ug/L N/A 30 16-DEC-19 1,2-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,2-Dichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,2-Dichloropropane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,3-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 1,4-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 Acetone <30 <30 RPD-NA ug/L N/A 30 16-DEC-19 Benzene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 Bromodichloromethane <2.0 <2.0 RPD-NA ug/L N/A 30 16-DEC-19 Bromoform <5.0 <5.0 RPD-NA ug/L N/A 30 16-DEC-19 Bromomethane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 Carbon tetrachloride <0.20 <0.20 RPD-NA ug/L N/A 30 16-DEC-19 Chlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 Chloroform <1.0 <1.0 RPD-NA ug/L N/A 30 16-DEC-19 cis-1,2-Dichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 cis-1,3-Dichloropropene <0.30 <0.30 RPD-NA ug/L N/A 30 16-DEC-19 Dibromochloromethane <2.0 <2.0 RPD-NA ug/L N/A 30 16-DEC-19 Dichlorodifluoromethane <2.0 <2.0 RPD-NA ug/L N/A 30 16-DEC-19 Ethylbenzene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 n-Hexane <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 m+p-Xylenes <0.40 <0.40 RPD-NA ug/L N/A 30 16-DEC-19 Methyl Ethyl Ketone <20 <20 RPD-NA ug/L N/A 30 16-DEC-19 Methyl Isobutyl Ketone <20 <20 RPD-NA ug/L N/A 30 16-DEC-19 Methylene Chloride <5.0 <5.0 RPD-NA ug/L N/A 30 16-DEC-19 MTBE <2.0 <2.0 RPD-NA ug/L N/A 30 16-DEC-19 o-Xylene <0.30 <0.30 RPD-NA ug/L N/A 30 16-DEC-19 Styrene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 Tetrachloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 Toluene <0.50 <0.50 ug/L 16-DEC-19 Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 7 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4943663 WG3235779-4 DUP WG3235779-3 Toluene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 trans-1,2-Dichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 trans-1,3-Dichloropropene <0.30 <0.30 RPD-NA ug/L N/A 30 16-DEC-19 Trichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 Trichlorofluoromethane <5.0 <5.0 RPD-NA ug/L N/A 30 16-DEC-19 Vinyl chloride <0.50 <0.50 RPD-NA ug/L N/A 30 16-DEC-19 WG3235779-1 LCS 1,1,1,2-Tetrachloroethane 87.1 % 70-130 16-DEC-19 1,1,2,2-Tetrachloroethane 99.98 % 70-130 16-DEC-19 1,1,1-Trichloroethane 94.0 % 70-130 16-DEC-19 1,1,2-Trichloroethane 93.2 % 70-130 16-DEC-19 1,1-Dichloroethane 96.2 % 70-130 16-DEC-19 1,1-Dichloroethylene 90.8 % 70-130 16-DEC-19 1,2-Dibromoethane 94.4 % 70-130 16-DEC-19 1,2-Dichlorobenzene 84.6 % 70-130 16-DEC-19 1,2-Dichloroethane 105.3 % 70-130 16-DEC-19 1,2-Dichloropropane 92.2 % 70-130 16-DEC-19 1,3-Dichlorobenzene 88.5 % 70-130 16-DEC-19 1,4-Dichlorobenzene 89.3 % 70-130 16-DEC-19 Acetone 101.1 % 60-140 16-DEC-19 Benzene 98.9 % 70-130 16-DEC-19 Bromodichloromethane 94.5 % 70-130 16-DEC-19 Bromoform 88.5 % 70-130 16-DEC-19 Bromomethane 87.6 % 60-140 16-DEC-19 Carbon tetrachloride 96.1 % 70-130 16-DEC-19 Chlorobenzene 86.0 % 70-130 16-DEC-19 Chloroform 98.9 % 70-130 16-DEC-19 cis-1,2-Dichloroethylene 87.5 % 70-130 16-DEC-19 cis-1,3-Dichloropropene 94.1 % 70-130 16-DEC-19 Dibromochloromethane 87.4 % 70-130 16-DEC-19 Dichlorodifluoromethane 94.8 % 50-140 16-DEC-19 Ethylbenzene 87.6 % 70-130 16-DEC-19 n-Hexane 91.5 % 70-130 16-DEC-19 Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 8 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4943663 WG3235779-1 LCS m+p-Xylenes 89.0 % 70-130 16-DEC-19 Methyl Ethyl Ketone 99.3 % 60-140 16-DEC-19 Methyl Isobutyl Ketone 86.4 % 60-140 16-DEC-19 Methylene Chloride 93.4 % 70-130 16-DEC-19 MTBE 95.9 % 70-130 16-DEC-19 o-Xylene 87.4 % 70-130 16-DEC-19 Styrene 87.4 % 70-130 16-DEC-19 Tetrachloroethylene 88.6 % 70-130 16-DEC-19 Toluene 89.5 % 70-130 16-DEC-19 trans-1,2-Dichloroethylene 93.5 % 70-130 16-DEC-19 trans-1,3-Dichloropropene 88.0 % 70-130 16-DEC-19 Trichloroethylene 94.0 % 70-130 16-DEC-19 Trichlorofluoromethane 97.2 % 60-140 16-DEC-19 Vinyl chloride 102.5 % 60-140 16-DEC-19 WG3235779-2 MB 1,1,1,2-Tetrachloroethane <0.50 ug/L 0.5 16-DEC-19 1,1,2,2-Tetrachloroethane <0.50 ug/L 0.5 16-DEC-19 1,1,1-Trichloroethane <0.50 ug/L 0.5 16-DEC-19 1,1,2-Trichloroethane <0.50 ug/L 0.5 16-DEC-19 1,1-Dichloroethane <0.50 ug/L 0.5 16-DEC-19 1,1-Dichloroethylene <0.50 ug/L 0.5 16-DEC-19 1,2-Dibromoethane <0.20 ug/L 0.2 16-DEC-19 1,2-Dichlorobenzene <0.50 ug/L 0.5 16-DEC-19 1,2-Dichloroethane <0.50 ug/L 0.5 16-DEC-19 1,2-Dichloropropane <0.50 ug/L 0.5 16-DEC-19 1,3-Dichlorobenzene <0.50 ug/L 0.5 16-DEC-19 1,4-Dichlorobenzene <0.50 ug/L 0.5 16-DEC-19 Acetone <30 ug/L 30 16-DEC-19 Benzene <0.50 ug/L 0.5 16-DEC-19 Bromodichloromethane <2.0 ug/L 2 16-DEC-19 Bromoform <5.0 ug/L 5 16-DEC-19 Bromomethane <0.50 ug/L 0.5 16-DEC-19 Carbon tetrachloride <0.20 ug/L 0.2 16-DEC-19 Chlorobenzene <0.50 ug/L 0.5 16-DEC-19 Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 9 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4943663 WG3235779-2 MB Chloroform <1.0 ug/L 1 16-DEC-19 cis-1,2-Dichloroethylene <0.50 ug/L 0.5 16-DEC-19 cis-1,3-Dichloropropene <0.30 ug/L 0.3 16-DEC-19 Dibromochloromethane <2.0 ug/L 2 16-DEC-19 Dichlorodifluoromethane <2.0 ug/L 2 16-DEC-19 Ethylbenzene <0.50 ug/L 0.5 16-DEC-19 n-Hexane <0.50 ug/L 0.5 16-DEC-19 m+p-Xylenes <0.40 ug/L 0.4 16-DEC-19 Methyl Ethyl Ketone <20 ug/L 20 16-DEC-19 Methyl Isobutyl Ketone <20 ug/L 20 16-DEC-19 Methylene Chloride <5.0 ug/L 5 16-DEC-19 MTBE <2.0 ug/L 2 16-DEC-19 o-Xylene <0.30 ug/L 0.3 16-DEC-19 Styrene <0.50 ug/L 0.5 16-DEC-19 Tetrachloroethylene <0.50 ug/L 0.5 16-DEC-19 Toluene <0.50 ug/L 0.5 16-DEC-19 trans-1,2-Dichloroethylene <0.50 ug/L 0.5 16-DEC-19 trans-1,3-Dichloropropene <0.30 ug/L 0.3 16-DEC-19 Trichloroethylene <0.50 ug/L 0.5 16-DEC-19 Trichlorofluoromethane <5.0 ug/L 5 16-DEC-19 Vinyl chloride <0.50 ug/L 0.5 16-DEC-19 Surrogate: 1,4-Difluorobenzene 102.2 % 70-130 16-DEC-19 Surrogate: 4-Bromofluorobenzene 96.6 % 70-130 16-DEC-19 WG3235779-5 MS WG3235779-3 1,1,1,2-Tetrachloroethane 86.3 % 50-140 16-DEC-19 1,1,2,2-Tetrachloroethane 94.8 % 50-140 16-DEC-19 1,1,1-Trichloroethane 94.0 % 50-140 16-DEC-19 1,1,2-Trichloroethane 89.8 % 50-140 16-DEC-19 1,1-Dichloroethane 96.7 % 50-140 16-DEC-19 1,1-Dichloroethylene 89.4 % 50-140 16-DEC-19 1,2-Dibromoethane 89.9 % 50-140 16-DEC-19 1,2-Dichlorobenzene 85.5 % 50-140 16-DEC-19 1,2-Dichloroethane 102.4 % 50-140 16-DEC-19 1,2-Dichloropropane 91.8 % 50-140 16-DEC-19 Quality Control Report
Workorder: L2395477 Report Date: 16-DEC-19 Page 10 of 11
Client: Morrison Hershfield Limited (Ottawa) 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R4943663 WG3235779-5 MS WG3235779-3 1,3-Dichlorobenzene 90.2 % 50-140 16-DEC-19 1,4-Dichlorobenzene 91.3 % 50-140 16-DEC-19 Acetone 97.1 % 50-140 16-DEC-19 Benzene 98.9 % 50-140 16-DEC-19 Bromodichloromethane 93.4 % 50-140 16-DEC-19 Bromoform 83.8 % 50-140 16-DEC-19 Bromomethane 83.1 % 50-140 16-DEC-19 Carbon tetrachloride 95.8 % 50-140 16-DEC-19 Chlorobenzene 85.6 % 50-140 16-DEC-19 Chloroform 98.9 % 50-140 16-DEC-19 cis-1,2-Dichloroethylene 86.4 % 50-140 16-DEC-19 cis-1,3-Dichloropropene 90.0 % 50-140 16-DEC-19 Dibromochloromethane 84.3 % 50-140 16-DEC-19 Dichlorodifluoromethane 86.2 % 50-140 16-DEC-19 Ethylbenzene 88.3 % 50-140 16-DEC-19 n-Hexane 88.8 % 50-140 16-DEC-19 m+p-Xylenes 90.1 % 50-140 16-DEC-19 Methyl Ethyl Ketone 86.0 % 50-140 16-DEC-19 Methyl Isobutyl Ketone 79.2 % 50-140 16-DEC-19 Methylene Chloride 91.7 % 50-140 16-DEC-19 MTBE 95.8 % 50-140 16-DEC-19 o-Xylene 88.0 % 50-140 16-DEC-19 Styrene 86.4 % 50-140 16-DEC-19 Tetrachloroethylene 88.9 % 50-140 16-DEC-19 Toluene 89.8 % 50-140 16-DEC-19 trans-1,2-Dichloroethylene 93.0 % 50-140 16-DEC-19 trans-1,3-Dichloropropene 82.1 % 50-140 16-DEC-19 Trichloroethylene 94.5 % 50-140 16-DEC-19 Trichlorofluoromethane 94.2 % 50-140 16-DEC-19 Vinyl chloride 97.5 % 50-140 16-DEC-19 Quality Control Report Workorder: L2395477 Report Date: 16-DEC-19
Client: Morrison Hershfield Limited (Ottawa) Page 11 of 11 2932 Baseline Rd Ottawa ON K2H 1B1 Contact: Mitchell Dawley
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description MS-B Matrix Spike recovery could not be accurately calculated due to high analyte background in sample. RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order. ALS Sample ID: L2395477-1 Client Sample ID: BH5 500
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Printed on 12/13/2019 5:51:00 PM ALS Sample ID: L2395477-2 Client Sample ID: BH6 500
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Printed on 12/13/2019 5:51:02 PM ALS Sample ID: L2395477-3 Client Sample ID: BH7 500
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Printed on 12/13/2019 5:51:04 PM ALS Sample ID: L2395477-4 Client Sample ID: BH8 500
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Printed on 12/13/2019 8:11:40 PM ALS Sample ID: L2395477-5 Client Sample ID: DUP 500
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Morrison Hershfield Limited (Ottawa) Date Received: 24-JUL-20 ATTN: Mitchell Dawley Report Date: 31-JUL-20 14:42 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2479593 Project P.O. #: NOT SUBMITTED Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2479593 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 15 190441800 31-JUL-20 14:42 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2479593-1 BH 11 SA2 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 10.1 0.25 % 29-JUL-20 Metals Antimony (Sb) <1.0 1.0 ug/g 30-JUL-20 1.3 7.5 40 Arsenic (As) 2.2 1.0 ug/g 30-JUL-20 18 18 18 Barium (Ba) 33.8 1.0 ug/g 30-JUL-20 220 390 670 Beryllium (Be) <0.50 0.50 ug/g 30-JUL-20 2.5 4 8 Boron (B) <5.0 5.0 ug/g 30-JUL-20 36 120 120 Boron (B), Hot Water Ext. 0.34 0.10 ug/g 30-JUL-20 36 1.5 2 Cadmium (Cd) <0.50 0.50 ug/g 30-JUL-20 1.2 1.2 1.9 Chromium (Cr) 16.2 1.0 ug/g 30-JUL-20 70 160 160 Cobalt (Co) 3.6 1.0 ug/g 30-JUL-20 21 22 80 Copper (Cu) 7.6 1.0 ug/g 30-JUL-20 92 140 230 Lead (Pb) 22.0 1.0 ug/g 30-JUL-20 120 120 120 Mercury (Hg) 0.0172 0.0050 ug/g 30-JUL-20 0.27 0.27 3.9 Molybdenum (Mo) <1.0 1.0 ug/g 30-JUL-20 2 6.9 40 Nickel (Ni) 9.2 1.0 ug/g 30-JUL-20 82 100 270 Selenium (Se) <1.0 1.0 ug/g 30-JUL-20 1.5 2.4 5.5 Silver (Ag) <0.20 0.20 ug/g 30-JUL-20 0.5 20 40 Thallium (Tl) <0.50 0.50 ug/g 30-JUL-20 1 1 3.3 Uranium (U) <1.0 1.0 ug/g 30-JUL-20 2.5 23 33 Vanadium (V) 22.1 1.0 ug/g 30-JUL-20 86 86 86 Zinc (Zn) 224 5.0 ug/g 30-JUL-20 290 340 340 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 30-JUL-20 0.66 8 8
L2479593-2 BH 11 SA3 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 23.6 0.25 % 29-JUL-20 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 29-JUL-20 0.5 16 16 Benzene 0.0299 0.0068 ug/g 29-JUL-20 *0.02 0.21 0.32 Bromodichloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 13 18 Bromoform <0.050 0.050 ug/g 29-JUL-20 0.05 0.27 0.61 Bromomethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.21 Chlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 2.4 2.4 Dibromochloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 9.4 13 Chloroform <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.47 1,2-Dibromoethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 3.4 6.8 1,3-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 4.8 9.6 1,4-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 0.083 0.2 Dichlorodifluoromethane <0.050 0.050 ug/g 29-JUL-20 0.05 16 16
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
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L2479593-2 BH 11 SA3 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds 1,1-Dichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 3.5 17 1,2-Dichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.064 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 3.4 55 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.084 1.3 Methylene Chloride <0.050 0.050 ug/g 29-JUL-20 0.05 0.1 1.6 1,2-Dichloropropane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.16 cis-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 trans-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 29-JUL-20 0.05 0.05 0.18 Ethylbenzene <0.018 0.018 ug/g 29-JUL-20 0.05 2 9.5 n-Hexane <0.050 0.050 ug/g 29-JUL-20 0.05 2.8 46 Methyl Ethyl Ketone <0.50 0.50 ug/g 29-JUL-20 0.5 16 70 Methyl Isobutyl Ketone <0.50 0.50 ug/g 29-JUL-20 0.5 1.7 31 MTBE <0.050 0.050 ug/g 29-JUL-20 0.05 0.75 11 Styrene <0.050 0.050 ug/g 29-JUL-20 0.05 0.7 34 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.058 0.087 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.28 4.5 Toluene <0.080 0.080 ug/g 29-JUL-20 0.2 2.3 68 1,1,1-Trichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.38 6.1 1,1,2-Trichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 29-JUL-20 0.05 0.061 0.91 Trichlorofluoromethane <0.050 0.050 ug/g 29-JUL-20 0.25 4 4 Vinyl chloride <0.020 0.020 ug/g 29-JUL-20 0.02 0.02 0.032 o-Xylene <0.020 0.020 ug/g 29-JUL-20 m+p-Xylenes <0.030 0.030 ug/g 29-JUL-20 Xylenes (Total) <0.050 0.050 ug/g 29-JUL-20 0.05 3.1 26 Surrogate: 4-Bromofluorobenzene 81.7 50-140 % 29-JUL-20 Surrogate: 1,4-Difluorobenzene 95.5 50-140 % 29-JUL-20 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 29-JUL-20 25 55 55 F1-BTEX <5.0 5.0 ug/g 30-JUL-20 25 55 55 F2 (C10-C16) <10 10 ug/g 29-JUL-20 10 98 230 F2-Naphth <10 10 ug/g 30-JUL-20 F3 (C16-C34) <50 50 ug/g 29-JUL-20 240 300 1700 F3-PAH <50 50 ug/g 30-JUL-20 F4 (C34-C50) <50 50 ug/g 29-JUL-20 120 2800 3300 Total Hydrocarbons (C6-C50) <72 72 ug/g 30-JUL-20 Chrom. to baseline at nC50 YES No Unit 29-JUL-20 Surrogate: 2-Bromobenzotrifluoride 82.8 60-140 % 29-JUL-20 Surrogate: 3,4-Dichlorotoluene 98.3 60-140 % 29-JUL-20 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 30-JUL-20 0.072 7.9 96 Acenaphthylene <0.050 0.050 ug/g 30-JUL-20 0.093 0.15 0.15 Anthracene <0.050 0.050 ug/g 30-JUL-20 0.16 0.67 0.67
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
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L2479593-2 BH 11 SA3 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Benzo(a)anthracene <0.050 0.050 ug/g 30-JUL-20 0.36 0.5 0.96 Benzo(a)pyrene <0.050 0.050 ug/g 30-JUL-20 0.3 0.3 0.3 Benzo(b)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.47 0.78 0.96 Benzo(g,h,i)perylene <0.050 0.050 ug/g 30-JUL-20 0.68 6.6 9.6 Benzo(k)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.48 0.78 0.96 Chrysene <0.050 0.050 ug/g 30-JUL-20 2.8 7 9.6 Dibenzo(ah)anthracene <0.050 0.050 ug/g 30-JUL-20 0.1 0.1 0.1 Fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.56 0.69 9.6 Fluorene <0.050 0.050 ug/g 30-JUL-20 0.12 62 62 Indeno(1,2,3-cd)pyrene <0.050 0.050 ug/g 30-JUL-20 0.23 0.38 0.76 1+2-Methylnaphthalenes 0.063 0.042 ug/g 30-JUL-20 0.59 0.99 76 1-Methylnaphthalene 0.063 0.030 ug/g 30-JUL-20 0.59 0.99 76 2-Methylnaphthalene <0.030 0.030 ug/g 30-JUL-20 0.59 0.99 76 Naphthalene <0.013 0.013 ug/g 30-JUL-20 0.09 0.6 9.6 Phenanthrene <0.046 0.046 ug/g 30-JUL-20 0.69 6.2 12 Pyrene <0.050 0.050 ug/g 30-JUL-20 1 78 96 Surrogate: 2-Fluorobiphenyl 97.0 50-140 % 30-JUL-20 Surrogate: p-Terphenyl d14 111.9 50-140 % 30-JUL-20
L2479593-3 BH 11 SA7 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 15.8 0.25 % 29-JUL-20 Hydrocarbons F2 (C10-C16) <10 10 ug/g 29-JUL-20 10 98 230 F3 (C16-C34) <50 50 ug/g 29-JUL-20 240 300 1700 F4 (C34-C50) <50 50 ug/g 29-JUL-20 120 2800 3300 Chrom. to baseline at nC50 YES No Unit 29-JUL-20 Surrogate: 2-Bromobenzotrifluoride 90.8 60-140 % 29-JUL-20
L2479593-4 BH 12 SA2 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 9.14 0.25 % 29-JUL-20 Metals Antimony (Sb) 1.3 1.0 ug/g 30-JUL-20 1.3 7.5 40 Arsenic (As) 8.0 1.0 ug/g 30-JUL-20 18 18 18 Barium (Ba) 82.3 1.0 ug/g 30-JUL-20 220 390 670 Beryllium (Be) <0.50 0.50 ug/g 30-JUL-20 2.5 4 8 Boron (B) 5.8 5.0 ug/g 30-JUL-20 36 120 120 Boron (B), Hot Water Ext. 0.24 0.10 ug/g 30-JUL-20 36 1.5 2 Cadmium (Cd) <0.50 0.50 ug/g 30-JUL-20 1.2 1.2 1.9 Chromium (Cr) 18.0 1.0 ug/g 30-JUL-20 70 160 160
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
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L2479593-4 BH 12 SA2 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Metals Cobalt (Co) 6.9 1.0 ug/g 30-JUL-20 21 22 80 Copper (Cu) 23.6 1.0 ug/g 30-JUL-20 92 140 230 Lead (Pb) 61.3 1.0 ug/g 30-JUL-20 120 120 120 Mercury (Hg) 0.0793 0.0050 ug/g 30-JUL-20 0.27 0.27 3.9 Molybdenum (Mo) 2.6 1.0 ug/g 30-JUL-20 *2 6.9 40 Nickel (Ni) 14.9 1.0 ug/g 30-JUL-20 82 100 270 Selenium (Se) <1.0 1.0 ug/g 30-JUL-20 1.5 2.4 5.5 Silver (Ag) <0.20 0.20 ug/g 30-JUL-20 0.5 20 40 Thallium (Tl) <0.50 0.50 ug/g 30-JUL-20 1 1 3.3 Uranium (U) <1.0 1.0 ug/g 30-JUL-20 2.5 23 33 Vanadium (V) 27.9 1.0 ug/g 30-JUL-20 86 86 86 Zinc (Zn) 98.3 5.0 ug/g 30-JUL-20 290 340 340 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 30-JUL-20 0.66 8 8
L2479593-5 BH 12 SA7 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 15.7 0.25 % 29-JUL-20 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 29-JUL-20 0.5 16 16 Benzene <0.0068 0.0068 ug/g 29-JUL-20 0.02 0.21 0.32 Bromodichloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 13 18 Bromoform <0.050 0.050 ug/g 29-JUL-20 0.05 0.27 0.61 Bromomethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.21 Chlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 2.4 2.4 Dibromochloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 9.4 13 Chloroform <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.47 1,2-Dibromoethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 3.4 6.8 1,3-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 4.8 9.6 1,4-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 0.083 0.2 Dichlorodifluoromethane <0.050 0.050 ug/g 29-JUL-20 0.05 16 16 1,1-Dichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 3.5 17 1,2-Dichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.064 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 3.4 55 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.084 1.3 Methylene Chloride <0.050 0.050 ug/g 29-JUL-20 0.05 0.1 1.6 1,2-Dichloropropane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.16 cis-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 trans-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 29-JUL-20 0.05 0.05 0.18
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
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L2479593-5 BH 12 SA7 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds Ethylbenzene <0.018 0.018 ug/g 29-JUL-20 0.05 2 9.5 n-Hexane <0.050 0.050 ug/g 29-JUL-20 0.05 2.8 46 Methyl Ethyl Ketone <0.50 0.50 ug/g 29-JUL-20 0.5 16 70 Methyl Isobutyl Ketone <0.50 0.50 ug/g 29-JUL-20 0.5 1.7 31 MTBE <0.050 0.050 ug/g 29-JUL-20 0.05 0.75 11 Styrene <0.050 0.050 ug/g 29-JUL-20 0.05 0.7 34 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.058 0.087 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.28 4.5 Toluene <0.080 0.080 ug/g 29-JUL-20 0.2 2.3 68 1,1,1-Trichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.38 6.1 1,1,2-Trichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 29-JUL-20 0.05 0.061 0.91 Trichlorofluoromethane <0.050 0.050 ug/g 29-JUL-20 0.25 4 4 Vinyl chloride <0.020 0.020 ug/g 29-JUL-20 0.02 0.02 0.032 o-Xylene <0.020 0.020 ug/g 29-JUL-20 m+p-Xylenes <0.030 0.030 ug/g 29-JUL-20 Xylenes (Total) <0.050 0.050 ug/g 29-JUL-20 0.05 3.1 26 Surrogate: 4-Bromofluorobenzene 88.4 50-140 % 29-JUL-20 Surrogate: 1,4-Difluorobenzene 103.9 50-140 % 29-JUL-20 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 29-JUL-20 25 55 55 F1-BTEX <5.0 5.0 ug/g 30-JUL-20 25 55 55 F2 (C10-C16) <10 10 ug/g 29-JUL-20 10 98 230 F2-Naphth <10 10 ug/g 30-JUL-20 F3 (C16-C34) <50 50 ug/g 29-JUL-20 240 300 1700 F3-PAH <50 50 ug/g 30-JUL-20 F4 (C34-C50) <50 50 ug/g 29-JUL-20 120 2800 3300 Total Hydrocarbons (C6-C50) <72 72 ug/g 30-JUL-20 Chrom. to baseline at nC50 YES No Unit 29-JUL-20 Surrogate: 2-Bromobenzotrifluoride 87.4 60-140 % 29-JUL-20 Surrogate: 3,4-Dichlorotoluene 103.7 60-140 % 29-JUL-20 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 30-JUL-20 0.072 7.9 96 Acenaphthylene <0.050 0.050 ug/g 30-JUL-20 0.093 0.15 0.15 Anthracene <0.050 0.050 ug/g 30-JUL-20 0.16 0.67 0.67 Benzo(a)anthracene <0.050 0.050 ug/g 30-JUL-20 0.36 0.5 0.96 Benzo(a)pyrene <0.050 0.050 ug/g 30-JUL-20 0.3 0.3 0.3 Benzo(b)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.47 0.78 0.96 Benzo(g,h,i)perylene <0.050 0.050 ug/g 30-JUL-20 0.68 6.6 9.6 Benzo(k)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.48 0.78 0.96 Chrysene <0.050 0.050 ug/g 30-JUL-20 2.8 7 9.6 Dibenzo(ah)anthracene <0.050 0.050 ug/g 30-JUL-20 0.1 0.1 0.1 Fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.56 0.69 9.6 Fluorene <0.050 0.050 ug/g 30-JUL-20 0.12 62 62 Indeno(1,2,3-cd)pyrene <0.050 0.050 ug/g 30-JUL-20 0.23 0.38 0.76 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
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L2479593-5 BH 12 SA7 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons 1+2-Methylnaphthalenes <0.042 0.042 ug/g 30-JUL-20 0.59 0.99 76 1-Methylnaphthalene <0.030 0.030 ug/g 30-JUL-20 0.59 0.99 76 2-Methylnaphthalene <0.030 0.030 ug/g 30-JUL-20 0.59 0.99 76 Naphthalene <0.013 0.013 ug/g 30-JUL-20 0.09 0.6 9.6 Phenanthrene <0.046 0.046 ug/g 30-JUL-20 0.69 6.2 12 Pyrene <0.050 0.050 ug/g 30-JUL-20 1 78 96 Surrogate: 2-Fluorobiphenyl 96.7 50-140 % 30-JUL-20 Surrogate: p-Terphenyl d14 110.9 50-140 % 30-JUL-20
L2479593-6 BH 12 SA17 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 15.8 0.25 % 29-JUL-20 Hydrocarbons F2 (C10-C16) <10 10 ug/g 29-JUL-20 10 98 230 F2-Naphth <10 10 ug/g 30-JUL-20 F3 (C16-C34) <50 50 ug/g 29-JUL-20 240 300 1700 F3-PAH <50 50 ug/g 30-JUL-20 F4 (C34-C50) <50 50 ug/g 29-JUL-20 120 2800 3300 Chrom. to baseline at nC50 YES No Unit 29-JUL-20 Surrogate: 2-Bromobenzotrifluoride 82.6 60-140 % 29-JUL-20 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 30-JUL-20 0.072 7.9 96 Acenaphthylene <0.050 0.050 ug/g 30-JUL-20 0.093 0.15 0.15 Anthracene <0.050 0.050 ug/g 30-JUL-20 0.16 0.67 0.67 Benzo(a)anthracene <0.050 0.050 ug/g 30-JUL-20 0.36 0.5 0.96 Benzo(a)pyrene <0.050 0.050 ug/g 30-JUL-20 0.3 0.3 0.3 Benzo(b)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.47 0.78 0.96 Benzo(g,h,i)perylene <0.050 0.050 ug/g 30-JUL-20 0.68 6.6 9.6 Benzo(k)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.48 0.78 0.96 Chrysene <0.050 0.050 ug/g 30-JUL-20 2.8 7 9.6 Dibenzo(ah)anthracene <0.050 0.050 ug/g 30-JUL-20 0.1 0.1 0.1 Fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.56 0.69 9.6 Fluorene <0.050 0.050 ug/g 30-JUL-20 0.12 62 62 Indeno(1,2,3-cd)pyrene <0.050 0.050 ug/g 30-JUL-20 0.23 0.38 0.76 1+2-Methylnaphthalenes <0.042 0.042 ug/g 30-JUL-20 0.59 0.99 76 1-Methylnaphthalene <0.030 0.030 ug/g 30-JUL-20 0.59 0.99 76 2-Methylnaphthalene <0.030 0.030 ug/g 30-JUL-20 0.59 0.99 76 Naphthalene <0.013 0.013 ug/g 30-JUL-20 0.09 0.6 9.6 Phenanthrene <0.046 0.046 ug/g 30-JUL-20 0.69 6.2 12 Pyrene <0.050 0.050 ug/g 30-JUL-20 1 78 96 Surrogate: 2-Fluorobiphenyl 98.9 50-140 % 30-JUL-20 Surrogate: p-Terphenyl d14 113.5 50-140 % 30-JUL-20
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) L2479593 CONTD.... ANALYTICAL GUIDELINE REPORT Page 8 of 15 190441800 31-JUL-20 14:42 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2479593-7 BH 13 SA5 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 13.6 0.25 % 29-JUL-20 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 29-JUL-20 0.5 16 16 Benzene 0.0388 0.0068 ug/g 29-JUL-20 *0.02 0.21 0.32 Bromodichloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 13 18 Bromoform <0.050 0.050 ug/g 29-JUL-20 0.05 0.27 0.61 Bromomethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.21 Chlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 2.4 2.4 Dibromochloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 9.4 13 Chloroform <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.47 1,2-Dibromoethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 3.4 6.8 1,3-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 4.8 9.6 1,4-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 0.083 0.2 Dichlorodifluoromethane <0.050 0.050 ug/g 29-JUL-20 0.05 16 16 1,1-Dichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 3.5 17 1,2-Dichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.064 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 3.4 55 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.084 1.3 Methylene Chloride <0.050 0.050 ug/g 29-JUL-20 0.05 0.1 1.6 1,2-Dichloropropane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.16 cis-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 trans-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 29-JUL-20 0.05 0.05 0.18 Ethylbenzene 0.024 0.018 ug/g 29-JUL-20 0.05 2 9.5 n-Hexane <0.050 0.050 ug/g 29-JUL-20 0.05 2.8 46 Methyl Ethyl Ketone <0.50 0.50 ug/g 29-JUL-20 0.5 16 70 Methyl Isobutyl Ketone <0.50 0.50 ug/g 29-JUL-20 0.5 1.7 31 MTBE <0.050 0.050 ug/g 29-JUL-20 0.05 0.75 11 Styrene <0.050 0.050 ug/g 29-JUL-20 0.05 0.7 34 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.058 0.087 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.28 4.5 Toluene <0.080 0.080 ug/g 29-JUL-20 0.2 2.3 68 1,1,1-Trichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.38 6.1 1,1,2-Trichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 29-JUL-20 0.05 0.061 0.91 Trichlorofluoromethane <0.050 0.050 ug/g 29-JUL-20 0.25 4 4 Vinyl chloride <0.020 0.020 ug/g 29-JUL-20 0.02 0.02 0.032 o-Xylene <0.020 0.020 ug/g 29-JUL-20 m+p-Xylenes 0.055 0.030 ug/g 29-JUL-20 Xylenes (Total) 0.055 0.050 ug/g 29-JUL-20 *0.05 3.1 26 Surrogate: 4-Bromofluorobenzene 87.9 50-140 % 29-JUL-20 Surrogate: 1,4-Difluorobenzene 101.3 50-140 % 29-JUL-20 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) L2479593 CONTD.... ANALYTICAL GUIDELINE REPORT Page 9 of 15 190441800 31-JUL-20 14:42 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2479593-7 BH 13 SA5 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Hydrocarbons F1 (C6-C10) 6.8 5.0 ug/g 29-JUL-20 25 55 55 F1-BTEX 6.7 5.0 ug/g 30-JUL-20 25 55 55 F2 (C10-C16) <10 10 ug/g 29-JUL-20 10 98 230 F2-Naphth <10 10 ug/g 30-JUL-20 F3 (C16-C34) <50 50 ug/g 29-JUL-20 240 300 1700 F3-PAH <50 50 ug/g 30-JUL-20 F4 (C34-C50) <50 50 ug/g 29-JUL-20 120 2800 3300 Total Hydrocarbons (C6-C50) <72 72 ug/g 30-JUL-20 Chrom. to baseline at nC50 YES No Unit 29-JUL-20 Surrogate: 2-Bromobenzotrifluoride 75.7 60-140 % 29-JUL-20 Surrogate: 3,4-Dichlorotoluene 99.4 60-140 % 29-JUL-20 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 30-JUL-20 0.072 7.9 96 Acenaphthylene <0.050 0.050 ug/g 30-JUL-20 0.093 0.15 0.15 Anthracene <0.050 0.050 ug/g 30-JUL-20 0.16 0.67 0.67 Benzo(a)anthracene <0.050 0.050 ug/g 30-JUL-20 0.36 0.5 0.96 Benzo(a)pyrene <0.050 0.050 ug/g 30-JUL-20 0.3 0.3 0.3 Benzo(b)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.47 0.78 0.96 Benzo(g,h,i)perylene <0.050 0.050 ug/g 30-JUL-20 0.68 6.6 9.6 Benzo(k)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.48 0.78 0.96 Chrysene <0.050 0.050 ug/g 30-JUL-20 2.8 7 9.6 Dibenzo(ah)anthracene <0.050 0.050 ug/g 30-JUL-20 0.1 0.1 0.1 Fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.56 0.69 9.6 Fluorene <0.050 0.050 ug/g 30-JUL-20 0.12 62 62 Indeno(1,2,3-cd)pyrene <0.050 0.050 ug/g 30-JUL-20 0.23 0.38 0.76 1+2-Methylnaphthalenes 0.082 0.042 ug/g 30-JUL-20 0.59 0.99 76 1-Methylnaphthalene 0.045 0.030 ug/g 30-JUL-20 0.59 0.99 76 2-Methylnaphthalene 0.037 0.030 ug/g 30-JUL-20 0.59 0.99 76 Naphthalene 0.023 R 0.013 ug/g 30-JUL-20 0.09 0.6 9.6 Phenanthrene <0.046 0.046 ug/g 30-JUL-20 0.69 6.2 12 Pyrene <0.050 0.050 ug/g 30-JUL-20 1 78 96 Surrogate: 2-Fluorobiphenyl 99.3 50-140 % 30-JUL-20 Surrogate: p-Terphenyl d14 115.6 50-140 % 30-JUL-20
L2479593-8 BH 13 SA7 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 8.50 0.25 % 29-JUL-20 Hydrocarbons F2 (C10-C16) 84 10 ug/g 29-JUL-20 *10 98 230 F3 (C16-C34) 72 50 ug/g 29-JUL-20 240 300 1700 F4 (C34-C50) <50 50 ug/g 29-JUL-20 120 2800 3300 Chrom. to baseline at nC50 YES No Unit 29-JUL-20 Surrogate: 2-Bromobenzotrifluoride 77.8 60-140 % 29-JUL-20
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) L2479593 CONTD.... ANALYTICAL GUIDELINE REPORT Page 10 of 15 190441800 31-JUL-20 14:42 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2479593-9 BH 13 SA15 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 17.3 0.25 % 30-JUL-20 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 30-JUL-20 0.5 16 16 Benzene 0.199 0.0068 ug/g 30-JUL-20 *0.02 0.21 0.32 Bromodichloromethane <0.050 0.050 ug/g 30-JUL-20 0.05 13 18 Bromoform <0.050 0.050 ug/g 30-JUL-20 0.05 0.27 0.61 Bromomethane <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.21 Chlorobenzene <0.050 0.050 ug/g 30-JUL-20 0.05 2.4 2.4 Dibromochloromethane <0.050 0.050 ug/g 30-JUL-20 0.05 9.4 13 Chloroform <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.47 1,2-Dibromoethane <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 30-JUL-20 0.05 3.4 6.8 1,3-Dichlorobenzene <0.050 0.050 ug/g 30-JUL-20 0.05 4.8 9.6 1,4-Dichlorobenzene <0.050 0.050 ug/g 30-JUL-20 0.05 0.083 0.2 Dichlorodifluoromethane <0.050 0.050 ug/g 30-JUL-20 0.05 16 16 1,1-Dichloroethane <0.050 0.050 ug/g 30-JUL-20 0.05 3.5 17 1,2-Dichloroethane <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.064 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 30-JUL-20 0.05 3.4 55 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 30-JUL-20 0.05 0.084 1.3 Methylene Chloride <0.050 0.050 ug/g 30-JUL-20 0.05 0.1 1.6 1,2-Dichloropropane <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.16 cis-1,3-Dichloropropene <0.030 0.030 ug/g 30-JUL-20 trans-1,3-Dichloropropene <0.030 0.030 ug/g 30-JUL-20 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 30-JUL-20 0.05 0.05 0.18 Ethylbenzene 0.087 0.018 ug/g 30-JUL-20 *0.05 2 9.5 n-Hexane 0.107 0.050 ug/g 30-JUL-20 *0.05 2.8 46 Methyl Ethyl Ketone <0.50 0.50 ug/g 30-JUL-20 0.5 16 70 Methyl Isobutyl Ketone <0.50 0.50 ug/g 30-JUL-20 0.5 1.7 31 MTBE <0.050 0.050 ug/g 30-JUL-20 0.05 0.75 11 Styrene <0.050 0.050 ug/g 30-JUL-20 0.05 0.7 34 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 30-JUL-20 0.05 0.058 0.087 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 30-JUL-20 0.05 0.28 4.5 Toluene 0.148 0.080 ug/g 30-JUL-20 0.2 2.3 68 1,1,1-Trichloroethane <0.050 0.050 ug/g 30-JUL-20 0.05 0.38 6.1 1,1,2-Trichloroethane <0.050 0.050 ug/g 30-JUL-20 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 30-JUL-20 0.05 0.061 0.91 Trichlorofluoromethane <0.050 0.050 ug/g 30-JUL-20 0.25 4 4 Vinyl chloride <0.020 0.020 ug/g 30-JUL-20 0.02 0.02 0.032 o-Xylene 0.052 0.020 ug/g 30-JUL-20 m+p-Xylenes 0.202 0.030 ug/g 30-JUL-20 Xylenes (Total) 0.255 0.050 ug/g 30-JUL-20 *0.05 3.1 26 Surrogate: 4-Bromofluorobenzene 98.7 50-140 % 30-JUL-20 Surrogate: 1,4-Difluorobenzene 111.9 50-140 % 30-JUL-20 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
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L2479593-9 BH 13 SA15 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Hydrocarbons F1 (C6-C10) 17.1 5.0 ug/g 30-JUL-20 25 55 55 Surrogate: 3,4-Dichlorotoluene 106.6 60-140 % 30-JUL-20
L2479593-10 BH 14 SA5 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 8.98 0.25 % 29-JUL-20 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 29-JUL-20 0.5 16 16 Benzene <0.0068 0.0068 ug/g 29-JUL-20 0.02 0.21 0.32 Bromodichloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 13 18 Bromoform <0.050 0.050 ug/g 29-JUL-20 0.05 0.27 0.61 Bromomethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.21 Chlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 2.4 2.4 Dibromochloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 9.4 13 Chloroform <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.47 1,2-Dibromoethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 3.4 6.8 1,3-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 4.8 9.6 1,4-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 0.083 0.2 Dichlorodifluoromethane <0.050 0.050 ug/g 29-JUL-20 0.05 16 16 1,1-Dichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 3.5 17 1,2-Dichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.064 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 3.4 55 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.084 1.3 Methylene Chloride <0.050 0.050 ug/g 29-JUL-20 0.05 0.1 1.6 1,2-Dichloropropane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.16 cis-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 trans-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 29-JUL-20 0.05 0.05 0.18 Ethylbenzene <0.018 0.018 ug/g 29-JUL-20 0.05 2 9.5 n-Hexane <0.050 0.050 ug/g 29-JUL-20 0.05 2.8 46 Methyl Ethyl Ketone <0.50 0.50 ug/g 29-JUL-20 0.5 16 70 Methyl Isobutyl Ketone <0.50 0.50 ug/g 29-JUL-20 0.5 1.7 31 MTBE <0.050 0.050 ug/g 29-JUL-20 0.05 0.75 11 Styrene <0.050 0.050 ug/g 29-JUL-20 0.05 0.7 34 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.058 0.087 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.28 4.5 Toluene <0.080 0.080 ug/g 29-JUL-20 0.2 2.3 68 1,1,1-Trichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.38 6.1 1,1,2-Trichloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 29-JUL-20 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) L2479593 CONTD.... ANALYTICAL GUIDELINE REPORT Page 12 of 15 190441800 31-JUL-20 14:42 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2479593-10 BH 14 SA5 Sampled By: CLIENT on 23-JUL-20 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds 0.05 0.061 0.91 Trichlorofluoromethane <0.050 0.050 ug/g 29-JUL-20 0.25 4 4 Vinyl chloride <0.020 0.020 ug/g 29-JUL-20 0.02 0.02 0.032 o-Xylene <0.020 0.020 ug/g 29-JUL-20 m+p-Xylenes <0.030 0.030 ug/g 29-JUL-20 Xylenes (Total) <0.050 0.050 ug/g 29-JUL-20 0.05 3.1 26 Surrogate: 4-Bromofluorobenzene 87.2 50-140 % 29-JUL-20 Surrogate: 1,4-Difluorobenzene 101.5 50-140 % 29-JUL-20 Hydrocarbons F1 (C6-C10) <5.0 5.0 ug/g 29-JUL-20 25 55 55 F1-BTEX <5.0 5.0 ug/g 30-JUL-20 25 55 55 F2 (C10-C16) 34 10 ug/g 29-JUL-20 *10 98 230 F2-Naphth 34 10 ug/g 30-JUL-20 F3 (C16-C34) <50 50 ug/g 29-JUL-20 240 300 1700 F3-PAH <50 50 ug/g 30-JUL-20 F4 (C34-C50) <50 50 ug/g 29-JUL-20 120 2800 3300 Total Hydrocarbons (C6-C50) <72 72 ug/g 30-JUL-20 Chrom. to baseline at nC50 YES No Unit 29-JUL-20 Surrogate: 2-Bromobenzotrifluoride 86.4 60-140 % 29-JUL-20 Surrogate: 3,4-Dichlorotoluene 87.3 60-140 % 29-JUL-20 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.050 0.050 ug/g 30-JUL-20 0.072 7.9 96 Acenaphthylene <0.050 0.050 ug/g 30-JUL-20 0.093 0.15 0.15 Anthracene <0.050 0.050 ug/g 30-JUL-20 0.16 0.67 0.67 Benzo(a)anthracene <0.050 0.050 ug/g 30-JUL-20 0.36 0.5 0.96 Benzo(a)pyrene <0.050 0.050 ug/g 30-JUL-20 0.3 0.3 0.3 Benzo(b)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.47 0.78 0.96 Benzo(g,h,i)perylene <0.050 0.050 ug/g 30-JUL-20 0.68 6.6 9.6 Benzo(k)fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.48 0.78 0.96 Chrysene <0.050 0.050 ug/g 30-JUL-20 2.8 7 9.6 Dibenzo(ah)anthracene <0.050 0.050 ug/g 30-JUL-20 0.1 0.1 0.1 Fluoranthene <0.050 0.050 ug/g 30-JUL-20 0.56 0.69 9.6 Fluorene <0.050 0.050 ug/g 30-JUL-20 0.12 62 62 Indeno(1,2,3-cd)pyrene <0.050 0.050 ug/g 30-JUL-20 0.23 0.38 0.76 1+2-Methylnaphthalenes 0.061 0.042 ug/g 30-JUL-20 0.59 0.99 76 1-Methylnaphthalene 0.061 0.030 ug/g 30-JUL-20 0.59 0.99 76 2-Methylnaphthalene <0.030 0.030 ug/g 30-JUL-20 0.59 0.99 76 Naphthalene 0.021 R 0.013 ug/g 30-JUL-20 0.09 0.6 9.6 Phenanthrene <0.046 0.046 ug/g 30-JUL-20 0.69 6.2 12 Pyrene <0.050 0.050 ug/g 30-JUL-20 1 78 96 Surrogate: 2-Fluorobiphenyl 95.1 50-140 % 30-JUL-20 Surrogate: p-Terphenyl d14 108.1 50-140 % 30-JUL-20
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-RPIICC-COARSE #1: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use #2: T3-Soil-Res/Park/Inst. Property Use (Coarse)
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) 190441800 L2479593 CONTD.... Page 13 of 15 31-JUL-20 14:42 (MT) Reference Information
Sample Parameter Qualifier key listed: Qualifier Description
R The ion abundance ratio(s) did not meet the acceptance criteria. Value is an estimated maximum.
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
B-HWS-R511-WT Soil Boron-HWE-O.Reg 153/04 (July HW EXTR, EPA 6010B 2011)
A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). CR-CR6-IC-WT Soil Hexavalent Chromium in Soil SW846 3060A/7199
This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in a sulphuric acid solution.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
F1-F4-511-CALC-WT Soil F1-F4 Hydrocarbon Calculated CCME CWS-PHC, Pub #1310, Dec 2001-S Parameters
Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.
Hydrocarbon results are expressed on a dry weight basis.
In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines and the gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes has been subtracted from F1.
In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.
Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range: 1. All extraction and analysis holding times were met. 2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene. 3. Linearity of gasoline response within 15% throughout the calibration range.
Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges: 1. All extraction and analysis holding times were met. 2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average. 3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors. 4. Linearity of diesel or motor oil response within 15% throughout the calibration range. F1-HS-511-WT Soil F1-O.Reg 153/04 (July 2011) E3398/CCME TIER 1-HS
Fraction F1 is determined by extracting a soil or sediment sample as received with methanol, then analyzing by headspace-GC/FID.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). 190441800 L2479593 CONTD.... Page 14 of 15 31-JUL-20 14:42 (MT) Reference Information
F2-F4-511-WT Soil F2-F4-O.Reg 153/04 (July 2011) CCME Tier 1
Petroleum Hydrocarbons (F2-F4 fractions) are extracted from soil with 1:1 hexane:acetone using a rotary extractor. Extracts are treated with silica gel to remove polar organic interferences. F2, F3, & F4 are analyzed by GC-FID. F4G-sg is analyzed gravimetrically.
Notes: 1. F2 (C10-C16): Sum of all hydrocarbons that elute between nC10 and nC16. 2. F3 (C16-C34): Sum of all hydrocarbons that elute between nC16 and nC34. 3. F4 (C34-C50): Sum of all hydrocarbons that elute between nC34 and nC50. 4. F4G: Gravimetric Heavy Hydrocarbons 5. F4G-sg: Gravimetric Heavy Hydrocarbons (F4G) after silica gel treatment. 6. Where both F4 (C34-C50) and F4G-sg are reported for a sample, the larger of the two values is used for comparison against the relevant CCME guideline for F4. 7. F4G-sg cannot be added to the C6 to C50 hydrocarbon results to obtain an estimate of total extractable hydrocarbons. 8. This method is validated for use. 9. Data from analysis of validation and quality control samples is available upon request. 10. Reported results are expressed as milligrams per dry kilogram, unless otherwise indicated.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). HG-200.2-CVAA-WT Soil Mercury in Soil by CVAAS EPA 200.2/1631E (mod)
Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
MET-200.2-CCMS-WT Soil Metals in Soil by CRC ICPMS EPA 200.2/6020B (mod)
Soil/sediment is dried, disaggregated, and sieved (2 mm). For tests intended to support Ontario regulations, the <2mm fraction is ground to pass through a 0.355 mm sieve. Strong Acid Leachable Metals in the <2mm fraction are solubilized by heated digestion with nitric and hydrochloric acids. Instrumental analysis is by Collision / Reaction Cell ICPMS.
Limitations: This method is intended to liberate environmentally available metals. Silicate minerals are not solubilized. Some metals may be only partially recovered (matrix dependent), including Al, Ba, Be, Cr, S, Sr, Ti, Tl, V, W, and Zr. Elemental Sulfur may be poorly recovered by this method. Volatile forms of sulfur (e.g. sulfide, H2S) may be excluded if lost during sampling, storage, or digestion.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). METHYLNAPS-CALC-WT Soil ABN-Calculated Parameters SW846 8270 MOISTURE-WT Soil % Moisture CCME PHC in Soil - Tier 1 (mod) PAH-511-WT Soil PAH-O.Reg 153/04 (July 2011) SW846 3510/8270
A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Results for benzo(b) fluoranthene may include contributions from benzo(j)fluoranthene, if also present in the sample.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). VOC-1,3-DCP-CALC-WT Soil Regulation 153 VOCs SW8260B/SW8270C VOC-511-HS-WT Soil VOC-O.Reg 153/04 (July 2011) SW846 8260 (511)
Soil and sediment samples are extracted in methanol and analyzed by headspace-GC/MS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). XYLENES-SUM-CALC- Soil Sum of Xylene Isomer CALCULATION WT Concentrations
Total xylenes represents the sum of o-xylene and m&p-xylene.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below: 190441800 L2479593 CONTD.... Page 15 of 15 31-JUL-20 14:42 (MT) Reference Information
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 1 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
B-HWS-R511-WT Soil Batch R5172186 WG3373240-4 DUP L2479605-5 Boron (B), Hot Water Ext. 0.46 0.46 ug/g 0.0 30 30-JUL-20 WG3373240-2 IRM WT SAR4 Boron (B), Hot Water Ext. 108.1 % 70-130 30-JUL-20 WG3373240-3 LCS Boron (B), Hot Water Ext. 101.0 % 70-130 30-JUL-20 WG3373240-1 MB Boron (B), Hot Water Ext. <0.10 ug/g 0.1 30-JUL-20
Batch R5172271 WG3373245-4 DUP L2479593-1 Boron (B), Hot Water Ext. 0.34 0.37 ug/g 7.0 30 30-JUL-20 WG3373245-2 IRM WT SAR4 Boron (B), Hot Water Ext. 99.0 % 70-130 30-JUL-20 WG3373245-3 LCS Boron (B), Hot Water Ext. 101.0 % 70-130 30-JUL-20 WG3373245-1 MB Boron (B), Hot Water Ext. <0.10 ug/g 0.1 30-JUL-20
CR-CR6-IC-WT Soil Batch R5172275 WG3372342-4 CRM WT-SQC012 Chromium, Hexavalent 103.1 % 70-130 30-JUL-20 WG3372342-3 DUP L2479593-1 Chromium, Hexavalent <0.20 <0.20 RPD-NA ug/g N/A 35 30-JUL-20 WG3372342-2 LCS Chromium, Hexavalent 102.4 % 80-120 30-JUL-20 WG3372342-1 MB Chromium, Hexavalent <0.20 ug/g 0.2 30-JUL-20
F1-HS-511-WT Soil Batch R5170098 WG3370779-4 DUP WG3370779-3 F1 (C6-C10) <5.0 <5.0 RPD-NA ug/g N/A 30 29-JUL-20 WG3370779-2 LCS F1 (C6-C10) 116.3 % 80-120 29-JUL-20 WG3370779-1 MB F1 (C6-C10) <5.0 ug/g 5 29-JUL-20 Surrogate: 3,4-Dichlorotoluene 117.1 % 60-140 29-JUL-20 WG3370779-6 MS L2479605-6 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 2 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
F1-HS-511-WT Soil Batch R5170098 WG3370779-6 MS L2479605-6 F1 (C6-C10) 127.4 % 60-140 29-JUL-20
Batch R5171898 WG3372442-2 LCS F1 (C6-C10) 100.1 % 80-120 30-JUL-20 WG3372442-1 MB F1 (C6-C10) <5.0 ug/g 5 30-JUL-20 Surrogate: 3,4-Dichlorotoluene 110.4 % 60-140 30-JUL-20
F2-F4-511-WT Soil Batch R5171718 WG3371774-8 DUP WG3371774-10 F2 (C10-C16) <10 <10 RPD-NA ug/g N/A 30 29-JUL-20 F3 (C16-C34) <50 <50 RPD-NA ug/g N/A 30 29-JUL-20 F4 (C34-C50) <50 <50 RPD-NA ug/g N/A 30 29-JUL-20 WG3371774-7 LCS F2 (C10-C16) 100.2 % 80-120 29-JUL-20 F3 (C16-C34) 98.4 % 80-120 29-JUL-20 F4 (C34-C50) 94.7 % 80-120 29-JUL-20 WG3371774-6 MB F2 (C10-C16) <10 ug/g 10 29-JUL-20 F3 (C16-C34) <50 ug/g 50 29-JUL-20 F4 (C34-C50) <50 ug/g 50 29-JUL-20 Surrogate: 2-Bromobenzotrifluoride 87.3 % 60-140 29-JUL-20 WG3371774-9 MS WG3371774-10 F2 (C10-C16) 94.2 % 60-140 29-JUL-20 F3 (C16-C34) 95.9 % 60-140 29-JUL-20 F4 (C34-C50) 99.6 % 60-140 29-JUL-20
HG-200.2-CVAA-WT Soil Batch R5172118 WG3373238-2 CRM WT-SS-1 Mercury (Hg) 96.2 % 70-130 30-JUL-20 WG3373238-6 DUP WG3373238-5 Mercury (Hg) <0.0050 <0.0050 RPD-NA ug/g N/A 40 30-JUL-20 WG3373238-3 LCS Mercury (Hg) 100.0 % 80-120 30-JUL-20 WG3373238-1 MB Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 3 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
HG-200.2-CVAA-WT Soil Batch R5172118 WG3373238-1 MB Mercury (Hg) <0.0050 mg/kg 0.005 30-JUL-20
Batch R5172141 WG3373234-2 CRM WT-SS-1 Mercury (Hg) 109.2 % 70-130 30-JUL-20 WG3373234-6 DUP WG3373234-5 Mercury (Hg) 0.0052 <0.0050 RPD-NA ug/g N/A 40 30-JUL-20 WG3373234-3 LCS Mercury (Hg) 92.0 % 80-120 30-JUL-20 WG3373234-1 MB Mercury (Hg) <0.0050 mg/kg 0.005 30-JUL-20
MET-200.2-CCMS-WT Soil Batch R5172682 WG3373234-2 CRM WT-SS-1 Antimony (Sb) 106.7 % 70-130 30-JUL-20 Arsenic (As) 111.2 % 70-130 30-JUL-20 Beryllium (Be) 102.3 % 70-130 30-JUL-20 Boron (B) 97.6 % 70-130 30-JUL-20 Cadmium (Cd) 92.9 % 70-130 30-JUL-20 Chromium (Cr) 100.5 % 70-130 30-JUL-20 Cobalt (Co) 96.5 % 70-130 30-JUL-20 Copper (Cu) 98.6 % 70-130 30-JUL-20 Lead (Pb) 95.5 % 70-130 30-JUL-20 Molybdenum (Mo) 93.2 % 70-130 30-JUL-20 Nickel (Ni) 100.6 % 70-130 30-JUL-20 Selenium (Se) 88.7 % 70-130 30-JUL-20 Silver (Ag) 90.2 % 70-130 30-JUL-20 Thallium (Tl) 80.6 % 70-130 30-JUL-20 Vanadium (V) 109.7 % 70-130 30-JUL-20 Zinc (Zn) 103.8 % 70-130 30-JUL-20 WG3373234-6 DUP WG3373234-5 Antimony (Sb) <0.10 <0.10 RPD-NA ug/g N/A 30 30-JUL-20 Arsenic (As) 1.36 1.36 ug/g 0.5 30 30-JUL-20 Barium (Ba) 46.0 45.2 ug/g 1.8 40 30-JUL-20 Beryllium (Be) 0.33 0.33 ug/g 1.4 30 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 4 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R5172682 WG3373234-6 DUP WG3373234-5 Boron (B) 6.0 5.6 ug/g 7.0 30 30-JUL-20 Cadmium (Cd) 0.044 0.042 ug/g 4.0 30 30-JUL-20 Chromium (Cr) 16.8 16.0 ug/g 4.7 30 30-JUL-20 Cobalt (Co) 5.85 5.70 ug/g 2.6 30 30-JUL-20 Copper (Cu) 13.5 13.3 ug/g 1.5 30 30-JUL-20 Lead (Pb) 2.85 2.68 ug/g 6.2 40 30-JUL-20 Molybdenum (Mo) 0.16 0.14 ug/g 16 40 30-JUL-20 Nickel (Ni) 10.4 10.2 ug/g 1.6 30 30-JUL-20 Selenium (Se) <0.20 <0.20 RPD-NA ug/g N/A 30 30-JUL-20 Silver (Ag) <0.10 <0.10 RPD-NA ug/g N/A 40 30-JUL-20 Thallium (Tl) 0.064 0.061 ug/g 4.9 30 30-JUL-20 Uranium (U) 0.307 0.310 ug/g 0.9 30 30-JUL-20 Vanadium (V) 38.2 36.6 ug/g 4.1 30 30-JUL-20 Zinc (Zn) 24.8 23.7 ug/g 4.6 30 30-JUL-20 WG3373234-4 LCS Antimony (Sb) 98.4 % 80-120 30-JUL-20 Arsenic (As) 101.9 % 80-120 30-JUL-20 Barium (Ba) 96.1 % 80-120 30-JUL-20 Beryllium (Be) 96.0 % 80-120 30-JUL-20 Boron (B) 95.6 % 80-120 30-JUL-20 Cadmium (Cd) 94.5 % 80-120 30-JUL-20 Chromium (Cr) 101.9 % 80-120 30-JUL-20 Cobalt (Co) 97.4 % 80-120 30-JUL-20 Copper (Cu) 97.6 % 80-120 30-JUL-20 Lead (Pb) 93.7 % 80-120 30-JUL-20 Molybdenum (Mo) 92.0 % 80-120 30-JUL-20 Nickel (Ni) 97.8 % 80-120 30-JUL-20 Selenium (Se) 101.1 % 80-120 30-JUL-20 Silver (Ag) 90.8 % 80-120 30-JUL-20 Thallium (Tl) 95.2 % 80-120 30-JUL-20 Uranium (U) 82.3 % 80-120 30-JUL-20 Vanadium (V) 102.6 % 80-120 30-JUL-20 Zinc (Zn) 95.7 % 80-120 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 5 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R5172682 WG3373234-1 MB Antimony (Sb) <0.10 mg/kg 0.1 30-JUL-20 Arsenic (As) <0.10 mg/kg 0.1 30-JUL-20 Barium (Ba) <0.50 mg/kg 0.5 30-JUL-20 Beryllium (Be) <0.10 mg/kg 0.1 30-JUL-20 Boron (B) <5.0 mg/kg 5 30-JUL-20 Cadmium (Cd) <0.020 mg/kg 0.02 30-JUL-20 Chromium (Cr) <0.50 mg/kg 0.5 30-JUL-20 Cobalt (Co) <0.10 mg/kg 0.1 30-JUL-20 Copper (Cu) <0.50 mg/kg 0.5 30-JUL-20 Lead (Pb) <0.50 mg/kg 0.5 30-JUL-20 Molybdenum (Mo) <0.10 mg/kg 0.1 30-JUL-20 Nickel (Ni) <0.50 mg/kg 0.5 30-JUL-20 Selenium (Se) <0.20 mg/kg 0.2 30-JUL-20 Silver (Ag) <0.10 mg/kg 0.1 30-JUL-20 Thallium (Tl) <0.050 mg/kg 0.05 30-JUL-20 Uranium (U) <0.050 mg/kg 0.05 30-JUL-20 Vanadium (V) <0.20 mg/kg 0.2 30-JUL-20 Zinc (Zn) <2.0 mg/kg 2 30-JUL-20
Batch R5172716 WG3373238-2 CRM WT-SS-1 Antimony (Sb) 120.1 % 70-130 30-JUL-20 Arsenic (As) 112.3 % 70-130 30-JUL-20 Beryllium (Be) 112.9 % 70-130 30-JUL-20 Boron (B) 104.3 % 70-130 30-JUL-20 Cadmium (Cd) 110.0 % 70-130 30-JUL-20 Chromium (Cr) 103.1 % 70-130 30-JUL-20 Cobalt (Co) 99.4 % 70-130 30-JUL-20 Copper (Cu) 100.1 % 70-130 30-JUL-20 Lead (Pb) 102.1 % 70-130 30-JUL-20 Molybdenum (Mo) 106.3 % 70-130 30-JUL-20 Nickel (Ni) 101.5 % 70-130 30-JUL-20 Selenium (Se) 87.1 % 70-130 30-JUL-20 Silver (Ag) 103.5 % 70-130 30-JUL-20 Thallium (Tl) 83.4 % 70-130 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 6 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R5172716 WG3373238-2 CRM WT-SS-1 Vanadium (V) 109.4 % 70-130 30-JUL-20 Zinc (Zn) 108.6 % 70-130 30-JUL-20 WG3373238-6 DUP WG3373238-5 Antimony (Sb) <0.10 <0.10 RPD-NA ug/g N/A 30 30-JUL-20 Arsenic (As) 1.36 1.37 ug/g 0.2 30 30-JUL-20 Barium (Ba) 13.9 13.4 ug/g 3.3 40 30-JUL-20 Beryllium (Be) 0.18 0.17 ug/g 3.6 30 30-JUL-20 Boron (B) <5.0 <5.0 RPD-NA ug/g N/A 30 30-JUL-20 Cadmium (Cd) <0.020 <0.020 RPD-NA ug/g N/A 30 30-JUL-20 Chromium (Cr) 7.02 7.18 ug/g 2.3 30 30-JUL-20 Cobalt (Co) 1.47 1.48 ug/g 0.5 30 30-JUL-20 Copper (Cu) 2.28 2.21 ug/g 3.1 30 30-JUL-20 Lead (Pb) 2.60 2.40 ug/g 8.1 40 30-JUL-20 Molybdenum (Mo) 0.53 0.55 ug/g 4.3 40 30-JUL-20 Nickel (Ni) 3.10 3.06 ug/g 1.1 30 30-JUL-20 Selenium (Se) <0.20 <0.20 RPD-NA ug/g N/A 30 30-JUL-20 Silver (Ag) <0.10 <0.10 RPD-NA ug/g N/A 40 30-JUL-20 Thallium (Tl) <0.050 <0.050 RPD-NA ug/g N/A 30 30-JUL-20 Uranium (U) 0.475 0.458 ug/g 3.6 30 30-JUL-20 Vanadium (V) 13.6 14.8 ug/g 8.9 30 30-JUL-20 Zinc (Zn) 9.8 9.4 ug/g 4.1 30 30-JUL-20 WG3373238-4 LCS Antimony (Sb) 111.1 % 80-120 30-JUL-20 Arsenic (As) 96.9 % 80-120 30-JUL-20 Barium (Ba) 97.5 % 80-120 30-JUL-20 Beryllium (Be) 100.2 % 80-120 30-JUL-20 Boron (B) 98.1 % 80-120 30-JUL-20 Cadmium (Cd) 99.8 % 80-120 30-JUL-20 Chromium (Cr) 95.3 % 80-120 30-JUL-20 Cobalt (Co) 95.4 % 80-120 30-JUL-20 Copper (Cu) 94.3 % 80-120 30-JUL-20 Lead (Pb) 99.9 % 80-120 30-JUL-20 Molybdenum (Mo) 102.9 % 80-120 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 7 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R5172716 WG3373238-4 LCS Nickel (Ni) 94.4 % 80-120 30-JUL-20 Selenium (Se) 95.4 % 80-120 30-JUL-20 Silver (Ag) 97.1 % 80-120 30-JUL-20 Thallium (Tl) 98.8 % 80-120 30-JUL-20 Uranium (U) 96.0 % 80-120 30-JUL-20 Vanadium (V) 96.7 % 80-120 30-JUL-20 Zinc (Zn) 93.6 % 80-120 30-JUL-20 WG3373238-1 MB Antimony (Sb) <0.10 mg/kg 0.1 30-JUL-20 Arsenic (As) <0.10 mg/kg 0.1 30-JUL-20 Barium (Ba) <0.50 mg/kg 0.5 30-JUL-20 Beryllium (Be) <0.10 mg/kg 0.1 30-JUL-20 Boron (B) <5.0 mg/kg 5 30-JUL-20 Cadmium (Cd) <0.020 mg/kg 0.02 30-JUL-20 Chromium (Cr) <0.50 mg/kg 0.5 30-JUL-20 Cobalt (Co) <0.10 mg/kg 0.1 30-JUL-20 Copper (Cu) <0.50 mg/kg 0.5 30-JUL-20 Lead (Pb) <0.50 mg/kg 0.5 30-JUL-20 Molybdenum (Mo) <0.10 mg/kg 0.1 30-JUL-20 Nickel (Ni) <0.50 mg/kg 0.5 30-JUL-20 Selenium (Se) <0.20 mg/kg 0.2 30-JUL-20 Silver (Ag) <0.10 mg/kg 0.1 30-JUL-20 Thallium (Tl) <0.050 mg/kg 0.05 30-JUL-20 Uranium (U) <0.050 mg/kg 0.05 30-JUL-20 Vanadium (V) <0.20 mg/kg 0.2 30-JUL-20 Zinc (Zn) <2.0 mg/kg 2 30-JUL-20
MOISTURE-WT Soil Batch R5170101 WG3372299-3 DUP L2479589-8 % Moisture 5.78 7.03 % 19 20 29-JUL-20 WG3372299-2 LCS % Moisture 100.2 % 90-110 29-JUL-20 WG3372299-1 MB % Moisture <0.25 % 0.25 29-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 8 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MOISTURE-WT Soil Batch R5171714 WG3372642-3 DUP L2479616-1 % Moisture 14.1 14.8 % 4.5 20 30-JUL-20 WG3372642-2 LCS % Moisture 100.4 % 90-110 30-JUL-20 WG3372642-1 MB % Moisture <0.25 % 0.25 30-JUL-20
PAH-511-WT Soil Batch R5172507 WG3371768-3 DUP WG3371768-5 1-Methylnaphthalene <0.030 <0.030 RPD-NA ug/g N/A 40 30-JUL-20 2-Methylnaphthalene <0.030 <0.030 RPD-NA ug/g N/A 40 30-JUL-20 Acenaphthene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Acenaphthylene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Benzo(a)anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Benzo(a)pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Benzo(b)fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Benzo(g,h,i)perylene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Benzo(k)fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Chrysene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Dibenzo(ah)anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Fluorene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Indeno(1,2,3-cd)pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 Naphthalene <0.013 <0.013 RPD-NA ug/g N/A 40 30-JUL-20 Phenanthrene <0.046 <0.046 RPD-NA ug/g N/A 40 30-JUL-20 Pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 30-JUL-20 WG3371768-2 LCS 1-Methylnaphthalene 91.9 % 50-140 30-JUL-20 2-Methylnaphthalene 88.4 % 50-140 30-JUL-20 Acenaphthene 94.3 % 50-140 30-JUL-20 Acenaphthylene 90.0 % 50-140 30-JUL-20 Anthracene 87.3 % 50-140 30-JUL-20 Benzo(a)anthracene 92.3 % 50-140 30-JUL-20 Benzo(a)pyrene 88.0 % 50-140 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 9 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R5172507 WG3371768-2 LCS Benzo(b)fluoranthene 87.6 % 50-140 30-JUL-20 Benzo(g,h,i)perylene 87.0 % 50-140 30-JUL-20 Benzo(k)fluoranthene 87.7 % 50-140 30-JUL-20 Chrysene 98.0 % 50-140 30-JUL-20 Dibenzo(ah)anthracene 90.1 % 50-140 30-JUL-20 Fluoranthene 88.4 % 50-140 30-JUL-20 Fluorene 89.0 % 50-140 30-JUL-20 Indeno(1,2,3-cd)pyrene 88.2 % 50-140 30-JUL-20 Naphthalene 89.0 % 50-140 30-JUL-20 Phenanthrene 89.4 % 50-140 30-JUL-20 Pyrene 89.1 % 50-140 30-JUL-20 WG3371768-1 MB 1-Methylnaphthalene <0.030 ug/g 0.03 30-JUL-20 2-Methylnaphthalene <0.030 ug/g 0.03 30-JUL-20 Acenaphthene <0.050 ug/g 0.05 30-JUL-20 Acenaphthylene <0.050 ug/g 0.05 30-JUL-20 Anthracene <0.050 ug/g 0.05 30-JUL-20 Benzo(a)anthracene <0.050 ug/g 0.05 30-JUL-20 Benzo(a)pyrene <0.050 ug/g 0.05 30-JUL-20 Benzo(b)fluoranthene <0.050 ug/g 0.05 30-JUL-20 Benzo(g,h,i)perylene <0.050 ug/g 0.05 30-JUL-20 Benzo(k)fluoranthene <0.050 ug/g 0.05 30-JUL-20 Chrysene <0.050 ug/g 0.05 30-JUL-20 Dibenzo(ah)anthracene <0.050 ug/g 0.05 30-JUL-20 Fluoranthene <0.050 ug/g 0.05 30-JUL-20 Fluorene <0.050 ug/g 0.05 30-JUL-20 Indeno(1,2,3-cd)pyrene <0.050 ug/g 0.05 30-JUL-20 Naphthalene <0.013 ug/g 0.013 30-JUL-20 Phenanthrene <0.046 ug/g 0.046 30-JUL-20 Pyrene <0.050 ug/g 0.05 30-JUL-20 Surrogate: 2-Fluorobiphenyl 96.7 % 50-140 30-JUL-20 Surrogate: p-Terphenyl d14 110.1 % 50-140 30-JUL-20 WG3371768-4 MS WG3371768-5 1-Methylnaphthalene 92.3 % 50-140 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 10 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R5172507 WG3371768-4 MS WG3371768-5 2-Methylnaphthalene 88.4 % 50-140 30-JUL-20 Acenaphthene 95.5 % 50-140 30-JUL-20 Acenaphthylene 89.3 % 50-140 30-JUL-20 Anthracene 88.9 % 50-140 30-JUL-20 Benzo(a)anthracene 93.0 % 50-140 30-JUL-20 Benzo(a)pyrene 89.6 % 50-140 30-JUL-20 Benzo(b)fluoranthene 82.4 % 50-140 30-JUL-20 Benzo(g,h,i)perylene 89.5 % 50-140 30-JUL-20 Benzo(k)fluoranthene 99.2 % 50-140 30-JUL-20 Chrysene 100.8 % 50-140 30-JUL-20 Dibenzo(ah)anthracene 91.6 % 50-140 30-JUL-20 Fluoranthene 89.9 % 50-140 30-JUL-20 Fluorene 90.3 % 50-140 30-JUL-20 Indeno(1,2,3-cd)pyrene 85.1 % 50-140 30-JUL-20 Naphthalene 89.3 % 50-140 30-JUL-20 Phenanthrene 91.4 % 50-140 30-JUL-20 Pyrene 90.7 % 50-140 30-JUL-20
VOC-511-HS-WT Soil Batch R5170098 WG3370779-4 DUP WG3370779-3 1,1,1,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,1,2,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,1,1-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,1,2-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,1-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,1-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,2-Dibromoethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,2-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,2-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,2-Dichloropropane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,3-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 1,4-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Acetone <0.50 <0.50 RPD-NA ug/g N/A 40 29-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 11 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170098 WG3370779-4 DUP WG3370779-3 Benzene <0.0068 <0.0068 RPD-NA ug/g N/A 40 29-JUL-20 Bromodichloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Bromoform <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Bromomethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Carbon tetrachloride <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Chlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Chloroform <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 cis-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 cis-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 29-JUL-20 Dibromochloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Dichlorodifluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Ethylbenzene <0.018 <0.018 RPD-NA ug/g N/A 40 29-JUL-20 n-Hexane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Methylene Chloride <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 MTBE <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 m+p-Xylenes <0.030 <0.030 RPD-NA ug/g N/A 40 29-JUL-20 Methyl Ethyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 29-JUL-20 Methyl Isobutyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 29-JUL-20 o-Xylene <0.020 <0.020 RPD-NA ug/g N/A 40 29-JUL-20 Styrene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Tetrachloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Toluene <0.080 <0.080 RPD-NA ug/g N/A 40 29-JUL-20 trans-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 trans-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 29-JUL-20 Trichloroethylene <0.010 <0.010 RPD-NA ug/g N/A 40 29-JUL-20 Trichlorofluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 29-JUL-20 Vinyl chloride <0.020 <0.020 RPD-NA ug/g N/A 40 29-JUL-20 WG3370779-2 LCS 1,1,1,2-Tetrachloroethane 97.2 % 60-130 29-JUL-20 1,1,2,2-Tetrachloroethane 108.7 % 60-130 29-JUL-20 1,1,1-Trichloroethane 66.1 % 60-130 29-JUL-20 1,1,2-Trichloroethane 98.2 % 60-130 29-JUL-20 1,1-Dichloroethane 67.7 % 60-130 29-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 12 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170098 WG3370779-2 LCS 1,1-Dichloroethylene 25.1 LCS-L % 60-130 29-JUL-20 1,2-Dibromoethane 97.3 % 70-130 29-JUL-20 1,2-Dichlorobenzene 102.8 % 70-130 29-JUL-20 1,2-Dichloroethane 85.4 % 60-130 29-JUL-20 1,2-Dichloropropane 92.3 % 70-130 29-JUL-20 1,3-Dichlorobenzene 99.7 % 70-130 29-JUL-20 1,4-Dichlorobenzene 100.7 % 70-130 29-JUL-20 Acetone 97.7 % 60-140 29-JUL-20 Benzene 77.6 % 70-130 29-JUL-20 Bromodichloromethane 101.7 % 50-140 29-JUL-20 Bromoform 106.7 % 70-130 29-JUL-20 Bromomethane 14.9 LCS-L % 50-140 29-JUL-20 Carbon tetrachloride 61.6 MES % 70-130 29-JUL-20 Chlorobenzene 96.5 % 70-130 29-JUL-20 Chloroform 87.2 % 70-130 29-JUL-20 cis-1,2-Dichloroethylene 71.8 % 70-130 29-JUL-20 cis-1,3-Dichloropropene 93.3 % 70-130 29-JUL-20 Dibromochloromethane 96.7 % 60-130 29-JUL-20 Dichlorodifluoromethane 0.0 LCS-L % 50-140 29-JUL-20 Ethylbenzene 88.1 % 70-130 29-JUL-20 n-Hexane 10.1 LCS-L % 70-130 29-JUL-20 Methylene Chloride 63.6 MES % 70-130 29-JUL-20 MTBE 78.7 % 70-130 29-JUL-20 m+p-Xylenes 90.2 % 70-130 29-JUL-20 Methyl Ethyl Ketone 117.8 % 60-140 29-JUL-20 Methyl Isobutyl Ketone 103.8 % 60-140 29-JUL-20 o-Xylene 97.7 % 70-130 29-JUL-20 Styrene 92.1 % 70-130 29-JUL-20 Tetrachloroethylene 79.0 % 60-130 29-JUL-20 Toluene 82.4 % 70-130 29-JUL-20 trans-1,2-Dichloroethylene 48.8 LCS-L % 60-130 29-JUL-20 trans-1,3-Dichloropropene 103.4 % 70-130 29-JUL-20 Trichloroethylene 79.6 % 60-130 29-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 13 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170098 WG3370779-2 LCS Trichlorofluoromethane 8.9 LCS-L % 50-140 29-JUL-20 Vinyl chloride 3.0 LCS-L % 60-140 29-JUL-20 WG3370779-1 MB 1,1,1,2-Tetrachloroethane <0.050 ug/g 0.05 29-JUL-20 1,1,2,2-Tetrachloroethane <0.050 ug/g 0.05 29-JUL-20 1,1,1-Trichloroethane <0.050 ug/g 0.05 29-JUL-20 1,1,2-Trichloroethane <0.050 ug/g 0.05 29-JUL-20 1,1-Dichloroethane <0.050 ug/g 0.05 29-JUL-20 1,1-Dichloroethylene <0.050 ug/g 0.05 29-JUL-20 1,2-Dibromoethane <0.050 ug/g 0.05 29-JUL-20 1,2-Dichlorobenzene <0.050 ug/g 0.05 29-JUL-20 1,2-Dichloroethane <0.050 ug/g 0.05 29-JUL-20 1,2-Dichloropropane <0.050 ug/g 0.05 29-JUL-20 1,3-Dichlorobenzene <0.050 ug/g 0.05 29-JUL-20 1,4-Dichlorobenzene <0.050 ug/g 0.05 29-JUL-20 Acetone <0.50 ug/g 0.5 29-JUL-20 Benzene <0.0068 ug/g 0.0068 29-JUL-20 Bromodichloromethane <0.050 ug/g 0.05 29-JUL-20 Bromoform <0.050 ug/g 0.05 29-JUL-20 Bromomethane <0.050 ug/g 0.05 29-JUL-20 Carbon tetrachloride <0.050 ug/g 0.05 29-JUL-20 Chlorobenzene <0.050 ug/g 0.05 29-JUL-20 Chloroform <0.050 ug/g 0.05 29-JUL-20 cis-1,2-Dichloroethylene <0.050 ug/g 0.05 29-JUL-20 cis-1,3-Dichloropropene <0.030 ug/g 0.03 29-JUL-20 Dibromochloromethane <0.050 ug/g 0.05 29-JUL-20 Dichlorodifluoromethane <0.050 ug/g 0.05 29-JUL-20 Ethylbenzene <0.018 ug/g 0.018 29-JUL-20 n-Hexane <0.050 ug/g 0.05 29-JUL-20 Methylene Chloride <0.050 ug/g 0.05 29-JUL-20 MTBE <0.050 ug/g 0.05 29-JUL-20 m+p-Xylenes <0.030 ug/g 0.03 29-JUL-20 Methyl Ethyl Ketone <0.50 ug/g 0.5 29-JUL-20 Methyl Isobutyl Ketone <0.50 ug/g 0.5 29-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 14 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170098 WG3370779-1 MB o-Xylene <0.020 ug/g 0.02 29-JUL-20 Styrene <0.050 ug/g 0.05 29-JUL-20 Tetrachloroethylene <0.050 ug/g 0.05 29-JUL-20 Toluene <0.080 ug/g 0.08 29-JUL-20 trans-1,2-Dichloroethylene <0.050 ug/g 0.05 29-JUL-20 trans-1,3-Dichloropropene <0.030 ug/g 0.03 29-JUL-20 Trichloroethylene <0.010 ug/g 0.01 29-JUL-20 Trichlorofluoromethane <0.050 ug/g 0.05 29-JUL-20 Vinyl chloride <0.020 ug/g 0.02 29-JUL-20 Surrogate: 1,4-Difluorobenzene 116.4 % 50-140 29-JUL-20 Surrogate: 4-Bromofluorobenzene 98.2 % 50-140 29-JUL-20 WG3370779-5 MS WG3370779-3 1,1,1,2-Tetrachloroethane 101.3 % 50-140 29-JUL-20 1,1,2,2-Tetrachloroethane 96.6 % 50-140 29-JUL-20 1,1,1-Trichloroethane 100.1 % 50-140 29-JUL-20 1,1,2-Trichloroethane 101.6 % 50-140 29-JUL-20 1,1-Dichloroethane 105.7 % 50-140 29-JUL-20 1,1-Dichloroethylene 97.0 % 50-140 29-JUL-20 1,2-Dibromoethane 103.1 % 50-140 29-JUL-20 1,2-Dichlorobenzene 101.8 % 50-140 29-JUL-20 1,2-Dichloroethane 101.0 % 50-140 29-JUL-20 1,2-Dichloropropane 108.0 % 50-140 29-JUL-20 1,3-Dichlorobenzene 97.3 % 50-140 29-JUL-20 1,4-Dichlorobenzene 97.5 % 50-140 29-JUL-20 Acetone 116.6 % 50-140 29-JUL-20 Benzene 108.2 % 50-140 29-JUL-20 Bromodichloromethane 110.2 % 50-140 29-JUL-20 Bromoform 107.5 % 50-140 29-JUL-20 Bromomethane 121.8 % 50-140 29-JUL-20 Carbon tetrachloride 98.7 % 50-140 29-JUL-20 Chlorobenzene 101.6 % 50-140 29-JUL-20 Chloroform 108.3 % 50-140 29-JUL-20 cis-1,2-Dichloroethylene 96.5 % 50-140 29-JUL-20 cis-1,3-Dichloropropene 92.9 % 50-140 29-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 15 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170098 WG3370779-5 MS WG3370779-3 Dibromochloromethane 99.7 % 50-140 29-JUL-20 Dichlorodifluoromethane 78.0 % 50-140 29-JUL-20 Ethylbenzene 96.7 % 50-140 29-JUL-20 n-Hexane 103.0 % 50-140 29-JUL-20 Methylene Chloride 105.7 % 50-140 29-JUL-20 MTBE 101.9 % 50-140 29-JUL-20 m+p-Xylenes 97.4 % 50-140 29-JUL-20 Methyl Ethyl Ketone 113.8 % 50-140 29-JUL-20 Methyl Isobutyl Ketone 102.6 % 50-140 29-JUL-20 o-Xylene 105.0 % 50-140 29-JUL-20 Styrene 95.4 % 50-140 29-JUL-20 Tetrachloroethylene 96.2 % 50-140 29-JUL-20 Toluene 98.2 % 50-140 29-JUL-20 trans-1,2-Dichloroethylene 96.9 % 50-140 29-JUL-20 trans-1,3-Dichloropropene 98.0 % 50-140 29-JUL-20 Trichloroethylene 112.6 % 50-140 29-JUL-20 Trichlorofluoromethane 93.8 % 50-140 29-JUL-20 Vinyl chloride 109.3 % 50-140 29-JUL-20
Batch R5171898 WG3372442-2 LCS 1,1,1,2-Tetrachloroethane 102.4 % 60-130 30-JUL-20 1,1,2,2-Tetrachloroethane 104.7 % 60-130 30-JUL-20 1,1,1-Trichloroethane 103.9 % 60-130 30-JUL-20 1,1,2-Trichloroethane 102.5 % 60-130 30-JUL-20 1,1-Dichloroethane 109.6 % 60-130 30-JUL-20 1,1-Dichloroethylene 99.4 % 60-130 30-JUL-20 1,2-Dibromoethane 102.0 % 70-130 30-JUL-20 1,2-Dichlorobenzene 107.7 % 70-130 30-JUL-20 1,2-Dichloroethane 102.8 % 60-130 30-JUL-20 1,2-Dichloropropane 111.1 % 70-130 30-JUL-20 1,3-Dichlorobenzene 107.5 % 70-130 30-JUL-20 1,4-Dichlorobenzene 107.5 % 70-130 30-JUL-20 Acetone 114.1 % 60-140 30-JUL-20 Benzene 112.8 % 70-130 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 16 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5171898 WG3372442-2 LCS Bromodichloromethane 113.7 % 50-140 30-JUL-20 Bromoform 106.2 % 70-130 30-JUL-20 Bromomethane 128.6 % 50-140 30-JUL-20 Carbon tetrachloride 102.3 % 70-130 30-JUL-20 Chlorobenzene 105.7 % 70-130 30-JUL-20 Chloroform 112.0 % 70-130 30-JUL-20 cis-1,2-Dichloroethylene 99.6 % 70-130 30-JUL-20 cis-1,3-Dichloropropene 103.8 % 70-130 30-JUL-20 Dibromochloromethane 100.1 % 60-130 30-JUL-20 Dichlorodifluoromethane 72.4 % 50-140 30-JUL-20 Ethylbenzene 99.2 % 70-130 30-JUL-20 n-Hexane 104.3 % 70-130 30-JUL-20 Methylene Chloride 108.2 % 70-130 30-JUL-20 MTBE 105.7 % 70-130 30-JUL-20 m+p-Xylenes 102.2 % 70-130 30-JUL-20 Methyl Ethyl Ketone 121.5 % 60-140 30-JUL-20 Methyl Isobutyl Ketone 101.3 % 60-140 30-JUL-20 o-Xylene 107.2 % 70-130 30-JUL-20 Styrene 97.8 % 70-130 30-JUL-20 Tetrachloroethylene 102.9 % 60-130 30-JUL-20 Toluene 100.6 % 70-130 30-JUL-20 trans-1,2-Dichloroethylene 103.1 % 60-130 30-JUL-20 trans-1,3-Dichloropropene 107.9 % 70-130 30-JUL-20 Trichloroethylene 107.6 % 60-130 30-JUL-20 Trichlorofluoromethane 95.0 % 50-140 30-JUL-20 Vinyl chloride 109.5 % 60-140 30-JUL-20 WG3372442-1 MB 1,1,1,2-Tetrachloroethane <0.050 ug/g 0.05 30-JUL-20 1,1,2,2-Tetrachloroethane <0.050 ug/g 0.05 30-JUL-20 1,1,1-Trichloroethane <0.050 ug/g 0.05 30-JUL-20 1,1,2-Trichloroethane <0.050 ug/g 0.05 30-JUL-20 1,1-Dichloroethane <0.050 ug/g 0.05 30-JUL-20 1,1-Dichloroethylene <0.050 ug/g 0.05 30-JUL-20 1,2-Dibromoethane <0.050 ug/g 0.05 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 17 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5171898 WG3372442-1 MB 1,2-Dichlorobenzene <0.050 ug/g 0.05 30-JUL-20 1,2-Dichloroethane <0.050 ug/g 0.05 30-JUL-20 1,2-Dichloropropane <0.050 ug/g 0.05 30-JUL-20 1,3-Dichlorobenzene <0.050 ug/g 0.05 30-JUL-20 1,4-Dichlorobenzene <0.050 ug/g 0.05 30-JUL-20 Acetone <0.50 ug/g 0.5 30-JUL-20 Benzene <0.0068 ug/g 0.0068 30-JUL-20 Bromodichloromethane <0.050 ug/g 0.05 30-JUL-20 Bromoform <0.050 ug/g 0.05 30-JUL-20 Bromomethane <0.050 ug/g 0.05 30-JUL-20 Carbon tetrachloride <0.050 ug/g 0.05 30-JUL-20 Chlorobenzene <0.050 ug/g 0.05 30-JUL-20 Chloroform <0.050 ug/g 0.05 30-JUL-20 cis-1,2-Dichloroethylene <0.050 ug/g 0.05 30-JUL-20 cis-1,3-Dichloropropene <0.030 ug/g 0.03 30-JUL-20 Dibromochloromethane <0.050 ug/g 0.05 30-JUL-20 Dichlorodifluoromethane <0.050 ug/g 0.05 30-JUL-20 Ethylbenzene <0.018 ug/g 0.018 30-JUL-20 n-Hexane <0.050 ug/g 0.05 30-JUL-20 Methylene Chloride <0.050 ug/g 0.05 30-JUL-20 MTBE <0.050 ug/g 0.05 30-JUL-20 m+p-Xylenes <0.030 ug/g 0.03 30-JUL-20 Methyl Ethyl Ketone <0.50 ug/g 0.5 30-JUL-20 Methyl Isobutyl Ketone <0.50 ug/g 0.5 30-JUL-20 o-Xylene <0.020 ug/g 0.02 30-JUL-20 Styrene <0.050 ug/g 0.05 30-JUL-20 Tetrachloroethylene <0.050 ug/g 0.05 30-JUL-20 Toluene <0.080 ug/g 0.08 30-JUL-20 trans-1,2-Dichloroethylene <0.050 ug/g 0.05 30-JUL-20 trans-1,3-Dichloropropene <0.030 ug/g 0.03 30-JUL-20 Trichloroethylene <0.010 ug/g 0.01 30-JUL-20 Trichlorofluoromethane <0.050 ug/g 0.05 30-JUL-20 Vinyl chloride <0.020 ug/g 0.02 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 18 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5171898 WG3372442-1 MB Surrogate: 1,4-Difluorobenzene 112.9 % 50-140 30-JUL-20 Surrogate: 4-Bromofluorobenzene 94.3 % 50-140 30-JUL-20 WG3372442-5 MS WG3372442-3 1,1,1,2-Tetrachloroethane 103.2 % 50-140 30-JUL-20 1,1,2,2-Tetrachloroethane 104.4 % 50-140 30-JUL-20 1,1,1-Trichloroethane 105.0 % 50-140 30-JUL-20 1,1,2-Trichloroethane 102.7 % 50-140 30-JUL-20 1,1-Dichloroethane 110.6 % 50-140 30-JUL-20 1,1-Dichloroethylene 101.1 % 50-140 30-JUL-20 1,2-Dibromoethane 102.8 % 50-140 30-JUL-20 1,2-Dichlorobenzene 104.9 % 50-140 30-JUL-20 1,2-Dichloroethane 102.0 % 50-140 30-JUL-20 1,2-Dichloropropane 110.9 % 50-140 30-JUL-20 1,3-Dichlorobenzene 104.4 % 50-140 30-JUL-20 1,4-Dichlorobenzene 104.2 % 50-140 30-JUL-20 Acetone 103.3 % 50-140 30-JUL-20 Benzene 112.8 % 50-140 30-JUL-20 Bromodichloromethane 113.1 % 50-140 30-JUL-20 Bromoform 105.2 % 50-140 30-JUL-20 Bromomethane 129.7 % 50-140 30-JUL-20 Carbon tetrachloride 103.5 % 50-140 30-JUL-20 Chlorobenzene 106.1 % 50-140 30-JUL-20 Chloroform 112.9 % 50-140 30-JUL-20 cis-1,2-Dichloroethylene 100.5 % 50-140 30-JUL-20 cis-1,3-Dichloropropene 103.0 % 50-140 30-JUL-20 Dibromochloromethane 99.2 % 50-140 30-JUL-20 Dichlorodifluoromethane 79.3 % 50-140 30-JUL-20 Ethylbenzene 102.8 % 50-140 30-JUL-20 n-Hexane 105.6 % 50-140 30-JUL-20 Methylene Chloride 108.8 % 50-140 30-JUL-20 MTBE 106.3 % 50-140 30-JUL-20 m+p-Xylenes 103.3 % 50-140 30-JUL-20 Methyl Ethyl Ketone 109.2 % 50-140 30-JUL-20 Methyl Isobutyl Ketone 101.4 % 50-140 30-JUL-20 Quality Control Report
Workorder: L2479593 Report Date: 31-JUL-20 Page 19 of 20
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5171898 WG3372442-5 MS WG3372442-3 o-Xylene 109.1 % 50-140 30-JUL-20 Styrene 98.6 % 50-140 30-JUL-20 Tetrachloroethylene 103.3 % 50-140 30-JUL-20 Toluene 99.9 % 50-140 30-JUL-20 trans-1,2-Dichloroethylene 103.0 % 50-140 30-JUL-20 trans-1,3-Dichloropropene 108.4 % 50-140 30-JUL-20 Trichloroethylene 108.4 % 50-140 30-JUL-20 Trichlorofluoromethane 97.8 % 50-140 30-JUL-20 Vinyl chloride 112.5 % 50-140 30-JUL-20 Quality Control Report Workorder: L2479593 Report Date: 31-JUL-20
Client: Morrison Hershfield Limited (Ottawa) Page 20 of 20 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description LCS-L Lab Control Sample recovery was below ALS DQO. Reference Material and/or Matrix Spike results were acceptable. Non-detected sample results are considered reliable. Other results, if reported, have been qualified. MES Data Quality Objective was marginally exceeded (by < 10% absolute) for < 10% of analytes in a Multi-Element Scan / Multi-Parameter Scan (considered acceptable as per OMOE & CCME). RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order. ALS Sample ID: L2479593-2 Client Sample ID: BH 11 SA3 500
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Morrison Hershfield Limited (Ottawa) Date Received: 24-JUL-20 ATTN: Mitchell Dawley Report Date: 31-JUL-20 14:33 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2479604 Project P.O. #: NOT SUBMITTED Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2479604 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 3 190441800 31-JUL-20 14:33 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2479604-1 TCLP-3 Sampled By: CLIENT on 23-JUL-20 #1 #2 Matrix: SOIL
Sample Preparation Initial pH 7.53 0.10 pH units 28-JUL-20 Final pH 5.13 0.10 pH units 28-JUL-20 TCLP Extractables Benzo(a)pyrene <0.0010 0.0010 mg/L 29-JUL-20 0.001 Surrogate: d12-Chrysene 84.6 60-140 % 29-JUL-20 TCLP Metals Arsenic (As) <0.050 0.050 mg/L 28-JUL-20 2.5 Barium (Ba) 1.09 0.50 mg/L 28-JUL-20 100 Boron (B) <2.5 2.5 mg/L 28-JUL-20 500 Cadmium (Cd) <0.0050 0.0050 mg/L 28-JUL-20 0.5 Chromium (Cr) <0.050 0.050 mg/L 28-JUL-20 5.0 Lead (Pb) <0.025 0.025 mg/L 28-JUL-20 5.0 Mercury (Hg) <0.00010 0.00010 mg/L 28-JUL-20 0.1 Selenium (Se) <0.025 0.025 mg/L 28-JUL-20 1.0 Silver (Ag) <0.0050 0.0050 mg/L 28-JUL-20 5.0 Uranium (U) <0.25 0.25 mg/L 28-JUL-20 10 TCLP VOCs 1,1-Dichloroethylene <0.025 0.025 mg/L 29-JUL-20 1.4 1,2-Dichlorobenzene <0.025 0.025 mg/L 29-JUL-20 20.0 1,2-Dichloroethane <0.025 0.025 mg/L 29-JUL-20 0.5 1,4-Dichlorobenzene <0.025 0.025 mg/L 29-JUL-20 0.5 Benzene <0.025 0.025 mg/L 29-JUL-20 0.5 Carbon tetrachloride <0.025 0.025 mg/L 29-JUL-20 0.5 Chlorobenzene <0.025 0.025 mg/L 29-JUL-20 8 Chloroform <0.10 0.10 mg/L 29-JUL-20 10 Dichloromethane <0.50 0.50 mg/L 29-JUL-20 5.0 Methyl Ethyl Ketone <1.0 1.0 mg/L 29-JUL-20 200.0 Tetrachloroethylene <0.025 0.025 mg/L 29-JUL-20 3 Trichloroethylene <0.025 0.025 mg/L 29-JUL-20 5 Vinyl chloride <0.050 0.050 mg/L 29-JUL-20 0.2 Surrogate: 4-Bromofluorobenzene 102.2 70-130 % 29-JUL-20 Volatile Organic Compounds Surrogate: 1,4-Difluorobenzene 103.5 70-130 % 29-JUL-20
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Federal & Provincial Waste Regulations (MAR, 2008) = [Suite] - ON-REG347/90 - Schedule 4 Leachate + Bulk PCB #1: Ontario Ministry of the Environment, General Waste Control Regulation No. 347/90
#2: Polychlorinated Biphenyls (PCBs) - Ontario Regulation 347/90 190441800 L2479604 CONTD.... Page 3 of 3 31-JUL-20 14:33 (MT) Reference Information
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
BAP-ONT-TCLP-WT Waste Benzo(a)pyrene for O. Reg 347 SW 846 8270-GC-MS on TCLP Leachate HG-TCLP-WT Waste Mercury (CVAA) for O.Reg 347 EPA 1631E
This analysis is carried out in accordance with the extraction procedure outlined in "Test Methods for Evaluating Solid Waste - Physical/Chemical Methods Volume 1C" SW-846 EPA Method 1311, published by the United States Environmental Protection Agency (EPA). In summary, the sample is extracted at a 20:1 liquid to solids ratio for 16 to 20 hours using either extraction fluid #1 (glacial acetic acid, water and sodium hydroxide) or extraction fluid #2 (glacial acetic acid), depending on the pH of the original sample. The extract is then filtered through a 0.6 to 0.8 micron glass fibre filter and analysed using atomic absorption spectrophotometry (EPA 1631E). LEACH-TCLP-WT Waste Leachate Procedure for Reg 347 EPA 1311
Inorganic and Semi-Volatile Organic contaminants are leached from waste samples in strict accordance with US EPA Method 1311, "Toxicity Characteristic Leaching Procedure" (TCLP). Test results are reported in leachate concentration units (normally mg/L). MET-TCLP-WT Waste O.Reg 347 TCLP Leachable EPA 6020B Metals
This analysis is carried out in accordance with the extraction procedure outlined in "Test Methods for Evaluating Solid Waste - Physical/Chemical Methods Volume 1C" SW-846 EPA Method 1311, published by the United States Environmental Protection Agency (EPA). In summary, the sample is extracted at a 20:1 liquid to solids ratio for 16 to 20 hours using either extraction fluid #1 (glacial acetic acid, water and sodium hydroxide) or extraction fluid #2 (glacial acetic acid), depending on the pH of the original sample. The extract is then filtered through a 0.6 to 0.8 micron glass fibre filter. Instrumental analysis of the digested extract is by collision cell inductively coupled plasma - mass spectrometry (modifed from EPA Method 6020B). VOC-TCLP-WT Waste VOC for O. Reg 347 SW846 8260
A sample of waste is leached in a zero headspace extractor at 30–2 rpm for 18–2.0 hours with the appropriate leaching solution. After tumbling the leachate is analyzed directly by headspace technology, followed by GC/MS using internal standard quantitation.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2479604 Report Date: 31-JUL-20 Page 1 of 5
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
BAP-ONT-TCLP-WT Waste Batch R5171318 WG3372055-5 DUP WG3372055-4 Benzo(a)pyrene <0.0010 <0.0010 RPD-NA mg/L N/A 50 29-JUL-20 WG3372055-2 LCS Benzo(a)pyrene 111.9 % 50-150 29-JUL-20 WG3372055-1 MB Benzo(a)pyrene <0.0010 mg/L 0.001 29-JUL-20 Surrogate: d12-Chrysene 103.5 % 60-140 29-JUL-20 WG3372055-3 MB Benzo(a)pyrene <0.0010 mg/L 0.001 29-JUL-20 Surrogate: d12-Chrysene 100.2 % 60-140 29-JUL-20 WG3372055-6 MS WG3372055-4 Benzo(a)pyrene 105.0 % 50-150 29-JUL-20
HG-TCLP-WT Waste Batch R5168502 WG3371697-3 DUP L2479390-1 Mercury (Hg) <0.00010 <0.00010 RPD-NA mg/L N/A 50 28-JUL-20 WG3371697-2 LCS Mercury (Hg) 111.0 % 70-130 28-JUL-20 WG3371697-1 MB Mercury (Hg) <0.00010 mg/L 0.0001 28-JUL-20 WG3371697-4 MS L2479390-1 Mercury (Hg) 103.0 % 50-140 28-JUL-20
MET-TCLP-WT Waste Batch R5170136 WG3371702-4 DUP WG3371702-3 Silver (Ag) <0.0050 <0.0050 RPD-NA mg/L N/A 50 28-JUL-20 Arsenic (As) <0.050 <0.050 RPD-NA mg/L N/A 50 28-JUL-20 Boron (B) 2.6 2.9 mg/L 9.0 50 28-JUL-20 Barium (Ba) <0.50 <0.50 RPD-NA mg/L N/A 50 28-JUL-20 Cadmium (Cd) 0.0087 0.0088 mg/L 0.3 50 28-JUL-20 Chromium (Cr) <0.050 <0.050 RPD-NA mg/L N/A 50 28-JUL-20 Lead (Pb) <0.025 <0.025 RPD-NA mg/L N/A 50 28-JUL-20 Selenium (Se) <0.025 <0.025 RPD-NA mg/L N/A 50 28-JUL-20 Uranium (U) <0.25 <0.25 RPD-NA mg/L N/A 50 28-JUL-20 WG3371702-2 LCS Silver (Ag) 92.1 % 70-130 28-JUL-20 Quality Control Report
Workorder: L2479604 Report Date: 31-JUL-20 Page 2 of 5
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-TCLP-WT Waste Batch R5170136 WG3371702-2 LCS Arsenic (As) 93.9 % 70-130 28-JUL-20 Boron (B) 85.2 % 70-130 28-JUL-20 Barium (Ba) 93.8 % 70-130 28-JUL-20 Cadmium (Cd) 92.0 % 70-130 28-JUL-20 Chromium (Cr) 89.7 % 70-130 28-JUL-20 Lead (Pb) 91.0 % 70-130 28-JUL-20 Selenium (Se) 92.2 % 70-130 28-JUL-20 Uranium (U) 91.8 % 70-130 28-JUL-20 WG3371702-1 MB Silver (Ag) <0.0050 mg/L 0.005 28-JUL-20 Arsenic (As) <0.050 mg/L 0.05 28-JUL-20 Boron (B) <2.5 mg/L 2.5 28-JUL-20 Barium (Ba) <0.50 mg/L 0.5 28-JUL-20 Cadmium (Cd) <0.0050 mg/L 0.005 28-JUL-20 Chromium (Cr) <0.050 mg/L 0.05 28-JUL-20 Lead (Pb) <0.025 mg/L 0.025 28-JUL-20 Selenium (Se) <0.025 mg/L 0.025 28-JUL-20 Uranium (U) <0.25 mg/L 0.25 28-JUL-20 WG3371702-5 MS WG3371702-3 Silver (Ag) 111.6 % 50-140 28-JUL-20 Arsenic (As) 96.3 % 50-140 28-JUL-20 Boron (B) 87.9 % 50-140 28-JUL-20 Barium (Ba) 96.7 % 50-140 28-JUL-20 Cadmium (Cd) 93.8 % 50-140 28-JUL-20 Chromium (Cr) 90.4 % 50-140 28-JUL-20 Lead (Pb) 95.6 % 50-140 28-JUL-20 Selenium (Se) 95.2 % 50-140 28-JUL-20 Uranium (U) 96.5 % 50-140 28-JUL-20
VOC-TCLP-WT Waste Batch R5168658 WG3365815-1 LCS 1,1-Dichloroethylene 92.7 % 70-130 28-JUL-20 1,2-Dichlorobenzene 99.8 % 70-130 28-JUL-20 1,2-Dichloroethane 104.2 % 70-130 28-JUL-20 Quality Control Report
Workorder: L2479604 Report Date: 31-JUL-20 Page 3 of 5
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-TCLP-WT Waste Batch R5168658 WG3365815-1 LCS 1,4-Dichlorobenzene 99.5 % 70-130 28-JUL-20 Benzene 100.2 % 70-130 28-JUL-20 Carbon tetrachloride 105.5 % 60-140 28-JUL-20 Chlorobenzene 101.5 % 70-130 28-JUL-20 Chloroform 105.9 % 70-130 28-JUL-20 Dichloromethane 97.6 % 70-130 28-JUL-20 Methyl Ethyl Ketone 97.4 % 50-150 28-JUL-20 Tetrachloroethylene 104.0 % 70-130 28-JUL-20 Trichloroethylene 104.6 % 70-130 28-JUL-20 Vinyl chloride 93.3 % 60-130 28-JUL-20 WG3365815-2 MB 1,1-Dichloroethylene <0.025 mg/L 0.025 28-JUL-20 1,2-Dichlorobenzene <0.025 mg/L 0.025 28-JUL-20 1,2-Dichloroethane <0.025 mg/L 0.025 28-JUL-20 1,4-Dichlorobenzene <0.025 mg/L 0.025 28-JUL-20 Benzene <0.025 mg/L 0.025 28-JUL-20 Carbon tetrachloride <0.025 mg/L 0.025 28-JUL-20 Chlorobenzene <0.025 mg/L 0.025 28-JUL-20 Chloroform <0.10 mg/L 0.1 28-JUL-20 Dichloromethane <0.50 mg/L 0.5 28-JUL-20 Methyl Ethyl Ketone <1.0 mg/L 1 28-JUL-20 Tetrachloroethylene <0.025 mg/L 0.025 28-JUL-20 Trichloroethylene <0.025 mg/L 0.025 28-JUL-20 Vinyl chloride <0.050 mg/L 0.05 28-JUL-20 Surrogate: 1,4-Difluorobenzene 101.3 % 70-130 28-JUL-20 Surrogate: 4-Bromofluorobenzene 101.7 % 70-130 28-JUL-20 WG3365815-4 MS WG3365815-3 1,1-Dichloroethylene 94.3 % 50-140 29-JUL-20 1,2-Dichlorobenzene 100.4 % 50-140 29-JUL-20 1,2-Dichloroethane 105.5 % 50-140 29-JUL-20 1,4-Dichlorobenzene 100.1 % 50-140 29-JUL-20 Benzene 99.6 % 50-140 29-JUL-20 Carbon tetrachloride 112.7 % 50-140 29-JUL-20 Chlorobenzene 101.9 % 50-140 29-JUL-20 Quality Control Report
Workorder: L2479604 Report Date: 31-JUL-20 Page 4 of 5
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-TCLP-WT Waste Batch R5168658 WG3365815-4 MS WG3365815-3 Chloroform 108.6 % 50-140 29-JUL-20 Dichloromethane 221.0 RRQC % 50-140 29-JUL-20 Methyl Ethyl Ketone 91.3 % 50-140 29-JUL-20 Tetrachloroethylene 107.3 % 50-140 29-JUL-20 Trichloroethylene 106.8 % 50-140 29-JUL-20 Vinyl chloride 90.7 % 50-140 29-JUL-20 COMMENTS: Matrix spike recovery was above ALS DQO non detect sample results were considered reliable. Other results if reported were qualified. Quality Control Report Workorder: L2479604 Report Date: 31-JUL-20
Client: Morrison Hershfield Limited (Ottawa) Page 5 of 5 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit. RRQC Refer to report remarks for information regarding this QC result.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.
Morrison Hershfield Limited (Ottawa) Date Received: 27-JUL-20 ATTN: Mitchell Dawley Report Date: 11-AUG-20 14:18 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2480127 Project P.O. #: 20102333-L3-681.50 Job Reference: 190441800 C of C Numbers: 14-448380 Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2480127 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 10 190441800 11-AUG-20 14:18 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2480127-1 BH10 SA1 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 17.2 0.25 % 30-JUL-20 Metals Antimony (Sb) 6.3 1.0 ug/g 31-JUL-20 *1 *1.3 40 Arsenic (As) 39.7 1.0 ug/g 31-JUL-20 *11 *18 *18 Barium (Ba) 145 1.0 ug/g 31-JUL-20 210 220 670 Beryllium (Be) 0.70 0.50 ug/g 31-JUL-20 2.5 2.5 8 Boron (B) 8.1 5.0 ug/g 31-JUL-20 36 36 120 Boron (B), Hot Water Ext. 0.35 0.10 ug/g 31-JUL-20 36 36 2 Cadmium (Cd) <0.50 0.50 ug/g 31-JUL-20 1 1.2 1.9 Chromium (Cr) 33.2 1.0 ug/g 31-JUL-20 67 70 160 Cobalt (Co) 9.3 1.0 ug/g 31-JUL-20 19 21 80 Copper (Cu) 99.2 1.0 ug/g 31-JUL-20 *62 *92 230 Lead (Pb) 160 1.0 ug/g 31-JUL-20 *45 *120 *120 Mercury (Hg) 0.267 0.0050 ug/g 31-JUL-20 *0.16 0.27 3.9 Molybdenum (Mo) 10.2 1.0 ug/g 31-JUL-20 *2 *2 40 Nickel (Ni) 23.3 1.0 ug/g 31-JUL-20 37 82 270 Selenium (Se) 1.4 1.0 ug/g 31-JUL-20 *1.2 1.5 5.5 Silver (Ag) <0.20 0.20 ug/g 31-JUL-20 0.5 0.5 40 Thallium (Tl) <0.50 0.50 ug/g 31-JUL-20 1 1 3.3 Uranium (U) <1.0 1.0 ug/g 31-JUL-20 1.9 2.5 33 Vanadium (V) 36.4 1.0 ug/g 31-JUL-20 86 86 86 Zinc (Zn) 150 5.0 ug/g 31-JUL-20 290 290 340 Speciated Metals Chromium, Hexavalent <0.20 0.20 ug/g 31-JUL-20 0.66 0.66 8 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.205 0.050 ug/g 31-JUL-20 *0.05 *0.072 96 Acenaphthylene 0.137 0.050 ug/g 31-JUL-20 *0.093 *0.093 0.15 Anthracene 0.319 0.050 ug/g 31-JUL-20 *0.05 *0.16 0.67 Benzo(a)anthracene 0.659 0.050 ug/g 31-JUL-20 *0.095 *0.36 0.96 Benzo(a)pyrene 0.399 0.050 ug/g 31-JUL-20 *0.05 *0.3 *0.3 Benzo(b)fluoranthene 0.501 0.050 ug/g 31-JUL-20 *0.3 *0.47 0.96 Benzo(g,h,i)perylene 0.176 0.050 ug/g 31-JUL-20 0.2 0.68 9.6 Benzo(k)fluoranthene 0.122 0.050 ug/g 31-JUL-20 *0.05 0.48 0.96 Chrysene 0.851 0.050 ug/g 31-JUL-20 *0.18 2.8 9.6 Dibenzo(ah)anthracene 0.074 0.050 ug/g 31-JUL-20 0.1 0.1 0.1 Fluoranthene 0.991 0.050 ug/g 31-JUL-20 *0.24 *0.56 9.6 Fluorene 0.216 R 0.050 ug/g 31-JUL-20 *0.05 *0.12 62 Indeno(1,2,3-cd)pyrene 0.130 0.050 ug/g 31-JUL-20 *0.11 0.23 0.76 1+2-Methylnaphthalenes 7.82 0.042 ug/g 04-AUG-20 *0.05 *0.59 76 1-Methylnaphthalene 3.87 0.030 ug/g 31-JUL-20 *0.05 *0.59 76 2-Methylnaphthalene 3.95 0.030 ug/g 31-JUL-20 *0.05 *0.59 76 Naphthalene 2.07 0.013 ug/g 31-JUL-20 *0.05 *0.09 9.6 Phenanthrene 2.74 0.046 ug/g 31-JUL-20 *0.19 *0.69 12 Pyrene 0.962 0.050 ug/g 31-JUL-20 *0.19 1 96 Surrogate: 2-Fluorobiphenyl 91.4 50-140 % 31-JUL-20
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-AG+RPIICC/ICC-C #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) L2480127 CONTD.... ANALYTICAL GUIDELINE REPORT Page 3 of 10 190441800 11-AUG-20 14:18 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2480127-1 BH10 SA1 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Surrogate: p-Terphenyl d14 102.7 50-140 % 31-JUL-20
L2480127-2 BH10 SA3 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 17.0 0.25 % 30-JUL-20 Volatile Organic Compounds Acetone <8.0 DLI 8.0 ug/g 04-AUG-20 **0.5 **0.5 16 Benzene 0.79 DLI 0.11 ug/g 04-AUG-20 *0.02 *0.02 *0.32 Bromodichloromethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 18 Bromoform <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.61 Bromomethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.05 Carbon tetrachloride <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.21 Chlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 2.4 Dibromochloromethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 13 Chloroform <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.47 1,2-Dibromoethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 6.8 1,3-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 9.6 1,4-Dichlorobenzene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.2 Dichlorodifluoromethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 16 1,1-Dichloroethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 17 1,2-Dichloroethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.05 1,1-Dichloroethylene <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.064 cis-1,2-Dichloroethylene <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 55 trans-1,2-Dichloroethylene <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 1.3 Methylene Chloride <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 1.6 1,2-Dichloropropane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.16 cis-1,3-Dichloropropene <0.48 DLI 0.48 ug/g 04-AUG-20 trans-1,3-Dichloropropene <0.030 0.030 ug/g 29-JUL-20 1,3-Dichloropropene (cis & trans) <0.48 0.48 ug/g 04-AUG-20 **0.05 **0.05 **0.18 Ethylbenzene 38.0 DLI 0.29 ug/g 04-AUG-20 *0.05 *0.05 *9.5 n-Hexane 37.3 DLI 0.80 ug/g 04-AUG-20 *0.05 *0.05 46 Methyl Ethyl Ketone <8.0 DLI 8.0 ug/g 04-AUG-20 **0.5 **0.5 70 Methyl Isobutyl Ketone <8.0 DLI 8.0 ug/g 04-AUG-20 **0.5 **0.5 31 MTBE <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 11 Styrene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 34 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 0.087 1,1,2,2-Tetrachloroethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.05 Tetrachloroethylene <0.050 0.050 ug/g 29-JUL-20 0.05 0.05 4.5 Toluene 0.504 0.080 ug/g 29-JUL-20 *0.2 *0.2 68 1,1,1-Trichloroethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 6.1 1,1,2-Trichloroethane <0.80 DLI 0.80 ug/g 04-AUG-20 **0.05 **0.05 **0.05 Trichloroethylene <0.16 DLI 0.16 ug/g 04-AUG-20 **0.05 **0.05 0.91 Trichlorofluoromethane <0.80 DLI 0.80 ug/g 04-AUG-20 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-AG+RPIICC/ICC-C #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2480127-2 BH10 SA3 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds **0.05 **0.25 4 Vinyl chloride <0.32 DLI 0.32 ug/g 04-AUG-20 **0.02 **0.02 **0.032 o-Xylene 1.64 0.020 ug/g 29-JUL-20 m+p-Xylenes 8.86 0.030 ug/g 29-JUL-20 Xylenes (Total) 10.5 0.050 ug/g 04-AUG-20 *0.05 *0.05 26 Surrogate: 4-Bromofluorobenzene 84.2 50-140 % 29-JUL-20 Surrogate: 1,4-Difluorobenzene 111.4 50-140 % 04-AUG-20 Hydrocarbons F1 (C6-C10) 1850 DLHC 80 ug/g 04-AUG-20 *17 *25 *55 F1-BTEX 1800 80 ug/g 04-AUG-20 *17 *25 *55 F2 (C10-C16) 1780 10 ug/g 31-JUL-20 *10 *10 *230 F2-Naphth 1780 10 ug/g 04-AUG-20 F3 (C16-C34) 1530 50 ug/g 31-JUL-20 *240 *240 1700 F3-PAH 1520 50 ug/g 04-AUG-20 F4 (C34-C50) 173 50 ug/g 31-JUL-20 *120 *120 3300 Total Hydrocarbons (C6-C50) 5330 110 ug/g 04-AUG-20 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 120.7 60-140 % 31-JUL-20 Surrogate: 3,4-Dichlorotoluene 186.9 SOL:MI 60-140 % 04-AUG-20 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.514 0.050 ug/g 31-JUL-20 *0.05 *0.072 96 Acenaphthylene <0.050 0.050 ug/g 31-JUL-20 0.093 0.093 0.15 Anthracene 0.094 AI 0.050 ug/g 31-JUL-20 *0.05 0.16 0.67 Benzo(a)anthracene <0.050 0.050 ug/g 31-JUL-20 0.095 0.36 0.96 Benzo(a)pyrene <0.050 0.050 ug/g 31-JUL-20 0.05 0.3 0.3 Benzo(b)fluoranthene <0.050 0.050 ug/g 31-JUL-20 0.3 0.47 0.96 Benzo(g,h,i)perylene <0.050 0.050 ug/g 31-JUL-20 0.2 0.68 9.6 Benzo(k)fluoranthene <0.050 0.050 ug/g 31-JUL-20 0.05 0.48 0.96 Chrysene <0.050 0.050 ug/g 31-JUL-20 0.18 2.8 9.6 Dibenzo(ah)anthracene <0.050 0.050 ug/g 31-JUL-20 0.1 0.1 0.1 Fluoranthene <0.050 0.050 ug/g 31-JUL-20 0.24 0.56 9.6 Fluorene 0.758 0.050 ug/g 31-JUL-20 *0.05 *0.12 62 Indeno(1,2,3-cd)pyrene <0.050 0.050 ug/g 31-JUL-20 0.11 0.23 0.76 1+2-Methylnaphthalenes 20.0 0.042 ug/g 04-AUG-20 *0.05 *0.59 76 1-Methylnaphthalene 7.55 0.030 ug/g 31-JUL-20 *0.05 *0.59 76 2-Methylnaphthalene 12.5 0.030 ug/g 31-JUL-20 *0.05 *0.59 76 Naphthalene 4.40 0.013 ug/g 31-JUL-20 *0.05 *0.09 9.6 Phenanthrene 1.16 0.046 ug/g 31-JUL-20 *0.19 *0.69 12 Pyrene 0.057 0.050 ug/g 31-JUL-20 0.19 1 96 Surrogate: 2-Fluorobiphenyl 103.8 50-140 % 31-JUL-20 Surrogate: p-Terphenyl d14 103.2 50-140 % 31-JUL-20
L2480127-3 BH10 SA5 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-AG+RPIICC/ICC-C #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
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L2480127-3 BH10 SA5 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 8.83 0.25 % 30-JUL-20 Hydrocarbons F2 (C10-C16) <10 10 ug/g 31-JUL-20 10 10 230 F3 (C16-C34) <50 50 ug/g 31-JUL-20 240 240 1700 F4 (C34-C50) <50 50 ug/g 31-JUL-20 120 120 3300 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 94.1 60-140 % 31-JUL-20
L2480127-4 BH9 SA4 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 10.9 0.25 % 30-JUL-20 Hydrocarbons F2 (C10-C16) 477 10 ug/g 31-JUL-20 *10 *10 *230 F3 (C16-C34) 241 50 ug/g 31-JUL-20 *240 *240 1700 F4 (C34-C50) <50 50 ug/g 31-JUL-20 120 120 3300 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 94.7 60-140 % 31-JUL-20
L2480127-5 BH9 SA5 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 15.3 0.25 % 08-AUG-20 Volatile Organic Compounds Acetone <0.50 0.50 ug/g 10-AUG-20 0.5 0.5 16 Benzene 0.141 0.0068 ug/g 10-AUG-20 *0.02 *0.02 0.32 Bromodichloromethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 18 Bromoform <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.61 Bromomethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.05 Carbon tetrachloride <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.21 Chlorobenzene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 2.4 Dibromochloromethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 13 Chloroform <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.47 1,2-Dibromoethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.05 1,2-Dichlorobenzene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 6.8 1,3-Dichlorobenzene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 9.6 1,4-Dichlorobenzene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.2 Dichlorodifluoromethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 16 1,1-Dichloroethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 17 1,2-Dichloroethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.05 1,1-Dichloroethylene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.064 cis-1,2-Dichloroethylene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 55 trans-1,2-Dichloroethylene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 1.3
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-AG+RPIICC/ICC-C #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) L2480127 CONTD.... ANALYTICAL GUIDELINE REPORT Page 6 of 10 190441800 11-AUG-20 14:18 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2480127-5 BH9 SA5 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Volatile Organic Compounds Methylene Chloride <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 1.6 1,2-Dichloropropane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.16 cis-1,3-Dichloropropene <0.030 0.030 ug/g 10-AUG-20 trans-1,3-Dichloropropene <0.030 0.030 ug/g 10-AUG-20 1,3-Dichloropropene (cis & trans) <0.042 0.042 ug/g 10-AUG-20 0.05 0.05 0.18 Ethylbenzene 0.050 0.018 ug/g 10-AUG-20 0.05 0.05 9.5 n-Hexane 0.457 0.050 ug/g 10-AUG-20 *0.05 *0.05 46 Methyl Ethyl Ketone <0.50 0.50 ug/g 10-AUG-20 0.5 0.5 70 Methyl Isobutyl Ketone <0.50 0.50 ug/g 10-AUG-20 0.5 0.5 31 MTBE <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 11 Styrene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 34 1,1,1,2-Tetrachloroethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.087 1,1,2,2-Tetrachloroethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.05 Tetrachloroethylene <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 4.5 Toluene <0.080 0.080 ug/g 10-AUG-20 0.2 0.2 68 1,1,1-Trichloroethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 6.1 1,1,2-Trichloroethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.05 0.05 Trichloroethylene <0.010 0.010 ug/g 10-AUG-20 0.05 0.05 0.91 Trichlorofluoromethane <0.050 0.050 ug/g 10-AUG-20 0.05 0.25 4 Vinyl chloride <0.020 0.020 ug/g 10-AUG-20 0.02 0.02 0.032 o-Xylene <0.020 0.020 ug/g 10-AUG-20 m+p-Xylenes 0.067 0.030 ug/g 10-AUG-20 Xylenes (Total) 0.067 0.050 ug/g 10-AUG-20 *0.05 *0.05 26 Surrogate: 4-Bromofluorobenzene 76.8 50-140 % 10-AUG-20 Surrogate: 1,4-Difluorobenzene 90.7 50-140 % 10-AUG-20 Hydrocarbons F1 (C6-C10) 7.5 5.0 ug/g 10-AUG-20 17 25 55 Surrogate: 3,4-Dichlorotoluene 76.5 60-140 % 10-AUG-20
L2480127-6 BH9 SA6 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Physical Tests % Moisture 18.8 0.25 % 30-JUL-20 Hydrocarbons F2 (C10-C16) 569 10 ug/g 31-JUL-20 *10 *10 *230 F2-Naphth 568 10 ug/g 04-AUG-20 F3 (C16-C34) 287 50 ug/g 31-JUL-20 *240 *240 1700 F3-PAH 286 50 ug/g 04-AUG-20 F4 (C34-C50) <50 50 ug/g 31-JUL-20 120 120 3300 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 96.2 60-140 % 31-JUL-20 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.122 0.050 ug/g 04-AUG-20 *0.05 *0.072 96 Acenaphthylene <0.050 0.050 ug/g 04-AUG-20 0.093 0.093 0.15 Anthracene <0.050 0.050 ug/g 04-AUG-20 0.05 0.16 0.67 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-AG+RPIICC/ICC-C #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) L2480127 CONTD.... ANALYTICAL GUIDELINE REPORT Page 7 of 10 190441800 11-AUG-20 14:18 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2480127-6 BH9 SA6 Sampled By: CLIENT on 24-JUL-20 #1 #2 #3 Matrix: SOIL
Polycyclic Aromatic Hydrocarbons Benzo(a)anthracene 0.064 0.050 ug/g 04-AUG-20 0.095 0.36 0.96 Benzo(a)pyrene <0.050 0.050 ug/g 04-AUG-20 0.05 0.3 0.3 Benzo(b)fluoranthene 0.065 0.050 ug/g 04-AUG-20 0.3 0.47 0.96 Benzo(g,h,i)perylene <0.050 0.050 ug/g 04-AUG-20 0.2 0.68 9.6 Benzo(k)fluoranthene <0.050 0.050 ug/g 04-AUG-20 0.05 0.48 0.96 Chrysene 0.070 0.050 ug/g 04-AUG-20 0.18 2.8 9.6 Dibenzo(ah)anthracene <0.050 0.050 ug/g 04-AUG-20 0.1 0.1 0.1 Fluoranthene 0.109 0.050 ug/g 04-AUG-20 0.24 0.56 9.6 Fluorene 0.154 0.050 ug/g 04-AUG-20 *0.05 *0.12 62 Indeno(1,2,3-cd)pyrene <0.050 0.050 ug/g 04-AUG-20 0.11 0.23 0.76 1+2-Methylnaphthalenes 3.10 0.042 ug/g 04-AUG-20 *0.05 *0.59 76 1-Methylnaphthalene 1.51 0.030 ug/g 04-AUG-20 *0.05 *0.59 76 2-Methylnaphthalene 1.60 0.030 ug/g 04-AUG-20 *0.05 *0.59 76 Naphthalene 0.515 0.013 ug/g 04-AUG-20 *0.05 *0.09 9.6 Phenanthrene 0.311 0.046 ug/g 04-AUG-20 *0.19 0.69 12 Pyrene 0.100 0.050 ug/g 04-AUG-20 0.19 1 96 Surrogate: 2-Fluorobiphenyl 94.8 50-140 % 04-AUG-20 Surrogate: p-Terphenyl d14 96.5 50-140 % 04-AUG-20
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-SOIL-AG+RPIICC/ICC-C #1: T1-Soil-Agricultural or Other Property Use #2: T1-Soil-Res/Park/Inst/Ind/Com/Commu Property Use
#3: T3-Soil-Ind/Com/Commu. Property Use (Coarse) 190441800 L2480127 CONTD.... Page 8 of 10 11-AUG-20 14:18 (MT) Reference Information
Sample Parameter Qualifier key listed: Qualifier Description
R The ion abundance ratio(s) did not meet the acceptance criteria. Value is an estimated maximum. DLI Detection Limit Raised: Dilution required to address Internal Standard response problems caused by matrix interference. AI Analytical interferences may be present. Result may be biased high. SOL:MI Surrogate recovery outside acceptable limits due to matrix interference DLHC Detection Limit Raised: Dilution required due to high concentration of test analyte(s).
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
B-HWS-R511-WT Soil Boron-HWE-O.Reg 153/04 (July HW EXTR, EPA 6010B 2011)
A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). CR-CR6-IC-WT Soil Hexavalent Chromium in Soil SW846 3060A/7199
This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in a sulphuric acid solution.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
F1-F4-511-CALC-WT Soil F1-F4 Hydrocarbon Calculated CCME CWS-PHC, Pub #1310, Dec 2001-S Parameters
Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.
Hydrocarbon results are expressed on a dry weight basis.
In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines and the gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes has been subtracted from F1.
In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.
Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range: 1. All extraction and analysis holding times were met. 2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene. 3. Linearity of gasoline response within 15% throughout the calibration range.
Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges: 1. All extraction and analysis holding times were met. 2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average. 3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors. 4. Linearity of diesel or motor oil response within 15% throughout the calibration range. F1-HS-511-WT Soil F1-O.Reg 153/04 (July 2011) E3398/CCME TIER 1-HS
Fraction F1 is determined by extracting a soil or sediment sample as received with methanol, then analyzing by headspace-GC/FID.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). 190441800 L2480127 CONTD.... Page 9 of 10 11-AUG-20 14:18 (MT) Reference Information
F2-F4-511-WT Soil F2-F4-O.Reg 153/04 (July 2011) CCME Tier 1
Petroleum Hydrocarbons (F2-F4 fractions) are extracted from soil with 1:1 hexane:acetone using a rotary extractor. Extracts are treated with silica gel to remove polar organic interferences. F2, F3, & F4 are analyzed by GC-FID. F4G-sg is analyzed gravimetrically.
Notes: 1. F2 (C10-C16): Sum of all hydrocarbons that elute between nC10 and nC16. 2. F3 (C16-C34): Sum of all hydrocarbons that elute between nC16 and nC34. 3. F4 (C34-C50): Sum of all hydrocarbons that elute between nC34 and nC50. 4. F4G: Gravimetric Heavy Hydrocarbons 5. F4G-sg: Gravimetric Heavy Hydrocarbons (F4G) after silica gel treatment. 6. Where both F4 (C34-C50) and F4G-sg are reported for a sample, the larger of the two values is used for comparison against the relevant CCME guideline for F4. 7. F4G-sg cannot be added to the C6 to C50 hydrocarbon results to obtain an estimate of total extractable hydrocarbons. 8. This method is validated for use. 9. Data from analysis of validation and quality control samples is available upon request. 10. Reported results are expressed as milligrams per dry kilogram, unless otherwise indicated.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). HG-200.2-CVAA-WT Soil Mercury in Soil by CVAAS EPA 200.2/1631E (mod)
Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).
MET-200.2-CCMS-WT Soil Metals in Soil by CRC ICPMS EPA 200.2/6020B (mod)
Soil/sediment is dried, disaggregated, and sieved (2 mm). For tests intended to support Ontario regulations, the <2mm fraction is ground to pass through a 0.355 mm sieve. Strong Acid Leachable Metals in the <2mm fraction are solubilized by heated digestion with nitric and hydrochloric acids. Instrumental analysis is by Collision / Reaction Cell ICPMS.
Limitations: This method is intended to liberate environmentally available metals. Silicate minerals are not solubilized. Some metals may be only partially recovered (matrix dependent), including Al, Ba, Be, Cr, S, Sr, Ti, Tl, V, W, and Zr. Elemental Sulfur may be poorly recovered by this method. Volatile forms of sulfur (e.g. sulfide, H2S) may be excluded if lost during sampling, storage, or digestion.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). METHYLNAPS-CALC-WT Soil ABN-Calculated Parameters SW846 8270 MOISTURE-WT Soil % Moisture CCME PHC in Soil - Tier 1 (mod) PAH-511-WT Soil PAH-O.Reg 153/04 (July 2011) SW846 3510/8270
A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Results for benzo(b) fluoranthene may include contributions from benzo(j)fluoranthene, if also present in the sample.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). VOC-1,3-DCP-CALC-WT Soil Regulation 153 VOCs SW8260B/SW8270C VOC-511-HS-WT Soil VOC-O.Reg 153/04 (July 2011) SW846 8260 (511)
Soil and sediment samples are extracted in methanol and analyzed by headspace-GC/MS.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). XYLENES-SUM-CALC- Soil Sum of Xylene Isomer CALCULATION WT Concentrations
Total xylenes represents the sum of o-xylene and m&p-xylene.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers:
14-448380 190441800 L2480127 CONTD.... Page 10 of 10 11-AUG-20 14:18 (MT) Reference Information
The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 1 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
B-HWS-R511-WT Soil Batch R5172934 WG3374231-4 DUP L2481477-1 Boron (B), Hot Water Ext. <0.10 <0.10 RPD-NA ug/g N/A 30 31-JUL-20 WG3374231-2 IRM WT SAR4 Boron (B), Hot Water Ext. 102.7 % 70-130 31-JUL-20 WG3374231-3 LCS Boron (B), Hot Water Ext. 98.7 % 70-130 31-JUL-20 WG3374231-1 MB Boron (B), Hot Water Ext. <0.10 ug/g 0.1 31-JUL-20
CR-CR6-IC-WT Soil Batch R5173766 WG3373347-4 CRM WT-SQC012 Chromium, Hexavalent 97.5 % 70-130 31-JUL-20 WG3373347-3 DUP L2480040-1 Chromium, Hexavalent <0.20 <0.20 RPD-NA ug/g N/A 35 31-JUL-20 WG3373347-2 LCS Chromium, Hexavalent 96.3 % 80-120 31-JUL-20 WG3373347-1 MB Chromium, Hexavalent <0.20 ug/g 0.2 31-JUL-20
F1-HS-511-WT Soil Batch R5170178 WG3371564-17 DUP WG3371564-16 F1 (C6-C10) <5.0 <5.0 RPD-NA ug/g N/A 30 31-JUL-20 WG3371564-2 LCS F1 (C6-C10) 102.1 % 80-120 29-JUL-20 WG3371564-1 MB F1 (C6-C10) <5.0 ug/g 5 29-JUL-20 Surrogate: 3,4-Dichlorotoluene 83.3 % 60-140 29-JUL-20 WG3371564-18 MS WG3371564-16 F1 (C6-C10) 102.2 % 60-140 31-JUL-20 WG3371564-6 MS L2480107-1 F1 (C6-C10) 104.5 % 60-140 29-JUL-20
Batch R5177137 WG3378198-4 DUP WG3378198-3 F1 (C6-C10) <5.0 <5.0 RPD-NA ug/g N/A 30 10-AUG-20 WG3378198-2 LCS F1 (C6-C10) 96.8 % 80-120 10-AUG-20 WG3378198-1 MB 5 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 2 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
F1-HS-511-WT Soil Batch R5177137 WG3378198-1 MB F1 (C6-C10) <5.0 ug/g 5 10-AUG-20 Surrogate: 3,4-Dichlorotoluene 85.4 % 60-140 10-AUG-20 WG3378198-6 MS L2484682-1 F1 (C6-C10) 106.7 % 60-140 10-AUG-20
F2-F4-511-WT Soil Batch R5173182 WG3373350-3 DUP WG3373350-5 F2 (C10-C16) <10 <10 RPD-NA ug/g N/A 30 31-JUL-20 F3 (C16-C34) <50 <50 RPD-NA ug/g N/A 30 31-JUL-20 F4 (C34-C50) <50 <50 RPD-NA ug/g N/A 30 31-JUL-20 WG3373350-2 LCS F2 (C10-C16) 105.2 % 80-120 31-JUL-20 F3 (C16-C34) 105.1 % 80-120 31-JUL-20 F4 (C34-C50) 103.8 % 80-120 31-JUL-20 WG3373350-1 MB F2 (C10-C16) <10 ug/g 10 31-JUL-20 F3 (C16-C34) <50 ug/g 50 31-JUL-20 F4 (C34-C50) <50 ug/g 50 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 95.5 % 60-140 31-JUL-20 WG3373350-4 MS WG3373350-5 F2 (C10-C16) 108.2 % 60-140 31-JUL-20 F3 (C16-C34) 112.4 % 60-140 31-JUL-20 F4 (C34-C50) 118.0 % 60-140 31-JUL-20
HG-200.2-CVAA-WT Soil Batch R5172867 WG3374211-2 CRM WT-SS-1 Mercury (Hg) 98.8 % 70-130 31-JUL-20 WG3374211-6 DUP WG3374211-5 Mercury (Hg) 0.0160 0.0153 ug/g 4.6 40 31-JUL-20 WG3374211-3 LCS Mercury (Hg) 115.0 % 80-120 31-JUL-20 WG3374211-1 MB Mercury (Hg) <0.0050 mg/kg 0.005 31-JUL-20
MET-200.2-CCMS-WT Soil Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 3 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R5172894 WG3374211-2 CRM WT-SS-1 Antimony (Sb) 113.5 % 70-130 31-JUL-20 Arsenic (As) 114.2 % 70-130 31-JUL-20 Beryllium (Be) 96.8 % 70-130 31-JUL-20 Boron (B) 83.8 % 70-130 31-JUL-20 Cadmium (Cd) 98.7 % 70-130 31-JUL-20 Chromium (Cr) 96.5 % 70-130 31-JUL-20 Cobalt (Co) 100.7 % 70-130 31-JUL-20 Copper (Cu) 98.4 % 70-130 31-JUL-20 Lead (Pb) 104.7 % 70-130 31-JUL-20 Molybdenum (Mo) 104.1 % 70-130 31-JUL-20 Nickel (Ni) 103.3 % 70-130 31-JUL-20 Selenium (Se) 86.1 % 70-130 31-JUL-20 Silver (Ag) 101.6 % 70-130 31-JUL-20 Thallium (Tl) 87.1 % 70-130 31-JUL-20 Vanadium (V) 105.9 % 70-130 31-JUL-20 Zinc (Zn) 102.9 % 70-130 31-JUL-20 WG3374211-6 DUP WG3374211-5 Antimony (Sb) <0.10 <0.10 RPD-NA ug/g N/A 30 31-JUL-20 Arsenic (As) 3.64 3.32 ug/g 9.2 30 31-JUL-20 Barium (Ba) 259 231 ug/g 11 40 31-JUL-20 Beryllium (Be) 0.73 0.64 ug/g 13 30 31-JUL-20 Boron (B) <5.0 <5.0 RPD-NA ug/g N/A 30 31-JUL-20 Cadmium (Cd) 0.059 0.054 ug/g 8.1 30 31-JUL-20 Chromium (Cr) 50.9 45.6 ug/g 11 30 31-JUL-20 Cobalt (Co) 13.8 12.6 ug/g 9.2 30 31-JUL-20 Copper (Cu) 24.8 22.6 ug/g 9.4 30 31-JUL-20 Lead (Pb) 7.11 6.15 ug/g 15 40 31-JUL-20 Molybdenum (Mo) 0.37 0.32 ug/g 16 40 31-JUL-20 Nickel (Ni) 30.3 27.4 ug/g 10 30 31-JUL-20 Selenium (Se) <0.20 <0.20 RPD-NA ug/g N/A 30 31-JUL-20 Silver (Ag) <0.10 <0.10 RPD-NA ug/g N/A 40 31-JUL-20 Thallium (Tl) 0.264 0.229 ug/g 14 30 31-JUL-20 Uranium (U) 0.673 0.589 ug/g 13 30 31-JUL-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 4 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R5172894 WG3374211-6 DUP WG3374211-5 Vanadium (V) 66.9 60.6 ug/g 9.9 30 31-JUL-20 Zinc (Zn) 68.4 62.4 ug/g 9.2 30 31-JUL-20 WG3374211-4 LCS Antimony (Sb) 107.6 % 80-120 31-JUL-20 Arsenic (As) 111.3 % 80-120 31-JUL-20 Barium (Ba) 116.2 % 80-120 31-JUL-20 Beryllium (Be) 103.3 % 80-120 31-JUL-20 Boron (B) 102.4 % 80-120 31-JUL-20 Cadmium (Cd) 103.8 % 80-120 31-JUL-20 Chromium (Cr) 108.4 % 80-120 31-JUL-20 Cobalt (Co) 106.9 % 80-120 31-JUL-20 Copper (Cu) 106.1 % 80-120 31-JUL-20 Lead (Pb) 106.8 % 80-120 31-JUL-20 Molybdenum (Mo) 105.8 % 80-120 31-JUL-20 Nickel (Ni) 106.4 % 80-120 31-JUL-20 Selenium (Se) 107.7 % 80-120 31-JUL-20 Silver (Ag) 105.6 % 80-120 31-JUL-20 Thallium (Tl) 105.6 % 80-120 31-JUL-20 Uranium (U) 98.3 % 80-120 31-JUL-20 Vanadium (V) 110.4 % 80-120 31-JUL-20 Zinc (Zn) 103.7 % 80-120 31-JUL-20 WG3374211-1 MB Antimony (Sb) <0.10 mg/kg 0.1 31-JUL-20 Arsenic (As) <0.10 mg/kg 0.1 31-JUL-20 Barium (Ba) <0.50 mg/kg 0.5 31-JUL-20 Beryllium (Be) <0.10 mg/kg 0.1 31-JUL-20 Boron (B) <5.0 mg/kg 5 31-JUL-20 Cadmium (Cd) <0.020 mg/kg 0.02 31-JUL-20 Chromium (Cr) <0.50 mg/kg 0.5 31-JUL-20 Cobalt (Co) <0.10 mg/kg 0.1 31-JUL-20 Copper (Cu) <0.50 mg/kg 0.5 31-JUL-20 Lead (Pb) <0.50 mg/kg 0.5 31-JUL-20 Molybdenum (Mo) <0.10 mg/kg 0.1 31-JUL-20 Nickel (Ni) <0.50 mg/kg 0.5 31-JUL-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 5 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
MET-200.2-CCMS-WT Soil Batch R5172894 WG3374211-1 MB Selenium (Se) <0.20 mg/kg 0.2 31-JUL-20 Silver (Ag) <0.10 mg/kg 0.1 31-JUL-20 Thallium (Tl) <0.050 mg/kg 0.05 31-JUL-20 Uranium (U) <0.050 mg/kg 0.05 31-JUL-20 Vanadium (V) <0.20 mg/kg 0.2 31-JUL-20 Zinc (Zn) <2.0 mg/kg 2 31-JUL-20
MOISTURE-WT Soil Batch R5171816 WG3373104-3 DUP L2480122-2 % Moisture 5.77 6.38 % 10 20 30-JUL-20 WG3373104-2 LCS % Moisture 101.6 % 90-110 30-JUL-20 WG3373104-1 MB % Moisture <0.25 % 0.25 30-JUL-20
Batch R5171818 WG3373209-6 DUP L2481490-1 % Moisture 3.95 3.94 % 0.4 20 30-JUL-20 WG3373209-5 LCS % Moisture 99.4 % 90-110 30-JUL-20 WG3373209-4 MB % Moisture <0.25 % 0.25 30-JUL-20
Batch R5176670 WG3378510-3 DUP L2484109-3 % Moisture 16.6 16.8 % 1.1 20 08-AUG-20 WG3378510-2 LCS % Moisture 101.4 % 90-110 08-AUG-20 WG3378510-1 MB % Moisture <0.25 % 0.25 08-AUG-20
PAH-511-WT Soil Batch R5173735 WG3372429-3 DUP WG3372429-5 1-Methylnaphthalene <0.030 <0.030 RPD-NA ug/g N/A 40 04-AUG-20 2-Methylnaphthalene <0.030 <0.030 RPD-NA ug/g N/A 40 04-AUG-20 Acenaphthene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Acenaphthylene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 6 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R5173735 WG3372429-3 DUP WG3372429-5 Anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(a)anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(a)pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(b)fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(g,h,i)perylene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(k)fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Chrysene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Dibenzo(ah)anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Fluorene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Indeno(1,2,3-cd)pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Naphthalene <0.013 <0.013 RPD-NA ug/g N/A 40 04-AUG-20 Phenanthrene <0.046 <0.046 RPD-NA ug/g N/A 40 04-AUG-20 Pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 WG3372429-2 LCS 1-Methylnaphthalene 85.7 % 50-140 04-AUG-20 2-Methylnaphthalene 82.5 % 50-140 04-AUG-20 Acenaphthene 84.2 % 50-140 04-AUG-20 Acenaphthylene 80.5 % 50-140 04-AUG-20 Anthracene 86.9 % 50-140 04-AUG-20 Benzo(a)anthracene 84.0 % 50-140 04-AUG-20 Benzo(a)pyrene 80.9 % 50-140 04-AUG-20 Benzo(b)fluoranthene 79.6 % 50-140 04-AUG-20 Benzo(g,h,i)perylene 72.4 % 50-140 04-AUG-20 Benzo(k)fluoranthene 86.5 % 50-140 04-AUG-20 Chrysene 88.9 % 50-140 04-AUG-20 Dibenzo(ah)anthracene 74.2 % 50-140 04-AUG-20 Fluoranthene 76.6 % 50-140 04-AUG-20 Fluorene 76.9 % 50-140 04-AUG-20 Indeno(1,2,3-cd)pyrene 70.3 % 50-140 04-AUG-20 Naphthalene 85.8 % 50-140 04-AUG-20 Phenanthrene 83.5 % 50-140 04-AUG-20 Pyrene 77.1 % 50-140 04-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 7 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R5173735 WG3372429-1 MB 1-Methylnaphthalene <0.030 ug/g 0.03 04-AUG-20 2-Methylnaphthalene <0.030 ug/g 0.03 04-AUG-20 Acenaphthene <0.050 ug/g 0.05 04-AUG-20 Acenaphthylene <0.050 ug/g 0.05 04-AUG-20 Anthracene <0.050 ug/g 0.05 04-AUG-20 Benzo(a)anthracene <0.050 ug/g 0.05 04-AUG-20 Benzo(a)pyrene <0.050 ug/g 0.05 04-AUG-20 Benzo(b)fluoranthene <0.050 ug/g 0.05 04-AUG-20 Benzo(g,h,i)perylene <0.050 ug/g 0.05 04-AUG-20 Benzo(k)fluoranthene <0.050 ug/g 0.05 04-AUG-20 Chrysene <0.050 ug/g 0.05 04-AUG-20 Dibenzo(ah)anthracene <0.050 ug/g 0.05 04-AUG-20 Fluoranthene <0.050 ug/g 0.05 04-AUG-20 Fluorene <0.050 ug/g 0.05 04-AUG-20 Indeno(1,2,3-cd)pyrene <0.050 ug/g 0.05 04-AUG-20 Naphthalene <0.013 ug/g 0.013 04-AUG-20 Phenanthrene <0.046 ug/g 0.046 04-AUG-20 Pyrene <0.050 ug/g 0.05 04-AUG-20 Surrogate: 2-Fluorobiphenyl 89.9 % 50-140 04-AUG-20 Surrogate: p-Terphenyl d14 92.7 % 50-140 04-AUG-20 WG3372429-4 MS WG3372429-5 1-Methylnaphthalene 89.5 % 50-140 04-AUG-20 2-Methylnaphthalene 86.2 % 50-140 04-AUG-20 Acenaphthene 88.5 % 50-140 04-AUG-20 Acenaphthylene 83.2 % 50-140 04-AUG-20 Anthracene 90.7 % 50-140 04-AUG-20 Benzo(a)anthracene 87.3 % 50-140 04-AUG-20 Benzo(a)pyrene 84.4 % 50-140 04-AUG-20 Benzo(b)fluoranthene 84.0 % 50-140 04-AUG-20 Benzo(g,h,i)perylene 75.9 % 50-140 04-AUG-20 Benzo(k)fluoranthene 89.5 % 50-140 04-AUG-20 Chrysene 94.0 % 50-140 04-AUG-20 Dibenzo(ah)anthracene 77.6 % 50-140 04-AUG-20 Fluoranthene 81.1 % 50-140 04-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 8 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R5173735 WG3372429-4 MS WG3372429-5 Fluorene 80.8 % 50-140 04-AUG-20 Indeno(1,2,3-cd)pyrene 73.8 % 50-140 04-AUG-20 Naphthalene 89.9 % 50-140 04-AUG-20 Phenanthrene 88.1 % 50-140 04-AUG-20 Pyrene 82.0 % 50-140 04-AUG-20
Batch R5174007 WG3373361-3 DUP WG3373361-5 1-Methylnaphthalene <0.030 <0.030 RPD-NA ug/g N/A 40 04-AUG-20 2-Methylnaphthalene <0.030 <0.030 RPD-NA ug/g N/A 40 04-AUG-20 Acenaphthene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Acenaphthylene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(a)anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(a)pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(b)fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(g,h,i)perylene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Benzo(k)fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Chrysene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Dibenzo(ah)anthracene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Fluoranthene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Fluorene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Indeno(1,2,3-cd)pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 Naphthalene <0.013 <0.013 RPD-NA ug/g N/A 40 04-AUG-20 Phenanthrene <0.046 <0.046 RPD-NA ug/g N/A 40 04-AUG-20 Pyrene <0.050 <0.050 RPD-NA ug/g N/A 40 04-AUG-20 WG3373361-2 LCS 1-Methylnaphthalene 90.0 % 50-140 04-AUG-20 2-Methylnaphthalene 87.7 % 50-140 04-AUG-20 Acenaphthene 89.9 % 50-140 04-AUG-20 Acenaphthylene 85.0 % 50-140 04-AUG-20 Anthracene 91.6 % 50-140 04-AUG-20 Benzo(a)anthracene 95.4 % 50-140 04-AUG-20 Benzo(a)pyrene 88.7 % 50-140 04-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 9 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R5174007 WG3373361-2 LCS Benzo(b)fluoranthene 94.7 % 50-140 04-AUG-20 Benzo(g,h,i)perylene 92.3 % 50-140 04-AUG-20 Benzo(k)fluoranthene 88.5 % 50-140 04-AUG-20 Chrysene 105.8 % 50-140 04-AUG-20 Dibenzo(ah)anthracene 92.3 % 50-140 04-AUG-20 Fluoranthene 82.8 % 50-140 04-AUG-20 Fluorene 83.6 % 50-140 04-AUG-20 Indeno(1,2,3-cd)pyrene 98.0 % 50-140 04-AUG-20 Naphthalene 90.1 % 50-140 04-AUG-20 Phenanthrene 89.9 % 50-140 04-AUG-20 Pyrene 82.7 % 50-140 04-AUG-20 WG3373361-1 MB 1-Methylnaphthalene <0.030 ug/g 0.03 04-AUG-20 2-Methylnaphthalene <0.030 ug/g 0.03 04-AUG-20 Acenaphthene <0.050 ug/g 0.05 04-AUG-20 Acenaphthylene <0.050 ug/g 0.05 04-AUG-20 Anthracene <0.050 ug/g 0.05 04-AUG-20 Benzo(a)anthracene <0.050 ug/g 0.05 04-AUG-20 Benzo(a)pyrene <0.050 ug/g 0.05 04-AUG-20 Benzo(b)fluoranthene <0.050 ug/g 0.05 04-AUG-20 Benzo(g,h,i)perylene <0.050 ug/g 0.05 04-AUG-20 Benzo(k)fluoranthene <0.050 ug/g 0.05 04-AUG-20 Chrysene <0.050 ug/g 0.05 04-AUG-20 Dibenzo(ah)anthracene <0.050 ug/g 0.05 04-AUG-20 Fluoranthene <0.050 ug/g 0.05 04-AUG-20 Fluorene <0.050 ug/g 0.05 04-AUG-20 Indeno(1,2,3-cd)pyrene <0.050 ug/g 0.05 04-AUG-20 Naphthalene <0.013 ug/g 0.013 04-AUG-20 Phenanthrene <0.046 ug/g 0.046 04-AUG-20 Pyrene <0.050 ug/g 0.05 04-AUG-20 Surrogate: 2-Fluorobiphenyl 92.1 % 50-140 04-AUG-20 Surrogate: p-Terphenyl d14 91.3 % 50-140 04-AUG-20 WG3373361-4 MS WG3373361-5 1-Methylnaphthalene 82.7 % 50-140 04-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 10 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Soil Batch R5174007 WG3373361-4 MS WG3373361-5 2-Methylnaphthalene 81.1 % 50-140 04-AUG-20 Acenaphthene 82.4 % 50-140 04-AUG-20 Acenaphthylene 78.2 % 50-140 04-AUG-20 Anthracene 85.6 % 50-140 04-AUG-20 Benzo(a)anthracene 91.1 % 50-140 04-AUG-20 Benzo(a)pyrene 82.3 % 50-140 04-AUG-20 Benzo(b)fluoranthene 90.6 % 50-140 04-AUG-20 Benzo(g,h,i)perylene 83.1 % 50-140 04-AUG-20 Benzo(k)fluoranthene 81.8 % 50-140 04-AUG-20 Chrysene 99.4 % 50-140 04-AUG-20 Dibenzo(ah)anthracene 83.3 % 50-140 04-AUG-20 Fluoranthene 76.4 % 50-140 04-AUG-20 Fluorene 76.7 % 50-140 04-AUG-20 Indeno(1,2,3-cd)pyrene 90.3 % 50-140 04-AUG-20 Naphthalene 83.7 % 50-140 04-AUG-20 Phenanthrene 83.1 % 50-140 04-AUG-20 Pyrene 76.0 % 50-140 04-AUG-20
VOC-511-HS-WT Soil Batch R5170178 WG3371564-17 DUP WG3371564-16 1,1,1,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,1,2,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,1,1-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,1,2-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,1-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,1-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,2-Dibromoethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,2-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,2-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,2-Dichloropropane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,3-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 1,4-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Acetone <0.50 <0.50 RPD-NA ug/g N/A 40 31-JUL-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 11 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170178 WG3371564-17 DUP WG3371564-16 Benzene <0.0068 <0.0068 RPD-NA ug/g N/A 40 31-JUL-20 Bromodichloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Bromoform <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Bromomethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Carbon tetrachloride <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Chlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Chloroform <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 cis-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 cis-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 31-JUL-20 Dibromochloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Dichlorodifluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Ethylbenzene <0.018 <0.018 RPD-NA ug/g N/A 40 31-JUL-20 n-Hexane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Methylene Chloride <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 MTBE <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 m+p-Xylenes <0.030 <0.030 RPD-NA ug/g N/A 40 31-JUL-20 Methyl Ethyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 31-JUL-20 Methyl Isobutyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 31-JUL-20 o-Xylene <0.020 <0.020 RPD-NA ug/g N/A 40 31-JUL-20 Styrene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Tetrachloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Toluene <0.080 <0.080 RPD-NA ug/g N/A 40 31-JUL-20 trans-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 trans-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 31-JUL-20 Trichloroethylene <0.010 <0.010 RPD-NA ug/g N/A 40 31-JUL-20 Trichlorofluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 31-JUL-20 Vinyl chloride <0.020 <0.020 RPD-NA ug/g N/A 40 31-JUL-20 WG3371564-2 LCS 1,1,1,2-Tetrachloroethane 102.5 % 60-130 29-JUL-20 1,1,2,2-Tetrachloroethane 93.1 % 60-130 29-JUL-20 1,1,1-Trichloroethane 102.6 % 60-130 29-JUL-20 1,1,2-Trichloroethane 108.1 % 60-130 29-JUL-20 1,1-Dichloroethane 100.9 % 60-130 29-JUL-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 12 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170178 WG3371564-2 LCS 1,1-Dichloroethylene 93.7 % 60-130 29-JUL-20 1,2-Dibromoethane 99.2 % 70-130 29-JUL-20 1,2-Dichlorobenzene 104.4 % 70-130 29-JUL-20 1,2-Dichloroethane 101.1 % 60-130 29-JUL-20 1,2-Dichloropropane 104.3 % 70-130 29-JUL-20 1,3-Dichlorobenzene 108.2 % 70-130 29-JUL-20 1,4-Dichlorobenzene 107.3 % 70-130 29-JUL-20 Acetone 108.3 % 60-140 29-JUL-20 Benzene 101.2 % 70-130 29-JUL-20 Bromodichloromethane 110.7 % 50-140 29-JUL-20 Bromoform 101.2 % 70-130 29-JUL-20 Bromomethane 115.2 % 50-140 29-JUL-20 Carbon tetrachloride 99.3 % 70-130 29-JUL-20 Chlorobenzene 108.2 % 70-130 29-JUL-20 Chloroform 101.8 % 70-130 29-JUL-20 cis-1,2-Dichloroethylene 107.1 % 70-130 29-JUL-20 cis-1,3-Dichloropropene 100.8 % 70-130 29-JUL-20 Dibromochloromethane 101.4 % 60-130 29-JUL-20 Dichlorodifluoromethane 73.2 % 50-140 29-JUL-20 Ethylbenzene 104.9 % 70-130 29-JUL-20 n-Hexane 94.0 % 70-130 29-JUL-20 Methylene Chloride 95.9 % 70-130 29-JUL-20 MTBE 103.1 % 70-130 29-JUL-20 m+p-Xylenes 105.0 % 70-130 29-JUL-20 Methyl Ethyl Ketone 96.9 % 60-140 29-JUL-20 Methyl Isobutyl Ketone 88.5 % 60-140 29-JUL-20 o-Xylene 110.6 % 70-130 29-JUL-20 Styrene 104.7 % 70-130 29-JUL-20 Tetrachloroethylene 106.6 % 60-130 29-JUL-20 Toluene 104.4 % 70-130 29-JUL-20 trans-1,2-Dichloroethylene 98.4 % 60-130 29-JUL-20 trans-1,3-Dichloropropene 111.9 % 70-130 29-JUL-20 Trichloroethylene 105.5 % 60-130 29-JUL-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 13 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170178 WG3371564-2 LCS Trichlorofluoromethane 92.5 % 50-140 29-JUL-20 Vinyl chloride 99.1 % 60-140 29-JUL-20 WG3371564-1 MB 1,1,1,2-Tetrachloroethane <0.050 ug/g 0.05 29-JUL-20 1,1,2,2-Tetrachloroethane <0.050 ug/g 0.05 29-JUL-20 1,1,1-Trichloroethane <0.050 ug/g 0.05 29-JUL-20 1,1,2-Trichloroethane <0.050 ug/g 0.05 29-JUL-20 1,1-Dichloroethane <0.050 ug/g 0.05 29-JUL-20 1,1-Dichloroethylene <0.050 ug/g 0.05 29-JUL-20 1,2-Dibromoethane <0.050 ug/g 0.05 29-JUL-20 1,2-Dichlorobenzene <0.050 ug/g 0.05 29-JUL-20 1,2-Dichloroethane <0.050 ug/g 0.05 29-JUL-20 1,2-Dichloropropane <0.050 ug/g 0.05 29-JUL-20 1,3-Dichlorobenzene <0.050 ug/g 0.05 29-JUL-20 1,4-Dichlorobenzene <0.050 ug/g 0.05 29-JUL-20 Acetone <0.50 ug/g 0.5 29-JUL-20 Benzene <0.0068 ug/g 0.0068 29-JUL-20 Bromodichloromethane <0.050 ug/g 0.05 29-JUL-20 Bromoform <0.050 ug/g 0.05 29-JUL-20 Bromomethane <0.050 ug/g 0.05 29-JUL-20 Carbon tetrachloride <0.050 ug/g 0.05 29-JUL-20 Chlorobenzene <0.050 ug/g 0.05 29-JUL-20 Chloroform <0.050 ug/g 0.05 29-JUL-20 cis-1,2-Dichloroethylene <0.050 ug/g 0.05 29-JUL-20 cis-1,3-Dichloropropene <0.030 ug/g 0.03 29-JUL-20 Dibromochloromethane <0.050 ug/g 0.05 29-JUL-20 Dichlorodifluoromethane <0.050 ug/g 0.05 29-JUL-20 Ethylbenzene <0.018 ug/g 0.018 29-JUL-20 n-Hexane <0.050 ug/g 0.05 29-JUL-20 Methylene Chloride <0.050 ug/g 0.05 29-JUL-20 MTBE <0.050 ug/g 0.05 29-JUL-20 m+p-Xylenes <0.030 ug/g 0.03 29-JUL-20 Methyl Ethyl Ketone <0.50 ug/g 0.5 29-JUL-20 Methyl Isobutyl Ketone <0.50 ug/g 0.5 29-JUL-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 14 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170178 WG3371564-1 MB o-Xylene <0.020 ug/g 0.02 29-JUL-20 Styrene <0.050 ug/g 0.05 29-JUL-20 Tetrachloroethylene <0.050 ug/g 0.05 29-JUL-20 Toluene <0.080 ug/g 0.08 29-JUL-20 trans-1,2-Dichloroethylene <0.050 ug/g 0.05 29-JUL-20 trans-1,3-Dichloropropene <0.030 ug/g 0.03 29-JUL-20 Trichloroethylene <0.010 ug/g 0.01 29-JUL-20 Trichlorofluoromethane <0.050 ug/g 0.05 29-JUL-20 Vinyl chloride <0.020 ug/g 0.02 29-JUL-20 Surrogate: 1,4-Difluorobenzene 119.6 % 50-140 29-JUL-20 Surrogate: 4-Bromofluorobenzene 101.9 % 50-140 29-JUL-20 WG3371564-18 MS WG3371564-16 1,1,1,2-Tetrachloroethane 104.1 % 50-140 31-JUL-20 1,1,2,2-Tetrachloroethane 89.6 % 50-140 31-JUL-20 1,1,1-Trichloroethane 104.8 % 50-140 31-JUL-20 1,1,2-Trichloroethane 108.1 % 50-140 31-JUL-20 1,1-Dichloroethane 101.5 % 50-140 31-JUL-20 1,1-Dichloroethylene 94.9 % 50-140 31-JUL-20 1,2-Dibromoethane 98.7 % 50-140 31-JUL-20 1,2-Dichlorobenzene 105.2 % 50-140 31-JUL-20 1,2-Dichloroethane 99.5 % 50-140 31-JUL-20 1,2-Dichloropropane 104.1 % 50-140 31-JUL-20 1,3-Dichlorobenzene 108.2 % 50-140 31-JUL-20 1,4-Dichlorobenzene 107.1 % 50-140 31-JUL-20 Acetone 109.2 % 50-140 31-JUL-20 Benzene 102.0 % 50-140 31-JUL-20 Bromodichloromethane 111.3 % 50-140 31-JUL-20 Bromoform 102.6 % 50-140 31-JUL-20 Bromomethane 114.8 % 50-140 31-JUL-20 Carbon tetrachloride 102.2 % 50-140 31-JUL-20 Chlorobenzene 108.9 % 50-140 31-JUL-20 Chloroform 102.9 % 50-140 31-JUL-20 cis-1,2-Dichloroethylene 107.7 % 50-140 31-JUL-20 cis-1,3-Dichloropropene 93.0 % 50-140 31-JUL-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 15 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5170178 WG3371564-18 MS WG3371564-16 Dibromochloromethane 102.2 % 50-140 31-JUL-20 Dichlorodifluoromethane 83.1 % 50-140 31-JUL-20 Ethylbenzene 105.8 % 50-140 31-JUL-20 n-Hexane 98.2 % 50-140 31-JUL-20 Methylene Chloride 96.3 % 50-140 31-JUL-20 MTBE 103.0 % 50-140 31-JUL-20 m+p-Xylenes 105.4 % 50-140 31-JUL-20 Methyl Ethyl Ketone 87.8 % 50-140 31-JUL-20 Methyl Isobutyl Ketone 85.4 % 50-140 31-JUL-20 o-Xylene 111.5 % 50-140 31-JUL-20 Styrene 105.5 % 50-140 31-JUL-20 Tetrachloroethylene 107.5 % 50-140 31-JUL-20 Toluene 105.6 % 50-140 31-JUL-20 trans-1,2-Dichloroethylene 97.5 % 50-140 31-JUL-20 trans-1,3-Dichloropropene 103.9 % 50-140 31-JUL-20 Trichloroethylene 107.3 % 50-140 31-JUL-20 Trichlorofluoromethane 96.6 % 50-140 31-JUL-20 Vinyl chloride 101.8 % 50-140 31-JUL-20
Batch R5177137 WG3378198-4 DUP WG3378198-3 1,1,1,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,1,2,2-Tetrachloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,1,1-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,1,2-Trichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,1-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,1-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,2-Dibromoethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,2-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,2-Dichloroethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,2-Dichloropropane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,3-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 1,4-Dichlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Acetone <0.50 <0.50 RPD-NA ug/g N/A 40 10-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 16 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5177137 WG3378198-4 DUP WG3378198-3 Benzene <0.0068 <0.0068 RPD-NA ug/g N/A 40 10-AUG-20 Bromodichloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Bromoform <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Bromomethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Carbon tetrachloride <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Chlorobenzene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Chloroform <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 cis-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 cis-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 10-AUG-20 Dibromochloromethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Dichlorodifluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Ethylbenzene <0.018 <0.018 RPD-NA ug/g N/A 40 10-AUG-20 n-Hexane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Methylene Chloride <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 MTBE <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 m+p-Xylenes <0.030 <0.030 RPD-NA ug/g N/A 40 10-AUG-20 Methyl Ethyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 10-AUG-20 Methyl Isobutyl Ketone <0.50 <0.50 RPD-NA ug/g N/A 40 10-AUG-20 o-Xylene <0.020 <0.020 RPD-NA ug/g N/A 40 10-AUG-20 Styrene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Tetrachloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Toluene <0.080 <0.080 RPD-NA ug/g N/A 40 10-AUG-20 trans-1,2-Dichloroethylene <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 trans-1,3-Dichloropropene <0.030 <0.030 RPD-NA ug/g N/A 40 10-AUG-20 Trichloroethylene <0.010 <0.010 RPD-NA ug/g N/A 40 10-AUG-20 Trichlorofluoromethane <0.050 <0.050 RPD-NA ug/g N/A 40 10-AUG-20 Vinyl chloride <0.020 <0.020 RPD-NA ug/g N/A 40 10-AUG-20 WG3378198-2 LCS 1,1,1,2-Tetrachloroethane 107.5 % 60-130 10-AUG-20 1,1,2,2-Tetrachloroethane 94.2 % 60-130 10-AUG-20 1,1,1-Trichloroethane 109.8 % 60-130 10-AUG-20 1,1,2-Trichloroethane 107.4 % 60-130 10-AUG-20 1,1-Dichloroethane 109.2 % 60-130 10-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 17 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5177137 WG3378198-2 LCS 1,1-Dichloroethylene 103.3 % 60-130 10-AUG-20 1,2-Dibromoethane 100.9 % 70-130 10-AUG-20 1,2-Dichlorobenzene 106.9 % 70-130 10-AUG-20 1,2-Dichloroethane 104.6 % 60-130 10-AUG-20 1,2-Dichloropropane 103.6 % 70-130 10-AUG-20 1,3-Dichlorobenzene 109.0 % 70-130 10-AUG-20 1,4-Dichlorobenzene 109.2 % 70-130 10-AUG-20 Acetone 109.2 % 60-140 10-AUG-20 Benzene 109.0 % 70-130 10-AUG-20 Bromodichloromethane 114.5 % 50-140 10-AUG-20 Bromoform 96.3 % 70-130 10-AUG-20 Bromomethane 131.4 % 50-140 10-AUG-20 Carbon tetrachloride 109.9 % 70-130 10-AUG-20 Chlorobenzene 110.1 % 70-130 10-AUG-20 Chloroform 112.4 % 70-130 10-AUG-20 cis-1,2-Dichloroethylene 102.0 % 70-130 10-AUG-20 cis-1,3-Dichloropropene 108.5 % 70-130 10-AUG-20 Dibromochloromethane 98.4 % 60-130 10-AUG-20 Dichlorodifluoromethane 78.1 % 50-140 10-AUG-20 Ethylbenzene 107.8 % 70-130 10-AUG-20 n-Hexane 104.5 % 70-130 10-AUG-20 Methylene Chloride 113.3 % 70-130 10-AUG-20 MTBE 107.2 % 70-130 10-AUG-20 m+p-Xylenes 106.7 % 70-130 10-AUG-20 Methyl Ethyl Ketone 91.1 % 60-140 10-AUG-20 Methyl Isobutyl Ketone 92.2 % 60-140 10-AUG-20 o-Xylene 110.6 % 70-130 10-AUG-20 Styrene 101.2 % 70-130 10-AUG-20 Tetrachloroethylene 111.3 % 60-130 10-AUG-20 Toluene 108.7 % 70-130 10-AUG-20 trans-1,2-Dichloroethylene 111.9 % 60-130 10-AUG-20 trans-1,3-Dichloropropene 122.9 % 70-130 10-AUG-20 Trichloroethylene 110.6 % 60-130 10-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 18 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5177137 WG3378198-2 LCS Trichlorofluoromethane 97.2 % 50-140 10-AUG-20 Vinyl chloride 104.8 % 60-140 10-AUG-20 WG3378198-1 MB 1,1,1,2-Tetrachloroethane <0.050 ug/g 0.05 10-AUG-20 1,1,2,2-Tetrachloroethane <0.050 ug/g 0.05 10-AUG-20 1,1,1-Trichloroethane <0.050 ug/g 0.05 10-AUG-20 1,1,2-Trichloroethane <0.050 ug/g 0.05 10-AUG-20 1,1-Dichloroethane <0.050 ug/g 0.05 10-AUG-20 1,1-Dichloroethylene <0.050 ug/g 0.05 10-AUG-20 1,2-Dibromoethane <0.050 ug/g 0.05 10-AUG-20 1,2-Dichlorobenzene <0.050 ug/g 0.05 10-AUG-20 1,2-Dichloroethane <0.050 ug/g 0.05 10-AUG-20 1,2-Dichloropropane <0.050 ug/g 0.05 10-AUG-20 1,3-Dichlorobenzene <0.050 ug/g 0.05 10-AUG-20 1,4-Dichlorobenzene <0.050 ug/g 0.05 10-AUG-20 Acetone <0.50 ug/g 0.5 10-AUG-20 Benzene <0.0068 ug/g 0.0068 10-AUG-20 Bromodichloromethane <0.050 ug/g 0.05 10-AUG-20 Bromoform <0.050 ug/g 0.05 10-AUG-20 Bromomethane <0.050 ug/g 0.05 10-AUG-20 Carbon tetrachloride <0.050 ug/g 0.05 10-AUG-20 Chlorobenzene <0.050 ug/g 0.05 10-AUG-20 Chloroform <0.050 ug/g 0.05 10-AUG-20 cis-1,2-Dichloroethylene <0.050 ug/g 0.05 10-AUG-20 cis-1,3-Dichloropropene <0.030 ug/g 0.03 10-AUG-20 Dibromochloromethane <0.050 ug/g 0.05 10-AUG-20 Dichlorodifluoromethane <0.050 ug/g 0.05 10-AUG-20 Ethylbenzene <0.018 ug/g 0.018 10-AUG-20 n-Hexane <0.050 ug/g 0.05 10-AUG-20 Methylene Chloride <0.050 ug/g 0.05 10-AUG-20 MTBE <0.050 ug/g 0.05 10-AUG-20 m+p-Xylenes <0.030 ug/g 0.03 10-AUG-20 Methyl Ethyl Ketone <0.50 ug/g 0.5 10-AUG-20 Methyl Isobutyl Ketone <0.50 ug/g 0.5 10-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 19 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5177137 WG3378198-1 MB o-Xylene <0.020 ug/g 0.02 10-AUG-20 Styrene <0.050 ug/g 0.05 10-AUG-20 Tetrachloroethylene <0.050 ug/g 0.05 10-AUG-20 Toluene <0.080 ug/g 0.08 10-AUG-20 trans-1,2-Dichloroethylene <0.050 ug/g 0.05 10-AUG-20 trans-1,3-Dichloropropene <0.030 ug/g 0.03 10-AUG-20 Trichloroethylene <0.010 ug/g 0.01 10-AUG-20 Trichlorofluoromethane <0.050 ug/g 0.05 10-AUG-20 Vinyl chloride <0.020 ug/g 0.02 10-AUG-20 Surrogate: 1,4-Difluorobenzene 105.6 % 50-140 10-AUG-20 Surrogate: 4-Bromofluorobenzene 84.7 % 50-140 10-AUG-20 WG3378198-5 MS WG3378198-3 1,1,1,2-Tetrachloroethane 112.4 % 50-140 10-AUG-20 1,1,2,2-Tetrachloroethane 106.9 % 50-140 10-AUG-20 1,1,1-Trichloroethane 114.6 % 50-140 10-AUG-20 1,1,2-Trichloroethane 112.4 % 50-140 10-AUG-20 1,1-Dichloroethane 113.9 % 50-140 10-AUG-20 1,1-Dichloroethylene 108.4 % 50-140 10-AUG-20 1,2-Dibromoethane 104.9 % 50-140 10-AUG-20 1,2-Dichlorobenzene 110.2 % 50-140 10-AUG-20 1,2-Dichloroethane 108.6 % 50-140 10-AUG-20 1,2-Dichloropropane 107.8 % 50-140 10-AUG-20 1,3-Dichlorobenzene 108.1 % 50-140 10-AUG-20 1,4-Dichlorobenzene 109.3 % 50-140 10-AUG-20 Acetone 117.7 % 50-140 10-AUG-20 Benzene 113.4 % 50-140 10-AUG-20 Bromodichloromethane 119.6 % 50-140 10-AUG-20 Bromoform 103.8 % 50-140 10-AUG-20 Bromomethane 128.4 % 50-140 10-AUG-20 Carbon tetrachloride 114.8 % 50-140 10-AUG-20 Chlorobenzene 114.2 % 50-140 10-AUG-20 Chloroform 117.0 % 50-140 10-AUG-20 cis-1,2-Dichloroethylene 105.4 % 50-140 10-AUG-20 cis-1,3-Dichloropropene 101.8 % 50-140 10-AUG-20 Quality Control Report
Workorder: L2480127 Report Date: 11-AUG-20 Page 20 of 21
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Soil Batch R5177137 WG3378198-5 MS WG3378198-3 Dibromochloromethane 103.1 % 50-140 10-AUG-20 Dichlorodifluoromethane 88.3 % 50-140 10-AUG-20 Ethylbenzene 111.5 % 50-140 10-AUG-20 n-Hexane 111.1 % 50-140 10-AUG-20 Methylene Chloride 117.5 % 50-140 10-AUG-20 MTBE 111.6 % 50-140 10-AUG-20 m+p-Xylenes 110.1 % 50-140 10-AUG-20 Methyl Ethyl Ketone 90.1 % 50-140 10-AUG-20 Methyl Isobutyl Ketone 100.5 % 50-140 10-AUG-20 o-Xylene 114.6 % 50-140 10-AUG-20 Styrene 104.6 % 50-140 10-AUG-20 Tetrachloroethylene 114.2 % 50-140 10-AUG-20 Toluene 112.3 % 50-140 10-AUG-20 trans-1,2-Dichloroethylene 115.8 % 50-140 10-AUG-20 trans-1,3-Dichloropropene 110.3 % 50-140 10-AUG-20 Trichloroethylene 114.9 % 50-140 10-AUG-20 Trichlorofluoromethane 103.0 % 50-140 10-AUG-20 Vinyl chloride 110.8 % 50-140 10-AUG-20 Quality Control Report Workorder: L2480127 Report Date: 11-AUG-20
Client: Morrison Hershfield Limited (Ottawa) Page 21 of 21 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order. ALS Sample ID: L2480127-2 Client Sample ID: BH10 SA3
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Printed on 7/31/2020 7:13:37 PM ALS Sample ID: L2480127-4 Client Sample ID: BH9 SA4 500
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Printed on 7/31/2020 7:13:39 PM ALS Sample ID: L2480127-6 Client Sample ID: BH9 SA6 500
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Printed on 7/31/2020 7:13:41 PM
Morrison Hershfield Limited (Ottawa) Date Received: 29-JUL-20 ATTN: Mitchell Dawley Report Date: 06-AUG-20 15:19 (MT) Version: FINAL 2440 Don Reid Drive Ottawa ON K1H 1E1
Client Phone: 613-739-2910
Certificate of Analysis Lab Work Order #: L2481358 Project P.O. #: 20102333-L3-$1,483.00 Job Reference: 190441800 C of C Numbers: Legal Site Desc:
______Emily Smith Account Manager [This report shall not be reproduced except in full without the written authority of the Laboratory.]
ADDRESS: 190 Colonnade Road, Unit 7, Ottawa, ON K2E 7J5 Canada | Phone: +1 613 225 8279 | Fax: +1 613 225 2801 ALS CANADA LTD Part of the ALS Group An ALS Limited Company L2481358 CONTD.... ANALYTICAL GUIDELINE REPORT Page 2 of 17 190441800 06-AUG-20 15:19 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2481358-1 BH9 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Physical Tests Total Suspended Solids 1060 DLHC 150 mg/L 04-AUG-20 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 05-AUG-20 2700 130000 130000 Benzene 88.3 OWP 0.50 ug/L 05-AUG-20 *0.5 *44 430 Bromodichloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 85000 85000 Bromoform <5.0 OWP 5.0 ug/L 05-AUG-20 5 380 770 Bromomethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.89 5.6 56 Carbon tetrachloride <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.79 8.4 Chlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 630 630 Dibromochloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 82000 82000 Chloroform <1.7 DLVH 1.7 ug/L 05-AUG-20 2 2.4 22 1,2-Dibromoethane <0.28 DLVH 0.28 ug/L 05-AUG-20 **0.2 **0.25 0.83 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4600 9600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 9600 9600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 8 67 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 05-AUG-20 590 4400 4400 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 320 3100 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 12 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 cis-1,2-Dichloroethylene <1.3 DLVH 1.3 ug/L 05-AUG-20 1.6 1.6 17 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 Methylene Chloride <5.0 OWP 5.0 ug/L 05-AUG-20 5 610 5500 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 16 140 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 06-AUG-20 0.5 5.2 45 Ethylbenzene 12.4 OWP 0.50 ug/L 05-AUG-20 *0.5 2300 2300 n-Hexane 14.0 OWP 0.50 ug/L 06-AUG-20 *5 51 520 Methyl Ethyl Ketone <20 OWP 20 ug/L 05-AUG-20 400 470000 1500000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 05-AUG-20 640 140000 580000 MTBE <2.0 OWP 2.0 ug/L 05-AUG-20 15 190 1400 Styrene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1300 9100 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 1.1 3.3 28 1,1,2,2-Tetrachloroethane <0.60 DLVH 0.60 ug/L 05-AUG-20 **0.5 3.2 15 Tetrachloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Toluene 6.73 OWP 0.50 ug/L 05-AUG-20 *0.8 18000 18000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 640 6700 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4.7 30 Trichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 05-AUG-20 150 2500 2500 Vinyl chloride <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 0.5 1.7 o-Xylene 1.32 OWP 0.30 ug/L 05-AUG-20 m+p-Xylenes 10.0 OWP 0.40 ug/L 05-AUG-20 Xylenes (Total) 11.4 0.50 ug/L 06-AUG-20 72 4200 4200 Surrogate: 4-Bromofluorobenzene 92.9 70-130 % 05-AUG-20 Surrogate: 1,4-Difluorobenzene 92.6 70-130 % 05-AUG-20 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
#3: T3-Non-Potable Ground Water-All Types of Property Uses (Fine) L2481358 CONTD.... ANALYTICAL GUIDELINE REPORT Page 3 of 17 190441800 06-AUG-20 15:19 (MT) Sample Details Grouping Analyte Result Qualifier D.L. Units Analyzed Guideline Limits
L2481358-1 BH9 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Hydrocarbons F1 (C6-C10) 513 OWP 25 ug/L 05-AUG-20 *420 750 750 F1-BTEX 394 25 ug/L 06-AUG-20 420 750 750 F2 (C10-C16) 620 100 ug/L 31-JUL-20 *150 *150 *150 F2-Naphth 620 100 ug/L 06-AUG-20 F3 (C16-C34) 320 250 ug/L 31-JUL-20 500 500 500 F3-PAH 320 250 ug/L 06-AUG-20 F4 (C34-C50) <250 250 ug/L 31-JUL-20 500 500 500 Total Hydrocarbons (C6-C50) 1450 370 ug/L 06-AUG-20 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 93.4 60-140 % 31-JUL-20 Surrogate: 3,4-Dichlorotoluene 82.1 60-140 % 05-AUG-20 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.248 0.020 ug/L 06-AUG-20 4.1 600 1700 Acenaphthylene <0.062 DLQ 0.062 ug/L 06-AUG-20 1 1.8 1.8 Anthracene <0.040 DLQ 0.040 ug/L 06-AUG-20 0.1 2.4 2.4 Benzo(a)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 4.7 4.7 Benzo(a)pyrene <0.010 0.010 ug/L 06-AUG-20 0.01 0.81 0.81 Benzo(b)fluoranthene <0.020 0.020 ug/L 06-AUG-20 0.1 0.75 0.75 Benzo(g,h,i)perylene <0.020 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 Benzo(k)fluoranthene <0.020 0.020 ug/L 06-AUG-20 0.1 0.4 0.4 Chrysene <0.020 0.020 ug/L 06-AUG-20 0.1 1 1 Dibenzo(ah)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 0.52 0.52 Fluoranthene 0.056 0.020 ug/L 06-AUG-20 0.4 130 130 Fluorene 0.265 0.020 ug/L 06-AUG-20 120 400 400 Indeno(1,2,3-cd)pyrene <0.020 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 1+2-Methylnaphthalenes 10.3 0.028 ug/L 06-AUG-20 *2 1800 1800 1-Methylnaphthalene 6.36 0.020 ug/L 06-AUG-20 *2 1800 1800 2-Methylnaphthalene 3.93 0.020 ug/L 06-AUG-20 *2 1800 1800 Naphthalene <1.62 DLQ 1.6 ug/L 06-AUG-20 7 1400 6400 Phenanthrene 0.256 0.020 ug/L 06-AUG-20 *0.1 580 580 Pyrene 0.087 0.020 ug/L 06-AUG-20 0.2 68 68 Surrogate: d10-Acenaphthene 91.7 60-140 % 06-AUG-20 Surrogate: d12-Chrysene 102.9 60-140 % 06-AUG-20 Surrogate: d8-Naphthalene 88.3 60-140 % 06-AUG-20 Surrogate: d10-Phenanthrene 102.0 60-140 % 06-AUG-20
L2481358-2 BH10 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Physical Tests Total Suspended Solids 1730 DLHC 150 mg/L 04-AUG-20 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 05-AUG-20 2700 130000 130000 Benzene 5.65 OWP 0.50 ug/L 05-AUG-20 *0.5 44 430 Bromodichloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 85000 85000 Bromoform <5.0 OWP 5.0 ug/L 05-AUG-20 5 380 770 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-2 BH10 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Volatile Organic Compounds Bromomethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.89 5.6 56 Carbon tetrachloride <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.79 8.4 Chlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 630 630 Dibromochloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 82000 82000 Chloroform <1.0 OWP 1.0 ug/L 05-AUG-20 2 2.4 22 1,2-Dibromoethane <0.46 DLVH 0.46 ug/L 05-AUG-20 **0.2 **0.25 0.83 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4600 9600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 9600 9600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 8 67 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 05-AUG-20 590 4400 4400 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 320 3100 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 12 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 Methylene Chloride <5.0 OWP 5.0 ug/L 05-AUG-20 5 610 5500 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 16 140 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 06-AUG-20 0.5 5.2 45 Ethylbenzene 17.9 OWP 0.50 ug/L 05-AUG-20 *0.5 2300 2300 n-Hexane 3.42 OWP 0.50 ug/L 06-AUG-20 5 51 520 Methyl Ethyl Ketone <20 OWP 20 ug/L 05-AUG-20 400 470000 1500000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 05-AUG-20 640 140000 580000 MTBE <2.0 OWP 2.0 ug/L 05-AUG-20 15 190 1400 Styrene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1300 9100 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 1.1 3.3 28 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 3.2 15 Tetrachloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Toluene 1.26 OWP 0.50 ug/L 05-AUG-20 *0.8 18000 18000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 640 6700 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4.7 30 Trichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 05-AUG-20 150 2500 2500 Vinyl chloride <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 0.5 1.7 o-Xylene 1.41 OWP 0.30 ug/L 05-AUG-20 m+p-Xylenes 6.20 OWP 0.40 ug/L 05-AUG-20 Xylenes (Total) 7.61 0.50 ug/L 06-AUG-20 72 4200 4200 Surrogate: 4-Bromofluorobenzene 95.8 70-130 % 05-AUG-20 Surrogate: 1,4-Difluorobenzene 97.7 70-130 % 05-AUG-20 Hydrocarbons F1 (C6-C10) 209 OWP 25 ug/L 05-AUG-20 420 750 750 F1-BTEX 177 25 ug/L 06-AUG-20 420 750 750 F2 (C10-C16) 100 100 ug/L 31-JUL-20 150 150 150 F2-Naphth 100 100 ug/L 06-AUG-20 F3 (C16-C34) <250 250 ug/L 31-JUL-20 500 500 500 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-2 BH10 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Hydrocarbons F3-PAH <250 250 ug/L 06-AUG-20 F4 (C34-C50) <250 250 ug/L 31-JUL-20 500 500 500 Total Hydrocarbons (C6-C50) <370 370 ug/L 06-AUG-20 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 90.3 60-140 % 31-JUL-20 Surrogate: 3,4-Dichlorotoluene 78.9 60-140 % 05-AUG-20 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.120 0.020 ug/L 06-AUG-20 4.1 600 1700 Acenaphthylene <0.020 0.020 ug/L 06-AUG-20 1 1.8 1.8 Anthracene <0.020 0.020 ug/L 06-AUG-20 0.1 2.4 2.4 Benzo(a)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 4.7 4.7 Benzo(a)pyrene <0.010 0.010 ug/L 06-AUG-20 0.01 0.81 0.81 Benzo(b)fluoranthene <0.020 0.020 ug/L 06-AUG-20 0.1 0.75 0.75 Benzo(g,h,i)perylene <0.020 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 Benzo(k)fluoranthene <0.020 0.020 ug/L 06-AUG-20 0.1 0.4 0.4 Chrysene <0.020 0.020 ug/L 06-AUG-20 0.1 1 1 Dibenzo(ah)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 0.52 0.52 Fluoranthene 0.033 0.020 ug/L 06-AUG-20 0.4 130 130 Fluorene 0.068 0.020 ug/L 06-AUG-20 120 400 400 Indeno(1,2,3-cd)pyrene <0.020 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 1+2-Methylnaphthalenes 1.87 0.028 ug/L 06-AUG-20 2 1800 1800 1-Methylnaphthalene 0.820 0.020 ug/L 06-AUG-20 2 1800 1800 2-Methylnaphthalene 1.05 0.020 ug/L 06-AUG-20 2 1800 1800 Naphthalene 1.91 0.050 ug/L 06-AUG-20 7 1400 6400 Phenanthrene 0.072 0.020 ug/L 06-AUG-20 0.1 580 580 Pyrene 0.035 0.020 ug/L 06-AUG-20 0.2 68 68 Surrogate: d10-Acenaphthene 94.1 60-140 % 06-AUG-20 Surrogate: d12-Chrysene 101.7 60-140 % 06-AUG-20 Surrogate: d8-Naphthalene 91.7 60-140 % 06-AUG-20 Surrogate: d10-Phenanthrene 101.2 60-140 % 06-AUG-20
L2481358-3 BH11 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Physical Tests Total Suspended Solids 11800 DLHC 150 mg/L 04-AUG-20 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 05-AUG-20 2700 130000 130000 Benzene 8.51 OWP 0.50 ug/L 05-AUG-20 *0.5 44 430 Bromodichloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 85000 85000 Bromoform <5.0 OWP 5.0 ug/L 05-AUG-20 5 380 770 Bromomethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.89 5.6 56 Carbon tetrachloride <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.79 8.4 Chlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 630 630 Dibromochloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 82000 82000 Chloroform <1.0 OWP 1.0 ug/L 05-AUG-20 2 2.4 22 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-3 BH11 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Volatile Organic Compounds 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.25 0.83 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4600 9600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 9600 9600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 8 67 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 05-AUG-20 590 4400 4400 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 320 3100 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 12 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 Methylene Chloride <5.0 OWP 5.0 ug/L 05-AUG-20 5 610 5500 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 16 140 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 06-AUG-20 0.5 5.2 45 Ethylbenzene 19.4 OWP 0.50 ug/L 05-AUG-20 *0.5 2300 2300 n-Hexane 2.96 OWP 0.50 ug/L 06-AUG-20 5 51 520 Methyl Ethyl Ketone <20 OWP 20 ug/L 05-AUG-20 400 470000 1500000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 05-AUG-20 640 140000 580000 MTBE <2.0 OWP 2.0 ug/L 05-AUG-20 15 190 1400 Styrene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1300 9100 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 1.1 3.3 28 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 3.2 15 Tetrachloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Toluene <0.50 OWP 0.50 ug/L 05-AUG-20 0.8 18000 18000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 640 6700 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4.7 30 Trichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 05-AUG-20 150 2500 2500 Vinyl chloride <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 0.5 1.7 o-Xylene 0.33 OWP 0.30 ug/L 05-AUG-20 m+p-Xylenes 0.94 OWP 0.40 ug/L 05-AUG-20 Xylenes (Total) 1.27 0.50 ug/L 06-AUG-20 72 4200 4200 Surrogate: 4-Bromofluorobenzene 93.4 70-130 % 05-AUG-20 Surrogate: 1,4-Difluorobenzene 95.7 70-130 % 05-AUG-20 Hydrocarbons F1 (C6-C10) 180 OWP 25 ug/L 05-AUG-20 420 750 750 F1-BTEX 151 25 ug/L 06-AUG-20 420 750 750 F2 (C10-C16) 240 100 ug/L 31-JUL-20 *150 *150 *150 F2-Naphth 240 100 ug/L 06-AUG-20 F3 (C16-C34) <250 250 ug/L 31-JUL-20 500 500 500 F3-PAH <250 250 ug/L 06-AUG-20 F4 (C34-C50) <250 250 ug/L 31-JUL-20 500 500 500 Total Hydrocarbons (C6-C50) 420 370 ug/L 06-AUG-20 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 90.4 60-140 % 31-JUL-20
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-3 BH11 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Hydrocarbons Surrogate: 3,4-Dichlorotoluene 69.4 60-140 % 05-AUG-20 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.304 0.020 ug/L 06-AUG-20 4.1 600 1700 Acenaphthylene 0.062 0.020 ug/L 06-AUG-20 1 1.8 1.8 Anthracene <0.060 DLQ 0.060 ug/L 06-AUG-20 0.1 2.4 2.4 Benzo(a)anthracene 0.075 0.020 ug/L 06-AUG-20 0.2 4.7 4.7 Benzo(a)pyrene 0.055 0.010 ug/L 06-AUG-20 *0.01 0.81 0.81 Benzo(b)fluoranthene 0.075 0.020 ug/L 06-AUG-20 0.1 0.75 0.75 Benzo(g,h,i)perylene 0.031 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 Benzo(k)fluoranthene 0.026 0.020 ug/L 06-AUG-20 0.1 0.4 0.4 Chrysene 0.067 0.020 ug/L 06-AUG-20 0.1 1 1 Dibenzo(ah)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 0.52 0.52 Fluoranthene 0.168 0.020 ug/L 06-AUG-20 0.4 130 130 Fluorene 0.372 0.020 ug/L 06-AUG-20 120 400 400 Indeno(1,2,3-cd)pyrene 0.040 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 1+2-Methylnaphthalenes 4.80 0.028 ug/L 06-AUG-20 *2 1800 1800 1-Methylnaphthalene 3.52 0.020 ug/L 06-AUG-20 *2 1800 1800 2-Methylnaphthalene 1.29 0.020 ug/L 06-AUG-20 2 1800 1800 Naphthalene <2.35 DLQ 2.4 ug/L 06-AUG-20 7 1400 6400 Phenanthrene 0.315 0.020 ug/L 06-AUG-20 *0.1 580 580 Pyrene 0.225 0.020 ug/L 06-AUG-20 *0.2 68 68 Surrogate: d10-Acenaphthene 100.2 60-140 % 06-AUG-20 Surrogate: d12-Chrysene 107.6 60-140 % 06-AUG-20 Surrogate: d8-Naphthalene 92.7 60-140 % 06-AUG-20 Surrogate: d10-Phenanthrene 107.1 60-140 % 06-AUG-20
L2481358-4 BH12 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Physical Tests Total Suspended Solids 4490 DLHC 150 mg/L 04-AUG-20 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 05-AUG-20 2700 130000 130000 Benzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 44 430 Bromodichloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 85000 85000 Bromoform <5.0 OWP 5.0 ug/L 05-AUG-20 5 380 770 Bromomethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.89 5.6 56 Carbon tetrachloride <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.79 8.4 Chlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 630 630 Dibromochloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 82000 82000 Chloroform <1.0 OWP 1.0 ug/L 05-AUG-20 2 2.4 22 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.25 0.83 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4600 9600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 9600 9600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 8 67 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 05-AUG-20 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-4 BH12 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Volatile Organic Compounds 590 4400 4400 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 320 3100 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 12 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 Methylene Chloride <5.0 OWP 5.0 ug/L 05-AUG-20 5 610 5500 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 16 140 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 05-AUG-20 0.5 5.2 45 Ethylbenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 2300 2300 n-Hexane <0.50 OWP 0.50 ug/L 05-AUG-20 5 51 520 Methyl Ethyl Ketone <20 OWP 20 ug/L 05-AUG-20 400 470000 1500000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 05-AUG-20 640 140000 580000 MTBE <2.0 OWP 2.0 ug/L 05-AUG-20 15 190 1400 Styrene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1300 9100 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 1.1 3.3 28 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 3.2 15 Tetrachloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Toluene <0.50 OWP 0.50 ug/L 05-AUG-20 0.8 18000 18000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 640 6700 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4.7 30 Trichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 05-AUG-20 150 2500 2500 Vinyl chloride <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 0.5 1.7 o-Xylene <0.30 OWP 0.30 ug/L 05-AUG-20 m+p-Xylenes <0.40 OWP 0.40 ug/L 05-AUG-20 Xylenes (Total) <0.50 0.50 ug/L 05-AUG-20 72 4200 4200 Surrogate: 4-Bromofluorobenzene 94.2 70-130 % 05-AUG-20 Surrogate: 1,4-Difluorobenzene 100.6 70-130 % 05-AUG-20 Hydrocarbons F1 (C6-C10) <25 OWP 25 ug/L 05-AUG-20 420 750 750 F1-BTEX <25 25 ug/L 06-AUG-20 420 750 750 F2 (C10-C16) <100 100 ug/L 31-JUL-20 150 150 150 F2-Naphth <100 100 ug/L 06-AUG-20 F3 (C16-C34) <250 250 ug/L 31-JUL-20 500 500 500 F3-PAH <250 250 ug/L 06-AUG-20 F4 (C34-C50) <250 250 ug/L 31-JUL-20 500 500 500 Total Hydrocarbons (C6-C50) <370 370 ug/L 06-AUG-20 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 87.7 60-140 % 31-JUL-20 Surrogate: 3,4-Dichlorotoluene 61.3 60-140 % 05-AUG-20 Polycyclic Aromatic Hydrocarbons Acenaphthene <0.020 0.020 ug/L 06-AUG-20 4.1 600 1700 Acenaphthylene <0.020 0.020 ug/L 06-AUG-20 1 1.8 1.8
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-4 BH12 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Polycyclic Aromatic Hydrocarbons Anthracene <0.020 0.020 ug/L 06-AUG-20 0.1 2.4 2.4 Benzo(a)anthracene 0.036 0.020 ug/L 06-AUG-20 0.2 4.7 4.7 Benzo(a)pyrene 0.025 0.010 ug/L 06-AUG-20 *0.01 0.81 0.81 Benzo(b)fluoranthene 0.034 0.020 ug/L 06-AUG-20 0.1 0.75 0.75 Benzo(g,h,i)perylene <0.020 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 Benzo(k)fluoranthene <0.020 0.020 ug/L 06-AUG-20 0.1 0.4 0.4 Chrysene 0.029 0.020 ug/L 06-AUG-20 0.1 1 1 Dibenzo(ah)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 0.52 0.52 Fluoranthene 0.088 0.020 ug/L 06-AUG-20 0.4 130 130 Fluorene <0.020 0.020 ug/L 06-AUG-20 120 400 400 Indeno(1,2,3-cd)pyrene <0.020 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 1+2-Methylnaphthalenes 0.052 0.028 ug/L 06-AUG-20 2 1800 1800 1-Methylnaphthalene 0.025 0.020 ug/L 06-AUG-20 2 1800 1800 2-Methylnaphthalene 0.027 0.020 ug/L 06-AUG-20 2 1800 1800 Naphthalene <0.050 0.050 ug/L 06-AUG-20 7 1400 6400 Phenanthrene 0.089 0.020 ug/L 06-AUG-20 0.1 580 580 Pyrene 0.110 0.020 ug/L 06-AUG-20 0.2 68 68 Surrogate: d10-Acenaphthene 96.6 60-140 % 06-AUG-20 Surrogate: d12-Chrysene 101.1 60-140 % 06-AUG-20 Surrogate: d8-Naphthalene 97.1 60-140 % 06-AUG-20 Surrogate: d10-Phenanthrene 100.0 60-140 % 06-AUG-20
L2481358-5 BH13 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Physical Tests Total Suspended Solids 8010 DLHC 150 mg/L 04-AUG-20 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 05-AUG-20 2700 130000 130000 Benzene 0.70 OWP 0.50 ug/L 05-AUG-20 *0.5 44 430 Bromodichloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 85000 85000 Bromoform <5.0 OWP 5.0 ug/L 05-AUG-20 5 380 770 Bromomethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.89 5.6 56 Carbon tetrachloride <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.79 8.4 Chlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 630 630 Dibromochloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 82000 82000 Chloroform <1.0 OWP 1.0 ug/L 05-AUG-20 2 2.4 22 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.25 0.83 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4600 9600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 9600 9600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 8 67 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 05-AUG-20 590 4400 4400 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 320 3100 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 12 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-5 BH13 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Volatile Organic Compounds trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 Methylene Chloride <5.0 OWP 5.0 ug/L 05-AUG-20 5 610 5500 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 16 140 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 05-AUG-20 0.5 5.2 45 Ethylbenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 2300 2300 n-Hexane <0.50 OWP 0.50 ug/L 05-AUG-20 5 51 520 Methyl Ethyl Ketone <20 OWP 20 ug/L 05-AUG-20 400 470000 1500000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 05-AUG-20 640 140000 580000 MTBE <2.0 OWP 2.0 ug/L 05-AUG-20 15 190 1400 Styrene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1300 9100 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 1.1 3.3 28 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 3.2 15 Tetrachloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Toluene <0.50 OWP 0.50 ug/L 05-AUG-20 0.8 18000 18000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 640 6700 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4.7 30 Trichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 05-AUG-20 150 2500 2500 Vinyl chloride <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 0.5 1.7 o-Xylene <0.30 OWP 0.30 ug/L 05-AUG-20 m+p-Xylenes 0.51 OWP 0.40 ug/L 05-AUG-20 Xylenes (Total) 0.51 0.50 ug/L 05-AUG-20 72 4200 4200 Surrogate: 4-Bromofluorobenzene 93.9 70-130 % 05-AUG-20 Surrogate: 1,4-Difluorobenzene 100.6 70-130 % 05-AUG-20 Hydrocarbons F1 (C6-C10) 26 OWP 25 ug/L 05-AUG-20 420 750 750 F1-BTEX <25 25 ug/L 06-AUG-20 420 750 750 F2 (C10-C16) 230 100 ug/L 31-JUL-20 *150 *150 *150 F2-Naphth 230 100 ug/L 06-AUG-20 F3 (C16-C34) 270 250 ug/L 31-JUL-20 500 500 500 F3-PAH 270 250 ug/L 06-AUG-20 F4 (C34-C50) <250 250 ug/L 31-JUL-20 500 500 500 Total Hydrocarbons (C6-C50) 530 370 ug/L 06-AUG-20 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 91.0 60-140 % 31-JUL-20 Surrogate: 3,4-Dichlorotoluene 71.0 60-140 % 05-AUG-20 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.083 0.020 ug/L 06-AUG-20 4.1 600 1700 Acenaphthylene <0.035 DLQ 0.035 ug/L 06-AUG-20 1 1.8 1.8 Anthracene <0.035 DLQ 0.035 ug/L 06-AUG-20 0.1 2.4 2.4 Benzo(a)anthracene 0.051 0.020 ug/L 06-AUG-20 0.2 4.7 4.7 Benzo(a)pyrene 0.035 0.010 ug/L 06-AUG-20 *0.01 0.81 0.81 Benzo(b)fluoranthene 0.050 0.020 ug/L 06-AUG-20 0.1 0.75 0.75 Benzo(g,h,i)perylene 0.026 0.020 ug/L 06-AUG-20 0.2 0.2 0.2
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-5 BH13 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Polycyclic Aromatic Hydrocarbons Benzo(k)fluoranthene <0.020 0.020 ug/L 06-AUG-20 0.1 0.4 0.4 Chrysene 0.043 0.020 ug/L 06-AUG-20 0.1 1 1 Dibenzo(ah)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 0.52 0.52 Fluoranthene 0.124 0.020 ug/L 06-AUG-20 0.4 130 130 Fluorene <0.042 DLQ 0.042 ug/L 06-AUG-20 120 400 400 Indeno(1,2,3-cd)pyrene 0.032 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 1+2-Methylnaphthalenes 0.096 0.028 ug/L 06-AUG-20 2 1800 1800 1-Methylnaphthalene 0.067 0.020 ug/L 06-AUG-20 2 1800 1800 2-Methylnaphthalene 0.028 0.020 ug/L 06-AUG-20 2 1800 1800 Naphthalene <0.130 DLQ 0.13 ug/L 06-AUG-20 7 1400 6400 Phenanthrene 0.034 0.020 ug/L 06-AUG-20 0.1 580 580 Pyrene 0.133 0.020 ug/L 06-AUG-20 0.2 68 68 Surrogate: d10-Acenaphthene 97.7 60-140 % 06-AUG-20 Surrogate: d12-Chrysene 106.8 60-140 % 06-AUG-20 Surrogate: d8-Naphthalene 91.3 60-140 % 06-AUG-20 Surrogate: d10-Phenanthrene 105.7 60-140 % 06-AUG-20
L2481358-6 BH14 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Physical Tests Total Suspended Solids 11400 DLHC 150 mg/L 04-AUG-20 Volatile Organic Compounds Acetone <30 OWP 30 ug/L 05-AUG-20 2700 130000 130000 Benzene 0.54 OWP 0.50 ug/L 05-AUG-20 *0.5 44 430 Bromodichloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 85000 85000 Bromoform <5.0 OWP 5.0 ug/L 05-AUG-20 5 380 770 Bromomethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.89 5.6 56 Carbon tetrachloride <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.79 8.4 Chlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 630 630 Dibromochloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 82000 82000 Chloroform <1.0 OWP 1.0 ug/L 05-AUG-20 2 2.4 22 1,2-Dibromoethane <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.25 0.83 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4600 9600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 9600 9600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 8 67 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 05-AUG-20 590 4400 4400 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 320 3100 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 12 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 Methylene Chloride <5.0 OWP 5.0 ug/L 05-AUG-20 5 610 5500 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 16 140 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-6 BH14 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Volatile Organic Compounds 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 05-AUG-20 0.5 5.2 45 Ethylbenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 2300 2300 n-Hexane <0.50 OWP 0.50 ug/L 05-AUG-20 5 51 520 Methyl Ethyl Ketone <20 OWP 20 ug/L 05-AUG-20 400 470000 1500000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 05-AUG-20 640 140000 580000 MTBE <2.0 OWP 2.0 ug/L 05-AUG-20 15 190 1400 Styrene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1300 9100 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 1.1 3.3 28 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 3.2 15 Tetrachloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Toluene <0.50 OWP 0.50 ug/L 05-AUG-20 0.8 18000 18000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 640 6700 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4.7 30 Trichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 05-AUG-20 150 2500 2500 Vinyl chloride <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 0.5 1.7 o-Xylene <0.30 OWP 0.30 ug/L 05-AUG-20 m+p-Xylenes 0.46 OWP 0.40 ug/L 05-AUG-20 Xylenes (Total) <0.50 0.50 ug/L 05-AUG-20 72 4200 4200 Surrogate: 4-Bromofluorobenzene 92.8 70-130 % 05-AUG-20 Surrogate: 1,4-Difluorobenzene 100.0 70-130 % 05-AUG-20 Hydrocarbons F1 (C6-C10) 67 OWP 25 ug/L 05-AUG-20 420 750 750 F1-BTEX 66 25 ug/L 06-AUG-20 420 750 750 F2 (C10-C16) 450 100 ug/L 31-JUL-20 *150 *150 *150 F2-Naphth 450 100 ug/L 06-AUG-20 F3 (C16-C34) 320 250 ug/L 31-JUL-20 500 500 500 F3-PAH 320 250 ug/L 06-AUG-20 F4 (C34-C50) <250 250 ug/L 31-JUL-20 500 500 500 Total Hydrocarbons (C6-C50) 830 370 ug/L 06-AUG-20 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 91.4 60-140 % 31-JUL-20 Surrogate: 3,4-Dichlorotoluene 70.3 60-140 % 05-AUG-20 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.331 0.020 ug/L 06-AUG-20 4.1 600 1700 Acenaphthylene <0.075 DLQ 0.075 ug/L 06-AUG-20 1 1.8 1.8 Anthracene <0.110 DLQ 0.11 ug/L 06-AUG-20 **0.1 2.4 2.4 Benzo(a)anthracene 0.074 0.020 ug/L 06-AUG-20 0.2 4.7 4.7 Benzo(a)pyrene 0.051 0.010 ug/L 06-AUG-20 *0.01 0.81 0.81 Benzo(b)fluoranthene 0.064 0.020 ug/L 06-AUG-20 0.1 0.75 0.75 Benzo(g,h,i)perylene 0.033 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 Benzo(k)fluoranthene 0.022 0.020 ug/L 06-AUG-20 0.1 0.4 0.4 Chrysene 0.056 0.020 ug/L 06-AUG-20 0.1 1 1 Dibenzo(ah)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 0.52 0.52 Fluoranthene 0.284 0.020 ug/L 06-AUG-20 0.4 130 130 Fluorene 0.197 0.020 ug/L 06-AUG-20 120 400 400 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-6 BH14 Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Polycyclic Aromatic Hydrocarbons Indeno(1,2,3-cd)pyrene 0.040 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 1+2-Methylnaphthalenes 0.423 0.028 ug/L 06-AUG-20 2 1800 1800 1-Methylnaphthalene 0.361 0.020 ug/L 06-AUG-20 2 1800 1800 2-Methylnaphthalene 0.062 0.020 ug/L 06-AUG-20 2 1800 1800 Naphthalene <0.120 DLQ 0.12 ug/L 06-AUG-20 7 1400 6400 Phenanthrene 0.362 0.020 ug/L 06-AUG-20 *0.1 580 580 Pyrene 0.295 0.020 ug/L 06-AUG-20 *0.2 68 68 Surrogate: d10-Acenaphthene 93.3 60-140 % 06-AUG-20 Surrogate: d12-Chrysene 95.3 60-140 % 06-AUG-20 Surrogate: d8-Naphthalene 86.1 60-140 % 06-AUG-20 Surrogate: d10-Phenanthrene 103.1 60-140 % 06-AUG-20
L2481358-7 DUP Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Volatile Organic Compounds Acetone <30 OWP 30 ug/L 05-AUG-20 2700 130000 130000 Benzene 5.43 OWP 0.50 ug/L 05-AUG-20 *0.5 44 430 Bromodichloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 85000 85000 Bromoform <5.0 OWP 5.0 ug/L 05-AUG-20 5 380 770 Bromomethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.89 5.6 56 Carbon tetrachloride <0.20 OWP 0.20 ug/L 05-AUG-20 0.2 0.79 8.4 Chlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 630 630 Dibromochloromethane <2.0 OWP 2.0 ug/L 05-AUG-20 2 82000 82000 Chloroform <1.0 OWP 1.0 ug/L 05-AUG-20 2 2.4 22 1,2-Dibromoethane <0.40 DLVH 0.40 ug/L 05-AUG-20 **0.2 **0.25 0.83 1,2-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4600 9600 1,3-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 9600 9600 1,4-Dichlorobenzene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 8 67 Dichlorodifluoromethane <2.0 OWP 2.0 ug/L 05-AUG-20 590 4400 4400 1,1-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 320 3100 1,2-Dichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 12 1,1-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 cis-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 trans-1,2-Dichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 1.6 1.6 17 Methylene Chloride <5.0 OWP 5.0 ug/L 05-AUG-20 5 610 5500 1,2-Dichloropropane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 16 140 cis-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 trans-1,3-Dichloropropene <0.30 OWP 0.30 ug/L 05-AUG-20 1,3-Dichloropropene (cis & trans) <0.50 0.50 ug/L 06-AUG-20 0.5 5.2 45 Ethylbenzene 16.8 OWP 0.50 ug/L 05-AUG-20 *0.5 2300 2300 n-Hexane 2.62 OWP 0.50 ug/L 06-AUG-20 5 51 520 Methyl Ethyl Ketone <20 OWP 20 ug/L 05-AUG-20 400 470000 1500000 Methyl Isobutyl Ketone <20 OWP 20 ug/L 05-AUG-20 640 140000 580000 MTBE <2.0 OWP 2.0 ug/L 05-AUG-20 15 190 1400 Styrene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1300 9100 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-7 DUP Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Volatile Organic Compounds 1,1,1,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 1.1 3.3 28 1,1,2,2-Tetrachloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 3.2 15 Tetrachloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Toluene 1.20 OWP 0.50 ug/L 05-AUG-20 *0.8 18000 18000 1,1,1-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 640 6700 1,1,2-Trichloroethane <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 4.7 30 Trichloroethylene <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 1.6 17 Trichlorofluoromethane <5.0 OWP 5.0 ug/L 05-AUG-20 150 2500 2500 Vinyl chloride <0.50 OWP 0.50 ug/L 05-AUG-20 0.5 0.5 1.7 o-Xylene 1.33 OWP 0.30 ug/L 05-AUG-20 m+p-Xylenes 5.79 OWP 0.40 ug/L 05-AUG-20 Xylenes (Total) 7.12 0.50 ug/L 06-AUG-20 72 4200 4200 Surrogate: 4-Bromofluorobenzene 93.4 70-130 % 05-AUG-20 Surrogate: 1,4-Difluorobenzene 98.0 70-130 % 05-AUG-20 Hydrocarbons F1 (C6-C10) 200 OWP 25 ug/L 05-AUG-20 420 750 750 F1-BTEX 169 25 ug/L 06-AUG-20 420 750 750 F2 (C10-C16) 110 100 ug/L 31-JUL-20 150 150 150 F2-Naphth 110 100 ug/L 06-AUG-20 F3 (C16-C34) <250 250 ug/L 31-JUL-20 500 500 500 F3-PAH <250 250 ug/L 06-AUG-20 F4 (C34-C50) <250 250 ug/L 31-JUL-20 500 500 500 Total Hydrocarbons (C6-C50) <370 370 ug/L 06-AUG-20 Chrom. to baseline at nC50 YES No Unit 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 84.9 60-140 % 31-JUL-20 Surrogate: 3,4-Dichlorotoluene 74.2 60-140 % 05-AUG-20 Polycyclic Aromatic Hydrocarbons Acenaphthene 0.121 0.020 ug/L 06-AUG-20 4.1 600 1700 Acenaphthylene <0.020 0.020 ug/L 06-AUG-20 1 1.8 1.8 Anthracene <0.020 0.020 ug/L 06-AUG-20 0.1 2.4 2.4 Benzo(a)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 4.7 4.7 Benzo(a)pyrene <0.010 0.010 ug/L 06-AUG-20 0.01 0.81 0.81 Benzo(b)fluoranthene <0.020 0.020 ug/L 06-AUG-20 0.1 0.75 0.75 Benzo(g,h,i)perylene <0.020 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 Benzo(k)fluoranthene <0.020 0.020 ug/L 06-AUG-20 0.1 0.4 0.4 Chrysene <0.020 0.020 ug/L 06-AUG-20 0.1 1 1 Dibenzo(ah)anthracene <0.020 0.020 ug/L 06-AUG-20 0.2 0.52 0.52 Fluoranthene 0.030 0.020 ug/L 06-AUG-20 0.4 130 130 Fluorene 0.067 0.020 ug/L 06-AUG-20 120 400 400 Indeno(1,2,3-cd)pyrene <0.020 0.020 ug/L 06-AUG-20 0.2 0.2 0.2 1+2-Methylnaphthalenes 1.84 0.028 ug/L 06-AUG-20 2 1800 1800 1-Methylnaphthalene 0.810 0.020 ug/L 06-AUG-20 2 1800 1800 2-Methylnaphthalene 1.03 0.020 ug/L 06-AUG-20 2 1800 1800 Naphthalene <1.90 DLQ 1.9 ug/L 06-AUG-20 7 1400 6400 Phenanthrene 0.069 0.020 ug/L 06-AUG-20 0.1 580 580 Pyrene 0.030 0.020 ug/L 06-AUG-20 0.2 68 68 ** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
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L2481358-7 DUP Sampled By: CLIENT on 28-JUL-20 #1 #2 #3 Matrix: WATER
Polycyclic Aromatic Hydrocarbons Surrogate: d10-Acenaphthene 94.3 60-140 % 06-AUG-20 Surrogate: d12-Chrysene 99.3 60-140 % 06-AUG-20 Surrogate: d8-Naphthalene 91.8 60-140 % 06-AUG-20 Surrogate: d10-Phenanthrene 101.8 60-140 % 06-AUG-20
** Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made. * Analytical result for this parameter exceeds Guideline Limit listed on this report. Guideline Limits applied: Ontario Regulation 153/04 - April 15, 2011 Standards = [Suite] - ON-511-T1/T3-WATER #1: T1-Ground Water-All Types of Property Uses #2: T3-Non-Potable Ground Water-All Types of Property Uses (Coarse)
#3: T3-Non-Potable Ground Water-All Types of Property Uses (Fine) 190441800 L2481358 CONTD.... Page 16 of 17 06-AUG-20 15:19 (MT) Reference Information
Sample Parameter Qualifier key listed: Qualifier Description
DLQ Detection Limit raised due to co-eluting interference. GCMS qualifier ion ratio did not meet acceptance criteria. DLVH Detection Limit raised due to interference from Volatile Hydrocarbons on VOC method. Chromatographic elution of interfering peaks in the same region as test analytes prevents a determination of whether VOC analyte is present or absent (above/below regular detection limits). OWP Organic water sample contained visible sediment (must be included as part of analysis). Measured concentrations of organic substances in water can be biased high due to presence of sediment. DLHC Detection Limit Raised: Dilution required due to high concentration of test analyte(s).
Methods Listed (if applicable): ALS Test Code Matrix Test Description Method Reference***
F1-F4-511-CALC-WT Water F1-F4 Hydrocarbon Calculated CCME CWS-PHC, Pub #1310, Dec 2001-L Parameters
Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.
In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines and the gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes has been subtracted from F1.
In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.
Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range: 1. All extraction and analysis holding times were met. 2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene. 3. Linearity of gasoline response within 15% throughout the calibration range.
Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges: 1. All extraction and analysis holding times were met. 2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average. 3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors. 4. Linearity of diesel or motor oil response within 15% throughout the calibration range. F1-HS-511-WT Water F1-O.Reg 153/04 (July 2011) E3398/CCME TIER 1-HS
Fraction F1 is determined by analyzing by headspace-GC/FID.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). F2-F4-511-WT Water F2-F4-O.Reg 153/04 (July 2011) EPA 3511/CCME Tier 1
Petroleum Hydrocarbons (F2-F4 fractions) are extracted from water using a hexane micro-extraction technique. Instrumental analysis is by GC-FID, as per the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Tier 1 Method, CCME, 2001.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). METHYLNAPS-CALC-WT Water PAH-Calculated Parameters SW846 8270 PAH-511-WT Water PAH-O. Reg 153/04 (July 2011) SW846 3510/8270
Aqueous samples, fortified with surrogates, are extracted using liquid/liquid extraction technique. The sample extracts are concentrated and then analyzed using GC/MS. Results for benzo(b) fluoranthene may include contributions from benzo(j)fluoranthene, if also present in the sample.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). SOLIDS-TSS-WT Water Suspended solids APHA 2540 D-Gravimetric
A well-mixed sample is filtered through a weighed standard glass fibre filter and the residue retained is dried in an oven at 104–1 C for a minimum of four hours or until a constant weight is achieved. VOC-1,3-DCP-CALC-WT Water Regulation 153 VOCs SW8260B/SW8270C VOC-511-HS-WT Water VOC by GCMS HS O.Reg SW846 8260 153/04 (July 2011)
Liquid samples are analyzed by headspace GC/MSD.
Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported). 190441800 L2481358 CONTD.... Page 17 of 17 06-AUG-20 15:19 (MT) Reference Information
XYLENES-SUM-CALC- Water Sum of Xylene Isomer CALCULATION WT Concentrations
Total xylenes represents the sum of o-xylene and m&p-xylene.
*** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Chain of Custody numbers: The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Definition Code Laboratory Location
WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA GLOSSARY OF REPORT TERMS
Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there. mg/kg - milligrams per kilogram based on dry weight of sample mg/kg wwt - milligrams per kilogram based on wet weight of sample mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to, fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information. Guideline limits are not adjusted for the hardness, pH or temperature of the sample (the most conservative values are used). Measurement uncertainty is not applied to test results prior to comparison with specified criteria values. Quality Control Report
Workorder: L2481358 Report Date: 06-AUG-20 Page 1 of 9
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
F1-HS-511-WT Water Batch R5174573 WG3376313-4 DUP WG3376313-3 F1 (C6-C10) <25 <25 RPD-NA ug/L N/A 30 05-AUG-20 WG3376313-1 LCS F1 (C6-C10) 109.5 % 80-120 05-AUG-20 WG3376313-2 MB F1 (C6-C10) <25 ug/L 25 05-AUG-20 Surrogate: 3,4-Dichlorotoluene 85.8 % 60-140 05-AUG-20 WG3376313-5 MS WG3376313-3 F1 (C6-C10) 95.8 % 60-140 05-AUG-20
F2-F4-511-WT Water Batch R5173040 WG3373911-2 LCS F2 (C10-C16) 106.4 % 70-130 31-JUL-20 F3 (C16-C34) 108.5 % 70-130 31-JUL-20 F4 (C34-C50) 118.6 % 70-130 31-JUL-20 WG3373911-1 MB F2 (C10-C16) <100 ug/L 100 31-JUL-20 F3 (C16-C34) <250 ug/L 250 31-JUL-20 F4 (C34-C50) <250 ug/L 250 31-JUL-20 Surrogate: 2-Bromobenzotrifluoride 89.6 % 60-140 31-JUL-20
PAH-511-WT Water Batch R5175580 WG3373911-2 LCS 1-Methylnaphthalene 97.6 % 50-140 06-AUG-20 2-Methylnaphthalene 97.8 % 50-140 06-AUG-20 Acenaphthene 113.7 % 50-140 06-AUG-20 Acenaphthylene 110.2 % 50-140 06-AUG-20 Anthracene 122.6 % 50-140 06-AUG-20 Benzo(a)anthracene 133.3 % 50-140 06-AUG-20 Benzo(a)pyrene 119.3 % 50-140 06-AUG-20 Benzo(b)fluoranthene 120.3 % 50-140 06-AUG-20 Benzo(g,h,i)perylene 111.4 % 50-140 06-AUG-20 Benzo(k)fluoranthene 110.6 % 50-140 06-AUG-20 Chrysene 126.6 % 50-140 06-AUG-20 Dibenzo(ah)anthracene 118.7 % 50-140 06-AUG-20 Fluoranthene 118.5 % 50-140 06-AUG-20 Quality Control Report
Workorder: L2481358 Report Date: 06-AUG-20 Page 2 of 9
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
PAH-511-WT Water Batch R5175580 WG3373911-2 LCS Fluorene 114.2 % 50-140 06-AUG-20 Indeno(1,2,3-cd)pyrene 126.9 % 50-140 06-AUG-20 Naphthalene 102.7 % 50-140 06-AUG-20 Phenanthrene 118.3 % 50-140 06-AUG-20 Pyrene 122.3 % 50-140 06-AUG-20 WG3373911-1 MB 1-Methylnaphthalene <0.020 ug/L 0.02 06-AUG-20 2-Methylnaphthalene <0.020 ug/L 0.02 06-AUG-20 Acenaphthene <0.020 ug/L 0.02 06-AUG-20 Acenaphthylene <0.020 ug/L 0.02 06-AUG-20 Anthracene <0.020 ug/L 0.02 06-AUG-20 Benzo(a)anthracene <0.020 ug/L 0.02 06-AUG-20 Benzo(a)pyrene <0.010 ug/L 0.01 06-AUG-20 Benzo(b)fluoranthene <0.020 ug/L 0.02 06-AUG-20 Benzo(g,h,i)perylene <0.020 ug/L 0.02 06-AUG-20 Benzo(k)fluoranthene <0.020 ug/L 0.02 06-AUG-20 Chrysene <0.020 ug/L 0.02 06-AUG-20 Dibenzo(ah)anthracene <0.020 ug/L 0.02 06-AUG-20 Fluoranthene <0.020 ug/L 0.02 06-AUG-20 Fluorene <0.020 ug/L 0.02 06-AUG-20 Indeno(1,2,3-cd)pyrene <0.020 ug/L 0.02 06-AUG-20 Naphthalene <0.050 ug/L 0.05 06-AUG-20 Phenanthrene <0.020 ug/L 0.02 06-AUG-20 Pyrene <0.020 ug/L 0.02 06-AUG-20 Surrogate: d8-Naphthalene 97.9 % 60-140 06-AUG-20 Surrogate: d10-Phenanthrene 103.5 % 60-140 06-AUG-20 Surrogate: d12-Chrysene 109.3 % 60-140 06-AUG-20 Surrogate: d10-Acenaphthene 99.4 % 60-140 06-AUG-20
SOLIDS-TSS-WT Water Batch R5173740 WG3375091-3 DUP L2481276-1 Total Suspended Solids 5.4 4.8 mg/L 12 20 04-AUG-20 WG3375091-2 LCS Total Suspended Solids 102.7 % 85-115 04-AUG-20 Quality Control Report
Workorder: L2481358 Report Date: 06-AUG-20 Page 3 of 9
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
SOLIDS-TSS-WT Water Batch R5173740 WG3375091-1 MB Total Suspended Solids <3.0 mg/L 3 04-AUG-20
Batch R5173741 WG3375092-3 DUP L2481440-2 Total Suspended Solids 14.6 14.8 mg/L 1.4 20 04-AUG-20 WG3375092-2 LCS Total Suspended Solids 99.3 % 85-115 04-AUG-20 WG3375092-1 MB Total Suspended Solids <3.0 mg/L 3 04-AUG-20
VOC-511-HS-WT Water Batch R5174573 WG3376313-4 DUP WG3376313-3 1,1,1,2-Tetrachloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,1,2,2-Tetrachloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,1,1-Trichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,1,2-Trichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,1-Dichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,1-Dichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,2-Dibromoethane <0.20 <0.20 RPD-NA ug/L N/A 30 05-AUG-20 1,2-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,2-Dichloroethane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,2-Dichloropropane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,3-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 1,4-Dichlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 Acetone <30 <30 RPD-NA ug/L N/A 30 05-AUG-20 Benzene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 Bromodichloromethane <2.0 <2.0 RPD-NA ug/L N/A 30 05-AUG-20 Bromoform <5.0 <5.0 RPD-NA ug/L N/A 30 05-AUG-20 Bromomethane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 Carbon tetrachloride <0.20 <0.20 RPD-NA ug/L N/A 30 05-AUG-20 Chlorobenzene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 Chloroform <1.0 <1.0 RPD-NA ug/L N/A 30 05-AUG-20 cis-1,2-Dichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 cis-1,3-Dichloropropene <0.30 <0.30 RPD-NA ug/L N/A 30 05-AUG-20 Quality Control Report
Workorder: L2481358 Report Date: 06-AUG-20 Page 4 of 9
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R5174573 WG3376313-4 DUP WG3376313-3 Dibromochloromethane <2.0 <2.0 RPD-NA ug/L N/A 30 05-AUG-20 Dichlorodifluoromethane <2.0 <2.0 RPD-NA ug/L N/A 30 05-AUG-20 Ethylbenzene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 n-Hexane <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 m+p-Xylenes <0.40 <0.40 RPD-NA ug/L N/A 30 05-AUG-20 Methyl Ethyl Ketone <20 <20 RPD-NA ug/L N/A 30 05-AUG-20 Methyl Isobutyl Ketone <20 <20 RPD-NA ug/L N/A 30 05-AUG-20 Methylene Chloride <5.0 <5.0 RPD-NA ug/L N/A 30 05-AUG-20 MTBE <2.0 <2.0 RPD-NA ug/L N/A 30 05-AUG-20 o-Xylene <0.30 <0.30 RPD-NA ug/L N/A 30 05-AUG-20 Styrene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 Tetrachloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 Toluene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 trans-1,2-Dichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 trans-1,3-Dichloropropene <0.30 <0.30 RPD-NA ug/L N/A 30 05-AUG-20 Trichloroethylene <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 Trichlorofluoromethane <5.0 <5.0 RPD-NA ug/L N/A 30 05-AUG-20 Vinyl chloride <0.50 <0.50 RPD-NA ug/L N/A 30 05-AUG-20 WG3376313-1 LCS 1,1,1,2-Tetrachloroethane 111.1 % 70-130 05-AUG-20 1,1,2,2-Tetrachloroethane 92.7 % 70-130 05-AUG-20 1,1,1-Trichloroethane 112.4 % 70-130 05-AUG-20 1,1,2-Trichloroethane 104.2 % 70-130 05-AUG-20 1,1-Dichloroethane 108.3 % 70-130 05-AUG-20 1,1-Dichloroethylene 106.4 % 70-130 05-AUG-20 1,2-Dibromoethane 98.2 % 70-130 05-AUG-20 1,2-Dichlorobenzene 107.5 % 70-130 05-AUG-20 1,2-Dichloroethane 95.3 % 70-130 05-AUG-20 1,2-Dichloropropane 101.7 % 70-130 05-AUG-20 1,3-Dichlorobenzene 110.7 % 70-130 05-AUG-20 1,4-Dichlorobenzene 109.8 % 70-130 05-AUG-20 Acetone 96.8 % 60-140 05-AUG-20 Benzene 107.4 % 70-130 05-AUG-20 Quality Control Report
Workorder: L2481358 Report Date: 06-AUG-20 Page 5 of 9
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R5174573 WG3376313-1 LCS Bromodichloromethane 109.0 % 70-130 05-AUG-20 Bromoform 97.2 % 70-130 05-AUG-20 Bromomethane 122.7 % 60-140 05-AUG-20 Carbon tetrachloride 112.6 % 70-130 05-AUG-20 Chlorobenzene 112.6 % 70-130 05-AUG-20 Chloroform 108.3 % 70-130 05-AUG-20 cis-1,2-Dichloroethylene 100.3 % 70-130 05-AUG-20 cis-1,3-Dichloropropene 98.7 % 70-130 05-AUG-20 Dibromochloromethane 98.3 % 70-130 05-AUG-20 Dichlorodifluoromethane 103.1 % 50-140 05-AUG-20 Ethylbenzene 117.6 % 70-130 05-AUG-20 n-Hexane 114.1 % 70-130 05-AUG-20 m+p-Xylenes 115.0 % 70-130 05-AUG-20 Methyl Ethyl Ketone 80.9 % 60-140 05-AUG-20 Methyl Isobutyl Ketone 86.8 % 60-140 05-AUG-20 Methylene Chloride 102.8 % 70-130 05-AUG-20 MTBE 108.5 % 70-130 05-AUG-20 o-Xylene 119.9 % 70-130 05-AUG-20 Styrene 111.1 % 70-130 05-AUG-20 Tetrachloroethylene 118.6 % 70-130 05-AUG-20 Toluene 115.7 % 70-130 05-AUG-20 trans-1,2-Dichloroethylene 109.4 % 70-130 05-AUG-20 trans-1,3-Dichloropropene 111.5 % 70-130 05-AUG-20 Trichloroethylene 111.1 % 70-130 05-AUG-20 Trichlorofluoromethane 102.1 % 60-140 05-AUG-20 Vinyl chloride 112.9 % 60-140 05-AUG-20 WG3376313-2 MB 1,1,1,2-Tetrachloroethane <0.50 ug/L 0.5 05-AUG-20 1,1,2,2-Tetrachloroethane <0.50 ug/L 0.5 05-AUG-20 1,1,1-Trichloroethane <0.50 ug/L 0.5 05-AUG-20 1,1,2-Trichloroethane <0.50 ug/L 0.5 05-AUG-20 1,1-Dichloroethane <0.50 ug/L 0.5 05-AUG-20 1,1-Dichloroethylene <0.50 ug/L 0.5 05-AUG-20 1,2-Dibromoethane <0.20 ug/L 0.2 05-AUG-20 Quality Control Report
Workorder: L2481358 Report Date: 06-AUG-20 Page 6 of 9
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R5174573 WG3376313-2 MB 1,2-Dichlorobenzene <0.50 ug/L 0.5 05-AUG-20 1,2-Dichloroethane <0.50 ug/L 0.5 05-AUG-20 1,2-Dichloropropane <0.50 ug/L 0.5 05-AUG-20 1,3-Dichlorobenzene <0.50 ug/L 0.5 05-AUG-20 1,4-Dichlorobenzene <0.50 ug/L 0.5 05-AUG-20 Acetone <30 ug/L 30 05-AUG-20 Benzene <0.50 ug/L 0.5 05-AUG-20 Bromodichloromethane <2.0 ug/L 2 05-AUG-20 Bromoform <5.0 ug/L 5 05-AUG-20 Bromomethane <0.50 ug/L 0.5 05-AUG-20 Carbon tetrachloride <0.20 ug/L 0.2 05-AUG-20 Chlorobenzene <0.50 ug/L 0.5 05-AUG-20 Chloroform <1.0 ug/L 1 05-AUG-20 cis-1,2-Dichloroethylene <0.50 ug/L 0.5 05-AUG-20 cis-1,3-Dichloropropene <0.30 ug/L 0.3 05-AUG-20 Dibromochloromethane <2.0 ug/L 2 05-AUG-20 Dichlorodifluoromethane <2.0 ug/L 2 05-AUG-20 Ethylbenzene <0.50 ug/L 0.5 05-AUG-20 n-Hexane <0.50 ug/L 0.5 05-AUG-20 m+p-Xylenes <0.40 ug/L 0.4 05-AUG-20 Methyl Ethyl Ketone <20 ug/L 20 05-AUG-20 Methyl Isobutyl Ketone <20 ug/L 20 05-AUG-20 Methylene Chloride <5.0 ug/L 5 05-AUG-20 MTBE <2.0 ug/L 2 05-AUG-20 o-Xylene <0.30 ug/L 0.3 05-AUG-20 Styrene <0.50 ug/L 0.5 05-AUG-20 Tetrachloroethylene <0.50 ug/L 0.5 05-AUG-20 Toluene <0.50 ug/L 0.5 05-AUG-20 trans-1,2-Dichloroethylene <0.50 ug/L 0.5 05-AUG-20 trans-1,3-Dichloropropene <0.30 ug/L 0.3 05-AUG-20 Trichloroethylene <0.50 ug/L 0.5 05-AUG-20 Trichlorofluoromethane <5.0 ug/L 5 05-AUG-20 Vinyl chloride <0.50 ug/L 0.5 05-AUG-20 Quality Control Report
Workorder: L2481358 Report Date: 06-AUG-20 Page 7 of 9
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R5174573 WG3376313-2 MB Surrogate: 1,4-Difluorobenzene 100.5 % 70-130 05-AUG-20 Surrogate: 4-Bromofluorobenzene 92.9 % 70-130 05-AUG-20 WG3376313-5 MS WG3376313-3 1,1,1,2-Tetrachloroethane 112.6 % 50-140 05-AUG-20 1,1,2,2-Tetrachloroethane 113.7 % 50-140 05-AUG-20 1,1,1-Trichloroethane 109.1 % 50-140 05-AUG-20 1,1,2-Trichloroethane 115.5 % 50-140 05-AUG-20 1,1-Dichloroethane 109.6 % 50-140 05-AUG-20 1,1-Dichloroethylene 100.7 % 50-140 05-AUG-20 1,2-Dibromoethane 111.8 % 50-140 05-AUG-20 1,2-Dichlorobenzene 107.6 % 50-140 05-AUG-20 1,2-Dichloroethane 108.7 % 50-140 05-AUG-20 1,2-Dichloropropane 108.0 % 50-140 05-AUG-20 1,3-Dichlorobenzene 103.6 % 50-140 05-AUG-20 1,4-Dichlorobenzene 104.2 % 50-140 05-AUG-20 Acetone 122.0 % 50-140 05-AUG-20 Benzene 108.9 % 50-140 05-AUG-20 Bromodichloromethane 116.7 % 50-140 05-AUG-20 Bromoform 109.9 % 50-140 05-AUG-20 Bromomethane 122.7 % 50-140 05-AUG-20 Carbon tetrachloride 107.8 % 50-140 05-AUG-20 Chlorobenzene 112.1 % 50-140 05-AUG-20 Chloroform 111.6 % 50-140 05-AUG-20 cis-1,2-Dichloroethylene 104.1 % 50-140 05-AUG-20 cis-1,3-Dichloropropene 104.7 % 50-140 05-AUG-20 Dibromochloromethane 106.4 % 50-140 05-AUG-20 Dichlorodifluoromethane 91.7 % 50-140 05-AUG-20 Ethylbenzene 110.4 % 50-140 05-AUG-20 n-Hexane 104.7 % 50-140 05-AUG-20 m+p-Xylenes 107.8 % 50-140 05-AUG-20 Methyl Ethyl Ketone 107.0 % 50-140 05-AUG-20 Methyl Isobutyl Ketone 109.8 % 50-140 05-AUG-20 Methylene Chloride 111.0 % 50-140 05-AUG-20 MTBE 108.2 % 50-140 05-AUG-20 Quality Control Report
Workorder: L2481358 Report Date: 06-AUG-20 Page 8 of 9
Client: Morrison Hershfield Limited (Ottawa) 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Test Matrix Reference Result Qualifier Units RPD Limit Analyzed
VOC-511-HS-WT Water Batch R5174573 WG3376313-5 MS WG3376313-3 o-Xylene 114.9 % 50-140 05-AUG-20 Styrene 109.1 % 50-140 05-AUG-20 Tetrachloroethylene 109.6 % 50-140 05-AUG-20 Toluene 111.2 % 50-140 05-AUG-20 trans-1,2-Dichloroethylene 106.8 % 50-140 05-AUG-20 trans-1,3-Dichloropropene 118.4 % 50-140 05-AUG-20 Trichloroethylene 107.6 % 50-140 05-AUG-20 Trichlorofluoromethane 95.3 % 50-140 05-AUG-20 Vinyl chloride 105.4 % 50-140 05-AUG-20
Batch R5175277 WG3376912-4 DUP WG3376912-3 n-Hexane <0.50 <0.50 RPD-NA ug/L N/A 30 06-AUG-20 WG3376912-1 LCS n-Hexane 102.8 % 70-130 06-AUG-20 WG3376912-2 MB n-Hexane <0.50 ug/L 0.5 06-AUG-20 WG3376912-5 MS WG3376912-3 n-Hexane 98.4 % 50-140 06-AUG-20 Quality Control Report Workorder: L2481358 Report Date: 06-AUG-20
Client: Morrison Hershfield Limited (Ottawa) Page 9 of 9 2440 Don Reid Drive Ottawa ON K1H 1E1 Contact: Mitchell Dawley
Legend: Limit ALS Control Limit (Data Quality Objectives) DUP Duplicate RPD Relative Percent Difference N/A Not Available LCS Laboratory Control Sample SRM Standard Reference Material MS Matrix Spike MSD Matrix Spike Duplicate ADE Average Desorption Efficiency MB Method Blank IRM Internal Reference Material CRM Certified Reference Material CCV Continuing Calibration Verification CVS Calibration Verification Standard LCSD Laboratory Control Sample Duplicate
Sample Parameter Qualifier Definitions: Qualifier Description RPD-NA Relative Percent Difference Not Available due to result(s) being less than detection limit.
Hold Time Exceedances: All test results reported with this submission were conducted within ALS recommended hold times.
ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.
The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre- determined data quality objectives to provide confidence in the accuracy of associated test results.
Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order. ALS Sample ID: L2481358-1 Client Sample ID: BH9 500
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Printed on 7/31/2020 4:13:09 PM ALS Sample ID: L2481358-2 Client Sample ID: BH10 500
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Printed on 7/31/2020 4:13:11 PM ALS Sample ID: L2481358-3 Client Sample ID: BH11 500
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Printed on 7/31/2020 4:13:13 PM ALS Sample ID: L2481358-4 Client Sample ID: BH12 500
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Printed on 7/31/2020 4:13:15 PM ALS Sample ID: L2481358-5 Client Sample ID: BH13 500
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Printed on 7/31/2020 4:13:17 PM ALS Sample ID: L2481358-6 Client Sample ID: BH14 500
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Printed on 7/31/2020 4:13:19 PM ALS Sample ID: L2481358-7 Client Sample ID: DUP 500
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Printed on 7/31/2020 4:13:21 PM